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2012-05-14.12CVCPxxxx.report.Remedial_Investigation_Report_draft.doc

59-63 NORTH 6TH

STREET

BROOKLYN, NEW YORK

Phase II Investigation Report

Block 2325, Lots 27, 28 & 29

OER Project Number 15EHAZ050K

E-Designation Site Number 203

CEQR Number 04DCP003K

Greenpoint-Williamsburg Rezoning

Prepared for:

Rehan Perveez

C/o Victor K. Han, RA, AIA

Victor K. Han, Architects. P.C.

151-19 Bayside Avenue

Flushing, New York 11354

718-746-1022

Prepared by:

GEI Consultants Inc., P.C.

110 Walt Whitman Road

Huntington Station, New York 11746

631-760-9300

October 2014

2

2012-05-15.12CVCPxxxx.report.Remedial_Investigation_Report_draft.doc

PHASE II INVESTIGATION REPORT

TABLE OF CONTENTS

FIGURES ................................................................................................................................. 3

LIST OF ACRONYMS ........................................................................................................... 6

CERTIFICATION ................................................................................................................... 7

EXECUTIVE SUMMARY ..................................................................................................... 7

PHASE II INVESTIGATION REPORT ............................................................................... 11

1.0 BACKGROUND ........................................................................................................ 11

1.1 Site Location and Current Usage ............................................................................ 11

1.2 Proposed Redevelopment Plan ............................................................................... 11

1.3 Description of Surrounding Property ...................................................................... 11

2.0 SITE HISTORY ......................................................................................................... 13

2.1 Past Uses and Ownership ........................................................................................ 13

2.2 Previous Investigations ........................................................................................... 13

2.3 Site Inspection ......................................................................................................... 13

2.4 Areas of Concern .................................................................................................... 13

3.0 PROJECT MANAGEMENT ..................................................................................... 14

3.1 Project Organization ............................................................................................... 14

3.2 Health and Safety .................................................................................................... 14

3.3 Materials Management............................................................................................ 14

4.0 PHASE II INVESTIGATION ACTIVITIES ............................................................. 15

4.1 Geophysical Investigation ....................................................................................... 15

4.2 Borings and Monitoring Wells................................................................................ 15

4.4 Sample Collection and Chemical Analysis ............................................................. 18

5.0 ENVIRONMENTAL EVALUATION....................................................................... 20

5.1 Geological and Hydrogeological Conditions .......................................................... 20

5.2 Soil Chemistry ........................................................................................................ 20

5.3 Groundwater Chemistry .......................................................................................... 21

5.4 Soil Vapor Chemistry ............................................................................................. 21

FIGURES

List of Figures

1 Sample Location Map

2 Surrounding Land Usage

3 Distribution of Soil Exceedances

4 Distribution of Groundwater Exceedances

TABLES

List of Tables

1 Soil Analytical Data

2 Groundwater Analytical Data

3 Soil Vapor Analytical Data

4 Soil Vapor Results Compared to NYSDOH Guidance Values

APPENDICES

List of Typical Appendices

A Phase 1 ESA Report

B Boring Logs

C Laboratory Data Deliverables for Soil and Groundwater Analytical Data

D Laboratory Data Deliverables for Soil Vapor Analytical Data

LIST OF ACRONYMS

Acronym Definition

AOC Area of Concern

CAMP Community Air Monitoring Plan

COC Contaminant of Concern

CPP Citizen Participation Plan

CSM Conceptual Site Model

DER-10 New York State Department of Environmental Conservation

Technical Guide 10

FID Flame Ionization Detector

GPS Global Positioning System

HASP Health and Safety Plan

HAZWOPER Hazardous Waste Operations and Emergency Response

IRM Interim Remedial Measure

NAPL Non-aqueous Phase Liquid

NYC VCP New York City Voluntary Cleanup Program

NYC DOHMH New York City Department of Health and Mental Hygiene

NYC OER New York City Office of Environmental Remediation

NYS DOH

ELAP

New York State Department of Health Environmental

Laboratory Accreditation Program

OSHA Occupational Safety and Health Administration

PID Photoionization Detector

QEP Qualified Environmental Professional

RI Remedial Investigation

RIR Remedial Investigation Report

SCO Soil Cleanup Objective

SPEED Searchable Property Environmental Electronic Database

EXECUTIVE SUMMARY

This Phase II Investigation Report was conducted to address recognized environmental

concerns (RECs) identified in the Site’s Phase I Environmental Site Assessment (ESA) Report

for the Site, dated July 2014.

Site Location and Current Usage

The Site is located in the Williamsburg section of Brooklyn, New York and is

identified as Block 2325, Lots 27, 28, & 29. Currently, the Site is a vacant parking lot,

containing a one-story cargo container in the southeastern portion of the Site. The

property is zoned as M1-2/R6A: Manufacturing/Residential District. The occupancy

code with the Department of Finance for the subject property is listed as vacant land.

The Little “E” restriction for the subject property is listed as “Hazmat”, and, according to

CEQR Table 11-3, based on 55-gallon drums identified at the adjacent E Designation Site

202, Lot 25.

Summary of Proposed Redevelopment Plan

The planned development of the Site will involve the excavation of the Site to a depth of

approximately ten feet. As part of development, the referenced lots are expected to be merged

into lot numbers 27 and 28. The water table is approximately 25 feet below ground surface

(bgs).

Summary of Past Uses of Site and Areas of Concern

Historical site usage was residential through 1951. Sometime between 1951 and 1965 the

subject property became vacant land and the site usage was changed to a parking lot.

A review of Sanborn atlases for the project site, conducted by American Environmental

Assessment & Solutions, Inc. in their Phase I ESA report, dated July 15th

, 2014, revealed the

following for available atlases:

1987 – three 3-story buildings, usage listed residential

1905 through 1951 – one additional 1-story building in the northwest; and two additional 1-

story buildings in the east

1965 through 2007 – parking lots occupy the entire project site

City Directory Abstract files, from the Phase I ESA, indicate that the current owner, Mr.

Rehan Perveez, has owned the property since at least 1997, with private individual owners prior

to that period.

The on-site and primary off-site RECs are:

• The Little "E” designation for the Hazmat classification of the subject property

• The historical usage of the subject property as a parking lot

• The historical usage of the property to the south for paint manufacturing and

chemical storage

• The historical usage of the western adjacent property for chemical storage

• The presence of historic fill at the site

Summary of the Work Performed under the Phase II Investigation

GEI performed the following scope of work, the scope of which was approved by the

Mayor’s Office of Environmental Remediation (MOER):

1. a geophysical survey; a ground penetrating radar (GPR) and electromagnetic (EM)

survey was conducted to investigate the presence of any potential underground

storage tanks (USTs) on the Site. The survey was conducted on August 8, 2014 by

Delta Geophysics, Inc. of Catasauqua, Pennsylvania, with the oversight of GEI. No

USTs were identified during the Phase I ESA report or in this survey.

2. six soil borings across the entire project Site, and the collection of 12 soil samples for

chemical analysis (one near the surface and one near the planned excavation depth)

3. three groundwater monitoring wells throughout the Site and the collection of

groundwater samples for chemical analysis

4. four soil vapor probes around the Site perimeter and the collection of four samples for

chemical analysis

Summary of Environmental Findings

1. Elevation of the property ranges from approximately 21 to 25 feet mean sea level.

2. Depth to groundwater ranges from approximately 21 to 24feet at the Site.

3. Groundwater flow is generally towards the east/northeast the Site.

4. Depth to bedrock is greater than 25 feet at the Site.

5. The stratigraphy of the site was determined from the findings of the six Geoprobe holes

conducted throughout the site. Fill was encountered in all test holes and was

characterized as fine to medium sand with fragments of bricks. The thickness of the fill

was approximately 2 feet in all test holes, except in B-1, located along the eastern portion

of the site, where 7 feet of fill was encountered. Underlain the fill unit was natural fine to

medium, to fine sand layers to at least 25 feet below ground surface, the maximum depth

of the borings.

6. The soil sampling results were compared to the New York State Department of

Environmental Conservation (NYSDEC) 6 NYCRR Part 375 Table 6.8 Soil Cleanup

Objectives (SCOs) for Unrestricted Use and Restricted Residential Use SCOs. Soil

sampling results indicated two VOCs, acetone (max 100 ug/kg) and methylene chloride

(53 ug/kg) exceeded Unrestricted Use SCOs. Several semi-volatile organic compounds

(SVOCs) including benz(a)anthracene (max 28,000 ug/kg), benzo(a)pyrene (max 20,000

ug/kg), benzo(b)fluoranthene (max 28,000 ug/kg), benzo(k)fluoranthene (max 8,500

ug/kg), chrysene (max 24,000 ug/kg), and indeno(1,2,3-cd)pyrene (max 8,400 ug/kg)

exceeded Restricted Residential Use SCOs in shallow soils. All SVOCs were below

Unrestricted Use SCOS in deeper soils. One polychlorinated biphenyls (PCB) was

detected above Unrestricted Use SCOs: PCB-1260 (270 ug/kg). Two pesticides were

detected above Unrestricted Use SCOs, 4,4’-DDE (25 ug/kg) and 4,4’-DDT (40 ug/kg),

but were well below Restricted Use SCOs. Several metals including arsenic (max 15.5

mg/kg), barium (max 480 mg/kg), cadmium (max 4.47 mg/kg), chromium (max 58.5

mg/kg), copper (max 135 mg/kg), lead (max 1,230 mg/kg), mercury (max 0.82 mg/kg),

nickel (max 37.8 mg/kg), and zinc (max 652 mg/kg) exceeded Unrestricted Use SCOs in

shallow soils. Of these, barium, cadmium, lead and mercury also exceeded Restricted

residential Use SCOs. Only chromium at 36.4 mg/kg exceeded Unrestricted Use SCOs in

one deeper soil sample. Overall, soil chemistry is unremarkable and does not indicate

any disposal.

7. Groundwater samples collected during the investigation were compared to NYSDEC

Technical & Operational Guidance Series (TOGS) Ambient Water Quality Standards

(GQS). Two VOCs, naphthalene (max 8.7 ug/L) and trichloroethene (max 4.3 ug/L),

were detected at trace concentrations below their respective GQS. Several SVOCs were

detected in all of the groundwater samples exceeding GQS. These included

benzo(a)anthracene (max 3.1 ug/L), benzo(a)pyrene (max 2.2 ug/L), (b)fluoranthene

(max 3 ug/L), benzo(k)fluoranthene (max 1 ug/L), chrysene (max 3 ug/L), and

indeno(1,2,3-cd)pyrene (max 1 ug/L). One PCB was above its detection limit, but below

its respective GQS. Pesticides were not detected above their detection limit. Several

metals were identified but only aluminum (max 0.31 ug/L), manganese (max 3.98 ug/L),

and sodium (max 57.2 ug/L) were detected above their respective GQS.

8. A summary of the soil vapor sample results is provided in Table 3. Most compounds

were detected at less than 20 μg/m3 except for acetone (max. of 750 μg/m3). Petroleum

related VOCs (BTEX) ranged from 105 μg/m3 to 260 μg/m3. Chlorinated VOCs,

trichloroethane was detected in three of four samples at a maximum concentration of 4

μg/m³. Tetrachloroethylene (max. 502 μg/m³) was detected in four of eight samples and

ranged from 0.6 μg/m³) to 502 μg/m³. TCA was detected at 21 μg/m3 and carbon

tetrachloride was not detected. The only established regulatory criteria for soil vapor are

provided in the New York State Department of Health (NYSDOH) Guidance. The

criteria as listed in the Volatile Chemical Matrix Tables, compare sub-slab vapor

concentrations to indoor air concentrations for, 1,1,1-trichloroethane, carbon

tetrachloride, tetrachloroethylene (PCE), and trichloroethylene (TCE). Since indoor air

concentrations were not sampled as part of this investigation, the criteria do not strictly

apply; however, a comparison between the minimum sub-slab concentrations in the

matrices to the soil vapor samples collected during this investigation can be performed

and the results used as a means to determine if additional investigation or mitigation

measures could be warranted.

Sample ID NYSDOH Action Level

SV-1 SV-2 SV-3 SV-4 Sampling Date 8/11/2014 8/11/2014 8/11/2014 8/11/2014 Units ug/m³ ug/m³ ug/m³ ug/m³ ug/m³ 1,1,1-Trichloroethane 100 2.10 3.05 2.89 8.67 Carbon tetrachloride 250 0.377 0.251 0.692 0.566 Tetrachloroethylene (PCE) 100 502 6.64 3.66 0.610

Trichloroethylene (TCE) 250 4.03 0.967 2.42 ND NOTES: ug/m3=micrograms per cubic meter ND: Not detected

Concentrations of PCE are elevated and require monitoring per the matrix established by

NYSDOH.

PHASE II INVESTIGATION REPORT

1.0 BACKGROUND

The property is a part of E-Designation 138 – Greenpoint-Williamsburg Rezoning. The

scope of the Phase II Investigation was conducted consistent with GEI Consultants, Inc., P. C.’s

(GEI) Work Plan , which was approved by the New York City Mayor’s Office of Environmental

Remediation (MOER) on August 8, 2014.

1.1 Site Location and Current Usage

The Site is located in the Williamsburg section of Brooklyn, New York and is

identified as Block 2325, Lots 27, 28, & 29. Currently, the Site is a vacant parking lot,

containing a one-story cargo-container in the southeastern portion of the property. The

property is zoned as M1-2/R6A: Manufacturing/Residential District. The occupancy

code with the Department of Finance for the subject property is listed as vacant land.

The Little “E” restriction for the subject property is listed as “Hazmat” and, according to

CEQR Table 11-3, is based on 55-gallon drums identified at the adjacent E Designation

Site 202, Lot 25.

1.2 Proposed Redevelopment Plan

The development of the project site will involve the excavation of the site to a depth of

approximately ten feet. As part of development, the above-referenced lots are expected to be

merged into tentative lot numbers 27 and 28. The water table is approximately 25 feet below

ground surface (bgs). The property shall be developed with a one story and cellar general

commercial building. The building shall be one story in height and shall be 23 feet tall. The

cellar shall be used for general mechanical space, meter rooms and storage for first floor tenants.

The first floor is expected to be used by general mercantile. No food services or restaurant uses

are proposed for the subject building. The first floor shall be serviced by a rooftop HVAC system

supplying both heat and air conditioning as well as ventilation. Storage space in the cellar shall

be provided with exhaust fans and make-up air fans located on the roof as well.

1.3 Description of Surrounding Property

The current and past usage of the adjoining properties consisted of commercial, industrial,

and residential buildings (see existing Phase I ESA in Appendix A). Details of the current

adjacent site uses are provided below.

North – a 1- and a 2-story residential building

South (across North 6th

Street) – a 1-story commercial building and restaurant

East – a 6-story residential building

West – a 2-story mixed use building

Figure 1 depicts the nature of the surrounding land usage. Figure 2 depicts the surrounding land

usage of the project site, obtained through the NYC Planning ZOLA website.

2.0 SITE HISTORY

2.1 Past Uses and Ownership

Historical usage of the subject property depicts the Site as residential through 1951.

Sometime between 1951 and 1965 the subject property became vacant land and the site usage

was changed to a parking lot. The usage of the Site as a parking lot was listed on historical maps

through 2007.

City Directory Abstract files, from the Phase I ESA, indicated that the current owner,

Mr. Rehan Perveez, has owned the property since at least 1997, with private individual owners

prior to that period.

2.2 Previous Investigations

A recent Phase I ESA was conducted by American Environmental Assessment & Solutions,

Inc., dated July 15, 2014. The report is provided as Appendix A.

2.3 Site Inspection

During the Phase II Investigation, conducted on August 8 and 11, 2014, the Site was

primarily an unpaved lot. A storage container, filled primarily with clothing manufacturing

equipment, was located in the southeast corner to the property. Miscellaneous materials, metal

frames, barbeques, among others, were present in the northeast corner of the Site.

2.4 Areas of Concern

The on-site and primary off-site RECs are:

• The Little "E” designation for the Hazmat of the subject property

• The historical usage of the subject property as a parking lot

• The historical usage of the property to the south for paint manufacturing and

chemical storage

• The historical usage of the western adjacent property for chemical storage

The Phase 1 ESA Report is presented in Appendix A. A site map is presented in Figure 1.

3.0 PROJECT MANAGEMENT

3.1 Project Organization

The Qualified Environmental Profession (QEP) responsible for preparation of this Phase II

Investigation is GEI Project Manager Albert Jaroszewski.

3.2 Health and Safety

All work described in this Phase II Investigation was performed in full compliance with

applicable laws and regulations, including Site and Occupational Safety and Health

Administration (OSHA) worker safety requirements and Hazardous Waste Operations and

Emergency Response (HAZWOPER) requirements.

3.3 Materials Management

All material encountered during the investigation was managed in accordance with

applicable laws and regulations.

4.0 PHASE II INVESTIGATION ACTIVITIES

GEI performed the following scope of work, the scope of which was approved by MOER:

1. A geophysical survey

2. Six soil borings across the entire project Site, and collection of 12 soil samples for

chemical analysis

3. Three groundwater monitoring wells installed across the Site, and the collection of

three groundwater samples for chemical analysis

4. Four soil vapor probes around the Site perimeter, and the collection of four soil vapor

samples

4.1 Geophysical Investigation

A ground penetrating radar (GPR) and electromagnetic (EM) survey was

conducted to investigate the presence of any potential underground storage tanks (USTs)

on the Site. The survey was conducted on August 8, 2014 by Delta Geophysics, Inc. of

Catasauqua, Pennsylvania, with the oversight of GEI. No USTs were identified during

the Phase I ESA report or in this survey.

4.2 Borings and Monitoring Wells

Drilling and Soil Logging

Twelve soil samples were collected for chemical analysis during this Phase II

Investigation. Figure 1 shows the location of the samples collected during this investigation.

Laboratories and analytical methods are shown below.

Six soil borings (designated B-1 through B-6) were completed during this investigation as

outlined in the approved work plan. Two soil samples from each boring were collected; a

shallow sample (0’-2’), and a deeper sample (10’-12’). The deeper samples were collected from

the approximate 2-foot interval near the proposed maximum excavation development depth.

The soil was characterized and logged for potential impacts (e.g., odor, staining,

anthropogenic materials) and screened for volatile organic vapors in 6-inch intervals with a

photoionization detector (PID). Boring logs are provided in Appendix B. All soil samples were

analyzed by Phoenix Environmental Laboratories, Inc., of Manchester, Connecticut for the

following parameters:

• VOCs by United Stated Environmental Protection Agency (USEPA)

Method 8260

• SVOCs by USEPA Method 8270 B/N

• Pesticides/PCBs using USEPA Method 8081/8082

• Target Analyte List (TAL) Metals

All soil samples were collected in laboratory supplied jars, properly labeled with the boring

number and the depth of the sample interval, the date and time of sampling, the analytical

requirements, and then placed on ice for the duration of the sampling and transport to the

laboratory. A chain of custody form was completed at the time of sampling and maintained until

disposition of the samples at the laboratory.

Groundwater Monitoring Well Construction

Three groundwater samples were collected for chemical analysis from monitoring wells

designated MW-1, MW-2, and MW-3. Figure 1 shows the location of the groundwater

monitoring wells.

Representative groundwater samples were collected consistent with USEPA's Low

Stress/Flow Groundwater Sampling Protocol (Standard Operating Procedure [SOP] # GW0001,

rev. Jan 2010), using a peristaltic pump and dedicated tubing.

Temporary groundwater monitoring wells were installed to intersect the groundwater

interface using a Geoprobe direct-push drilling rig. One groundwater sample (filtered and

unfiltered for metals, and unfiltered for all other listed parameters) was collected from each

monitoring well and submitted for laboratory analysis. The groundwater samples were tested for

the following chemical parameters:

• VOCs by USEPA Method 8260

• SVOCs by USEPA Method 8270 B/N/A

• Pesticides/PCBs using USEPA Method 8081/8082

• TAL Metals (filtered and unfiltered)

All groundwater samples were collected in laboratory supplied jars, properly labeled with

the well ID, the date and time of sampling, the analytical requirements, and then placed on ice

for the duration of the sampling and transport to the laboratory. A chain of custody form was

completed at the time of sampling and maintained until disposition of the samples at the

laboratory.

Survey

Each sample point location at the Site was accurately measured to permanent features on

and adjacent to the Site

Water Level Measurement

Per the approved Work Plan and subsequent clarifications, temporary wells were installed

as part of the investigation. Groundwater was encountered in the wells between approximately

21’ and 24’ below the existing grade.

4.3 Sample Collection and Chemical Analysis

Samples were collected in accordance with the Final Guidance for Evaluating Soil Vapor

Intrusion in the State of New York (NYSDOH October 2006).

To collect the soil vapor samples, implants were set at a depth of approximately ten feet.

The soil vapor probe was installed between one or two feet above the groundwater interface.

The vapor implants were installed using 1-inch diameter steel drill rods advanced using direct

push drilling methods. The soil vapor probes consisted of a prefabricated 2-3 inch perforated

steel vapor probe tip attached to 3/8-inch diameter low density polyethylene (LDPE) plastic riser

tubing. Once driven to depth, the rods were removed leaving only the tip and the tubing. The

vapor probe borehole was backfilled to grade gravel. A surface seal was placed using an

impermeable clay seal installed within the last 6-inches of the probe-hole annulus from surface

grade level. The vapor well was purged using a hand pump or equivalent device after

installation. Sampling occurred for the duration of 2 hours.

Four samples were collected in appropriate sized Summa canisters that have been

certified clean by the laboratory and samples were analyzed by using USEPA Method TO-15.

Flow rate for both purging and sampling did not exceed 0.2 L/min. Approximately 60 hours

following soil vapor probe installation, one to three implant volumes were purged prior to the

collection of the soil-vapor samples. A sample log sheet was maintained summarizing sample

identification, date and time of sample collection, sampling depth, identity of samplers, sampling

methods and devices, soil vapor purge volumes, volume of the soil vapor extracted, vacuum of

canisters before and after the samples are collected, apparent moisture content of the sampling

zone, and chain of custody protocols.

As part of the vapor intrusion evaluation, a tracer gas was used in accordance with

NYSDOH protocols to serve as a quality control/quality assurance (QA/QC) device to verify the

integrity of the soil vapor probe seal. A container (box, plastic pail, etc.) served to keep the

tracer gas in contact with the probe during testing. A portable monitoring device was used to

analyze a sample of soil vapor for the tracer gas prior to sampling. The tracer sample results did

not show any significant presence of the tracer. At the conclusion of the sampling round, tracer

monitoring was performed a second time to confirm the integrity of the probe seals.

4.4 Sample Collection and Chemical Analysis

All of the sampling performed as part of the field investigation was conducted for all RECs

consistent with MOER project requirements. This included the sampling locations, sample

analytes, and sampling methodologies noted above.

Chemical Analysis

Chemical analytical work presented in this Phase II Investigation has been performed in the

following manner:

Factor Description

Quality Assurance Officer The chemical analytical quality assurance program was directed by

Erik Curran

Chemical Analytical

Laboratory

Chemical analytical laboratory used in the Phase II is New York

State Environmental Laboratory Approval Program (ELAP)

certified and was Phoenix Environmental Laboratories, Inc., of

Manchester, CT

Chemical Analytical

Methods

Soil analytical methods:

TAL Metals by EPA Method 6010C and 7471C (rev. 2007);

VOCs by EPA Method 8260C (rev. 2006);

SVOCs by EPA Method 8270D (rev. 2007);

Pesticides by EPA Method 8081B (rev. 2000);

PCBs by EPA Method 8082A (rev. 2000);

Groundwater analytical methods:

TAL Metals by EPA Method 6010C and 7471 (rev. 2007);

VOCs by EPA Method 8260C (rev. 2006);

SVOCs by EPA Method 8270D (rev. 2007);

Pesticides by EPA Method 8081B (rev. 2000);

PCBs by EPA Method 8082A (rev. 2000);

Soil vapor analytical methods:

VOCs by TO-15

Results of Chemical Analyses

Laboratory data for soil and groundwater are summarized in Tables 1 and 2. Laboratory data

deliverables for all samples evaluated in this Phase II Investigation are provided in Appendices

C and D.

5.0 ENVIRONMENTAL EVALUATION

5.1 Geological and Hydrogeological Conditions

Stratigraphy

The stratigraphy of the site, from the surface, consists of generally approximately two feet,

and up to seven feet, of fill underlain by natural fine to medium, to fine sand layers to at least 25

feet below ground surface. Bedrock was not encountered and is greater than 25 feet below

ground surface. Boring logs are provided in Appendix B.

Hydrogeology

The depth to groundwater at the Site was encountered between approximately 21 and 25 feet

below ground surface. The groundwater flow is to the east/northeast towards the East River.

5.2 Soil Chemistry

The twelve soil samples collected as part of this investigation were compared to 6 NYCRR

Subpart 375-6.8; (a): Unrestricted Use SCOs. Detections identified above the SCOs are

identified in Table 1. The table also includes Restricted Use SCOs for reference.

Based on observations noted in the field (visual, olfactory, and PID readings) no impacts

were identified to the soil encountered (see boring logs in Appendix B).

VOC exceedances of the SCOs were limited to acetone and methylene chloride in most of

the soil/fill samples. These compounds are typical laboratory remnants. The exceedances were

marginal, generally within an order of magnitude of the Unrestricted Use SCO, and all were well

below the Restricted Use SCOs.

SVOC exceedances of the SCOs included compounds which were only identified in two

shallow fill samples (B-3, 0-2’ and B-4, 0-2’) (see Table 1). Up to six compounds exceeded the

SCOs in the samples, with concentrations ranging from one to two orders-of-magnitude above

their Unrestricted SCOs.

TAL metals exceedances of SCOs were identified in five of the six borings conducted. The

exceedances were limited to the shallow 0-2’ fill samples in all but one boring (B-4 0-10’) where

chromium was detected at 36.4 mg/Kg, marginally above its Unrestricted SCO of 30 mg/Kg.

The exceedances in the shallow fill samples were associated with arsenic, barium, cadmium,

chromium, copper, lead, mercury, nickel and zinc, and were relatively low, generally within the

same order-of-magnitude of their respective SCOs.

One PCB (1260) was detected in one boring (B-4) in the shallow (0-2’) fill sample

marginally above its Unrestricted SCO of 100 ug/Kg, but below the Restricted SCO of 1,000

ug/Kg.

Up to two PCBs (4,4’-DDE and 4,4,-DDT) were detected in two borings (B-4 and B-6)

between 14 ug/Kg and 40 ug/Kg above their Unrestricted SCO of 100 ug/Kg, but below the

Restricted SCO of 1,000 ug/Kg. The detections were in the near-surface shallow fill samples.

5.3 Groundwater Chemistry

The three groundwater samples were compared to the New York State Department of

Environmental Conservation (NYSDEC) Division of Water Technical and Operation Guidance

Series (TOGS) 1.1.1 Ambient Water Quality Standards (AWQS) (Table 2). No VOCs, PCBs, or

pesticide was detected above their respective standards in the samples.

Metals exceedances of standards were detected for most of the metals analyzed in all three

groundwater samples (Table 2). Most of these exceedances occurred for the unfiltered samples.

The dissolved metals concentrations were generally several orders-of-magnitude lower than the

unfiltered total concentrations. The only dissolved metals concentrations above standards were

for aluminum, manganese and sodium. The concentrations were generally within the same

order-of-magnitude of their standards.

Up to five SVOCs were detected in all of the groundwater samples. These included

benzo(a)anthracene, benzo(b)fluoranthene, benzo(k)fluoranthene, chrysene, and indeno(1,2,3-

cd)pyrene. The concentrations ranged from 0.02 ug/L to 3/1 ug/L.

5.4 Soil Vapor Chemistry

Laboratory analytical results for the soil vapor samples are provided in Appendix D and

summarized in Table 3. All samples were analyzed for VOCs using EPA Method TO-15.

Helium levels were measured prior to and following sample collection to verify the integrity of

the soil vapor probe seal. No helium was detected in the pre-sample or post-sample

measurements.

Most compounds were detected at less than 20 μg/m3 except for acetone (max. of 750

μg/m3). Petroleum related VOCs (BTEX) ranged from 105 μg/m3 to 260 μg/m3. Chlorinated

VOCs, trichloroethane was detected in three of four samples at a maximum concentration of 4

μg/m³. Tetrachloroethylene (max. 502 μg/m³) was detected in four of eight samples and ranged

from 0.6 μg/m³) to 502 μg/m³. TCA was detected at 21 μg/m3 and carbon tetrachloride was not

detected.

The only established regulatory criteria for soil vapor are provided in the New York State

Department of Health (NYSDOH) Guidance. The criteria as listed in the Volatile Chemical

Matrix Tables, compare sub-slab vapor concentrations to indoor air concentrations for, 1,1,1-

trichloroethane, carbon tetrachloride, tetrachloroethylene (PCE), and trichloroethylene (TCE).

Since indoor air concentrations were not sampled as part of this investigation, the criteria do not

strictly apply; however, a comparison between the minimum sub-slab concentrations in the

matrices to the soil vapor samples collected during this investigation can be performed and the

results used as a means to determine if additional investigation or mitigation measures could be

warranted.

Sample ID NYSDOH Action Level

SV-1 SV-2 SV-3 SV-4 Sampling Date 8/11/2014 8/11/2014 8/11/2014 8/11/2014 Units ug/m³ ug/m³ ug/m³ ug/m³ ug/m³ 1,1,1-Trichloroethane 100 2.10 3.05 2.89 8.67 Carbon tetrachloride 250 0.377 0.251 0.692 0.566 Tetrachloroethylene (PCE) 100 502 6.64 3.66 0.610


Figure _____________________________________________

Tables ____________________________________________

GEI Consultants, Inc., P. C.Page 1 of 10

Project 1408950

August 2014I:\Tech\Environmental Projects\Rehan Perveez\Phase II Report\Lab Results\

Table 1 SoilsTable 1 Soils

Table 1. Soil Sample Analytical ResultsPhase II Investigation59-63 North 6th StreetBrooklyn, New York

Sample ID NY-Res. NY-UnRestricted B-1 (0-2 FT) B-1 (10-12 FT) B-2 (0-2 FT) B-2 (10-12 FT) B-3 (0-2 FT) B-3 (10-12 FT)Sampling Date 8/8/2014 8/8/2014 8/8/2014 8/8/2014 8/8/2014 8/8/2014

CompoundMiscellaneous/Inorganics mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/KgPercent Solid 86 90 77 88 85 88Total Cyanide 27 27 < 0.58 < 0.56 < 0.65 < 0.57 < 0.59 < 0.57Metals, Total mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/KgAluminum 14,600 8,610 15,400 7,910 8,150 7,140Antimony < 3.5 < 3.5 < 4.2 < 4.1 < 4.0 < 3.4Arsenic 16 13 3.2 < 0.7 3.5 2.4 3.2 < 0.7Barium 350 350 73.2 49.7 49.1 20.7 137 40.9Beryllium 14 7.2 0.58 0.49 0.37 0.51 0.44 0.46Cadmium 2.5 2.5 < 0.35 < 0.35 < 0.42 < 0.41 0.62 < 0.34Calcium 1,540 733 1,160 773 2,750 768Chromium 30 17.6 22.8 20.8 15 20.9 19.3Cobalt 7.34 9.27 6.56 6.13 8.26 8.98Copper 270 50 13.5 16.8 21.3 12.8 27.7 15.5Iron 18,400 30,600 17,500 15,900 23,100 25,700Lead 400 63 109 7.89 20.7 5.13 206 6.29Magnesium 2,340 1,990 2,980 1,990 1,870 1,670Manganese 2,000 1,600 794 525 172 206 544 417Mercury 0.81 0.18 0.25 < 0.06 < 0.09 < 0.07 < 0.07 < 0.07Nickel 140 30 12.4 12.9 13.4 10.8 14.2 11.4Potassium 798 1,680 1,170 1,100 1,260 1,410Selenium 36 3.9 < 1.4 < 1.4 < 1.7 < 1.6 < 1.6 < 1.4Silver 36 2 < 0.35 < 0.35 < 0.42 < 0.41 < 0.40 < 0.34Sodium 68.8 49 44 37.9 67.6 47.6Thallium < 3.2 < 3.1 < 3.7 < 3.7 < 3.6 < 3.0Vanadium 25.8 36.1 32.4 21.8 33.7 33.1Zinc 2,200 109 47.3 42.3 33.9 24.3 126 58.9PCBs By SW 8082 ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/KgPCB-1016 1,000 100 < 75 < 74 < 84 < 74 < 78 < 75PCB-1221 1,000 100 < 75 < 74 < 84 < 74 < 78 < 75PCB-1232 1,000 100 < 75 < 74 < 84 < 74 < 78 < 75PCB-1242 1,000 100 < 75 < 74 < 84 < 74 < 78 < 75PCB-1248 1,000 100 < 75 < 74 < 84 < 74 < 78 < 75PCB-1254 1,000 100 < 75 < 74 < 84 < 74 < 78 < 75PCB-1260 1,000 100 < 75 < 74 < 84 < 74 < 78 < 75PCB-1262 < 75 < 74 < 84 < 74 < 78 < 75PCB-1268 < 75 < 74 < 84 < 74 < 78 < 75Volatiles by SW 8260 ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg1,1,1,2-Tetrachloroethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,1,1-Trichloroethane 100,000 680 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,1,2,2-Tetrachloroethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,1,2-Trichloroethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7


Project 1408950





Compound1,1-Dichloroethane 19,000 270 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,1-Dichloroethene 100,000 330 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,1-Dichloropropene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,2,3-Trichlorobenzene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,2,3-Trichloropropane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,2,4-Trichlorobenzene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,2,4-Trimethylbenzene 47,000 3,600 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,2-Dibromo-3-chloropropane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,2-Dibromoethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,2-Dichlorobenzene 100,000 1,100 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,2-Dichloroethane 2,300 20 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,2-Dichloropropane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,3,5-Trimethylbenzene 47,000 8,400 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,3-Dichlorobenzene 17,000 2,400 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,3-Dichloropropane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.71,4-Dichlorobenzene 9,800 1,800 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.72,2-Dichloropropane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.72-Chlorotoluene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.72-Hexanone < 29 < 28 < 32 < 28 < 29 < 282-Isopropyltoluene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.74-Chlorotoluene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.74-Methyl-2-pentanone < 29 < 28 < 32 < 28 < 29 < 28Acetone 100,000 50 < 29 56 < 32 < 28 < 29 55Acrylonitrile < 12 < 11 < 13 < 11 < 12 < 11Benzene 2,900 60 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Bromobenzene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Bromochloromethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Bromodichloromethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Bromoform < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Bromomethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Carbon Disulfide < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Carbon tetrachloride 1,400 760 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Chlorobenzene 100,000 1,100 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Chloroethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Chloroform 10,000 370 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Chloromethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7cis-1,2-Dichloroethene 59,000 250 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7cis-1,3-Dichloropropene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Dibromochloromethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Dibromomethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Dichlorodifluoromethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Ethylbenzene 30,000 1,000 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Hexachlorobutadiene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Isopropylbenzene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7m&p-Xylene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7


