PGA NORTH – GROUNDWATER SAMPLING VALIDATION OF …DUP001-09142012 EB001-09142012 The calibration...

PVI1060_LVL_4.doc Created on 11/23/2012 1:07:00 PM

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PGA NORTH – GROUNDWATER SAMPLING VALIDATION OF LABORATORY RESULTS

TESTAMERICA LABORATORY (PHOENIX, AZ)

LABORATORY REPORT # PVI1060 DATED SEPTEMBER 20, 2012

LEVEL 4 – FULL QC DELIVERABLES EVALUATION

INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected six groundwater samples and three associated quality control samples on September 14, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 17, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09142012 PVI1060-01 Quality Control VOCs / Trip Blank EPA-MW11A-09142012 PVI1060-02 Groundwater VOCs EPA-MW2C-09142012 PVI1060-03 Groundwater VOCs and Perchlorate EPA-MW19C-09142012 PVI1060-04 Groundwater VOCs and Perchlorate EPA-MW4C-09142012 PVI1060-05 Groundwater VOCs and Perchlorate EPA-MW8C-09142012 PVI1060-06 Groundwater VOCs and Perchlorate EPA-MW58A-09142012 PVI1060-07 Groundwater VOCs DUP001-09142012 PVI1060-08 Quality Control VOCs / Field Duplicate or primary sample

EPA-MW58A-09142012 EB001-09142012 PVI1060-09 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method

8260B Perchlorate – EPA 314.0 Quality Control for the water samples is evaluated in the following checklist tables and comments. A summary of data quality for the samples analyzed is provided in the final page of this validation report.

SDMS DOCID# 1142995


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VALIDATION CHECKLIST SUMMARY PGA NORTH – GROUNDWATER SAMPLING

VOLATILE ORGANIC COMPOUNDS BY METHOD 8260B

PROJECT SPECIFIC SHORT LIST LEVEL 4 VALIDATION

REPORTED

PERFORMANCE ACCEPTABLE

DATA QUALIFIED -

REQUIREMENTS NO YES NO YES COMMENTS

GAS CHROMATOGRAPHY/ MASS SPECTROMETRY (GC/MS)

1. Holding times X X 2. Detection limits X X Yes – See note

#2 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X No 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X LEVEL 4 QC DELIVERABLES 10. Instrument tune / performance check X X 11. Initial calibration RRFs and %RSDs X X Yes 12. Continuing calibration RRFs and %Ds X X Yes 13. Internal standard retention times/areas X X 14. TIC search (Not required) X X 15. Run logs X X 16. Compound identification /quantitation X X

%R - percent recovery RPD - relative percent difference CCV – continuing calibration verification

COMMENTS: Performance was acceptable, with the following exceptions and/or notes. 1) The water samples were received chilled at an acceptable temperature of 3.5

degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on September 14, 2012. The samples were analyzed by September 18, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.

2) No sample dilutions were required to quantitate any VOCs. All reporting limits

are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these


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VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).

Sample ID Qualified VOCs (ug/L)

EPA-MW11A Chloroform = 0.52 J EPA-MW11A PCE = 0.46 J DUP001 Chloroform = 0.16 J

3) Results from two full suite method blanks were provided in association with the groundwater sample analyses. Acetone was detected in the method blank from batch 12I0648 at an estimated concentration of 4.99 ug/L. Acetone was not detected in any of the associated samples, and no action is required.

One trip blank was analyzed, with no VOCs detected. Results from one equipment blank were provided, with no VOCs detected.

4-5) TestAmerica provided results from two full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exception. The trichlorofluoromethane recovery in one LCS was high at 126 percent (upper control limit of 123 percent). Trichlorofluoromethane was not detected in any of the associated samples, and no action is required.

6-7) TestAmerica provided results from one set of project specific MS and MSD analyses

(spike on project sample EPA-MW11A), and from one set of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.

8) Three surrogates were spiked into each groundwater sample in support of the VOC

analyses. Surrogate recoveries were acceptable, ranging from 93 to 111 percent. 9) Sample DUP001 was submitted as a blind field duplicate of primary sample

EPA-MW58A. Precision between the duplicate sample results, measured as the relative percent difference (RPD) between the primary and duplicate sample results, is calculated in the following table. Results are presented in micrograms per liter (ug/L).

Sample ID Chloroform PCE TCE EPA-MW58A <1.0 4.2 1.8 DUP001 0.16 4.1 1.7 RPD (%) +/- RL 2.4 5.7 +/- RL – Results agree within a reporting limit increment.

Precision between the duplicate sample results is very good, with a maximum RPD between duplicate results of 5.7 percent.


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10) Results from several bromofluorobenzene instrument tunes were provided in

support of all sample analyses and calibrations. Frequency of tunes was acceptable for each analytical batch at 12 hours or less between tunes. Ion abundance criteria for each of the tunes were acceptable.

11) Results were provided from two initial calibrations associated with the VOC

analyses in this SDG. One calibration is dated July 9, 2012 (GCMS#4), and the other is dated September 18, 2012 (GCMS#9).

The July 9, 2012 initial calibration is associated with the following samples:

TB001-09142012 EPA-MW2C-09142012 EPA-MW19C-09142012 EPA-MW4C-09142012 EPA-MW8C-09142012

The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compounds. Low end standards for acetone (three) and 2-butanone (two) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, methylene chloride, trans-1,2-DCE, cis-1,2-DCE, and 1,1,1-TCA were quantified from linear calibrations. The correlation coefficients for these calibrations were acceptable at 0.995 or greater. A 25 ug/L second source calibration standard was analyzed on July 9, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.

The September 18, 2012 calibration is associated with the following samples:

EPA-MW11A-09142012 EPA-MW58A-09142012

DUP001-09142012 EB001-09142012 The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compounds, with the exception of 2-butanone at 0.037. 2-Butanone was not detected in any of the associated samples. Due to the low calibration response, 2-butanone results for the samples listed above are qualified as R/Rejected. Low end


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standards for acetone (three) and 2-butanone (two) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, methylene chloride was quantified from a linear calibration. The correlation coefficient for this calibration was acceptable at 0.999. A 25 ug/L second source calibration standard was analyzed on September 18, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.

12) TestAmerica provided results from two sets of continuing calibration verification

(CCV) standard analyses. Both CCVs are dated September 18, 2012. The CCVs are distinguished by the ICAL date and the GCMS instrument number.

September 18, 2012 (GCMS-#9) - This CCV is associated with the all groundwater samples in this SDG analyzed on instrument GCMS #9 under the September 18, 2012 initial calibration Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05, with the exception of that for 2-butanone at 0.044. 2-Butanone results are already qualified due to the initial calibration. September 18, 2012 (GCMS-#4) - This CCV is associated with the all groundwater samples in this SDG analyzed on instrument GCMS#4 under the July 9, 2012 initial calibration Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05.

13) Three internal standards were reported for each sample analyzed. Standard areas (responses) were within –50 and +100 percent of the associated standard. Retention times were within 30 seconds of the associated standard.

14) Results for tentatively Identified Compounds (TICs) were not required for the

PGAN investigation.


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15) TestAmerica provided results of all appropriate run logs shown analytical sequences of standards and samples.

16) Reconstructed ion chromatograms were reviewed for each of the samples in this SDG.

Chromatographic peaks were verified for each VOC reported as detected. Retention times were verified against quantitation reports for each of the detections. Quantitation reports were reviewed for each of the samples. Concentrations were verified against the Form I data reports for all detections and were found to be consistent for each sample.


PERCHLORATE – EPA METHOD 314.0 LEVEL 4 VALIDATION

REPORTED / EVALUATED


DATA QUALIFIED -


EPA METHOD 314.0– ION CHROMATOGRAPHY

1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X Yes 4. Initial and Continuing Calibration %R X X 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only LEVEL 4 QC DELIVERABLES 9. Initial Calibration and Verification X X 10. Continuing Calibration Verification X X 11. Retention Times X X 12. Results Quantitation X X

%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The groundwater samples were received by TestAmerica on September 17, 2012.

The water samples were received chilled at a temperature of 3.5 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by September 18, 2012, within prescribed holding times.

2) No sample dilutions were required to quantitate perchlorate. Reporting limits are

determined to be acceptable.


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3) Results from one method blank were provided in support of the groundwater sample

analyses, with no perchlorate detected. Results from one equipment blank were also provided. Perchlorate was detected in the equipment blank at an estimated concentration of 1.2 ug/L. Perchlorate was detected in several samples at concentrations within 5 times that of the equipment blank. Due to potential blank contamination bias, the following perchlorate results are qualified as U/non-detect at the concentration reported.

Sample ID Qualified Perchlorate (ug/L) EPA-MW2C Perchlorate = 4.7 U EPA-MW19C Perchlorate = 2.8 U EPA-MW4C Perchlorate = 2.6 U EPA-MW8C Perchlorate = 2.1 U

4) Results from continuing calibration analyses are described in note #9. 5-6) TestAmerica provided results from one set of project specific MS and MSD

analyses in support of the perchlorate analyses (spike on project sample EPA-MW2C). Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were each 91 percent, with an RPD between MS and MSD recoveries of 0.5 percent.

7) TestAmerica provided results from one set of LCS and LCS duplicate analyses in

support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries were 92 and 102 percent. The RPD between LCS and LCSD results was acceptable at 11 percent.

8) Field duplicate samples were not collected with this chain-of-custody in support of

the perchlorate analyses.

TestAmerica provided results from one set of project specific laboratory duplicate sample analyses (duplicate of project sample EPA-MW8C). Laboratory duplicate precision is acceptable, as the results are in agreement within a reporting limit increment (the RPD of 43 percent is not evaluated in this situation).

9) Results from one 5-point initial calibration (standard levels of 2 ug/L, 5 ug/L, 10

ug/L, 25 ug/L, and 50 ug/L) dated May 29, 2012 were provided. The correlation coefficient for the calibration was acceptable at 0.9994. A mid range initial performance check (IPC) standard (25 ug/L) was analyzed following the initial calibration with an acceptable recovery of 93.2 percent

10) Perchlorate analyses were performed under one continuing calibration dated

September 18, 2012. This continuing calibration is associated with all samples


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analyzed under this SDG. Results for the continuing calibration are described below: September 18, 2012 - Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 6.1 percent. The IPC recovery was acceptable at 88.4 percent (control limits of 80 – 120 percent). Results from an initial calibration check standard (ICCS) at 2 ug/L were provided with an acceptable 104 percent recovery (upper control limit of 125 percent). Results from one continuing calibration check standard (CCC) analysis at 25 ug/L were provided with an acceptable recovery of 104 percent. Results from one CCC analysis at 40 ug/L were provided with acceptable recovery of 101 percent. Results from one ending calibration standard were provided at 40 ug/L, with a recovery of 89 percent.

11) Retention times for perchlorate were within +/- 10 percent of the associated standard

retention times. 12) All ion chromatograms from the September 18, 2012 analyses were reviewed to

verify that the sample results reported matched those presented in the raw data, and that dilution factors were correctly applied.


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Geomatrix Consultants, Inc. (Geomatrix) collected six groundwater samples and three associated quality control samples on September 14, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)

Reason(s) For Qualification

EPA-MW11A-09142012 / Chloroform and PCE DUP001-09142012 / Chloroform

J/Estimated

These VOCs were reported at

concentrations between the method detection limit and the

reporting limit. Accuracy in this portion of the calibration curve

may be limited. EPA-MW2C-09142012 / Perchlorate EPA-MW19C-09142012 / Perchlorate EPA-MW4C-09142012 / Perchlorate EPA-MW8C-09142012 / Perchlorate

U/Non-detect at

the concentrations

reported

Perchlorate was detected in the

equipment blank at a concentration within 5 times

those of the samples. Perchlorate detections may be

the result of blank contamination bias.

EPA-MW11A-09142012, EPA-MW58A-09142012, and DUP001-09142012/ 2-Butanone

R/Rejected

2-Butanone was not detected in the groundwater samples. The

response factors in the initial and continuing calibrations were less

than 0.05 indicating that 2-butanone data are not reliable.

SIGNATURE:

DATE:

September 25, 2012, Revised for Level 4 January 5, 2013.


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INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 11 groundwater samples and four associated quality control samples on September 20 and 211, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 24, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09202012 PVI1553-01 Quality Control VOCs / Trip Blank EPA-MW17C-09202012 PVI1553-02 Groundwater VOCs EPA-MW54A-09202012 PVI1553-03 Groundwater VOCs EPA-MW36A-09202012 PVI1553-04 Groundwater VOCs EPA-MW22C-09202012 PVI1553-05 Groundwater VOCs and Perchlorate EPA-MW18A-09202012 PVI1553-06 Groundwater VOCs EB001-09202012 PVI1553-07 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW43A-09212012 PVI1553-08 Groundwater VOCs EPA-MW10C-09212012 PVI1553-09 Groundwater VOCs DUP001-09212012 PVI1553-10 Quality Control VOCs / Field Duplicate or primary sample

EPA-MW10C-09212012 EPA-MW9C-09212012 PVI1553-11 Groundwater VOCs EPA-MW10A-09212012 PVI1553-12 Groundwater VOCs EPA-MW38A-09212012 PVI1553-13 Groundwater VOCs EPA-MW16A-09212012 PVI1553-14 Groundwater VOCs EB001-09212012 PVI1553-15 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



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PROJECT SPECIFIC SHORT LIST

LEVEL 4 VALIDATION

REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X LEVEL 4 QC DELIVERABLES 10. Instrument tune / performance check X X 11. Initial calibration RRFs and %RSDs X X Yes 12. Continuing calibration RRFs and %Ds X X Yes 13. Internal standard retention times/areas X X 14. TIC search (Not required) X X 15. Run logs X X 16. Compound identification /quantitation X X



degrees Celsius on wet ice. This temperature is below the recommended minimum temperature of 2 degrees Celsius. No action is taken, as the samples were not frozen. The groundwater samples were properly preserved with


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hydrochloric acid at the time of collection on September 20 and 21, 2012. The samples were analyzed by September 26, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.


are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).


EPA-MW17C Chloroform = 0.63 J EPA-MW17C Carbon tetrachloride = 0.66 J EPA-MW54A Chloroform = 0.44 J EPA-MW54A TCE = 0.22 J EPA-MW18A PCE = 0.57 J EPA-MW18A TCE = 0.91 J EPA-MW10C Chloroform = 0.24 J DUP001 Chloroform = 0.21 J EPA-MW9C Chloroform = 0.21 J EPA-MW10A Chloroform = 0.23 J

EPA-MW38A Chloroform = 0.25 J EPA-MW16A Chloroform = 0.29 J

3) Results from one full suite method blank were provided in association with the groundwater sample analyses. Acetone was detected in the method blank at an estimated concentration of 5.88 ug/L. Acetone was not detected in the associated samples, and no action is required. Results from one trip blank were provided. No VOCs were detected in the trip blank. Results from two equipment blanks were provided. Chloroform was detected in the equipment blanks collected on September 20 and 21, 2012, at estimated concentrations of 0.70 ug/L and 0.90 ug/L, respectively. All chloroform detections for the groundwater samples are at concentration equal to or less than these in the equipment blanks. Due to potential blank contamination bias, ass


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chloroform results are qualified as U/non-detect at the concentrations reported, as follows.

Sample ID Qualified VOCs (ug/L) EPA-MW17C Chloroform = 0.63 U EPA-MW54A Chloroform = 0.44 U EPA-MW18A Chloroform = 2.4 U EPA-MW10C Chloroform = 0.24 U DUP001 Chloroform = 0.21 U EPA-MW9C Chloroform = 0.21 U EPA-MW10A Chloroform = 0.23 U EPA-MW38A Chloroform = 0.25 U EPA-MW16A Chloroform = 0.29 U

4-5) TestAmerica provided results from one full set of laboratory control sample (LCS)

and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.


(spike on project sample EPA-MW43A) in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable for all VOCs.



EPA-MW10C. TCE was detected in the primary or duplicate samples at concentrations of 4.4 ug/L and 4.6 ug/L, respectively. Precision between the TCE detections is acceptable, with an RPD of 4.4 percent. Chloroform was detected in both samples at estimated concentrations. Both chloroform results are qualified due to blank contamination, and precision for chloroform is not calculated. Field duplicate precision is determined to be acceptable.



11) Results were provided from one initial calibration associated with the VOC

analyses in this SDG. The initial calibration is dated September 24, 2012 and was performed on instrument GCMS#2. The September 24, 2012 initial calibration is associated with analysis of all groundwater samples in this SDG.


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The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compound, with the exception of 2-butanone at 0.028. 2-Butanone was not detected in any of the associated samples. Due to the low initial calibration response, all 2-butanone sample results are qualified as R/Rejected. Low end standards for acetone (four) and 2-butanone (two) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, no linear calibrations were required. A 25 ug/L second source calibration standard was analyzed on September 24, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.

12) TestAmerica provided results from one set of continuing calibration verification

(CCV) standard analyses dated September 25, 2012. The September 25, 2012 CCV is associated with all groundwater samples analyzed under this SDG.

September 25, 2012 - This CCV is associated with the all groundwater samples in this SDG analyzed on instrument GCMS #2 under the September 24, 2012 initial calibration Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05, within the exception of that for 2-butanone at 0.027. 2-Butanone results are already qualified as R/Rejected due to the initial calibration, and no further action is required.



PGAN investigation. 15) TestAmerica provided results of all appropriate run logs shown analytical

sequences of standards and samples.


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16) Reconstructed ion chromatograms were reviewed for each of the samples in this SDG. Chromatographic peaks were verified for each VOC reported as detected. Retention times were verified against quantitation reports for each of the detections. Quantitation reports were reviewed for each of the samples. Concentrations were verified against the Form I data reports for all detections and were found to be consistent for each sample.

VALIDATION CHECKLIST SUMMARY

PGA NORTH – GROUNDWATER SAMPLING PERCHLORATE – EPA METHOD 314.0

LEVEL 4 VALIDATION



DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only LEVEL 4 QC DELIVERABLES 9. Initial Calibration and Verification X X 10. Continuing Calibration Verification X X 11. Retention Times X X 12. Results Quantitation X X


The water samples were received chilled at a temperature of 0.6 degrees Celsius on wet ice. This temperature is below the recommended minimum temperature of 2 degrees Celsius. No action is taken, as the samples were not frozen. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by September 27, 2012, within prescribed holding times.




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analyses, with no perchlorate detected. Results from two equipment blanks were also provided, with no perchlorate detected.

4) Results from continuing calibration analyses are described in note #9. 5-6) TestAmerica provided results from one set of batch specific MS and MSD analyses

in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were each 98 percent, with an RPD between MS and MSD recoveries of 0.4 percent.



8) Field duplicate samples were not collected in support of perchlorate with the

samples under this chain-of-custody.

TestAmerica provided results from one set of batch specific laboratory duplicate sample analyses. Laboratory duplicate precision is acceptable, with an RPD of 2.0 percent between primary and duplicate sample results.

9) Perchlorate analyses were initially performed under a May 29, 2012 initial

calibration. However, this calibration was not supported during the continuing calibration due to poor resolution. Therefore, all perchlorate samples were re-analyzed under a new initial calibration dated September 26, 2012.

Results from one 5-point initial calibration (standard levels of 2 ug/L, 5 ug/L, 10 ug/L, 25 ug/L, and 50 ug/L) dated September 26, 2012 were provided. The correlation coefficient for the calibration was acceptable at 0.9999. A mid range initial performance check (IPC) standard (25 ug/L) was analyzed following the initial calibration with an acceptable recovery of 97.6 percent

10) Perchlorate analyses were performed under one continuing calibration dated

September 27, 2012. This continuing calibration is associated with all samples analyzed under this SDG. Results for the continuing calibration are described below: September 27, 2012 - Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 18.7 percent (upper drift control limit of 20 percent). The IPC recovery was acceptable at 101 percent (control limits of 80 – 120 percent). Results from an initial calibration check standard (ICCS) at 2 ug/L were provided with an acceptable 99 percent recovery. Results from one continuing calibration check standard (CCC)


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analysis at 25 ug/L were provided with an acceptable recovery of 101 percent. Results from one ending calibration standard were provided at 40 ug/L, with an acceptable recovery of 107 percent.


retention times. 12) All ion chromatograms from the September 27, 2012 analyses were reviewed to



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Geomatrix Consultants, Inc. (Geomatrix) collected 11 groundwater samples and four associated quality control samples on September 20 and 211, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW17C-09202012 / Carbon tetrachloride EPA-MW54A-09202012 / TCE EPA-MW18A-09202012 / PCE EPA-MW18A-09202012 / TCE

J/Estimated




may be limited. EPA-MW17C-09202012 / Chloroform EPA-MW54A-09202012 / Chloroform EPA-MW10C-09212012 / Chloroform DUP001-09212012 / Chloroform EPA-MW9C-09212012 / Chloroform EPA-MW18A-09202012 / Chloroform EPA-MW10A-09212012 / Chloroform EPA-MW38A-09212012 / Chloroform EPA-MW16A-09212012 / Chloroform

U/Non-detect at

the concentrations

reported

Chloroform was detected in the associated equipment blanks at concentrations within 5 times

those of the groundwater samples. Chloroform detections

may be the results of blank contamination bias.

All groundwater samples / 2-Butanone

R/Rejected




SIGNATURE:

DATE:

October 9, 2012, Revised for Level 4 January 5, 2013.


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LABORATORY REPORT # PVI1869 DATED OCTOBER 3, 2012


INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 14 groundwater samples and five associated quality control samples on September 27, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 27, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09272012 PVI1869-01 Quality Control VOCs / Trip Blank MW18-09272012 PVI1869-02 Groundwater VOCs MW12-09272012 PVI1869-03 Groundwater VOCs EB001-09272012 PVI1869-04 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW35A-09272012 PVI1869-05 Groundwater VOCs IR34B-09272012 PVI1869-06 Groundwater VOCs GCLake-09272012 PVI1869-07 Groundwater VOCs IR3B-09272012 PVI1869-08 Groundwater VOCs MW16-09272012 PVI1869-09 Groundwater VOCs DUP001-09272012 PVI1869-10 Quality Control VOCs / Field Duplicate or primary sample

MW16-09272012 EA07-09272012 PVI1869-11 Groundwater VOCs MW15-09272012 PVI1869-12 Groundwater VOCs EPA-MW42A-09272012 PVI1869-13 Groundwater VOCs and Perchlorate EPA-MW26A-09272012 PVI1869-14 Groundwater VOCs MW25-09272012 PVI1869-15 Groundwater VOCs EPA-MW62A-09272012 PVI1869-16 Groundwater VOCs and Perchlorate DUP002-09272012 PVI1869-17 Quality Control VOCs and Perchlorate / Field duplicate or

primary sample EPA-MW62A-09272012 EPA-MW23A-09272012 PVI1869-18 Groundwater VOCs EB002-09272012 PVI1869-19 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method

8260B Perchlorate – EPA 314.0


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Quality Control for the water samples is evaluated in the following checklist tables and comments. A summary of data quality for the samples analyzed is provided in the final page of this validation report.




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X Yes 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X See Note #8. 9. Field Duplicate Comparison X X LEVEL 4 QC DELIVERABLES 10. Instrument tune / performance check X X 11. Initial calibration RRFs and %RSDs X X 12. Continuing calibration RRFs and %Ds X X 13. Internal standard retention times/areas X X 14. TIC search (Not required) X X 15. Run logs X X 16. Compound identification /quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on September 27, 2012. The samples were analyzed by October 1, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.


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2) Sample MW12 was diluted by a factor of 20 times for TCE only. Samples EPA-MW62A and DUP002-09272012 were diluted by factors of 5 times each for TCE only. No other sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).


MW18 Chloroform = 0.28 J MW12 Chloroform = 0.78 J GCLake Chloroform = 0.22 J IR3B Chloroform = 0.32 J MW16 Chloroform = 0.24 J DUP001-09272012 Chloroform = 0.29 J EA07 Acetone = 4.2 J MW15 Chloroform = 0.31 J EPA-MW26A Chloroform = 0.50 J MW25 Chloroform = 0.38 J EPA-MW62A Chloroform = 0.44 J EPA-MW62A 1,1-DCE = 0.25 J EPA-MW62A Acetone = 3.8 J DUP002-09272012 Chloroform = 0.56 J DUP002-09272012 PCE = 0.23 J EPA-MW23A Chloroform = 0.35 J

3) Results from two full suite VOC method blanks were provided in association with the groundwater sample analyses. No VOCs were detected in any of the method blanks. Results from one trip blank were provided. Acetone was detected in the trip blank at an estimated concentration of 6.0 ug/L.


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Results from two equipment blanks were provided. Several VOCs were detected in the equipment blanks, as follows:

Sample ID Qualified VOCs (ug/L) EB001-09272012 Acetone = 5.4 EB001-09272012 Chloroform = 0.97 EB001-09272012 TCE = 0.35 EB002-09272012 Acetone = 4.2 J EB002-09272012 Chloroform = 1.5 J

Acetone was detected in several samples at concentrations within 10 times those of the associated equipment blanks. Due to potential blank contamination bias, the following Acetone results are qualified as U/non-detect at the concentration reported

Sample ID Qualified VOCs (ug/L) EA07 Acetone = 4.2 U EPA-MW62A Acetone = 3.8 U GCLake Acetone = 20 U

Chloroform was detected in several samples at concentrations within 5 times those of the associated equipment blanks. Due to potential blank contamination bias, the following Chloroform results are qualified as U/non-detect at the concentration reported

Sample ID Qualified VOCs (ug/L) MW18 Chloroform = 0.28 U MW12 Chloroform = 0.78 U GCLake Chloroform = 0.22 U IR3B Chloroform = 0.32 U MW16 Chloroform = 0.24 U DUP001-09272012 Chloroform = 0.29 U MW15 Chloroform = 0.31 U EPA-MW26A Chloroform = 0.50 U MW25 Chloroform = 0.38 U EPA-MW62A Chloroform = 0.44 U DUP002-09272012 Chloroform = 0.56 U EPA-MW23A Chloroform = 0.35 U

TCE was detected in one sample at a concentration within 5 times those of the associated equipment blank. Due to potential blank contamination bias, the following TCE results are qualified as U/non-detect at the concentration reported


5

Sample ID Qualified VOCs (ug/L) IR3B TCE = 1.4 U

4-5) TestAmerica provided results from two sets of laboratory control sample (LCS) and

LCS duplicate (LCSD) analyses in support of the groundwater VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.


(spike on project sample EPA-MW35A), and from one set of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable for all VOCs, with the following exceptions. MSD recoveries in the project spike were high for cis-1,2-DCE, TCE, and trichlorofluoromethane. No action is required, as the associated LCS recoveries for these VOCs demonstrated acceptable accuracy.


analyses. Surrogate recoveries ranged from 102 to 129 percent, and were within prescribed control limits, with the following exceptions. The toluene-d8 surrogate was slightly high in the following samples (upper control limit of 111 percent):

Sample ID High Toluene-D8 Surrogate

GCLake 112 % MW15 112 % EPA-MW62A 113 % DUP002 113 % EPA-MW23A 112 %

No action is taken, for the slightly high surrogate recoveries at 112 percent, given a 1 percent allowance for rounding issues. VOCs detections in undiluted analyses for samples EPA-MW26A and it duplicate DUP002 are qualified as J/Estimated due to potential high bias. No additional data are qualified as all detections are either between the MDL and RL, or a qualified due to blank contamination.

9) Two sets of field duplicate samples were collected in support of the VOC analyses.

Sample DUP001 was submitted as a field duplicate of primary sample MW16. TCE was detected in the primary and duplicate samples at concentrations of 15 ug/L, each. Precision between TCE results is acceptable, with an RPD of 0 percent. Chloroform was detected in both samples at estimated concentrations between the MDL and RL. Chloroform is qualified due to equipment blank contamination, and is not further assessed in the precision evaluation.

Sample DUP002 was submitted as a field duplicate of primary sample EPA-MW62A. Precision between the duplicate sample results, measured as the relative percent difference (RPD) between the primary and duplicate sample results, is calculated in the following table. Results are presented in micrograms per liter (ug/L).


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Sample ID 1,1-DCE Acetone Chloroform PCE TCE

EPA-MW62A 0.25 3.8 0.44 <1.0 210 DUP002 <1.0 <20 0.56 0.23 190 RPD (%) +/- RL NC NC +/- RL 10

+/- RL = Results agree within a reporting limit increment NC – Not calculated as acetone detection is qualified due to blank contamination. Precision between the duplicate sample results is very good, with a maximum RPD between duplicate results of 10 percent between TCE.

10) Results from several bromofluorobenzene instrument tunes were provided in support of all sample analyses and calibrations. Frequency of tunes was acceptable for each analytical batch at 12 hours or less between tunes. Ion abundance criteria for each of the tunes were acceptable.


analyses in this SDG, dated September 27, 2012 (GCMS#9). The September 27, 2012 initial calibration is associated with analysis of all groundwater samples in this SDG. The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compounds. Low end standards for acetone (three) and 2-butanone (three) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, no linear calibrations were required. A 25 ug/L second source calibration standard was analyzed on September 27, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.

12) TestAmerica provided results from two sets of continuing calibration verification

(CCV) standard analyses dated September 29, 2012 and October 1, 2012.

The September 29, 2012 CCV is associated with all initial analyses for all groundwater samples analyzed under this SDG, with the exceptions of samples EPA-MW23A and EB002-09272012.


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Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05 The October 1, 2012 CCV is associated with all dilution analyses for TCE (samples MW12, EPA-MW62A, and DUP002), as well as for the initial analyses of samples EPA-MW23A and EB002-09272012.

Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05




sequences of standards and samples. 16) Reconstructed ion chromatograms were reviewed for each of the samples in this SDG.

Chromatographic peaks were verified for each VOC reported as detected. Retention times were verified against quantitation reports for each of the detections. Quantitation reports were reviewed for each of the samples. Concentrations were verified against the Form I data reports for all detections and were found to be consistent for each sample.


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DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only LEVEL 4 QC DELIVERABLES 9. Initial Calibration and Verification X X 10. Continuing Calibration Verification X X 11. Retention Times X X 12. Results Quantitation X X


The water samples were received chilled at a temperature of 2.1 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by October 1 2012, within prescribed holding times.


determined to be acceptable 3) Results from one method blank were provided in support of the groundwater sample

analyses, with no perchlorate detected. Results from two equipment blanks were also provided. Perchlorate was not detected in the equipment blanks.

4) Results from continuing calibration analyses are described in note #9.


9

5-6) TestAmerica provided results from one set of project specific MS and MSD analyses (spike on project sample EPA-MW62A) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were 98 percent and 100 percent, with an RPD between MS and MSD recoveries of 2 percent.


support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries ranged from 104 to 106 percent. The RPD between LCS and LCSD results was acceptable at 2 percent.