Project 1408950





CompoundMethyl Ethyl Ketone 100,000 120 < 29 < 28 < 32 < 28 < 29 < 28Methyl t-butyl ether (MTBE) 62,000 930 < 12 < 11 < 13 < 11 < 12 < 11Methylene chloride 51,000 50 29 12 8.7 13 21 10Naphthalene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7n-Butylbenzene 100,000 12,000 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7n-Propylbenzene 100,000 3,900 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7o-Xylene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7p-Isopropyltoluene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7sec-Butylbenzene 100,000 11,000 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Styrene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7tert-Butylbenzene 100,000 5,900 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Tetrachloroethene 5,500 1,300 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Tetrahydrofuran (THF) < 12 < 11 < 13 < 11 < 12 < 11Toluene 100,000 700 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Total Xylenes 260 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7trans-1,2-Dichloroethene 100,000 190 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7trans-1,3-Dichloropropene < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7trans-1,4-dichloro-2-butene < 12 < 11 < 13 < 11 < 12 < 11Trichloroethene 10,000 470 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Trichlorofluoromethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Trichlorotrifluoroethane < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Vinyl chloride 210 20 < 5.8 < 5.6 < 6.5 < 5.7 < 5.9 < 5.7Semivolatiles By SW 8270 ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg1,2,4,5-Tetrachlorobenzene < 270 < 250 < 300 < 260 < 270 < 2601,2,4-Trichlorobenzene < 270 < 250 < 300 < 260 < 270 < 2601,2-Dichlorobenzene < 270 < 250 < 300 < 260 < 270 < 2601,2-Diphenylhydrazine < 380 < 360 < 430 < 370 < 390 < 3801,3-Dichlorobenzene < 270 < 250 < 300 < 260 < 270 < 2601,4-Dichlorobenzene < 270 < 250 < 300 < 260 < 270 < 2602,4,5-Trichlorophenol < 270 < 250 < 300 < 260 < 270 < 2602,4,6-Trichlorophenol < 270 < 250 < 300 < 260 < 270 < 2602,4-Dichlorophenol < 270 < 250 < 300 < 260 < 270 < 2602,4-Dimethylphenol < 270 < 250 < 300 < 260 < 270 < 2602,4-Dinitrophenol < 610 < 580 < 690 < 590 < 620 < 6002,4-Dinitrotoluene < 270 < 250 < 300 < 260 < 270 < 2602,6-Dinitrotoluene < 270 < 250 < 300 < 260 < 270 < 2602-Chloronaphthalene < 270 < 250 < 300 < 260 < 270 < 2602-Chlorophenol < 270 < 250 < 300 < 260 < 270 < 2602-Methylnaphthalene < 270 < 250 < 300 < 260 < 270 < 2602-Methylphenol (o-cresol) 100,000 330 < 270 < 250 < 300 < 260 < 270 < 2602-Nitroaniline < 610 < 580 < 690 < 590 < 620 < 6002-Nitrophenol < 270 < 250 < 300 < 260 < 270 < 2603&4-Methylphenol (m&p-cresol) < 380 < 360 < 430 < 370 < 390 < 3803,3'-Dichlorobenzidine < 270 < 250 < 300 < 260 < 270 < 2603-Nitroaniline < 610 < 580 < 690 < 590 < 620 < 6004,6-Dinitro-2-methylphenol < 1100 < 1100 < 1300 < 1100 < 1100 < 1100


Project 1408950





Compound4-Bromophenyl phenyl ether < 380 < 360 < 430 < 370 < 390 < 3804-Chloro-3-methylphenol < 270 < 250 < 300 < 260 < 270 < 2604-Chloroaniline < 270 < 250 < 300 < 260 < 270 < 2604-Chlorophenyl phenyl ether < 270 < 250 < 300 < 260 < 270 < 2604-Nitroaniline < 610 < 580 < 690 < 590 < 620 < 6004-Nitrophenol < 1100 < 1100 < 1300 < 1100 < 1100 < 1100Acenaphthene 100,000 20,000 < 270 < 250 < 300 < 260 < 270 < 260Acenaphthylene 100,000 100,000 < 270 < 250 < 300 < 260 < 270 < 260Acetophenone < 270 < 250 < 300 < 260 < 270 < 260Aniline < 1100 < 1100 < 1300 < 1100 < 1100 < 1100Anthracene 100,000 100,000 < 270 < 250 < 300 < 260 690 < 260Benz(a)anthracene 1,000 1,000 820 < 250 < 300 < 260 2,800 < 260Benzidine < 450 < 430 < 520 < 440 < 470 < 450Benzo(a)pyrene 1,000 1,000 740 < 250 < 300 < 260 2,600 < 260Benzo(b)fluoranthene 1,000 1,000 1,000 < 250 < 300 < 260 3,300 < 260Benzo(ghi)perylene 100,000 100,000 460 < 250 < 300 < 260 1,100 < 260Benzo(k)fluoranthene 1,000 800 300 < 250 < 300 < 260 1,200 < 260Benzoic acid < 1100 < 1100 < 1300 < 1100 < 1100 < 1100Benzyl butyl phthalate < 270 < 250 < 300 < 260 < 270 < 260Bis(2-chloroethoxy)methane < 270 < 250 < 300 < 260 < 270 < 260Bis(2-chloroethyl)ether < 380 < 360 < 430 < 370 < 390 < 380Bis(2-chloroisopropyl)ether < 270 < 250 < 300 < 260 < 270 < 260Bis(2-ethylhexyl)phthalate < 270 < 250 < 300 < 260 < 270 < 260Carbazole < 570 < 540 < 650 < 550 < 590 < 560Chrysene 1,000 1,000 880 < 250 < 300 < 260 2,900 < 260Dibenz(a,h)anthracene 330 330 < 270 < 250 < 300 < 260 < 270 < 260Dibenzofuran 7,000 < 270 < 250 < 300 < 260 < 270 < 260Diethyl phthalate < 270 < 250 < 300 < 260 < 270 < 260Dimethylphthalate < 270 < 250 < 300 < 260 < 270 < 260Di-n-butylphthalate < 270 < 250 < 300 < 260 < 270 < 260Di-n-octylphthalate < 270 < 250 < 300 < 260 < 270 < 260Fluoranthene 100,000 100,000 1,800 < 250 < 300 < 260 6,100 < 260Fluorene 100,000 30,000 < 270 < 250 < 300 < 260 < 270 < 260Hexachlorobenzene < 270 < 250 < 300 < 260 < 270 < 260Hexachlorobutadiene < 270 < 250 < 300 < 260 < 270 < 260Hexachlorocyclopentadiene < 270 < 250 < 300 < 260 < 270 < 260Hexachloroethane < 270 < 250 < 300 < 260 < 270 < 260Indeno(1,2,3-cd)pyrene 500 500 380 < 250 < 300 < 260 1,100 < 260Isophorone < 270 < 250 < 300 < 260 < 270 < 260Naphthalene 100,000 12,000 < 270 < 250 < 300 < 260 < 270 < 260Nitrobenzene < 270 < 250 < 300 < 260 < 270 < 260N-Nitrosodimethylamine < 380 < 360 < 430 < 370 < 390 < 380N-Nitrosodi-n-propylamine < 270 < 250 < 300 < 260 < 270 < 260N-Nitrosodiphenylamine < 380 < 360 < 430 < 370 < 390 < 380Pentachloronitrobenzene < 380 < 360 < 430 < 370 < 390 < 380Pentachlorophenol 2,400 800 < 380 < 360 < 430 < 370 < 390 < 380Phenanthrene 100,000 100,000 830 < 250 < 300 < 260 3,800 < 260


Project 1408950





CompoundPhenol 100,000 330 < 270 < 250 < 300 < 260 < 270 < 260Pyrene 100,000 100,000 1,600 < 250 < 300 < 260 5,600 < 260Pyridine < 380 < 360 < 430 < 370 < 390 < 380Pesticides - Soil By SW8081 ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg4,4' -DDD 2,600 3.3 < 2.7 < 2.6 < 3.0 < 2.7 < 2.8 < 2.74,4' -DDE 1,800 3.3 < 2.7 < 2.6 < 3.0 < 2.7 < 2.8 < 2.74,4' -DDT 1,700 3.3 < 2.7 < 2.6 < 3.0 < 2.7 < 2.8 < 2.7a-BHC 97 20 < 1.9 < 1.8 < 2.1 < 1.8 < 1.9 < 1.9a-Chlordane 910 94 < 3.8 < 3.7 < 4.2 < 3.7 < 3.9 < 3.7Aldrin 19 5 < 1.9 < 1.8 < 2.1 < 1.8 < 1.9 < 1.9b-BHC 72 36 < 1.9 < 1.8 < 2.1 < 1.8 < 1.9 < 1.9Chlordane < 23 < 22 < 25 < 22 < 23 < 22d-BHC 100,000 40 < 1.9 < 1.8 < 2.1 < 1.8 < 1.9 < 1.9Dieldrin 39 5 < 1.9 < 1.8 < 2.1 < 1.8 < 1.9 < 1.9Endosulfan I 4,800 2,400 < 3.8 < 3.7 < 4.2 < 3.7 < 3.9 < 3.7Endosulfan II 4,800 2,400 < 3.8 < 3.7 < 4.2 < 3.7 < 3.9 < 3.7Endosulfan sulfate 4,800 2,400 < 3.8 < 3.7 < 4.2 < 3.7 < 3.9 < 3.7Endrin 2,200 14 < 1.9 < 1.8 < 2.1 < 1.8 < 1.9 < 1.9Endrin aldehyde < 3.8 < 3.7 < 4.2 < 3.7 < 3.9 < 3.7Endrin ketone < 1.9 < 1.8 < 2.1 < 1.8 < 1.9 < 1.9g-BHC 280 100 < 1.9 < 1.8 < 2.1 < 1.8 < 1.9 < 1.9g-Chlordane < 3.8 < 3.7 < 4.2 < 3.7 < 3.9 < 3.7Heptachlor 420 42 < 1.9 < 1.8 < 2.1 < 1.8 < 1.9 < 1.9Heptachlor epoxide < 1.9 < 1.8 < 2.1 < 1.8 < 1.9 < 1.9Methoxychlor < 7.5 < 7.4 < 8.4 < 7.4 < 7.8 < 7.5Toxaphene < 190 < 180 < 210 < 180 < 190 < 190


Project 1408950




Sample ID NY-Res. NY-UnRestrictedSampling Date

CompoundMiscellaneous/Inorganics mg/Kg mg/KgPercent SolidTotal Cyanide 27 27Metals, Total mg/Kg mg/KgAluminumAntimonyArsenic 16 13Barium 350 350Beryllium 14 7.2Cadmium 2.5 2.5CalciumChromium 30CobaltCopper 270 50IronLead 400 63MagnesiumManganese 2,000 1,600Mercury 0.81 0.18Nickel 140 30PotassiumSelenium 36 3.9Silver 36 2SodiumThalliumVanadiumZinc 2,200 109PCBs By SW 8082 ug/Kg ug/KgPCB-1016 1,000 100PCB-1221 1,000 100PCB-1232 1,000 100PCB-1242 1,000 100PCB-1248 1,000 100PCB-1254 1,000 100PCB-1260 1,000 100PCB-1262PCB-1268Volatiles by SW 8260 ug/Kg ug/Kg1,1,1,2-Tetrachloroethane1,1,1-Trichloroethane 100,000 6801,1,2,2-Tetrachloroethane1,1,2-Trichloroethane

B-4 (0-2 FT) B-4 (10-12 FT) B-5 (0-2 FT) B-5 (10-12 FT) B-6 (0-2 FT) B-6 (10-12 FT)8/8/2014 8/8/2014 8/8/2014 8/8/2014 8/8/2014 8/8/2014

mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg79 80 82 79 89 88

2.09 < 0.52 < 0.61 < 0.58 < 0.56 < 0.57mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg

8,790 11,700 14,000 6,980 8,760 7,5505.8 < 3.8 < 3.8 < 3.9 5.4 < 3.8

15.5 2.1 5.6 < 0.8 5.4 < 0.8480 80.5 116 46.6 186 32.4

0.56 0.73 0.51 0.4 0.42 0.574.47 < 0.38 < 0.38 < 0.39 2.74 < 0.38

5,220 1,530 1,550 732 1,550 78948.9 36.4 22.1 16.4 58.5 21.19.3 13.7 6.49 8.18 6.99 9.45

135 38.7 36.7 13.6 30.3 19.424,000 38,900 22,500 20,600 19,100 29,1001,230 9.09 96.9 5.64 293 8.542,030 3,170 2,670 2,000 2,030 1,650

316 688 258 396 293 5070.82 < 0.08 1.04 < 0.08 0.44 < 0.0837.8 19.2 14 9.91 16.3 11.8793 1,600 1,150 1,390 994 1,330

< 1.5 < 1.5 < 1.5 < 1.5 < 1.3 < 1.5< 1.0 < 0.38 < 0.38 < 0.39 < 1.0 < 0.38

221 67 67.4 61.7 51.1 44< 3.5 < 3.4 < 3.4 < 3.5 < 3.0 < 3.480.6 56.9 30.6 30.3 30.5 39.3538 60.2 88.7 34.6 652 38.7

ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg< 82 < 82 < 81 < 84 < 74 < 74< 82 < 82 < 81 < 84 < 74 < 74< 82 < 82 < 81 < 84 < 74 < 74< 82 < 82 < 81 < 84 < 74 < 74< 82 < 82 < 81 < 84 < 74 < 74< 82 < 82 < 81 < 84 < 74 < 74270 < 82 < 81 < 84 < 74 < 74

< 82 < 82 < 81 < 84 < 74 < 74< 82 < 82 < 81 < 84 < 74 < 74

ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7


Project 1408950





Compound1,1-Dichloroethane 19,000 2701,1-Dichloroethene 100,000 3301,1-Dichloropropene1,2,3-Trichlorobenzene1,2,3-Trichloropropane1,2,4-Trichlorobenzene1,2,4-Trimethylbenzene 47,000 3,6001,2-Dibromo-3-chloropropane1,2-Dibromoethane1,2-Dichlorobenzene 100,000 1,1001,2-Dichloroethane 2,300 201,2-Dichloropropane1,3,5-Trimethylbenzene 47,000 8,4001,3-Dichlorobenzene 17,000 2,4001,3-Dichloropropane1,4-Dichlorobenzene 9,800 1,8002,2-Dichloropropane2-Chlorotoluene2-Hexanone2-Isopropyltoluene4-Chlorotoluene4-Methyl-2-pentanoneAcetone 100,000 50AcrylonitrileBenzene 2,900 60BromobenzeneBromochloromethaneBromodichloromethaneBromoformBromomethaneCarbon DisulfideCarbon tetrachloride 1,400 760Chlorobenzene 100,000 1,100ChloroethaneChloroform 10,000 370Chloromethanecis-1,2-Dichloroethene 59,000 250cis-1,3-DichloropropeneDibromochloromethaneDibromomethaneDichlorodifluoromethaneEthylbenzene 30,000 1,000HexachlorobutadieneIsopropylbenzenem&p-Xylene


< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 32 < 31 < 30 < 32 < 28 < 28

< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 32 < 31 < 30 < 32 < 28 < 28< 32 75 100 < 32 < 28 51< 13 < 13 < 12 < 13 < 11 < 11< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7


Project 1408950





CompoundMethyl Ethyl Ketone 100,000 120Methyl t-butyl ether (MTBE) 62,000 930Methylene chloride 51,000 50Naphthalenen-Butylbenzene 100,000 12,000n-Propylbenzene 100,000 3,900o-Xylenep-Isopropyltoluenesec-Butylbenzene 100,000 11,000Styrenetert-Butylbenzene 100,000 5,900Tetrachloroethene 5,500 1,300Tetrahydrofuran (THF)Toluene 100,000 700Total Xylenes 260trans-1,2-Dichloroethene 100,000 190trans-1,3-Dichloropropenetrans-1,4-dichloro-2-buteneTrichloroethene 10,000 470TrichlorofluoromethaneTrichlorotrifluoroethaneVinyl chloride 210 20Semivolatiles By SW 8270 ug/Kg ug/Kg1,2,4,5-Tetrachlorobenzene1,2,4-Trichlorobenzene1,2-Dichlorobenzene1,2-Diphenylhydrazine1,3-Dichlorobenzene1,4-Dichlorobenzene2,4,5-Trichlorophenol2,4,6-Trichlorophenol2,4-Dichlorophenol2,4-Dimethylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-Dinitrotoluene2-Chloronaphthalene2-Chlorophenol2-Methylnaphthalene2-Methylphenol (o-cresol) 100,000 3302-Nitroaniline2-Nitrophenol3&4-Methylphenol (m&p-cresol)3,3'-Dichlorobenzidine3-Nitroaniline4,6-Dinitro-2-methylphenol


< 32 < 31 < 30 < 32 < 28 < 28< 13 < 13 < 12 < 13 < 11 < 11

53 22 33 11 30 13< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

< 320 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 13 < 13 < 12 < 13 < 11 < 11

< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

< 630 < 13 < 12 < 13 < 11 < 11< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7< 6.3 < 6.3 < 6.1 < 6.3 < 5.6 < 5.7

ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 2100 < 410 < 400 < 410 < 370 < 370< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 3400 < 660 < 640 < 650 < 600 < 600< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 3400 < 660 < 640 < 650 < 600 < 600< 1500 < 290 < 280 < 290 < 260 < 260< 2100 < 410 < 400 < 410 < 370 < 370< 1500 < 290 < 280 < 290 < 260 < 260< 3400 < 660 < 640 < 650 < 600 < 600< 6100 < 1200 < 1200 < 1200 < 1100 < 1100


Project 1408950





Compound4-Bromophenyl phenyl ether4-Chloro-3-methylphenol4-Chloroaniline4-Chlorophenyl phenyl ether4-Nitroaniline4-NitrophenolAcenaphthene 100,000 20,000Acenaphthylene 100,000 100,000AcetophenoneAnilineAnthracene 100,000 100,000Benz(a)anthracene 1,000 1,000BenzidineBenzo(a)pyrene 1,000 1,000Benzo(b)fluoranthene 1,000 1,000Benzo(ghi)perylene 100,000 100,000Benzo(k)fluoranthene 1,000 800Benzoic acidBenzyl butyl phthalateBis(2-chloroethoxy)methaneBis(2-chloroethyl)etherBis(2-chloroisopropyl)etherBis(2-ethylhexyl)phthalateCarbazoleChrysene 1,000 1,000Dibenz(a,h)anthracene 330 330Dibenzofuran 7,000Diethyl phthalateDimethylphthalateDi-n-butylphthalateDi-n-octylphthalateFluoranthene 100,000 100,000Fluorene 100,000 30,000HexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethaneIndeno(1,2,3-cd)pyrene 500 500IsophoroneNaphthalene 100,000 12,000NitrobenzeneN-NitrosodimethylamineN-Nitrosodi-n-propylamineN-NitrosodiphenylaminePentachloronitrobenzenePentachlorophenol 2,400 800Phenanthrene 100,000 100,000


< 2100 < 410 < 400 < 410 < 370 < 370< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 3400 < 660 < 640 < 650 < 600 < 600< 6100 < 1200 < 1200 < 1200 < 1100 < 1100

1,900 < 290 < 280 < 290 < 260 < 2603,300 < 290 < 280 < 290 < 260 < 260

< 1500 < 290 < 280 < 290 < 260 < 260< 6100 < 1200 < 1200 < 1200 < 1100 < 1100

7,800 < 290 < 280 < 290 < 260 < 26028,000 < 290 < 280 < 290 < 260 < 260< 2500 < 500 < 480 < 490 < 450 < 45020,000 < 290 < 280 < 290 < 260 < 26028,000 < 290 < 280 < 290 280 < 2608,000 < 290 < 280 < 290 < 260 < 2608,500 < 290 < 280 < 290 < 260 < 260

< 6100 < 1200 < 1200 < 1200 < 1100 < 1100< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 2100 < 410 < 400 < 410 < 370 < 370< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260

4,500 < 620 < 600 < 610 < 560 < 56024,000 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260

2,000 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 26076,000 < 290 < 280 < 290 330 < 2603,200 < 290 < 280 < 290 < 260 < 260

< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260

8,400 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 1500 < 290 < 280 < 290 < 260 < 260< 2100 < 410 < 400 < 410 < 370 < 370< 1500 < 290 < 280 < 290 < 260 < 260< 2100 < 410 < 400 < 410 < 370 < 370< 2100 < 410 < 400 < 410 < 370 < 370< 2100 < 410 < 400 < 410 < 370 < 37045,000 < 290 < 280 < 290 < 260 < 260


Project 1408950





CompoundPhenol 100,000 330Pyrene 100,000 100,000PyridinePesticides - Soil By SW8081 ug/Kg ug/Kg4,4' -DDD 2,600 3.34,4' -DDE 1,800 3.34,4' -DDT 1,700 3.3a-BHC 97 20a-Chlordane 910 94Aldrin 19 5b-BHC 72 36Chlordaned-BHC 100,000 40Dieldrin 39 5Endosulfan I 4,800 2,400Endosulfan II 4,800 2,400Endosulfan sulfate 4,800 2,400Endrin 2,200 14Endrin aldehydeEndrin ketoneg-BHC 280 100g-ChlordaneHeptachlor 420 42Heptachlor epoxideMethoxychlorToxaphene


< 1500 < 290 < 280 < 290 < 260 < 26061,000 < 290 < 280 < 290 280 < 260< 2100 < 410 < 400 < 410 < 370 < 370

ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg< 3.0 < 3.0 < 2.9 < 3.0 < 2.7 < 2.7< 3.0 < 3.0 < 2.9 < 3.0 25 < 2.7

14 < 3.0 < 2.9 < 3.0 40 < 2.7< 2.1 < 2.1 < 2.0 < 2.1 < 1.9 < 1.8< 4.1 < 4.1 < 4.0 < 4.2 < 3.7 < 3.7< 2.1 < 2.1 < 2.0 < 2.1 < 1.9 < 1.8< 5.0 < 2.1 < 2.0 < 2.1 < 1.9 < 1.8< 25 < 25 < 24 < 25 < 22 < 22

< 6.0 < 2.1 < 2.0 < 2.1 < 1.9 < 1.8< 2.1 < 2.1 < 2.0 < 2.1 < 1.9 < 1.8< 4.1 < 4.1 < 4.0 < 4.2 < 3.7 < 3.7< 4.1 < 4.1 < 4.0 < 4.2 < 3.7 < 3.7< 25 < 4.1 < 4.0 < 4.2 < 3.7 < 3.7

< 2.1 < 2.1 < 2.0 < 2.1 < 1.9 < 1.8< 4.1 < 4.1 < 4.0 < 4.2 < 3.7 < 3.7< 30 < 2.1 < 2.0 < 2.1 < 1.9 < 1.8

< 2.1 < 2.1 < 2.0 < 2.1 < 1.9 < 1.8< 4.1 < 4.1 < 4.0 < 4.2 < 3.7 < 3.7< 5.0 < 2.1 < 2.0 < 2.1 < 1.9 < 1.8< 5.0 < 2.1 < 2.0 < 2.1 < 1.9 < 1.8< 8.2 < 8.2 < 8.1 < 8.4 < 7.4 < 7.4< 210 < 210 < 200 < 210 < 190 < 180

NOTES:mg/Kg = milligrams per kilogramug/Kg = micrograms per kilogramRegulatory Exceedences are shaded


Project 1408950


Table 2 GroundwaterTable 2 GW

Table 2. Groundwater Analytical ResultsPhase II Investigation59-63 North 6th StreetBrooklyn, New York

Sample ID GW-1 GW-2 GW-3Sampling Date TOGS-WQ/GA 8/11/2014 8/11/2014 8/11/2014

CompoundMiscellaneous/Inorganics (mg/L)Total Cyanide 0.2 0.03 < 0.01 < 0.01Metals, Total (mg/L)Aluminum 0.1 579 288 223Aluminum (Dissolved) 0.1 0.13 0.31 0.15Antimony 0.003 < 0.003 < 0.003 < 0.003Antimony (Dissolved) 0.003 < 0.003 < 0.003 < 0.003Arsenic 0.025 0.498 0.151 0.156Arsenic (Dissolved) 0.025 < 0.004 < 0.004 < 0.004Barium 1 9.96 3.39 2.23Barium (Dissolved) 1 0.049 0.053 0.045Beryllium 0.003 0.031 0.015 0.012Beryllium (Dissolved) 0.003 < 0.001 < 0.001 < 0.001Cadmium 0.005 0.017 0.016 0.009Cadmium (Dissolved) 0.005 < 0.001 < 0.001 < 0.001Calcium 881 342 90Calcium (Dissolved) 71.3 111 107Chromium 0.05 2.66 1.29 0.711Chromium (Dissolved) 0.05 < 0.001 < 0.001 < 0.001Cobalt 0.7 0.329 0.204Cobalt (Dissolved) 0.001 0.004 0.005Copper 0.2 2.16 0.963 0.573Copper (Dissolved) 0.2 < 0.005 < 0.005 0.008Iron 0.3 1,400 714 550Iron (Dissolved) 0.3 0.093 0.082 0.11Lead 0.025 9.29 3.81 0.207Lead (Dissolved) 0.025 < 0.002 < 0.002 < 0.002Magnesium 35 228 110 94Magnesium (Dissolved) 35 9.94 18.5 21.7Manganese 0.3 56.5 25.5 31.5Manganese (Dissolved) 0.3 0.823 3.98 3.5Mercury 0.0007 0.0008 < 0.0002 < 0.0002Mercury (Dissolved) 0.0007 < 0.0002 < 0.0002 < 0.0002Nickel 0.1 1.38 0.673 0.539Nickel (Dissolved) 0.1 0.004 0.009 0.011Potassium 117 45.5 31.7Potassium (Dissolved) 8.1 10.3 11.5Selenium 0.01 < 0.01 0.011 < 0.01Selenium (Dissolved) 0.01 < 0.002 < 0.005 < 0.010Silver 0.05 < 0.005 < 0.001 < 0.001Silver (Dissolved) 0.05 < 0.001 < 0.001 < 0.001Sodium 20 49.6 45.8 56.4Sodium (Dissolved) 20 55.8 51.4 57.2Thallium 0.0005 < 0.0005 < 0.0005 < 0.0005Thallium (Dissolved) 0.0005 < 0.0005 < 0.0005 < 0.0005Vanadium 1.59 0.695 0.444Vanadium (Dissolved) < 0.002 < 0.002 < 0.002Zinc 5 7.65 3.33 1.11Zinc (Dissolved) 5 0.003 0.021 0.006PCBs By 608/ 8082 (ug/L)PCB-1016 0.09 0.067 < 0.053 < 0.050PCB-1221 0.09 < 0.058 < 0.053 < 0.050PCB-1232 0.09 < 0.058 < 0.053 < 0.050PCB-1242 0.09 < 0.058 < 0.053 < 0.050PCB-1248 0.09 < 0.058 < 0.053 < 0.050PCB-1254 0.09 < 0.058 < 0.053 < 0.050PCB-1260 0.09 < 0.058 < 0.053 < 0.050PCB-1262 < 0.058 < 0.053 < 0.050PCB-1268 < 0.058 < 0.053 < 0.050Volatiles By SW8260 (ug/L)1,1,1,2-Tetrachloroethane 5 < 1.0 < 1.0 < 1.01,1,1-Trichloroethane 5 < 1.0 < 1.0 < 1.01,1,2,2-Tetrachloroethane 5 < 0.50 < 0.50 < 0.501,1,2-Trichloroethane 1 < 1.0 < 1.0 < 1.01,1-Dichloroethane 5 < 1.0 < 1.0 < 1.01,1-Dichloroethene 5 < 1.0 < 1.0 < 1.01,1-Dichloropropene 5 < 1.0 < 1.0 < 1.01,2,3-Trichlorobenzene < 1.0 < 1.0 < 1.0


Project 1408950





Compound1,2,3-Trichloropropane 0.04 < 1.0 < 1.0 < 1.01,2,4-Trichlorobenzene < 1.0 < 1.0 < 1.01,2,4-Trimethylbenzene 5 < 1.0 < 1.0 < 1.01,2-Dibromo-3-chloropropane 0.04 < 1.0 < 1.0 < 1.01,2-Dibromoethane 0.0006 < 1.0 < 1.0 < 1.01,2-Dichlorobenzene < 1.0 < 1.0 < 1.01,2-Dichloroethane 0.6 < 0.60 < 0.60 < 0.601,2-Dichloropropane 1 < 1.0 < 1.0 < 1.01,3,5-Trimethylbenzene 5 < 1.0 < 1.0 < 1.01,3-Dichlorobenzene 3 < 1.0 < 1.0 < 1.01,3-Dichloropropane 5 < 1.0 < 1.0 < 1.01,4-Dichlorobenzene < 1.0 < 1.0 < 1.02,2-Dichloropropane 5 < 1.0 < 1.0 < 1.02-Chlorotoluene 5 < 1.0 < 1.0 < 1.02-Hexanone 50 < 5.0 < 5.0 < 5.02-Isopropyltoluene 5 < 1.0 < 1.0 < 1.04-Chlorotoluene 5 < 1.0 < 1.0 < 1.04-Methyl-2-pentanone < 5.0 < 5.0 < 5.0Acetone 50 < 25 < 25 < 25Acrylonitrile 5 < 5.0 < 5.0 < 5.0Benzene 1 < 0.70 < 0.70 < 0.70Bromobenzene 5 < 1.0 < 1.0 < 1.0Bromochloromethane 5 < 1.0 < 1.0 < 1.0Bromodichloromethane 50 < 0.50 < 0.50 < 0.50Bromoform 50 < 1.0 < 1.0 < 1.0Bromomethane 5 < 1.0 < 1.0 < 1.0Carbon Disulfide < 5.0 < 5.0 < 5.0Carbon tetrachloride 5 < 1.0 < 1.0 < 1.0Chlorobenzene 5 < 1.0 < 1.0 < 1.0Chloroethane 5 < 1.0 < 1.0 < 1.0Chloroform 7 < 1.0 < 1.0 < 1.0Chloromethane 5 < 1.0 < 1.0 < 1.0cis-1,2-Dichloroethene 5 < 1.0 < 1.0 < 1.0cis-1,3-Dichloropropene 0.4 < 0.40 < 0.40 < 0.40Dibromochloromethane 50 < 0.50 < 0.50 < 0.50Dibromomethane 5 < 1.0 < 1.0 < 1.0Dichlorodifluoromethane 5 < 1.0 < 1.0 < 1.0Ethylbenzene 5 < 1.0 < 1.0 < 1.0Hexachlorobutadiene 0.5 < 0.40 < 0.40 < 0.40Isopropylbenzene 5 < 1.0 < 1.0 < 1.0m&p-Xylene < 1.0 < 1.0 < 1.0Methyl ethyl ketone 50 < 5.0 < 5.0 < 5.0Methyl t-butyl ether (MTBE) < 1.0 < 1.0 < 1.0Methylene chloride 5 < 1.0 < 1.0 < 1.0Naphthalene 10 8.7 5.7 < 1.0n-Butylbenzene 5 < 1.0 < 1.0 < 1.0n-Propylbenzene 5 < 1.0 < 1.0 < 1.0o-Xylene 5 < 1.0 < 1.0 < 1.0p-Isopropyltoluene 5 < 1.0 < 1.0 < 1.0sec-Butylbenzene 5 < 1.0 < 1.0 < 1.0Styrene 5 < 1.0 < 1.0 < 1.0tert-Butylbenzene 5 < 1.0 < 1.0 < 1.0Tetrachloroethene 5 < 1.0 < 1.0 < 1.0Tetrahydrofuran (THF) 50 < 2.5 < 2.5 < 2.5Toluene 5 < 1.0 < 1.0 < 1.0Total Xylenes 5 < 1.0 < 1.0 < 1.0trans-1,2-Dichloroethene 5 < 1.0 < 1.0 < 1.0trans-1,3-Dichloropropene 0.4 < 0.40 < 0.40 < 0.40trans-1,4-dichloro-2-butene 5 < 5.0 < 5.0 < 5.0Trichloroethene 5 < 1.0 4.3 2.6Trichlorofluoromethane 5 < 1.0 < 1.0 < 1.0Trichlorotrifluoroethane 5 < 1.0 < 1.0 < 1.0Vinyl chloride 2 < 1.0 < 1.0 < 1.0