8) Field duplicate samples were not collected for analysis of perchlorate with the

samples under this chain-of-custody Results from one set of batch specific laboratory duplicate samples were provided, with acceptable precision, as both results were non-detect.


ug/L, 25 ug/L, and 50 ug/L) dated September 26, 2012 were provided. The correlation coefficient for the calibration was acceptable at 0.9999. A mid range initial performance check (IPC) standard (25 ug/L) was analyzed following the initial calibration with an acceptable recovery of 97.7 percent

10) Perchlorate analyses were performed under one continuing calibration dated October

1, 2012. This continuing calibration is associated with all samples analyzed under this SDG. Results for the continuing calibration are described below: October 1, 2012 - Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 12 percent. The IPC recovery was acceptable at 100 percent. Results from an initial calibration check standard (ICCS) at 2 ug/L were provided with an acceptable 115 percent recovery (upper control limit of 125 percent). Results from two continuing calibration check standards (CCC) analysis at 25 ug/L were provided with an acceptable recoveries of 105 and 108 percent. Results from one CCC analysis at 40 ug/L were provided with acceptable recovery of 106 percent. Results from one ending calibration standard were provided at 40 ug/L, with a recovery of 108 percent.

11) Retention times for perchlorate were within +/- 10 percent of the associated standard retention times.

12) All ion chromatograms from the October 1, 2012 analyses were reviewed to



10





Geomatrix Consultants, Inc. (Geomatrix) collected 14 groundwater samples and five associated quality control samples on September 27, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW62A-09272012 / 1,1-DCE DUP002-09272012 / PCE

J/Estimated

These VOCs were reported at concentrations between the method

detection limit and the reporting limit. Accuracy in this portion of the

calibration curve may be limited. MW18-09272012 , MW12-09272012 GCLake-09272012, IR3B-09272012 MW16-09272012 , DUP001-09272012-09272012 MW15-09272012 , EPA-MW26A-09272012 MW25-09272012, EPA-MW62A-09272012 DUP002-09272012, and EPA-MW23A-09272012 / Chloroform

U/Non-detect at the concentration

reported

Chloroform was detected in the associated equipment blanks at

concentrations greater than in the groundwater samples. Chloroform

detections may be the result of blank contamination bias.

EA07-09272012, EPA-MW62A-09272012, GCLake-09272012 / Acetone

U/Non-detect at

the concentration reported

Acetone was detected in the

associated equipment blanks at concentrations within 10 times those of the associated samples. Acetone


SIGNATURE:

DATE:

October 13, 2012, Revised January 7, 2012 for Level 4

PVJ0513_lvl_4.doc Created on 1/8/2013 12:01:00 AM

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LABORATORY REPORT # PVJ0513 DATED OCTOBER 11, 2012


INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 11 groundwater samples and four associated quality control samples on October 4 and 5, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on October 5, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-10042012 PVJ0513-01 Quality Control VOCs / Trip Blank COG03-10042012 PVJ0513-02 Groundwater VOCs EPA-MW58A-10042012 PVJ0513-03 Groundwater VOCs EPA-MW10C-10042012 PVJ0513-04 Groundwater VOCs EPA-MW10A-10042012 PVJ0513-05 Groundwater VOCs and Perchlorate EB001-10042012 PVJ0513-06 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW36A-10052012 PVJ0513-07 Groundwater VOCs EPA-MW40C-10052012 PVJ0513-08 Groundwater VOCs and Perchlorate EPA-MW40A-10052012 PVJ0513-09 Groundwater VOCs EPA-MW11A-10052012 PVJ0513-10 Groundwater VOCs EPA-MW8C-10052012 PVJ0513-11 Groundwater VOCs and Perchlorate DUP001-10052012 PVJ0513-12 Quality Control VOCs and Perchlorate / Field Duplicate of

primary sample EPA-MW8C-08202012 EPA-MW2C-10052012 PVJ0513-13 Groundwater VOCs and Perchlorate EPA-MW9C-10052012 PVJ0513-14 Groundwater VOCs EB001-10052012 PVJ0513-15 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




LEVEL 4 VALIDATION

REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X LEVEL 4 QC DELIVERABLES 10. Instrument tune / performance check X X 11. Initial calibration RRFs and %RSDs X X 12. Continuing calibration RRFs and %Ds X X 13. Internal standard retention times/areas X X 14. TIC search (Not required) X X 15. Run logs X X 16. Compound identification /quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on October 4 and 5, 2012. The samples were analyzed by October 8, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.


3

2) No sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).

Sample ID Qualified VOCs (ug/L) EPA-MW10C Chloroform = 0.22 J

EPA-MW10A Chloroform = 0.21 J

EPA-MW36A Chloroform = 0.20 J EPA-MW11A PCE = 0.89 J EPA-MW11A Chloroform = 0.48 J EPA-MW8C PCE = 0.87 J EPA-MW8C TCE = 0.28 J EPA-MW9C Chloroform = 0.17 J 3) Results from one full suite method blank were provided in association with the

groundwater sample analyses. Acetone was detected in the method blank at an estimated concentration of 9.09 ug/L. Acetone was not detected in any of the associated groundwater samples, and no action is required..

Results from one trip blank were provided, with no VOCs detected. Results from two equipment blanks were provided, one for each day of sampling. Chloroform was detected in the equipment blanks at concentrations of 0.65 ug/L and 0.76 ug/L. Chloroform was detected in several associated samples at concentrations within 5 times those of the equipment blanks. Due to potential blank contamination bias, the following chloroform results are qualified as U/non-detect at the concentrations reported.

Sample ID Qualified VOCs (ug/L) EPA-MW10C Chloroform = 0.22 U EPA-MW10A Chloroform = 0.21 U EPA-MW36A Chloroform = 0.20 U EPA-MW11A Chloroform = 0.48 U EPA-MW9C Chloroform = 0.17 U




4


(spike on project sample EPA-MW58A) in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.


analyses. Surrogate recoveries were acceptable, ranging from 99 to 111 percent. 9) Sample DUP001-10052012 was submitted as a blind field duplicate of primary

sample EPA-MW8C. PCE was detected in the primary and duplicate samples at estimated concentrations of 0.87 ug/L and 1.0 ug/L, respectively. Precision between the duplicate PCE results is acceptable, with an RPD of 14 percent. TCE was detected in the primary samples at an estimated concentration of 0.28 ug/L and was not detected in the duplicate sample at <1.0 ug/L. TCE precision is acceptable, as both results agree within a reporting limit increment.




analyses in this SDG. The initial calibration is dated October 1, 2012 (GCMS#4). The October 1, 2012 initial calibration is associated with analysis of all groundwater samples in this SDG. The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compounds. Low end standards for acetone (three) and 2-butanone (two) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear or quadratic calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, acetone was quantified from a quadratic calibration. The correlation coefficient for acetone was acceptable at 0.990. A 25 ug/L second source calibration standard was analyzed on October 1, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.


5

A 20 ug/L second source calibration gas standard was analyzed on October 1, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.


(CCV) standard analyses dated October 7, 2012. The October 7, 2012 CCV is associated with all groundwater samples analyzed under this SDG.

October 7, 2012 - This CCV is associated with the all groundwater samples in this SDG analyzed on instrument GCMS #4 under the October 1, 2012 initial calibration Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05.




sequences of standards and samples. 16) Reconstructed ion chromatograms were reviewed for each of the samples in this

SDG. Chromatographic peaks were verified for each VOC reported as detected. Retention times were verified against quantitation reports for each of the detections. Quantitation reports were reviewed for each of the samples. Concentrations were verified against the Form I data reports for all detections and were found to be consistent.


6


PERCHLORATE – EPA METHOD 314.0

LEVEL 4 VALIDATION



DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X Yes – See note

#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X LEVEL 4 QC DELIVERABLES 9. Initial Calibration and Verification X X 10. Continuing Calibration Verification X X 11. Retention Times X X 12. Results Quantitation X X

%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The groundwater samples were received by TestAmerica on October 5, 2012. The

water samples were received chilled at a temperature of 2.1 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by October 9, 2012, within prescribed holding times.


determined to be acceptable, with the following consideration. Perchlorate was reported as concentration between the method detection limit (MDL) and the standard reporting limit in the following samples. Due to limited accuracy in this portion of the calibration curve, these perchlorate results are qualified as J/Estimated.

Sample ID Qualified Perchlorate (ug/L) EPA-MW40C Perchlorate = 1.3 J EPA-MW8C Perchlorate = 1.3 J


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3) Results from two method blanks were provided in support of the groundwater sample analyses, with no perchlorate detected. Results from two equipment blanks were also provided, with no perchlorate detected.

4) Results from continuing calibration analyses are discussed in item #9. 5-6) TestAmerica provided results from two sets of project specific MS and MSD

analyses (spikes on project samples EPA-MW40C and DUP001) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 102 to 104 percent, with a maximum RPD between MS and MSD recoveries of 2 percent.

7) TestAmerica provided results from two sets of LCS and LCSD analyses in support of

the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS and LCSD recoveries ranged from 106 to 109 percent, with a maximum RPD of 2 percent between LCS duplicate results.

8) Sample DUP001-10052012 was submitted as a blind field duplicate of primary

sample EPA-MW8C. Perchlorate was detected in the primary and duplicate samples at concentrations of 1.9 ug/L and 2.2 ug/L, respectively. Precision between the duplicate perchlorate results is acceptable, with an RPD of 15 percent.

TestAmerica provided results from two sets of laboratory duplicate sample analyses performed on batch samples. Laboratory duplicate precision is acceptable, with a maximum RPD between duplicate samples of 0.2 percent.

9) Results from one 5-point initial calibration (standard levels of 2 ug/L, 5 ug/L, 10 ug/L, 25 ug/L, and 50 ug/L) dated September 26, 2012 were provided. The correlation coefficient for the calibration was acceptable at 0.9999. A mid range initial performance check (IPC) standard (25 ug/L) was analyzed following the initial calibration with an acceptable recovery of 97.7 percent

10) Perchlorate analyses were performed under two continuing calibrations dated

October 8, 2012 and October 9, 2012. These continuing calibrations are associated with all samples analyzed under this SDG. Results for the continuing calibration are described below: October 8, 2012 - This continuing calibration is associated with the following samples: EPA-MW10A-10042012 EB001-10042012 EPA-MW40C-10052012 EPA-MW8C-10052012 Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 10.9 percent. The IPC recovery was acceptable at 103 percent. Results from an initial calibration check


8

standard (ICCS) at 2 ug/L were provided with an acceptable 120 percent recovery (upper control limit of 125 percent). Results from two continuing calibration check standard (CCC) analyses at 25 ug/L were provided with a acceptable recoveries of 104 and 107 percent. Results from one CCC analysis at 40 ug/L were provided with an acceptable recovery of 109 percent. Results from one ending CCC analysis at 40 ug/L were provided with an acceptable recovery of 109 percent. October 9, 2012 - This continuing calibration is associated with the following samples: DUP001-10052012 EPA-MW2C-10052012 EB001-10052012 Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 13.3 percent. The IPC recovery was acceptable at 104 percent. Results from an initial calibration check standard (ICCS) at 2 ug/L were provided with an acceptable 123 percent recovery (upper control limit of 125 percent). Results from one continuing calibration check standard (CCC) analysis at 25 ug/L were provided with an acceptable recovery of 111 percent. Results from two CCC analyses at 40 ug/L were provided with acceptable recoveries of 116 percent, each. Results from one ending CCC analysis at 40 ug/L were provided with an acceptable recovery of 110 percent.


12) All ion chromatograms from the October 8 and 9, 2012 analyses were reviewed to



9





Geomatrix Consultants, Inc. (Geomatrix) collected 11 groundwater samples and four associated quality control samples on October 4 and 5, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW11A-10052012 / PCE EPA-MW8C-10052012 / PCE EPA-MW8C-10052012 / TCE

J/Estimated



calibration curve may be limited.

EPA-MW10C-10042012 / Chloroform EPA-MW10A-10042012 / Chloroform EPA-MW36A-10052012 / Chloroform EPA-MW11A-10052012 / Chloroform EPA-MW9C-10052012 / Chloroform

U/Non-detect at

the concentration reported.


concentrations greater than those detected in the samples. Chloroform detections may be the result of blank

contamination bias. EPAMW40C-10052012 and EPAMW8C-10052012 / Perchlorate

J/Estimated

Perchlorate was reported at concentrations between the method


calibration curve may be limited

SIGNATURE:

DATE: October 25, 2012, Revised January 7, 2013 for level 4

PVJ1065_LVL_4.doc Created on 11/23/2012 1:20:00 PM

1





INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected seven groundwater samples and three associated quality control samples on October 12, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on October 15, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-10122012 PVJ1065-01 Quality Control VOCs / Trip Blank EPA-MW19C-10122012 PVJ1065-02 Groundwater VOCs and Perchlorate EPA-MW4C-10122012 PVJ1065-03 Groundwater VOCs and Perchlorate EPA-MW22C-10122012 PVJ1065-04 Groundwater VOCs and Perchlorate EPA-MW44A-10122012 PVJ1065-05 Groundwater VOCs and Perchlorate EPA-MW20A-10122012 PVJ1065-06 Groundwater VOCs EPA-MW21A-10122012 PVJ1065-07 Groundwater VOCs and Perchlorate EPA-MW62A-10122012 PVJ1065-08 Groundwater VOCs and Perchlorate DUP001-10122012 PVJ1065-09 Quality Control VOCs / Field Duplicate of primary sample

EPA-MW62A-10122012 EB001-10122012 PVJ1065-10 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2


PGA NORTH – GROUNDWATER SAMPLING

VOLATILE ORGANIC COMPOUNDS BY METHOD 8260B PROJECT SPECIFIC SHORT LIST

LEVEL 4 VALIDATION

REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X LEVEL 4 QC DELIVERABLES 10. Instrument tune / performance check X X 11. Initial calibration RRFs and %RSDs X X Yes 12. Continuing calibration RRFs and %Ds X X Yes 13. Internal standard retention times/areas X X 14. TIC search (Not required) X X 15. Run logs X X 16. Compound identification /quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on October 12, 2012. The samples were analyzed by October 16, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.


are acceptable with the following considerations. Some VOCs were reported at


3

concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).

Sample ID Qualified VOCs (ug/L) EPA-MW44A Chloroform = 0.50 J EPA-MW21A TCE = 0.42 J

EPA-MW62A Chloroform = 0.34 J DUP001 Chloroform = 0.39 J 3) Results from one full suite method blank were provided in association with the

groundwater sample analyses. No VOCs were detected in the method blank.

Results from one trip blank were provided, with no VOCs detected. Results from one equipment blank were provided. Methylene chloride and TCE were detected in the equipment blank at estimated concentrations of 0.55 ug/L and 0.21 ug/L, respectively. Methylene chloride was not detected in any associated samples, and no action is required. TCE was detected in sample EPA-MW21A at a concentration within two times that of the equipment blank. Due to potential blank contamination bias, this TCE results is qualified as U/non-detect at the concentration reported.




(spike on project sample EPA-MW19C) in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.



sample EPA-MW62A. TCE was detected in the primary and duplicate samples at concentrations of 150 ug/L, each. Precision between the duplicate TCE results is acceptable, with an RPD of 0 percent. Chloroform was detected in the primary and duplicate samples at estimated concentrations of 0.34 ug/L and 0.39 ug/L. Precision between the duplicate chloroform results is acceptable, with an RPD of 14 percent.


4



analyses in this SDG. The initial calibration is dated October 15, 2012 (GCMS#2). The October 15, 2012 initial calibration is associated with analysis of all groundwater samples in this SDG. The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compounds, with the exception of 2-butanone at 0.033. 2-Butanone was not detected in any of the associated samples. Due to the poor calibration response, 2-butanone results for this SDG are qualified as R/Rejected. Low end standards for acetone (four) and 2-butanone (one) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, acetone was quantified from a linear calibration. The correlation coefficient for acetone was acceptable at 0.997. A 25 ug/L second source calibration standard was analyzed on October 15, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits. A 20 ug/L second source calibration gas standard was analyzed on October 15, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.


(CCV) standard analyses dated October 16, 2012. The October 16, 2012 CCV is associated with all groundwater samples analyzed under this SDG.

October 16, 2012 - This CCV is associated with the all groundwater samples in this SDG analyzed on instrument GCMS #2 under the October 15, 2012 initial calibration Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the


5

continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05, with the exception of that for 2-butanone at 0.030. 2-Butanone results are already qualified due to poor initial calibration response.





SDG. Chromatographic peaks were verified for each VOC reported as detected. Retention times were verified against quantitation reports for each of the detections. Quantitation reports were reviewed for each of the samples. Concentrations were verified against the Form I data reports for all detections and were found to be consistent for each sample.


6





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X LEVEL 4 QC DELIVERABLES 9. Initial Calibration and Verification X X 10. Continuing Calibration Verification X X No 11. Retention Times X X 12. Results Quantitation X X




determined to be acceptable. 3) Results from two method blanks were provided in support of the groundwater sample

analyses, with no perchlorate detected. Results from one equipment blank were also provided. Perchlorate was not detected in the equipment blank.

4) Results from continuing calibration analyses are discussed in item #9. 5-6) TestAmerica provided results from two sets of project specific MS and MSD

analyses (spikes on project samples EPA-MW4C and DUP001) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is


7

acceptable. MS and MSD recoveries ranged from 99 to 100 percent, with a maximum RPD between MS and MSD recoveries of 1 percent.




sample EPA-MW62A. Perchlorate was detected in the primary and duplicate samples at concentrations of 3.5 ug/L and 3.7 ug/L, respectively. Field duplicate precision is acceptable, with an RPD of 5.6 percent between duplicate sample results

TestAmerica provided results from two sets of laboratory duplicate sample analyses performed on project samples EPA-MW4C and DUP001. Laboratory duplicate precision is acceptable, with a maximum RPD between duplicate samples of 10 percent.



16, 2012. This continuing calibration is associated with all samples analyzed under this SDG. Results for the continuing calibration are described below: October 16, 2012 - Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 12.4 percent. The IPC recovery was acceptable at 99.6 percent. Results from an initial calibration check standard (ICCS) at 2 ug/L were provided with an acceptable 123 percent recovery (upper control limit of 125 percent). Results from one continuing calibration check standard (CCC) analysis at 25 ug/L were provided with an acceptable recovery of 108 percent. Results from one CCC analysis at 40 ug/L were provided with a high recovery of 116 percent. No action is taken, as the 25 ug/L CCC analyzed directly after the project samples had an acceptable recovery.


12) All ion chromatograms from the October 16, 2012 analyses were reviewed to



8





Geomatrix Consultants, Inc. (Geomatrix) collected ten groundwater samples and four associated quality control samples on October 15 and 16, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW44A-10122012 / Chloroform EPA-MW62A-10122012 / Chloroform DUP001-10122012 / Chloroform

J/Estimated

Chloroform was reported at

concentrations between the method detection limit and the reporting

limit. Accuracy in this portion of the calibration curve may be limited.

EPA-MW21A-10122012 / TCE

U/Non-detect at


TCE was detected in the associated equipment blank at a concentration

within tow times that of the groundwater sample. The TCE

detection may be the results of blank contamination bias.

All groundwater samples / 2-Butanone

R/Rejected

2-Butanone was not detected in the groundwater samples. The response factors in the initial and continuing

calibrations were less than 0.05 indicating that 2-butanone data are

not reliable.

SIGNATURE:

DATE:

October 26, 2012, Revised January 7, 2013 for Level 4

PVJ1237_LVL_4.doc Created on 1/8/2013 12:51:00 AM

1





INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected ten groundwater samples and four associated quality control samples on October 15 and 16, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on October 17, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-10152012 PVJ1237-01 Quality Control VOCs / Trip Blank EPA-MW53A-10152012 PVJ1237-02 Groundwater VOCs and Perchlorate EPA-MW52A-10152012 PVJ1237-03 Groundwater VOCs and Perchlorate EPA-MW17C-10152012 PVJ1237-04 Groundwater VOCs EPA-MW18A-10152012 PVJ1237-05 Groundwater VOCs EB001-10152012 PVJ1237-06 Quality Control VOCs and Perchlorate / Equipment Blank COA18-10162012 PVJ1237-07 Groundwater VOCs and Perchlorate IR26A-10162012 PVJ1237-08 Groundwater VOCs EPA-MW60A-10162012 PVJ1237-09 Groundwater VOCs and Perchlorate EPA-MW34A-10162012 PVJ1237-10 Groundwater VOCs EPA-MW31A-10162012 PVJ1237-11 Groundwater VOCs EPA-MW23A-10162012 PVJ1237-12 Groundwater VOCs DUP001-10162012 PVJ1237-13 Quality Control VOCs / Field Duplicate of primary sample




2




LEVEL 4 VALIDATION

REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X LEVEL 4 QC DELIVERABLES 10. Instrument tune / performance check X X 11. Initial calibration RRFs and %RSDs X X 12. Continuing calibration RRFs and %Ds X X 13. Internal standard retention times/areas X X 14. TIC search (Not required) X X 15. Run logs X X 16. Compound identification /quantitation X X





are acceptable with the following considerations. Some VOCs were reported at


3

concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).

Sample ID Qualified VOCs (ug/L) EPA-MW17C Carbon tetrachloride = 0.52 J EPA-MW17C Chloroform = 0.52 J

EPA-MW18A PCE = 0.43 J EPA-MW18A TCE = 0.85 J IR26A TCE = 0.30 J IR26A Chloroform = 0.31 J EPA-MW60A TCE = 0.28 J EPA-MW60A Chloroform = 0.39 J EPA-MW34A PCE = 0.43 J EPA-MW34A TCE = 0.75 J EPA-MW31A PCE = 0.76 J EPA-MW31A TCE = 0.85 J EPA-MW23A Chloroform = 0.31 J DUP001 Chloroform = 0.31 J 3) Results from one full suite method blank were provided in association with the

groundwater sample analyses. Acetone was detected in the method blank at an estimated concentration of 10.8 ug/L. Acetone was not detected in any of the associated groundwater samples, and no action is required.

Results from one trip blank were provided, with no VOCs detected. Results from two equipment blanks were provided, with no VOCs detected.






4

8) Three surrogates were spiked into each groundwater sample in support of the VOC analyses. Surrogate recoveries were acceptable, ranging from 94 to 103 percent.


sample EPA-MW23A. TCE was detected in the primary and duplicate samples at concentrations of 160 ug/L, each. Precision between the duplicate TCE results is acceptable, with an RPD of 0 percent. Chloroform was detected in the primary and duplicate samples at estimated concentrations of 0.31 ug/L, each. Precision between the duplicate chloroform results is acceptable, with an RPD of 0 percent.




analyses in this SDG. The initial calibration is dated October 1, 2012 (GCMS#4). The October 1, 2012 initial calibration is associated with analysis of all groundwater samples in this SDG. The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compounds. Low end standards for acetone (three) and 2-butanone (two) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear or quadratic calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, acetone was quantified from a quadratic calibration. The correlation coefficient for acetone was acceptable at 0.990. A 25 ug/L second source calibration standard was analyzed on October 1, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits. A 20 ug/L second source calibration gas standard was analyzed on October 1, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.


(CCV) standard analyses dated October 18, 2012. The October 18, 2012 CCV is associated with all samples under this SDG


5

October 18, 2012 - This CCV is associated with the all groundwater samples in this SDG analyzed on instrument GCMS #4 under the October 1, 2012 initial calibration Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05







6



LEVEL 4 VALIDATION



DATA QUALIFIED -




#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X Yes 4. Initial and Continuing Calibration %R X X 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab Only LEVEL 4 QC DELIVERABLES 9. Initial Calibration and Verification X X 10. Continuing Calibration Verification X X 11. Retention Times X X 12. Results Quantitation X X





Sample ID Qualified Perchlorate (ug/L) COA18 Perchlorate = 1.3 J


7


analyses, with no perchlorate detected. Results from two equipment blanks were also provided; one for each day of sampling. Perchlorate was detected in the equipment blank collected on October 16, 2012 at an estimated concentration of 0.56 ug/L. Perchlorate was detected in sample COA18, collected on October 16, 2012 at a concentration within 5 times that of the equipment blank. Due to potential blank contamination bias, this perchlorate results is qualified as U/non-detect at the concentration reported.

4) Results from continuing calibration analyses are described in item #9. 5-6) TestAmerica provided results from one set of project specific MS and MSD

analyses (spike on project sample EPA-MW53A) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 93 to 102 percent, with an RPD between MS and MSD recoveries of 8 percent.

7) TestAmerica provided results from one set of LCS and LCSD analyses in support of

the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS and LCSD recoveries ranged from 103 to 106 percent, with an RPD of 3 percent between LCS duplicate results.

8) Field duplicate samples were not collected in support of the perchlorate samples

with this chain-of-custody.

TestAmerica provided results from one set of laboratory duplicate sample analyses performed on batch samples. Laboratory duplicate precision is acceptable, with an RPD between duplicate samples of 3 percent.



18, 2012. This continuing calibration is associated with all samples analyzed under this SDG. Results for the continuing calibration are described below: October 18, 2012 - Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 5.1 percent. The IPC recovery was acceptable at 98 percent. Results from an initial calibration check standard (ICCS) at 2 ug/L were provided with an acceptable 115 percent recovery (upper control limit of 125 percent). Results from one continuing calibration check standard (CCC) analysis at 25 ug/L were provided with


8

an acceptable recovery of 106 percent. Results from one ending CCC analysis at 40 ug/L were provided with acceptable recovery of 109 percent.


retention times. 12) All ion chromatograms from the October 18, 2012 analyses were reviewed to



9






Data Qualifier(s)


EPA-MW17C-10152012 / Carbon tetrachloride and Chloroform EPA-MW18A-10162012 / PCE and TCE IR26A-10162012 / TCE and Chloroform EPA-MW60A-10162012 / TCE and Chloroform EPA-MW34A-10162012 / PCE and TCE EPA-MW31A-10162012 / PCE and TCE EPA-MW23A-10162012 / Chloroform DUP001-10162012 / Chloroform

J/Estimated




COA18-10162012 / Perchlorate

U/non-detect at


Perchlorate was detected in the associated equipment blank at a

concentration within 5 times that of the groundwater sample.

Perchlorate detection may be the result of blank contamination bias

SIGNATURE:

DATE:

October 25, 2012, Revised January 7, 2013 for level 4

PVK0684_LVL_4.doc Created on 1/9/2013 8:28:00 PM

1



LABORATORY REPORT # PVK0684 DATED NOVEMBER 19, 2012


INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected seven groundwater samples and three associated quality control samples on November 8, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on November 8, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-11082012 PVK0684-01 Quality Control VOCs / Trip Blank EPA-MW11A-11082012 PVK0684-02 Groundwater VOCs and Perchlorate EPA-MW2C-11082012 PVK0684-03 Groundwater VOCs and Perchlorate EPA-MW8C-11082012 PVK0684-04 Groundwater VOCs and Perchlorate EPA-MW58A-11082012 PVK0684-05 Groundwater VOCs and Perchlorate EPA-MW10C-11082012 PVK0684-06 Groundwater VOCs and Perchlorate EPA-MW9C-11082012 PVK0684-07 Groundwater VOCs and Perchlorate EPA-MW10A-11082012 PVK0684-08 Groundwater VOCs and Perchlorate DUP001-11082012 PVK0684-09 Quality Control VOCs and Perchlorate / Field Duplicate or

primary sample EPA-MW10A-11082012 EB001-11082012 PVK0684-10 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




LEVEL 4 VALIDATION

REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X LEVEL 4 QC DELIVERABLES 10. Instrument tune / performance check X X 11. Initial calibration RRFs and %RSDs X X Yes 12. Continuing calibration RRFs and %Ds X X Yes 13. Internal standard retention times/areas X X 14. TIC search (Not required) X X 15. Run logs X X 16. Compound identification /quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on November 8, 2012. The samples were analyzed by November 15, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.


are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting


3

limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).


EPA-MW8C PCE = 0.95 J EPA-MW8C TCE = 0.31 J DUP001 Chloroform = 0.30 J

3) Results from two full suite method blanks were provided in association with the groundwater sample analyses. No VOCs were detected in either of the method blanks.


4-5) TestAmerica provided results from two full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with one exception. One LCSD recovery was high for carbon tetrachloride. Carbon tetrachloride was not detected in the associated samples, and no action is required.


(spike on project sample EPA-MW11A), and from one set of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable for all VOCs, with the following exception. The MSD recovery for trichlorofluoromethane was high in the batch spike at 138 percent. Trichlorofluoromethane was not detected in the associated samples, and no action is required.


analyses. Surrogate recoveries ranged from 106 to 129 percent. Numerous 4-bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent upper project control limit. Toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit, as follows:

Sample ID High Surr Rec (%) Data Qualified

EPA-MW11A 4-BFB = 116 PCE EPA-MW11A Tol-d8 = 114 PCE EPA-MW2C 4-BFB = 115 None EPA-MW8C 4-BFB = 119 None EPA-MW8C Tol-d8 = 115 None


4


EPA-MW58A 4-BFB = 115 PCE and TCE EPA-MW58A Tol-d8 = 114 PCE and TCE EPA-MW10C 4-BFB = 115 TCE EPA-MW9C Tol-d8 = 117 TCE EPA-MW10A 4-BFB = 121 PCE and TCE EPA-MW10A Tol-d8 = 113 PCE and TCE DUP001 4-BFB = 120 PCE and TCE DUP001 Tol-d8 = 114 PCE and TCE

Some detections for these samples are already qualified, due to reporting limit (MDL/RL) considerations. Any additional VOC detections are listed above, and are qualified as J/Estimated, due to potential high bias.

9) Sample DUP001 was submitted as a blind field duplicate of primary sample

EPA-MW10C. TCE was detected in the primary and duplicate samples at concentrations of 130 ug/L and 120 ug/L, respectively. Precision between the TCE detections is acceptable, with an RPD of 8 percent. PCE was detected in the primary and duplicate samples at concentrations of 1.2 ug/L and 1.1 ug/L, respectively. Precision between the TCE detections is acceptable, with an RPD of 8.7 percent. Chloroform was detected in the duplicate sample at a concentration between the MDL and RL and was not detected in the primary sample. Chloroform results agree within a reporting limit increment. Field duplicate precision is determined to be acceptable.




analyses in this SDG. The initial calibrations are dated November 8, 2012 (GCMS#9) and November 12, 2012 (GCMS#2). The November 8, 2012 initial calibration is associated with the analysis of the following samples.

TB001-11082012 EPA-MW11A-11082012 EPA-MW2C-11082012 EPA-MW8C-11082012 EPA-MW58A-11082012 EPA-MW10C-11082012 EPA-MW9C-11082012 DUP001-11082012


5

The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compounds. Low end standards for acetone (four) and 2-butanone (one) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, no linear calibrations were required. A 25 ug/L second source calibration standard was analyzed on November 8, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.

The November 12, 2012 initial calibration is associated with analysis of the following groundwater samples in this SDG one GCMS#2).

EPA-MW10A-11082012 (re-analysis) EB001-11082012 The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compounds, with the following exception. The RRF for 2-butanone is low at 0.036. 2-Butanone was not detected in any of the associated samples. Due to the low response factor, all associated 2-butanone results are qualified as R/Rejected. Low end standards for acetone (three) and 2-butanone (three) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, no linear calibrations were required. A 25 ug/L second source calibration standard was analyzed on November 12, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.

A 20 ug/L second source gas calibration standard was analyzed on November 12, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.


(CCV) standard analyses dated November 14 and November 15, 2012.


6

November 14, 2012 - This CCV is associated with the following groundwater samples in this SDG analyzed on instrument GCMS #9 under the November 8, 2012 initial calibration:

TB001-11082012 EPA-MW11A-11082012 EPA-MW2C-11082012 EPA-MW8C-11082012 EPA-MW58A-11082012 EPA-MW10C-11082012 EPA-MW9C-11082012 DUP001-11082012

Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05. November 15, 2012 - This CCV is associated with the following groundwater samples in this SDG analyzed on instrument GCMS #2 under the November 12, 2012 initial calibration:

EPA-MW10A-11082012 (re-analysis) EB001-11082012 Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05, with the exception of that for 2-butanone at 0.030. 2-Butanone results are already qualified due to poor initial calibration response.







7





DATA QUALIFIED -




#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X LEVEL 4 QC DELIVERABLES 9. Initial Calibration and Verification X X 10. Continuing Calibration Verification X X No – see notes 11. Retention Times X X 12. Results Quantitation X X

%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The groundwater samples were received by TestAmerica on November 8, 2012.

The water samples were received chilled at a temperature of 3.3 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by November 13, 2012, within prescribed holding times.


determined to be acceptable, with the following considerations. Perchlorate was reported at a concentration between the method detection limit (MDL) and the reporting limit in sample EPA-MW8C. Due to limited accuracy in this portion of the calibration range, this perchlorate result is qualified as J/Estimated.

3) Results from two method blanks were provided in support of the groundwater sample

analyses, with no perchlorate detected. Results from one equipment blank were also provided, with no perchlorate detected.

4) Results from continuing calibration analyses were not provided.


8

5-6) TestAmerica provided results from one set of project specific MS and MSD

analyses in support of the perchlorate analyses (spike on project sample EPA-MW11A), and from one set of batch specific MS and MSD analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 105 to 109 percent, with a maximum RPD between MS and MSD recoveries of 2 percent.

7) TestAmerica provided results from two sets of LCS and LCS duplicate analyses in

support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries ranged from 107 and 113 percent. The maximum RPD between LCS and LCSD results was acceptable at 2 percent.


EPA-MW10A. Perchlorate was detected in the primary and duplicate samples at concentrations of 30 ug/L, each. Precision between the field duplicate samples is acceptable, with an RPD of 0 percent.

TestAmerica provided results from one set of batch specific laboratory duplicate sample analyses. Laboratory duplicate precision is acceptable, with an RPD of 5 percent between primary and duplicate sample results.


ug/L, 25 ug/L, and 50 ug/L) dated September 26, 2012 were provided. The correlation coefficient for the calibration was acceptable at 0.9999. A mid range initial performance check (IPC) standard (25 ug/L) was analyzed following the initial calibration with an acceptable recovery of 97.7 percent


November 12, 2012 and November 13, 2012 November 12, 2012 - This continuing calibration is associated with the following groundwater samples (other samples were analyzed, but were re-analyzed on November 13, 2012 due to failed QC):

EB001-11082012 Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 14 percent. The IPC recovery was acceptable at 103 percent. Results from an initial calibration check standard (ICCS) at 2 ug/L were provided with an acceptable 110 percent recovery (upper control limit of 125 percent). Results from two continuing calibration check standards (CCC) analyses at 25 ug/L were provided with acceptable recoveries of 114 and 111 percent. Results from one CCC analysis at 40 ug/L were provided with a high recovery of 119 percent. Due to the high recovery, all associated samples with perchlorate detections were re-analyzed on November 13, 2013.


9

No action is taken for sample EB001, as no perchlorate was detected. An ending CCC at 40 ug/L was provided with an acceptable recovery of 114 percent.

November 13, 2012 - This continuing calibration is associated with the following groundwater samples: EPA-MW11A-11082012 EPA-MW2C-11082012 (re-analysis) EPA-MW8C-11082012 EPA-MW58A-11082012 (re-analysis) EPA-MW10C-11082012 (re-analysis) EPA-MW9C-11082012 (re-analysis) EPA-MW10A-11082012 (re-analysis) DUP001-11082012 (re-analysis) EB001-11082012 Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 12.1 percent. The IPC recovery was acceptable at 102 percent. Results from an initial calibration check standard (ICCS) at 2 ug/L were provided with an acceptable 102 percent recovery (upper control limit of 125 percent). Results from two continuing calibration check standard (CCC) analyses at 25 ug/L were provided with acceptable recoveries of 108 and 112 percent. Results from one CCC analysis at 40 ug/L were provided with an acceptable recovery of 114 percent. Results from one ending CCC analysis at 40 ug/L were provided with an acceptable recovery of 115 percent.


12) All ion chromatograms from the November 12 and November 14, 2012 analyses

were reviewed to verify that the sample results reported matched those presented in the raw data, and that dilution factors were correctly applied.


10





Geomatrix Consultants, Inc. (Geomatrix) collected seven groundwater samples and three associated quality control samples on November 8, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW8C-11082012 / PCE and TCE DUP001-11082012 / Chloroform

J/Estimated



calibration curve may be limited. EPA-MW11A-11082012 / PCE EPA-MW58A-11082012 / PCE and TCE EPA-MW10C-11082012 /TCE EPA-MW9C-11082012 / TCE EPA-MW10A-11082012 / PCE and TCE DUP001-11082012 / PCE and TCE

J/Estimated

Associated surrogate recoveries were

high. Sample detections for these VOCs may be biased high.

EPA-MW8C-11082012 / Perchlorate

J/Estimated

Perchlorate was reported at a concentration between the method detection limit and the reporting


EPA-MW10A-11082012 / 2-Butanone

R/Rejected

2-Butanone was not detected in the groundwater sample. The response factors in the initial and continuing

calibrations were less than 0.05 indicating that 2-butanone data are

not reliable.

SIGNATURE:

DATE: November 27, 2012, Revised January 9, 2012 for Level 4

PVK1220_LVL_4.doc Created on 1/8/2013 2:46:00 AM

1





INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 13 groundwater samples and four associated quality control samples on November 14 and 15, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on November 16, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-11142012 PVK1220-01 Quality Control VOCs / Trip Blank EPA-MW44A-11142012 PVK1220-02 Groundwater VOCs and Perchlorate MW17-11142012 PVK1220-03 Groundwater VOCs EB001-11142012 PVK1220-04 Quality Control VOCs and Perchlorate / Equipment Blank COA15-11152012 PVK1220-05 Groundwater Perchlorate COA18-11152012 PVK1220-06 Groundwater VOCs and Perchlorate COG03-11152012 PVK1220-07 Groundwater VOCs and Perchlorate COG06-11152012 PVK1220-08 Groundwater VOCs and Perchlorate COG18A-11152012 PVK1220-09 Groundwater VOCs and Perchlorate COG18B-11152012 PVK1220-10 Groundwater VOCs and Perchlorate EPA-MW24C-11152012 PVK1220-11 Groundwater VOCs EPA-MW20A-11152012 PVK1220-12 Groundwater VOCs EPA-MW17A-11152012 PVK1220-13 Groundwater VOCs EPA-MW32A-11152012 PVK1220-14 Groundwater VOCs DUP001-11152012 PVK1220-15 Quality Control VOCs / Field Duplicate of primary sample

EPA-MW32A-11152012 EPA-MW37A-11152012 PVK1220-16 Groundwater VOCs EB001-11152012 PVK1220-17 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




LEVEL 4 VALIDATION

REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X No C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X LEVEL 4 QC DELIVERABLES 10. Instrument tune / performance check X X 11. Initial calibration RRFs and %RSDs X X Yes 12. Continuing calibration RRFs and %Ds X X Yes 13. Internal standard retention times/areas X X 14. TIC search (Not required) X X 15. Run logs X X 16. Compound identification /quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on November 14 and 15, 2012. The samples were analyzed by November 23, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.


3

2) No sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).

Sample ID Qualified VOCs (ug/L) EPA-MW44A Chloroform = 0.72 J

MW17 Chloroform = 0.68 J

EPA-MW20A PCE = 0.49 J EPA-MW37A Chloroform = 0.46 J 3) Results from five full suite method blanks were provided in association with the

groundwater sample analyses. No VOCs were detected in any of the method blanks.

Results from one trip blank were provided, with no VOCs detected. Results from two equipment blanks were provided. Methylene chloride was detected in the equipment blank collected on November 15, 2012 at a concentration of 2.4 ug/L. Methylene chloride was not detected in any of the associated samples, and no action is required.

4-5) TestAmerica provided results from five full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. Precision between LCS and LCSD recoveries for acetone and 2-butanone was poor, with RPDs of 43 percent and 34 percent, respectively in one LCS set (project precision control limit of 25 percent). Precision between LCS and LCSD recoveries for acetone was poor, with RPDs of 37 and 28 percent in two other LCS sets. Acetone and 2-butanone were not detected in the associated samples, and no bias to the sample results is indicated.


(spike on project sample EPA-MW44A), and from four sets of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with one exception. The MS recovery for 1,1,2,2-tetrachloroethane was high in one batch spike at 130 percent (upper control limit of 124 percent). 1,1,2,2-Tetrachloroethane was not detected in any of the associated samples, and no action is required.


analyses. Surrogate recoveries ranged from 109 to 128 percent. Numerous 4-


4

bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent upper project control limit. Several toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit, as follows:

Sample ID High Surr Rec (%) Data qualified ?

EPA-MW41A 4-BFB = 117 Chloroform EPA-MW41A Tol-d8 = 112 Chloroform MW17 4-BFB = 120 Chloroform COA18 4-BFB = 120 None COA18 Tol-d8 = 112 None COG03 4-BFB = 117 None COG03 Tol-d8 = 113 None COG06 4-BFB = 121 None COG18A 4-BFB = 117 None COG18A Tol-d8 = 112 None COG18B 4-BFB = 122 None COG18B Tol-d8 = 118 None EPA-MW24C 4-BFB = 120 None EPA-MW24C Tol-d8 = 116 None EPA-MW20A 4-BFB = 121 Chloroform, PCE, TCE EPA-MW20A Tol-d8 = 114 Chloroform, PCE, TCE EPA-MW17A Tol-d8 = 114 None EPA-MW32A 4-BFB = 122 None EPA-MW32A Tol-d8 = 113 None DUP001 4-BFB = 117 None DUP001 Tol-d8 = 114 None EPA-MW37A Tol-d8 = 114 Chloroform

Most of these detections are already qualified, due to reporting limit (MDL/RL) considerations. Chloroform and TCE in sample EPA-MW20A are additionally qualified due to the high surrogates.

9) Sample DUP001-08202012 was submitted as a blind field duplicate of primary sample

EPA-MW32A. No VOCs were detected in either of the samples, and field duplicate precision is acceptable


5



analyses in this SDG. The initial calibrations are dated November 8, 2012 (GCMS#9) and November 17, 2012 (GCMS#2). The November 8, 2012 initial calibration is associated with the analysis of the following samples.

TB001-11142012 The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compounds. Low end standards for acetone (four) and 2-butanone (one) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, no linear calibrations were required. A 25 ug/L second source calibration standard was analyzed on November 8, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.

The November 17, 2012 initial calibration is associated with analysis of the following groundwater samples in this SDG one GCMS#2).

EPA-MW44A-11142012 MW17-11142012 EB001-11142012 COA18-11152012 COG03-11152012 COG06-11152012 COG18A-11152012 COG18B-11152012 EPA-MW24C-11152012 EPA-MW20A-11152012 EPA-MW17A-11152012 EPA-MW32A-11152012 DUP001-11152012 EPA-MW37A-11152012 EB001-11152012

The calibration was a 9-point calibration analyzed at the following concentrations (0.5, 1.0 2.0, 5.0, 10, 25, 50, 100, and 200 ug/L). Average Relative Response Factors (RRFs) were greater than 0.05 for all VOC short list target compounds, with the following exception. The RRF for 2-butanone is low at 0.037. 2-Butanone


6

was not detected in any of the associated samples. Due to the low response factor, all associated 2-butanone results are qualified as R/Rejected. Low end standards for acetone (three) and 2-butanone (two) were omitted in order to improve response factors. Percent relative standard deviations (%RSDs) were reported when quantitation was based on average response factors. %RSDs reported for target short list VOCs were acceptable and less than 30 percent for all VOCs. Linear or quadratic calibrations were performed for VOCs with RSDs greater than 15 percent. For the project short list, quadratic calibrations were performed for acetone and 2-butanone. Calibration coefficients were 0.990 and 0.995 for the two VOCs, respectively, and are acceptable. A 25 ug/L second source calibration standard was analyzed on November 17, 2012. All second source recoveries for the short list target VOCs were within prescribed control limits.

12) TestAmerica provided results from four sets of continuing calibration verification

(CCV) standard analyses dated November 20, 2012 (GCMS#9), November 20, 2012 (GCMS#2), November 21, 2012, and November 23, 2012.

November 20, 2012 - This CCV is associated with the following groundwater samples in this SDG analyzed on instrument GCMS #9 under the November 8, 2012 initial calibration

TB001-11142012 Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05. November 20, 2012 - This CCV is associated with the following groundwater samples in this SDG analyzed on instrument GCMS #2 under the November 17, 2012 initial calibration

MW17-11142012 EB001-11142012

Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent, for all VOCs with the exception of acetone at 29 percent. Acetone was not detected in the associated samples, and no bias to the acetone sample results is indicated.


7

All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05, with the exception of that for 2-butanone at 0.048. 2-Butanone results are already qualified due to the poor response in the associated initial calibration. November 21, 2012 - This CCV is associated with the following groundwater samples in this SDG analyzed on instrument GCMS #2 under the November 17, 2012 initial calibration

EPA-MW44A-11142012 COA18-11152012 COG03-11152012 COG06-11152012 COG18A-11152012 COG18B-11152012 EPA-MW24C-11152012 EPA-MW20A-11152012 EPA-MW17A-11152012 EPA-MW32A-11152012 DUP001-11152012 EB001-11152012

Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent, for all VOCs with the exception of acetone at 29 percent. Acetone was not detected in the associated samples, and no bias to the acetone sample results is indicated. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05, with the exception of that for 2-butanone at 0.048. 2-Butanone results are already qualified due to the poor response in the associated initial calibration. November 23, 2012 - This CCV is associated with the following groundwater samples in this SDG analyzed on instrument GCMS #2 under the November 17, 2012 initial calibration

EPA-MW37A-11142012

Results from one CCV were provided at the 25 ug/L level. The percent differences (%D) between the response factors in the initial calibration and the continuing calibration were less than 25 percent, for all VOCs with the exception of acetone at 29 percent. Acetone was not detected in the associated sample. Due to the high percent difference between ICAL and CCAL response factors, the acetone result for sample EPA-MW37A is qualified as UJ/Estimated and non-detect at the reporting limits stated. All CCV recoveries were within prescribed control limits. Response factors for all target VOCs in the CCV were greater than 0.05, with the exception of that for 2-butanone at 0.034. 2-Butanone results are already qualified due to the poor response in the associated initial calibration.


8






.


9



LEVEL 4 VALIDATION



DATA QUALIFIED -




#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab Only LEVEL 4 QC DELIVERABLES 9. Initial Calibration and Verification X X 10. Continuing Calibration Verification X X 11. Retention Times X X 12. Results Quantitation X X




determined to be acceptable, with the following consideration. Perchlorate was reported at concentrations between the method detection limit (MDL) and the standard reporting limit in the following samples. Due to limited accuracy in this portion of the calibration curve, these perchlorate results are qualified as J/Estimated.

Sample ID Qualified Perchlorate (ug/L) COA18 Perchlorate = 1.6 J COG18B Perchlorate = 0.93 J


10

3) Results from two method blanks were provided in support of the groundwater sample analyses, with no perchlorate detected. Results from two equipment blanks were also provided, with no perchlorate detected.

4) Results from continuing calibration analyses are described in item #9. 5-6) TestAmerica provided results from one set of project specific MS and MSD analyses

(spike on project sample EPA-MW44A), and from two sets of batch specific MS and MSD analyses in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 104 to 110 percent, with a maximum RPD between MS and MSD recoveries of 3 percent.



8) Field duplicate samples were not collected in support of the perchlorate analyses.

TestAmerica provided results from two sets of laboratory duplicate sample analyses; one performed on project sample COA15. The laboratory duplicate precision is acceptable, with an RPD of 3 percent for the batch duplicate, and an RPD of 47 percent for the project duplicate. This 47 percent RPD exceeds the project RPD maximum control limit of 25 percent, but no action is taken as the duplicate results agree within a reporting limit increment.

9) Results from one 5-point initial calibration (standard levels of 2 ug/L, 5 ug/L, 10 ug/L,

25 ug/L, and 50 ug/L) dated September 26, 2012 were provided. The correlation coefficient for the calibration was acceptable at 0.9999. A mid range initial performance check (IPC) standard (25 ug/L) was analyzed following the initial calibration with an acceptable recovery of 97.7 percent


November 19, 2012 and November 20, 2012. This continuing calibration is associated with all samples analyzed under this SDG. Results for the continuing calibration are described below: November 19, 2012 - Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 9.7 percent. The IPC recovery was acceptable at 99.6 percent. Results from an initial calibration check standard (ICCS) at 2 ug/L were provided with an acceptable 110 percent recovery (upper control limit of 125 percent). Results from one continuing calibration check standard (CCC) analysis at 25 ug/L were provided with an acceptable recovery of 108 percent. Results from one continuing calibration check


11

standard analysis at 40 ug/L were provided with an acceptable recovery of 104 percent. November 20, 2012 - Results from one 25 ug/L initial performance check (IPC) standard were provided, with an acceptable percent drift from the initial calibration of 8.3 percent. The IPC recovery was acceptable at 97.5 percent. Results from an initial calibration check standard (ICCS) at 2 ug/L were provided with an acceptable 102 percent recovery (upper control limit of 125 percent). Results from one continuing calibration check standard (CCC) analysis at 40 ug/L were provided with an acceptable recovery of 103 percent.


12) All ion chromatograms from the November 19 and November 20, 2012 analyses were

reviewed to verify that the sample results reported matched those presented in the raw data, and that dilution factors were correctly applied.

.


12





Geomatrix Consultants, Inc. (Geomatrix) collected 13 groundwater samples and four associated quality control samples on November 14 and 15, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the table on the following pages. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW44A-11142012 / Chloroform MW17-11142012 / Chloroform EPA-MW20A-11152012 / PCE EPA-MW37A-11152012 / Chloroform

J/Estimated



limit. Accuracy in this portion of the calibration curve may be

limited. Surrogate recoveries for these VOCs are also high. Results

may be biased high.

EPA-MW20A-11152012 / Chloroform and TCE

J/Estimated

Surrogate recoveries are high.

Sample results may be biased high. .

COA18-11152012 and COG18B-11152012 / Perchlorate

J/Estimated

Perchlorate was reported at



limited.


13

Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW44A-11142012 MW17-11142012 EB001-11142012 COA18-11152012 COG03-11152012 COG06-11152012 COG18A-11152012 COG18B-11152012 EPA-MW24C-11152012 EPA-MW20A-11152012 EPA-MW17A-11152012 EPA-MW32A-11152012 DUP001-11152012 EPA-MW37A-11152012 EB001-11152012 / 2-Butanone

R/Rejected




EPA-MW37A / Acetone

UJ/Estimated

and non-detect at the reporting limits stated.

Percent difference between

response factors form initial and continuing calibrations exceed 25 percent. Acetone was not detected

in the associated sample.

SIGNATURE:

DATE:

November 27, 2012, Revised for Level 4 on January 8, 2013

C24848.doc Created on 12/26/2012 12:54:00 PM

1


ACCUTEST LABORATORY (SAN JOSE, CA)

LABORATORY REPORT # C23118 DATED AUGUST 27, 2012

INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 20 groundwater samples and five associated quality control samples on November 13 and 14, 2012. The samples were shipped to Accutest Laboratory, located in San Jose, California on November 15, 2012, and arrived at the laboratory on the following day. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-11132012 C24848-01 Quality Control VOCs / Trip Blank EPA-MW57A-11132012 C24848-02 Groundwater VOCs and Perchlorate EPA-MW46A-11132012 C24848-03 Groundwater VOCs and Perchlorate EPA-MW48C-11132012 C24848-04 Groundwater VOCs and Perchlorate EPA-MW15C-11132012 C24848-05 Groundwater VOCs MW01-11132012 C24848-06 Groundwater VOCs and Perchlorate EPA-MW1A-11132012 C24848-07 Groundwater VOCs and Perchlorate MW23-11132012 C24848-08 Groundwater VOCs and Perchlorate MW06-11132012 C24848-09 Groundwater VOCs and Perchlorate MW04-11132012 C24848-10 Groundwater VOCs and Perchlorate MW02-11132012 C24848-11 Groundwater VOCs and Perchlorate DUP001-11132012 C24848-12 Quality Control VOCs and Perchlorate / Field duplicate of

primary sample MW02-11132012 MW03-11132012 C24848-13 Groundwater VOCs and Perchlorate EB001-11132012 C24848-14 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW1M-11142012 C24848-15 Groundwater VOCs MW21-11142012 C24848-16 Groundwater VOCs and Perchlorate MW27-11142012 C24848-17 Groundwater VOCs and Perchlorate EPA-MW1C-11142012 C24848-18 Groundwater VOCs and Perchlorate EPA-MW5C-11142012 C24848-19 Groundwater VOCs and Perchlorate EPA-MW7A-11142012 C24848-20 Groundwater VOCs and Perchlorate EPA-MW56A-11142012 C24848-21 Groundwater VOCs and Perchlorate EPA-MW48A-11142012 C24848-22 Groundwater VOCs and Perchlorate EPA-MW3C-11142012 C24848-23 Groundwater VOCs and Perchlorate DUP001-11142012 C24848-24 Quality Control VOCs and Perchlorate / Field duplicate of

primary sample EPA-MW3C-11142012 EB002-11142012 C24848-25 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method

8260B


2

Perchlorate – EPA 314.0 Quality Control for the water samples is evaluated in the following checklist tables and comments. A summary of data quality for the samples analyzed is provided in the final page of this validation report.




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X Yes 10. Results Quantitation X X




2) Samples DUP002-11132012 and EPA-MW56A were diluted by a factor of two for

all VOCs. Sample EPA-MW48A was diluted by a factor of 5 times for all VOCs. Samples EPA-MW3C and DUP001-08092012 were diluted by factors of 10 times and 20 times, respectively, for all VOCs. No other sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following


3

considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).


MW23 1,1-DCE = 0.45 J MW06 Chloroform = 0.25 J MW04 1,1-DCE = 0.24 J EPA-MW1M TCE = 0.31 J EPA-MW7A Chloroform = 0.47 J

3) Results from four full suite method blanks were provided in association with the groundwater sample analyses. No VOCs were detected in the method blanks. Results from one trip blank were provided, with no VOCs detected. Results from two equipment blanks were provided. No VOCs were detected in the equipment blanks.

4-5) Accutest provided results from four full sets of laboratory control sample (LCS) and

LCS duplicate (LCSD) analyses (identified as blank spike analyses) in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.

6-7) Accutest provided results from two full sets of project specific MS and MSD analyses

(spikes on project samples EPA-MW57A and EPA-MW3C), and from two sets of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses, are acceptable, with the following exceptions. The MS recovery for TCE in the project spike of sample EPA-MW3C was high 187 percent. TCE precision for this spike was also poor, with an RPD of 29 percent. The TCE concentration in the sample spiked was more than 3 times higher than the spike added amount, and no action is required.


analyses. Surrogate recoveries were acceptable, ranging from 89 to 110 percent. 9) Two sets of blind field duplicate samples were submitted with the sample under this

chain-of-custody. Sample DUP001-11132012 was submitted as a blind field duplicate of primary sample MW02. TCE was detected in the primary and duplicate samples at


4

concentrations of 99.8 ug/L and 85.7 ug/L, respectively. Precision between the TCE detections is acceptable, with an RPD of 15 percent.

Sample DUP001-11142012 was submitted as a blind field duplicate of primary sample

EPA-MW3C. TCE was detected in the primary and duplicate samples at concentrations of 611 ug/L and 861 ug/L, respectively. Precision between the TCE detections is slightly poor, with an RPD of 34 percent. Due to the poor field duplicate precision, the TCE concentrations for the primary and duplicate samples are qualified as J/Estimated.

10) No anomalies were noted with respect to results quantitation or reporting.


5





DATA QUALIFIED -




#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not evaluated 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X 9. Results Quantitation X X

%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The groundwater samples were received by Accutest on November 16, 2012. The

water samples were received chilled at a temperature of 2.6 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by November 16, 2012, within prescribed holding times.

2) Samples MW23, EPA-MW1C, EPA-MW3C, and DUP001-11142012 were each

diluted by a factor of 2 times to quantitate perchlorate due to elevated conductivity. No other sample dilutions were required to quantitate perchlorate. Reporting limits are determined to be acceptable, with the following considerations. Some perchlorate results were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these perchlorate results are qualified as J/Estimated, as follows:

Sample ID Qualified Results(ug/L) EPA-MW57A Perchlorate = 2.6 J EPA-MW46A Perchlorate = 2.9 J EPA-MW21 Perchlorate = 2.9 J 3) Results from two method blanks were provided in support of the groundwater sample

analyses, with no perchlorate detected. Results from two equipment blanks were also provided. Perchlorate was not detected in any of the blanks.


6

4) Results from continuing calibration analyses were not evaluated. 5-6) Accutest provided results from two sets of project specific MS and MSD analyses

(spikes on project samples EPA-MW57A and EPA-MW3C) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 82.0 to 96.6 percent, with a maximum RPD between MS and MSD recoveries of 2.1 percent (spike recovery control limits of 80 to 120 percent).

4-6) Accutest provided results from two sets of laboratory control sample (LCS) and LCS

duplicate (LCSD) analyses (identified as blank spike analyses) in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries ranged from 93.2 to 100.4 percent. The maximum RPD between the LCS and LCSD results was acceptable at 7.4 percent.

8) Two sets of blind field duplicate samples were submitted with the sample under this

chain-of-custody. DUP001-11132012 was submitted as a blind field duplicate of primary sample MW02. Perchlorate was detected in the primary and duplicate samples at concentrations of 5.5 ug/L and 5.2 ug/L, respectively. Precision between the perchlorate detections is acceptable, with an RPD of 5.6 percent.

Sample DUP001-11142012 was submitted as a blind field duplicate of primary sample

EPA-MW3C. Perchlorate was detected in the primary and duplicate samples at concentrations of 21.7 ug/L and 21.6 ug/L, respectively. Precision between the perchlorate detections is acceptable, with an RPD of 0.5 percent.

9) No anomalies were noted with respect to the perchlorate reporting.


7



LABORATORY REPORT # C23118 DATED AUGUST 27, 2012

Geomatrix Consultants, Inc. (Geomatrix) collected 20 groundwater samples and five associated quality control samples on November 13 and 14, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


MW23-11132012 / 1,1-DCE MW06-11132012 / Chloroform MW04-11132012 / 1,1-DCE EPA-MW1M-11142012 / TCE EPA-MW7A-11142012 / Chloroform

J/Estimated




EPA-MW3C-11142012 and DUP001-11142012 / TCE

J/Estimated

Poor precision between results of field duplicate samples. RPD exceed

25 percent.

EPA-MW57A-11132012, EPA-MW46A-11132012, and MW21-11142012 / Perchlorate

J/Estimated




SIGNATURE:

DATE:

December 26, 2012


1



LABORATORY REPORT # C25005 DATED DECEMBER 14, 2012

INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected two groundwater samples (blind performance evaluation samples) and one associated trip blank on November 27, 2012. The samples were shipped to Accutest Laboratory, located in San Jose, California on November 28, 2012, and arrived at the laboratory on the following day. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-11272012 C25005-01 Quality Control VOCs / Trip Blank MW030-11272012 C25005-02 Groundwater VOCs and Perchlorate MW031-11272012 C25005-03 Groundwater VOCs and Perchlorate Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -



1. Holding times X X 2. Detection limits X X 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X




2) No sample dilutions were required to quantitate any VOCs. All reporting limits are

determined to be acceptable. 3) Results from one full suite method blank were provided in association with the water

sample analyses. No VOCs were detected in the method blank.

One trip blank was analyzed. No VOCs were detected in the trip blank.

4-5) Accutest provided results from one full set of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses (identified as blank spike analyses) in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. LCS recoveries ranged from 92 to 130 percent (control limits


3

of 60-130 percent). The maximum RPD between LCS and LCSD results was 27 percent for acetone (upper laboratory control limit of 30 percent).

6-7) Accutest provided results from one full set of project specific MS and MSD analyses

in support of the VOC analyses (spike performed on project sample MW030). Precision and accuracy, as demonstrated by these analyses, are acceptable. MS recoveries ranged from 84 to 116 percent, with a maximum RPD between MS and MSD recoveries of 15 percent.

8) Three surrogates were spiked into each water sample in support of the VOC analyses.

Surrogate recoveries were acceptable, ranging from 94 to 104 percent. 9) Field duplicate samples were not collected with the samples under this chain-of-

custody.



4





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not evaluated 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X 9. Results Quantitation X X

%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The groundwater samples were sampled on November 27, 2012 and were received by

Accutest on November 29, 2012. The water samples were received chilled to an temperature of 3.0 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by December 6, 2012, within prescribed holding times.

2) Sample MW031 was diluted by a factor of 2 times to quantitate perchlorate due to

elevated perchlorate concentrations. No other sample dilutions were required to quantitate perchlorate. Reporting limits are determined to be acceptable.


analyses, with no perchlorate detected. 4) Results from continuing calibration analyses were not evaluated. 5-6) Accutest provided results from one set of project specific MS and MSD analyses in

support of the perchlorate analyses (spike on sample MW030). MS and MSD recoveries ranged from 95.2 to 98.0 percent. The RPD between the MS and MSD results was 2.5 percent. Precision and accuracy, as demonstrated by these analyses is acceptable.

4-6) Accutest provided results from one set of laboratory control sample (LCS) and LCS

duplicate (LCSD) analyses (identified as blank spike analyses) in support of the


5

groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries ranged from 92.8 to 98.0 percent. The RPD between the LCS and LCSD results was acceptable at 5.5 percent.

8) Field duplicate samples were not collected with the samples under this chain-of-

custody. 9) No anomalies were noted with respect to the perchlorate reporting.



LABORATORY REPORT # C25005 DATED DECEMBER 14, 2012

Geomatrix Consultants, Inc. (Geomatrix) collected two groundwater samples (blind performance evaluation samples) and one associated trip blank on November 27, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with no data qualifications required.

SIGNATURE:

DATE: December 26, 2012

L605508.doc Created on 12/19/2012 1:19:00 PM

1


ESC LABORATORY (MT JULIET, TENNESSEE)

LABORATORY REPORT # L605508 DATED NOVEMBER 30, 2012

INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 23 groundwater samples and seven associated quality control sample on November 5, 6, 7, and 8, 2012. The samples were shipped via overnight courier to ESC Laboratory, located in Mt. Juliet, Tennessee, on November 8, 2012. Samples arrived at the laboratory on the following day. Sample identifications and requested analyses are listed below.

Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-11052012 L605508-01 Quality Control VOCs / Trip Blank EPA-MW12A-11052012 L605508-02 Groundwater VOCs and Perchlorate EPA-MW12C-11052012 L605508-03 Groundwater VOCs and Perchlorate EB001-11052012 L605508-04 Quality Control VOCs and Perchlorate / Equipment Blank MW11-11062012 L605508-05 Groundwater VOCs and Perchlorate EPA-MW6A-11062012 L605508-06 Groundwater VOCs and Perchlorate EPA-MW28M-11062012 L605508-07 Groundwater VOCs MW10-11062012 L605508-08 Groundwater VOCs and Perchlorate EPA-MW13C-11062012 L605508-09 Groundwater VOCs and Perchlorate MW08-11062012 L605508-10 Groundwater VOCs and Perchlorate OWC-11062012 L605508-11 Groundwater VOCs and Perchlorate EB001-11062012 L605508-12 Quality Control VOCs and Perchlorate / Equipment Blank MW24-11072012 L605508-13 Groundwater VOCs DUP001-11072012 L605508-14 Quality Control VOCs / Field Duplicate of primary sample

MW24-11072012 EPA-MW51A-11072012 L605508-15 Groundwater VOCs and Perchlorate OWB-11072012 L605508-16 Groundwater VOCs and Perchlorate EA03 -11072012 L605508-17 Groundwater VOCs and Perchlorate EPA-MW26C-11072012 L605508-18 Groundwater VOCs and Perchlorate MW29-11072012 L605508-19 Groundwater VOCs and Perchlorate EC01-11072012 L605508-20 Groundwater VOCs and Perchlorate EB01-11072012 L605508-21 Groundwater VOCs and Perchlorate EA01-11072012 L605508-22 Groundwater VOCs and Perchlorate MW20-11072012 L605508-23 Groundwater VOCs and Perchlorate PZ01-11072012 L605508-24 Groundwater VOCs and Perchlorate DUP002-11072012 L605508-25 Quality Control VOCs and Perchlorate / Field Duplicate of

primary sample PZ01-11072012 EB001-11072012 L605508-26 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW47C-11082012 L605508-27 Groundwater VOCs and Perchlorate EPA-MW47A-11082012 L605508-28 Groundwater VOCs and Perchlorate EPA-MW13A-11082012 L605508-29 Groundwater VOCs and Perchlorate EB002-11082012 L605508-30 Quality Control VOCs and Perchlorate / Equipment Blank


2

Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method





REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X No C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on November 5, 6, 7, and 8, 2012.


3

The samples were analyzed by November 14, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.

2) Samples EPA-MW47C, EPA-MW47A, PZ01 and DUP002 were diluted by

factors of 10 times for TCE only. Sample EPA-MW13A was diluted by factor of 20 times for TCE only. No other sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).

Sample ID Qualified VOCs (ug/L) EPA-MW12A Chloroform = 0.80 J EPA-PZ01 Chloroform = 0.40 J EPA-PZ01 1,1-DCE = 0.74 J EPA-PZ01 PCE = 0.47 J DUP002-11072012 Chloroform = 0.39 J DUP002-11072012 1,1-DCE = 0.88 J DUP002-11072012 PCE = 0.38 J

EPA-MW47A Chloroform = 0.49 J EPA-MW47A 1,1-DCE = 0.46 J EPA-MW13A Carbon tetrachloride = 0.94 J EPA-MW13A Chloroform = 1.3 J EPA-MW13A 1,1-DCE = 0.88 J EPA-MW13A PCE = 0.55 J

3) Results from five full suite method blanks were provided in association with the groundwater sample analyses. Two additional method blanks were provided for TCE only. No VOCs were detected in the method blanks.

Results from one trip blank were provided, with no VOCs detected. Results from four equipment blanks were provided. Acetone was detected in equipment blank EB002-1182012 at an estimated concentration of 5.0 ug/L. Acetone was not detected in any of the associated samples, an no action is taken. No other VOCs were detected in the equipment blanks.

4-5) ESC Laboratory provided results from five full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses. Two additional sets of LCS/LCSD analyses were provided for TCE only. Precision and accuracy, as demonstrated by these analyses is acceptable.


4

6-7) ESC Laboratory provided results from three sets of project specific MS and MSD

analyses (spikes on project samples EPA-MW12A, EB001-11052012 and EB001-11-62012), and from two sets of batch specific MS and MSD analyses. Two additional set of batch specific MS and MSD analyses were performed for TCE only. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. The 1,1,2,2-tetrachloroethane MS and MSD recoveries were high in the project spike of sample EPA-MW12A spike at 194 percent and 200 percent (upper control limit of 149 percent). No action is required, as 1,1,2,2-tetrachloroethane was not detected in any of the associated samples.

8) Three primary surrogates, and one alternate surrogate, were spiked into each

groundwater sample in support of the VOC analyses. All surrogate recoveries were within prescribed control limits, ranging from 90.9 to 119 percent.

9) Two sets of blind field duplicate samples were submitted with the samples under this

chain-of-custody. Sample DUP001-11072012 was submitted as a blind field duplicate of primary sample MW24. No VOCs were detected in either of the samples. Field duplicate precision is determined to be acceptable.

Sample DUP002-11072012 was submitted as a blind field duplicate of primary

sample PZ01. Precision between the duplicate sample results, measured as the relative percent difference (RPD) between the primary and duplicate sample results, is calculated in the following table. Results are presented in micrograms per liter (ug/L).

DUP002 PZ01 % RPD

Chloroform 0.39 J 0.40 J 2.5 1,1-Dichloroethene 0.88 J 0.74 J 17 PCE 0.38 J 0.47 J 11 TCE 450 450 21

Field duplicate precision is determined to be acceptable, with all RPDs less than 25

percent. 10) No anomalies were noted with respect to results quantitation or reporting.


5





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X See note #2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X Yes 6. MS Duplicate (MSD) %R and RPD X X Yes 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Yes 9. Results Quantitation X X

%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The water samples were received by ESC Laboratory on November 9, 2012. The

water samples were received at an acceptable temperature of 3.1 degrees on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by November 20, 2012, within prescribed holding times.

2) All groundwater samples were analyzed at 5 times dilutions, except for samples

EPA-MW47C, EPA-MW47A, EPA-MW13A and EB01 (10 times); and MW10 and OWC (2 times). Reporting limits are determined to be acceptable, with the following considerations. Perchlorate was only detected in one of the sample analyzed (PZ-01). The five fold dilution results in a reporting limit of 2.5 ug/L, which is similar to the 2.0 ug/L reporting limit used by TestAmerica for undiluted samples. The laboratory noted matrix interference for all samples analyzed at dilutions, where no perchlorate was detected.

3) Results from three method blanks were provided in support of the groundwater sample

analyses with no perchlorate detected. Results from four equipment blanks were also provided. Perchlorate was not detected in any of the equipment blanks.

4) Results from continuing calibration analyses were not provided. 5-6) ESC Laboratory provided results from two sets of project specific MS and MSD

analyses (spikes on project samples EPA-MW12A and EB001-11072012), and from one batch MS and MSD set in support of the perchlorate analyses. MS and


6

MSD recoveries ranged from 43 percent to 145 percent, with a maximum RPD between MS and MSD recoveries of 28 percent. MS recoveries were low for the project spike of sample EPA-MW12A at 43 and 52 percent (lower laboratory control limit of 80 percent). MS and MSD recoveries for the batch spike analyzed in the same analytical batch were high at 130 percent and 140 percent (upper control limit of 120 percent). The MS recovery for the spike of the equipment blank were high at 145 percent and precision was poor with an RPD of 28 percent (project precision control limit of 25 percent maximum). Due to the poor precision and accuracy demonstrated by the MS and MSD results, and low bias shown by the groundwater project spike, all perchlorate results are qualified as UJ/Estimated and non-detect at the reporting limits stated. for non-detects, and J/Estimated for the detection in sample PZ01.

7) ESC Laboratory provided results from three sets of LCS and LCSD analyses in

support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS and LCSD recoveries ranged from 90.8 to 109 percent, with a maximum RPD of 0.9 percent between LCS duplicate results.


PZ01. Perchlorate was detected in the primary sample at 6.7 ug/L and was not detected in the duplicate sample at <2.5 ug/L. Precision between the perchlorate duplicate sample results is very poor, with an RPD of at least 91 percent. Due to the poor field duplicate precision, perchlorate results for the primary and duplicate samples are qualified as J/Estimated.

ESC Laboratory provided results from four sets of project specific laboratory

duplicate sample analyses, performed on project samples EB001-11052012, EB001-11062012, EPA-MW26A and EB002-11082012. The laboratory duplicate precision is acceptable. No perchlorate was detected in any of the samples. Laboratory duplicates of equipment blanks do not provide significant information.



7



LABORATORY REPORT # L605508 DATED NOVEMBER 30, 2012

Geomatrix Consultants, Inc. (Geomatrix) collected 23 groundwater samples and seven associated quality control sample on November 5, 6, 7, and 8, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s) Reason(s) For Qualification

EPA-MW12A-11052012 / Chloroform EPA-PZ01-11072012 / Chloroform, 1,1-DCE, and PCE DUP002-11072012 / Chloroform, 1,1-DCE, and PCE EPA-MW47A-11082012 / Chloroform and 1,1-DCE EPA-MW13A-11082012 / Carbon tetrachloride, Chloroform, 1,1-DCE, and PCE

J/Estimated




All samples analyzed for perchlorate / Perchlorate

UJ/Estimated and non-detect at the reporting limits stated. for non-

detects

J/Estimated (PZ01)

Low matrix spike recoveries on project spike. Poor QC sample

selection on spikes and duplicates. Stated matrix interference issues.

Poor precision between results of field duplicate samples. RPD far

exceeds 25 percent

SIGNATURE:

DATE:

December 20, 2012

L608220.doc 12/20/2012 10:59:00 AM

1



LABORATORY REPORT # L608220 DATED DECEMBER 10, 2012

INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected two groundwater samples (blind performance evaluation samples) and one associated trip blank on November 27, 2012. The samples were shipped via overnight courier to ESC Laboratory, located in Mt. Juliet, Tennessee, on November 28, 2012. Samples arrived at the laboratory on the following day. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB004-11272012 L608220-01 Quality Control VOCs / Trip Blank MW030-11272012SP1 L608220-02 Groundwater VOCs and Perchlorate MW031-11272012SP1 L608220-03 Groundwater VOCs and Perchlorate Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method


L608220.doc 12/20/2012 10:59:00 AM

2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X Yes 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X






Sample ID Qualified VOCs (ug/L) MW030 Methylene chloride = 1.9 J

MW031 Methylene chloride = 1.1 J

L608220.doc 12/20/2012 10:59:00 AM

3

3) Results from one full suite method blank were provided in association with the groundwater sample analyses. No VOCs were detected in the method blank.

Results from one trip blank were provided. Methylene chloride was detected in the trip blank at an estimated concentration of 0.96 ug/L. Methylene chloride was also detected in both water samples at concentrations within 10 times that of the trip blank (rule for common blank contaminants, though methylene chloride detections are within a factor of 2 times the trip blank detection). Due to potential blank contamination bias, the following methylene chloride results are qualified as U/non-detect at the concentration reported.

Sample ID Qualified VOCs (ug/L) MW030 Methylene chloride = 1.9 U

MW031 Methylene chloride = 1.1 U

4-5) ESC Laboratory provided results from one full set of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. LCS and LCSD recoveries ranged from 85.1 to 109 percent. The maximum RPD between LCS and LCSD recoveries was 13 percent.

6-7) ESC Laboratory provided results from one set of project specific MS and MSD

analyses (spike on project sample MW030) in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 44.8 to 103 percent. The maximum RPD between MS and MSD recoveries was 11 percent for acetone.


groundwater sample in support of the VOC analyses. All primary surrogate recoveries were within prescribed control limits, ranging from 94.1 to 111 percent.


custody. 10) No anomalies were noted with respect to results quantitation or reporting.

L608220.doc 12/20/2012 10:59:00 AM

4





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only, see

note #8 9. Results Quantitation X X

%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The water samples were collected on November 27, 2012 and were received by

ESC Laboratory on November 29, 2012. The water samples were received at an acceptable temperature of 3.1 degrees on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by December 16, 2012, within prescribed holding times.


determined to be acceptable. 3) Results from one method blank were provided in support of the groundwater sample

analyses with no perchlorate detected. 4) Results from continuing calibration analyses were not provided. 5-6) ESC Laboratory provided results from one set of project specific MS and MSD

analyses (spike on project sample MW031) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were 112 and 113 percent, with an RPD between spike results of 0.7 percent.

7) ESC Laboratory provided results from one set of LCS and LCSD analyses in support

of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses

L608220.doc 12/20/2012 10:59:00 AM

5

is acceptable. Aqueous LCS and LCSD recoveries were 92.5 and 97.5 percent, with an RPD of 5.3 percent between LCS duplicate results.


custody. ESC Laboratory provided results from one set of laboratory duplicate sample

analyses performed on project sample MW030. Perchlorate was not detected in the primary analyses at <0.5 ug/L but was detected in the duplicate analysis at 1.4 ug/L. ESC flagged the results for poor precision, noting that the RPD is not applicable to samples results less than 5 times below reporting limits. Both results agree within the standard project reporting limit of 2.5 ug/L used by TestAmerica. Therefore, the results are not qualified due to the poor precision near reporting limits.


L608220.doc 12/20/2012 10:59:00 AM

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LABORATORY REPORT # L608220 DATED DECEMBER 10, 2012

Geomatrix Consultants, Inc. (Geomatrix) collected two groundwater samples (blind performance evaluation samples) and one associated trip blank on November 27, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)


MW030-11272012 / Methylene chloride MW031-11272012 / Methylene chloride

U/Non-detect at the

concentration reported

Methylene chloride was detected in the associated trip blank at a

concentration within 10 times those of the associated samples.

Methylene chloride detections may be the result of blank contamination

bias.

SIGNATURE:

DATE: December 20, 2012

PVK0632.doc Created on 11/27/2012 5:23:00 PM

1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 17 groundwater/wastewater samples and one associated trip blank on November 5, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on November 8, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

PH1-EFF-11052012 PVK0632-01 Groundwater VOCsPH1-INF-11052012 PVK0632-02 Groundwater VOCsPH23-EFF-11052012 PVK0632-03 Groundwater VOCsPH23-INF-11052012 PVK0632-04 Groundwater VOCsIX-EFF-11052012 PVK0632-05 Groundwater Perchlorate IX-VI-11052012 PVK0632-06 Groundwater Perchlorate IX-INF-11052012 PVK0632-07 Groundwater Perchlorate TB001-11052012 PVK0632-08 Quality Control VOCs / Trip Blank EA05-EFF-11052012 PVK0632-09 Groundwater VOCs EA05-MID-11052012 PVK0632-10 Groundwater VOCs EA05-INF-11052012 PVK0632-11 Groundwater VOCs and Perchlorate EA06-EFF-11052012 PVK0632-12 Groundwater VOCs EA06-MID-11052012 PVK0632-13 Groundwater VOCs EA06-INF-11052012 PVK0632-14 Groundwater VOCs and Perchlorate 33A-EFF-11052012 PVK0632-15 Groundwater VOCs 33A-101-11052012 PVK0632-16 Groundwater VOCs 33A-202-11052012 PVK0632-17 Groundwater VOCs 33A-INF-11052012 PVK0632-18 Groundwater VOCs and Perchlorate Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2



REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X No 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X




2) No sample dilutions were required. All reporting limits are acceptable with the

following considerations. Numerous VOCs were reported at concentrations between the method detection limit (MDL) and the standard reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (Pending results of the blank evaluation):


PH1-INF 1,1-DCE = 0.30 J PH1-INF Chloroform = 0.21 J PH23-INF 1,1-DCE = 0.30 J


3

Sample ID Qualified VOCs (ug/L) EA05-MID Chloroform = 0.47 J EA05-INF Chloroform = 0.37 J 33A-101 Chloroform = 0.71 J 33A-INF Chloroform = 0.63 J

3) Results from two full suite method blanks were provided in association with the groundwater sample analyses. No VOCs were detected in the method blanks.

Results from one trip blank were provided. No VOCs were detected in the trip blank.

4-5) TestAmerica provided results two full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. For batch 12K0522, the LCSD recovery for 1,1,2,2-tetrachloroethane was high at 131 percent (upper limit of 125 percent). No action is required, as 1,1,2,2-tetrachloroethane was not detected in any associated samples. For batch 12K0523, the LCS recovery for trichlorofluoromethane was high at 126 percent (upper limit of 123 percent). No action is required, as trichlorofluoromethane was not detected in any associated samples.


(spike on project sample EA05-EFF), and from one set of batch specific MS and MSD analyses, in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses are acceptable, with the following exceptions. For the batch spike, MS/MSD recoveries were low for m/p-xylenes and ethylbenzene. No action is required, as acceptable precision and accuracy for these VOCs is demonstrated by the results of the LCS and LCSD analyses. MS and MSD recoveries for the project spike are in control.


analyses. Surrogate recoveries ranged from 106 to 124 percent. Numerous 4-bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent upper project control limit. Some toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit, as follows:


PH1-EFF-11052012 4-BFB = 119 None PH1-INF-11052012 4-BFB = 123 TCE PH23-EFF-11052012 4-BFB = 119 None PH23-INF-11052012 4-BFB = 122 TCE EA05-EFF-11052012 4-BFB = 117 None EA05-MID-11052012 4-BFB = 122 TCE


4

Sample ID High Surr Rec (%) Data qualified ? EA05-INF-11052012 4-BFB = 122 TCE EA06-EFF-11052012 4-BFB = 123 None EA06-MID-11052012 4-BFB = 122 TCE and Chloroform EA06-MID-11052012 Toluene-d8 = 122 TCE and Chloroform EA06-INF-11052012 4-BFB = 121 TCE and Chloroform 33A-EFF-11052012 4-BFB = 124 None 33A-EFF-11052012 Toluene-d8 = 115 None 33A-101-11052012 4-BFB = 122 None 33A-202-11052012 4-BFB = 123 Chloroform 33A-INF-11052012 4-BFB = 123 TCE 33A-INF-11052012 Toluene-d8 = 123 TCE

Many detections for these samples are already qualified, due to reporting limit (MDL/RL) considerations. Any additional VOC detections are listed above, and are qualified as J/Estimated, due to potential high bias.

9) Field duplicate samples were not submitted with the samples under this chain-of-



5





DATA QUALIFIED -




#2 3. Blanks A. Method/Prep Blanks X X B. Equipment /Decon / Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only 9. Results Quantitation X X




determined to be acceptable, with the following consideration. Perchlorate was reported at a concentration between the method detection limit (MDL) and standard reporting limit in groundwater sample IX-EFF. Due to limited accuracy in this portion of the calibration range, this perchlorate result is qualified as J/Estimated.


analyses with no perchlorate detected. 4) Results from continuing calibration analyses were not provided. 5-6) TestAmerica provided results from one set of project specific MS and MSD analyses

(spike on project sample EA05-INF), and from one set of batch specific MS and MSD analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.


6

Aqueous MS and MSD recoveries ranged from 105 to 109 percent, with a maximum RPD between MS and MSD recoveries of 2 percent.


the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. LCS and LCSD recoveries ranged from 107 to 113 percent, with a maximum RPD between LCS and LCSD results of 2 percent.


Results from one set of project specific laboratory duplicate sample analyses were provided on sample IX-INF. Perchlorate precision was acceptable, with an RPD between duplicate detections of 5 percent.



7




Geomatrix Consultants, Inc. (Geomatrix) collected 17 groundwater/wastewater samples and one associated trip blank on November 5, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most recent versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


PH1-INF-11052012 / 1,1-DCE and Chloroform PH23-INF-11052012 / 1,1-DCE EA05-MID-11052012 / Chloroform EA05-INF-11052012 / Chloroform 33A-101-11052012 / Chloroform 33A-INF-11052012 / Chloroform

J/Estimated




Surrogate recoveries for these samples were also high.

PH1-INF-11052012 / TCE PH23-INF-11052012 / TCE EA05-MID-11052012 / TCE EA05-INF-11052012 / TCE EA06-MID-11052012 / TCE and Chloroform EA06-INF-11052012 / TCE and Chloroform 33A-202-11052012 / Chloroform 33A-INF-11052012 / TCE

J/Estimated

Associated surrogate recoveries were high. Results for these VOCs may be

biased high

IX-EFF-11052012/ Perchlorate

J/Estimated



SIGNATURE:

DATE:

November 27, 2012


1





TB001-11082012 PVK0684-01 Quality Control VOCs / Trip Blank EPA-MW11A-11082012 PVK0684-02 Groundwater VOCs and Perchlorate EPA-MW2C-11082012 PVK0684-03 Groundwater VOCs and Perchlorate EPA-MW8C-11082012 PVK0684-04 Groundwater VOCs and Perchlorate EPA-MW58A-11082012 PVK0684-05 Groundwater VOCs and Perchlorate EPA-MW10C-11082012 PVK0684-06 Groundwater VOCs and Perchlorate EPA-MW9C-11082012 PVK0684-07 Groundwater VOCs and Perchlorate EPA-MW10A-11082012 PVK0684-08 Groundwater VOCs and Perchlorate DUP001-11082012 PVK0684-09 Quality Control VOCs and Perchlorate / Field Duplicate or

primary sample EPA-MW10A-11082012 EB001-11082012 PVK0684-10 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X







EPA-MW8C PCE = 0.95 J EPA-MW8C TCE = 0.31 J DUP001 Chloroform = 0.30 J


3

3) Results from two full suite method blanks were provided in association with the groundwater sample analyses. No VOCs were detected in either of the method blanks.


4-5) TestAmerica provided results from two full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with one exception. One LCSD recovery was high for carbon tetrachloride. Carbon tetrachloride was not detected in the associated samples, and no action is required.


(spike on project sample EPA-MW11A), and from one set of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable for all VOCs, with the following exception. The MSD recovery for trichlorofluoromethane was high in the batch spike at 138 percent. Trichlorofluoromethane was not detected in the associated samples, and no action is required.


analyses. Surrogate recoveries ranged from 106 to 129 percent. Numerous 4-bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent upper project control limit. Toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit, as follows:


EPA-MW11A 4-BFB = 116 PCE EPA-MW11A Tol-d8 = 114 PCE EPA-MW2C 4-BFB = 115 None EPA-MW8C 4-BFB = 119 None EPA-MW8C Tol-d8 = 115 None EPA-MW58A 4-BFB = 115 PCE and TCE EPA-MW58A Tol-d8 = 114 PCE and TCE EPA-MW10C 4-BFB = 115 TCE EPA-MW9C Tol-d8 = 117 TCE EPA-MW10A 4-BFB = 121 PCE and TCE EPA-MW10A Tol-d8 = 113 PCE and TCE


4

Sample ID High Surr Rec (%) Data qualified ? DUP001 4-BFB = 120 PCE and TCE DUP001 Tol-d8 = 114 PCE and TCE

Some detections for these samples are already qualified, due to reporting limit (MDL/RL) considerations. Any additional VOC detections are listed above, and are qualified as J/Estimated, due to potential high bias.


EPA-MW10C. TCE was detected in the primary and duplicate samples at concentrations of 130 ug/L and 120 ug/L, respectively. Precision between the TCE detections is acceptable, with an RPD of 8 percent. PCE was detected in the primary and duplicate samples at concentrations of 1.2 ug/L and 1.1 ug/L, respectively. Precision between the TCE detections is acceptable, with an RPD of 8.7 percent. Chloroform was detected in the duplicate sample at a concentration between the MDL and RL and was not detected in the primary sample. Chloroform results agree within a reporting limit increment. Field duplicate precision is determined to be acceptable.



5





DATA QUALIFIED -




#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X 9. Results Quantitation X X




determined to be acceptable, with the following considerations. Perchlorate was reported at a concentration between the method detection limit (MDL) and the reporting limit in sample EPA-MW8C. Due to limited accuracy in this portion of the calibration range, this perchlorate result is qualified as J/Estimated.



4) Results from continuing calibration analyses were not provided. 5-6) TestAmerica provided results from one set of project specific MS and MSD

analyses in support of the perchlorate analyses (spike on project sample EPA-MW11A), and from one set of batch specific MS and MSD analyses. Precision and


6

accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 105 to 109 percent, with a maximum RPD between MS and MSD recoveries of 2 percent.


support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries ranged from 107 and 113 percent. The maximum RPD between LCS and LCSD results was acceptable at 2 percent.


EPA-MW10A. Perchlorate was detected in the primary and duplicate samples at concentrations of 30 ug/L, each. Precision between the field duplicate samples is acceptable, with an RPD of 0 percent.




7




Geomatrix Consultants, Inc. (Geomatrix) collected seven groundwater samples and three associated quality control samples on November 8, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW8C-11082012 / PCE and TCE DUP001-11082012 / Chloroform

J/Estimated




may be limited. EPA-MW11A-11082012 / PCE EPA-MW58A-11082012 / PCE and TCE EPA-MW10C-11082012 /TCE EPA-MW9C-11082012 / TCE EPA-MW10A-11082012 / PCE and TCE DUP001-11082012 / PCE and TCE

J/Estimated

Associated surrogate recoveries were high. Sample detections for these VOCs may be biased

high.


J/Estimated

Perchlorate was reported at a concentration between the

method detection limit and the reporting limit. Accuracy in this portion of the calibration curve

may be limited.

SIGNATURE:

DATE:

November 27, 2012


1





TB001-11142012 PVK1220-01 Quality Control VOCs / Trip Blank EPA-MW44A-11142012 PVK1220-02 Groundwater VOCs and Perchlorate MW17-11142012 PVK1220-03 Groundwater VOCs EB001-11142012 PVK1220-04 Quality Control VOCs and Perchlorate / Equipment Blank COA15-11152012 PVK1220-05 Groundwater Perchlorate COA18-11152012 PVK1220-06 Groundwater VOCs and Perchlorate COG03-11152012 PVK1220-07 Groundwater VOCs and Perchlorate COG06-11152012 PVK1220-08 Groundwater VOCs and Perchlorate COG18A-11152012 PVK1220-09 Groundwater VOCs and Perchlorate COG18B-11152012 PVK1220-10 Groundwater VOCs and Perchlorate EPA-MW24C-11152012 PVK1220-11 Groundwater VOCs EPA-MW20A-11152012 PVK1220-12 Groundwater VOCs EPA-MW17A-11152012 PVK1220-13 Groundwater VOCs EPA-MW32A-11152012 PVK1220-14 Groundwater VOCs DUP001-11152012 PVK1220-15 Quality Control VOCs / Field Duplicate of primary sample

EPA-MW32A-11152012 EPA-MW37A-11152012 PVK1220-16 Groundwater VOCs EB001-11152012 PVK1220-17 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X No C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X





acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).

Sample ID Qualified VOCs (ug/L) EPA-MW44A Chloroform = 0.72 J



3

Sample ID Qualified VOCs (ug/L) EPA-MW20A PCE = 0.49 J

EPA-MW37A Chloroform = 0.46 J 3) Results from five full suite method blanks were provided in association with the


Results from one trip blank were provided, with no VOCs detected. Results from two equipment blanks were provided. Methylene chloride was detected in the equipment blank collected on November 15, 2012 at a concentration of 2.4 ug/L. Methylene chloride was not detected in any of the associated samples, and no action is required.

4-5) TestAmerica provided results from five full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. Precision between LCS and LCSD recoveries for acetone and 2-butanone was poor, with RPDs of 43 percent and 34 percent, respectively in one LCS set (project precision control limit of 25 percent). Precision between LCS and LCSD recoveries for acetone was poor, with RPDs of 37 and 28 percent in two other LCS sets. Acetone and 2-butanone were not detected in the associated samples, and no bias to the sample results is indicated.


(spike on project sample EPA-MW44A), and from four sets of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with one exception. The MS recovery for 1,1,2,2-tetrachloroethane was high in one batch spike at 130 percent (upper control limit of 124 percent). 1,1,2,2-Tetrachloroethane was not detected in any of the associated samples, and no action is required.


analyses. Surrogate recoveries ranged from 109 to 128 percent. Numerous 4-bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent upper project control limit. Several toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit, as follows:


EPA-MW41A 4-BFB = 117 Chloroform EPA-MW41A Tol-d8 = 112 Chloroform MW17 4-BFB = 120 Chloroform COA18 4-BFB = 120 None COA18 Tol-d8 = 112 None


4

Sample ID High Surr Rec (%) Data qualified ? COG03 4-BFB = 117 None COG03 Tol-d8 = 113 None COG06 4-BFB = 121 None COG18A 4-BFB = 117 None COG18A Tol-d8 = 112 None COG18B 4-BFB = 122 None COG18B Tol-d8 = 118 None EPA-MW24C 4-BFB = 120 None EPA-MW24C Tol-d8 = 116 None EPA-MW20A 4-BFB = 121 Chloroform, PCE, TCE EPA-MW20A Tol-d8 = 114 Chloroform, PCE, TCE EPA-MW17A Tol-d8 = 114 None EPA-MW32A 4-BFB = 122 None EPA-MW32A Tol-d8 = 113 None DUP001 4-BFB = 117 None DUP001 Tol-d8 = 114 None EPA-MW37A Tol-d8 = 114 Chloroform

Most of these detections are already qualified, due to reporting limit (MDL/RL) considerations. Chloroform and TCE in sample EPA-MW20A are additionally qualified due to the high surrogates.


EPA-MW32A. No VOCs were detected in either of the samples, and field duplicate precision is acceptable

10) No anomalies were noted with respect to results quantitation or reporting. .


5





DATA QUALIFIED -




#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab Only 9. Results Quantitation X X




determined to be acceptable, with the following consideration. Perchlorate was reported at concentrations between the method detection limit (MDL) and the standard reporting limit in the following samples. Due to limited accuracy in this portion of the calibration curve, these perchlorate results are qualified as J/Estimated.

Sample ID Qualified Perchlorate (ug/L) COA18 Perchlorate = 1.6 J COG18B Perchlorate = 0.93 J 3) Results from two method blanks were provided in support of the groundwater sample




6


(spike on project sample EPA-MW44A), and from two sets of batch specific MS and MSD analyses in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 104 to 110 percent, with a maximum RPD between MS and MSD recoveries of 3 percent.




TestAmerica provided results from two sets of laboratory duplicate sample analyses; one performed on project sample COA15. The laboratory duplicate precision is acceptable, with an RPD of 3 percent for the batch duplicate, and an RPD of 47 percent for the project duplicate. This 47 percent RPD exceeds the project RPD maximum control limit of 25 percent, but no action is taken as the duplicate results agree within a reporting limit increment.

9) No anomalies were noted with respect to results quantitation or reporting. .


7




Geomatrix Consultants, Inc. (Geomatrix) collected 13 groundwater samples and four associated quality control samples on November 14 and 15, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW44A-11142012 / Chloroform MW17-11142012 / Chloroform EPA-MW20A-11152012 / PCE EPA-MW37A-11152012 / Chloroform

J/Estimated




limited. Surrogate recoveries for these VOCs are also high. Results

may be biased high.

EPA-MW20A-11152012 / Chloroform and TCE J/Estimated Surrogate recoveries are high. Sample results may be biased high.

. COA18-11152012 and COG18B-11152012 / Perchlorate

J/Estimated


detection limit and the reporting limit. Accuracy in this portion of

the calibration curve may be limited.