Project 1408950





CompoundSemivolatiles By SW8270 (SIM) (ug/L)1,2,4,5-Tetrachlorobenzene < 0.50 < 0.56 < 0.51Acenaphthene 20 0.64 0.12 < 0.05Acenaphthylene 0.25 0.06 < 0.05Anthracene 50 1.4 0.21 0.04Benz(a)anthracene 0.002 3.1 0.4 0.07Benzo(a)pyrene 2.2 0.26 < 0.02Benzo(b)fluoranthene 0.002 3 0.4 0.05Benzo(ghi)perylene 1.1 < 0.56 < 0.51Benzo(k)fluoranthene 0.002 1 0.12 0.02Bis(2-ethylhexyl)phthalate 5 3 4.9 3.4Chrysene 0.002 3 0.38 0.05Dibenz(a,h)anthracene < 0.02 < 0.02 < 0.02Fluoranthene 50 7.7 1 0.14Hexachlorobenzene 0.04 < 0.04 < 0.04 < 0.04Hexachlorobutadiene 0.5 < 0.50 < 0.5 < 0.5Hexachloroethane 5 < 0.50 < 0.56 < 0.51Indeno(1,2,3-cd)pyrene 0.002 1 0.12 < 0.02Nitrobenzene 0.4 < 0.10 < 0.11 < 0.10Pentachloronitrobenzene < 0.10 < 0.11 < 0.10Pentachlorophenol 1 < 0.80 < 0.89 < 0.82Phenanthrene 50 6.6 1.1 < 0.05Pyrene 50 6 0.78 0.11Pyridine 50 < 0.50 < 0.56 < 0.51Semivolatiles By SW8270 (ug/L)1,2,4-Trichlorobenzene < 5.0 < 5.0 < 5.01,2-Dichlorobenzene < 2.5 < 2.5 < 2.51,2-Diphenylhydrazine < 5.0 < 5.0 < 5.01,3-Dichlorobenzene 3 < 2.5 < 2.5 < 2.51,4-Dichlorobenzene < 2.5 < 2.5 < 2.52,4,5-Trichlorophenol 1 < 1.0 < 1.0 < 1.02,4,6-Trichlorophenol 1 < 1.0 < 1.0 < 1.02,4-Dichlorophenol 5 < 1.0 < 1.0 < 1.02,4-Dimethylphenol 1 < 1.0 < 1.0 < 1.02,4-Dinitrophenol 5 < 1.0 < 1.0 < 1.02,4-Dinitrotoluene 5 < 5.0 < 5.0 < 5.02,6-Dinitrotoluene 5 < 5.0 < 5.0 < 5.02-Chloronaphthalene 10 < 5.0 < 5.0 < 5.02-Chlorophenol 1 < 1.0 < 1.0 < 1.02-Methylnaphthalene < 5.0 < 5.0 < 5.02-Methylphenol (o-cresol) 1 < 1.0 < 1.0 < 1.02-Nitroaniline 5 < 5.0 < 5.0 < 5.02-Nitrophenol 1 < 1.0 < 1.0 < 1.03&4-Methylphenol (m&p-cresol) < 10 < 10 < 103,3'-Dichlorobenzidine 5 < 5.0 < 5.0 < 5.03-Nitroaniline 5 < 5.0 < 5.0 < 5.04,6-Dinitro-2-methylphenol 1 < 1.0 < 1.0 < 1.04-Bromophenyl phenyl ether < 5.0 < 5.0 < 5.04-Chloro-3-methylphenol 1 < 1.0 < 1.0 < 1.04-Chloroaniline 5 < 5.0 < 5.0 < 5.04-Chlorophenyl phenyl ether < 1.0 < 1.0 < 1.04-Nitroaniline 5 < 5.0 < 5.0 < 5.04-Nitrophenol 1 < 1.0 < 1.0 < 1.0Acetophenone < 5.0 < 5.0 < 5.0Aniline 5 < 5.0 < 5.0 < 5.0Benzidine 5 < 5 < 5 < 5Benzoic acid < 50 < 50 < 50Benzyl butyl phthalate 50 < 5.0 < 5.0 < 5.0Bis(2-chloroethoxy)methane 5 < 5.0 < 5.0 < 5.0Bis(2-chloroethyl)ether 1 < 1.0 < 1.0 < 1.0Bis(2-chloroisopropyl)ether < 5.0 < 5.0 < 5.0Carbazole < 5.0 < 5.0 < 5.0Dibenzofuran < 5.0 < 5.0 < 5.0Diethyl phthalate 50 < 5.0 < 5.0 < 5.0Dimethylphthalate 50 < 5.0 < 5.0 < 5.0Di-n-butylphthalate 50 < 5.0 < 5.0 < 5.0Di-n-octylphthalate 50 < 5.0 < 5.0 < 5.0


Project 1408950





CompoundFluorene 50 < 5.0 < 5.0 < 5.0Hexachlorocyclopentadiene 5 < 5.0 < 5.0 < 5.0Isophorone 50 < 5.0 < 5.0 < 5.0Naphthalene 10 < 5.0 < 5.0 < 5.0N-Nitrosodimethylamine < 5.0 < 5.0 < 5.0N-Nitrosodi-n-propylamine < 5.0 < 5.0 < 5.0N-Nitrosodiphenylamine 50 < 5.0 < 5.0 < 5.0Phenol 1 < 1.0 < 1.0 < 1.0Pesticides By SW8081 (ug/L)4,4' -DDD 0.3 < 0.010 < 0.030 < 0.0504,4' -DDE 0.2 < 0.010 < 0.027 < 0.0504,4' -DDT 0.2 < 0.010 < 0.030 < 0.050a-BHC 0.01 < 0.005 < 0.050 < 0.025Alachlor 0.5 < 0.075 < 0.80 < 0.075Aldrin < 0.002 < 0.016 < 0.002b-BHC 0.04 < 0.005 < 0.053 < 0.005Chlordane 0.05 < 0.030 < 0.30 < 0.30d-BHC 0.04 < 0.025 < 0.050 < 0.025Dieldrin 0.004 < 0.035 < 0.15 < 0.002Endosulfan I < 0.10 < 0.11 < 0.050Endosulfan II < 0.050 < 0.050 < 0.050Endosulfan Sulfate < 0.050 < 0.050 < 0.050Endrin < 0.030 < 0.050 < 0.050Endrin Aldehyde 5 < 0.050 < 0.53 < 0.050Endrin ketone 5 < 0.060 < 0.53 < 0.050g-BHC (Lindane) 0.05 < 0.025 < 0.050 < 0.025Heptachlor 0.04 < 0.020 < 0.050 < 0.025Heptachlor epoxide 0.03 < 0.005 < 0.050 < 0.025Methoxychlor 35 < 0.10 < 1.1 < 0.10Toxaphene 0.06 < 0.20 < 2.0 < 1.0

NOTES:mg/L = milligrams per Literug/L = micrograms per literRegulatory Exceedences are shaded

Table 3: Soil Vapor Analytical ResultsPhase II Investigation59-63 North 6th StreetBrooklyn, NY

Sample IDSampling Date

Volatiles (ug/m3)

1,1,1,2-Tetrachloroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,1,1-Trichloroethane 3.05 1 8.67 1 21 1 2.89 11,1,2,2-Tetrachloroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,1,2-Trichloroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,1-Dichloroethane 9.5 1 < 1.00 1 < 1.00 1 < 1.00 11,1-Dichloroethene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,2,4-Trichlorobenzene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,2,4-Trimethylbenzene 36.4 1 7.27 1 37.5 1 25.7 11,2-Dibromoethane(EDB) < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,2-Dichlorobenzene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,2-Dichloroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,2-dichloropropane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,2-Dichlorotetrafluoroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,3,5-Trimethylbenzene 9.28 1 2.11 1 10.7 1 7.37 11,3-Butadiene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,3-Dichlorobenzene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,4-Dichlorobenzene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 11,4-Dioxane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 12-Hexanone(MBK) < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 14-Ethyltoluene 9.38 1 1.92 1 8.3 1 6.29 14-Isopropyltoluene 1.81 1 < 1.00 1 1.86 1 1.32 14-Methyl-2-pentanone(MIBK) 1.31 1 1.39 1 < 1.00 1 4.79 1Acetone 144 1 750 1 129 1 266 1Acrylonitrile < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Benzene 2.74 1 6.51 1 1.92 1 10.5 1Benzyl chloride < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Bromodichloromethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Bromoform < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Bromomethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Carbon Disulfide 4.39 1 2.05 1 2.61 1 140 1Carbon Tetrachloride 0.251 0.25 0.566 0.25 0.377 0.25 0.692 0.25Chlorobenzene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Chloroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Chloroform 1.17 1 < 1.00 1 9.56 1 < 1.00 1Chloromethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Cis-1,2-Dichloroethene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1cis-1,3-Dichloropropene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Cyclohexane 1.79 1 3.85 1 < 1.00 1 3.47 1Dibromochloromethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Dichlorodifluoromethane 1.14 1 1.78 1 1.53 1 < 1.00 1Ethanol 27.1 1 31.6 1 6.52 1 6.5 1Ethyl acetate < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Ethylbenzene 12.5 1 7.12 1 19.1 1 23.7 1Heptane 6.22 1 15.3 1 7.04 1 14.9 1Hexachlorobutadiene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Hexane 5.88 1 13.8 1 2.96 1 11.9 1Isopropylalcohol 4.79 1 14.2 1 2.68 1 4.25 1Isopropylbenzene 1.08 1 < 1.00 1 1.52 1 1.52 1m,p-Xylene 55.5 1 24.1 1 78.1 1 79.4 1Methyl Ethyl Ketone 7.72 1 29.5 1 7.87 1 18.8 1Methyl tert-butyl ether(MTBE) < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Methylene Chloride < 1.00 1 1.22 1 1.7 1 1.11 1n-Butylbenzene 2.58 1 < 1.00 1 2.41 1 1.92 1o-Xylene 20.6 1 8.64 1 27.7 1 27.3 1Propylene 43.5 1 13 1 1.38 1 32.2 1sec-Butylbenzene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Styrene 2.21 1 < 1.00 1 2.81 1 2.3 1Tetrachloroethene 6.64 0.25 0.61 0.25 502 0.25 3.66 0.25Tetrahydrofuran 7.1 1 35.4 1 5.89 1 31.2 1Toluene 51.2 1 59.1 1 71.6 1 120 1Trans-1,2-Dichloroethene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1trans-1,3-Dichloropropene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Trichloroethene 0.967 0.25 < 0.25 0.25 4.03 0.25 2.42 0.25Trichlorofluoromethane 13 1 2.58 1 2.58 1 4.88 1Trichlorotrifluoroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1Vinyl Chloride < 0.25 0.25 < 0.25 0.25 < 0.25 0.25 < 0.25 0.25

8/11/2014SV-3

8/11/2014SV-4

8/11/2014SV-2

8/11/2014SV-1

Table 4: Soil Vapor Results Compared to NYSDOH Guidance Values Phase II Investigation 59-63 North 6th Street Brooklyn, NY

Sample ID NYSDOH

Action Level SV-1 SV-2 SV-3 SV-4

Sampling Date 8/11/2014 8/11/2014 8/11/2014 8/11/2014 Units ug/m³ ug/m³ ug/m³ ug/m³ ug/m³ 1,1,1-Trichloroethane 100 2.10 3.05 2.89 8.67 Carbon tetrachloride 250 0.377 0.251 0.692 0.566 Tetrachloroethylene (PCE) 100 502 6.64 3.66 0.610


Appendix A (Under Separate Cover) _____________________________________________ Phase I ESA Report

Appendix B _____________________________________________ Boring Logs

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70% light brown fine to medium sand1 25% construction & debris (bricks and rocks

0.0 5% silt (no odors)2

0.03 36

0.04

5 0.0 Fill to approximately 7'85% light brown fine sand

6 15% fine gravel10% fines, no odor

7 60

8

9

10 0.0 85% fine to medium brown sand10% fine to coarse gravel

11 5% fines, no odor dry

12 48

13

14

15 0.0

16

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18

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20

21

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23

24 GW @ 24'

25

SOIL BORING (B1)Boring/Well ID: B-1 Client: Rehan Perveez

Project Name: Phase II Subsurface InvestigationLogged By: EC Site Address: 59-63 North 6th Street, Brooklyn, New YorkProject Number: 1408950

Total Depth (feet): 15.0 Driller:Date: 8/8/2014 Contractor: C.G. Environmental

EXPLORATION LOG

Vertical Datum:

Sample Description

Drilling Method:Elevation (Ground):

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70% fine to coarse sand dark brown1 25% construction & debris

0.0 5% silt, no odor2 Fill to approximately 2'

0.03 24

0.04

5 0.0 80% brown fine to medium sand15% fine gravel

6 5% fine, dry

7 60

8

9

10 0.0 80% brown fine to medium sand15% fine gravel

11 5% fine, dry

12 36

13

14

15 0.0

16

17

18

19

20

21

22

23

24

25 GW @ 25'

EXPLORATION LOG

SOIL BORING (B2)Boring/Well ID: B-2 Client: Rehan PerveezProject Number: 1408950 Project Name: Phase II Subsurface InvestigationLogged By: EC Site Address: 59-63 North 6th Street, Brooklyn, New YorkDate: 8/8/2014 Contractor: C.G. EnvironmentalTotal Depth (feet): 15.0 Driller:

Sample Description

Drilling Method:Elevation (Ground): Vertical Datum:

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70% brown fine to medium sand1 20% fine to coarse gravel

0.0 10% silt, dry, no odors2 Fill to approximately 2'

0.03 48

0.04

5 0.0 80% medium brown fine to medium soil15% fine to coarse gravel

6 5% fine, dry, no odor

7 36

8

9



12 60

13

14

15 0.0

16

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23 GW @ 23'

24

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EXPLORATION LOG


Sample Description


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70% light brown fine to medium sand1 20% construction and debris (brick)l

0.0 10% silt, dry, no odors2 Fill to approximately 2'

0.03 48

0.04



7 48

8

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12 48

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15 0.0

16

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Sample Description


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0"-12" - 75% light brown fine to medium sand1 20% fine gravel

0.0 5% silt, dry, no odor2 12"-24" - brick and construction and debris

0.0 Fill to approximately 2'3 36 80% fine to medium brown sand

0.0 15% fine gravel4

5 0.0 85% fine to medium light brown sand15% silt, dry, no odor

6

7 54

8

9

10 0.0 80% fine to medium dark brown sand15% fine to coarse gravel

11 5% silt, dry, no odor

12 60

13

14

15 0.0

16

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Sample Description


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70% light brown fine to medium sand1 25% construction and debris (bricks)

0.0 5% silt2 Fill to approximately 2'

0.03 36

0.04

5 0.0 80% fine to medium light brown sand25% silt, no odor, dry

6

7 54

8

9

10 0.0 85% fine to medium light brown sand15% silts, dry, no odor

11

12 60

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15 0.0

16

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23

24

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EXPLORATION LOG


Sample Description


Appendix C _____________________________________________ Laboratory Data Deliverables for Soil and Groundwater

BG91924 - BG91938

Wednesday, August 20, 2014

Sample ID#s:

Attn: Erik CurranGEI Consultants, Inc. P.C.110 Walt Whitman Rd Suite 204Huntington Station, NY 11746

Project ID: 59-63 N 6TH STREET

Sincerely yours,

Laboratory DirectorPhyllis Shiller

If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.

NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B

NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301

This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.

This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.

587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823

SDG CommentsAugust 20, 2014

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GBG91924

8260 Volatile Organics:1,2-Dibromoethane, 1,2,3 Trichloropropane, and 1,2-Dibromo-3-chloropropane do not meet NY TOGS GA criteria, these compounds are analyzed by GC/ECD method 504 or 8011 to achieve this criteria.

SIM Analysis:The lowest possible reporting limit under SIM conditions is 0.02 ug/L. The NY TOGS GA criteria for some PAHs is 0.002 ug/L. This level can not be achieved.

8081 Pesticides: Toxaphene is reported to the lowest possible reporting level. The NY TOGS criteria for this compound can not be achieved.

Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.

Client provided soil jar for volatile analysis. Phoenix prepared sample per method 5035.

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOILGEICONSStandard408950

08/08/14SWsee "By" below

EC

Laboratory Data

B-1 (0-2 FT)

Phoenix ID: BG91924

08/12/148:15

15:35

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Erik CurranGEI Consultants, Inc. P.C.110 Walt Whitman Rd Suite 204Huntington Station, NY 11746

Analysis ReportAugust 20, 2014

Date Time



SDG ID: GBG91924

Client ID:Project ID: 59-63 N 6TH STREET

LOD/MDL

< 0.35Silver 0.35 08/13/14 EK SW6010mg/Kg14600Aluminum 53 08/14/14 EK SW6010mg/Kg

3.2Arsenic 0.7 08/13/14 EK SW6010mg/Kg73.2Barium 0.35 08/13/14 EK SW6010mg/Kg0.58Beryllium 0.28 08/13/14 EK SW6010mg/Kg1540Calcium 5.3 08/13/14 EK SW6010mg/Kg

< 0.35Cadmium 0.35 08/13/14 EK SW6010mg/Kg7.34Cobalt 0.35 08/13/14 EK SW6010mg/Kg17.6Chromium 0.35 08/13/14 EK SW6010mg/Kg13.5Copper 0.35 08/13/14 EK SW6010mg/kg

18400Iron 53 08/14/14 EK SW6010mg/Kg0.25Mercury 0.09 08/13/14 MA SW-7471mg/Kg798Potassium 5.3 08/13/14 EK SW6010mg/Kg

2340Magnesium 5.3 08/13/14 EK SW6010mg/Kg794Manganese 3.5 08/14/14 EK SW6010mg/Kg68.8Sodium 5.3 08/13/14 LK SW6010mg/Kg12.4Nickel 0.35 08/13/14 EK SW6010mg/Kg109Lead 0.35 08/13/14 EK SW6010mg/Kg

< 3.5Antimony 3.5 08/13/14 EK SW6010mg/Kg< 1.4Selenium 1.4 08/13/14 EK SW6010mg/Kg< 3.2Thallium 3.2 08/13/14 EK SW6010mg/Kg25.8Vanadium 0.35 08/13/14 EK SW6010mg/Kg47.3Zinc 0.35 08/13/14 EK SW6010mg/Kg B

86Percent Solid 08/12/14 I E160.3%< 0.58Total Cyanide 0.58 08/13/14 O/E SW 9010/9012mg/Kg

CompletedSoil Extraction for PCB 08/12/14 BB/H SW3545CompletedSoil Extraction for Pesticide 08/12/14 BB SW3545CompletedSoil Extraction for SVOA 08/12/14 BJ/VF SW3545

Page 1 of 93 Ver 1

B-1 (0-2 FT)Phoenix I.D.: BG91924

Client ID:59-63 N 6TH STREETProject ID:


LOD/MDL

CompletedMercury Digestion 08/13/14 I/I SW7471CompletedTotal Metals Digest 08/12/14 AG/W SW846 - 3050

Polychlorinated BiphenylsNDPCB-1016 75 08/13/14 AW SW 8082ug/KgNDPCB-1221 75 08/13/14 AW SW 8082ug/KgNDPCB-1232 75 08/13/14 AW SW 8082ug/KgNDPCB-1242 75 08/13/14 AW SW 8082ug/KgNDPCB-1248 75 08/13/14 AW SW 8082ug/KgNDPCB-1254 75 08/13/14 AW SW 8082ug/KgNDPCB-1260 75 08/13/14 AW SW 8082ug/KgNDPCB-1262 75 08/13/14 AW SW 8082ug/KgNDPCB-1268 75 08/13/14 AW SW 8082ug/Kg

QA/QC Surrogates84% DCBP 08/13/14 AW 30 - 150 %%75% TCMX 08/13/14 AW 30 - 150 %%

Pesticides - SoilND4,4' -DDD 2.7 08/14/14 MH SW8081ug/KgND4,4' -DDE 2.7 08/14/14 MH SW8081ug/KgND4,4' -DDT 2.7 08/14/14 MH SW8081ug/KgNDa-BHC 1.9 08/14/14 MH SW8081ug/KgNDa-Chlordane 3.8 08/14/14 MH SW8081ug/KgNDAldrin 1.9 08/14/14 MH SW8081ug/KgNDb-BHC 1.9 08/14/14 MH SW8081ug/KgNDChlordane 23 08/14/14 MH SW8081ug/KgNDd-BHC 1.9 08/14/14 MH SW8081ug/KgNDDieldrin 1.9 08/14/14 MH SW8081ug/KgNDEndosulfan I 3.8 08/14/14 MH SW8081ug/KgNDEndosulfan II 3.8 08/14/14 MH SW8081ug/KgNDEndosulfan sulfate 3.8 08/14/14 MH SW8081ug/KgNDEndrin 1.9 08/14/14 MH SW8081ug/KgNDEndrin aldehyde 3.8 08/14/14 MH SW8081ug/KgNDEndrin ketone 1.9 08/14/14 MH SW8081ug/KgNDg-BHC 1.9 08/14/14 MH SW8081ug/KgNDg-Chlordane 3.8 08/14/14 MH SW8081ug/KgNDHeptachlor 1.9 08/14/14 MH SW8081ug/KgNDHeptachlor epoxide 1.9 08/14/14 MH SW8081ug/KgNDMethoxychlor 7.5 08/14/14 MH SW8081ug/KgNDToxaphene 190 08/14/14 MH SW8081ug/Kg

QA/QC Surrogates90% DCBP 08/14/14 MH 30 - 150 %%82% TCMX 08/14/14 MH 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 5.8 08/18/14 JLI SW8260ug/KgND1,1,1-Trichloroethane 5.8 08/18/14 JLI SW8260ug/KgND1,1,2,2-Tetrachloroethane 5.8 08/18/14 JLI SW8260ug/KgND1,1,2-Trichloroethane 5.8 08/18/14 JLI SW8260ug/KgND1,1-Dichloroethane 5.8 08/18/14 JLI SW8260ug/Kg

Page 2 of 93 Ver 1




LOD/MDL

ND1,1-Dichloroethene 5.8 08/18/14 JLI SW8260ug/KgND1,1-Dichloropropene 5.8 08/18/14 JLI SW8260ug/KgND1,2,3-Trichlorobenzene 5.8 08/18/14 JLI SW8260ug/KgND1,2,3-Trichloropropane 5.8 08/18/14 JLI SW8260ug/KgND1,2,4-Trichlorobenzene 5.8 08/18/14 JLI SW8260ug/KgND1,2,4-Trimethylbenzene 5.8 08/18/14 JLI SW8260ug/KgND1,2-Dibromo-3-chloropropane 5.8 08/18/14 JLI SW8260ug/KgND1,2-Dibromoethane 5.8 08/18/14 JLI SW8260ug/KgND1,2-Dichlorobenzene 5.8 08/18/14 JLI SW8260ug/KgND1,2-Dichloroethane 5.8 08/18/14 JLI SW8260ug/KgND1,2-Dichloropropane 5.8 08/18/14 JLI SW8260ug/KgND1,3,5-Trimethylbenzene 5.8 08/18/14 JLI SW8260ug/KgND1,3-Dichlorobenzene 5.8 08/18/14 JLI SW8260ug/KgND1,3-Dichloropropane 5.8 08/18/14 JLI SW8260ug/KgND1,4-Dichlorobenzene 5.8 08/18/14 JLI SW8260ug/KgND2,2-Dichloropropane 5.8 08/18/14 JLI SW8260ug/KgND2-Chlorotoluene 5.8 08/18/14 JLI SW8260ug/KgND2-Hexanone 29 08/18/14 JLI SW8260ug/KgND2-Isopropyltoluene 5.8 08/18/14 JLI SW8260ug/Kg 1

ND4-Chlorotoluene 5.8 08/18/14 JLI SW8260ug/KgND4-Methyl-2-pentanone 29 08/18/14 JLI SW8260ug/KgNDAcetone 29 08/18/14 JLI SW8260ug/KgNDAcrylonitrile 12 08/18/14 JLI SW8260ug/KgNDBenzene 5.8 08/18/14 JLI SW8260ug/KgNDBromobenzene 5.8 08/18/14 JLI SW8260ug/KgNDBromochloromethane 5.8 08/18/14 JLI SW8260ug/KgNDBromodichloromethane 5.8 08/18/14 JLI SW8260ug/KgNDBromoform 5.8 08/18/14 JLI SW8260ug/KgNDBromomethane 5.8 08/18/14 JLI SW8260ug/KgNDCarbon Disulfide 5.8 08/18/14 JLI SW8260ug/KgNDCarbon tetrachloride 5.8 08/18/14 JLI SW8260ug/KgNDChlorobenzene 5.8 08/18/14 JLI SW8260ug/KgNDChloroethane 5.8 08/18/14 JLI SW8260ug/KgNDChloroform 5.8 08/18/14 JLI SW8260ug/KgNDChloromethane 5.8 08/18/14 JLI SW8260ug/KgNDcis-1,2-Dichloroethene 5.8 08/18/14 JLI SW8260ug/KgNDcis-1,3-Dichloropropene 5.8 08/18/14 JLI SW8260ug/KgNDDibromochloromethane 5.8 08/18/14 JLI SW8260ug/KgNDDibromomethane 5.8 08/18/14 JLI SW8260ug/KgNDDichlorodifluoromethane 5.8 08/18/14 JLI SW8260ug/KgNDEthylbenzene 5.8 08/18/14 JLI SW8260ug/KgNDHexachlorobutadiene 5.8 08/18/14 JLI SW8260ug/KgNDIsopropylbenzene 5.8 08/18/14 JLI SW8260ug/KgNDm&p-Xylene 5.8 08/18/14 JLI SW8260ug/KgNDMethyl Ethyl Ketone 29 08/18/14 JLI SW8260ug/KgNDMethyl t-butyl ether (MTBE) 12 08/18/14 JLI SW8260ug/Kg29Methylene chloride 5.8 08/18/14 JLI SW8260ug/KgNDNaphthalene 5.8 08/18/14 JLI SW8260ug/KgNDn-Butylbenzene 5.8 08/18/14 JLI SW8260ug/Kg

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LOD/MDL

NDn-Propylbenzene 5.8 08/18/14 JLI SW8260ug/KgNDo-Xylene 5.8 08/18/14 JLI SW8260ug/KgNDp-Isopropyltoluene 5.8 08/18/14 JLI SW8260ug/KgNDsec-Butylbenzene 5.8 08/18/14 JLI SW8260ug/KgNDStyrene 5.8 08/18/14 JLI SW8260ug/KgNDtert-Butylbenzene 5.8 08/18/14 JLI SW8260ug/KgNDTetrachloroethene 5.8 08/18/14 JLI SW8260ug/KgNDTetrahydrofuran (THF) 12 08/18/14 JLI SW8260ug/Kg 1

NDToluene 5.8 08/18/14 JLI SW8260ug/KgNDTotal Xylenes 5.8 08/18/14 JLI SW8260ug/KgNDtrans-1,2-Dichloroethene 5.8 08/18/14 JLI SW8260ug/KgNDtrans-1,3-Dichloropropene 5.8 08/18/14 JLI SW8260ug/KgNDtrans-1,4-dichloro-2-butene 12 08/18/14 JLI SW8260ug/KgNDTrichloroethene 5.8 08/18/14 JLI SW8260ug/KgNDTrichlorofluoromethane 5.8 08/18/14 JLI SW8260ug/KgNDTrichlorotrifluoroethane 5.8 08/18/14 JLI SW8260ug/KgNDVinyl chloride 5.8 08/18/14 JLI SW8260ug/Kg

QA/QC Surrogates98% 1,2-dichlorobenzene-d4 08/18/14 JLI 70 - 130 %%93% Bromofluorobenzene 08/18/14 JLI 70 - 130 %%101% Dibromofluoromethane 08/18/14 JLI 70 - 130 %%93% Toluene-d8 08/18/14 JLI 70 - 130 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 270 08/13/14 DD SW 8270ug/KgND1,2,4-Trichlorobenzene 270 08/13/14 DD SW 8270ug/KgND1,2-Dichlorobenzene 270 08/13/14 DD SW 8270ug/KgND1,2-Diphenylhydrazine 380 08/13/14 DD SW 8270ug/KgND1,3-Dichlorobenzene 270 08/13/14 DD SW 8270ug/KgND1,4-Dichlorobenzene 270 08/13/14 DD SW 8270ug/KgND2,4,5-Trichlorophenol 270 08/13/14 DD SW 8270ug/KgND2,4,6-Trichlorophenol 270 08/13/14 DD SW 8270ug/KgND2,4-Dichlorophenol 270 08/13/14 DD SW 8270ug/KgND2,4-Dimethylphenol 270 08/13/14 DD SW 8270ug/KgND2,4-Dinitrophenol 610 08/13/14 DD SW 8270ug/KgND2,4-Dinitrotoluene 270 08/13/14 DD SW 8270ug/KgND2,6-Dinitrotoluene 270 08/13/14 DD SW 8270ug/KgND2-Chloronaphthalene 270 08/13/14 DD SW 8270ug/KgND2-Chlorophenol 270 08/13/14 DD SW 8270ug/KgND2-Methylnaphthalene 270 08/13/14 DD SW 8270ug/KgND2-Methylphenol (o-cresol) 270 08/13/14 DD SW 8270ug/KgND2-Nitroaniline 610 08/13/14 DD SW 8270ug/KgND2-Nitrophenol 270 08/13/14 DD SW 8270ug/KgND3&4-Methylphenol (m&p-cresol) 380 08/13/14 DD SW 8270ug/KgND3,3'-Dichlorobenzidine 270 08/13/14 DD SW 8270ug/KgND3-Nitroaniline 610 08/13/14 DD SW 8270ug/KgND4,6-Dinitro-2-methylphenol 1100 08/13/14 DD SW 8270ug/KgND4-Bromophenyl phenyl ether 380 08/13/14 DD SW 8270ug/KgND4-Chloro-3-methylphenol 270 08/13/14 DD SW 8270ug/KgND4-Chloroaniline 270 08/13/14 DD SW 8270ug/Kg

Page 4 of 93 Ver 1




LOD/MDL

ND4-Chlorophenyl phenyl ether 270 08/13/14 DD SW 8270ug/KgND4-Nitroaniline 610 08/13/14 DD SW 8270ug/KgND4-Nitrophenol 1100 08/13/14 DD SW 8270ug/KgNDAcenaphthene 270 08/13/14 DD SW 8270ug/KgNDAcenaphthylene 270 08/13/14 DD SW 8270ug/KgNDAcetophenone 270 08/13/14 DD SW 8270ug/KgNDAniline 1100 08/13/14 DD SW 8270ug/KgNDAnthracene 270 08/13/14 DD SW 8270ug/Kg820Benz(a)anthracene 270 08/13/14 DD SW 8270ug/KgNDBenzidine 450 08/13/14 DD SW 8270ug/Kg740Benzo(a)pyrene 270 08/13/14 DD SW 8270ug/Kg

1000Benzo(b)fluoranthene 270 08/13/14 DD SW 8270ug/Kg460Benzo(ghi)perylene 270 08/13/14 DD SW 8270ug/Kg300Benzo(k)fluoranthene 270 08/13/14 DD SW 8270ug/KgNDBenzoic acid 1100 08/13/14 DD SW 8270ug/Kg 1

NDBenzyl butyl phthalate 270 08/13/14 DD SW 8270ug/KgNDBis(2-chloroethoxy)methane 270 08/13/14 DD SW 8270ug/KgNDBis(2-chloroethyl)ether 380 08/13/14 DD SW 8270ug/KgNDBis(2-chloroisopropyl)ether 270 08/13/14 DD SW 8270ug/Kg 1

NDBis(2-ethylhexyl)phthalate 270 08/13/14 DD SW 8270ug/KgNDCarbazole 570 08/13/14 DD SW 8270ug/Kg880Chrysene 270 08/13/14 DD SW 8270ug/KgNDDibenz(a,h)anthracene 270 08/13/14 DD SW 8270ug/KgNDDibenzofuran 270 08/13/14 DD SW 8270ug/KgNDDiethyl phthalate 270 08/13/14 DD SW 8270ug/KgNDDimethylphthalate 270 08/13/14 DD SW 8270ug/KgNDDi-n-butylphthalate 270 08/13/14 DD SW 8270ug/KgNDDi-n-octylphthalate 270 08/13/14 DD SW 8270ug/Kg

1800Fluoranthene 270 08/13/14 DD SW 8270ug/KgNDFluorene 270 08/13/14 DD SW 8270ug/KgNDHexachlorobenzene 270 08/13/14 DD SW 8270ug/KgNDHexachlorobutadiene 270 08/13/14 DD SW 8270ug/KgNDHexachlorocyclopentadiene 270 08/13/14 DD SW 8270ug/KgNDHexachloroethane 270 08/13/14 DD SW 8270ug/Kg380Indeno(1,2,3-cd)pyrene 270 08/13/14 DD SW 8270ug/KgNDIsophorone 270 08/13/14 DD SW 8270ug/KgNDNaphthalene 270 08/13/14 DD SW 8270ug/KgNDNitrobenzene 270 08/13/14 DD SW 8270ug/KgNDN-Nitrosodimethylamine 380 08/13/14 DD SW 8270ug/KgNDN-Nitrosodi-n-propylamine 270 08/13/14 DD SW 8270ug/KgNDN-Nitrosodiphenylamine 380 08/13/14 DD SW 8270ug/KgNDPentachloronitrobenzene 380 08/13/14 DD SW 8270ug/KgNDPentachlorophenol 380 08/13/14 DD SW 8270ug/Kg830Phenanthrene 270 08/13/14 DD SW 8270ug/KgNDPhenol 270 08/13/14 DD SW 8270ug/Kg

1600Pyrene 270 08/13/14 DD SW 8270ug/KgNDPyridine 380 08/13/14 DD SW 8270ug/Kg

QA/QC Surrogates75% 2,4,6-Tribromophenol 08/13/14 DD 30 - 130 %%

Page 5 of 93 Ver 1




LOD/MDL

59% 2-Fluorobiphenyl 08/13/14 DD 30 - 130 %%67% 2-Fluorophenol 08/13/14 DD 30 - 130 %%68% Nitrobenzene-d5 08/13/14 DD 30 - 130 %%69% Phenol-d5 08/13/14 DD 30 - 130 %%87% Terphenyl-d14 08/13/14 DD 30 - 130 %%

Comments:

Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.


This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.