SIGNATURE:

DATE:

November 27, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected six groundwater/wastewater samples on November 19, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on November 19, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

EA06-EFF-11192012 PVK1286-01 Groundwater VOCs EA06-MID-11192012 PVK1286-02 Groundwater VOCs EA06-INF-11192012 PVK1286-03 Groundwater VOCs EA08-EFF-11192012 PVK1286-04 Groundwater VOCs EA08-MID-11192012 PVK1286-05 Groundwater VOCs EA08-INF-11192012 PVK1286-06 Groundwater VOCs and Perchlorate Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2



REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X



degrees Celsius on wet ice (no samples arrived at the laboratory frozen). The groundwater samples were properly preserved with hydrochloric acid at the time of collection on November 19, 2012. The samples were analyzed by November 22, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.


are acceptable with the following considerations. Chloroform was detected at concentrations between the method detection limit (MDL) and the standard reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (Pending results of the blank evaluation):


EA06-EFF Chloroform = 0.44 J EA08-EFF Chloroform = 0.65 J EA08-INF Chloroform = 0.94 J


3

3) Results from one full suite method blank were provided in association with the groundwater sample analyses. No VOCs were detected in the method blank. A trip blank was not submitted with the samples.

4-5) TestAmerica provided results one full set of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. Precision between LCS and LCSD recoveries for acetone was poor with an RPD of 28 percent. Acetone was not detected in any of the groundwater samples, and no bias to the sample results is indicated.

6-7) TestAmerica provided results from one set of batch specific MS and MSD analyses

in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses are acceptable.



Sample ID High Surr Rec (%) Data qualified

EA06-EFF 4-BFB = 119 Chloroform EA06-EFF Tol-d8 = 114 Chloroform EA06-MID 4-BFB = 118 Chloroform and TCE EA06-MID Tol-d8 = 113 Chloroform and TCE EA06-INF 4-BFB = 120 Chloroform and TCE EA06-INF Tol-d8 = 113 Chloroform and TCE EA08-EFF 4-BFB = 122 Chloroform EA08-EFF Tol-d8 = 112 Chloroform EA08-MID 4-BFB = 119 Chloroform and TCE EA08-MID Tol-d8 = 114 Chloroform and TCE EA08-INF 4-BFB = 121 Chloroform and TCE EA08-INF Tol-d8 = 117 Chloroform and TCE

Some of these detections are already qualified, due to reporting limit (MDL/RL) considerations. Other chloroform and TCE detections are additionally qualified due to the high surrogates.


custody.


4






DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment /Decon / Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only 9. Results Quantitation X X





analyses with no perchlorate detected. 4) Results from continuing calibration analyses were not provided. 5-6) TestAmerica provided results from two sets of batch specific MS and MSD analyses.

Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous MS and MSD recoveries ranged from 107 to 110 percent, with maximum RPD between MS and MSD recoveries of 2 percent.


5


the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. LCS and LCSD recoveries were 99 and 108 percent, with an RPD between LCS and LCSD results of 9 percent.


Results from one set of laboratory duplicate sample analyses were provided for a duplicate of project sample EA08-INF. Perchlorate precision was acceptable, with an RPD between duplicate detections of 3 percent.



6




Geomatrix Consultants, Inc. (Geomatrix) collected six groundwater/wastewater samples on November 19, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most recent versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EA06-EFF-11192012 / Chloroform EA08-EFF-11192012 / Chloroform EA08-INF-11192012 / Chloroform

J/Estimated

Chloroform was reported at concentrations between the method



EA06-EFF-11192012 / Chloroform EA06-MID-11192012 / Chloroform and TCE EA06-INF-11192012 / Chloroform and TCE EA08-EFF-11192012 / Chloroform EA08-MID-11192012 / Chloroform and TCE EA08-INF-11192012 / Chloroform and TCE

J/Estimated

Surrogate recoveries exceed project specific control limits. Sample

results may be biased high.

SIGNATURE:

DATE:

December 9, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected five groundwater samples and two associated quality control samples on November 16, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on November 19, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-11162012 PVK1288-01 Quality Control VOCs / Trip Blank AEIW-11162012 PVK1288-02 Groundwater VOCs and Perchlorate EPA-MW36A-11162012 PVK1288-03 Groundwater VOCs EPA-MW41A-11162012 PVK1288-04 Groundwater VOCs EPA-MW19C-11162012 PVK1288-05 Groundwater VOCs and Perchlorate EPA-MW4C-11162012 PVK1288-06 Groundwater VOCs and Perchlorate EB001-11162012 PVK1288-07 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X No C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X



degrees Celsius on wet ice (no samples were frozen). The groundwater samples were properly preserved with hydrochloric acid at the time of collection on November 16, 2012. The samples were analyzed by November 21, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.







3

One trip blank was analyzed, with no VOCs detected. Results from one equipment blank were provided. Methylene chloride was detected in the equipment blank at a concentration of 2.4 ug/L. Methylene chloride was not detected in any associated samples, and no action is required.

4-5) TestAmerica provided results from one full set of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with one exception. Precision between LCS and LCSD recoveries was poor for acetone with an RPD of 28 percent. No action is taken, as acetone was not detected in any associated samples, and no bias to the acetone results is indicated.






AEIW 4-BFB = 124 None AEIW Tol-d8 = 115 None EPA-MW36A 4-BFB = 121 None EPA-MW41A 4-BFB = 120 Chloroform EPA-MW41A Tol-d8 = 115 Chloroform EPA-MW19C 4-BFB = 126 None EPA-MW19C Tol-d8 = 113 None EPA-MW4C 4-BFB = 121 None EPA-MW4C Tol-d8 = 115 None

The chloroform detection is already qualified, due to reporting limit (MDL/RL) considerations. No additional VOC detections are qualified.




4





DATA QUALIFIED -




#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only 9. Results Quantitation X X




determined to be acceptable, with the following considerations. Perchlorate was reported at a concentration between the method detection limit (MDL) and the reporting limit in sample AEIW. Due to limited accuracy in this portion of the calibration range, this perchlorate result is qualified as J/Estimated.




analyses in support of the perchlorate analyses (spike on project sample AEIW), and from one set of batch specific MS and MSD analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged


5

from 107 to 110 percent, with a maximum RPD between MS and MSD recoveries of 2 percent.


support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries ranged from 99 and 108 percent. The RPD between LCS and LCSD results was acceptable at 9 percent.


custody.




6




Geomatrix Consultants, Inc. (Geomatrix) collected five groundwater samples and two associated quality control samples on November 16, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW41A-11162012/ Chloroform

`

J/Estimated

Chloroform was reported at a

concentration between the method detection limit and the


may be limited. EPA-MW41A-11162012/ Chloroform

J/Estimated

Associated surrogate recoveries were high. Sample detections for these VOCs may be biased

high. AEIW-11162012 / Perchlorate

`

J/Estimated

Perchlorate was reported at a

concentration between the method detection limit and the


may be limited.

SIGNATURE:

DATE:

November 27, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 12 groundwater samples and four associated quality control samples on November 19, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on November 20, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-11192012 PVK1375-01 Quality Control VOCs / Trip Blank MW28-11192012 PVK1375-02 Groundwater VOCs and Perchlorate MW14-11192012 PVK1375-03 Groundwater VOCs and Perchlorate DUP001-11192012 PVK1375-04 Quality Control VOCs and Perchlorate / Field Duplicate of

primary sample MW14-11192012 MW13-11192012 PVK1375-05 Groundwater VOCs and Perchlorate EPA-MW40C-11192012 PVK1375-06 Groundwater VOCs and Perchlorate EPA-MW40A-11192012 PVK1375-07 Groundwater VOCs EPA-MW53A-11192012 PVK1375-08 Groundwater VOCs and Perchlorate EPA-MW52A-11192012 PVK1375-09 Groundwater VOCs and Perchlorate EPA-MW61A-11192012 PVK1375-10 Groundwater VOCs and Perchlorate EPA-MW17C-11192012 PVK1375-11 Groundwater VOCs EPA-MW18A-11192012 PVK1375-12 Groundwater VOCs EA06-11192012 PVK1375-13 Groundwater VOCs and Perchlorate EPA-MW23A-11192012 PVK1375-14 Groundwater VOCs DUP002-11192012 PVK1375-15 Quality Control VOCs / Field Duplicate of primary sample

EPA-MW23A-11192012 EB001-11192012 PVK1375-16 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X No C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X No 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X






Sample ID Qualified VOCs (ug/L) MW13 Chloroform = 0.65 J

EPA-MW53A Acetone = 4.2 J EPA-MW17C Chloroform = 0.48 J


3

Sample ID Qualified VOCs (ug/L) EPA-MW18A PCE= 0.51 J EPA-MW18A TCE = 0.81 J EPA-MW23A Chloroform = 0.29 J 3) Results from three full suite method blanks were provided in association with the


Results from one trip blank were provided, with no VOCs detected. Results from one equipment blank were provided. Methylene chloride was detected in the equipment blank at an estimated concentration of 1.7 ug/L. Methylene chloride was not detected in any of the associated samples, and no action is required.

4-5) TestAmerica provided results from three full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. LCSD and LCSD recoveries for several VOCs from batch 12K0905 are high. This batch is associated with analysis of the equipment blank only, and no action is required.

6-7) TestAmerica provided results from two sets of project specific MS and MSD

analyses (spikes on project samples MW28 and EPA-MW53A-11192012), and from one set of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. For the project spikes of sample MW28, the MS recovery was high for 1,1,2,2-tetrachloroethane. No action is required, as 1,1,2,2-tetrachloroethane was not detected in the associated samples. Several VOCs were high in the batch spike which is associated with the equipment blank only. No action is taken for these exceedences.

8) Three surrogates were spiked into each water sample in support of the VOC



MW28 4-BFB = 120 None MW14 4-BFB = 117 None MW14 Tol-d8 = 114 None DUP001 4-BFB = 122 None DUP001 Tol-d8 = 116 None


4


MW13 4-BFB = 117 Chloroform MW13 Tol-d8 = 116 Chloroform EPA-MW40A 4-BFB = 118 None EPA-MW40A Tol-d8 = 113 None EPA-MW53A 4-BFB = 118 Acetone EPA-MW53A Tol-d8 = 116 Acetone EPA-MW52A 4-BFB = 115 None EPA-MW52A Tol-d8 = 115 None EPA-MW61A 4-BFB = 116 None EPA-MW61A Tol-d8 = 116 None EPA-MW17C 4-BFB = 115 Chloroform EPA-MW17C Tol-d8 = 115 Chloroform EPA-MW18A 4-BFB = 117 Chloroform, PCE, TCE EPA-MW18A Tol-d8 = 115 Chloroform, PCE, TCE EA06 4-BFB = 116 Chloroform and TCE EA06 Tol-d8 = 116 Chloroform and TCE EPA-MW23A 4-BFB = 119 Chloroform and TCE EPA-MW23A Tol-d8 = 116 Chloroform and TCE DUP002 4-BFB = 118 TCE DUP002 Tol-d8 = 115 TCE

Some of these detections are already qualified, due to reporting limit (MDL/RL) considerations. Remaining detections are qualified due to the high surrogates.

9) Two sets of blind field duplicate samples were submitted with the samples under this

chain-of-custody. Sample DUP001-11192012 was submitted as a blind field duplicate of primary sample MW14. No VOCs were detected in either of the samples, and field duplicate precision is acceptable

Sample DUP002-11192012 was submitted as a blind field duplicate of primary

sample EPA-MW23A. TCE was detected in the primary and duplicate samples at concentrations of 170 ug/L and 160 ug/L, respectively. Precision between the duplicate TCE results is acceptable, with an RPD of 6.1 percent. Chloroform was detected in the primary sample at an estimated concentration, and was not detected in the duplicate sample. Chloroform results agree within a reporting limit increment. Field duplicate precision is determined to be acceptable.


5






DATA QUALIFIED -









Sample ID Qualified Perchlorate (ug/L) MW14 Perchlorate = 1.3 J DUP001 Perchlorate = 1.5 J EPA-MW40C Perchlorate = 0.97 J EPA-MW53A Perchlorate = 1.5 J


6

3) Results from two method blanks were provided in support of the groundwater sample analyses, with no perchlorate detected. Results from one equipment blank were also provided, with no perchlorate detected.

4) Results from continuing calibration analyses were not provided. 5-6) TestAmerica provided results from two sets of project specific MS and MSD

analyses (spikes on project samples MW28 and DUP001), and from one set of batch specific MS and MSD analyses, in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 107 to 110 percent, with a maximum RPD between MS and MSD recoveries of 2 percent.




sample MW14. Perchlorate was detected in the primary and duplicate samples at estimated concentrations of 1.3 ug/L and 1.5 ug/L, respectively. Precision between the duplicate perchlorate results is acceptable, as the results agree within a reporting limit increment.

TestAmerica provided results from two sets of batch specific laboratory duplicate sample analyses. Laboratory duplicate precision is acceptable, with a maximum RPD of 3 percent.



7




Geomatrix Consultants, Inc. (Geomatrix) collected 12 groundwater samples and four associated quality control samples on November 19, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


MW13-11192012 / Chloroform EPA-MW53A-11192012 / Acetone EPA-MW17C-11192012 / Chloroform EPA-MW18A-11192012 / PCE EPA-MW18A-11192012 / TCE EPA-MW23A-11192012 / Chloroform

J/Estimated



calibration curve may be limited. MW13-11192012 / Chloroform EPA-MW53A-11192012 / Acetone EPA-MW17C-11192012 / Chloroform EPA-MW18A-11192012 / Chloroform, PCE, TCE EA06-11192012 / Chloroform and TCE EPA-MW23A-11192012 / Chloroform and TCE DUP002-11192012 / TCE

J/Estimated

Surrogate recoveries are high. Associated sample detections may

also be biased high.

MW14-11192012 DUP001-11192012 EPA-MW40C-11192012 EPA-MW53A-11192012 / Perchlorate

J/Estimated




SIGNATURE:

DATE:

December 10, 2012


1



LABORATORY REPORT # PVK1450 DATED DECEMBER 5, 2012


TB001-11202012 PVK1450-01 Quality Control VOCs / Trip Blank LPW-894-11202012 PVK1450-02 Groundwater VOCs and Perchlorate EPA-MW22C-11202012 PVK1450-03 Groundwater VOCs and Perchlorate EPA-MW55A-11202012 PVK1450-04 Groundwater VOCs EPA-MW39C-11202012 PVK1450-05 Groundwater VOCs EPA-MW39A-11202012 PVK1450-06 Groundwater VOCs EPA-MW45A-11202012 PVK1450-07 Groundwater VOCs EPA-MW16C-11202012 PVK1450-08 Groundwater VOCs EPA-MW35A-11202012 PVK1450-09 Groundwater VOCs EA02-11202012 PVK1450-10 Groundwater VOCs and Perchlorate EA07-11202012 PVK1450-11 Groundwater VOCs and Perchlorate EPA-MW16A-11202012 PVK1450-12 Groundwater VOCs DUP001-11202012 PVK1450-13 Quality Control VOCs / Field Duplicate of primary sample

EPA-MW16A-11202012 EPA-MW62A-11202012 PVK1450-14 Groundwater VOCs and Perchlorate EB001-11202012 PVK1450-15 Quality Control VOCs and Perchlorate / Equipment Blank MW19-11212012 PVK1450-16 Groundwater VOCs EPA-MW6C-11212012 PVK1450-17 Groundwater VOCs and Perchlorate IRZ-MWC-11212012 PVK1450-18 Groundwater VOCs and Perchlorate MW09-11212012 PVK1450-19 Groundwater VOCs and Perchlorate EB001-11212012 PVK1450-20 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X Yes 4. Laboratory Control Sample (LCS) %R X X Yes 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on November 20 and 21, 2012. The samples were analyzed by December 3, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.

2) TCE was diluted by a factor of 5 times in sample EPA-MW62A. No other sample

dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).




3



EA02 Acetone = 7.2 J

EA07 Chloroform = 0.88 J EPA-MW16A Chloroform = 0.92 J DUP001 Chloroform = 0.70 J


EPA-MW6C Chloroform = 0.64 J 3) Results from three full suite method blanks were provided in association with the


Results from one trip blank were provided. Chloroform was detected in the trip blank at an estimated concentration of 0.84 ug/L. Results from two equipment blanks were provided. Chloroform was detected in equipment blank EB001-11202012 at an estimated concentration of 0.82 ug/L. . Chloroform was detected in equipment blank EB001-11212012 at an estimated concentration of 1.2 ug/L. Chloroform was detected in several samples at concentrations within 5 times those of the trip blank and the equipment blanks. Due to potential blank contamination bias, the following chloroform results are qualified as U/non-detect at the concentration reported.

Sample ID Qualified VOCs (ug/L) LPW-894 Chloroform = 3.0 U EPA-MW39C Chloroform = 0.34 U EPA-MW39A Chloroform = 0.72 U EPA-MW45A Chloroform = 1.6 U EPA-MW16C Chloroform = 0.51 U EPA-MW35A Chloroform = 0.53 U

EA02 Chloroform = 1.4 U EA07 Chloroform = 0.88 U

EPA-MW16A Chloroform = 0.92 U DUP001 Chloroform = 0.70 U

EPA-MW62A Chloroform = 0.68 U MW19 Chloroform = 1.3 U EPA-MW6C Chloroform = 0.64 U MW09 Chloroform = 1.1 U


4

4-5) TestAmerica provided results from three full sets of laboratory control sample (LCS)

and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. The LCS for PCE was low at 83 percent (lower control limit of 85 percent) in batch 12K1134. PCE was not detected in the associated samples. Due to potential low bias, the following samples are qualified as “UJ/Estimated and non-detect at the reporting limits stated,” for PCE.

LPW894-11202012 EPA-MW22C-11202012 EPA-MW55A-11202012 EPA-MW39C-11202012 EPA-MW39A-11202012 EPA-MW45A-11202012 EPA-MW16C-11202012 EPA-MW35A-11202012

Precision between LCS and LCSD recoveries for acetone was poor in the same batch, with an RPD of 27 percent (upper control limit of 25 percent). No bias to the acetone results is indicated. The o-xylene LCSD recovery was high at 118 percent in the spike from batch 12K1135. The trichlorofluoromethane LCSD recovery was high at 129 percent (upper control limit of 123 percent) in the spike from batch 12K0036. Precision for acetone was also poor in this batch, with an RPD of 53 percent. O-xylene and trichlorofluoromethane were not detected in any associated samples and no action is taken. No bias to the acetone sample results is indicated.

6-7) TestAmerica provided results from three sets of project specific MS and MSD

analyses (spikes on project samples EPA-MW22C, EA02, and EPA-MW6C) in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. For the project spike of sample EPA-MW22C, several spike recoveries were high, including carbon tetrachloride, chloroform, ethylbenzene, o-xylene, and trichlorofluoromethane. None of these VOCs were detected in the sample spiked, and no bias to the sample results is indicated. MS recoveries for the other project samples spiked were in control.


analyses. Surrogate recoveries ranged from 109 to 132 percent. Numerous 4-bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent upper project control limit. Several toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit. One dibromofluoromethane surrogate was high, exceeding 130 percent. A one percent leeway is provided for rounding considerations, as follows:


LPW-894 4-BFB = 129 Chloroform LPW-894 Tol-d8 = 112 Chloroform EPA-MW22C 4-BFB = 124 None EPA-MW22C Tol-d8 = 115 None EPA-MW55A 4-BFB = 122 None


5

EPA-MW55A Tol-d8 = 117 None EPA-MW39C 4-BFB = 131 Chloroform EPA-MW39C Tol-d8 = 112 Chloroform EPA-MW39A 4-BFB = 127 Chloroform EPA-MW39A Tol-d8 = 114 Chloroform EPA-MW45A 4-BFB = 130 Chloroform EPA-MW16C 4-BFB = 127 Chloroform EPA-MW16C Tol-d8 = 114 Chloroform EPA-MW35A 4-BFB = 125 Chloroform and TCE EPA-MW35A Tol-d8 = 114 Chloroform and TCE EA02 4-BFB = 127 Chloroform, Toluene, EA02 Tol-d8 = 114 TCE, and Acetone EA07 4-BFB = 116 Chloroform and TCE EA07 Tol-d8 = 112 Chloroform and TCE EPA-MW16A 4-BFB = 116 Chloroform and TCE EPA-MW16A Tol-d8 = 112 Chloroform and TCE DUP001 4-BFB = 116 Chloroform and TCE DUP001 Tol-d8 = 113 Chloroform and TCE EPA-MW62A DBFM= 132 None EPA-MW62A Tol-d8 = 114 None EPA-MW62A Tol-d8 = 115 Chloroform (rerun) EPA-MW62A 4-BFB = 115 TCE (rerun) EPA-MW62A Tol-d8 = 116 TCE (rerun) MW19 4-BFB = 115 Chloroform and TCE MW19 Tol-d8 = 113 Chloroform and TCE MW09 Tol-d8 = 115 Chloroform and TCE

Many of these detections are already qualified, due to reporting limit (MDL/RL) considerations. Remaining detections are qualified due to the high surrogates.


sample EPA-MW16A. TCE was detected in the primary and duplicate samples at concentrations of 130 ug/L, each. Precision between the duplicate TCE results is acceptable, with an RPD of 0 percent. Chloroform was detected in the primary and duplicate samples at estimated concentrations. Chloroform is qualified due to


6

blank contamination, for both samples, and the precision assessment is not applicable






DATA QUALIFIED -




#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab Only 9. Results Quantitation X X



2) Sample MW09 was diluted by a factor of 2 times to quantitate perchlorate. No

other sample dilutions were required to quantitate perchlorate. Reporting limits are determined to be acceptable, with the following consideration. Perchlorate was reported as concentration between the method detection limit (MDL) and the standard reporting limit in the following sample. Due to limited accuracy in this portion of the calibration curve, these perchlorate results are qualified as J/Estimated.

Sample ID Qualified Perchlorate (ug/L) LPW-894 Perchlorate = 1.6 J


7

3) Results from one method blank were provided in support of the groundwater sample analyses, with no perchlorate detected. Results from two equipment blanks were also provided, with no perchlorate detected.


analyses (spike on project sample EPA-MW22C) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 107 to 107 percent, with an RPD between MS and MSD recoveries of 2 percent.




TestAmerica provided results from one set of project specific laboratory duplicate sample analyses on sample LPW894. Laboratory duplicate precision is acceptable, with an RPD of 0.4 percent.



8




Geomatrix Consultants, Inc. (Geomatrix) collected 16 groundwater samples and four associated quality control samples on November 20 and 21, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EA02-11202012 / Acetone

J/Estimated

Acetone was reported at a concentration between the method detection limit and the reporting


LPW-894-11202012, EPA-MW39C-11202012, EPA-MW39A-11202012, EPA-MW45A-11202012, EPA-MW16C-11202012, EPA-MW35A-11202012, EA02-11202012, EA07-11202012, EPA-MW16A-11202012, DUP001-11202012, EPA-MW62A-11202012, MW19-11202012, EPA-MW6C-11212012, MW09-11212012 / Chloroform

U/non-detect

Chloroform was detected in the trip blank and the equipment blanks at

concentrations within five times the concentrations in the associated

groundwater samples. Chloroform detections may be the result of blank

contamination bias.

LPW894-11202012, EPA-MW22C-11202012, EPA-MW55A-11202012, EPA-MW39C-11202012, EPA-MW39A-11202012, EPA-MW45A-11202012 EPA-MW16C-11202012, EPA-MW35A-11202012 / PCE

UJ/Estimated


LCS recovery for PCE is low. PCE

was not detected in any of the associated samples. PCE sample

results may be biased low.

EPA-MW35A-11202012 / TCE EA02-11202012 / Toluene, TCE, and Acetone EA07-11202012 TCE EPA-MW16A-11202012 TCE DUP001-11202012 / TCE EPA-MW62A-11202012 / TCE MW19-11212012 / TCE MW09-11212012 / TCE

J/Estimated




9


Data Qualifier(s)


LPW-894-11202012 / Perchlorate

J/Estimated




SIGNATURE:

DATE:

December 10, 2012

PVK1630.doc Created on 12/11/2012 10:12:00 AM

1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected six groundwater samples and three associated quality control samples on November 26, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on November 27, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-11262012 PVK1630-01 Quality Control VOCs / Trip Blank MW26-11262012 PVK1630-02 Groundwater VOCs EPA-MW54A-11262012 PVK1630-03 Groundwater VOCs PSDW-11262012 PVK1630-04 Groundwater VOCs and Perchlorate APS-MW03-11262012 PVK1630-05 Groundwater VOCs and Perchlorate EPA-MW21A-11262012 PVK1630-06 Groundwater VOCs and Perchlorate DUP001-11262012 PVK1630-07 Quality Control VOCs and Perchlorate / Field duplicate of

primary sample EPA-MW21A-11262012 EPA-MW34A-11262012 PVK1630-08 Groundwater VOCs EB001-11262012 PVK1630-09 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X Yes 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on November 26, 2012. The samples were analyzed by December 2, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.



Sample ID Qualified VOCs (ug/L) MW26 Chloroform = 0.72 J EPA-MW54A Chloroform = 0.79 J


3

Sample ID Qualified VOCs (ug/L) APS-MW03 Chloroform = 0.72 J APS-MW03 TCE = 0.44 J EPA-MW21A Chloroform = 0.74 J EPA-MW21A TCE = 0.39 J DUP001 TCE = 0.41 J EPA-MW34A TCE = 0.26 J 3) Results from one full suite method blank were provided in association with the


One trip blank was analyzed. Chloroform was detected in the trip blank at an estimated concentration of 0.75 ug/L. Results from one equipment blank were provided. Chloroform was detected in the equipment blank at an estimated concentration of 0.60 ug/L. Chloroform was detected in several samples at concentrations within 5 times those of the trip blank and the equipment blank. Due to potential blank contamination bias, the following chloroform results are qualified as U/non-detect at the concentration reported.

Sample ID Qualified VOCs (ug/L) MW26 Chloroform = 0.72 U EPA-MW54A Chloroform = 0.79 U PSDW Chloroform = 1.0 U APS-MW03 Chloroform = 0.72 U EPA-MW21A Chloroform = 0.74 U EPA-MW34A Chloroform = 3.1 U 4-5) TestAmerica provided results from one full set of laboratory control sample (LCS)



(spike on project sample MW26). Precision and accuracy, as demonstrated by these analyses is acceptable.


analyses. Surrogate recoveries ranged from 107 to 128 percent. Some 4-bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent


4

upper project control limit. Some toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit, as follows:


MW26 4-BFB = 121 Chloroform EPA-MW54A Tol-d8 = 113 Chloroform APS-MW03 4-BFB = 117 Chloroform and TCE APS-MW03 Tol-d8 = 112 Chloroform and TCE

. EPA-MW21A 4-BFB = 120 Chloroform and TCE EPA-MW21A Tol-d8 = 118 Chloroform and TCE

DUP001 4-BFB = 120 TCE

EPA-MW34A Tol-d8 = 116 Chloroform and TCE

All chloroform results are already qualified due to blank contamination, and no

further qualification is required. These TCE results may be biased high, and are qualified as J/Estimated due to the high surrogate recoveries.


sample EPA-MW21A. TCE was detected in the primary and duplicate samples at estimated concentrations of 0.39 ug/L and 0.41 ug/L, respectively. TCE precision is acceptable with an RPD of 5.0 percent. Chloroform was detected in the primary and duplicate samples at estimated concentrations of 0.72 ug/L and 0.74 ug/L, respectively. Chloroform precision not calculated, as all chloroform results are qualified due to blank contamination issues.

. 10) No anomalies were noted with respect to results quantitation or reporting.


5





DATA QUALIFIED -







2) Samples EPA-MW21A and DUP001 were each diluted by a factor of two times to

quantitate perchlorate. No other sample dilutions were required to quantitate perchlorate. Reporting limits are determined to be acceptable, with the following considerations. One perchlorate result was reported at a concentration between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, this perchlorate result is qualified as J/Estimated. The following result is qualified (pending the results of the blank evaluation).

Sample ID Qualified Perchlorate (ug/L) APS-MW03 Perchlorate = 1.5 J 3) Results from one method blank were provided in support of the groundwater sample




6


analyses (spikes on project samples EPA-MW8C and MW21) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 91 and 97 percent, with a maximum RPD between MS and MSD recoveries of 2 percent.


support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries ranged from 101 to 102 percent. The maximum RPD between LCS and LCSD results was acceptable at 0.8 percent.

8) Sample DUP001 was submitted as a blind field duplicate of primary sample EPA-

MW21A. Perchlorate was detected in the primary and duplicate samples at concentrations of 5.3 ug/L and 5.6 ug/L, respectively. Perchlorate precision is acceptable with an RPD of 5.5 percent.

TestAmerica provided results from one set of project specific laboratory duplicate sample analyses performed on project sample APS-MW03. Laboratory duplicate precision is acceptable, with an RPD of 1 percent between laboratory duplicate analyses.



7




Geomatrix Consultants, Inc. (Geomatrix) collected six groundwater samples and three associated quality control samples on November 26, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


APS-MW03-11262012 / TCE EPA-MW21A-11262012 / TCE DUP001-11262012 / TCE

J/Estimated

TCE was reported at concentrations between the method detection limit and the reporting limit. Accuracy in this portion of the calibration curve

may be limited.

MW26-11262012, EPA-MW54A-11262012, PSDW-11262012, APS-MW03-11262012, EPA-MW21A-11262012, and EPA-MW34A / Chloroform

U/non-detect at the concentration

reported

Chloroform was detected in the trip blank and the equipment blank at

concentrations within five times the concentrations in the associated

groundwater samples. Chloroform detections may be the result of blank

contamination bias. APS-MW03-11262012 / TCE EPA-MW21A-11262012 / TCE DUP001-11262012 / TCE EPA-MW34A-11262012 / TCE

J/Estimated

Surrogate recoveries are high.

Associated sample detections may also be biased high.

APS-MW03-11262012 / Perchlorate

J/Estimated




SIGNATURE:

DATE:

December 11, 2012


1





TB001-11272012 PVK1721-01 Quality Control VOCs / Trip Blank MW18-11272012 PVK1721-02 Groundwater VOCs EB001-11272012 PVK1721-03 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW14C-11272012 PVK1721-04 Groundwater VOCs EPA-MW31A-11272012 PVK1721-05 Groundwater VOCs MW15-11272012 PVK1721-06 Groundwater VOCs MW16-11272012 PVK1721-07 Groundwater VOCs EPA-MW25A-11272012 PVK1721-08 Groundwater VOCs EPA-MW42A-11272012 PVK1721-09 Groundwater VOCs and Perchlorate EB002-11272012 PVK1721-10 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X Yes 4. Laboratory Control Sample (LCS) %R X X No 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X





acceptable, with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).

Sample ID Qualified VOCs (ug/L) EPA-MW14C Chloroform = 0.68 J EPA-MW31A PCE = 0.84 J EPA-MW31A TCE = 0.78 J


3

Sample ID Qualified VOCs (ug/L) EPA-MW15 Chloroform = 0.60 J EPA-MW16 Chloroform = 0.45 J EPA-MW25A Chloroform = 0.98 J 3) Results from three full suite method blanks were provided in association with the


Results from one trip blank were provided. Chloroform was detected in the trip blank at an estimated concentration of 0.95 ug/L. Results from two equipment blanks were provided. Chloroform was detected in equipment blank EB001 at a concentration of 1.2 ug/L. Chloroform was detected in equipment blank EB002 at an estimated concentration of 0.74 ug/L. Acetone was also detected in equipment blank EB002 at an estimated concentration of 5.4 ug/L. Acetone was not detected in any of the associated samples, and no action is required. Chloroform was detected in several samples at concentrations within 5 times those of the trip blank and the equipment blanks. Due to potential blank contamination bias, the following chloroform results are qualified as U/non-detect at the concentration reported.