Phyllis Shiller, Laboratory DirectorAugust 20, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Greg Lawrence, Assistant Lab Director

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

Page 6 of 93 Ver 1



GROUND WATERGEICONSStandard408950


EC

Laboratory Data

B-1 (10-12 FT)

Phoenix ID: BG91925

08/12/148:40

15:35




Date Time



SDG ID: GBG91924


LOD/MDL

< 0.35Silver 0.35 08/14/14 EK SW6010mg/Kg8610Aluminum 52 08/15/14 LK SW6010mg/Kg< 0.7Arsenic 0.7 08/14/14 EK SW6010mg/Kg49.7Barium 0.35 08/14/14 EK SW6010mg/Kg0.49Beryllium 0.28 08/14/14 EK SW6010mg/Kg733Calcium 5.2 08/14/14 EK SW6010mg/Kg


30600Iron 52 08/15/14 LK SW6010mg/Kg< 0.06Mercury 0.06 08/13/14 MA SW-7471mg/Kg1680Potassium 5.2 08/14/14 EK SW6010mg/Kg1990Magnesium 5.2 08/14/14 EK SW6010mg/Kg525Manganese 3.5 08/15/14 LK SW6010mg/Kg49.0Sodium 5.2 08/14/14 EK SW6010mg/Kg12.9Nickel 0.35 08/14/14 EK SW6010mg/Kg7.89Lead 0.35 08/14/14 EK SW6010mg/Kg< 3.5Antimony 3.5 08/14/14 EK SW6010mg/Kg< 1.4Selenium 1.4 08/14/14 EK SW6010mg/Kg< 3.1Thallium 3.1 08/14/14 EK SW6010mg/Kg36.1Vanadium 0.35 08/14/14 EK SW6010mg/Kg42.3Zinc 0.35 08/14/14 EK SW6010mg/Kg90Percent Solid 08/12/14 I E160.3%

< 0.56Total Cyanide 0.56 08/13/14 O/E SW 9010/9012mg/KgCompletedSoil Extraction for PCB 08/12/14 BB/H SW3545CompletedSoil Extraction for Pesticide 08/12/14 BB SW3545CompletedSoil Extraction for SVOA 08/12/14 BJ/VF SW3545

Page 7 of 93 Ver 1




LOD/MDL

CompletedMercury Digestion 08/13/14 I/I SW7471CompletedTotal Metals Digest 08/12/14 CB/AG SW846 - 3050



Pesticides - SoilND4,4' -DDD 2.6 08/14/14 MH SW8081ug/KgND4,4' -DDE 2.6 08/14/14 MH SW8081ug/KgND4,4' -DDT 2.6 08/14/14 MH SW8081ug/KgNDa-BHC 1.8 08/14/14 MH SW8081ug/KgNDa-Chlordane 3.7 08/14/14 MH SW8081ug/KgNDAldrin 1.8 08/14/14 MH SW8081ug/KgNDb-BHC 1.8 08/14/14 MH SW8081ug/KgNDChlordane 22 08/14/14 MH SW8081ug/KgNDd-BHC 1.8 08/14/14 MH SW8081ug/KgNDDieldrin 1.8 08/14/14 MH SW8081ug/KgNDEndosulfan I 3.7 08/14/14 MH SW8081ug/KgNDEndosulfan II 3.7 08/14/14 MH SW8081ug/KgNDEndosulfan sulfate 3.7 08/14/14 MH SW8081ug/KgNDEndrin 1.8 08/14/14 MH SW8081ug/KgNDEndrin aldehyde 3.7 08/14/14 MH SW8081ug/KgNDEndrin ketone 1.8 08/14/14 MH SW8081ug/KgNDg-BHC 1.8 08/14/14 MH SW8081ug/KgNDg-Chlordane 3.7 08/14/14 MH SW8081ug/KgNDHeptachlor 1.8 08/14/14 MH SW8081ug/KgNDHeptachlor epoxide 1.8 08/14/14 MH SW8081ug/KgNDMethoxychlor 7.4 08/14/14 MH SW8081ug/KgNDToxaphene 180 08/14/14 MH SW8081ug/Kg

QA/QC Surrogates109% DCBP 08/14/14 MH 30 - 150 %%100% TCMX 08/14/14 MH 30 - 150 %%


Page 8 of 93 Ver 1




LOD/MDL


ND4-Chlorotoluene 5.6 08/18/14 JLI SW8260ug/KgND4-Methyl-2-pentanone 28 08/18/14 JLI SW8260ug/Kg56Acetone 28 08/18/14 JLI SW8260ug/KgNDAcrylonitrile 11 08/18/14 JLI SW8260ug/KgNDBenzene 5.6 08/18/14 JLI SW8260ug/KgNDBromobenzene 5.6 08/18/14 JLI SW8260ug/KgNDBromochloromethane 5.6 08/18/14 JLI SW8260ug/KgNDBromodichloromethane 5.6 08/18/14 JLI SW8260ug/KgNDBromoform 5.6 08/18/14 JLI SW8260ug/KgNDBromomethane 5.6 08/18/14 JLI SW8260ug/KgNDCarbon Disulfide 5.6 08/18/14 JLI SW8260ug/KgNDCarbon tetrachloride 5.6 08/18/14 JLI SW8260ug/KgNDChlorobenzene 5.6 08/18/14 JLI SW8260ug/KgNDChloroethane 5.6 08/18/14 JLI SW8260ug/KgNDChloroform 5.6 08/18/14 JLI SW8260ug/KgNDChloromethane 5.6 08/18/14 JLI SW8260ug/KgNDcis-1,2-Dichloroethene 5.6 08/18/14 JLI SW8260ug/KgNDcis-1,3-Dichloropropene 5.6 08/18/14 JLI SW8260ug/KgNDDibromochloromethane 5.6 08/18/14 JLI SW8260ug/KgNDDibromomethane 5.6 08/18/14 JLI SW8260ug/KgNDDichlorodifluoromethane 5.6 08/18/14 JLI SW8260ug/KgNDEthylbenzene 5.6 08/18/14 JLI SW8260ug/KgNDHexachlorobutadiene 5.6 08/18/14 JLI SW8260ug/KgNDIsopropylbenzene 5.6 08/18/14 JLI SW8260ug/KgNDm&p-Xylene 5.6 08/18/14 JLI SW8260ug/KgNDMethyl Ethyl Ketone 28 08/18/14 JLI SW8260ug/KgNDMethyl t-butyl ether (MTBE) 11 08/18/14 JLI SW8260ug/Kg12Methylene chloride 5.6 08/18/14 JLI SW8260ug/KgNDNaphthalene 5.6 08/18/14 JLI SW8260ug/KgNDn-Butylbenzene 5.6 08/18/14 JLI SW8260ug/Kg

Page 9 of 93 Ver 1




LOD/MDL





Page 10 of 93 Ver 1




LOD/MDL

ND4-Chlorophenyl phenyl ether 250 08/13/14 DD SW 8270ug/KgND4-Nitroaniline 580 08/13/14 DD SW 8270ug/KgND4-Nitrophenol 1100 08/13/14 DD SW 8270ug/KgNDAcenaphthene 250 08/13/14 DD SW 8270ug/KgNDAcenaphthylene 250 08/13/14 DD SW 8270ug/KgNDAcetophenone 250 08/13/14 DD SW 8270ug/KgNDAniline 1100 08/13/14 DD SW 8270ug/KgNDAnthracene 250 08/13/14 DD SW 8270ug/KgNDBenz(a)anthracene 250 08/13/14 DD SW 8270ug/KgNDBenzidine 430 08/13/14 DD SW 8270ug/KgNDBenzo(a)pyrene 250 08/13/14 DD SW 8270ug/KgNDBenzo(b)fluoranthene 250 08/13/14 DD SW 8270ug/KgNDBenzo(ghi)perylene 250 08/13/14 DD SW 8270ug/KgNDBenzo(k)fluoranthene 250 08/13/14 DD SW 8270ug/KgNDBenzoic acid 1100 08/13/14 DD SW 8270ug/Kg 1


NDBis(2-ethylhexyl)phthalate 250 08/13/14 DD SW 8270ug/KgNDCarbazole 540 08/13/14 DD SW 8270ug/KgNDChrysene 250 08/13/14 DD SW 8270ug/KgNDDibenz(a,h)anthracene 250 08/13/14 DD SW 8270ug/KgNDDibenzofuran 250 08/13/14 DD SW 8270ug/KgNDDiethyl phthalate 250 08/13/14 DD SW 8270ug/KgNDDimethylphthalate 250 08/13/14 DD SW 8270ug/KgNDDi-n-butylphthalate 250 08/13/14 DD SW 8270ug/KgNDDi-n-octylphthalate 250 08/13/14 DD SW 8270ug/KgNDFluoranthene 250 08/13/14 DD SW 8270ug/KgNDFluorene 250 08/13/14 DD SW 8270ug/KgNDHexachlorobenzene 250 08/13/14 DD SW 8270ug/KgNDHexachlorobutadiene 250 08/13/14 DD SW 8270ug/KgNDHexachlorocyclopentadiene 250 08/13/14 DD SW 8270ug/KgNDHexachloroethane 250 08/13/14 DD SW 8270ug/KgNDIndeno(1,2,3-cd)pyrene 250 08/13/14 DD SW 8270ug/KgNDIsophorone 250 08/13/14 DD SW 8270ug/KgNDNaphthalene 250 08/13/14 DD SW 8270ug/KgNDNitrobenzene 250 08/13/14 DD SW 8270ug/KgNDN-Nitrosodimethylamine 360 08/13/14 DD SW 8270ug/KgNDN-Nitrosodi-n-propylamine 250 08/13/14 DD SW 8270ug/KgNDN-Nitrosodiphenylamine 360 08/13/14 DD SW 8270ug/KgNDPentachloronitrobenzene 360 08/13/14 DD SW 8270ug/KgNDPentachlorophenol 360 08/13/14 DD SW 8270ug/KgNDPhenanthrene 250 08/13/14 DD SW 8270ug/KgNDPhenol 250 08/13/14 DD SW 8270ug/KgNDPyrene 250 08/13/14 DD SW 8270ug/KgNDPyridine 360 08/13/14 DD SW 8270ug/Kg


Page 11 of 93 Ver 1




LOD/MDL


Comments:






1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.




Page 12 of 93 Ver 1





EC

Laboratory Data

B-6 (0-2 FT)

Phoenix ID: BG91926

08/12/149:40

15:35




Date Time



SDG ID: GBG91924


LOD/MDL

NDSilver 1.0 08/14/14 EK SW6010mg/Kg8760Aluminum 50 08/15/14 LK SW6010mg/Kg5.4Arsenic 0.7 08/14/14 EK SW6010mg/Kg186Barium 0.33 08/14/14 EK SW6010mg/Kg0.42Beryllium 0.27 08/14/14 EK SW6010mg/Kg1550Calcium 5.0 08/14/14 EK SW6010mg/Kg2.74Cadmium 0.33 08/14/14 EK SW6010mg/Kg6.99Cobalt 0.33 08/14/14 EK SW6010mg/Kg58.5Chromium 0.33 08/14/14 EK SW6010mg/Kg30.3Copper 0.33 08/14/14 EK SW6010mg/kg

19100Iron 50 08/15/14 LK SW6010mg/Kg0.44Mercury 0.09 08/13/14 MA SW-7471mg/Kg994Potassium 5.0 08/14/14 EK SW6010mg/Kg

2030Magnesium 5.0 08/14/14 EK SW6010mg/Kg293Manganese 3.3 08/15/14 LK SW6010mg/Kg51.1Sodium 5.0 08/14/14 EK SW6010mg/Kg16.3Nickel 0.33 08/14/14 EK SW6010mg/Kg293Lead 3.3 08/15/14 LK SW6010mg/Kg5.4Antimony 3.3 08/14/14 LK SW6010mg/Kg

< 1.3Selenium 1.3 08/14/14 EK SW6010mg/Kg< 3.0Thallium 3.0 08/14/14 EK SW6010mg/Kg30.5Vanadium 0.33 08/14/14 EK SW6010mg/Kg652Zinc 3.3 08/15/14 LK SW6010mg/Kg89Percent Solid 08/12/14 I E160.3%


Page 13 of 93 Ver 1




LOD/MDL




Pesticides - SoilND4,4' -DDD 2.7 08/14/14 KCA SW8081ug/Kg254,4' -DDE 2.7 08/14/14 KCA SW8081ug/Kg404,4' -DDT 2.7 08/14/14 KCA SW8081ug/KgNDa-BHC 1.9 08/14/14 KCA SW8081ug/KgNDa-Chlordane 3.7 08/14/14 KCA SW8081ug/KgNDAldrin 1.9 08/14/14 KCA SW8081ug/KgNDb-BHC 1.9 08/14/14 KCA SW8081ug/KgNDChlordane 22 08/14/14 KCA SW8081ug/KgNDd-BHC 1.9 08/14/14 KCA SW8081ug/KgNDDieldrin 1.9 08/14/14 KCA SW8081ug/KgNDEndosulfan I 3.7 08/14/14 KCA SW8081ug/KgNDEndosulfan II 3.7 08/14/14 KCA SW8081ug/KgNDEndosulfan sulfate 3.7 08/14/14 KCA SW8081ug/KgNDEndrin 1.9 08/14/14 KCA SW8081ug/KgNDEndrin aldehyde 3.7 08/14/14 KCA SW8081ug/KgNDEndrin ketone 1.9 08/14/14 KCA SW8081ug/KgNDg-BHC 1.9 08/14/14 KCA SW8081ug/KgNDg-Chlordane 3.7 08/14/14 KCA SW8081ug/KgNDHeptachlor 1.9 08/14/14 KCA SW8081ug/KgNDHeptachlor epoxide 1.9 08/14/14 KCA SW8081ug/KgNDMethoxychlor 7.4 08/14/14 KCA SW8081ug/KgNDToxaphene 190 08/14/14 KCA SW8081ug/Kg

QA/QC Surrogates140% DCBP 08/14/14 KCA 30 - 150 %%93% TCMX 08/14/14 KCA 30 - 150 %%


Page 14 of 93 Ver 1




LOD/MDL



Page 15 of 93 Ver 1




LOD/MDL





Page 16 of 93 Ver 1




LOD/MDL

ND4-Chlorophenyl phenyl ether 260 08/13/14 DD SW 8270ug/KgND4-Nitroaniline 600 08/13/14 DD SW 8270ug/KgND4-Nitrophenol 1100 08/13/14 DD SW 8270ug/KgNDAcenaphthene 260 08/13/14 DD SW 8270ug/KgNDAcenaphthylene 260 08/13/14 DD SW 8270ug/KgNDAcetophenone 260 08/13/14 DD SW 8270ug/KgNDAniline 1100 08/13/14 DD SW 8270ug/KgNDAnthracene 260 08/13/14 DD SW 8270ug/KgNDBenz(a)anthracene 260 08/13/14 DD SW 8270ug/KgNDBenzidine 450 08/13/14 DD SW 8270ug/KgNDBenzo(a)pyrene 260 08/13/14 DD SW 8270ug/Kg280Benzo(b)fluoranthene 260 08/13/14 DD SW 8270ug/KgNDBenzo(ghi)perylene 260 08/13/14 DD SW 8270ug/KgNDBenzo(k)fluoranthene 260 08/13/14 DD SW 8270ug/KgNDBenzoic acid 1100 08/13/14 DD SW 8270ug/Kg 1


NDBis(2-ethylhexyl)phthalate 260 08/13/14 DD SW 8270ug/KgNDCarbazole 560 08/13/14 DD SW 8270ug/KgNDChrysene 260 08/13/14 DD SW 8270ug/KgNDDibenz(a,h)anthracene 260 08/13/14 DD SW 8270ug/KgNDDibenzofuran 260 08/13/14 DD SW 8270ug/KgNDDiethyl phthalate 260 08/13/14 DD SW 8270ug/KgNDDimethylphthalate 260 08/13/14 DD SW 8270ug/KgNDDi-n-butylphthalate 260 08/13/14 DD SW 8270ug/KgNDDi-n-octylphthalate 260 08/13/14 DD SW 8270ug/Kg330Fluoranthene 260 08/13/14 DD SW 8270ug/KgNDFluorene 260 08/13/14 DD SW 8270ug/KgNDHexachlorobenzene 260 08/13/14 DD SW 8270ug/KgNDHexachlorobutadiene 260 08/13/14 DD SW 8270ug/KgNDHexachlorocyclopentadiene 260 08/13/14 DD SW 8270ug/KgNDHexachloroethane 260 08/13/14 DD SW 8270ug/KgNDIndeno(1,2,3-cd)pyrene 260 08/13/14 DD SW 8270ug/KgNDIsophorone 260 08/13/14 DD SW 8270ug/KgNDNaphthalene 260 08/13/14 DD SW 8270ug/KgNDNitrobenzene 260 08/13/14 DD SW 8270ug/KgNDN-Nitrosodimethylamine 370 08/13/14 DD SW 8270ug/KgNDN-Nitrosodi-n-propylamine 260 08/13/14 DD SW 8270ug/KgNDN-Nitrosodiphenylamine 370 08/13/14 DD SW 8270ug/KgNDPentachloronitrobenzene 370 08/13/14 DD SW 8270ug/KgNDPentachlorophenol 370 08/13/14 DD SW 8270ug/KgNDPhenanthrene 260 08/13/14 DD SW 8270ug/KgNDPhenol 260 08/13/14 DD SW 8270ug/Kg280Pyrene 260 08/13/14 DD SW 8270ug/KgNDPyridine 370 08/13/14 DD SW 8270ug/Kg


Page 17 of 93 Ver 1




LOD/MDL


Comments:










Page 18 of 93 Ver 1





EC

Laboratory Data

B-6 (10-12 FT)

Phoenix ID: BG91927

08/12/1410:0015:35




Date Time



SDG ID: GBG91924


LOD/MDL




< 0.57Total Cyanide 0.57 08/13/14 O/E SW 9010/9012mg/KgCompletedSoil Extraction for PCB 08/12/14 BB/H SW3545CompletedSoil Extraction for Pesticide 08/12/14 BB SW3545CompletedSoil Extraction for SVOA 08/14/14 JJ/VF SW3545

Page 19 of 93 Ver 1




LOD/MDL




Pesticides - SoilND4,4' -DDD 2.7 08/14/14 KCA SW8081ug/KgND4,4' -DDE 2.7 08/14/14 KCA SW8081ug/KgND4,4' -DDT 2.7 08/14/14 KCA SW8081ug/KgNDa-BHC 1.8 08/14/14 KCA SW8081ug/KgNDa-Chlordane 3.7 08/14/14 KCA SW8081ug/KgNDAldrin 1.8 08/14/14 KCA SW8081ug/KgNDb-BHC 1.8 08/14/14 KCA SW8081ug/KgNDChlordane 22 08/14/14 KCA SW8081ug/KgNDd-BHC 1.8 08/14/14 KCA SW8081ug/KgNDDieldrin 1.8 08/14/14 KCA SW8081ug/KgNDEndosulfan I 3.7 08/14/14 KCA SW8081ug/KgNDEndosulfan II 3.7 08/14/14 KCA SW8081ug/KgNDEndosulfan sulfate 3.7 08/14/14 KCA SW8081ug/KgNDEndrin 1.8 08/14/14 KCA SW8081ug/KgNDEndrin aldehyde 3.7 08/14/14 KCA SW8081ug/KgNDEndrin ketone 1.8 08/14/14 KCA SW8081ug/KgNDg-BHC 1.8 08/14/14 KCA SW8081ug/KgNDg-Chlordane 3.7 08/14/14 KCA SW8081ug/KgNDHeptachlor 1.8 08/14/14 KCA SW8081ug/KgNDHeptachlor epoxide 1.8 08/14/14 KCA SW8081ug/KgNDMethoxychlor 7.4 08/14/14 KCA SW8081ug/KgNDToxaphene 180 08/14/14 KCA SW8081ug/Kg



Page 20 of 93 Ver 1




LOD/MDL



Page 21 of 93 Ver 1




LOD/MDL





Page 22 of 93 Ver 1




LOD/MDL





Page 23 of 93 Ver 1




LOD/MDL


Comments:










Page 24 of 93 Ver 1



SOLIDGEICONSStandard408950


EC

Laboratory Data

B-5 (0-2 FT)

Phoenix ID: BG91928

08/12/1410:5015:35




Date Time



SDG ID: GBG91924


LOD/MDL

< 0.38Silver 0.38 08/14/14 EK SW6010mg/Kg14000Aluminum 57 08/15/14 LK SW6010mg/Kg

5.6Arsenic 0.8 08/14/14 EK SW6010mg/Kg116Barium 0.38 08/14/14 EK SW6010mg/Kg0.51Beryllium 0.30 08/14/14 EK SW6010mg/Kg1550Calcium 5.7 08/14/14 EK SW6010mg/Kg


22500Iron 57 08/15/14 LK SW6010mg/Kg1.04Mercury 0.07 08/13/14 MA SW-7471mg/Kg1150Potassium 5.7 08/14/14 EK SW6010mg/Kg2670Magnesium 5.7 08/14/14 EK SW6010mg/Kg258Manganese 3.8 08/15/14 LK SW6010mg/Kg67.4Sodium 5.7 08/14/14 EK SW6010mg/Kg14.0Nickel 0.38 08/14/14 EK SW6010mg/Kg96.9Lead 0.38 08/14/14 EK SW6010mg/Kg< 3.8Antimony 3.8 08/14/14 EK SW6010mg/Kg< 1.5Selenium 1.5 08/14/14 EK SW6010mg/Kg< 3.4Thallium 3.4 08/14/14 EK SW6010mg/Kg30.6Vanadium 0.38 08/14/14 EK SW6010mg/Kg88.7Zinc 0.38 08/14/14 EK SW6010mg/Kg82Percent Solid 08/12/14 I E160.3%


Page 25 of 93 Ver 1




LOD/MDL







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LOD/MDL



Page 27 of 93 Ver 1




LOD/MDL





Page 28 of 93 Ver 1




LOD/MDL





Page 29 of 93 Ver 1




LOD/MDL


Comments:










Page 30 of 93 Ver 1





EC

Laboratory Data

B-5 (10-12 FT)

Phoenix ID: BG91929

08/12/1411:2015:35




Date Time



SDG ID: GBG91924


LOD/MDL





Page 31 of 93 Ver 1




LOD/MDL







Page 32 of 93 Ver 1




LOD/MDL



Page 33 of 93 Ver 1




LOD/MDL





Page 34 of 93 Ver 1




LOD/MDL





Page 35 of 93 Ver 1




LOD/MDL


Comments:










Page 36 of 93 Ver 1





EC

Laboratory Data

B-3 (0-2 FT)

Phoenix ID: BG91930

08/12/1411:3015:35




Date Time



SDG ID: GBG91924


LOD/MDL

< 0.40Silver 0.40 08/14/14 EK SW6010mg/Kg8150Aluminum 60 08/15/14 LK SW6010mg/Kg3.2Arsenic 0.8 08/14/14 EK SW6010mg/Kg137Barium 0.40 08/14/14 EK SW6010mg/Kg0.44Beryllium 0.32 08/14/14 EK SW6010mg/Kg2750Calcium 6.0 08/14/14 EK SW6010mg/Kg0.62Cadmium 0.40 08/14/14 EK SW6010mg/Kg8.26Cobalt 0.40 08/14/14 EK SW6010mg/Kg20.9Chromium 0.40 08/14/14 EK SW6010mg/Kg27.7Copper 0.40 08/14/14 EK SW6010mg/kg

23100Iron 60 08/15/14 LK SW6010mg/Kg< 0.07Mercury 0.07 08/13/14 MA SW-7471mg/Kg1260Potassium 6.0 08/14/14 EK SW6010mg/Kg1870Magnesium 6.0 08/14/14 EK SW6010mg/Kg544Manganese 4.0 08/15/14 LK SW6010mg/Kg67.6Sodium 6.0 08/14/14 EK SW6010mg/Kg14.2Nickel 0.40 08/14/14 EK SW6010mg/Kg206Lead 4.0 08/15/14 LK SW6010mg/Kg

< 4.0Antimony 4.0 08/14/14 EK SW6010mg/Kg< 1.6Selenium 1.6 08/14/14 EK SW6010mg/Kg< 3.6Thallium 3.6 08/14/14 EK SW6010mg/Kg33.7Vanadium 0.40 08/14/14 EK SW6010mg/Kg126Zinc 0.40 08/14/14 EK SW6010mg/Kg85Percent Solid 08/12/14 I E160.3%


Page 37 of 93 Ver 1




LOD/MDL







Page 38 of 93 Ver 1




LOD/MDL



Page 39 of 93 Ver 1




LOD/MDL





Page 40 of 93 Ver 1




LOD/MDL

ND4-Chlorophenyl phenyl ether 270 08/13/14 DD SW 8270ug/KgND4-Nitroaniline 620 08/13/14 DD SW 8270ug/KgND4-Nitrophenol 1100 08/13/14 DD SW 8270ug/KgNDAcenaphthene 270 08/13/14 DD SW 8270ug/KgNDAcenaphthylene 270 08/13/14 DD SW 8270ug/KgNDAcetophenone 270 08/13/14 DD SW 8270ug/KgNDAniline 1100 08/13/14 DD SW 8270ug/Kg690Anthracene 270 08/13/14 DD SW 8270ug/Kg

2800Benz(a)anthracene 270 08/13/14 DD SW 8270ug/KgNDBenzidine 470 08/13/14 DD SW 8270ug/Kg

2600Benzo(a)pyrene 270 08/13/14 DD SW 8270ug/Kg3300Benzo(b)fluoranthene 270 08/13/14 DD SW 8270ug/Kg1100Benzo(ghi)perylene 270 08/13/14 DD SW 8270ug/Kg1200Benzo(k)fluoranthene 270 08/13/14 DD SW 8270ug/KgNDBenzoic acid 1100 08/13/14 DD SW 8270ug/Kg 1


NDBis(2-ethylhexyl)phthalate 270 08/13/14 DD SW 8270ug/KgNDCarbazole 590 08/13/14 DD SW 8270ug/Kg

2900Chrysene 270 08/13/14 DD SW 8270ug/KgNDDibenz(a,h)anthracene 270 08/13/14 DD SW 8270ug/KgNDDibenzofuran 270 08/13/14 DD SW 8270ug/KgNDDiethyl phthalate 270 08/13/14 DD SW 8270ug/KgNDDimethylphthalate 270 08/13/14 DD SW 8270ug/KgNDDi-n-butylphthalate 270 08/13/14 DD SW 8270ug/KgNDDi-n-octylphthalate 270 08/13/14 DD SW 8270ug/Kg

6100Fluoranthene 270 08/13/14 DD SW 8270ug/KgNDFluorene 270 08/13/14 DD SW 8270ug/KgNDHexachlorobenzene 270 08/13/14 DD SW 8270ug/KgNDHexachlorobutadiene 270 08/13/14 DD SW 8270ug/KgNDHexachlorocyclopentadiene 270 08/13/14 DD SW 8270ug/KgNDHexachloroethane 270 08/13/14 DD SW 8270ug/Kg

1100Indeno(1,2,3-cd)pyrene 270 08/13/14 DD SW 8270ug/KgNDIsophorone 270 08/13/14 DD SW 8270ug/KgNDNaphthalene 270 08/13/14 DD SW 8270ug/KgNDNitrobenzene 270 08/13/14 DD SW 8270ug/KgNDN-Nitrosodimethylamine 390 08/13/14 DD SW 8270ug/KgNDN-Nitrosodi-n-propylamine 270 08/13/14 DD SW 8270ug/KgNDN-Nitrosodiphenylamine 390 08/13/14 DD SW 8270ug/KgNDPentachloronitrobenzene 390 08/13/14 DD SW 8270ug/KgNDPentachlorophenol 390 08/13/14 DD SW 8270ug/Kg

3800Phenanthrene 270 08/13/14 DD SW 8270ug/KgNDPhenol 270 08/13/14 DD SW 8270ug/Kg



Page 41 of 93 Ver 1




LOD/MDL


Comments:










Page 42 of 93 Ver 1





EC

Laboratory Data

B-3 (10-12 FT)

Phoenix ID: BG91931

08/12/1411:4015:35




Date Time



SDG ID: GBG91924


LOD/MDL





Page 43 of 93 Ver 1




LOD/MDL







Page 44 of 93 Ver 1




LOD/MDL



Page 45 of 93 Ver 1




LOD/MDL





Page 46 of 93 Ver 1




LOD/MDL





Page 47 of 93 Ver 1




LOD/MDL


Comments:










Page 48 of 93 Ver 1





EC

Laboratory Data

B-2 (0-2 FT)

Phoenix ID: BG91932

08/12/1414:1015:35




Date Time



SDG ID: GBG91924


LOD/MDL






Page 49 of 93 Ver 1




LOD/MDL







Page 50 of 93 Ver 1




LOD/MDL


ND4-Chlorotoluene 6.5 08/18/14 JLI SW8260ug/KgND4-Methyl-2-pentanone 32 08/18/14 JLI SW8260ug/KgNDAcetone 32 08/18/14 JLI SW8260ug/KgNDAcrylonitrile 13 08/18/14 JLI SW8260ug/KgNDBenzene 6.5 08/18/14 JLI SW8260ug/KgNDBromobenzene 6.5 08/18/14 JLI SW8260ug/KgNDBromochloromethane 6.5 08/18/14 JLI SW8260ug/KgNDBromodichloromethane 6.5 08/18/14 JLI SW8260ug/KgNDBromoform 6.5 08/18/14 JLI SW8260ug/KgNDBromomethane 6.5 08/18/14 JLI SW8260ug/KgNDCarbon Disulfide 6.5 08/18/14 JLI SW8260ug/KgNDCarbon tetrachloride 6.5 08/18/14 JLI SW8260ug/KgNDChlorobenzene 6.5 08/18/14 JLI SW8260ug/KgNDChloroethane 6.5 08/18/14 JLI SW8260ug/KgNDChloroform 6.5 08/18/14 JLI SW8260ug/KgNDChloromethane 6.5 08/18/14 JLI SW8260ug/KgNDcis-1,2-Dichloroethene 6.5 08/18/14 JLI SW8260ug/KgNDcis-1,3-Dichloropropene 6.5 08/18/14 JLI SW8260ug/KgNDDibromochloromethane 6.5 08/18/14 JLI SW8260ug/KgNDDibromomethane 6.5 08/18/14 JLI SW8260ug/KgNDDichlorodifluoromethane 6.5 08/18/14 JLI SW8260ug/KgNDEthylbenzene 6.5 08/18/14 JLI SW8260ug/KgNDHexachlorobutadiene 6.5 08/18/14 JLI SW8260ug/KgNDIsopropylbenzene 6.5 08/18/14 JLI SW8260ug/KgNDm&p-Xylene 6.5 08/18/14 JLI SW8260ug/KgNDMethyl Ethyl Ketone 32 08/18/14 JLI SW8260ug/KgNDMethyl t-butyl ether (MTBE) 13 08/18/14 JLI SW8260ug/Kg8.7Methylene chloride 6.5 08/18/14 JLI SW8260ug/KgNDNaphthalene 6.5 08/18/14 JLI SW8260ug/KgNDn-Butylbenzene 6.5 08/18/14 JLI SW8260ug/Kg

Page 51 of 93 Ver 1




LOD/MDL





Page 52 of 93 Ver 1




LOD/MDL





Page 53 of 93 Ver 1




LOD/MDL


Comments:










Page 54 of 93 Ver 1





EC

Laboratory Data

B-2 (10-12 FT)

Phoenix ID: BG91933

08/12/1414:3015:35




Date Time



SDG ID: GBG91924


LOD/MDL

< 0.41Silver 0.41 08/14/14 EK SW6010mg/Kg7910Aluminum 61 08/15/14 LK SW6010mg/Kg2.4Arsenic 0.8 08/14/14 EK SW6010mg/Kg

20.7Barium 0.41 08/14/14 EK SW6010mg/Kg0.51Beryllium 0.32 08/14/14 EK SW6010mg/Kg773Calcium 6.1 08/14/14 EK SW6010mg/Kg




Page 55 of 93 Ver 1




LOD/MDL







Page 56 of 93 Ver 1




LOD/MDL



Page 57 of 93 Ver 1




LOD/MDL





Page 58 of 93 Ver 1




LOD/MDL





Page 59 of 93 Ver 1




LOD/MDL


Comments:










Page 60 of 93 Ver 1





EC

Laboratory Data

B-4 (0-2 FT)

Phoenix ID: BG91934

08/12/1413:3515:35




Date Time



SDG ID: GBG91924


LOD/MDL

NDSilver 1.0 08/14/14 EK SW6010mg/Kg8790Aluminum 58 08/15/14 LK SW6010mg/Kg15.5Arsenic 0.8 08/14/14 EK SW6010mg/Kg480Barium 0.39 08/14/14 EK SW6010mg/Kg0.56Beryllium 0.31 08/14/14 EK SW6010mg/Kg5220Calcium 5.8 08/14/14 EK SW6010mg/Kg4.47Cadmium 0.39 08/14/14 EK SW6010mg/Kg9.30Cobalt 0.39 08/14/14 EK SW6010mg/Kg48.9Chromium 0.39 08/14/14 EK SW6010mg/Kg135Copper 0.39 08/14/14 EK SW6010mg/kg

24000Iron 58 08/15/14 LK SW6010mg/Kg0.82Mercury 0.09 08/13/14 MA SW-7471mg/Kg793Potassium 5.8 08/14/14 EK SW6010mg/Kg

2030Magnesium 5.8 08/14/14 EK SW6010mg/Kg316Manganese 3.9 08/15/14 LK SW6010mg/Kg221Sodium 5.8 08/14/14 EK SW6010mg/Kg37.8Nickel 0.39 08/14/14 EK SW6010mg/Kg1230Lead 3.9 08/15/14 LK SW6010mg/Kg5.8Antimony 3.9 08/14/14 LK SW6010mg/Kg

< 1.5Selenium 1.5 08/14/14 EK SW6010mg/Kg< 3.5Thallium 3.5 08/14/14 EK SW6010mg/Kg80.6Vanadium 0.39 08/14/14 EK SW6010mg/Kg538Zinc 3.9 08/15/14 LK SW6010mg/Kg79Percent Solid 08/12/14 I E160.3%

2.09Total Cyanide 0.63 08/13/14 O/E SW 9010/9012mg/KgCompletedSoil Extraction for PCB 08/12/14 BB/H SW3545CompletedSoil Extraction for Pesticide 08/12/14 BB SW3545CompletedSoil Extraction for SVOA 08/12/14 BJ/VF SW3545

Page 61 of 93 Ver 1




LOD/MDL


Polychlorinated BiphenylsNDPCB-1016 82 08/15/14 AW SW 8082ug/KgNDPCB-1221 82 08/15/14 AW SW 8082ug/KgNDPCB-1232 82 08/15/14 AW SW 8082ug/KgNDPCB-1242 82 08/15/14 AW SW 8082ug/KgNDPCB-1248 82 08/15/14 AW SW 8082ug/KgNDPCB-1254 82 08/15/14 AW SW 8082ug/Kg270PCB-1260 82 08/15/14 AW SW 8082ug/KgNDPCB-1262 82 08/15/14 AW SW 8082ug/KgNDPCB-1268 82 08/15/14 AW SW 8082ug/Kg


Pesticides - SoilND4,4' -DDD 3.0 08/14/14 KCA SW8081ug/KgND4,4' -DDE 3.0 08/14/14 KCA SW8081ug/Kg144,4' -DDT 3.0 08/14/14 KCA SW8081ug/KgNDa-BHC 2.1 08/14/14 KCA SW8081ug/KgNDa-Chlordane 4.1 08/14/14 KCA SW8081ug/KgNDAldrin 2.1 08/14/14 KCA SW8081ug/KgNDb-BHC 5.0 08/14/14 KCA SW8081ug/KgNDChlordane 25 08/14/14 KCA SW8081ug/KgNDd-BHC 6.0 08/14/14 KCA SW8081ug/KgNDDieldrin 2.1 08/14/14 KCA SW8081ug/KgNDEndosulfan I 4.1 08/14/14 KCA SW8081ug/KgNDEndosulfan II 4.1 08/14/14 KCA SW8081ug/KgNDEndosulfan sulfate 25 08/14/14 KCA SW8081ug/KgNDEndrin 2.1 08/14/14 KCA SW8081ug/KgNDEndrin aldehyde 4.1 08/14/14 KCA SW8081ug/KgNDEndrin ketone 30 08/14/14 KCA SW8081ug/KgNDg-BHC 2.1 08/14/14 KCA SW8081ug/KgNDg-Chlordane 4.1 08/14/14 KCA SW8081ug/KgNDHeptachlor 5.0 08/14/14 KCA SW8081ug/KgNDHeptachlor epoxide 5.0 08/14/14 KCA SW8081ug/KgNDMethoxychlor 8.2 08/14/14 KCA SW8081ug/KgNDToxaphene 210 08/14/14 KCA SW8081ug/Kg