Sample ID Qualified VOCs (ug/L) MW18 Chloroform = 1.0 U EPA-MW14C Chloroform = 0.68 U EPA-MW31A Chloroform = 5.4 U EPA-MW15 Chloroform = 0.60 U EPA-MW16 Chloroform = 0.45 U EPA-MW25A Chloroform = 0.98 U EPA-MW42A Chloroform = 1.0 U


and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. The LCSD recoveries for carbon tetrachloride and trichlorofluoromethane were high at 129 and 126 percent, respectively, (upper control limits of 123 percent, each) in batch 12L0017. Carbon tetrachloride and trichlorofluoromethane were not detected in the associated samples, and no action is required. The trichlorofluoromethane LCS recovery was high at 129 percent in batch 12L0036. The acetone recovery was high at 155 percent (upper control limit of 153 percent) in the same batch. Precision was also poor for acetone. This batch is associated with the analysis of equipment blank EB002 only, and no action is taken.


4

6-7) TestAmerica provided results from one set of project specific MS and MSD analyses (spike on project sample EPA-MW14C), and from two sets of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.

8) Three surrogates were spiked into each water sample in support of the VOC analyses.

Surrogate recoveries ranged from 110 to 128 percent. Numerous 4-bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent upper project control limit. Several toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit, as follows:


MW18 4-BFB = 118 Chloroform and TCE MW18 Tol-d8 = 118 Chloroform and TCE EPA-MW14C 4-BFB = 128 Chloroform EPA-MW14C Tol-d8 = 118 Chloroform EPA-MW31A 4-BFB = 116 Chloroform, TCE, PCE EPA-MW31A Tol-d8 = 116 Chloroform, TCE, PCE MW15 4-BFB = 117 Chloroform and TCE MW16 4-BFB = 116 Chloroform, TCE MW16 Tol-d8 = 112 Chloroform, TCE EPA-MW25A 4-BFB = 116 Chloroform, TCE EPA-MW42A Tol-d8 = 120 Chloroform, TCE

Many of these detections are already qualified, due to reporting limit (MDL/RL) considerations and blank contamination for chloroform. Remaining detections are qualified due to the high surrogates. The U/Non-detect qualifier for chloroform supersedes any qualifiers for surrogate recoveries.


custody .



5





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab Only 9. Results Quantitation X X

%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The groundwater samples were received by TestAmerica on November 28 2012. The

water samples were received chilled at a temperature of 0.9 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by November 29, 2012, within prescribed holding times.

2) No sample dilutions were required to quantitate perchlorate. 3) Results from one method blank were provided in support of the groundwater sample


4) Results from continuing calibration analyses were not provided. 5-6) TestAmerica provided results from one set of project specific MS and MSD analyses

(spike on project sample EPA-MW42A) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 103 to 104 percent, with an RPD between MS and MSD recoveries of 1 percent.

7) TestAmerica provided results from one set of LCS and LCSD analyses in support of the

perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is


6

acceptable. Aqueous LCS and LCSD recoveries ranged from 101 to 103 percent, with an RPD of 2 percent between LCS duplicate results.

8) Field duplicate samples were not submitted with the samples sunder this chain-of-

custody in support of the perchlorate analyses.

TestAmerica provided results from one set of project specific laboratory duplicate sample analyses performed on sample EB002. Laboratory duplicate precision is acceptable, with no perchlorate detected in either of the samples.



7




Geomatrix Consultants, Inc. (Geomatrix) collected seven groundwater samples and three associated quality control samples on November 27, 2012.. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW31A-11272012 / PCE EPA-MW31A-11272012 / TCE

J/Estimated



calibration curve may be limited. MW18-11272012, EPA-MW14C-11272012 , EPA-MW31A-11272012, EPA-MW15-11272012, EPA-MW16-11272012, EPA-MW25A-11272012, and EPA-MW42A-11272012 / Chloroform

`U/Non-detect at the concentration

reported

Chloroform was detected in the

associated trip blank and equipment blanks at concentrations within 5 times those of the groundwater

samples. Chloroform detections may be the results of blank

contamination bias. MW18-11272012 / TCE EPA-MW31A-11272012 / PCE and TCE MW15-11272012 / TCE MW16-11272012 / TCE EPA-MW25A-11272012 / TCE EPA-MW42A-11272012 / TCE

J/Estimated



SIGNATURE:

DATE:

December 13, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected two groundwater samples (blind performance evaluation samples) and one associated trip blank on November 27, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on November 28, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-11272012 PVK1726-01 Quality Control VOCs / Trip Blank MW030-11272012 PVK1726-02 Groundwater VOCs and Perchlorate MW031-11272012 PVK1726-03 Groundwater VOCs and Perchlorate Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -



1. Holding times X X 2. Detection limits X X Yes – See Note

#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X Yes 5. LCS Duplicate %R and (RPD) X X Yes 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X


COMMENTS: Performance was acceptable, with the following exceptions and/or notes. 1) The water samples were received chilled at an acceptable temperature of 0.



are determined to be acceptable, with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).

Sample ID Qualified VOCs (ug/L) MW030 Chloroform = 0.62 J MW030 Acetone = 4.5 J MW031 Chloroform = 0.56 J MW031 Acetone = 5.0 J


3

3) Results from one full suite method blank were provided in association with the

groundwater sample analyses. No VOCs were detected in the method blank. Results from one trip blank were provided. No VOCs were detected in the trip blank. Equipment blanks were not collected with the samples under this chain-of-custody.

4-5) TestAmerica provided results from one full set of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses. Precision and accuracy, as demonstrated by these analyses, is acceptable, with the following exceptions. The LCS recovery for trichlorofluoromethane was high at 129 percent high (upper control limit of 123 percent). Trichlorofluoromethane was not detected in any of the associated samples, and no action is required. The acetone LCSD recovery was high at 155 percent (upper control limit of 153 percent), with resulting poor precision. Acetone was detected in both associated groundwater samples. Due to potential high bias, the acetone detections for the two performance evaluation samples are qualified as J/Estimated.

6-7) TestAmerica provided results from one set of batch specific MS and MSD analyses,

in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses, is acceptable. MS and MSD recoveries ranged from 72 to 121 percent. The maximum RPD between MS and MSD recoveries was acceptable at 4 percent.


analyses. Surrogate recoveries ranged from 112 to 128 percent. Surrogate recoveries were high, relative to project specific control levels, in both PE samples. Note that both PE samples were re-analyzed for trichlorofluoromethane due to initial LCS failures.

Sample ID High Surrogate Control limits MW030 Toluene=d8 = 112 88.4-111 MW031 Toluene=d8 = 119 88.4-111 Previous validation efforts have allowed for one surrogate to be out on control by 1

percent or less to account for rounding. Therefore, detections from the analysis of sample MW030 are not qualified. All VOC detections for sample MW031 (acetone, chloroform, PCE, and TCE) are qualified as J/Estimated, due to potential high bias, as listed below.




4





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab Only 9. Results Quantitation X X

%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The groundwater sample was received by TestAmerica on November 28, 2011.

The water samples were received chilled at a temperature of 0.9 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by December 3, 2012, within prescribed holding times.

2) Sample MW031 was diluted by a factor of 5 times to quantitate perchlorate. No

other sample dilutions were required to quantitate perchlorate. Reporting limits are determined to be acceptable.

3) Results from two method blanks were provided in support of the water sample

analyses, with no perchlorate detected 4) Results from continuing calibration analyses were not provided. 5-6) TestAmerica provided results from two set of batch specific MS and MSD analyses

in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 100 to 104 percent, with a maximum RPD between MS and MSD recoveries of 1 percent.

7) TestAmerica provided results from two sets of LCS/LCS duplicate analyses in support

of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries ranged from 93 to 103 percent. The


5

maximum RPD between perchlorate LCS duplicate recoveries was acceptable at 5 percent.

8) Field duplicate samples were not collected in support of perchlorate with the samples

under this chain-of-custody.

TestAmerica provided results from two sets of laboratory duplicate sample analyses performed on batch samples. Laboratory duplicate precision was acceptable, with a maximum RPD of 6 percent between duplicate sample results.



6




Geomatrix Consultants, Inc. (Geomatrix) collected two groundwater samples (blind performance evaluation samples) and one associated trip blank on November 27, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


MW030-11272012 / Chloroform MW030-11272012 / Acetone MW031-11272012 / Chloroform MW031-11272012 / Acetone

J/Estimated




may be limited. MW030-11272012 / Acetone MW031-11272012 / Acetone

J/Estimated

Associated LCS recoveries were

high. Sample results may be biased high.

MW031-11272012 / Acetone, Chloroform, PCE, and TCE

J/Estimated

Associated surrogate recoveries were high. Sample results may

be biased high.

SIGNATURE:

DATE:

December 14, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 14 groundwater samples and five associated quality control samples on November 28, 29, and 30, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on November 30, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-11282012 PVK1911-01 Quality Control VOCs / Trip Blank EPA-MW59A-11282012 PVK1911-02 Groundwater` VOCs and Perchlorate EPA-MW60A-11282012 PVK1911-03 Groundwater` VOCs and Perchlorate DUP001-11282012 PVK1911-04 Quality Control VOCs and Perchlorate / Field duplicate of

primary sample EPA-MW60A-11282012 IR26A-11282012 PVK1911-05 Groundwater VOCs and Perchlorate EPA-MW50A-11282012 PVK1911-06 Groundwater` VOCs EPA-MW30A-11282012 PVK1911-07 Groundwater` VOCs EPA-MW49C-11282012 PVK1911-08 Groundwater` VOCs IR34B-11282012 PVK1911-09 Groundwater VOCs and Perchlorate GCLake-11282012 PVK1911-10 Groundwater VOCs and Perchlorate EB001-11282012 PVK1911-11 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW43A-11292012 PVK1911-12 Groundwater VOCs EPA-MW26A-11292012 PVK1911-13 Groundwater` VOCs MW25-11292012 PVK1911-14 Groundwater VOCs IR3B-11292012 PVK1911-15 Groundwater VOCs and Perchlorate EPA-MW38A-11292012 PVK1911-16 Groundwater VOCs EB001-11292012 PVK1911-17 Quality Control VOCs and Perchlorate / Equipment Blank MW12-11302012 PVK1911-18 Groundwater VOCs and Perchlorate DUP001-11302012 PVK1911-19 Quality Control VOCs and Perchlorate / Field duplicate of

primary groundwater sample MW12-11302012

Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X No 4. Laboratory Control Sample (LCS) %R X X No 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on November 28, 29, and 30, 2012. The samples were analyzed by December 7, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.

2) Samples MW12 and DUP001 were each diluted by a factor of 10 times for TCE

only. No other sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).


3

Sample ID Qualified VOCs (ug/L) EPA-MW59A Chloroform = 0.23 J EPA-MW60A Chloroform = 0.56 J EPA-MW60A TCE = 0.21 J DUP001-11282012 Chloroform = 0.66 J IR26A Chloroform = 0.74 J IR26A TCE = 0.25 J

EPA-MW50A PCE = 0.72 J

EPA-MW30A Chloroform = 0.56 J EPA-MW49C Chloroform = 0.32 J GCLake Chloroform = 0.40 J EPA-MW26A Chloroform = 0.64 J MW25 Chloroform = 0.60 J IR3B Chloroform = 0.43 J IR3B TCE = 0.83 J EPA-MW38A Chloroform = 0.61 J

MW12 Chloroform = 0.79 J MW12 PCE = 0.91 J

DUP001-11302012 Chloroform = 0.88 J 3) Results from three full suite method blanks were provided in association with the

groundwater sample analyses. No VOCs were detected in the method blanks.

One trip blank was analyzed. Acetone was detected in the trip blank at an estimated concentration of 3.9 ug/L. Acetone was not detected in any of the associated samples, and no action is required. Results from two equipment blanks were provided. Chloroform was detected in one of the equipment blanks, as follows.

Blank ID VOCs Detected (ug/L) EB001-11292012 Chloroform = 0.38 J


4

Chloroform was detected in the following samples associated samples (collected on November 29, 2012) at concentrations within five times that of the equipment blank. Due to potential blank contamination bias, chloroform results for the following samples are qualified as U/non-detect at the concentration reported.

Sample ID Qualified VOCs (ug/L) EPA-MW26A Chloroform = 0.64 U MW25 Chloroform = 0.60 U

IR3B Chloroform = 0.43 U EPA-MW38A Chloroform = 0.61 U


and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. An o-xylene LCS recovery was high in one spike. O-Xylene was not detected in the associated samples, and no action is required. Carbon tetrachloride LCS recoveries were high in one spike set. Carbon tetrachloride was not detected in the associated samples, and no action is required. Acetone and 2-butanone LCS recoveries were high in the same spike. Precision was also poor for these two VOCs. Acetone and 2-butanone were not detected in the associated samples, and not action is taken. A 1,2-dichloropropane LCS recovery was high in one LCS. 1,2-Dichloropropane was not detected in the associated samples, and no action is required.


analyses (spikes on project samples EPA-MW59A and EPA-MW43A), and from one set of batch specific MS and MSD analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. The ethylbenzene spike recoveries were high in one project spike, and in the batch spike. Ethylbenzene was not detected in any associated samples, and no action is required.


analyses. Surrogate recoveries ranged from 100 to 136 percent. Numerous 4-bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent upper project control limit. Several toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit. Some dibromofluoromethane (DBFM) surrogate recoveries were high, exceeding the 130 upper control limit, as follows:


EPA-MW60A DBFM = 132 Chloroform and TCE EPA-MW60A Tol-d8 = 114 Chloroform and TCE EPA-MW60A 4-BFB = 118 Chloroform and TCE DUP001-11282012 DBFM = 133 Chloroform DUP001-11282012 Tol-d8 = 116 Chloroform DUP001-11282012 4-BFB = 117 Chloroform


5

Sample ID High Surr Rec (%) Data qualified ? IR26A DBFM = 135 Chloroform and TCE IR26A Tol-d8 = 115 Chloroform and TCE IR26A 4-BFB = 115 Chloroform and TCE EPA-MW50A DBFM = 132 PCE EPA-MW50A Tol-d8 = 114 PCE EPA-MW50A 4-BFB = 117 PCE EPA-MW30A 4-BFB = 122 Chloroform and TCE EPA-MW30A Tol-d8 = 113 Chloroform and TCE EPA-MW49C DBFM = 132 Chloroform EPA-MW49C Tol-d8 = 115 Chloroform IR34B DBFM = 134 None IR34B Tol-d8 = 114 None IR34B 4-BFB = 115 None GCLake DBFM = 133 Chloroform GCLake Tol-d8 = 114 Chloroform GCLake 4-BFB = 118 Chloroform EPA-MW43A 4-BFB = 135 None EPA-MW43A Tol-d8 = 120 None EPA-MW26A 4-BFB = 136 Chloroform EPA-MW26A Tol-d8 = 114 Chloroform MW25 4-BFB = 131 Chloroform IR3B 4-BFB = 130 Chloroform and TCE IR3B Tol-d8 = 113 Chloroform and TCE EPA-MW38A 4-BFB = 130 Chloroform and TCE EPA-MW38A Tol-d8 = 112 Chloroform and TCE MW12 4-BFB = 129 Chloroform and PCE MW12 Tol-d8 = 114 Chloroform and PCE

Most of these detections are already qualified, due to reporting limit (MDL/RL) considerations. Remaining detections are qualified due to the high surrogates. For chloroform, the final qualifier for results impacted by blank contamination is U/Non-detect.

. 9) Two sets of field duplicate samples were collected with the sample under this chain-

of-custody. Sample DUP001-11292012 was submitted as a blind field duplicate of primary sample EPA-MW60A. TCE and chloroform were detected in the primary and duplicate samples at estimated concentrations. Chloroform was detected in the


6

duplicate sample at an estimated concentration. Chloroform and TCE precision is acceptable, as all results agree within reporting limit increments.

Sample DUP001-11302012 was submitted as a blind field duplicate of primary sample MW12. TCE was detected in the primary and duplicate samples at concentrations of 1,000 ug/L, each. TCE precision is acceptable with an RPD of 0 percent. PCE was detected in the primary and duplicate samples at concentrations of 0.91 ug/L and 1.1 ug/L, respectively. PCE precision is acceptable, with an RPD of 19 percent. 1,1-DCE was detected in the duplicate sample at 1.1 ug/L and was not detected in the primary sample at <1 ug/L. 1,1-DCE precision is acceptable, with results in agreement within a reporting limit increment. Chloroform was detected in both samples at estimated concentrations. Chloroform precision is acceptable, as both results agree within a reporting limit increment.

. 10) No anomalies were noted with respect to results quantitation or reporting.





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X Yes – See Note

#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X Yes 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X 9. Results Quantitation X X


The water samples were received chilled at a temperature of 2.0 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by December 3, 2012, within prescribed holding times.


7

2) Reporting limits are determined to be acceptable, with the following

considerations. Perchlorate was reported at concentration between the method detection limit (MDL) and the reporting limit in the following samples. Due to limited accuracy in this portion of the calibration range, these perchlorate results are qualified as J/Estimated. The following result is qualified (pending the results of the blank evaluation).

Sample ID Qualified Perchlorate (ug/L) EPA-MW59A Perchlorate = 1.4 J 3) Results from one method blank were provided in support of the groundwater sample

analyses, with no perchlorate detected. Results from two equipment blanks were also provided, with no perchlorate detected. Perchlorate was detected on the equipment blank collected on November 29, 2012 at an estimated concentration of 0.60 ug/L. Perchlorate was detected in the following associated samples (collected on November 29, 2012) at concentrations within 5 times that of the blank. These perchlorate results are qualified as U/non-detect at the concentration reported due to potential blank contamination bias.

Sample ID Qualified Perchlorate (ug/L) IR3B Perchlorate = 2.8 U 4) Results from continuing calibration analyses were not provided. 5-6) TestAmerica provided results from one set of project specific MS and MSD

analyses (spike on project sample EPA-MW59A) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were 100 and 101 percent, with an RPD between MS and MSD recoveries of 1 percent.




EPA-MW60A. Perchlorate was detected in the primary and duplicate samples at concentrations of 3.5 ug/L and 3.3 ug/L, respectively. Perchlorate precision is acceptable, with an RPD between field duplicate results of 5.9 percent.

TestAmerica provided results from one set of project specific laboratory duplicate sample analyses on sample IR34B. Laboratory duplicate precision is acceptable, with an RPD of 6 percent between laboratory duplicate analyses.



8




Geomatrix Consultants, Inc. (Geomatrix) collected 14 groundwater samples and five associated quality control samples on November 28, 29, and 30, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the table on the following page. Validation Summary Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW59A-11282012 / Chloroform EPA-MW60A-11282012 / Chloroform and TCE DUP001-11282012 / Chloroform IR26A-11282012 / Chloroform and TCE EPA-MW50A-11282012 / PCE EPA-MW30A-11282012 / Chloroform EPA-MW49C-11282012 / Chloroform GCLake-11282012 / Chloroform IR3B-11292012 / TCE MW12-11302012 / Chloroform and PCE DUP001-11302012 / Chloroform

J/Estimated




EPA-MW26A-11292012 / Chloroform MW25-11292012 / Chloroform IR3B-11292012 / Chloroform EPA-MW38A-11292012 / Chloroform


reported

Chloroform was detected in the associated equipment blank at

concentrations within 5 times those of the samples. Chloroform


EPA-MW60A-11282012 / Chloroform and TCE DUP001-11282012 / Chloroform IR26A-11282012 / Chloroform and TCE EPA-MW50A-11282012 / PCE EPA-MW30A-11282012 / Chloroform and TCE EPA-MW49C-11282012 / Chloroform GCLake-11282012 / Chloroform IR3B-11292012 / TCE EPA-MW38A-11292012 / TCE MW12-11302012 / Chloroform and PCE

J/Estimated

Associated surrogate recoveries are high. Sample results may be biased

high.


9


Data Qualifier(s)


EPA-MW59A-11282012 / Perchlorate

J/Estimated




IR3B-11292012 / Perchlorate


reported


concentration within 5 times those of the samples. Perchlorate detection

may be the result of blank contamination bias.

SIGNATURE:

DATE:

December 18, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected three groundwater samples on November 29, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on November 30, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

IR27A-180-11292012 PVK1912-01 Groundwater VOCs / Passive Diffusion Bag Samples IR27C-170-11292012 PVK1912-02 Groundwater VOCs / Passive Diffusion Bag Samples IR27C-258-11292012 PVK1912-03 Groundwater VOCs / Passive Diffusion Bag Samples Samples were submitted for analysis of organic compounds, as listed below. Analyses for ketone class VOCs (acetone and 2-butanone) were not performed, as these VOCs do not diffuse well through the passive diffusion bag. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method

8260B Quality Control for the water samples is evaluated in the following checklist tables and comments. A summary of data quality for the samples analyzed is provided in the final page of this validation report.


2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X No 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X


COMMENTS: Performance was acceptable, with the following exceptions and/or notes. 1) The groundwater samples were received chilled at an acceptable temperature of

2.0 degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on November 29, 2012. The samples were analyzed by December 6, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.



Sample ID Qualified VOCs (ug/L) IR27A-180 PCE = 0.52 J

IR27C-170 Chloroform = 0.38 J IR27C-258 Chloroform = 0.34 J


3

3) Results from two full suite method blanks were provided in association with the groundwater sample analyses. No VOCs were detected in the method blank.

4-5) TestAmerica provided results from two full sets of laboratory control sample (LCS)

and LCS duplicate (LCSD) analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. For batch 12L0076, the LCS and LCSD recoveries for carbon tetrachloride were high at 132 and 129 percent (upper control limit of 123 percent). No action is required, as carbon tetrachloride was not detected in the associated samples.

For batch 12L0232, the LCSD recovery for 1,2-dichloropropane was high at 117 percent (upper control limit of 115 percent). No action is required, as 1,2-dichloropropane was not detected in the associated samples.

6-7) TestAmerica provided results from two sets of batch specific MS and MSD analyses

in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. MS and MSD recoveries were high for ethylbenzene and 1,2-dichloropropane. These VOCs were not detected in the associated samples, and no action is required.


analyses. Surrogate recoveries ranged from 104 to 130 percent. Some 4-bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent upper project control limit. Some toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit, as follows:


IR27A-180 4-BFB = 130 Chloroform and PCE IR27A-180 Tol-d8 = 117 Chloroform and PCE IR27C-170 4-BFB = 129 Chloroform and TCE IR27C-170 Tol-d8 = 114 Chloroform and TCE

. IR27C-258 4-BFB = 130 Chloroform and TCE IR27C-258 Tol-d8 = 112 Chloroform and TCE




4




Geomatrix Consultants, Inc. (Geomatrix) collected three groundwater samples on November 29, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


IR27A-180-11292012 / PCE IR27C-170-11292012 / Chloroform IR27C-258-11292012 / Chloroform

J/Estimated




IR27A-180-11292012 / Chloroform and PCE IR27C-170-11292012 / Chloroform and TCE IR27C-258-11292012 / Chloroform and TCE

J/Estimated

Associated surrogate recoveries

exceed project control limits. Sample results may be biased high.

SIGNATURE:

DATE:

December 18, 2012

C24140.doc Created on 10/26/2012 10:43:00 AM

1



LABORATORY REPORT # C24140 DATED OCTOBER 23, 2012

INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 10 groundwater samples and four associated quality control samples on October 9 and 10, 2012. The samples were shipped to Accutest Laboratory, located in San Jose, California on October 10, 2012, and arrived at the laboratory on the following day. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-10092012 C24140-01 Quality Control VOCs / Trip Blank EPA-MW15C-10092012 C24140-02 Groundwater VOCs EPA-MW57A-10092012 C24140-03 Groundwater VOCs and Perchlorate MW21-10092012 C24140-04 Groundwater VOCs EB001-10092012 C24140-05 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW1A-10102012 C24140-06 Groundwater VOCs and Perchlorate MW27-10102012 C24140-07 Groundwater VOCs and Perchlorate EPA-MW1C-10102012 C24140-08 Groundwater VOCs EPA-MW5C-10102012 C24140-09 Groundwater VOCs and Perchlorate EPA-MW56A-10102012 C24140-10 Groundwater VOCs EPA-MW48A-10102012 C24140-11 Groundwater VOCs EPA-MW3C-10102012 C24140-12 Groundwater VOCs and Perchlorate DUP001-10102012 C24140-13 Quality Control VOCs and Perchlorate / Field duplicate of




2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on October 9 and 10, 2012. It was noted that sample EPA-MW48A was not preserved to pH <2. No action is taken, as the sample was analyzed within 6 days after sample collection, and the sample bottle was acidified prior to collection. The samples were analyzed by October 17, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.

2) Sample EPA-MW48A was diluted by a factor of 5 times for all VOCs. Samples

EPA-MW3C and DUP001 were diluted by a factor of 20 times for all VOCs. No other sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).


3

Sample ID Qualified VOCs (ug/L) EPA-MW15C Acetone= 4.2 J

3) Results from four full suite method blanks were provided in association with the groundwater sample analyses. No VOCs were detected in the method blanks. Results from one trip blank were provided. No VOCs were detected in the trip blank. Results from two equipment blanks were provided; one for each day of sampling. Acetone was detected in the equipment blanks at estimated concentrations, as follows:

Sample ID Detected VOCs (ug/L) EB001-10092012 Acetone = 7.1 J EB001-10102012 Acetone = 4.7 J

Acetone was detected in sample EPA-MW15C at a concentration less than

those detected in the equipment blanks. Due to potential blank contamination bias, this acetone result is qualified as U/non-detect at the concentration reported.

4-5) Accutest provided results from four full sets of laboratory control sample (LCS) and

LCS duplicate (LCSD) analyses (identified as blank spike analyses) in support of the ground. Precision and accuracy, as demonstrated by these analyses is acceptable. All LCS analyses were well within prescribed control limits (60 to 130 percent). Precision between LCS and LCSD recoveries was within prescribed control limits.


(spike on project sample EPA-MW15C), and from three sets of batch specific MS and MSD analyses. Precision and accuracy, as demonstrated by these analyses, are acceptable.


analyses. Surrogate recoveries were acceptable, ranging from 90 to 101 percent. 9) Sample DUP001 was submitted as a blind field duplicate of primary sample EPA-

MW3C. TCE was detected in the primary and duplicate samples at concentrations of 849 ug/L and 843 ug/L, respectively. Precision between the TCE detections is acceptable, with an RPD of 0.7 percent between duplicate sample results.



4





DATA QUALIFIED -





%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The groundwater samples were received by Accutest on October 11, 2012. The


2) Some groundwater samples were reported from dilutions, as follows:

Sample ID Perchlorate dilution EPA-MW5C 2 times EPA-MW3C 2 times DUP001 2 times

Reporting limits are determined to be acceptable, with the following considerations. Some perchlorate results were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these perchlorate results are qualified as J/Estimated, as follows (pending results of the blank evaluation):

Sample ID Qualified Results(ug/L)

EPA-MW57A Perchlorate = 1.9 J


5


4) Results from continuing calibration analyses were not evaluated. 5-6) Accutest provided results from one set of project specific MS and MSD analyses

(spike on project sample EPA-MW57A) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 86.0 to 87.2 percent, with an RPD between MS and MSD recoveries of 1.3 percent.


duplicate (LCSD) analyses (identified as blank spike analyses) in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries were each 98.8 percent. The RPD between the LCS and LCSD results was acceptable at 0 percent.


EPA-MW3C. Perchlorate was detected in the primary and duplicate samples at concentrations of 21.2 ug/L and 21.4 ug/L, respectively. Precision between the perchlorate detections is acceptable, with an RPD between duplicate perchlorate results of 0.9 percent.



6



LABORATORY REPORT # C24140 DATED OCTOBER 23, 2012


Data Qualifier(s)


EPA-MW15C-10092012 / Acetone


reported.


associated equipment blanks at concentrations greater than that in the

groundwater sample. Acetone detection may be the result of blank

contamination bias.


J/Estimated




SIGNATURE:

DATE:

October 26, 2012


1



LABORATORY REPORT # L600820 DATED OCTOBER 19, 2012

INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 12 groundwater samples and four associated quality control samples on October 10 and 11, 2012. The samples were shipped via overnight courier to ESC Laboratory, located in Mt. Juliet, Tennessee, on October 12, 2012. Samples arrived at the laboratory on the following day. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-10102012 L600820-01 Quality Control VOCs / Trip Blank EPA-MW6A-10102012 L600820-02 Groundwater VOCs EPA-MW12A-10102012 L600820-03 Groundwater VOCs and Perchlorate EPA-MW12C-10102012 L600820-04 Groundwater VOCs and Perchlorate EB002-10102012 L600820-05 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW13C-10112012 L600820-06 Groundwater VOCs and Perchlorate EPA-MW51A-10112012 L600820-07 Groundwater VOCs and Perchlorate EPA-MW26C-10112012 L600820-08 Groundwater VOCs and Perchlorate OWB-10112012 L600820-09 Groundwater VOCs MW29-10112012 L600820-10 Groundwater VOCs MW20-10112012 L600820-11 Groundwater VOCs EPA-MW47C-10112012 L600820-12 Groundwater VOCs EPA-MW47A-10112012 L600820-13 Groundwater VOCs and Perchlorate DUP001-10112012 L600820-14 Quality Control VOCs and Perchlorate/ Field Duplicate of

primary sample EPA-MW47A-10112012 EPA-MW13A-10112012 L600820-15 Groundwater VOCs and Perchlorate EB001-10112012 L600820-16 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X Yes 4. Laboratory Control Sample (LCS) %R X X No 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X




2) Samples MW-20 and MW13A were diluted by factors of 5 and 20 times,

respectively, for TCE only. Samples EPA-MW47C, EPA-MW47A, and DUP001 were each diluted by 5 times for all VOCs. No other sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).


3

Sample ID Qualified VOCs (ug/L) EPA-MW6A Acetone = 6.2 J EPA-MW12A Chloroform = 0.80 J EPA-MW13A Carbon tetrachloride = 0.94 J EPA-MW13A Chloroform = 1.4 J EPA-MW13A 1,1-DCE = 0.75 J EPA-MW13A PCE = 0.64 J

3) Results from one full suite method blank were provided in association with the groundwater sample analyses. One additional method blank was provided for TCE only. No VOCs were detected in the method blanks.

Results from one trip blank were provided. Acetone was detected in the trip blank at an estimated concentration of 6.5 ug/L. Acetone was detected in sample EPA-MW6A at a concentration less than that of the trip blank at 6.2 ug/L. Due to potential blank contamination bias, this acetone result is qualified as U/Non-detect at the concentration reported. Results from two equipment blanks were provided, with no VOCs detected

4-5) ESC Laboratory provided results from one full set of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses. One additional set of LCS/LCSD analyses were provided for TCE only. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exception. The LCS recovery for acetone was slightly low at 48.7 percent for acetone (lower control limit of 49 percent). No action is taken for the slightly low recovery. Precision for 1,2-dichloropropane was slightly poor, with an RPD of 20 percent (control limit of 20 percent). No action is taken for the slightly poor precision.