QA/QC SurrogatesInterference% DCBP 08/14/14 KCA 30 - 150 %%

66% TCMX 08/14/14 KCA 30 - 150 %%


Page 62 of 93 Ver 1




LOD/MDL

ND1,1-Dichloroethene 6.3 08/18/14 JLI SW8260ug/KgND1,1-Dichloropropene 6.3 08/18/14 JLI SW8260ug/KgND1,2,3-Trichlorobenzene 320 08/18/14 JLI SW8260ug/KgND1,2,3-Trichloropropane 320 08/18/14 JLI SW8260ug/KgND1,2,4-Trichlorobenzene 320 08/18/14 JLI SW8260ug/KgND1,2,4-Trimethylbenzene 320 08/18/14 JLI SW8260ug/KgND1,2-Dibromo-3-chloropropane 320 08/18/14 JLI SW8260ug/KgND1,2-Dibromoethane 6.3 08/18/14 JLI SW8260ug/KgND1,2-Dichlorobenzene 320 08/18/14 JLI SW8260ug/KgND1,2-Dichloroethane 6.3 08/18/14 JLI SW8260ug/KgND1,2-Dichloropropane 6.3 08/18/14 JLI SW8260ug/KgND1,3,5-Trimethylbenzene 320 08/18/14 JLI SW8260ug/KgND1,3-Dichlorobenzene 320 08/18/14 JLI SW8260ug/KgND1,3-Dichloropropane 6.3 08/18/14 JLI SW8260ug/KgND1,4-Dichlorobenzene 320 08/18/14 JLI SW8260ug/KgND2,2-Dichloropropane 6.3 08/18/14 JLI SW8260ug/KgND2-Chlorotoluene 320 08/18/14 JLI SW8260ug/KgND2-Hexanone 32 08/18/14 JLI SW8260ug/KgND2-Isopropyltoluene 320 08/18/14 JLI SW8260ug/Kg 1

ND4-Chlorotoluene 320 08/18/14 JLI SW8260ug/KgND4-Methyl-2-pentanone 32 08/18/14 JLI SW8260ug/KgNDAcetone 32 08/18/14 JLI SW8260ug/KgNDAcrylonitrile 13 08/18/14 JLI SW8260ug/KgNDBenzene 6.3 08/18/14 JLI SW8260ug/KgNDBromobenzene 320 08/18/14 JLI SW8260ug/KgNDBromochloromethane 6.3 08/18/14 JLI SW8260ug/KgNDBromodichloromethane 6.3 08/18/14 JLI SW8260ug/KgNDBromoform 6.3 08/18/14 JLI SW8260ug/KgNDBromomethane 6.3 08/18/14 JLI SW8260ug/KgNDCarbon Disulfide 6.3 08/18/14 JLI SW8260ug/KgNDCarbon tetrachloride 6.3 08/18/14 JLI SW8260ug/KgNDChlorobenzene 6.3 08/18/14 JLI SW8260ug/KgNDChloroethane 6.3 08/18/14 JLI SW8260ug/KgNDChloroform 6.3 08/18/14 JLI SW8260ug/KgNDChloromethane 6.3 08/18/14 JLI SW8260ug/KgNDcis-1,2-Dichloroethene 6.3 08/18/14 JLI SW8260ug/KgNDcis-1,3-Dichloropropene 6.3 08/18/14 JLI SW8260ug/KgNDDibromochloromethane 6.3 08/18/14 JLI SW8260ug/KgNDDibromomethane 6.3 08/18/14 JLI SW8260ug/KgNDDichlorodifluoromethane 6.3 08/18/14 JLI SW8260ug/KgNDEthylbenzene 6.3 08/18/14 JLI SW8260ug/KgNDHexachlorobutadiene 320 08/18/14 JLI SW8260ug/KgNDIsopropylbenzene 320 08/18/14 JLI SW8260ug/KgNDm&p-Xylene 6.3 08/18/14 JLI SW8260ug/KgNDMethyl Ethyl Ketone 32 08/18/14 JLI SW8260ug/KgNDMethyl t-butyl ether (MTBE) 13 08/18/14 JLI SW8260ug/Kg53Methylene chloride 6.3 08/18/14 JLI SW8260ug/KgNDNaphthalene 320 08/18/14 JLI SW8260ug/KgNDn-Butylbenzene 320 08/18/14 JLI SW8260ug/Kg

Page 63 of 93 Ver 1




LOD/MDL

NDn-Propylbenzene 320 08/18/14 JLI SW8260ug/KgNDo-Xylene 6.3 08/18/14 JLI SW8260ug/KgNDp-Isopropyltoluene 320 08/18/14 JLI SW8260ug/KgNDsec-Butylbenzene 320 08/18/14 JLI SW8260ug/KgNDStyrene 6.3 08/18/14 JLI SW8260ug/KgNDtert-Butylbenzene 320 08/18/14 JLI SW8260ug/KgNDTetrachloroethene 6.3 08/18/14 JLI SW8260ug/KgNDTetrahydrofuran (THF) 13 08/18/14 JLI SW8260ug/Kg 1




Page 64 of 93 Ver 1




LOD/MDL

ND4-Chlorophenyl phenyl ether 1500 08/13/14 DD SW 8270ug/KgND4-Nitroaniline 3400 08/13/14 DD SW 8270ug/KgND4-Nitrophenol 6100 08/13/14 DD SW 8270ug/Kg

1900Acenaphthene 1500 08/13/14 DD SW 8270ug/Kg3300Acenaphthylene 1500 08/13/14 DD SW 8270ug/KgNDAcetophenone 1500 08/13/14 DD SW 8270ug/KgNDAniline 6100 08/13/14 DD SW 8270ug/Kg

7800Anthracene 1500 08/13/14 DD SW 8270ug/Kg28000Benz(a)anthracene 1500 08/13/14 DD SW 8270ug/Kg

NDBenzidine 2500 08/13/14 DD SW 8270ug/Kg20000Benzo(a)pyrene 1500 08/13/14 DD SW 8270ug/Kg28000Benzo(b)fluoranthene 1500 08/13/14 DD SW 8270ug/Kg8000Benzo(ghi)perylene 1500 08/13/14 DD SW 8270ug/Kg8500Benzo(k)fluoranthene 1500 08/13/14 DD SW 8270ug/KgNDBenzoic acid 6100 08/13/14 DD SW 8270ug/Kg 1


NDBis(2-ethylhexyl)phthalate 1500 08/13/14 DD SW 8270ug/Kg4500Carbazole 3200 08/13/14 DD SW 8270ug/Kg24000Chrysene 1500 08/13/14 DD SW 8270ug/Kg

NDDibenz(a,h)anthracene 1500 08/13/14 DD SW 8270ug/Kg2000Dibenzofuran 1500 08/13/14 DD SW 8270ug/KgNDDiethyl phthalate 1500 08/13/14 DD SW 8270ug/KgNDDimethylphthalate 1500 08/13/14 DD SW 8270ug/KgNDDi-n-butylphthalate 1500 08/13/14 DD SW 8270ug/KgNDDi-n-octylphthalate 1500 08/13/14 DD SW 8270ug/Kg

76000Fluoranthene 7400 08/14/14 DD SW 8270ug/Kg3200Fluorene 1500 08/13/14 DD SW 8270ug/KgNDHexachlorobenzene 1500 08/13/14 DD SW 8270ug/KgNDHexachlorobutadiene 1500 08/13/14 DD SW 8270ug/KgNDHexachlorocyclopentadiene 1500 08/13/14 DD SW 8270ug/KgNDHexachloroethane 1500 08/13/14 DD SW 8270ug/Kg

8400Indeno(1,2,3-cd)pyrene 1500 08/13/14 DD SW 8270ug/KgNDIsophorone 1500 08/13/14 DD SW 8270ug/KgNDNaphthalene 1500 08/13/14 DD SW 8270ug/KgNDNitrobenzene 1500 08/13/14 DD SW 8270ug/KgNDN-Nitrosodimethylamine 2100 08/13/14 DD SW 8270ug/KgNDN-Nitrosodi-n-propylamine 1500 08/13/14 DD SW 8270ug/KgNDN-Nitrosodiphenylamine 2100 08/13/14 DD SW 8270ug/KgNDPentachloronitrobenzene 2100 08/13/14 DD SW 8270ug/KgNDPentachlorophenol 2100 08/13/14 DD SW 8270ug/Kg

45000Phenanthrene 7400 08/14/14 DD SW 8270ug/KgNDPhenol 1500 08/13/14 DD SW 8270ug/Kg



Page 65 of 93 Ver 1




LOD/MDL


Comments:




Volatile Comment:There was a suppression of the last internal standard in the low level analysis, all affected compounds are reported from the methanol preserved high level analysis which did not exhibit this interference.







Page 66 of 93 Ver 1





EC

Laboratory Data

B-4 (10-12 FT)

Phoenix ID: BG91935

08/12/1413:4515:35




Date Time



SDG ID: GBG91924


LOD/MDL






Page 67 of 93 Ver 1




LOD/MDL







Page 68 of 93 Ver 1




LOD/MDL



Page 69 of 93 Ver 1




LOD/MDL





Page 70 of 93 Ver 1




LOD/MDL





Page 71 of 93 Ver 1




LOD/MDL


Comments:










Page 72 of 93 Ver 1





EC

Laboratory Data

GW-1

Phoenix ID: BG91936

08/12/149:00

15:35




Date Time



SDG ID: GBG91924


LOD/MDL

< 0.005Silver 0.005 08/16/14 LK SW6010mg/L579Aluminum 1.0 08/16/14 EK SW6010mg/L

0.498Arsenic 0.020 08/16/14 LK SW6010mg/L9.96Barium 0.20 08/16/14 EK SW6010mg/L0.031Beryllium 0.005 08/16/14 LK SW6010mg/L881Calcium 0.10 08/18/14 EK SW6010mg/L

0.017Cadmium 0.005 08/16/14 LK SW6010mg/L0.700Cobalt 0.010 08/16/14 LK SW6010mg/L2.66Chromium 0.10 08/16/14 EK SW6010mg/L2.16Copper 0.50 08/16/14 EK SW6010mg/L

< 0.001Silver (Dissolved) 0.001 08/13/14 EK SW6010mg/L0.13Aluminum (Dissolved) 0.01 08/14/14 LK SW6010mg/L

< 0.004Arsenic (Dissolved) 0.004 08/13/14 EK SW6010mg/L0.049Barium (Dissolved) 0.002 08/13/14 EK SW6010mg/L

< 0.001Beryllium (Dissolved) 0.001 08/13/14 EK SW6010mg/L71.3Calcium (Dissolved) 0.01 08/13/14 EK SW6010mg/L

< 0.001Cadmium (Dissolved) 0.001 08/13/14 EK SW6010mg/L0.001Cobalt (Dissolved) 0.001 08/13/14 EK SW6010mg/L

< 0.001Chromium (Dissolved) 0.001 08/13/14 EK SW6010mg/L< 0.005Copper (Dissolved) 0.005 08/13/14 EK SW6010mg/L0.093Iron (Dissolved) 0.011 08/13/14 EK SW6010mg/L

< 0.0002Mercury (Dissolved) 0.0002 08/14/14 MA SW7470mg/L8.1Potassium (Dissolved) 0.1 08/13/14 EK SW6010mg/L

9.94Magnesium (Dissolved) 0.01 08/13/14 EK SW6010mg/L0.823Manganese (Dissolved) 0.001 08/13/14 EK SW6010mg/L55.8Sodium (Dissolved) 0.11 08/13/14 EK SW6010mg/L0.004Nickel (Dissolved) 0.001 08/13/14 EK SW6010mg/L

< 0.002Lead (Dissolved) 0.002 08/13/14 EK SW6010mg/L

Page 73 of 93 Ver 1

GW-1Phoenix I.D.: BG91936



LOD/MDL

< 0.003Antimony (Dissolved) 0.003 08/13/14 EK SW6010mg/L< 0.002Selenium (Dissolved) 0.002 08/12/14 R/T SW6010mg/L

< 0.0005Thallium (Dissolved) 0.0005 08/13/14 RS SW7010mg/L< 0.002Vanadium (Dissolved) 0.002 08/13/14 EK SW6010mg/L0.003Zinc (Dissolved) 0.002 08/13/14 EK SW6010mg/L1400Iron 1.0 08/16/14 EK SW6010mg/L

0.0008Mercury 0.0002 08/13/14 MA SW7470mg/L117Potassium 0.5 08/16/14 LK SW6010mg/L228Magnesium 0.05 08/16/14 LK SW6010mg/L56.5Manganese 0.10 08/16/14 EK SW6010mg/L49.6Sodium 0.5 08/16/14 LK SW6010mg/L1.38Nickel 0.10 08/16/14 EK SW6010mg/L9.29Lead 0.20 08/16/14 EK SW6010mg/L

< 0.003Antimony 0.003 08/14/14 LK SW6010mg/L< 0.01Selenium 0.01 08/16/14 LK SW6010mg/L

< 0.0005Thallium 0.0005 08/13/14 RS SM3113B/SW70mg/L1.59Vanadium 0.20 08/16/14 EK SW6010mg/L7.65Zinc 0.20 08/16/14 EK SW6010mg/L0.03Total Cyanide 0.01 08/14/14 O/EG 335.4/9010mg/L

CompletedFiltration 08/12/14 AG 0.45um Filter

CompletedDissolved Mercury Digestion 08/14/14 I/I SW7470CompletedMercury Digestion 08/13/14 I/I SW7470CompletedPCB Extraction (2 Liter) 08/14/14 L SW3510CompletedExtraction for Pest (2 Liter) 08/14/14 L SW3510CompletedSemi-Volatile Extraction 08/12/14 E/D SW3520CompletedDissolved Metals Preparation 08/12/14 AG SW846-3005CompletedTotal Metals Digestion 08/12/14 AG SW846 - 3050

Polychlorinated Biphenyls0.067PCB-1016 0.058 08/13/14 AW 608/ 8082ug/LNDPCB-1221 0.058 08/13/14 AW 608/ 8082ug/LNDPCB-1232 0.058 08/13/14 AW 608/ 8082ug/LNDPCB-1242 0.058 08/13/14 AW 608/ 8082ug/LNDPCB-1248 0.058 08/13/14 AW 608/ 8082ug/LNDPCB-1254 0.058 08/13/14 AW 608/ 8082ug/LNDPCB-1260 0.058 08/13/14 AW 608/ 8082ug/LNDPCB-1262 0.058 08/13/14 AW 608/ 8082ug/LNDPCB-1268 0.058 08/13/14 AW 608/ 8082ug/L

QA/QC Surrogates50% DCBP 08/13/14 AW 608/ 8082%79% TCMX 08/13/14 AW 608/ 8082%

PesticidesND4,4' -DDD 0.010 08/18/14 CE SW8081ug/LND4,4' -DDE 0.010 08/18/14 CE SW8081ug/LND4,4' -DDT 0.010 08/18/14 CE SW8081ug/LNDa-BHC 0.005 08/18/14 CE SW8081ug/LNDAlachlor 0.075 08/18/14 CE SW8081ug/L 1

NDAldrin 0.002 08/18/14 CE SW8081ug/LNDb-BHC 0.005 08/18/14 CE SW8081ug/L

Page 74 of 93 Ver 1




LOD/MDL

NDChlordane 0.030 08/18/14 CE SW8081ug/LNDd-BHC 0.025 08/18/14 CE SW8081ug/LNDDieldrin 0.035 08/18/14 CE SW8081ug/LNDEndosulfan I 0.10 08/18/14 CE SW8081ug/LNDEndosulfan II 0.050 08/18/14 CE SW8081ug/LNDEndosulfan Sulfate 0.050 08/18/14 CE SW8081ug/LNDEndrin 0.030 08/18/14 CE SW8081ug/LNDEndrin Aldehyde 0.050 08/18/14 CE SW8081ug/LNDEndrin ketone 0.060 08/18/14 CE SW8081ug/LNDg-BHC (Lindane) 0.025 08/18/14 CE SW8081ug/LNDHeptachlor 0.020 08/18/14 CE SW8081ug/LNDHeptachlor epoxide 0.005 08/18/14 CE SW8081ug/LNDMethoxychlor 0.10 08/18/14 CE SW8081ug/LNDToxaphene 0.20 08/18/14 CE SW8081ug/L

QA/QC Surrogates126%DCBP (Surrogate Rec) 08/18/14 CE 30 - 150 %%78%TCMX (Surrogate Rec) 08/18/14 CE 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 1.0 08/12/14 HM SW8260ug/LND1,1,1-Trichloroethane 1.0 08/12/14 HM SW8260ug/LND1,1,2,2-Tetrachloroethane 0.50 08/12/14 HM SW8260ug/LND1,1,2-Trichloroethane 1.0 08/12/14 HM SW8260ug/LND1,1-Dichloroethane 1.0 08/12/14 HM SW8260ug/LND1,1-Dichloroethene 1.0 08/12/14 HM SW8260ug/LND1,1-Dichloropropene 1.0 08/12/14 HM SW8260ug/LND1,2,3-Trichlorobenzene 1.0 08/12/14 HM SW8260ug/LND1,2,3-Trichloropropane 1.0 08/12/14 HM SW8260ug/LND1,2,4-Trichlorobenzene 1.0 08/12/14 HM SW8260ug/LND1,2,4-Trimethylbenzene 1.0 08/12/14 HM SW8260ug/LND1,2-Dibromo-3-chloropropane 1.0 08/12/14 HM SW8260ug/LND1,2-Dibromoethane 1.0 08/12/14 HM SW8260ug/LND1,2-Dichlorobenzene 1.0 08/12/14 HM SW8260ug/LND1,2-Dichloroethane 0.60 08/12/14 HM SW8260ug/LND1,2-Dichloropropane 1.0 08/12/14 HM SW8260ug/LND1,3,5-Trimethylbenzene 1.0 08/12/14 HM SW8260ug/LND1,3-Dichlorobenzene 1.0 08/12/14 HM SW8260ug/LND1,3-Dichloropropane 1.0 08/12/14 HM SW8260ug/LND1,4-Dichlorobenzene 1.0 08/12/14 HM SW8260ug/LND2,2-Dichloropropane 1.0 08/12/14 HM SW8260ug/LND2-Chlorotoluene 1.0 08/12/14 HM SW8260ug/LND2-Hexanone 5.0 08/12/14 HM SW8260ug/LND2-Isopropyltoluene 1.0 08/12/14 HM SW8260ug/L 1

ND4-Chlorotoluene 1.0 08/12/14 HM SW8260ug/LND4-Methyl-2-pentanone 5.0 08/12/14 HM SW8260ug/LNDAcetone 25 08/12/14 HM SW8260ug/LNDAcrylonitrile 5.0 08/12/14 HM SW8260ug/LNDBenzene 0.70 08/12/14 HM SW8260ug/LNDBromobenzene 1.0 08/12/14 HM SW8260ug/LNDBromochloromethane 1.0 08/12/14 HM SW8260ug/L

Page 75 of 93 Ver 1




LOD/MDL

NDBromodichloromethane 0.50 08/12/14 HM SW8260ug/LNDBromoform 1.0 08/12/14 HM SW8260ug/LNDBromomethane 1.0 08/12/14 HM SW8260ug/LNDCarbon Disulfide 5.0 08/12/14 HM SW8260ug/LNDCarbon tetrachloride 1.0 08/12/14 HM SW8260ug/LNDChlorobenzene 1.0 08/12/14 HM SW8260ug/LNDChloroethane 1.0 08/12/14 HM SW8260ug/LNDChloroform 1.0 08/12/14 HM SW8260ug/LNDChloromethane 1.0 08/12/14 HM SW8260ug/LNDcis-1,2-Dichloroethene 1.0 08/12/14 HM SW8260ug/LNDcis-1,3-Dichloropropene 0.40 08/12/14 HM SW8260ug/LNDDibromochloromethane 0.50 08/12/14 HM SW8260ug/LNDDibromomethane 1.0 08/12/14 HM SW8260ug/LNDDichlorodifluoromethane 1.0 08/12/14 HM SW8260ug/LNDEthylbenzene 1.0 08/12/14 HM SW8260ug/LNDHexachlorobutadiene 0.40 08/12/14 HM SW8260ug/LNDIsopropylbenzene 1.0 08/12/14 HM SW8260ug/LNDm&p-Xylene 1.0 08/12/14 HM SW8260ug/LNDMethyl ethyl ketone 5.0 08/12/14 HM SW8260ug/LNDMethyl t-butyl ether (MTBE) 1.0 08/12/14 HM SW8260ug/LNDMethylene chloride 1.0 08/12/14 HM SW8260ug/L8.7Naphthalene 1.0 08/12/14 HM SW8260ug/LNDn-Butylbenzene 1.0 08/12/14 HM SW8260ug/LNDn-Propylbenzene 1.0 08/12/14 HM SW8260ug/LNDo-Xylene 1.0 08/12/14 HM SW8260ug/LNDp-Isopropyltoluene 1.0 08/12/14 HM SW8260ug/LNDsec-Butylbenzene 1.0 08/12/14 HM SW8260ug/LNDStyrene 1.0 08/12/14 HM SW8260ug/LNDtert-Butylbenzene 1.0 08/12/14 HM SW8260ug/LNDTetrachloroethene 1.0 08/12/14 HM SW8260ug/LNDTetrahydrofuran (THF) 2.5 08/12/14 HM SW8260ug/L 1

NDToluene 1.0 08/12/14 HM SW8260ug/LNDTotal Xylenes 1.0 08/12/14 HM SW8260ug/LNDtrans-1,2-Dichloroethene 1.0 08/12/14 HM SW8260ug/LNDtrans-1,3-Dichloropropene 0.40 08/12/14 HM SW8260ug/LNDtrans-1,4-dichloro-2-butene 5.0 08/12/14 HM SW8260ug/LNDTrichloroethene 1.0 08/12/14 HM SW8260ug/LNDTrichlorofluoromethane 1.0 08/12/14 HM SW8260ug/LNDTrichlorotrifluoroethane 1.0 08/12/14 HM SW8260ug/LNDVinyl chloride 1.0 08/12/14 HM SW8260ug/L

QA/QC Surrogates103% 1,2-dichlorobenzene-d4 08/12/14 HM 70 - 130 %%90% Bromofluorobenzene 08/12/14 HM 70 - 130 %%103% Dibromofluoromethane 08/12/14 HM 70 - 130 %%102% Toluene-d8 08/12/14 HM 70 - 130 %%

SemivolatilesND1,2,4-Trichlorobenzene 5.0 08/14/14 DD SW8270ug/LND1,2-Dichlorobenzene 2.5 08/14/14 DD SW8270ug/LND1,2-Diphenylhydrazine 5.0 08/14/14 DD SW8270ug/L

Page 76 of 93 Ver 1




LOD/MDL

ND1,3-Dichlorobenzene 2.5 08/14/14 DD SW8270ug/LND1,4-Dichlorobenzene 2.5 08/14/14 DD SW8270ug/LND2,4,5-Trichlorophenol 1.0 08/14/14 DD SW8270ug/LND2,4,6-Trichlorophenol 1.0 08/14/14 DD SW8270ug/LND2,4-Dichlorophenol 1.0 08/14/14 DD SW8270ug/LND2,4-Dimethylphenol 1.0 08/14/14 DD SW8270ug/LND2,4-Dinitrophenol 1.0 08/14/14 DD SW8270ug/LND2,4-Dinitrotoluene 5.0 08/14/14 DD SW8270ug/LND2,6-Dinitrotoluene 5.0 08/14/14 DD SW8270ug/LND2-Chloronaphthalene 5.0 08/14/14 DD SW8270ug/LND2-Chlorophenol 1.0 08/14/14 DD SW8270ug/LND2-Methylnaphthalene 5.0 08/14/14 DD SW8270ug/LND2-Methylphenol (o-cresol) 1.0 08/14/14 DD SW8270ug/LND2-Nitroaniline 5.0 08/14/14 DD SW8270ug/LND2-Nitrophenol 1.0 08/14/14 DD SW8270ug/LND3&4-Methylphenol (m&p-cresol) 10 08/14/14 DD SW8270ug/LND3,3'-Dichlorobenzidine 5.0 08/14/14 DD SW8270ug/LND3-Nitroaniline 5.0 08/14/14 DD SW8270ug/LND4,6-Dinitro-2-methylphenol 1.0 08/14/14 DD SW8270ug/LND4-Bromophenyl phenyl ether 5.0 08/14/14 DD SW8270ug/LND4-Chloro-3-methylphenol 1.0 08/14/14 DD SW8270ug/LND4-Chloroaniline 5.0 08/14/14 DD SW8270ug/LND4-Chlorophenyl phenyl ether 1.0 08/14/14 DD SW8270ug/LND4-Nitroaniline 5.0 08/14/14 DD SW8270ug/LND4-Nitrophenol 1.0 08/14/14 DD SW8270ug/LNDAcetophenone 5.0 08/14/14 DD SW8270ug/LNDAniline 5.0 08/14/14 DD SW8270ug/LNDBenzidine 5 08/14/14 DD SW8270ug/LNDBenzoic acid 50 08/14/14 DD SW8270ug/LNDBenzyl butyl phthalate 5.0 08/14/14 DD SW8270ug/LNDBis(2-chloroethoxy)methane 5.0 08/14/14 DD SW8270ug/LNDBis(2-chloroethyl)ether 1.0 08/14/14 DD SW8270ug/LNDBis(2-chloroisopropyl)ether 5.0 08/14/14 DD SW8270ug/LNDCarbazole 5.0 08/14/14 DD SW8270ug/LNDDibenzofuran 5.0 08/14/14 DD SW8270ug/LNDDiethyl phthalate 5.0 08/14/14 DD SW8270ug/LNDDimethylphthalate 5.0 08/14/14 DD SW8270ug/LNDDi-n-butylphthalate 5.0 08/14/14 DD SW8270ug/LNDDi-n-octylphthalate 5.0 08/14/14 DD SW8270ug/LNDFluorene 5.0 08/14/14 DD SW8270ug/LNDHexachlorocyclopentadiene 5.0 08/14/14 DD SW8270ug/LNDIsophorone 5.0 08/14/14 DD SW8270ug/LNDNaphthalene 5.0 08/14/14 DD SW8270ug/LNDN-Nitrosodimethylamine 5.0 08/14/14 DD SW8270ug/LNDN-Nitrosodi-n-propylamine 5.0 08/14/14 DD SW8270ug/LNDN-Nitrosodiphenylamine 5.0 08/14/14 DD SW8270ug/LNDPhenol 1.0 08/14/14 DD SW8270ug/L


Page 77 of 93 Ver 1




LOD/MDL


SemivolatilesND1,2,4,5-Tetrachlorobenzene 0.50 08/13/14 DD SW8270 (SIM)ug/L0.64Acenaphthene 0.05 08/13/14 DD SW8270 (SIM)ug/L0.25Acenaphthylene 0.05 08/13/14 DD SW8270 (SIM)ug/L1.4Anthracene 0.02 08/13/14 DD SW8270 (SIM)ug/L3.1Benz(a)anthracene 0.02 08/13/14 DD SW8270 (SIM)ug/L2.2Benzo(a)pyrene 0.02 08/13/14 DD SW8270 (SIM)ug/L3.0Benzo(b)fluoranthene 0.02 08/13/14 DD SW8270 (SIM)ug/L1.1Benzo(ghi)perylene 0.50 08/13/14 DD SW8270 (SIM)ug/L1.0Benzo(k)fluoranthene 0.02 08/13/14 DD SW8270 (SIM)ug/L3.0Bis(2-ethylhexyl)phthalate 0.50 08/13/14 DD SW8270 (SIM)ug/L3.0Chrysene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDDibenz(a,h)anthracene 0.02 08/13/14 DD SW8270 (SIM)ug/L7.7Fluoranthene 0.04 08/13/14 DD SW8270 (SIM)ug/LNDHexachlorobenzene 0.04 08/13/14 DD SW8270 (SIM)ug/LNDHexachlorobutadiene 0.50 08/13/14 DD SW8270 (SIM)ug/LNDHexachloroethane 0.50 08/13/14 DD SW8270 (SIM)ug/L1.0Indeno(1,2,3-cd)pyrene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDNitrobenzene 0.10 08/13/14 DD SW8270 (SIM)ug/LNDPentachloronitrobenzene 0.10 08/13/14 DD SW8270 (SIM)ug/LNDPentachlorophenol 0.80 08/13/14 DD SW8270 (SIM)ug/L6.6Phenanthrene 0.05 08/13/14 DD SW8270 (SIM)ug/L6.0Pyrene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDPyridine 0.50 08/13/14 DD SW8270 (SIM)ug/L

QA/QC Surrogates94% 2,4,6-Tribromophenol 08/13/14 DD 15 - 110 %%76% 2-Fluorobiphenyl 08/13/14 DD 30 - 130 %%75% 2-Fluorophenol 08/13/14 DD 15 - 110 %%95% Nitrobenzene-d5 08/13/14 DD 30 - 130 %%79% Phenol-d5 08/13/14 DD 15 - 110 %%99% Terphenyl-d14 08/13/14 DD 30 - 130 %%

Page 78 of 93 Ver 1




LOD/MDL

Comments:


Pesticide Comment:Due to matrix interference caused by the presence of PCBs in the sample, an elevated RL was reported.






Page 79 of 93 Ver 1





EC

Laboratory Data

GW-2

Phoenix ID: BG91937

08/12/149:30

15:35




Date Time



SDG ID: GBG91924


LOD/MDL


0.151Arsenic 0.004 08/14/14 LK SW6010mg/L3.39Barium 0.002 08/14/14 LK SW6010mg/L0.015Beryllium 0.001 08/14/14 LK SW6010mg/L342Calcium 1.0 08/18/14 EK SW6010mg/L

0.016Cadmium 0.001 08/14/14 LK SW6010mg/L0.329Cobalt 0.002 08/14/14 LK SW6010mg/L1.29Chromium 0.001 08/14/14 LK SW6010mg/L0.963Copper 0.005 08/14/14 LK SW6010mg/L

< 0.001Silver (Dissolved) 0.001 08/13/14 LK SW6010mg/L0.31Aluminum (Dissolved) 0.11 08/14/14 LK SW6010mg/L

< 0.004Arsenic (Dissolved) 0.004 08/13/14 LK SW6010mg/L0.053Barium (Dissolved) 0.002 08/13/14 LK SW6010mg/L

< 0.001Beryllium (Dissolved) 0.001 08/13/14 LK SW6010mg/L111Calcium (Dissolved) 0.01 08/13/14 LK SW6010mg/L

< 0.001Cadmium (Dissolved) 0.001 08/13/14 LK SW6010mg/L0.004Cobalt (Dissolved) 0.001 08/13/14 LK SW6010mg/L

< 0.001Chromium (Dissolved) 0.001 08/13/14 LK SW6010mg/L< 0.005Copper (Dissolved) 0.005 08/13/14 LK SW6010mg/L0.082Iron (Dissolved) 0.011 08/13/14 LK SW6010mg/L

< 0.0002Mercury (Dissolved) 0.0002 08/14/14 MA SW7470mg/L10.3Potassium (Dissolved) 0.1 08/13/14 LK SW6010mg/L18.5Magnesium (Dissolved) 0.01 08/13/14 LK SW6010mg/L3.98Manganese (Dissolved) 0.011 08/14/14 LK SW6010mg/L51.4Sodium (Dissolved) 0.11 08/13/14 LK SW6010mg/L0.009Nickel (Dissolved) 0.001 08/13/14 LK SW6010mg/L

< 0.002Lead (Dissolved) 0.002 08/13/14 LK SW6010mg/L

Page 80 of 93 Ver 1




LOD/MDL

< 0.003Antimony (Dissolved) 0.003 08/13/14 LK SW6010mg/LNDSelenium (Dissolved) 0.005 08/12/14 R/T SW6010mg/L

< 0.0005Thallium (Dissolved) 0.0005 08/13/14 RS SW7010mg/L< 0.002Vanadium (Dissolved) 0.002 08/13/14 LK SW6010mg/L0.021Zinc (Dissolved) 0.002 08/13/14 LK SW6010mg/L714Iron 0.10 08/16/14 EK SW6010mg/L

< 0.0002Mercury 0.0002 08/13/14 MA SW7470mg/L45.5Potassium 0.1 08/14/14 LK SW6010mg/L110Magnesium 1.0 08/18/14 EK SW6010mg/L25.5Manganese 0.10 08/18/14 EK SW6010mg/L45.8Sodium 0.1 08/14/14 LK SW6010mg/L0.673Nickel 0.001 08/14/14 LK SW6010mg/L3.81Lead 0.020 08/16/14 EK SW6010mg/L

< 0.003Antimony 0.003 08/14/14 LK SW6010mg/L0.011Selenium 0.01 08/14/14 LK SW6010mg/L

< 0.0005Thallium 0.0005 08/13/14 RS SM3113B/SW70mg/L0.695Vanadium 0.002 08/14/14 LK SW6010mg/L3.33Zinc 0.020 08/16/14 EK SW6010mg/L

< 0.01Total Cyanide 0.01 08/14/14 O/EG 335.4/9010mg/LCompletedFiltration 08/12/14 AG 0.45um Filter


Polychlorinated BiphenylsNDPCB-1016 0.053 08/14/14 AW 608/ 8082ug/LNDPCB-1221 0.053 08/14/14 AW 608/ 8082ug/LNDPCB-1232 0.053 08/14/14 AW 608/ 8082ug/LNDPCB-1242 0.053 08/14/14 AW 608/ 8082ug/LNDPCB-1248 0.053 08/14/14 AW 608/ 8082ug/LNDPCB-1254 0.053 08/14/14 AW 608/ 8082ug/LNDPCB-1260 0.053 08/14/14 AW 608/ 8082ug/LNDPCB-1262 0.053 08/14/14 AW 608/ 8082ug/LNDPCB-1268 0.053 08/14/14 AW 608/ 8082ug/L


PesticidesND4,4' -DDD 0.030 08/18/14 CE SW8081ug/LND4,4' -DDE 0.027 08/18/14 CE SW8081ug/LND4,4' -DDT 0.030 08/18/14 CE SW8081ug/LNDa-BHC 0.050 08/18/14 CE SW8081ug/LNDAlachlor 0.80 08/18/14 CE SW8081ug/L 1

NDAldrin 0.016 08/18/14 CE SW8081ug/LNDb-BHC 0.053 08/18/14 CE SW8081ug/L

Page 81 of 93 Ver 1




LOD/MDL

NDChlordane 0.30 08/18/14 CE SW8081ug/LNDd-BHC 0.050 08/18/14 CE SW8081ug/LNDDieldrin 0.15 08/18/14 CE SW8081ug/LNDEndosulfan I 0.11 08/18/14 CE SW8081ug/LNDEndosulfan II 0.050 08/18/14 CE SW8081ug/LNDEndosulfan Sulfate 0.050 08/18/14 CE SW8081ug/LNDEndrin 0.050 08/18/14 CE SW8081ug/LNDEndrin Aldehyde 0.53 08/18/14 CE SW8081ug/LNDEndrin ketone 0.53 08/18/14 CE SW8081ug/LNDg-BHC (Lindane) 0.050 08/18/14 CE SW8081ug/LNDHeptachlor 0.050 08/18/14 CE SW8081ug/LNDHeptachlor epoxide 0.050 08/18/14 CE SW8081ug/LNDMethoxychlor 1.1 08/18/14 CE SW8081ug/LNDToxaphene 2.0 08/18/14 CE SW8081ug/L

QA/QC SurrogatesDiluted Out%DCBP (Surrogate Rec) 08/18/14 CE 30 - 150 %%Diluted Out%TCMX (Surrogate Rec) 08/18/14 CE 30 - 150 %%



Page 82 of 93 Ver 1




LOD/MDL

NDBromodichloromethane 0.50 08/12/14 HM SW8260ug/LNDBromoform 1.0 08/12/14 HM SW8260ug/LNDBromomethane 1.0 08/12/14 HM SW8260ug/LNDCarbon Disulfide 5.0 08/12/14 HM SW8260ug/LNDCarbon tetrachloride 1.0 08/12/14 HM SW8260ug/LNDChlorobenzene 1.0 08/12/14 HM SW8260ug/LNDChloroethane 1.0 08/12/14 HM SW8260ug/LNDChloroform 1.0 08/12/14 HM SW8260ug/LNDChloromethane 1.0 08/12/14 HM SW8260ug/LNDcis-1,2-Dichloroethene 1.0 08/12/14 HM SW8260ug/LNDcis-1,3-Dichloropropene 0.40 08/12/14 HM SW8260ug/LNDDibromochloromethane 0.50 08/12/14 HM SW8260ug/LNDDibromomethane 1.0 08/12/14 HM SW8260ug/LNDDichlorodifluoromethane 1.0 08/12/14 HM SW8260ug/LNDEthylbenzene 1.0 08/12/14 HM SW8260ug/LNDHexachlorobutadiene 0.40 08/12/14 HM SW8260ug/LNDIsopropylbenzene 1.0 08/12/14 HM SW8260ug/LNDm&p-Xylene 1.0 08/12/14 HM SW8260ug/LNDMethyl ethyl ketone 5.0 08/12/14 HM SW8260ug/LNDMethyl t-butyl ether (MTBE) 1.0 08/12/14 HM SW8260ug/LNDMethylene chloride 1.0 08/12/14 HM SW8260ug/L5.7Naphthalene 1.0 08/12/14 HM SW8260ug/LNDn-Butylbenzene 1.0 08/12/14 HM SW8260ug/LNDn-Propylbenzene 1.0 08/12/14 HM SW8260ug/LNDo-Xylene 1.0 08/12/14 HM SW8260ug/LNDp-Isopropyltoluene 1.0 08/12/14 HM SW8260ug/LNDsec-Butylbenzene 1.0 08/12/14 HM SW8260ug/LNDStyrene 1.0 08/12/14 HM SW8260ug/LNDtert-Butylbenzene 1.0 08/12/14 HM SW8260ug/LNDTetrachloroethene 1.0 08/12/14 HM SW8260ug/LNDTetrahydrofuran (THF) 2.5 08/12/14 HM SW8260ug/L 1

NDToluene 1.0 08/12/14 HM SW8260ug/LNDTotal Xylenes 1.0 08/12/14 HM SW8260ug/LNDtrans-1,2-Dichloroethene 1.0 08/12/14 HM SW8260ug/LNDtrans-1,3-Dichloropropene 0.40 08/12/14 HM SW8260ug/LNDtrans-1,4-dichloro-2-butene 5.0 08/12/14 HM SW8260ug/L4.3Trichloroethene 1.0 08/12/14 HM SW8260ug/LNDTrichlorofluoromethane 1.0 08/12/14 HM SW8260ug/LNDTrichlorotrifluoroethane 1.0 08/12/14 HM SW8260ug/LNDVinyl chloride 1.0 08/12/14 HM SW8260ug/L



Page 83 of 93 Ver 1




LOD/MDL



Page 84 of 93 Ver 1




LOD/MDL


SemivolatilesND1,2,4,5-Tetrachlorobenzene 0.56 08/13/14 DD SW8270 (SIM)ug/L0.12Acenaphthene 0.06 08/13/14 DD SW8270 (SIM)ug/L0.06Acenaphthylene 0.06 08/13/14 DD SW8270 (SIM)ug/L0.21Anthracene 0.02 08/13/14 DD SW8270 (SIM)ug/L0.40Benz(a)anthracene 0.02 08/13/14 DD SW8270 (SIM)ug/L0.26Benzo(a)pyrene 0.02 08/13/14 DD SW8270 (SIM)ug/L0.40Benzo(b)fluoranthene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDBenzo(ghi)perylene 0.56 08/13/14 DD SW8270 (SIM)ug/L0.12Benzo(k)fluoranthene 0.02 08/13/14 DD SW8270 (SIM)ug/L4.9Bis(2-ethylhexyl)phthalate 0.56 08/13/14 DD SW8270 (SIM)ug/L

0.38Chrysene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDDibenz(a,h)anthracene 0.02 08/13/14 DD SW8270 (SIM)ug/L1.0Fluoranthene 0.04 08/13/14 DD SW8270 (SIM)ug/LNDHexachlorobenzene 0.04 08/13/14 DD SW8270 (SIM)ug/LNDHexachlorobutadiene 0.5 08/13/14 DD SW8270 (SIM)ug/LNDHexachloroethane 0.56 08/13/14 DD SW8270 (SIM)ug/L0.12Indeno(1,2,3-cd)pyrene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDNitrobenzene 0.11 08/13/14 DD SW8270 (SIM)ug/LNDPentachloronitrobenzene 0.11 08/13/14 DD SW8270 (SIM)ug/LNDPentachlorophenol 0.89 08/13/14 DD SW8270 (SIM)ug/L1.1Phenanthrene 0.06 08/13/14 DD SW8270 (SIM)ug/L

0.78Pyrene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDPyridine 0.56 08/13/14 DD SW8270 (SIM)ug/L


Page 85 of 93 Ver 1




LOD/MDL

Comments:


Pesticide Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported.






Page 86 of 93 Ver 1





EC

Laboratory Data

GW-3

Phoenix ID: BG91938

08/12/1410:0015:35




Date Time



SDG ID: GBG91924


LOD/MDL


0.156Arsenic 0.004 08/14/14 LK SW6010mg/L2.23Barium 0.002 08/14/14 LK SW6010mg/L0.012Beryllium 0.001 08/14/14 LK SW6010mg/L90.0Calcium 0.010 08/14/14 LK SW6010mg/L0.009Cadmium 0.001 08/14/14 LK SW6010mg/L0.204Cobalt 0.002 08/14/14 LK SW6010mg/L0.711Chromium 0.001 08/14/14 LK SW6010mg/L0.573Copper 0.005 08/14/14 LK SW6010mg/L

< 0.001Silver (Dissolved) 0.001 08/13/14 LK SW6010mg/L0.15Aluminum (Dissolved) 0.01 08/14/14 LK SW6010mg/L

< 0.004Arsenic (Dissolved) 0.004 08/13/14 LK SW6010mg/L0.045Barium (Dissolved) 0.002 08/13/14 LK SW6010mg/L

< 0.001Beryllium (Dissolved) 0.001 08/13/14 LK SW6010mg/L107Calcium (Dissolved) 0.01 08/13/14 LK SW6010mg/L

< 0.001Cadmium (Dissolved) 0.001 08/13/14 LK SW6010mg/L0.005Cobalt (Dissolved) 0.001 08/13/14 LK SW6010mg/L

< 0.001Chromium (Dissolved) 0.001 08/13/14 LK SW6010mg/L0.008Copper (Dissolved) 0.005 08/13/14 LK SW6010mg/L0.110Iron (Dissolved) 0.011 08/13/14 LK SW6010mg/L

< 0.0002Mercury (Dissolved) 0.0002 08/14/14 MA SW7470mg/L11.5Potassium (Dissolved) 0.1 08/13/14 LK SW6010mg/L21.7Magnesium (Dissolved) 0.01 08/13/14 LK SW6010mg/L3.50Manganese (Dissolved) 0.011 08/14/14 LK SW6010mg/L57.2Sodium (Dissolved) 0.11 08/13/14 LK SW6010mg/L0.011Nickel (Dissolved) 0.001 08/13/14 LK SW6010mg/L

< 0.002Lead (Dissolved) 0.002 08/13/14 LK SW6010mg/L

Page 87 of 93 Ver 1




LOD/MDL

< 0.003Antimony (Dissolved) 0.003 08/13/14 LK SW6010mg/L< 0.010Selenium (Dissolved) 0.010 08/12/14 R/T SW6010mg/L

< 0.0005Thallium (Dissolved) 0.0005 08/13/14 RS SW7010mg/L< 0.002Vanadium (Dissolved) 0.002 08/13/14 LK SW6010mg/L0.006Zinc (Dissolved) 0.002 08/13/14 LK SW6010mg/L550Iron 0.10 08/16/14 EK SW6010mg/L

< 0.0002Mercury 0.0002 08/13/14 MA SW7470mg/L31.7Potassium 0.1 08/14/14 LK SW6010mg/L94.0Magnesium 0.10 08/18/14 EK SW6010mg/L31.5Manganese 0.10 08/19/14 LK SW6010mg/L56.4Sodium 0.1 08/14/14 LK SW6010mg/L0.539Nickel 0.001 08/14/14 LK SW6010mg/L0.207Lead 0.002 08/14/14 LK SW6010mg/L

< 0.003Antimony 0.003 08/14/14 LK SW6010mg/L< 0.01Selenium 0.01 08/16/14 LK SW6010mg/L

< 0.0005Thallium 0.0005 08/13/14 RS SM3113B/SW70mg/L0.444Vanadium 0.002 08/14/14 LK SW6010mg/L1.11Zinc 0.002 08/14/14 LK SW6010mg/L

< 0.01Total Cyanide 0.01 08/14/14 O/EG 335.4/9010mg/LCompletedFiltration 08/12/14 AG 0.45um Filter


Polychlorinated BiphenylsNDPCB-1016 0.050 08/14/14 AW 608/ 8082ug/LNDPCB-1221 0.050 08/14/14 AW 608/ 8082ug/LNDPCB-1232 0.050 08/14/14 AW 608/ 8082ug/LNDPCB-1242 0.050 08/14/14 AW 608/ 8082ug/LNDPCB-1248 0.050 08/14/14 AW 608/ 8082ug/LNDPCB-1254 0.050 08/14/14 AW 608/ 8082ug/LNDPCB-1260 0.050 08/14/14 AW 608/ 8082ug/LNDPCB-1262 0.050 08/14/14 AW 608/ 8082ug/LNDPCB-1268 0.050 08/14/14 AW 608/ 8082ug/L


PesticidesND4,4' -DDD 0.050 08/15/14 MH SW8081ug/LND4,4' -DDE 0.050 08/15/14 MH SW8081ug/LND4,4' -DDT 0.050 08/15/14 MH SW8081ug/LNDa-BHC 0.025 08/15/14 MH SW8081ug/LNDAlachlor 0.075 08/15/14 MH SW8081ug/L 1

NDAldrin 0.002 08/15/14 MH SW8081ug/LNDb-BHC 0.005 08/15/14 MH SW8081ug/L

Page 88 of 93 Ver 1




LOD/MDL

NDChlordane 0.30 08/15/14 MH SW8081ug/LNDd-BHC 0.025 08/15/14 MH SW8081ug/LNDDieldrin 0.002 08/15/14 MH SW8081ug/LNDEndosulfan I 0.050 08/15/14 MH SW8081ug/LNDEndosulfan II 0.050 08/15/14 MH SW8081ug/LNDEndosulfan Sulfate 0.050 08/15/14 MH SW8081ug/LNDEndrin 0.050 08/15/14 MH SW8081ug/LNDEndrin Aldehyde 0.050 08/15/14 MH SW8081ug/LNDEndrin ketone 0.050 08/15/14 MH SW8081ug/LNDg-BHC (Lindane) 0.025 08/15/14 MH SW8081ug/LNDHeptachlor 0.025 08/15/14 MH SW8081ug/LNDHeptachlor epoxide 0.025 08/15/14 MH SW8081ug/LNDMethoxychlor 0.10 08/15/14 MH SW8081ug/LNDToxaphene 1.0 08/15/14 MH SW8081ug/L

QA/QC Surrogates54%DCBP (Surrogate Rec) 08/15/14 MH 30 - 150 %%71%TCMX (Surrogate Rec) 08/15/14 MH 30 - 150 %%



Page 89 of 93 Ver 1




LOD/MDL

NDBromodichloromethane 0.50 08/12/14 HM SW8260ug/LNDBromoform 1.0 08/12/14 HM SW8260ug/LNDBromomethane 1.0 08/12/14 HM SW8260ug/LNDCarbon Disulfide 5.0 08/12/14 HM SW8260ug/LNDCarbon tetrachloride 1.0 08/12/14 HM SW8260ug/LNDChlorobenzene 1.0 08/12/14 HM SW8260ug/LNDChloroethane 1.0 08/12/14 HM SW8260ug/LNDChloroform 1.0 08/12/14 HM SW8260ug/LNDChloromethane 1.0 08/12/14 HM SW8260ug/LNDcis-1,2-Dichloroethene 1.0 08/12/14 HM SW8260ug/LNDcis-1,3-Dichloropropene 0.40 08/12/14 HM SW8260ug/LNDDibromochloromethane 0.50 08/12/14 HM SW8260ug/LNDDibromomethane 1.0 08/12/14 HM SW8260ug/LNDDichlorodifluoromethane 1.0 08/12/14 HM SW8260ug/LNDEthylbenzene 1.0 08/12/14 HM SW8260ug/LNDHexachlorobutadiene 0.40 08/12/14 HM SW8260ug/LNDIsopropylbenzene 1.0 08/12/14 HM SW8260ug/LNDm&p-Xylene 1.0 08/12/14 HM SW8260ug/LNDMethyl ethyl ketone 5.0 08/12/14 HM SW8260ug/LNDMethyl t-butyl ether (MTBE) 1.0 08/12/14 HM SW8260ug/LNDMethylene chloride 1.0 08/12/14 HM SW8260ug/LNDNaphthalene 1.0 08/12/14 HM SW8260ug/LNDn-Butylbenzene 1.0 08/12/14 HM SW8260ug/LNDn-Propylbenzene 1.0 08/12/14 HM SW8260ug/LNDo-Xylene 1.0 08/12/14 HM SW8260ug/LNDp-Isopropyltoluene 1.0 08/12/14 HM SW8260ug/LNDsec-Butylbenzene 1.0 08/12/14 HM SW8260ug/LNDStyrene 1.0 08/12/14 HM SW8260ug/LNDtert-Butylbenzene 1.0 08/12/14 HM SW8260ug/LNDTetrachloroethene 1.0 08/12/14 HM SW8260ug/LNDTetrahydrofuran (THF) 2.5 08/12/14 HM SW8260ug/L 1

NDToluene 1.0 08/12/14 HM SW8260ug/LNDTotal Xylenes 1.0 08/12/14 HM SW8260ug/LNDtrans-1,2-Dichloroethene 1.0 08/12/14 HM SW8260ug/LNDtrans-1,3-Dichloropropene 0.40 08/12/14 HM SW8260ug/LNDtrans-1,4-dichloro-2-butene 5.0 08/12/14 HM SW8260ug/L2.6Trichloroethene 1.0 08/12/14 HM SW8260ug/LNDTrichlorofluoromethane 1.0 08/12/14 HM SW8260ug/LNDTrichlorotrifluoroethane 1.0 08/12/14 HM SW8260ug/LNDVinyl chloride 1.0 08/12/14 HM SW8260ug/L



Page 90 of 93 Ver 1




LOD/MDL



Page 91 of 93 Ver 1




LOD/MDL


SemivolatilesND1,2,4,5-Tetrachlorobenzene 0.51 08/13/14 DD SW8270 (SIM)ug/LNDAcenaphthene 0.05 08/13/14 DD SW8270 (SIM)ug/LNDAcenaphthylene 0.05 08/13/14 DD SW8270 (SIM)ug/L0.04Anthracene 0.02 08/13/14 DD SW8270 (SIM)ug/L0.07Benz(a)anthracene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDBenzo(a)pyrene 0.02 08/13/14 DD SW8270 (SIM)ug/L0.05Benzo(b)fluoranthene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDBenzo(ghi)perylene 0.51 08/13/14 DD SW8270 (SIM)ug/L0.02Benzo(k)fluoranthene 0.02 08/13/14 DD SW8270 (SIM)ug/L3.4Bis(2-ethylhexyl)phthalate 0.51 08/13/14 DD SW8270 (SIM)ug/L

0.05Chrysene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDDibenz(a,h)anthracene 0.02 08/13/14 DD SW8270 (SIM)ug/L0.14Fluoranthene 0.04 08/13/14 DD SW8270 (SIM)ug/LNDHexachlorobenzene 0.04 08/13/14 DD SW8270 (SIM)ug/LNDHexachlorobutadiene 0.5 08/13/14 DD SW8270 (SIM)ug/LNDHexachloroethane 0.51 08/13/14 DD SW8270 (SIM)ug/LNDIndeno(1,2,3-cd)pyrene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDNitrobenzene 0.10 08/13/14 DD SW8270 (SIM)ug/LNDPentachloronitrobenzene 0.10 08/13/14 DD SW8270 (SIM)ug/LNDPentachlorophenol 0.82 08/13/14 DD SW8270 (SIM)ug/LNDPhenanthrene 0.05 08/13/14 DD SW8270 (SIM)ug/L0.11Pyrene 0.02 08/13/14 DD SW8270 (SIM)ug/LNDPyridine 0.51 08/13/14 DD SW8270 (SIM)ug/L


Page 92 of 93 Ver 1




LOD/MDL

Comments:


Total Cyanide: This sample was received with a pH<12; pH was adjusted to >12 (EPA requires preservation at time of sampling to a pH of >12.) A sample bias can not be ruled out.






Page 93 of 93 Ver 1

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

QA/QC ReportAugust 20, 2014



SDG I.D.: GBG91924

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

QA/QC Batch 283164, QC Sample No: BG90256 (BG91936, BG91937, BG91938)118 112Mercury (Dissolved) BRL 5.2117NC 117 0.0 70 - 130 20<0.0002 <0.0002

Additional Mercury criteria: LCS acceptance range for waters is 80-120% and for soils is 70-130%.

Comment:

QA/QC Batch 282704, QC Sample No: BG90256 (BG91936, BG91937, BG91938)98.1 98.7Selenium (Dissolved) BRL 0.6109NC 109 0.0 75 - 125 20<0.002 <0.002

107 106Thallium (Dissolved) BRL 0.9107NC 107 0.0 75 - 125 20<0.002 <0.005

QA/QC Batch 282720, QC Sample No: BG90256 (BG91936, BG91937, BG91938)83.9 83.1Thallium - Water BRL 1.097.9NC 95.0 3.0 75 - 125 20<0.002 <0.002

QA/QC Batch 283038, QC Sample No: BG91658 (BG91924, BG91925, BG91926, BG91927, BG91928, BG91929, BG91930, BG91931, BG91932, BG91933, BG91934, BG91935)

113 116Mercury - Soil BRL 2.697.8NC 96.6 1.2 70 - 130 30<0.09 <0.09


Comment:

QA/QC Batch 283030, QC Sample No: BG91896 (BG91936, BG91937, BG91938)

ICP Metals - Aqueous98.0 96.3Aluminum BRL 1.7104NC 89.8 14.7 75 - 125 200.037 0.033

116 117Antimony BRL 0.998.9NC 95.7 3.3 75 - 125 20<0.005 <0.005

117 117Arsenic BRL 0.096.4NC 93.2 3.4 75 - 125 20<0.004 <0.004

114 114Barium BRL 0.01095.10 94.6 14.1 75 - 125 200.038 0.040

112 112Beryllium BRL 0.0104NC 88.9 15.7 75 - 125 20<0.001 <0.001

110 111Cadmium BRL 0.996.6NC 93.6 3.2 75 - 125 20<0.001 <0.001

NC NCCalcium BRL NC1056.60 90.0 15.4 75 - 125 2082.4 88.0

117 118Chromium BRL 0.9101NC 97.8 3.2 75 - 125 200.001 <0.001

110 111Cobalt BRL 0.997.5NC 94.2 3.4 75 - 125 20<0.002 <0.002

109 109Copper BRL 0.01076.70 90.8 16.4 75 - 125 200.031 0.029

112 112Iron BRL 0.098.6NC 95.5 3.2 75 - 125 200.029 0.021

111 111Lead BRL 0.097.4NC 93.9 3.7 75 - 125 20<0.002 <0.002

NC NCMagnesium BRL NC98.85.40 97.6 1.2 75 - 125 2030.7 32.4

116 116Manganese BRL 0.0100NC 98.3 1.7 75 - 125 200.002 0.002

110 111Nickel BRL 0.997.6NC 94.7 3.0 75 - 125 200.002 0.001

89.4 83.0Potassium BRL 7.41002.20 98.2 1.8 75 - 125 2018.4 18.8

112 54.9Selenium BRL 68.495.8NC 92.2 3.8 m,r75 - 125 20<0.010 <0.010

106 106Silver BRL 0.0102NC 86.1 16.9 75 - 125 20<0.001 <0.001

NC NCSodium BRL NC1012.80 97.9 3.1 75 - 125 2074.9 77.0

111 112Vanadium BRL 0.9104NC 88.7 15.9 75 - 125 200.002 <0.002

111 111Zinc BRL 0.098.1NC 94.3 4.0 75 - 125 200.026 0.006

QA/QC Batch 283022, QC Sample No: BG91924 (BG91924)

ICP Metals - SoilNC NCAluminum BRL NC1106.20 110 0.0 75 - 125 3015000 14100

80.1 84.1Antimony BRL 4.995.2NC 97.9 2.8 75 - 125 30<3.5 <3.5

95.3 98.8Arsenic BRL 3.6103NC 102 1.0 75 - 125 303.2 3.51

Page 1 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

109 112Barium BRL 2.71088.00 110 1.8 75 - 125 3073.2 79.3

99.8 104Beryllium BRL 4.1107NC 106 0.9 75 - 125 300.58 0.59

97.3 100Cadmium BRL 2.7101NC 102 1.0 75 - 125 30<0.35 <0.35

NC NCCalcium BRL NC98.36.30 98.1 0.2 75 - 125 301540 1640

102 105Chromium BRL 2.91088.30 108 0.0 75 - 125 3017.6 16.2

96.7 101Cobalt BRL 4.41030.10 103 0.0 75 - 125 307.34 7.35

106 111Copper BRL 4.611110.5 110 0.9 75 - 125 3013.5 15.0

NC NCIron BRL NC1054.10 108 2.8 75 - 125 3017300 16600

91.2 104Lead BRL 13.110537.9 114 8.2 r75 - 125 30109 160

NC NCMagnesium BRL NC97.63.90 100 2.4 75 - 125 302340 2250

NC NCManganese BRL NC1071.50 107 0.0 75 - 125 30794 806

98.1 102Nickel BRL 3.91030.80 104 1.0 75 - 125 3012.4 12.5

>130 >130Potassium BRL NC1159.70 119 3.4 m75 - 125 30798 879

82.8 85.4Selenium BRL 3.187.1NC 87.5 0.5 75 - 125 30<1.4 <1.4

98.4 102Silver BRL 3.6104NC 103 1.0 75 - 125 30<0.35 <0.35

>130 >130Sodium BRL NC11510.5 115 0.0 m75 - 125 3068.8 76.4

98.8 103Thallium BRL 4.2105NC 105 0.0 75 - 125 30<3.2 <3.2

103 107Vanadium BRL 3.81139.30 113 0.0 75 - 125 3025.8 23.5

99.0 99.9Zinc 0.65 0.999.811.0 100 0.2 75 - 125 3047.3 52.8

QA/QC Batch 282996, QC Sample No: BG91929 (BG91925, BG91926, BG91927, BG91928, BG91929, BG91930, BG91931, BG91932, BG91933, BG91934, BG91935)

ICP Metals - SoilNC NCAluminum BRL NC1135.10 114 0.9 75 - 125 306830 6490

91.3 91.6Antimony BRL 0.398.1NC 102 3.9 75 - 125 30<3.9 <3.8

98.1 98.6Arsenic BRL 0.5103NC 103 0.0 75 - 125 30<0.8 <0.75

106 102Barium BRL 3.81054.00 108 2.8 75 - 125 3046.6 48.5

102 102Beryllium BRL 0.0105NC 106 0.9 75 - 125 300.40 0.36

100 99.9Cadmium BRL 0.1106NC 107 0.9 75 - 125 30<0.39 <0.38

>130 >130Calcium BRL NC10344.4 117 12.7 m,r75 - 125 30732 1150

102 104Chromium BRL 1.91082.40 108 0.0 75 - 125 3016.4 16.8

100 101Cobalt BRL 1.01049.80 103 1.0 75 - 125 308.18 9.02

107 109Copper BRL 1.911010.0 112 1.8 75 - 125 3013.6 12.3

NC NCIron BRL NC1165.70 117 0.9 75 - 125 3020600 21800

101 102Lead BRL 1.010513.6 105 0.0 75 - 125 305.64 4.92

NC NCMagnesium BRL NC10221.4 103 1.0 75 - 125 302000 2480

114 122Manganese BRL 6.81093.10 110 0.9 75 - 125 30395 383

101 102Nickel BRL 1.01053.10 103 1.9 75 - 125 309.91 9.61

>130 >130Potassium BRL NC12032.0 122 1.7 m,r75 - 125 301390 1920

89.6 89.7Selenium BRL 0.194.7NC 95.7 1.1 75 - 125 30<1.5 <1.5

101 102Silver BRL 1.0102NC 103 1.0 75 - 125 30<0.39 <0.38

>130 >130Sodium BRL NC11510.9 112 2.6 m75 - 125 3061.7 68.8

101 102Thallium BRL 1.0110NC 105 4.7 75 - 125 30<3.5 <3.4

106 104Vanadium BRL 1.91171.00 117 0.0 75 - 125 3030.3 30.0

99.0 101Zinc BRL 2.01040.60 104 0.0 75 - 125 3034.6 34.8


ICP Metals - Dissolved101 98.4Aluminum BRL 2.61086.90 107 0.9 75 - 125 200.15 0.14

103 101Antimony BRL 2.0102NC 103 1.0 75 - 125 20<0.005 <0.005

104 101Arsenic BRL 2.9101NC 102 1.0 75 - 125 20<0.004 <0.004

101 98.1Barium BRL 2.91042.10 102 1.9 75 - 125 200.049 0.048

103 98.7Beryllium BRL 4.3102NC 101 1.0 75 - 125 20<0.001 <0.001

105 101Cadmium BRL 3.9105NC 107 1.9 75 - 125 20<0.001 <0.001

Page 2 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

NC NCCalcium BRL NC1071.40 104 2.8 75 - 125 2071.3 70.3

105 102Chromium BRL 2.9104NC 105 1.0 75 - 125 20<0.001 0.001

100 97.0Cobalt BRL 3.0101NC 102 1.0 75 - 125 200.001 0.001

105 101Copper BRL 3.9107NC 105 1.9 75 - 125 20<0.005 <0.005

102 99.3Iron BRL 2.71028.20 103 1.0 75 - 125 200.093 0.101

102 99.4Lead BRL 2.6103NC 104 1.0 75 - 125 20<0.002 <0.002

NC NCMagnesium BRL NC1041.90 106 1.9 75 - 125 209.94 9.75

99.7 95.5Manganese BRL 4.31051.70 106 0.9 75 - 125 200.823 0.809

100 97.1Nickel BRL 2.9101NC 102 1.0 75 - 125 200.004 0.004

94.8 87.4Potassium BRL 8.199.53.80 98.2 1.3 75 - 125 208.1 7.8

90.2 87.6Silver BRL 2.9100NC 99.5 0.5 75 - 125 20<0.001 <0.001

NC NCSodium BRL NC1023.50 100 2.0 75 - 125 2055.8 53.9

102 98.9Vanadium BRL 3.1102NC 101 1.0 75 - 125 20<0.002 <0.002

102 98.6Zinc BRL 3.499.8NC 101 1.2 75 - 125 200.003 0.003

QA/QC Batch 283041, QC Sample No: BG92353 (BG91936, BG91937, BG91938)98.3 97.5Mercury - Water BRL 0.898.6NC 96.6 2.0 70 - 130 20<0.0002 <0.0002


Comment:

m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.

Page 3 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD




SDG I.D.: GBG91924

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult


95.8Total Cyanide BRL 96.8NC 85 - 115 300.64 1.02

QA/QC Batch 283319, QC Sample No: BG92589 (BG91936, BG91937, BG91938)99.0Total Cyanide BRL 98.0NC 85 - 115 20<0.01 <0.01

Page 4 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD




SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

QA/QC Batch 283615, QC Sample No: BG90281 (BG91924, BG91925, BG91926, BG91927, BG91928, BG91929)

Volatiles - Soil, Solid99 981,1,1,2-Tetrachloroethane ND 1.0102 101 1.0 70 - 130 30

98 1001,1,1-Trichloroethane ND 2.0103 101 2.0 70 - 130 30

96 971,1,2,2-Tetrachloroethane ND 1.099 100 1.0 70 - 130 30


98 1011,1-Dichloroethane ND 3.0102 101 1.0 70 - 130 30

71 701,1-Dichloroethene ND 1.4109 105 3.7 70 - 130 30

100 1001,1-Dichloropropene ND 0.0103 101 2.0 70 - 130 30

101 1021,2,3-Trichlorobenzene ND 1.093 94 1.1 70 - 130 30

98 991,2,3-Trichloropropane ND 1.0101 97 4.0 70 - 130 30


105 1041,2,4-Trimethylbenzene ND 1.092 92 0.0 70 - 130 30

106 1091,2-Dibromo-3-chloropropane ND 2.8101 101 0.0 70 - 130 30

98 991,2-Dibromoethane ND 1.099 100 1.0 70 - 130 30

104 1041,2-Dichlorobenzene ND 0.098 98 0.0 70 - 130 30


101 1011,2-Dichloropropane ND 0.0103 102 1.0 70 - 130 30






101 1012-Chlorotoluene ND 0.099 97 2.0 70 - 130 30

88 902-Hexanone ND 2.287 88 1.1 70 - 130 30

102 1032-Isopropyltoluene ND 1.0100 98 2.0 70 - 130 30


98 994-Methyl-2-pentanone ND 1.095 98 3.1 70 - 130 30

71 71Acetone ND 0.092 93 1.1 70 - 130 30

98 100Acrylonitrile ND 2.098 102 4.0 70 - 130 30

98 98Benzene ND 0.0102 100 2.0 70 - 130 30

100 100Bromobenzene ND 0.098 98 0.0 70 - 130 30

98 100Bromochloromethane ND 2.0102 104 1.9 70 - 130 30

97 99Bromodichloromethane ND 2.0105 104 1.0 70 - 130 30

88 92Bromoform ND 4.4100 101 1.0 70 - 130 30

68 72Bromomethane ND 5.7128 124 3.2 m70 - 130 30

65 65Carbon Disulfide ND 0.0109 108 0.9 m70 - 130 30

93 96Carbon tetrachloride ND 3.2103 100 3.0 70 - 130 30

102 102Chlorobenzene ND 0.0100 99 1.0 70 - 130 30

30 31Chloroethane ND 3.3113 111 1.8 m70 - 130 30

90 92Chloroform ND 2.299 98 1.0 70 - 130 30

93 99Chloromethane ND 6.3120 121 0.8 70 - 130 30

97 100cis-1,2-Dichloroethene ND 3.0101 102 1.0 70 - 130 30

Page 5 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

97 98cis-1,3-Dichloropropene ND 1.0103 101 2.0 70 - 130 30

96 97Dibromochloromethane ND 1.0105 106 0.9 70 - 130 30

99 99Dibromomethane ND 0.0101 100 1.0 70 - 130 30

85 94Dichlorodifluoromethane ND 10.1121 117 3.4 70 - 130 30

102 102Ethylbenzene ND 0.0102 99 3.0 70 - 130 30

106 107Hexachlorobutadiene ND 0.9100 98 2.0 70 - 130 30

100 99Isopropylbenzene ND 1.098 96 2.1 70 - 130 30

101 103m&p-Xylene ND 2.099 98 1.0 70 - 130 30

79 80Methyl ethyl ketone ND 1.379 84 6.1 70 - 130 30

82 99Methyl t-butyl ether (MTBE) ND 18.8104 99 4.9 70 - 130 30

95 96Methylene chloride ND 1.0102 102 0.0 70 - 130 30

100 99Naphthalene ND 1.094 96 2.1 70 - 130 30

105 105n-Butylbenzene ND 0.094 93 1.1 70 - 130 30

102 102n-Propylbenzene ND 0.093 91 2.2 70 - 130 30

102 101o-Xylene ND 1.099 98 1.0 70 - 130 30

103 103p-Isopropyltoluene ND 0.097 95 2.1 70 - 130 30

102 102sec-Butylbenzene ND 0.0102 99 3.0 70 - 130 30

100 101Styrene ND 1.098 98 0.0 70 - 130 30

102 102tert-Butylbenzene ND 0.099 97 2.0 70 - 130 30

101 102Tetrachloroethene ND 1.0100 98 2.0 70 - 130 30

97 100Tetrahydrofuran (THF) ND 3.095 100 5.1 70 - 130 30

101 101Toluene ND 0.0102 100 2.0 70 - 130 30

96 97trans-1,2-Dichloroethene ND 1.0109 107 1.9 70 - 130 30

98 99trans-1,3-Dichloropropene ND 1.0104 103 1.0 70 - 130 30

89 89trans-1,4-dichloro-2-butene ND 0.096 98 2.1 70 - 130 30

100 100Trichloroethene ND 0.0106 103 2.9 70 - 130 30

22 23Trichlorofluoromethane ND 4.4120 116 3.4 m70 - 130 30

84 85Trichlorotrifluoroethane ND 1.2106 102 3.8 70 - 130 30

102 111Vinyl chloride ND 8.5122 120 1.7 70 - 130 30

100 101% 1,2-dichlorobenzene-d4 97 1.0100 99 1.0 70 - 130 30

100 99% Bromofluorobenzene 100 1.099 98 1.0 70 - 130 30

98 98% Dibromofluoromethane 102 0.099 99 0.0 70 - 130 30

100 100% Toluene-d8 94 0.0101 100 1.0 70 - 130 30

Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.