6-7) ESC Laboratory provided results from one full set of project specific MS and MSD

analyses (spike on project samples EPA-MW6A). One additional sets of batch specific MS and MSD analyses were performed for TCE only. Precision and accuracy, as demonstrated by these analyses is acceptable.


groundwater sample in support of the VOC analyses. Surrogate recoveries ranged from 83.6 to 107 percent. The 83.6 percent toluene-d8 surrogate recovery is low for sample EPA-MW12C (control limits of 92 to 112 percent). No VOCs were detected in the sample. Due to potential low bias, all VOC result for sample EPA-MW12C are qualified as UJ/Estimated and non-detect at the reporting limits stated.


sample EPA-MW13A. TCE was detected in the primary and duplicate samples at


4

concentrations of 510 ug/L and 560 ug/L, respectively. Precision between the TCE duplicate sample results is acceptable, with an RPD of 9.3 percent.






DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X 9. Results Quantitation X X

%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The groundwater samples were received by ESC Laboratory on October 13, 2012.

The water samples were received at an acceptable temperature of 3.1 degrees on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by October 15, 2012, within prescribed holding times.

2) All groundwater samples were analyzed at 2 or 5 times dilutions to quantitate

perchlorate. Reporting limits are determined to be acceptable, with the following considerations. Perchlorate was not detected in samples EPA-MW12C, EPA-MW12A, EPA-MW51A, and EPA-MW13C, which were analyzed at dilutions. Samples were diluted due to matrix issues. The final reporting limit for the sample diluted by 5 times is acceptable at 2.5 ug/L.


analyses with no perchlorate detected. Results from two equipment blanks were also provided. Perchlorate was not detected in the equipment blanks.



5

5-6) ESC Laboratory provided results from one set of project specific MS and MSD analyses (spike on project sample EB002) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were 91.5 percent and 92.8 percent, with an RPD between MS and MSD recoveries of 1.4 percent.


of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS and LCSD recoveries were 97.5 and 100 percent, with an RPD of 2.5 percent between LCS duplicate results.


sample EPA-MW47A. Perchlorate was detected in the primary and duplicate samples at concentrations of 9.9 ug/L and 9.5 ug/L, respectively. Precision between the perchlorate duplicate sample results is acceptable, with an RPD of 4.1 percent.

. ESC Laboratory provided results from one set of project specific laboratory

duplicate sample analyses, performed on project sample EB001. The laboratory duplicate precision is acceptable, with no perchlorate detected in the duplicate samples.



6



LABORATORY REPORT # L600820 DATED OCTOBER 19, 2012



EPA-MW12A-10102012 / Chloroform EPA-MW13A-10102012 / Carbon tetrachloride, Chloroform, 1,1-DCE, and PCE

J/Estimated




EPA-MW6A / Acetone


reported

Acetone was detected in the associated trip blank at a

concentration similar to that of the sample. Acetone detection may be the results of blank contamination

bias. EPA-MW12C / All VOCs UJ/Estimated and

non-detect at the reporting limits

stated.

Surrogate recovery was low. Sample results may be biased low. No VOCs

detected in the sample.

SIGNATURE:

DATE:

October 25, 2012

PVJ0513.doc Created on 10/25/2012 2:55:00 PM

1





TB001-10042012 PVJ0513-01 Quality Control VOCs / Trip Blank COG03-10042012 PVJ0513-02 Groundwater VOCs EPA-MW58A-10042012 PVJ0513-03 Groundwater VOCs EPA-MW10C-10042012 PVJ0513-04 Groundwater VOCs EPA-MW10A-10042012 PVJ0513-05 Groundwater VOCs and Perchlorate EB001-10042012 PVJ0513-06 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW36A-10052012 PVJ0513-07 Groundwater VOCs EPA-MW40C-10052012 PVJ0513-08 Groundwater VOCs and Perchlorate EPA-MW40A-10052012 PVJ0513-09 Groundwater VOCs EPA-MW11A-10052012 PVJ0513-10 Groundwater VOCs EPA-MW8C-10052012 PVJ0513-11 Groundwater VOCs and Perchlorate DUP001-10052012 PVJ0513-12 Quality Control VOCs and Perchlorate / Field Duplicate of

primary sample EPA-MW8C-08202012 EPA-MW2C-10052012 PVJ0513-13 Groundwater VOCs and Perchlorate EPA-MW9C-10052012 PVJ0513-14 Groundwater VOCs EB001-10052012 PVJ0513-15 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X









3

Sample ID Qualified VOCs (ug/L) EPA-MW36A Chloroform = 0.20 J EPA-MW11A PCE = 0.89 J EPA-MW11A Chloroform = 0.48 J EPA-MW8C PCE = 0.87 J EPA-MW8C TCE = 0.28 J EPA-MW9C Chloroform = 0.17 J 3) Results from one full suite method blank were provided in association with the

groundwater sample analyses. Acetone was detected in the method blank at an estimated concentration of 9.09 ug/L Acetone was not detected in any of the associated groundwater samples, and no action is required..

Results from one trip blank were provided, with no VOCs detected. Results from two equipment blanks were provided, one for each day of sampling. Chloroform was detected in the equipment blanks at concentrations of 0.65 ug/L and 0.76 ug/L. Chloroform was detected in several associated samples at concentrations within 5 times those of the equipment blanks. Due to potential blank contamination bias, the following chloroform results are qualified as U/non-detect at the concentrations reported.

Sample ID Qualified VOCs (ug/L) EPA-MW10C Chloroform = 0.22 U EPA-MW10A Chloroform = 0.21 U EPA-MW36A Chloroform = 0.20 U EPA-MW11A Chloroform = 0.48 U EPA-MW9C Chloroform = 0.17 U







sample EPA-MW8C. PCE was detected in the primary and duplicate samples at estimated concentrations of 0.87 ug/L and 1.0 ug/L, respectively. Precision between


4

the duplicate PCE results is acceptable, with an RPD of 14 percent. TCE was detected in the primary samples at an estimated concentration of 0.28 ug/L and was not detected in the duplicate sample at <1.0 ug/L. TCE precision is acceptable, as both results agree within a reporting limit increment.






DATA QUALIFIED -










5

Sample ID Qualified Perchlorate (ug/L) EPA-MW40C Perchlorate = 1.3 J EPA-MW8C Perchlorate = 1.3 J 3) Results from two method blanks were provided in support of the groundwater sample







sample EPA-MW8C. Perchlorate was detected in the primary and duplicate samples at concentrations of 1.9 ug/L and 2.2 ug/L, respectively. Precision between the duplicate perchlorate results is acceptable, with an RPD of 15 percent.

TestAmerica provided results from two sets of laboratory duplicate sample analyses performed on batch samples. Laboratory duplicate precision is acceptable, with a maximum RPD between duplicate samples of 0.2 percent.



6





Data Qualifier(s)


EPA-MW11A-10052012 / PCE EPA-MW8C-10052012 / PCE EPA-MW8C-10052012 / TCE

J/Estimated




EPA-MW10C-10042012 / Chloroform EPA-MW10A-10042012 / Chloroform EPA-MW36A-10052012 / Chloroform EPA-MW11A-10052012 / Chloroform EPA-MW9C-10052012 / Chloroform

U/Non-detect at

the concentration reported.


concentrations greater than those detected in the samples. Chloroform detections may be the result of blank

contamination bias. EPAMW40C-10052012 and EPAMW8C-10052012 / Perchlorate

J/Estimated




SIGNATURE:

DATE:

October 25, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 20 groundwater/wastewater samples and one associated trip blank on October 8, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on October 9, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

EA05-EFF-10082012 PVJ0682-01 Groundwater VOCs EA05-MID-10082012 PVJ0682-02 Groundwater VOCs EA05-INF-10082012 PVJ0682-03 Groundwater VOCs and Perchlorate EA06-EFF-10082012 PVJ0682-04 Groundwater VOCs EA06-MID-10082012 PVJ0682-05 Groundwater VOCs EA06-INF-10082012 PVJ0682-06 Groundwater VOCs and Perchlorate EA08-EFF-10082012 PVJ0682-07 Groundwater VOCs EA08-MID-10082012 PVJ0682-08 Groundwater VOCs EA08-INF-10082012 PVJ0682-09 Groundwater VOCs and Perchlorate 33A-EFF-10082012 PVJ0682-10 Groundwater VOCs 33A-102-10082012 PVJ0682-11 Groundwater VOCs 33A-201-10082012 PVJ0682-12 Groundwater VOCs 33A-INF-10082012 PVJ0682-13 Groundwater VOCs and Perchlorate PH1-EFF-10082012 PVJ0682-14 Groundwater VOCsPH1-INF-10082012 PVJ0682-15 Groundwater VOCsPH23-EFF-10082012 PVJ0682-16 Groundwater VOCsPH23-INF-10082012 PVJ0682-17 Groundwater VOCsIX-EFF-10082012 PVJ0682-18 Groundwater Perchlorate IX-VI-10082012 PVJ0682-19 Groundwater Perchlorate IX-INF-10082012 PVJ0682-20 Groundwater Perchlorate TB001-10082012 PVJ0682-21 Quality Control VOCs / Trip Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2



REPORTED


DATA QUALIFIED -



1. Holding times X X 2. Detection limits X X 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X Yes 5. LCS Duplicate %R and (RPD) X X Yes 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X







EA05-MID Chloroform = 0.41 J EA05-EFF Acetone = 7.5 J EA05-INF Chloroform = 0.28 J EA06-EFF Chloroform = 0.69 J


3


EA06-INF Chloroform = 0.84 J EA08-INF Chloroform = 0.83 J 33A-EFF Chloroform = 0.54 J 33A-102 Chloroform = 0.67 J 33A-201 Chloroform = 0.69 J 33A-INF Chloroform = 0.56 J PH1-EFF TCE = 0.27 J PH1-INF 1,1-DCE = 0.28 J PH1-INF Chloroform = 0.17 J PH23-INF 1,1-DCE = 0.30 J PH23-INF Chloroform = 0.20 J

3) Results from two full suite method blanks were provided in association with the groundwater sample analyses. Acetone was detected in the method blank from batch 12J0455 at an estimated concentration of 7.12 ug/L. Acetone was not detected in any associated samples from that batch, and no action is taken Results from one trip blank were provided, with no VOCs detected.

4-5) TestAmerica provided results from two full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. Methylene chloride LCS/LCSD recoveries were 1 to 2 percent low for both LCS sets. Methylene chloride was not detected in any of the associated samples. Due to potential low bias, all methylene chloride results for the water samples are qualified as UJ/Estimated and non-detect at the reporting limits stated.


analyses (spikes on samples EA05-EFF and PH23-INF) in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses are acceptable, with the following exceptions. MS and MSD recoveries for methylene chloride in the PH23-INF spike were low. Methylene chloride data is already qualified due to low LCS recoveries, and no additional action is required.


analyses. Surrogate recoveries were acceptable, ranging from 95 to 110 percent.


4







DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment /Decon / Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only 9. Results Quantitation X X





analyses with no perchlorate detected. 4) Results from continuing calibration analyses were not provided.


5

5-6) TestAmerica provided results from one set of project specific MS and MSD analyses (spike on project sample EA05-INF). Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous MS and MSD recoveries ranged from 103 to 104 percent, with an RPD between MS and MSD recoveries of 1 percent.


the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. LCS and LCSD ranged from 108 and 109 percent, with an RPD between LCS and LCSD results of 0.3 percent.


Results from one set of laboratory duplicate sample analyses were provided for a duplicate of project sample EA06-INF. Perchlorate precision was acceptable, with an RPD between duplicate detections of 7 percent.



6




Geomatrix Consultants, Inc. (Geomatrix) collected 20 groundwater/wastewater samples and one associated trip blank on October 8, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most recent versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EA05-EFF-10082012 / Acetone EA05-MID-10082012 / Chloroform EA05-INF-10082012 / Chloroform EA06-EFF-10082012 / Chloroform EA06-INF-10082012 / Chloroform EA08-INF-10082012 / Chloroform 33A-EFF-10082012 / Chloroform 33A-102-10082012 / Chloroform 33A-201-10082012 / Chloroform 33A-INF-10082012 / Chloroform PH1-EFF-10082012 / TCE PH1-INF-10082012 / 1,1-DCE and Chloroform PH23-INF-10082012 / 1,1-DCE and Chloroform

J/Estimated




All Samples / Methylene chloride

UJ/Estimated and non-detect at the reporting limits

stated.

LCS and LCSD recoveries were low. Methylene chloride sample

results may be biased low.

SIGNATURE:

DATE:

April 28, 2012

PVJ1065.doc Created on 10/26/2012 8:41:00 AM

1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected seven groundwater samples and three associated quality control samples on October 12, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on October 15, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-10122012 PVJ1065-01 Quality Control VOCs / Trip Blank EPA-MW19C-10122012 PVJ1065-02 Groundwater VOCs and Perchlorate EPA-MW4C-10122012 PVJ1065-03 Groundwater VOCs and Perchlorate EPA-MW22C-10122012 PVJ1065-04 Groundwater VOCs and Perchlorate EPA-MW44A-10122012 PVJ1065-05 Groundwater VOCs and Perchlorate EPA-MW20A-10122012 PVJ1065-06 Groundwater VOCs EPA-MW21A-10122012 PVJ1065-07 Groundwater VOCs and Perchlorate EPA-MW62A-10122012 PVJ1065-08 Groundwater VOCs and Perchlorate DUP001-10122012 PVJ1065-09 Quality Control VOCs / Field Duplicate of primary sample




2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X






Sample ID Qualified VOCs (ug/L) EPA-MW44A Chloroform = 0.50 J EPA-MW21A TCE = 0.42 J


3

Sample ID Qualified VOCs (ug/L) EPA-MW62A Chloroform = 0.34 J DUP001 Chloroform = 0.39 J 3) Results from one full suite method blank were provided in association with the


Results from one trip blank were provided, with no VOCs detected. Results from one equipment blank were provided. Methylene chloride and TCE were detected in the equipment blank at estimated concentrations of 0.55 ug/L and 0.21 ug/L, respectively. Methylene chloride was not detected in any associated samples, and no action is required. TCE was detected in sample EPA-MW21A at a concentration within two times that of the equipment blank. Due to potential blank contamination bias, this TCE results is qualified as U/non-detect at the concentration reported.




(spike on project sample EPA-MW19C) in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.



sample EPA-MW62A. TCE was detected in the primary and duplicate samples at concentrations of 150 ug/L, each. Precision between the duplicate TCE results is acceptable, with an RPD of 0 percent. Chloroform was detected in the primary and duplicate samples at estimated concentrations of 0.34 ug/L and 0.39 ug/L. Precision between the duplicate chloroform results is acceptable, with an RPD of 14 percent.



4





DATA QUALIFIED -







determined to be acceptable. 3) Results from two method blanks were provided in support of the groundwater sample





the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is


5

acceptable. Aqueous LCS and LCSD recoveries ranged from 101 to 109 percent, with a maximum RPD of 5 percent between LCS duplicate results.


sample EPA-MW62A. Perchlorate was detected in the primary and duplicate samples at concentrations of 3.5 ug/L and 3.7 ug/L, respectively. Field duplicate precision is acceptable, with an RPD of 5.6 percent between duplicate sample results

TestAmerica provided results from two sets of laboratory duplicate sample analyses performed on project samples EPA-MW4C and DUP001. Laboratory duplicate precision is acceptable, with a maximum RPD between duplicate samples of 10 percent.



6





Data Qualifier(s)


EPA-MW44A-10122012 / Chloroform EPA-MW62A-10122012 / Chloroform DUP001-10122012 / Chloroform

J/Estimated




EPA-MW21A-10122012 / TCE

U/Non-detect at


TCE was detected in the associated equipment blank at a concentration

within tow times that of the groundwater sample. The TCE

detection may be the results of blank contamination bias.

SIGNATURE:

DATE:

October 26, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected ten groundwater samples and four associated quality control samples on October 15 and 16, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on October 17, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-10152012 PVJ1237-01 Quality Control VOCs / Trip Blank EPA-MW53A-10152012 PVJ1237-02 Groundwater VOCs and Perchlorate EPA-MW52A-10152012 PVJ1237-03 Groundwater VOCs and Perchlorate EPA-MW17C-10152012 PVJ1237-04 Groundwater VOCs EPA-MW18A-10152012 PVJ1237-05 Groundwater VOCs EB001-10152012 PVJ1237-06 Quality Control VOCs and Perchlorate / Equipment Blank COA18-10162012 PVJ1237-07 Groundwater VOCs and Perchlorate IR26A-10162012 PVJ1237-08 Groundwater VOCs EPA-MW60A-10162012 PVJ1237-09 Groundwater VOCs and Perchlorate EPA-MW34A-10162012 PVJ1237-10 Groundwater VOCs EPA-MW31A-10162012 PVJ1237-11 Groundwater VOCs EPA-MW23A-10162012 PVJ1237-12 Groundwater VOCs DUP001-10162012 PVJ1237-13 Quality Control VOCs / Field Duplicate of primary sample




2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X






Sample ID Qualified VOCs (ug/L) EPA-MW17C Carbon tetrachloride = 0.52 J EPA-MW17C Chloroform = 0.52 J


3

Sample ID Qualified VOCs (ug/L) EPA-MW18A PCE = 0.43 J EPA-MW18A TCE = 0.85 J IR26A TCE = 0.30 J IR26A Chloroform = 0.31 J EPA-MW60A TCE = 0.28 J EPA-MW60A Chloroform = 0.39 J EPA-MW34A PCE = 0.43 J EPA-MW34A TCE = 0.75 J EPA-MW31A PCE = 0.76 J EPA-MW31A TCE = 0.85 J EPA-MW23A Chloroform = 0.31 J DUP001 Chloroform = 0.31 J 3) Results from one full suite method blank were provided in association with the

groundwater sample analyses. Acetone was detected in the method blank at an estimated concentration of 10.8 ug/L. Acetone was not detected in any of the associated groundwater samples, and no action is required.

Results from one trip blank were provided, with no VOCs detected. Results from two equipment blanks were provided, with no VOCs detected.







sample EPA-MW23A. TCE was detected in the primary and duplicate samples at concentrations of 160 ug/L, each. Precision between the duplicate TCE results is acceptable, with an RPD of 0 percent. Chloroform was detected in the primary and duplicate samples at estimated concentrations of 0.31 ug/L, each. Precision between the duplicate chloroform results is acceptable, with an RPD of 0 percent.


4






DATA QUALIFIED -




#2 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X Yes 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab Only 9. Results Quantitation X X





Sample ID Qualified Perchlorate (ug/L) COA18 Perchlorate = 1.3 J 3) Results from one method blank were provided in support of the groundwater sample

analyses, with no perchlorate detected. Results from two equipment blanks were also


5

provided; one for each day of sampling. Perchlorate was detected in the equipment blank collected on October 16, 2012 at an estimated concentration of 0.56 ug/L. Perchlorate was detected in sample COA18, collected on October 16, 2012 at a concentration within 5 times that of the equipment blank. Due to potential blank contamination bias, this perchlorate results is qualified as U/non-detect at the concentration reported.


analyses (spike on project sample EPA-MW53A) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 93 to 102 percent, with an RPD between MS and MSD recoveries of 8 percent.


the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS and LCSD recoveries ranged from 103 to 106 percent, with an RPD of 3 percent between LCS duplicate results.

8) Field duplicate samples were not collected in support of the perchlorate samples

with this chain-of-custody.

TestAmerica provided results from one set of laboratory duplicate sample analyses performed on batch samples. Laboratory duplicate precision is acceptable, with an RPD between duplicate samples of 3 percent.



6





Data Qualifier(s)


EPA-MW17C-10152012 / Carbon tetrachloride and Chloroform EPA-MW18A-10162012 / PCE and TCE IR26A-10162012 / TCE and Chloroform EPA-MW60A-10162012 / TCE and Chloroform EPA-MW34A-10162012 / PCE and TCE EPA-MW31A-10162012 / PCE and TCE EPA-MW23A-10162012 / Chloroform DUP001-10162012 / Chloroform

J/Estimated




COA18-10162012 / Perchlorate


reported


concentration within 5 times that of the groundwater sample.

Perchlorate detection may be the result of blank contamination bias

SIGNATURE:

DATE:

October 25, 2012


1





TB001-10172012 PVJ1405-01 Quality Control VOCs / Trip Blank EPA-MW39C-10172012 PVJ1405-02 Groundwater VOCs EPA-MW39A-10172012 PVJ1405-03 Groundwater VOCs EPA-MW45A-10172012 PVJ1405-04 Groundwater VOCs EPA-MW54A-10172012 PVJ1405-05 Groundwater VOCs EPA-MW35A-10172012 PVJ1405-06 Groundwater VOCs IR3B-10172012 PVJ1405-07 Groundwater VOCs EA07-10172012 PVJ1405-08 Groundwater VOCs EB001-10172012 PVJ1405-09 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW59A-10182012 PVJ1405-10 Groundwater VOCs and Perchlorate EPA-MW61A-10182012 PVJ1405-11 Groundwater VOCs and Perchlorate IR34B-10182012 PVJ1405-12 Groundwater VOCs DUP001-10182012 PVJ1405-13 Quality Control VOCs / Field Duplicate or primary sample

IR34B-10182012 GCLake-10182012 PVJ1405-14 Groundwater VOCs MW25-10182012 PVJ1405-15 Groundwater VOCs EPA-MW38A-10182012 PVJ1405-16 Groundwater VOCs EPA-MW16A-10182012 PVJ1405-17 Groundwater VOCs EB001-10182012 PVJ1405-18 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X Yes 5. LCS Duplicate %R and (RPD) X X Yes 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X



2.2 degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on October 17 and 18, 2012. The samples were analyzed by October 22, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.






3

Sample ID Qualified VOCs (ug/L) EPA-MW54A Chloroform = 0.45 J IR3B Chloroform = 0.33 J GCLake Chloroform = 0.18 J GCLake TCE = 0.57 J MW25 Chloroform = 0.37 J EPA-MW38A Chloroform = 0.28 J EPA-MW38A Cis-1,2-DCE = 0.28 J EPA-MW16A Chloroform = 0.28 J

3) Results from two full suite method blanks were provided in association with the groundwater sample analyses. Acetone was detected in both method blanks at estimated concentrations of 3.93 ug/L and 5.07 ug/L. Acetone was not detected in any associated samples, and no action is required.

Results from one trip blank were provided. No VOCs were detected in the trip blank. Results from two equipment blanks were provided. No VOCs were detected in the equipment blanks.

4-5) TestAmerica provided results from two full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. Vinyl chloride LCS and LCSD recoveries were low at 77 percent and 75 percent (lower control limit of 80.9 percent) in the LCS from batch 12J0821. Vinyl chloride was not detected in any of the associated samples. Vinyl chloride results in the following samples analyzed in batch 12J0821 are qualified as UJ/Estimated and non-detect at the reporting limits stated.

EPA-MW39C-10172012 EPA-MW39A-10172012 EPA-MW45A-10172012 EPA-MW54A-10172012 EPA-MW35A-10172012 IR3B-10172012 EA07-10172012 EPA-MW59A-10182012 EPA-MW61A-10182012 IR34B-10182012 DUP001-10182012 GCLake-10182012 MW25-10182012 EPA-MW38A-10182012


analyses (spikes on project samples EPA-MW39C and EPA-MW16A) in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is


4

acceptable for all VOCs, with the following exceptions. MSD recoveries for cis-1,2-DCE and toluene were high in the spike of sample EPA-MW39C. MS and MSD recoveries for TCE were each low in the spike of sample EPA-MW16A. No action is taken for these VOCs, as acceptable precision and accuracy for these VOCs is demonstrated by the results of the LCS and LCSD analyses.


analyses. Surrogate recoveries were acceptable, ranging from 96 to 110 percent. 9) Sample DUP001 was submitted as a blind field duplicate of primary sample IR3B.

TCE was detected in the primary and duplicate samples at concentrations of 7.1 ug/L and 6.5 ug/l, respectively. Precision between the duplicate TCE detections is acceptable, with an RPD of 8.8 percent.



5





DATA QUALIFIED -




#2. 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only 9. Results Quantitation X X



2) No sample dilutions were required to quantitate perchlorate. All reporting limits

are acceptable with the following consideration. Perchlorate was detected at a concentration between the method detection limit (MDL) and the reporting limit in sample EPA-MW59A. Due to limited accuracy in this portion of the calibration range, this perchlorate result is qualified as J/Estimated.




analyses in support of the perchlorate analyses (spike on project sample EPA-MW59A). Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were each 101 percent, with an RPD between MS and MSD recoveries of 0.1 percent.


6





TestAmerica provided results from one set of batch specific laboratory duplicate sample analyses. Laboratory duplicate precision is acceptable, with no perchlorate detected in either of the samples.





Geomatrix Consultants, Inc. (Geomatrix) collected 14 groundwater samples and four associated quality control samples on October 17 and 18, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the table on the following page.


7

Validation Summary Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW45A-10172012 / Chloroform EPA-MW54A-10172012 / Chloroform IR3B-10172012 / Chloroform GCLake-10182012 / Chloroform and TCE MW25-10182012 / Chloroform EPA-MW38A-10182012 / Chloroform and Cis-1,2-DCE EPA-MW16A-10182012 / Chloroform

J/Estimated




may be limited.


J/Estimated

Perchlorate was detected at a concentration between the


may be limited. EPA-MW39C-10172012 EPA-MW39A-10172012 EPA-MW45A-10172012 EPA-MW54A-10172012 EPA-MW35A-10172012 IR3B-10172012 EA07-10172012 EPA-MW59A-10182012 EPA-MW61A-10182012 IR34B-10182012 DUP001-10182012 GCLake-10182012 MW25-10182012 EPA-MW38A-10182012

Vinyl chloride

UJ/Estimated


LCS and LCSD recoveries for vinyl chloride were low. Vinyl chloride sample results may be

biased low.

SIGNATURE:

DATE:

October 26, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected two groundwater samples on October 23, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on October 23, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

IR27C-170-10232012 PVJ1575-01 Groundwater VOCs / Passive Diffusion Bag Samples* IR27C-258-10232012 PVJ1575-02 Groundwater VOCs / Passive Diffusion Bag Samples* * These samples were not analyzed for MTBE or Ketones (acetone and 2-butanone) Samples were submitted for analysis of organic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -



1. Holding times X X 2. Detection limits X X 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X Yes 5. LCS Duplicate %R and (RPD) X X Yes 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X



1.1 degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on October 23, 2012. The samples were analyzed by October 25, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.


are acceptable. 3) Results from one full suite method blank were provided in association with the

groundwater sample analyses. No VOCs were detected in the method blank. 4-5) TestAmerica provided results from one full set of laboratory control sample (LCS)

and LCS duplicate (LCSD) analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. The vinyl chloride LCS and LCSD recoveries were low at 77 percent and 73 percent (lower control limit of 80.9 percent) in the LCS from batch 12J1010. Vinyl chloride was not detected in any of the associated samples. Vinyl chloride results in the


3

following samples analyzed in batch 12J1010 are qualified as UJ/Estimated and non-detect at the reporting limits stated.

IR27C-170-10232012 IR27C-258-10232012. 6-7) TestAmerica provided results from one set of batch specific MS and MSD analyses

in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. MS recoveries for ethylbenzene and toluene were slightly high. No action is taken, as these VOCs were not detected in the associated samples.


analyses. Surrogate recoveries were acceptable, ranging from 106 to 112 percent. 9) Field duplicate samples were not collected with the samples under this chain-of-



4




Geomatrix Consultants, Inc. (Geomatrix) collected two groundwater samples on October 23, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


IR27C-170-10232012 and IR27C-258-10232012 / Vinyl chloride

UJ/Estimated



biased low.

SIGNATURE:

DATE:

November 15, 2012


1



LABORATORY REPORT # PVJ1577 DATED NOVEMBER 12, 2012

INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 13 groundwater samples and six associated quality control samples on October 22 and 23, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on October 23, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-10222012 PVJ1577-01 Quality Control VOCs / Trip Blank EPA-MW9C-10222012 PVJ1577-02 Groundwater VOCs EPA-MW10C-10222012 PVJ1577-03 Groundwater VOCs MW15-10222012 PVJ1577-04 Groundwater VOCs MW16-10222012 PVJ1577-05 Groundwater VOCs EPA-MW26A-10222012 PVJ1577-06 Groundwater VOCs EPA-MW10A-10222012 PVJ1577-07 Groundwater VOCs DUP001-10222012 PVJ1577-08 Quality Control VOCs / Field Duplicate or primary sample

EPA-MW10A-10222012 COG03-10222012 PVJ1577-09 Groundwater VOCs EB001-10222012 PVJ1577-10 Quality Control VOCs and Perchlorate / Equipment Blank MW18-10232012 PVJ1577-11 Groundwater VOCs EB001-10232012 PVJ1577-12 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW43A-10232012 PVJ1577-13 Groundwater VOCs EPA-MW30A-10232012 PVJ1577-14 Groundwater VOCs EPA-MW50A-10232012 PVJ1577-15 Groundwater VOCs EPA-MW42A-10232012 PVJ1577-16 Groundwater VOCs and Perchlorate DUP001-10232012 PVJ1577-17 Quality Control VOCs and Perchlorate / Field Duplicate or

primary sample EPA-MW42A-10232012 MW12-10232012 PVJ1577-18 Groundwater VOCs EB001-10232012 PVJ1577-19 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X Yes 5. LCS Duplicate %R and (RPD) X X Yes 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X



1.1 degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on October 22 and 23, 2012. The samples were analyzed by October 26, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.

2) Sample MW12 was diluted by a factor of 10 times for TCE only. No other

sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).


3


EPA-MW9C Chloroform = 0.23 J EPA-MW10C Chloroform = 0.25 J MW15 Chloroform = 0.34 J EPA-MW26A Chloroform = 0.43 J EPA-MW10A Chloroform = 0.33 J DUP001 Chloroform = 0.25 J EPA-MW30A Chloroform = 0.21 J EPA-MW50A PCE = 0.56 J EPA-MW42A Chloroform = 0.20 J DUP001 Chloroform = 0.24 J MW12 Chloroform = 0.70 J

3) Results from four full suite method blanks were provided in association with the groundwater sample analyses. Acetone was detected in three of the four method blanks at estimated concentrations of 5.26 ug/L, 3.82 ug/L, and 4.29 ug/L. Acetone was not detected in any associated samples, and no action is required.

Results from one trip blank were provided. No VOCs were detected in the trip blank. Results from three equipment blanks were provided. No VOCs were detected in the equipment blanks.

4-5) TestAmerica provided results from four full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. Precision for both 2-butanone and acetone was poor, with RPDs of 50 percent and 75 percent, respectively, in the LCSD for batch 12J0972. No action is taken, as these VOCs were not detected in the associated sample and no bias to the sample results is indicated.

The vinyl chloride LCS and LCSD recoveries were low at 77 percent and 73 percent (lower control limit of 80.9 percent) in the LCS from batch 12J1010. Vinyl chloride was not detected in any of the associated samples. Vinyl chloride


4

results in the following samples analyzed in batch 12J1010 are qualified as UJ/Estimated and non-detect at the reporting limits stated. EPA-MW30A-10232012 EPA-MW50A-10232012 EPA-MW42A-10232012 DUP001-10232012 MW12-10232012

The vinyl chloride LCS was slightly low at 80 percent in batch 12J1059. This

batch is not associated with any vinyl chloride analyses, and no action is taken. 6-7) TestAmerica provided results from two sets of project specific MS and MSD

analyses (spikes on project samples EPA-MW9C and MW12), and from two sets of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable for all VOCs, with the following exceptions. MS/MSD recoveries for acetone, ethylbenzene, and toluene were high in one of the batch spikes. No action is taken for these VOCs, as acceptable precision and accuracy for these VOCs is demonstrated by the results of the LCS and LCSD analyses.


analyses. Surrogate recoveries were acceptable, ranging from 98 to 119 percent, with one exception. The 118 percent 4-bromofluorobenzene surrogate recovery for the 10 times dilution of TCE in sample MW12 is high (upper control limit of 114 percent). Due to potential high bias associated with the high surrogate recovery, the TCE result for sample MW12 is qualified as J/Estimated.