Comment:


Volatiles - Ground Water98 981,1,1,2-Tetrachloroethane ND 0.0103 95 8.1 70 - 130 30















Page 6 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits








100 1002-Hexanone ND 0.084 91 8.0 70 - 130 30




99 93Acetone ND 6.373 88 18.6 70 - 130 30


92 93Benzene ND 1.1102 90 12.5 70 - 130 30

91 96Bromobenzene ND 5.399 88 11.8 70 - 130 30



97 100Bromoform ND 3.093 96 3.2 70 - 130 30

111 148Bromomethane ND 28.6110 96 13.6 m70 - 130 30

85 94Carbon Disulfide ND 10.1105 102 2.9 70 - 130 30



74 97Chloroethane ND 26.997 86 12.0 70 - 130 30

91 109Chloroform ND 18.090 86 4.5 70 - 130 30

77 89Chloromethane ND 14.598 86 13.0 70 - 130 30





69 78Dichlorodifluoromethane ND 12.287 75 14.8 m70 - 130 30

95 97Ethylbenzene ND 2.1112 89 22.9 70 - 130 30



94 96m&p-Xylene ND 2.1108 89 19.3 70 - 130 30




90 101Naphthalene ND 11.584 95 12.3 70 - 130 30



99 99o-Xylene ND 0.0109 92 16.9 70 - 130 30



101 100Styrene ND 1.0105 94 11.1 70 - 130 30




90 94Toluene ND 4.3102 88 14.7 70 - 130 30





82 94Trichlorofluoromethane ND 13.690 80 11.8 70 - 130 30

Page 7 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits


66 88Vinyl chloride ND 28.697 87 10.9 m70 - 130 30




98 99% Toluene-d8 100 1.0100 101 1.0 70 - 130 30

A blank MS/MSD was analyzed with this batch.


Comment:


Pesticides - Ground Water4,4' -DDD ND 97 98 1.0 40 - 140 20

4,4' -DDE ND 87 89 2.3 40 - 140 20

4,4' -DDT ND 89 90 1.1 40 - 140 20

a-BHC ND 88 87 1.1 40 - 140 20

a-Chlordane ND 86 89 3.4 40 - 140 20

Alachlor ND NA NA NC 40 - 140 20

Aldrin ND 56 60 6.9 40 - 140 20

b-BHC ND 91 93 2.2 40 - 140 20

Chlordane ND 88 89 1.1 40 - 140 20

d-BHC ND 91 93 2.2 40 - 140 20

Dieldrin ND 93 94 1.1 40 - 140 20

Endosulfan I ND 92 93 1.1 40 - 140 20

Endosulfan II ND 97 100 3.0 40 - 140 20

Endosulfan sulfate ND 92 93 1.1 40 - 140 20

Endrin ND 98 93 5.2 40 - 140 20

Endrin aldehyde ND 113 115 1.8 40 - 140 20

Endrin ketone ND 93 98 5.2 40 - 140 20

g-BHC ND 92 92 0.0 40 - 140 20

g-Chlordane ND 88 89 1.1 40 - 140 20

Heptachlor ND 80 77 3.8 40 - 140 20

Heptachlor epoxide ND 91 92 1.1 40 - 140 20

Methoxychlor ND 101 103 2.0 40 - 140 20

Toxaphene ND NA NA NC 40 - 140 20

% DCBP 85 91 91 0.0 30 - 150 20

% TCMX 85 92 80 14.0 30 - 150 20

Alpha and gamma chlordane were spiked and analyzed instead of technical chlordane. Gamma chlordane recovery is reported in the LCS, LCSD, MS and MSD.

Comment:

QA/QC Batch 282891, QC Sample No: BG91693 (BG91924)

Semivolatiles - Soil82 861,2,4,5-Tetrachlorobenzene ND 4.879 78 1.3 30 - 130 30



77 801,2-Diphenylhydrazine ND 3.888 87 1.1 30 - 130 30



81 862,4,5-Trichlorophenol ND 6.077 77 0.0 30 - 130 30


77 812,4-Dichlorophenol ND 5.174 73 1.4 30 - 130 30

56 572,4-Dimethylphenol ND 1.854 53 1.9 30 - 130 30

Page 8 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

11 112,4-Dinitrophenol ND 0.019 21 10.0 l,m30 - 130 30

75 792,4-Dinitrotoluene ND 5.273 73 0.0 30 - 130 30


84 862-Chloronaphthalene ND 2.480 79 1.3 30 - 130 30

74 762-Chlorophenol ND 2.771 69 2.9 30 - 130 30

72 762-Methylnaphthalene ND 5.470 69 1.4 30 - 130 30

74 772-Methylphenol (o-cresol) ND 4.071 68 4.3 30 - 130 30

106 1112-Nitroaniline ND 4.695 102 7.1 30 - 130 30

82 852-Nitrophenol ND 3.680 79 1.3 30 - 130 30

74 773&4-Methylphenol (m&p-cresol) ND 4.072 70 2.8 30 - 130 30

106 1123,3'-Dichlorobenzidine ND 5.5113 108 4.5 30 - 130 30

79 823-Nitroaniline ND 3.780 82 2.5 30 - 130 30

65 704,6-Dinitro-2-methylphenol ND 7.453 59 10.7 30 - 130 30

89 914-Bromophenyl phenyl ether ND 2.288 85 3.5 30 - 130 30

77 814-Chloro-3-methylphenol ND 5.173 73 0.0 30 - 130 30

57 574-Chloroaniline ND 0.060 61 1.7 30 - 130 30

76 814-Chlorophenyl phenyl ether ND 6.473 72 1.4 30 - 130 30

82 864-Nitroaniline ND 4.877 77 0.0 30 - 130 30

82 864-Nitrophenol ND 4.877 82 6.3 30 - 130 30

75 79Acenaphthene ND 5.272 71 1.4 30 - 130 30

75 79Acenaphthylene ND 5.271 71 0.0 30 - 130 30

81 84Acetophenone ND 3.679 78 1.3 30 - 130 30

64 65Aniline ND 1.670 70 0.0 30 - 130 30

81 81Anthracene ND 0.075 76 1.3 30 - 130 30

81 85Benz(a)anthracene ND 4.878 76 2.6 30 - 130 30

170 174Benzidine ND 2.3134 145 7.9 l,m30 - 130 30

80 81Benzo(a)pyrene ND 1.276 75 1.3 30 - 130 30

78 78Benzo(b)fluoranthene ND 0.081 76 6.4 30 - 130 30

81 81Benzo(ghi)perylene ND 0.071 73 2.8 30 - 130 30

79 79Benzo(k)fluoranthene ND 0.071 70 1.4 30 - 130 30

<10 <10Benzoic Acid ND NC<10 <10 NC l,m30 - 130 30

70 73Benzyl butyl phthalate ND 4.273 68 7.1 30 - 130 30

74 77Bis(2-chloroethoxy)methane ND 4.071 70 1.4 30 - 130 30

65 67Bis(2-chloroethyl)ether ND 3.063 62 1.6 30 - 130 30

69 72Bis(2-chloroisopropyl)ether ND 4.368 65 4.5 30 - 130 30

69 74Bis(2-ethylhexyl)phthalate ND 7.071 65 8.8 30 - 130 30

108 112Carbazole ND 3.6100 102 2.0 30 - 130 30

79 82Chrysene ND 3.775 74 1.3 30 - 130 30

88 87Dibenz(a,h)anthracene ND 1.175 77 2.6 30 - 130 30

78 83Dibenzofuran ND 6.275 76 1.3 30 - 130 30

77 81Diethyl phthalate ND 5.173 73 0.0 30 - 130 30

79 82Dimethylphthalate ND 3.775 74 1.3 30 - 130 30

80 84Di-n-butylphthalate ND 4.980 77 3.8 30 - 130 30

77 78Di-n-octylphthalate ND 1.377 69 11.0 30 - 130 30

82 84Fluoranthene ND 2.477 78 1.3 30 - 130 30

78 82Fluorene ND 5.073 73 0.0 30 - 130 30

81 82Hexachlorobenzene ND 1.280 77 3.8 30 - 130 30


51 55Hexachlorocyclopentadiene ND 7.548 52 8.0 30 - 130 30

73 76Hexachloroethane ND 4.071 70 1.4 30 - 130 30

86 86Indeno(1,2,3-cd)pyrene ND 0.075 77 2.6 30 - 130 30

77 80Isophorone ND 3.873 72 1.4 30 - 130 30

76 78Naphthalene ND 2.674 73 1.4 30 - 130 30

Page 9 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

76 78Nitrobenzene ND 2.673 72 1.4 30 - 130 30

58 52N-Nitrosodimethylamine ND 10.951 51 0.0 30 - 130 30

73 78N-Nitrosodi-n-propylamine ND 6.675 72 4.1 30 - 130 30

89 93N-Nitrosodiphenylamine ND 4.484 85 1.2 30 - 130 30

83 87Pentachloronitrobenzene ND 4.784 80 4.9 30 - 130 30

80 83Pentachlorophenol ND 3.778 78 0.0 30 - 130 30

80 82Phenanthrene ND 2.577 75 2.6 30 - 130 30

81 82Phenol ND 1.278 76 2.6 30 - 130 30

80 83Pyrene ND 3.777 77 0.0 30 - 130 30

45 38Pyridine ND 16.936 34 5.7 30 - 130 30

81 83% 2,4,6-Tribromophenol 77 2.481 79 2.5 30 - 130 30

79 81% 2-Fluorobiphenyl 71 2.577 74 4.0 30 - 130 30

67 69% 2-Fluorophenol 65 2.965 64 1.6 30 - 130 30

77 79% Nitrobenzene-d5 74 2.677 75 2.6 30 - 130 30

76 77% Phenol-d5 69 1.373 72 1.4 30 - 130 30

91 93% Terphenyl-d14 84 2.287 88 1.1 30 - 130 30

Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)

Comment:

QA/QC Batch 282971, QC Sample No: BG91830 (BG91924, BG91925, BG91926, BG91927, BG91928, BG91929, BG91930, BG91931, BG91932)

Pesticides - Soil, Solid82 784,4' -DDD ND 5.074 71 4.1 40 - 140 30

81 764,4' -DDE ND 6.476 71 6.8 40 - 140 30

86 834,4' -DDT ND 3.676 72 5.4 40 - 140 30

81 77a-BHC ND 5.179 75 5.2 40 - 140 30

80 77a-Chlordane ND 3.876 71 6.8 40 - 140 30

76 73Aldrin ND 4.074 69 7.0 40 - 140 30

82 79b-BHC ND 3.780 75 6.5 40 - 140 30

83 81Chlordane ND 2.476 71 6.8 40 - 140 30

78 74d-BHC ND 5.367 62 7.8 40 - 140 30

80 76Dieldrin ND 5.177 70 9.5 40 - 140 30

92 86Endosulfan I ND 6.769 65 6.0 40 - 140 30

81 64Endosulfan II ND 23.443 35 20.5 l40 - 140 30

92 83Endosulfan sulfate ND 10.351 49 4.0 40 - 140 30

79 74Endrin ND 6.580 75 6.5 40 - 140 30

63 63Endrin aldehyde ND 0.059 51 14.5 40 - 140 30

77 70Endrin ketone ND 9.570 68 2.9 40 - 140 30

80 78g-BHC ND 2.578 74 5.3 40 - 140 30

83 81g-Chlordane ND 2.476 71 6.8 40 - 140 30

79 78Heptachlor ND 1.377 73 5.3 40 - 140 30

79 74Heptachlor epoxide ND 6.576 72 5.4 40 - 140 30

92 80Methoxychlor ND 14.079 77 2.6 40 - 140 30

NA NAToxaphene ND NCNA NA NC 40 - 140 30

94 86% DCBP 100 8.998 94 4.2 30 - 150 30

91 88% TCMX 96 3.495 88 7.7 30 - 150 30

Alpha and gamma chlordane were spiked and analyzed instead of technical chlordane. Gamma chlordane recovery is reported in theLCS, LCSD, MS and MSD.

Comment:

Page 10 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

QA/QC Batch 282992, QC Sample No: BG91910 (BG91925, BG91926, BG91927, BG91928, BG91929, BG91930, BG91931, BG91932, BG91933, BG91934, BG91935)

Semivolatiles - Solid95 981,2,4,5-Tetrachlorobenzene ND 3.1104 102 1.9 30 - 130 30



86 891,2-Diphenylhydrazine ND 3.496 99 3.1 30 - 130 30





92 962,4-Dichlorophenol ND 4.3104 99 4.9 30 - 130 30

55 612,4-Dimethylphenol ND 10.371 66 7.3 30 - 130 30

<10 132,4-Dinitrophenol ND NC26 31 17.5 l,m30 - 130 30



90 922-Chloronaphthalene ND 2.298 95 3.1 30 - 130 30

82 852-Chlorophenol ND 3.689 87 2.3 30 - 130 30

91 922-Methylnaphthalene ND 1.1100 96 4.1 30 - 130 30

81 872-Methylphenol (o-cresol) ND 7.187 84 3.5 30 - 130 30

98 1192-Nitroaniline ND 19.4112 126 11.8 30 - 130 30

86 892-Nitrophenol ND 3.493 90 3.3 30 - 130 30

79 863&4-Methylphenol (m&p-cresol) ND 8.591 88 3.4 30 - 130 30

102 1343,3'-Dichlorobenzidine ND 27.1127 126 0.8 m30 - 130 30

100 1153-Nitroaniline ND 14.0114 113 0.9 30 - 130 30

44 684,6-Dinitro-2-methylphenol ND 42.962 71 13.5 r30 - 130 30

100 964-Bromophenyl phenyl ether ND 4.1104 97 7.0 30 - 130 30

91 964-Chloro-3-methylphenol ND 5.3102 97 5.0 30 - 130 30

72 814-Chloroaniline ND 11.881 74 9.0 30 - 130 30

91 914-Chlorophenyl phenyl ether ND 0.097 96 1.0 30 - 130 30

85 914-Nitroaniline ND 6.893 91 2.2 30 - 130 30

52 644-Nitrophenol ND 20.772 78 8.0 30 - 130 30

81 84Acenaphthene ND 3.689 85 4.6 30 - 130 30

85 88Acenaphthylene ND 3.592 90 2.2 30 - 130 30

83 86Acetophenone ND 3.690 88 2.2 30 - 130 30

71 78Aniline ND 9.488 82 7.1 30 - 130 30

89 92Anthracene ND 3.396 94 2.1 30 - 130 30

87 83Benz(a)anthracene ND 4.789 85 4.6 30 - 130 30

49 115Benzidine ND 80.5142 >200 NC l,r30 - 130 30

89 90Benzo(a)pyrene ND 1.194 91 3.2 30 - 130 30

87 90Benzo(b)fluoranthene ND 3.495 87 8.8 30 - 130 30

84 89Benzo(ghi)perylene ND 5.893 93 0.0 30 - 130 30

93 89Benzo(k)fluoranthene ND 4.492 91 1.1 30 - 130 30

<10 <10Benzoic Acid ND NC25 11 77.8 l,m,r30 - 130 30

106 97Benzyl butyl phthalate ND 8.9106 93 13.1 30 - 130 30

87 88Bis(2-chloroethoxy)methane ND 1.195 91 4.3 30 - 130 30

77 78Bis(2-chloroethyl)ether ND 1.383 81 2.4 30 - 130 30

79 80Bis(2-chloroisopropyl)ether ND 1.385 84 1.2 30 - 130 30

116 94Bis(2-ethylhexyl)phthalate ND 21.0112 95 16.4 30 - 130 30

115 129Carbazole ND 11.5128 134 4.6 l30 - 130 30

87 92Chrysene ND 5.694 93 1.1 30 - 130 30

83 89Dibenz(a,h)anthracene ND 7.093 93 0.0 30 - 130 30

Page 11 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

85 90Dibenzofuran ND 5.793 93 0.0 30 - 130 30

89 90Diethyl phthalate ND 1.197 92 5.3 30 - 130 30

87 89Dimethylphthalate ND 2.395 91 4.3 30 - 130 30

99 93Di-n-butylphthalate ND 6.3103 95 8.1 30 - 130 30

104 94Di-n-octylphthalate ND 10.1102 95 7.1 30 - 130 30

85 91Fluoranthene ND 6.894 95 1.1 30 - 130 30

87 88Fluorene ND 1.192 94 2.2 30 - 130 30

98 93Hexachlorobenzene ND 5.2101 95 6.1 30 - 130 30


49 55Hexachlorocyclopentadiene ND 11.556 60 6.9 30 - 130 30

76 78Hexachloroethane ND 2.684 82 2.4 30 - 130 30

85 90Indeno(1,2,3-cd)pyrene ND 5.793 94 1.1 30 - 130 30

93 95Isophorone ND 2.1101 97 4.0 30 - 130 30

88 90Naphthalene ND 2.296 93 3.2 30 - 130 30

79 82Nitrobenzene ND 3.786 85 1.2 30 - 130 30

68 72N-Nitrosodimethylamine ND 5.776 73 4.0 30 - 130 30

80 86N-Nitrosodi-n-propylamine ND 7.287 81 7.1 30 - 130 30

105 112N-Nitrosodiphenylamine ND 6.5114 114 0.0 30 - 130 30

100 99Pentachloronitrobenzene ND 1.0106 99 6.8 30 - 130 30

45 59Pentachlorophenol ND 26.967 64 4.6 30 - 130 30

91 92Phenanthrene ND 1.196 94 2.1 30 - 130 30

80 82Phenol ND 2.588 85 3.5 30 - 130 30

84 93Pyrene ND 10.296 97 1.0 30 - 130 30

49 55Pyridine ND 11.560 54 10.5 30 - 130 30

86 84% 2,4,6-Tribromophenol 84 2.494 87 7.7 30 - 130 30

88 88% 2-Fluorobiphenyl 85 0.095 92 3.2 30 - 130 30

80 81% 2-Fluorophenol 87 1.287 85 2.3 30 - 130 30

81 82% Nitrobenzene-d5 81 1.287 85 2.3 30 - 130 30

81 83% Phenol-d5 84 2.489 86 3.4 30 - 130 30

91 96% Terphenyl-d14 100 5.3102 104 1.9 30 - 130 30


Comment:

QA/QC Batch 283595, QC Sample No: BG91930 (BG91930, BG91931, BG91932, BG91933, BG91934, BG91935)

Volatiles - Solid101 1021,1,1,2-Tetrachloroethane ND 1.0103 102 1.0 70 - 130 30

















Page 12 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits






112 1072-Hexanone ND 4.693 96 3.2 70 - 130 30




74 70Acetone ND 5.678 83 6.2 70 - 130 30


102 101Benzene ND 1.0106 106 0.0 70 - 130 30

98 99Bromobenzene ND 1.0102 102 0.0 70 - 130 30



100 101Bromoform ND 1.099 100 1.0 70 - 130 30

92 92Bromomethane ND 0.0117 120 2.5 70 - 130 30

79 81Carbon Disulfide ND 2.5100 99 1.0 70 - 130 30



82 86Chloroethane ND 4.8107 105 1.9 70 - 130 30

106 106Chloroform ND 0.0108 108 0.0 70 - 130 30

89 94Chloromethane ND 5.5131 136 3.7 l70 - 130 30





73 82Dichlorodifluoromethane ND 11.6123 125 1.6 70 - 130 30

96 97Ethylbenzene ND 1.0102 99 3.0 70 - 130 30



95 96m&p-Xylene ND 1.098 99 1.0 70 - 130 30




109 105Naphthalene ND 3.7107 108 0.9 70 - 130 30



100 101o-Xylene ND 1.0102 102 0.0 70 - 130 30



100 100Styrene ND 0.0102 102 0.0 70 - 130 30




96 96Toluene ND 0.0100 101 1.0 70 - 130 30





81 84Trichlorofluoromethane ND 3.6103 100 3.0 70 - 130 30


85 90Vinyl chloride ND 5.7118 116 1.7 70 - 130 30

Page 13 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits




103 102% Toluene-d8 96 1.0103 104 1.0 70 - 130 30

A blank MS/MSD was analyzed with this batch.


Comment:


Pesticides - Solid73 774,4' -DDD ND 5.381 77 5.1 40 - 140 30

74 774,4' -DDE ND 4.081 79 2.5 40 - 140 30

71 734,4' -DDT ND 2.880 77 3.8 40 - 140 30

75 79a-BHC ND 5.282 80 2.5 40 - 140 30

76 79a-Chlordane ND 3.981 79 2.5 40 - 140 30

71 75Aldrin ND 5.578 76 2.6 40 - 140 30

80 83b-BHC ND 3.784 82 2.4 40 - 140 30

75 78Chlordane ND 3.982 79 3.7 40 - 140 30

75 78d-BHC ND 3.975 73 2.7 40 - 140 30

77 79Dieldrin ND 2.681 80 1.2 40 - 140 30

77 81Endosulfan I ND 5.176 75 1.3 40 - 140 30

77 80Endosulfan II ND 3.856 53 5.5 40 - 140 30

64 68Endosulfan sulfate ND 6.159 53 10.7 40 - 140 30

80 83Endrin ND 3.786 82 4.8 40 - 140 30

72 79Endrin aldehyde ND 9.370 59 17.1 40 - 140 30

73 77Endrin ketone ND 5.375 69 8.3 40 - 140 30

77 82g-BHC ND 6.382 79 3.7 40 - 140 30

75 78g-Chlordane ND 3.982 79 3.7 40 - 140 30

74 79Heptachlor ND 6.582 79 3.7 40 - 140 30

76 80Heptachlor epoxide ND 5.182 79 3.7 40 - 140 30

76 78Methoxychlor ND 2.682 79 3.7 40 - 140 30

NA NAToxaphene ND NCNA NA NC 40 - 140 30

86 89% DCBP 100 3.495 93 2.1 30 - 150 30

83 90% TCMX 97 8.195 92 3.2 30 - 150 30

Alpha and gamma chlordane were spiked and analyzed instead of technical chlordane. Gamma chlordane recovery is reported in theLCS, LCSD, MS and MSD.

Comment:


Polychlorinated Biphenyls - Soil, Solid95 101PCB-1016 ND 6.194 96 2.1 40 - 140 30

PCB-1221 ND 40 - 140 30

PCB-1232 ND 40 - 140 30

PCB-1242 ND 40 - 140 30

PCB-1248 ND 40 - 140 30

PCB-1254 ND 40 - 140 30

97 105PCB-1260 ND 7.9101 100 1.0 40 - 140 30

PCB-1262 ND 40 - 140 30

PCB-1268 ND 40 - 140 30

114 123% DCBP (Surrogate Rec) 113 7.6117 120 2.5 30 - 150 30

105 111% TCMX (Surrogate Rec) 104 5.6107 107 0.0 30 - 150 30

Page 14 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits


Polychlorinated Biphenyls - Ground WaterPCB-1016 ND 64 72 11.8 40 - 140 20

PCB-1221 ND 40 - 140 20

PCB-1232 ND 40 - 140 20

PCB-1242 ND 40 - 140 20

PCB-1248 ND 40 - 140 20

PCB-1254 ND 40 - 140 20

PCB-1260 ND 77 88 13.3 40 - 140 20

PCB-1262 ND 40 - 140 20

PCB-1268 ND 40 - 140 20

% DCBP (Surrogate Rec) 91 54 64 16.9 30 - 150 20

% TCMX (Surrogate Rec) 84 61 64 4.8 30 - 150 20

A LCS and LCS Duplicate were performed instead of a matrix spike and matrix spike duplicate.

Comment:


Semivolatiles - Ground Water1,2,4,5-Tetrachlorobenzene ND 91 86 5.6 30 - 130 20

1,2,4-Trichlorobenzene ND 88 85 3.5 30 - 130 20

1,2-Dichlorobenzene ND 74 73 1.4 30 - 130 20

1,2-Diphenylhydrazine ND 83 88 5.8 30 - 130 20



2,4,5-Trichlorophenol ND 92 89 3.3 30 - 130 20

2,4,6-Trichlorophenol ND 85 83 2.4 30 - 130 20

2,4-Dichlorophenol ND 89 87 2.3 30 - 130 20

2,4-Dimethylphenol ND 58 59 1.7 30 - 130 20

2,4-Dinitrophenol ND 60 58 3.4 30 - 130 20

2,4-Dinitrotoluene ND 91 87 4.5 30 - 130 20

2,6-Dinitrotoluene ND 86 86 0.0 30 - 130 20

2-Chloronaphthalene ND 85 85 0.0 30 - 130 20

2-Chlorophenol ND 74 73 1.4 30 - 130 20

2-Methylnaphthalene ND 85 83 2.4 30 - 130 20

2-Methylphenol (o-cresol) ND 71 71 0.0 30 - 130 20

2-Nitroaniline ND 101 102 1.0 30 - 130 20

2-Nitrophenol ND 85 88 3.5 30 - 130 20

3&4-Methylphenol (m&p-cresol) ND 74 76 2.7 30 - 130 20

3,3'-Dichlorobenzidine ND 138 135 2.2 l30 - 130 20

3-Nitroaniline ND 103 104 1.0 30 - 130 20

4,6-Dinitro-2-methylphenol ND 89 84 5.8 30 - 130 20

4-Bromophenyl phenyl ether ND 89 87 2.3 30 - 130 20

4-Chloro-3-methylphenol ND 89 87 2.3 30 - 130 20

4-Chloroaniline ND 63 70 10.5 30 - 130 20

4-Chlorophenyl phenyl ether ND 86 84 2.4 30 - 130 20

4-Nitroaniline ND 84 90 6.9 30 - 130 20

4-Nitrophenol ND 78 78 0.0 15 - 130 20

Acenaphthene ND 76 76 0.0 30 - 130 20

Acenaphthylene ND 80 81 1.2 30 - 130 20

Acetophenone ND 79 79 0.0 30 - 130 20

Aniline ND 27 28 3.6 l30 - 130 20

Anthracene ND 87 87 0.0 30 - 130 20

Page 15 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Benz(a)anthracene ND 89 89 0.0 30 - 130 20

Benzidine ND 19 23 19.0 l30 - 130 20

Benzo(a)pyrene ND 87 87 0.0 30 - 130 20

Benzo(b)fluoranthene ND 92 93 1.1 30 - 130 20

Benzo(ghi)perylene ND 94 89 5.5 30 - 130 20

Benzo(k)fluoranthene ND 78 83 6.2 30 - 130 20

Benzoic acid ND 58 55 5.3 30 - 130 20

Benzyl butyl phthalate ND 101 103 2.0 30 - 130 20

Bis(2-chloroethoxy)methane ND 82 84 2.4 30 - 130 20

Bis(2-chloroethyl)ether ND 71 73 2.8 30 - 130 20

Bis(2-chloroisopropyl)ether ND 75 79 5.2 30 - 130 20

Bis(2-ethylhexyl)phthalate ND 93 101 8.2 30 - 130 20

Carbazole ND 109 106 2.8 30 - 130 20

Chrysene ND 97 97 0.0 30 - 130 20

Dibenz(a,h)anthracene ND 90 87 3.4 30 - 130 20

Dibenzofuran ND 83 81 2.4 30 - 130 20

Diethyl phthalate ND 86 85 1.2 30 - 130 20

Dimethylphthalate ND 85 84 1.2 30 - 130 20

Di-n-butylphthalate ND 93 93 0.0 30 - 130 20

Di-n-octylphthalate ND 95 99 4.1 30 - 130 20

Fluoranthene ND 94 91 3.2 30 - 130 20

Fluorene ND 82 83 1.2 30 - 130 20

Hexachlorobenzene ND 87 90 3.4 30 - 130 20

Hexachlorobutadiene ND 86 83 3.6 30 - 130 20

Hexachlorocyclopentadiene ND 47 44 6.6 30 - 130 20

Hexachloroethane ND 74 75 1.3 30 - 130 20

Indeno(1,2,3-cd)pyrene ND 91 89 2.2 30 - 130 20

Isophorone ND 88 91 3.4 30 - 130 20

Naphthalene ND 82 83 1.2 30 - 130 20

Nitrobenzene ND 75 78 3.9 30 - 130 20

N-Nitrosodimethylamine ND 59 62 5.0 30 - 130 20

N-Nitrosodi-n-propylamine ND 72 75 4.1 30 - 130 20

N-Nitrosodiphenylamine ND 104 101 2.9 30 - 130 20

Pentachloronitrobenzene ND 96 95 1.0 30 - 130 20

Pentachlorophenol ND 76 72 5.4 30 - 130 20

Phenanthrene ND 87 86 1.2 30 - 130 20

Phenol ND 64 65 1.6 15 - 130 20

Pyrene ND 96 93 3.2 30 - 130 20

Pyridine ND 28 30 6.9 l30 - 130 20

% 2,4,6-Tribromophenol 93 82 90 9.3 15 - 110 20

% 2-Fluorobiphenyl 80 81 81 0.0 30 - 130 20

% 2-Fluorophenol 82 62 63 1.6 15 - 110 20

% Nitrobenzene-d5 99 76 78 2.6 30 - 130 20

% Phenol-d5 81 63 64 1.6 15 - 110 20

% Terphenyl-d14 95 101 100 1.0 30 - 130 20


Comment:

QA/QC Batch 283711, QC Sample No: BG92472 (BG91934 (50X) )

Volatiles - Solid101 1121,2,3-Trichlorobenzene ND 10.396 104 8.0 70 - 130 30


Page 16 of 17

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG91924

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits











106 113Bromobenzene ND 6.495 104 9.0 70 - 130 30



99 112Naphthalene ND 12.399 111 11.4 70 - 130 30










Comment:

l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.

MS - Matrix SpikePhyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

August 20, 2014MS Dup - Matrix Spike Duplicate

RPD - Relative Percent DifferenceLCS - Laboratory Control Sample

LCSD - Laboratory Control Sample Duplicate

NC - No CriteriaIntf - Interference

Page 17 of 17

Sample Criteria Exceedences ReportWednesday, August 20, 2014 Page 1 of 5

Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis

UnitsCriteria

GBG91924 - GEICONSCriteria: NY: 375, 375RS, GW

RLCriteria

State: NY

HG-SM Mercury 0.180.25 0.09 mg/KgBG91924 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SM Lead 63109 0.35 mg/KgBG91924 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$8260SMR Acetone 5056 28 ug/KgBG91925 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50

$PESTSMDPR 4,4' -DDE 3.325 2.7 ug/KgBG91926 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3$PESTSMDPR 4,4' -DDT 3.340 2.7 ug/KgBG91926 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3CD-SM Cadmium 2.52.74 0.33 mg/KgBG91926 NY / 375-6.8 Metals / Residential 2.5CD-SM Cadmium 2.52.74 0.33 mg/KgBG91926 NY / 375-6.8 Metals / Unrestricted Use Soil 2.5CR-SM Chromium 3058.5 0.33 mg/KgBG91926 NY / 375-6.8 Metals / Unrestricted Use SoilHG-SM Mercury 0.180.44 0.09 mg/KgBG91926 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SM Lead 63293 3.3 mg/KgBG91926 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SM Zinc 109652 3.3 mg/KgBG91926 NY / 375-6.8 Metals / Unrestricted Use Soil 109


$8260SMR Acetone 50100 30 ug/KgBG91928 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50HG-SM Mercury 0.811.04 0.07 mg/KgBG91928 NY / 375-6.8 Metals / Residential 0.81HG-SM Mercury 0.181.04 0.07 mg/KgBG91928 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SM Lead 6396.9 0.38 mg/KgBG91928 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$8270-SMR Benz(a)anthracene 10002800 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Residential 1000$8270-SMR Benzo(a)pyrene 10002600 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Residential 1000$8270-SMR Indeno(1,2,3-cd)pyrene 5001100 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Residential 500$8270-SMR Benzo(b)fluoranthene 10003300 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Residential 1000$8270-SMR Chrysene 10002900 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Residential 1000$8270-SMR Benzo(k)fluoranthene 10001200 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Residential 1000$8270-SMR Benzo(k)fluoranthene 8001200 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270-SMR Indeno(1,2,3-cd)pyrene 5001100 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270-SMR Benzo(b)fluoranthene 10003300 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270-SMR Benzo(a)pyrene 10002600 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270-SMR Benz(a)anthracene 10002800 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270-SMR Chrysene 10002900 270 ug/KgBG91930 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000PB-SM Lead 63206 4.0 mg/KgBG91930 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SM Zinc 109126 0.40 mg/KgBG91930 NY / 375-6.8 Metals / Unrestricted Use Soil 109


$8260SMR Methylene chloride 5053 6.3 ug/KgBG91934 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8270-SMR Benzo(a)pyrene 100020000 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Residential 1000$8270-SMR Indeno(1,2,3-cd)pyrene 5008400 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Residential 500$8270-SMR Dibenz(a,h)anthracene 330ND 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Residential 330$8270-SMR Chrysene 100024000 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Residential 1000



UnitsCriteria


RLCriteria

State: NY

$8270-SMR Benzo(k)fluoranthene 10008500 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Residential 1000$8270-SMR Benzo(b)fluoranthene 100028000 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Residential 1000$8270-SMR Benz(a)anthracene 100028000 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Residential 1000$8270-SMR Benzo(b)fluoranthene 100028000 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270-SMR Phenol 330ND 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270-SMR Benzo(k)fluoranthene 8008500 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270-SMR Benz(a)anthracene 100028000 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270-SMR Chrysene 100024000 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270-SMR Dibenz(a,h)anthracene 330ND 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270-SMR 2-Methylphenol (o-cresol) 330ND 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270-SMR Indeno(1,2,3-cd)pyrene 5008400 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270-SMR Pentachlorophenol 800ND 2100 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270-SMR Benzo(a)pyrene 100020000 1500 ug/KgBG91934 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$PCB_SMR PCB-1260 100270 82 ug/KgBG91934 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PESTSMDPR 4,4' -DDT 3.314 3.0 ug/KgBG91934 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3AS-SM Arsenic 1315.5 0.8 mg/KgBG91934 NY / 375-6.8 Metals / Unrestricted Use Soil 13BA-SM Barium 350480 0.39 mg/KgBG91934 NY / 375-6.8 Metals / Residential 350BA-SM Barium 350480 0.39 mg/KgBG91934 NY / 375-6.8 Metals / Unrestricted Use Soil 350CD-SM Cadmium 2.54.47 0.39 mg/KgBG91934 NY / 375-6.8 Metals / Residential 2.5CD-SM Cadmium 2.54.47 0.39 mg/KgBG91934 NY / 375-6.8 Metals / Unrestricted Use Soil 2.5CR-SM Chromium 3048.9 0.39 mg/KgBG91934 NY / 375-6.8 Metals / Unrestricted Use SoilCU-SM Copper 50135 0.39 mg/kgBG91934 NY / 375-6.8 Metals / Unrestricted Use Soil 50HG-SM Mercury 0.810.82 0.09 mg/KgBG91934 NY / 375-6.8 Metals / Residential 0.81HG-SM Mercury 0.180.82 0.09 mg/KgBG91934 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18NI-SM Nickel 3037.8 0.39 mg/KgBG91934 NY / 375-6.8 Metals / Unrestricted Use Soil 30PB-SM Lead 4001230 3.9 mg/KgBG91934 NY / 375-6.8 Metals / Residential 400PB-SM Lead 631230 3.9 mg/KgBG91934 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SM Zinc 109538 3.9 mg/KgBG91934 NY / 375-6.8 Metals / Unrestricted Use Soil 109

$8260SMR Acetone 5075 31 ug/KgBG91935 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50CR-SM Chromium 3036.4 0.38 mg/KgBG91935 NY / 375-6.8 Metals / Unrestricted Use Soil

$8260GWR Naphthalene 58.7 1.0 ug/LBG91936 NY / TAGM - Volatile Organics / Groundwater Standards 5$8260GWR 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.04$8260GWR 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.04$8260GWR 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.0006$8270-SIMR Benz(a)anthracene 0.0023.1 0.02 ug/LBG91936 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Benz(a)anthracene 0.0023.1 0.02 ug/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Chrysene 0.0023.0 0.02 ug/LBG91936 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Chrysene 0.0023.0 0.02 ug/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Benzo(b)fluoranthene 0.0023.0 0.02 ug/LBG91936 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Benzo(b)fluoranthene 0.0023.0 0.02 ug/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.002



UnitsCriteria


RLCriteria

State: NY

$8270-SIMR Benzo(k)fluoranthene 0.0021.0 0.02 ug/LBG91936 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Benzo(k)fluoranthene 0.0021.0 0.02 ug/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Benzo(a)pyrene 0.0022.2 0.02 ug/LBG91936 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.0021.0 0.02 ug/LBG91936 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.0021.0 0.02 ug/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.002$PEST_GAWR Dieldrin 0.01ND 0.035 ug/LBG91936 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Endrin 0.01ND 0.030 ug/LBG91936 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Heptachlor 0.01ND 0.020 ug/LBG91936 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Toxaphene 0.06ND 0.20 ug/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.06$PEST_GAWR Dieldrin 0.004ND 0.035 ug/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.004AL-WM Aluminum 0.1579 1.0 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.1AS-WM Arsenic 0.0250.498 0.020 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.025BA-WM Barium 19.96 0.20 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 1BE-WM Beryllium 0.0030.031 0.005 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.003CD-WM Cadmium 0.0050.017 0.005 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.005CR-WM Chromium 0.052.66 0.10 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.05CU-WM Copper 0.22.16 0.50 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.2D-AL Aluminum (Dissolved) 0.10.13 0.01 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.1D-MN Manganese (Dissolved) 0.30.823 0.001 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.3D-NA Sodium (Dissolved) 2055.8 0.11 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 20FE-WM Iron 0.31400 1.0 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.3HG-WM Mercury 0.00070.0008 0.0002 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.0007MG-WM Magnesium 35228 0.05 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 35MN-WM Manganese 0.356.5 0.10 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 2049.6 0.5 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 20NI-WM Nickel 0.11.38 0.10 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.1PB-WM Lead 0.0259.29 0.20 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 0.025ZN-WM Zinc 57.65 0.20 mg/LBG91936 NY / TOGS - Water Quality / GA Criteria 5

$8260GWR Naphthalene 55.7 1.0 ug/LBG91937 NY / TAGM - Volatile Organics / Groundwater Standards 5$8260GWR 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.04$8260GWR 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.04$8260GWR 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.0006$8270-SIMR Benz(a)anthracene 0.0020.40 0.02 ug/LBG91937 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Benz(a)anthracene 0.0020.40 0.02 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Chrysene 0.0020.38 0.02 ug/LBG91937 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Chrysene 0.0020.38 0.02 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Benzo(b)fluoranthene 0.0020.40 0.02 ug/LBG91937 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Benzo(b)fluoranthene 0.0020.40 0.02 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Benzo(k)fluoranthene 0.0020.12 0.02 ug/LBG91937 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Benzo(k)fluoranthene 0.0020.12 0.02 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Benzo(a)pyrene 0.0020.26 0.02 ug/LBG91937 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002



UnitsCriteria


RLCriteria

State: NY

$8270-SIMR Indeno(1,2,3-cd)pyrene 0.0020.12 0.02 ug/LBG91937 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.0020.12 0.02 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.002$PEST_GAWR Aldrin 0.01ND 0.016 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR a-BHC 0.01ND 0.050 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.01$PEST_GAWR b-BHC 0.05ND 0.053 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.05$PEST_GAWR b-BHC 0.04ND 0.053 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.04$PEST_GAWR d-BHC 0.04ND 0.050 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.04$PEST_GAWR Chlordane 0.1ND 0.30 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$PEST_GAWR Chlordane 0.05ND 0.30 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.05$PEST_GAWR 4,4' -DDD 0.01ND 0.030 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR 4,4' -DDE 0.01ND 0.027 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR 4,4' -DDT 0.01ND 0.030 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Dieldrin 0.01ND 0.15 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Dieldrin 0.004ND 0.15 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.004$PEST_GAWR Endosulfan I 0.1ND 0.11 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$PEST_GAWR Endrin 0.01ND 0.050 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Heptachlor 0.01ND 0.050 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Heptachlor 0.04ND 0.050 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.04$PEST_GAWR Heptachlor epoxide 0.01ND 0.050 ug/LBG91937 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Heptachlor epoxide 0.03ND 0.050 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.03$PEST_GAWR Alachlor 0.5ND 0.80 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.5$PEST_GAWR Toxaphene 0.06ND 2.0 ug/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.06AL-WM Aluminum 0.1288 0.10 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.1AS-WM Arsenic 0.0250.151 0.004 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.025BA-WM Barium 13.39 0.002 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 1BE-WM Beryllium 0.0030.015 0.001 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.003CD-WM Cadmium 0.0050.016 0.001 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.005CR-WM Chromium 0.051.29 0.001 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.05CU-WM Copper 0.20.963 0.005 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.2D-AL Aluminum (Dissolved) 0.10.31 0.11 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.1D-MN Manganese (Dissolved) 0.33.98 0.011 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.3D-NA Sodium (Dissolved) 2051.4 0.11 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 20FE-WM Iron 0.3714 0.10 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.3MG-WM Magnesium 35110 1.0 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 35MN-WM Manganese 0.325.5 0.10 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 2045.8 0.1 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 20NI-WM Nickel 0.10.673 0.001 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.1PB-WM Lead 0.0253.81 0.020 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.025SE-WM Selenium 0.010.011 0.01 mg/LBG91937 NY / TOGS - Water Quality / GA Criteria 0.01

$8260GWR 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.04$8260GWR 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.04



UnitsCriteria


RLCriteria

State: NY

$8260GWR 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.0006$8270-SIMR Benz(a)anthracene 0.0020.07 0.02 ug/LBG91938 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Benz(a)anthracene 0.0020.07 0.02 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Chrysene 0.0020.05 0.02 ug/LBG91938 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Chrysene 0.0020.05 0.02 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Benzo(b)fluoranthene 0.0020.05 0.02 ug/LBG91938 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Benzo(b)fluoranthene 0.0020.05 0.02 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Benzo(k)fluoranthene 0.0020.02 0.02 ug/LBG91938 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Benzo(k)fluoranthene 0.0020.02 0.02 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.002$8270-SIMR Benzo(a)pyrene 0.002ND 0.02 ug/LBG91938 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBG91938 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.002$PEST_GAWR Endrin 0.01ND 0.050 ug/LBG91938 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR 4,4' -DDD 0.01ND 0.050 ug/LBG91938 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Heptachlor 0.01ND 0.025 ug/LBG91938 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Heptachlor epoxide 0.01ND 0.025 ug/LBG91938 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR 4,4' -DDE 0.01ND 0.050 ug/LBG91938 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR 4,4' -DDT 0.01ND 0.050 ug/LBG91938 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$PEST_GAWR Chlordane 0.1ND 0.30 ug/LBG91938 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$PEST_GAWR Chlordane 0.05ND 0.30 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.05$PEST_GAWR a-BHC 0.01ND 0.025 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.01$PEST_GAWR Toxaphene 0.06ND 1.0 ug/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.06AL-WM Aluminum 0.1223 0.10 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.1AS-WM Arsenic 0.0250.156 0.004 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.025BA-WM Barium 12.23 0.002 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 1BE-WM Beryllium 0.0030.012 0.001 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.003CD-WM Cadmium 0.0050.009 0.001 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.005CR-WM Chromium 0.050.711 0.001 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.05CU-WM Copper 0.20.573 0.005 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.2D-AL Aluminum (Dissolved) 0.10.15 0.01 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.1D-MN Manganese (Dissolved) 0.33.50 0.011 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.3D-NA Sodium (Dissolved) 2057.2 0.11 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 20FE-WM Iron 0.3550 0.10 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.3MG-WM Magnesium 3594.0 0.10 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 35MN-WM Manganese 0.331.5 0.10 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 2056.4 0.1 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 20NI-WM Nickel 0.10.539 0.001 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.1PB-WM Lead 0.0250.207 0.002 mg/LBG91938 NY / TOGS - Water Quality / GA Criteria 0.025

Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.

NY Temperature NarrationAugust 20, 2014



SDG I.D.: GBG91924

The samples in this delivery group were received at 4°C.(Note acceptance criteria is above freezing up to 6°C)

Page 1 of 1

Appendix D _____________________________________________ Laboratory Data Deliverables for Soil Vapor

BG91920 - BG91923

Tuesday, August 19, 2014

Sample ID#s:

Attn: Erik CurranGEI Consultants, Inc. P.C.110 Walt Whitman Rd Suite 204Huntington Station, NY 11746

Project ID: 59-63 N 6TH STREET

Sincerely yours,

Laboratory DirectorPhyllis Shiller

If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.

NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B

NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301

This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.

This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.

A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.

587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823



AIRGEICONSStandard408950


EC

Laboratory Data

SV-2

Phoenix ID: BG91920

08/12/1410:5815:35

Parameterppbv

ResultppbvRL

ug/m3Result Date/Time By Reference



Date Time



SDG ID: GBG91920


ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 08/14/14 KCA TO15ND 11.00

0.5601,1,1-Trichloroethane 0.183 08/14/14 KCA TO153.05 1.00ND1,1,2,2-Tetrachloroethane 0.146 08/14/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 08/14/14 KCA TO15ND 1.002.351,1-Dichloroethane 0.247 08/14/14 KCA TO159.50 1.00ND1,1-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 08/14/14 KCA TO15ND 1.007.411,2,4-Trimethylbenzene 0.204 08/14/14 KCA TO1536.4 1.00ND1,2-Dibromoethane(EDB) 0.130 08/14/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 08/14/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 08/14/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 08/14/14 KCA TO15ND 1.001.891,3,5-Trimethylbenzene 0.204 08/14/14 KCA TO159.28 1.00ND1,3-Butadiene 0.452 08/14/14 KCA TO15ND 1.00ND1,3-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,4-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 08/14/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 08/14/14 KCA TO15ND 11.001.914-Ethyltoluene 0.204 08/14/14 KCA TO159.38 11.000.3304-Isopropyltoluene 0.182 08/14/14 KCA TO151.81 11.000.3204-Methyl-2-pentanone(MIBK) 0.244 08/14/14 KCA TO151.31 1.0060.6Acetone 0.421 08/14/14 KCA TO15144 1.00NDAcrylonitrile 0.461 08/14/14 KCA TO15ND 1.00

0.860Benzene 0.313 08/14/14 KCA TO152.74 1.00NDBenzyl chloride 0.193 08/14/14 KCA TO15ND 1.00

Page 1 of 12 Ver 1

SV-2Phoenix I.D.: BG91920


Parameterppbv

ResultppbvRL


ug/m3RL

NDBromodichloromethane 0.149 08/14/14 KCA TO15ND 1.00NDBromoform 0.097 08/14/14 KCA TO15ND 1.00NDBromomethane 0.258 08/14/14 KCA TO15ND 1.001.41Carbon Disulfide 0.321 08/14/14 KCA TO154.39 1.000.040Carbon Tetrachloride 0.040 08/14/14 KCA TO150.251 0.25NDChlorobenzene 0.217 08/14/14 KCA TO15ND 1.00NDChloroethane 0.379 08/14/14 KCA TO15ND 1.00

0.240Chloroform 0.205 08/14/14 KCA TO151.17 1.00NDChloromethane 0.484 08/14/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 08/14/14 KCA TO15ND 1.00

0.520Cyclohexane 0.291 08/14/14 KCA TO151.79 1.00NDDibromochloromethane 0.117 08/14/14 KCA TO15ND 1.00

0.230Dichlorodifluoromethane 0.202 08/14/14 KCA TO151.14 1.0014.4Ethanol 0.531 08/14/14 KCA TO1527.1 11.00NDEthyl acetate 0.278 08/14/14 KCA TO15ND 11.002.88Ethylbenzene 0.230 08/14/14 KCA TO1512.5 1.001.52Heptane 0.244 08/14/14 KCA TO156.22 1.00NDHexachlorobutadiene 0.094 08/14/14 KCA TO15ND 1.001.67Hexane 0.284 08/14/14 KCA TO155.88 1.001.95Isopropylalcohol 0.407 08/14/14 KCA TO154.79 1.000.220Isopropylbenzene 0.204 08/14/14 KCA TO151.08 1.0012.8m,p-Xylene 0.230 08/14/14 KCA TO1555.5 1.002.62Methyl Ethyl Ketone 0.339 08/14/14 KCA TO157.72 1.00NDMethyl tert-butyl ether(MTBE) 0.278 08/14/14 KCA TO15ND 1.00NDMethylene Chloride 0.288 08/14/14 KCA TO15ND 1.00

0.470n-Butylbenzene 0.182 08/14/14 KCA TO152.58 11.004.75o-Xylene 0.230 08/14/14 KCA TO1520.6 1.0025.3Propylene 0.581 08/14/14 KCA TO1543.5 11.00NDsec-Butylbenzene 0.182 08/14/14 KCA TO15ND 11.00

0.520Styrene 0.235 08/14/14 KCA TO152.21 1.000.980Tetrachloroethene 0.037 08/14/14 KCA TO156.64 0.252.41Tetrahydrofuran 0.339 08/14/14 KCA TO157.10 11.0013.6Toluene 0.266 08/14/14 KCA TO1551.2 1.00NDTrans-1,2-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 08/14/14 KCA TO15ND 1.00

0.180Trichloroethene 0.047 08/14/14 KCA TO150.967 0.252.32Trichlorofluoromethane 0.178 08/14/14 KCA TO1513.0 1.00NDTrichlorotrifluoroethane 0.130 08/14/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 08/14/14 KCA TO15ND 0.25

QA/QC Surrogates107% Bromofluorobenzene % 08/14/14 KCA TO15107 %

Page 2 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

Comments:





RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level

Page 3 of 12 Ver 1





EC

Laboratory Data

SV-4

Phoenix ID: BG91921

08/12/1411:0515:35

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBG91920


ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 08/14/14 KCA TO15ND 11.001.591,1,1-Trichloroethane 0.183 08/14/14 KCA TO158.67 1.00ND1,1,2,2-Tetrachloroethane 0.146 08/14/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 08/14/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 08/14/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 08/14/14 KCA TO15ND 1.001.481,2,4-Trimethylbenzene 0.204 08/14/14 KCA TO157.27 1.00ND1,2-Dibromoethane(EDB) 0.130 08/14/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 08/14/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 08/14/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 08/14/14 KCA TO15ND 1.00

0.4301,3,5-Trimethylbenzene 0.204 08/14/14 KCA TO152.11 1.00ND1,3-Butadiene 0.452 08/14/14 KCA TO15ND 1.00ND1,3-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,4-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 08/14/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 08/14/14 KCA TO15ND 11.00

0.3904-Ethyltoluene 0.204 08/14/14 KCA TO151.92 11.00ND4-Isopropyltoluene 0.182 08/14/14 KCA TO15ND 11.00

0.3404-Methyl-2-pentanone(MIBK) 0.244 08/14/14 KCA TO151.39 1.00316Acetone 0.421 08/14/14 KCA TO15750 1.00NDAcrylonitrile 0.461 08/14/14 KCA TO15ND 1.002.04Benzene 0.313 08/14/14 KCA TO156.51 1.00NDBenzyl chloride 0.193 08/14/14 KCA TO15ND 1.00

Page 4 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

NDBromodichloromethane 0.149 08/14/14 KCA TO15ND 1.00NDBromoform 0.097 08/14/14 KCA TO15ND 1.00NDBromomethane 0.258 08/14/14 KCA TO15ND 1.00

0.660Carbon Disulfide 0.321 08/14/14 KCA TO152.05 1.000.090Carbon Tetrachloride 0.040 08/14/14 KCA TO150.566 0.25NDChlorobenzene 0.217 08/14/14 KCA TO15ND 1.00NDChloroethane 0.379 08/14/14 KCA TO15ND 1.00NDChloroform 0.205 08/14/14 KCA TO15ND 1.00NDChloromethane 0.484 08/14/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 08/14/14 KCA TO15ND 1.001.12Cyclohexane 0.291 08/14/14 KCA TO153.85 1.00NDDibromochloromethane 0.117 08/14/14 KCA TO15ND 1.00

0.360Dichlorodifluoromethane 0.202 08/14/14 KCA TO151.78 1.0016.8Ethanol 0.531 08/14/14 KCA TO1531.6 11.00NDEthyl acetate 0.278 08/14/14 KCA TO15ND 11.001.64Ethylbenzene 0.230 08/14/14 KCA TO157.12 1.003.73Heptane 0.244 08/14/14 KCA TO1515.3 1.00NDHexachlorobutadiene 0.094 08/14/14 KCA TO15ND 1.003.92Hexane 0.284 08/14/14 KCA TO1513.8 1.005.78Isopropylalcohol 0.407 08/14/14 KCA TO1514.2 1.00NDIsopropylbenzene 0.204 08/14/14 KCA TO15ND 1.005.55m,p-Xylene 0.230 08/14/14 KCA TO1524.1 1.0010.0Methyl Ethyl Ketone 0.339 08/14/14 KCA TO1529.5 1.00NDMethyl tert-butyl ether(MTBE) 0.278 08/14/14 KCA TO15ND 1.00

0.350Methylene Chloride 0.288 08/14/14 KCA TO151.22 1.00NDn-Butylbenzene 0.182 08/14/14 KCA TO15ND 11.001.99o-Xylene 0.230 08/14/14 KCA TO158.64 1.007.53Propylene 0.581 08/14/14 KCA TO1513.0 11.00NDsec-Butylbenzene 0.182 08/14/14 KCA TO15ND 11.00NDStyrene 0.235 08/14/14 KCA TO15ND 1.00

0.090Tetrachloroethene 0.037 08/14/14 KCA TO150.610 0.2512.0Tetrahydrofuran 0.339 08/14/14 KCA TO1535.4 11.0015.7Toluene 0.266 08/14/14 KCA TO1559.1 1.00NDTrans-1,2-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 08/14/14 KCA TO15ND 1.00NDTrichloroethene 0.047 08/14/14 KCA TO15ND 0.25

0.460Trichlorofluoromethane 0.178 08/14/14 KCA TO152.58 1.00NDTrichlorotrifluoroethane 0.130 08/14/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 08/14/14 KCA TO15ND 0.25


Page 5 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

Comments:






Page 6 of 12 Ver 1





EC

Laboratory Data

SV-1

Phoenix ID: BG91922

08/12/1410:5515:35

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBG91920


ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 08/14/14 KCA TO15ND 11.003.861,1,1-Trichloroethane 0.183 08/14/14 KCA TO1521.0 1.00ND1,1,2,2-Tetrachloroethane 0.146 08/14/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 08/14/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 08/14/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 08/14/14 KCA TO15ND 1.007.641,2,4-Trimethylbenzene 0.204 08/14/14 KCA TO1537.5 1.00ND1,2-Dibromoethane(EDB) 0.130 08/14/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 08/14/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 08/14/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 08/14/14 KCA TO15ND 1.002.171,3,5-Trimethylbenzene 0.204 08/14/14 KCA TO1510.7 1.00ND1,3-Butadiene 0.452 08/14/14 KCA TO15ND 1.00ND1,3-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,4-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 08/14/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 08/14/14 KCA TO15ND 11.001.694-Ethyltoluene 0.204 08/14/14 KCA TO158.30 11.000.3404-Isopropyltoluene 0.182 08/14/14 KCA TO151.86 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 08/14/14 KCA TO15ND 1.0054.2Acetone 0.421 08/14/14 KCA TO15129 1.00NDAcrylonitrile 0.461 08/14/14 KCA TO15ND 1.00

0.600Benzene 0.313 08/14/14 KCA TO151.92 1.00NDBenzyl chloride 0.193 08/14/14 KCA TO15ND 1.00

Page 7 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

NDBromodichloromethane 0.149 08/14/14 KCA TO15ND 1.00NDBromoform 0.097 08/14/14 KCA TO15ND 1.00NDBromomethane 0.258 08/14/14 KCA TO15ND 1.00

0.840Carbon Disulfide 0.321 08/14/14 KCA TO152.61 1.000.060Carbon Tetrachloride 0.040 08/14/14 KCA TO150.377 0.25NDChlorobenzene 0.217 08/14/14 KCA TO15ND 1.00NDChloroethane 0.379 08/14/14 KCA TO15ND 1.001.96Chloroform 0.205 08/14/14 KCA TO159.56 1.00NDChloromethane 0.484 08/14/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 08/14/14 KCA TO15ND 1.00NDCyclohexane 0.291 08/14/14 KCA TO15ND 1.00NDDibromochloromethane 0.117 08/14/14 KCA TO15ND 1.00

0.310Dichlorodifluoromethane 0.202 08/14/14 KCA TO151.53 1.003.46Ethanol 0.531 08/14/14 KCA TO156.52 11.00NDEthyl acetate 0.278 08/14/14 KCA TO15ND 11.004.41Ethylbenzene 0.230 08/14/14 KCA TO1519.1 1.001.72Heptane 0.244 08/14/14 KCA TO157.04 1.00NDHexachlorobutadiene 0.094 08/14/14 KCA TO15ND 1.00

0.840Hexane 0.284 08/14/14 KCA TO152.96 1.001.09Isopropylalcohol 0.407 08/14/14 KCA TO152.68 1.000.310Isopropylbenzene 0.204 08/14/14 KCA TO151.52 1.0018.0m,p-Xylene 0.230 08/14/14 KCA TO1578.1 1.002.67Methyl Ethyl Ketone 0.339 08/14/14 KCA TO157.87 1.00NDMethyl tert-butyl ether(MTBE) 0.278 08/14/14 KCA TO15ND 1.00

0.490Methylene Chloride 0.288 08/14/14 KCA TO151.70 1.000.440n-Butylbenzene 0.182 08/14/14 KCA TO152.41 11.006.38o-Xylene 0.230 08/14/14 KCA TO1527.7 1.000.800Propylene 0.581 08/14/14 KCA TO151.38 11.00NDsec-Butylbenzene 0.182 08/14/14 KCA TO15ND 11.00

0.660Styrene 0.235 08/14/14 KCA TO152.81 1.0074.0Tetrachloroethene 0.037 08/14/14 KCA TO15502 0.252.00Tetrahydrofuran 0.339 08/14/14 KCA TO155.89 11.0019.0Toluene 0.266 08/14/14 KCA TO1571.6 1.00NDTrans-1,2-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 08/14/14 KCA TO15ND 1.00



Page 8 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

Comments:






Page 9 of 12 Ver 1





EC

Laboratory Data

SV-3

Phoenix ID: BG91923

08/12/1410:5915:35

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBG91920


ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 08/14/14 KCA TO15ND 11.00

0.5301,1,1-Trichloroethane 0.183 08/14/14 KCA TO152.89 1.00ND1,1,2,2-Tetrachloroethane 0.146 08/14/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 08/14/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 08/14/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 08/14/14 KCA TO15ND 1.005.241,2,4-Trimethylbenzene 0.204 08/14/14 KCA TO1525.7 1.00ND1,2-Dibromoethane(EDB) 0.130 08/14/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 08/14/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 08/14/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 08/14/14 KCA TO15ND 1.001.501,3,5-Trimethylbenzene 0.204 08/14/14 KCA TO157.37 1.00ND1,3-Butadiene 0.452 08/14/14 KCA TO15ND 1.00ND1,3-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,4-Dichlorobenzene 0.166 08/14/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 08/14/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 08/14/14 KCA TO15ND 11.001.284-Ethyltoluene 0.204 08/14/14 KCA TO156.29 11.000.2404-Isopropyltoluene 0.182 08/14/14 KCA TO151.32 11.001.174-Methyl-2-pentanone(MIBK) 0.244 08/14/14 KCA TO154.79 1.00112Acetone 0.421 08/14/14 KCA TO15266 1.00NDAcrylonitrile 0.461 08/14/14 KCA TO15ND 1.003.28Benzene 0.313 08/14/14 KCA TO1510.5 1.00NDBenzyl chloride 0.193 08/14/14 KCA TO15ND 1.00

Page 10 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

NDBromodichloromethane 0.149 08/14/14 KCA TO15ND 1.00NDBromoform 0.097 08/14/14 KCA TO15ND 1.00NDBromomethane 0.258 08/14/14 KCA TO15ND 1.0045.0Carbon Disulfide 0.321 08/14/14 KCA TO15140 1.000.110Carbon Tetrachloride 0.040 08/14/14 KCA TO150.692 0.25NDChlorobenzene 0.217 08/14/14 KCA TO15ND 1.00NDChloroethane 0.379 08/14/14 KCA TO15ND 1.00NDChloroform 0.205 08/14/14 KCA TO15ND 1.00NDChloromethane 0.484 08/14/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 08/14/14 KCA TO15ND 1.001.01Cyclohexane 0.291 08/14/14 KCA TO153.47 1.00NDDibromochloromethane 0.117 08/14/14 KCA TO15ND 1.00NDDichlorodifluoromethane 0.202 08/14/14 KCA TO15ND 1.003.45Ethanol 0.531 08/14/14 KCA TO156.50 11.00NDEthyl acetate 0.278 08/14/14 KCA TO15ND 11.005.47Ethylbenzene 0.230 08/14/14 KCA TO1523.7 1.003.64Heptane 0.244 08/14/14 KCA TO1514.9 1.00NDHexachlorobutadiene 0.094 08/14/14 KCA TO15ND 1.003.39Hexane 0.284 08/14/14 KCA TO1511.9 1.001.73Isopropylalcohol 0.407 08/14/14 KCA TO154.25 1.000.310Isopropylbenzene 0.204 08/14/14 KCA TO151.52 1.0018.3m,p-Xylene 0.230 08/14/14 KCA TO1579.4 1.006.38Methyl Ethyl Ketone 0.339 08/14/14 KCA TO1518.8 1.00NDMethyl tert-butyl ether(MTBE) 0.278 08/14/14 KCA TO15ND 1.00

0.320Methylene Chloride 0.288 08/14/14 KCA TO151.11 1.000.350n-Butylbenzene 0.182 08/14/14 KCA TO151.92 11.006.29o-Xylene 0.230 08/14/14 KCA TO1527.3 1.0018.7Propylene 0.581 08/14/14 KCA TO1532.2 11.00NDsec-Butylbenzene 0.182 08/14/14 KCA TO15ND 11.00

0.540Styrene 0.235 08/14/14 KCA TO152.30 1.000.540Tetrachloroethene 0.037 08/14/14 KCA TO153.66 0.2510.6Tetrahydrofuran 0.339 08/14/14 KCA TO1531.2 11.0032.0Toluene 0.266 08/14/14 KCA TO15120 1.00NDTrans-1,2-Dichloroethene 0.252 08/14/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 08/14/14 KCA TO15ND 1.00



Page 11 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

Comments:






Page 12 of 12 Ver 1

QA/QC Data

ParameterBlankppbv

SampleResultppbv

SampleDupppbv

DUPRPD




SDG I.D.: GBG91920

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlankug/m3

QA/QC Batch 283435, QC Sample No: BG91920 (BG91920, BG91921, BG91922, BG91923)

VolatilesND ND1,1,1,2-Tetrachloroethane ND NC121 ND ND 70 - 130 20ND

0.560 0.5601,1,1-Trichloroethane ND 0.0108 3.05 3.05 70 - 130 20ND

ND ND1,1,2,2-Tetrachloroethane ND NC104 ND ND 70 - 130 20ND

ND ND1,1,2-Trichloroethane ND NC107 ND ND 70 - 130 20ND

2.35 2.291,1-Dichloroethane ND 2.6102 9.50 9.26 70 - 130 20ND

ND ND1,1-Dichloroethene ND NC99 ND ND 70 - 130 20ND

ND ND1,2,4-Trichlorobenzene ND NC100 ND ND 70 - 130 20ND

7.41 7.371,2,4-Trimethylbenzene ND 0.5110 36.4 36.2 70 - 130 20ND

ND ND1,2-Dibromoethane(EDB) ND NC110 ND ND 70 - 130 20ND

ND ND1,2-Dichlorobenzene ND NC111 ND ND 70 - 130 20ND

ND ND1,2-Dichloroethane ND NC101 ND ND 70 - 130 20ND

ND ND1,2-dichloropropane ND NC99 ND ND 70 - 130 20ND

ND ND1,2-Dichlorotetrafluoroethane ND NC121 ND ND 70 - 130 20ND

1.89 1.891,3,5-Trimethylbenzene ND 0.0107 9.28 9.28 70 - 130 20ND

ND ND1,3-Butadiene ND NC100 ND ND 70 - 130 20ND



ND ND1,4-Dioxane ND NC105 ND ND 70 - 130 20ND

ND ND2-Hexanone(MBK) ND NC102 ND ND 70 - 130 20ND

1.91 1.884-Ethyltoluene ND 1.6110 9.38 9.24 70 - 130 20ND

0.330 0.3204-Isopropyltoluene ND 3.1107 1.81 1.76 70 - 130 20ND

0.320 0.3304-Methyl-2-pentanone(MIBK) ND 3.1101 1.31 1.35 70 - 130 20ND

61.6 59.4Acetone ND 3.6104 146 141 70 - 130 20ND

ND NDAcrylonitrile ND NC104 ND ND 70 - 130 20ND

0.860 0.840Benzene ND 2.499 2.74 2.68 70 - 130 20ND

ND NDBenzyl chloride ND NC129 ND ND 70 - 130 20ND

ND NDBromodichloromethane ND NC109 ND ND 70 - 130 20ND

ND NDBromoform ND NC128 ND ND 70 - 130 20ND

ND NDBromomethane ND NC104 ND ND 70 - 130 20ND

1.41 1.35Carbon Disulfide ND 4.3102 4.39 4.20 70 - 130 20ND

0.040 0.040Carbon Tetrachloride ND 0.0113 0.251 0.251 70 - 130 20ND

ND NDChlorobenzene ND NC104 ND ND 70 - 130 20ND

ND NDChloroethane ND NC98 ND ND 70 - 130 20ND

0.240 0.230Chloroform ND 4.398 1.17 1.12 70 - 130 20ND

ND NDChloromethane ND NC99 ND ND 70 - 130 20ND

ND NDCis-1,2-Dichloroethene ND NC108 ND ND 70 - 130 20ND

ND NDcis-1,3-Dichloropropene ND NC107 ND ND 70 - 130 20ND

0.520 0.570Cyclohexane ND 9.297 1.79 1.96 70 - 130 20ND

ND NDDibromochloromethane ND NC119 ND ND 70 - 130 20ND

0.230 0.220Dichlorodifluoromethane ND 4.4105 1.14 1.09 70 - 130 20ND

14.4 13.8Ethanol ND 4.391 27.1 26.0 70 - 130 20ND

Page 1 of 2

QA/QC Data

ParameterBlankppbv

SampleResultppbv

SampleDupppbv

DUPRPD

SDG I.D.: GBG91920

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlankug/m3

ND NDEthyl acetate ND NC116 ND ND 70 - 130 20ND

2.88 2.95Ethylbenzene ND 2.4111 12.5 12.8 70 - 130 20ND

1.52 1.56Heptane ND 2.694 6.22 6.39 70 - 130 20ND

ND NDHexachlorobutadiene ND NC90 ND ND 70 - 130 20ND

1.67 1.65Hexane ND 1.296 5.88 5.81 70 - 130 20ND

1.95 1.94Isopropylalcohol ND 0.5104 4.79 4.76 70 - 130 20ND

0.220 0.210Isopropylbenzene ND 4.7108 1.08 1.03 70 - 130 20ND

12.8 12.8m,p-Xylene ND 0.0113 55.5 55.5 70 - 130 20ND

2.62 2.54Methyl Ethyl Ketone ND 3.1104 7.72 7.49 70 - 130 20ND

ND NDMethyl tert-butyl ether(MTBE) ND NC108 ND ND 70 - 130 20ND

ND NDMethylene Chloride ND NC87 ND ND 70 - 130 20ND

0.470 0.510n-Butylbenzene ND 8.2109 2.58 2.80 70 - 130 20ND

4.75 4.76o-Xylene ND 0.2110 20.6 20.6 70 - 130 20ND

25.3 25.4Propylene ND 0.499 43.5 43.7 70 - 130 20ND

ND NDsec-Butylbenzene ND NC104 ND ND 70 - 130 20ND

0.520 0.530Styrene ND 1.9115 2.21 2.26 70 - 130 20ND

0.980 0.920Tetrachloroethene ND 6.3112 6.64 6.24 70 - 130 20ND

2.41 2.43Tetrahydrofuran ND 0.8105 7.10 7.16 70 - 130 20ND

13.6 13.3Toluene ND 2.2106 51.2 50.1 70 - 130 20ND

ND NDTrans-1,2-Dichloroethene ND NC102 ND ND 70 - 130 20ND

ND NDtrans-1,3-Dichloropropene ND NC115 ND ND 70 - 130 20ND

0.180 0.180Trichloroethene ND 0.0103 0.967 0.967 70 - 130 20ND

2.32 2.13Trichlorofluoromethane ND 8.5109 13.0 12.0 70 - 130 20ND

ND NDTrichlorotrifluoroethane ND NC99 ND ND 70 - 130 20ND

ND NDVinyl Chloride ND NC96 ND ND 70 - 130 20ND

107 109% Bromofluorobenzene 96 1.9101 107 109 70 - 130 2096

MS - Matrix SpikePhyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

August 19, 2014MS Dup - Matrix Spike Duplicate

RPD - Relative Percent DifferenceLCS - Laboratory Control Sample

LCSD - Laboratory Control Sample Duplicate

NC - No CriteriaIntf - Interference

Page 2 of 2

Sample Criteria Exceedences ReportTuesday, August 19, 2014 Page 1 of 1


UnitsCriteria

GBG91920 - GEICONSCriteria: NY: DOH

RLCriteria

State: NY

#Error*** No Data to Display ***

Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.

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