9) Two sets of field duplicate samples were submitted with the sample under this

chain-of-custody. Sample DUP001-10222012 was submitted as a blind field duplicate of primary sample EPA-MW10A. TCE was detected in the primary and duplicate samples at concentrations of 120 ug/L and 130 ug/l, respectively. Precision between the duplicate TCE detections is acceptable, with an RPD of 8.0 percent. PCE was detected in both samples of the field duplicate pair at concentrations of 1.2 ug/L, each. Chloroform was detected in both samples of the field duplicate pair at estimated concentrations between the MDL and RL. PCE and chloroform precision are acceptable for the duplicate pair.

Sample DUP001-10223012 was submitted as a blind field duplicate of primary sample EPA-MW42A. TCE was detected in the primary and duplicate samples at concentrations of 31 ug/L and 33 ug/l, respectively. Precision between the duplicate TCE detections is acceptable, with an RPD of 6.3 percent. Chloroform was detected in both samples of the field duplicate pair at estimated concentrations between the MDL and RL. Chloroform precision is acceptable, as duplicate results agree within a reporting limit increment.



5





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X No 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X 9. Results Quantitation X X



2) No sample dilutions were required to quantitate perchlorate. All reporting limits

are determined to be acceptable. 3) Results from one method blank were provided in support of the groundwater sample

analyses, with no perchlorate detected. Results from three equipment blanks were also provided. Perchlorate was detected at an estimated concentration of 0.56 ug/L in the equipment blank collected on October 23, 2012. Perchlorate was not detected in any of the associated groundwater samples at concentration within 5 times the equipment blank concentration, and no action is required.


analyses in support of the perchlorate analyses (spike on project sample DUP001-10232012). Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were 98 and 99 percent, with an RPD between MS and MSD recoveries of 0.8 percent.


6

7) TestAmerica provided results from one set of LCS and LCS duplicate analyses in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries were 102 and 104 percent. The RPD between LCS and LCSD results was acceptable at 2 percent.

8) Sample DUP001-10233012 was submitted as a field duplicate of primary sample

EPA-MW42A. Perchlorate precision is acceptable, with an RPD of 25 percent between the primary and duplicate samples.

TestAmerica provided results from one set of project specific laboratory duplicate sample analyses performed on project sample EPA-MW42A. Laboratory duplicate precision is acceptable, with an RPD of 25 percent (this exceeds the laboratory specific control limit of 15 percent, but meets the project precision control limit of 25 percent).



7



LABORATORY REPORT # PVJ1577 DATED NOVEMBER 12, 2012

Geomatrix Consultants, Inc. (Geomatrix) collected 13 groundwater samples and six associated quality control samples on October 22 and 23, 2012. . The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the table on the following page. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW9C-10222012 / Chloroform EPA-MW10C-10222012 / Chloroform MW15-10222012 / Chloroform EPA-MW26A-10222012 / Chloroform EPA-MW10A-10222012 / Chloroform DUP001-10222012 / Chloroform EPA-MW30A-10232012 / Chloroform EPA-MW50A-10232012 / PCE EPA-MW42A-10232012 / Chloroform DUP001-10232012 / Chloroform MW12-10232012 / Chloroform

J/Estimated

These VOCs were reported at concentrations between the


may be limited.

EPA-MW30A-10232012 EPA-MW50A-10232012 EPA-MW42A-10232012 DUP001-10232012 MW12-10232012 / Vinyl chloride

UJ/Estimated



biased low.

MW12-10232012 / TCE J/Estimated

Associated surrogate recovery is high. TCE sample result may be

biased high.

SIGNATURE:

DATE:

November 13, 2012


1



LABORATORY REPORT # C23633 DATED SEPTEMBER 26, 2012

INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected ten groundwater samples and four associated quality control samples on September 12 and 13, 2012. The samples were shipped to Accutest Laboratory, located in San Jose, California on September 13, 2012, and arrived at the laboratory on the following day. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09122012 C23633-01 Quality Control VOCs / Trip Blank EPA-MW57A-09122012 C23633-02 Groundwater VOCs and Perchlorate EPA-MW15C-09122012 C23633-03 Groundwater VOCs MW21-09122012 C23633-04 Groundwater VOCs EPA-MW1A-09122012 C23633-05 Groundwater VOCs and Perchlorate EPA-MW1C-09122012 C23633-06 Groundwater VOCs EB001-09122012 C23633-07 Quality Control VOCs and Perchlorate / Equipment Blank MW27-09132012 C23633-08 Groundwater VOCs and Perchlorate EPA-MW5C-09132012 C23633-09 Groundwater VOCs and Perchlorate EPA-MW56A-09132012 C23633-10 Groundwater VOCs EPA-MW48A-09132012 C23633-11 Groundwater VOCs EPA-MW3C-09132012 C23633-12 Groundwater VOCs and Perchlorate DUP001-09132012 C23633-13 Quality Control VOCs and Perchlorate / Field duplicate of




2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X No 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X No 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X



degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on September 12 and 13, 2012. The samples were analyzed by September 18, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.

2) Sample EPA-MW48A was diluted by a factor of 10 for all VOCs. Samples EPA-

MW3C and DUP001 were diluted by factors of 20 times each for all VOCs. No other sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).




3

3) Results from one full suite method blank were provided in association with the groundwater sample analyses. No VOCs were detected in the method blank. Results from one trip blank were provided. Acetone was detected in the trip blank at an estimated concentration of 5.2 ug/L. Acetone was not detected in any of the associated samples, and no action is required. Results from two equipment blanks were provided. No VOCs were detected in either of the equipment blanks.

4-5) Accutest provided results from one full set of laboratory control sample (LCS) and

LCS duplicate (LCSD) analyses (identified as blank spike analyses) in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. LCSD recoveries were high for benzene, ethylbenzene, toluene, and xylene isomers. These BTEX VOCs were not detected in any of the samples and no bias to the sample results is indicated.


(spike on project samples EPA-MW57A ) in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses, are acceptable.


analyses. Surrogate recoveries were acceptable, ranging from 94 to 103 percent. 9) Sample DUP001-09132012 was submitted as a blind field duplicate of primary sample

EPA-MW3C. TCE was detected in the primary and duplicate samples at concentrations of 975 ug/L and 1080 ug/L, respectively. Precision between the TCE detections is acceptable, with an RPD of 10 percent.



4





DATA QUALIFIED -





%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The groundwater samples were received by Accutest on September 14, 2012. The

water samples were received chilled at a temperature of 3.2 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by September 20, 2012, within prescribed holding times.

2) Samples EPA-MW5C, EPA-MW3C, and DUP001-09132012 were each diluted by

a factor of 2 times to quantitate perchlorate due to elevated conductivity. No other sample dilutions were required to quantitate perchlorate. Reporting limits are determined to be acceptable, with the following considerations. Some perchlorate results were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these perchlorate results are qualified as J/Estimated, as follows:

Sample ID Qualified Results(ug/L) EPA-MW57A Perchlorate = 2.1 J 3) Results from one method blank were provided in support of the groundwater sample

analyses, with no perchlorate detected. Results from two equipment blanks were also provided. Perchlorate was not detected in any of the blanks.

4) Results from continuing calibration analyses were not evaluated.


5

5-6) Accutest provided results from one set of project specific MS and MSD analyses

(spike on project samples EPA-MW57A ) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 92 to 93 percent, with an RPD between MS and MSD recoveries of 0.4 percent (spike recovery control limits of 80 to 120 percent).


duplicate (LCSD) analyses (identified as blank spike analyses) in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries ranged from 101 to 103 percent. The RPD between the LCS and LCSD results was acceptable at 2.4 percent.


EPA-MW3C. Perchlorate was detected in the primary and duplicate samples at concentrations of 22.7 ug/L, each. Precision between the perchlorate detections is acceptable, with an RPD of 0 percent.

Accutest provide results from one set of laboratory duplicate analyses in support of

perchlorate. Laboratory duplicate precision was acceptable, with an RPD of 0.7 percent.



6



LABORATORY REPORT # C23633 DATED SEPTEMBER 26, 2012

Geomatrix Consultants, Inc. (Geomatrix) collected ten groundwater samples and four associated quality control samples on September 12 and 13, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW57A-09122012 / TCE

J/Estimated

TCE was reported at a concentration between the method detection limit and the reporting limit. Accuracy in this portion of the calibration curve

may be limited.


J/Estimated



SIGNATURE:

DATE:

October 9, 2012

L596529.doc Created on 10/25/2012 7:23:00 AM

1



LABORATORY REPORT # L596529 DATED SEPTEMBER 28, 2012

INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 12 groundwater samples and four associated quality control sample on September 18 and 19, 2012. The samples were shipped via overnight courier to ESC Laboratory, located in Mt. Juliet, Tennessee, on September 20, 2012. Samples arrived at the laboratory on the following day. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09182012 L596529-01 Quality Control VOCs / Trip Blank EPA-MW6A-09182012 L596529-02 Groundwater VOCs EPA-MW12A-09182012 L596529-03 Groundwater VOCs and Perchlorate EPA-MW12C-09182012 L596529-04 Groundwater VOCs and Perchlorate EPA-MW26C-09182012 L596529-05 Groundwater VOCs and Perchlorate OWB-09182012 L596529-06 Groundwater VOCs MW29-09182012 L596529-07 Groundwater VOCs MW20-09182012 L596529-08 Groundwater VOCs EPA-MW47C-09182012 L596529-09 Groundwater VOCs EPA-MW47A-09182012 L596529-10 Groundwater VOCs and Perchlorate DUP001-09182012 L596529-11 Quality Control VOCs and Perchlorate/ Field Duplicate of

primary sample EPA-MW47A-09182012 EB001-09182012 L596529-12 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW51A-09192012 L596529-13 Groundwater VOCs and Perchlorate EPA-MW13C-09192012 L596529-14 Groundwater VOCs and Perchlorate EPA-MW13A-09192012 L596529-15 Groundwater VOCs and Perchlorate EB001-09192012 L596529-16 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X Yes 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X Yes 9. Field Duplicate Comparison X X 10. Results Quantitation X X




2) Samples MW-20 and EPA-MW47C were each diluted by a factor of 2 times for

all VOCs. Sample EPA-MW47A was diluted by 5 times for all VOCs. Samples DUP001 and EPA-MW13A were by factors of 10 and 20 times, respectively, for TCE only. No other sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).


3


EPA-MW12A Chloroform = 0.55 J DUP001 Chloroform = 0.51 J DUP001 1,1-DCE = 0.44 J EPA-MW13C Toluene = 4.0 J EPA-MW13A Carbon tetrachloride = 0.84 J EPA-MW13A Chloroform = 1.1 J EPA-MW13A 1,1-DCE = 0.80 J EPA-MW13A PCE = 0.51 J

3) Results from one full suite method blank were provided in association with the groundwater sample analyses. Two additional method blanks were provided for TCE only. No VOCs were detected in the method blanks.

Results from one trip blank were provided. Chloroform was detected in the trip blank at an estimated concentration of 0.54 ug/L. Results from two equipment blanks were provided; one for each day of sampling. Chloroform was detected in the equipment blanks at estimated concentrations of 0.54 ug/l and 0.69 ug/L. Chloroform was detected in several samples at concentrations within 5 time those of the associated blanks. Due to potential blank contamination bias, the following chloroform results are qualified as U/non-detect at the concentration reported.

Sample ID Qualified VOCs (ug/L) EPA-MW12A Chloroform = 0.55 U DUP001 Chloroform = 0.51 U EPA-MW13A Chloroform = 1.1 U

4-5) ESC Laboratory provided results from one full set of laboratory control sample

(LCS) and LCS duplicate (LCSD) analyses. Two additional sets of LCS/LCSD analyses were provided for TCE only. Precision and accuracy, as demonstrated by these analyses is acceptable.

6-7) ESC Laboratory provided results from one full set of project specific MS and MSD

analyses (spike on project samples EPA-MW12A). Two additional sets of batch specific MS and MSD analyses were performed for TCE only. Precision and accuracy, as demonstrated by these analyses is acceptable.


groundwater sample in support of the VOC analyses. Surrogate recoveries ranged from 84.6 to 97.8 percent. The Toluene-d8 surrogate recovery was low for


4

samples DUP001 and EPA-MW13A at 87.9 percent and 84.6 percent, respectively. Due to the low surrogate recoveries, all detections from the non-diluted analyses are qualified as J/Estimated. All non-detects are qualified as UJ/Estimated and non-detect at the reporting limits stated.


sample EPA-MW47A. TCE was detected in the primary and duplicate samples at concentrations of 640 ug/L and 560 ug/L, respectively. Precision between the TCE duplicate sample results is acceptable, with an RPD of 13 percent. Chloroform and 1,1-DCE were detected in the duplicate sample at estimated concentrations. These VOCs were not detected in the primary sample. Duplicate results for these VOCs all agree within reporting limit increments, and field duplicate precision is determined to be acceptable.






DATA QUALIFIED -




%R - percent recovery RPD - relative percent difference COMMENTS: Performance was acceptable, with the following exceptions and/or notes: 1) The water samples were received by ESC Laboratory on September 21, 2012. The

water samples were received at an acceptable temperature of 3.4 degrees on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by September 25, 2012, within prescribed holding times.


5

2) All groundwater samples were analyzed at 2 or 5 times dilutions to quantitate perchlorate. Reporting limits are determined to be acceptable. Samples were diluted due to matrix issues. The final reporting limit for the sample diluted by 5 times is acceptable at 2.5 ug/L.


analyses with no perchlorate detected. Results from two equipment blanks were also provided. Perchlorate was not detected in the equipment blanks.

4) Results from continuing calibration analyses were not provided. 5-6) ESC Laboratory provided results from one set of project specific MS and MSD

analyses (spike on project sample EB001-09182012) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were 86.4 and 87.6 percent, with an RPD between MS and MSD recoveries of 1.4 percent.


of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS and LCSD recoveries were each 99.2 percent, with an RPD of 0 percent between LCS duplicate results.


sample EPA-MW47A. Perchlorate was detected in the primary and duplicate samples at concentrations of 9.0 ug/L and 8.9 ug/L, respectively. Precision between the perchlorate duplicate sample results is acceptable, with an RPD of 1.1 percent

. ESC Laboratory provided results from one set of project specific laboratory

duplicate sample analyses, performed on project sample EB001-09192012. The laboratory duplicate precision is acceptable, with no perchlorate detected in the duplicate samples.



6



LABORATORY REPORT # L596529 DATED SEPTEMBER 28, 2012

Geomatrix Consultants, Inc. (Geomatrix) collected 12 groundwater samples and four associated quality control sample on September 18 and 19, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)


DUP001-09182012 / 1,1-DCE EPA-MW13C-09192012 / Toluene EPA-MW13A-09192012 / Carbon tetrachloride, 1,1-DCE, and PCE

J/Estimated




EPA-MW12A-09182012 / Chloroform DUP001-09182012 / Chloroform EPA-MW13A-09192012 / Chloroform


reported.

Chloroform was detected in the associated equipment blanks and trip

blank at concentrations within 5 times those of the groundwater

samples. Chloroform detections may be the result of blank contamination

bias. DUP001-09182012 and EPA-MW13A-09192012 / All VOCs from undiluted analyses

J/Estimated for detections

UJ/Estimated and non-detect at the

reporting limits stated for non-detects

Surrogate recovery was low.

Associated sample results may be biased low.

SIGNATURE:

DATE:

October 24, 2012

PVI0290.doc Created on 9/21/2012 6:59:00 AM

1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected four groundwater samples and two associated quality control samples on September 6, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 6, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09062012 PVI0290-01 Quality Control VOCs / Trip Blank COG03-09062012 PVI0290-02 Groundwater VOCs EPA-MW10C-09062012 PVI0290-03 Groundwater VOCs EPA-MW9C-09062012 PVI0290-04 Groundwater VOCs EPA-MW10A-09062012 PVI0290-05 Groundwater VOCs and Perchlorate EB001-09062012 PVI0290-06 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X Yes 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X






Sample ID Qualified VOCs (ug/L) EPA-MW10C Chloroform = 0.19 J EPA-MW9C Chloroform = 0.25 J EPA-MW10A Chloroform = 0.28 J


3



4-5) TestAmerica provided results from one full set of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exception. The LCSD recovery for methylene chloride was low at 78 percent (lower control limit of 79.7 percent). Due to potential low bias, methylene chloride results for the groundwater samples in this SDG are qualified as UJ/Estimated and non-detect at the reporting limits stated.


(spike on sample EPA-MW10C) in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses are acceptable.


analyses. Surrogate recoveries were acceptable, ranging from 96 to 102 percent. 9) Field duplicate samples were not collected with the samples under this chain-of-

custody. . 10) No anomalies were noted with respect to results quantitation or reporting.


4





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X Yes 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab Only 9. Results Quantitation X X





analyses, with no perchlorate detected. Results from one equipment blank were also provided. Perchlorate was detected in the equipment blank at an estimated concentration of 1.8 ug/L. Perchlorate was detected in sample EPA-MW10A at a concentration within 5 times that of the equipment blank at 5.5 ug/L. Due to potential blank contamination bias, this perchlorate results is qualified as U/non-detect at the concentration reported.


analyses (spike on project sample EPA-MW10A) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were 87 percent and 109 percent. The RPD between MS and MSD recoveries was high at 19 percent (upper laboratory control limit of 15


5

percent), but within the project precision limit of 25 percent. No action is taken, as the perchlorate detection in groundwater is qualified due to blank contamination..




custody.

TestAmerica provided results from one set of batch specific laboratory duplicate sample analyses. Laboratory duplicate precision is acceptable, with an RPD of 3 percent between laboratory duplicate analyses.



6




Geomatrix Consultants, Inc. (Geomatrix) collected four groundwater samples and two associated quality control samples on September 6, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW10C-09062012 / Chloroform EPA-MW9C-09062012 / Chloroform EPA-MW10A-09062012 / Chloroform

J/Estimated




COG03-09062012, EPA-MW10A-09062012 EPA-MW10C-09062012, and EPA-MW9C-09062012 / Methylene chloride

UJ/Estimated


LCS recovery for methylene chloride was low. Methylene chloride results

in groundwater samples may be biased low.



reported


concentration within 5 times that of the groundwater samples.

Perchlorate detection may be the result of blank contamination bias.

SIGNATURE:

DATE:

September 21, 2012

PVI0609.doc Created on 9/20/2012 3:24:00 PM

1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 20 groundwater/wastewater samples and one associated trip blank on September 10, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 11, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

PH1-EFF-09102012 PVI0609-01 Groundwater VOCsPH1-INF-09102012 PVI0609-02 Groundwater VOCsPH23-EFF-09102012 PVI0609-03 Groundwater VOCsPH23-INF-09102012 PVI0609-04 Groundwater VOCsIX-EFF-09102012 PVI0609-05 Groundwater Perchlorate IX-VI-09102012 PVI0609-06 Groundwater Perchlorate IX-INF-09102012 PVI0609-07 Groundwater Perchlorate TB001-09102012 PVI0609-08 Quality Control VOCs / Trip Blank 33A-EFF-09102012 PVI0609-09 Groundwater VOCs 33A-102-09102012 PVI0609-10 Groundwater VOCs 33A-201-09102012 PVI0609-11 Groundwater VOCs 33A-INF-09102012 PVI0609-12 Groundwater VOCs and Perchlorate EA08-EFF-09102012 PVI0609-13 Groundwater VOCs EA08-MID-09102012 PVI0609-14 Groundwater VOCs EA08-INF-09102012 PVI0609-15 Groundwater VOCs and Perchlorate EA06-EFF-09102012 PVI0609-16 Groundwater VOCs EA06-MID-09102012 PVI0609-17 Groundwater VOCs EA06-INF-09102012 PVI0609-18 Groundwater VOCs and Perchlorate EA05-EFF-09102012 PVI0609-19 Groundwater VOCs EA05-MID-09102012 PVI0609-20 Groundwater VOCs EA05-INF-09102012 PVI0609-21 Groundwater VOCs and Perchlorate Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2



REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X Yes B. Equipment/Field Blanks X X C. Trip Blanks X X Yes 4. Laboratory Control Sample (LCS) %R X X Yes 5. LCS Duplicate %R and (RPD) X X Yes 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X







PH1-EFF Acetone = 5.8 J PH1-INF 1,1-DCE = 0.46 J PH23-EFF Acetone = 5.8 J


3

Sample ID Qualified VOCs (ug/L) PH23-INF 1,1-DCE = 0.38 J PH23-INF Acetone = 6.0 J PH23-INF Chloroform = 0.26 J 33A-EFF Acetone = 4.7 J 33A-EFF Chloroform = 0.62 J 33A-102 Chloroform = 0.74 J 33A-201 Acetone = 5.2 J 33A-201 Chloroform = 0.78 J 33A-INF Chloroform = 0.58 J EA08-EFF Acetone = 5.1 J EA08-INF Acetone = 5.0 J EA06-EFF Acetone = 4.8 J EA06-MID Acetone = 5.0 J EA06-INF Chloroform = 0.88 J EA05-EFF Chloroform = 0.43 J

EA05-MID Chloroform = 0.45 J EA05-INF Chloroform = 0.29 J

3) Results from two full suite method blanks were provided in association with the

groundwater sample analyses. No VOCs were detected in the method blanks, with the following exceptions. Methylene chloride was detected in the method blank from batch 12I0394 at an estimated concentration of 0.59 ug/L. Methylene chloride was not detected in any of the associated water samples, and no action is required. Acetone was detected in the method blank from batch 12I0352 at an estimated concentration of 4.65 ug/L.

Results from one trip blank were provided. Acetone was detected in the trip blank at an estimated concentration of 4.1 ug/L. Acetone was detected in several associated sample at concentrations within 10 times those of the trip blank and the method blank. Due to potential blank contamination bias, the following acetone results are qualified as U/non-detect at the concentrations reported.


4

Sample ID Qualified VOCs (ug/L) PH1-EFF Acetone = 5.8 U PH23-EFF Acetone = 5.8 U PH23-INF Acetone = 6.0 U 33A-EFF Acetone = 4.7 U 33A-201 Acetone = 5.2 U EA08-EFF Acetone = 5.1 U EA08-INF Acetone = 5.0 U EA06-EFF Acetone = 4.8 U EA06-MID Acetone = 5.0 U

4-5) TestAmerica provided results two full sets of laboratory control sample (LCS) and

LCS duplicate (LCSD) analyses in support of the groundwater VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. For batch 12I0394, the LCS recoveries for trichlorofluoromethane were high at 130 and 131 percent (upper limit of 123 percent). No action is required, as trichlorofluoromethane was not detected in any associated samples. For the same batch, LCS and LCS duplicate recoveries for 1,2-dichloropropane were low at 79 percent and 83 percent, respectively (lower control limit of 85 percent). This batch is associated with samples EA05-EFF, EA05-MID, and EA05-INF. Based on the low LCS recoveries, the 1,2-dichloropropane results for these samples may be biased low, and are qualified as UJ/Estimated and non-detect at the reporting limits stated. Precision for acetone is poor in the LCS/LCSD pair, with a RPD of 52 percent. No action is taken, as all acetone data are qualified due to blank contamination, and the acetone LCS results agree within a reporting limit increment.


(spikes on sample 33A-EFF), and from one set of batch specific MS and MSD analyses. Precision and accuracy, as demonstrated by these analyses are acceptable, with the following exceptions. MS and/or MSD recoveries were high for trichlorofluoromethane and TCE in the batch spike. Trichlorofluoromethane was not detected in any associated samples, and no action is required. Precision and accuracy for TCE are demonstrated by the results of the LCS and LCSD analyses, and no action is required.


analyses. Surrogate recoveries were acceptable, ranging from 92 to 110 percent. 9) Field duplicate samples were not submitted with the samples under this chain-of-



5





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment /Decon / Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X No 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only 9. Results Quantitation X X





analyses with no perchlorate detected. Equipment blanks were not collected. 4) Results from continuing calibration analyses were not provided. 5-6) TestAmerica provided results from one set of project specific MS and MSD analyses

(spike on project samples EA08-INF). Precision and accuracy, as demonstrated by these analyses is acceptable, with the following considerations. Aqueous MS and MSD recoveries ranged from 77 to 95 percent, with an RPD between MS and MSD recoveries of 17 percent. The LCS recovery of 77 percent was low relative to the lower laboratory control limit of 80 percent. Precision between the MS and MSD recoveries was high at 19 percent (laboratory control limit of 15 percent), but within the project perchlorate control limit of 25 percent. No action is taken for the 77


6

percent MS recovery, as typical EPA control limits for inorganics are 75 to 125 percent, and the associated LCS and LCSD recoveries are in control.


the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. LCS and LCSD recoveries were 97 and 103 percent, with a maximum RPD between LCS and LCSD results of 6 percent.


Results from one set of project specific laboratory duplicate sample analyses were provided on sample IX-EFF. Perchlorate was not detected in either of the samples. Perchlorate precision is determined to be acceptable.



7




Geomatrix Consultants, Inc. (Geomatrix) collected 20 groundwater/wastewater samples and one associated trip blank on September 10, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


PH1-INF-09102012 / 1,1-DCE PH23-INF-09102012 / 1,1-DCE and Chloroform 33A-EFF-09102012 / Chloroform 33A-102-09102012 / Chloroform 33A-201-09102012 / Chloroform 33A-INF-09102012 / Chloroform EA06-INF-09102012 / Chloroform EA05-EFF-09102012 / Chloroform EA05-MID-09102012 / Chloroform EA05-INF-09102012 / Chloroform

J/Estimated




PH1-EFF-09102012 / Acetone PH23-EFF-09102012 / Acetone PH23-INF-09102012 / Acetone 33A-EFF-09102012 / Acetone 33A-201-09102012 / Acetone EA08-EFF-09102012 / Acetone EA08-INF-09102012 / Acetone EA06-EFF-09102012 / Acetone EA06-MID-09102012 / Acetone


reported

Acetone was detected in the associated method blank and trip blank at a concentration within 10

times that of the associated samples.

EA05-EFF-09102012, EA05-MID-09102012, and EA05-INF-09102012 / 1,2-Dichloropropane

UJ/Estimated and non-detect at the reporting limits

stated.

LCS recoveries for 1,2-Dichloropropane were low. 1,2-

Dichloropropane sample results may be biased low

SIGNATURE:

DATE:

September 20, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected six groundwater samples and three associated quality control samples on September 14, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 17, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09142012 PVI1060-01 Quality Control VOCs / Trip Blank EPA-MW11A-09142012 PVI1060-02 Groundwater VOCs EPA-MW2C-09142012 PVI1060-03 Groundwater VOCs and Perchlorate EPA-MW19C-09142012 PVI1060-04 Groundwater VOCs and Perchlorate EPA-MW4C-09142012 PVI1060-05 Groundwater VOCs and Perchlorate EPA-MW8C-09142012 PVI1060-06 Groundwater VOCs and Perchlorate EPA-MW58A-09142012 PVI1060-07 Groundwater VOCs DUP001-09142012 PVI1060-08 Quality Control VOCs / Field Duplicate or primary sample

EPA-MW58A-09142012 EB001-09142012 PVI1060-09 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X No 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X







EPA-MW11A Chloroform = 0.52 J EPA-MW11A PCE = 0.46 J DUP001 Chloroform = 0.16 J


3

3) Results from two full suite method blanks were provided in association with the

groundwater sample analyses. Acetone was detected in the method blank from batch 12I0648 at an estimated concentration of 4.99 ug/L. Acetone was not detected in any of the associated samples, and no action is required.


4-5) TestAmerica provided results from two full sets of laboratory control sample (LCS) and LCS duplicate (LCSD) analyses in support of the groundwater sample analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exception. The trichlorofluoromethane recovery in one LCS was high at 126 percent (upper control limit of 123 percent). Trichlorofluoromethane was not detected in any of the associated samples, and no action is required.


(spike on project sample EPA-MW11A), and from one set of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.



EPA-MW58A. Precision between the duplicate sample results, measured as the relative percent difference (RPD) between the primary and duplicate sample results, is calculated in the following table. Results are presented in micrograms per liter (ug/L).

Sample ID Chloroform PCE TCE EPA-MW58A <1.0 4.2 1.8 DUP001 0.16 4.1 1.7 RPD (%) +/- RL 2.4 5.7 +/- RL – Results agree within a reporting limit increment.

Precision between the duplicate sample results is very good, with a maximum RPD between duplicate results of 5.7 percent.



4





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X Yes 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only 9. Results Quantitation X X





3) Results from one method blank were provided in support of the groundwater sample analyses, with no perchlorate detected. Results from one equipment blank were also provided. Perchlorate was detected in the equipment blank at an estimated concentration of 1.2 ug/L. Perchlorate was detected in several samples at concentrations within 5 times that of the equipment blank. Due to potential blank contamination bias, the following perchlorate results are qualified as U/non-detect at the concentration reported.

Sample ID Qualified Perchlorate (ug/L) EPA-MW2C Perchlorate = 4.7 U EPA-MW19C Perchlorate = 2.8 U EPA-MW4C Perchlorate = 2.6 U EPA-MW8C Perchlorate = 2.1 U


5


analyses in support of the perchlorate analyses (spike on project sample EPA-MW2C). Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were each 91 percent, with an RPD between MS and MSD recoveries of 0.5 percent.



8) Field duplicate samples were not collected with this chain-of-custody in support of

the perchlorate analyses.

TestAmerica provided results from one set of project specific laboratory duplicate sample analyses (duplicate of project sample EPA-MW8C). Laboratory duplicate precision is acceptable, as the results are in agreement within a reporting limit increment (the RPD of 43 percent is not evaluated in this situation).



6




Geomatrix Consultants, Inc. (Geomatrix) collected six groundwater samples and three associated quality control samples on September 14, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW11A-09142012 / Chloroform and PCE DUP001-09142012 / Chloroform

J/Estimated




may be limited. EPA-MW2C-09142012 / Perchlorate EPA-MW19C-09142012 / Perchlorate EPA-MW4C-09142012 / Perchlorate EPA-MW8C-09142012 / Perchlorate

U/Non-detect at

the concentrations

reported

Perchlorate was detected in the

equipment blank at a concentration within 5 times

those of the samples. Perchlorate detections may be

the result of blank contamination bias.

SIGNATURE:

DATE:

September 25, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 11 groundwater samples and four associated quality control samples on September 20 and 211, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 24, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09202012 PVI1553-01 Quality Control VOCs / Trip Blank EPA-MW17C-09202012 PVI1553-02 Groundwater VOCs EPA-MW54A-09202012 PVI1553-03 Groundwater VOCs EPA-MW36A-09202012 PVI1553-04 Groundwater VOCs EPA-MW22C-09202012 PVI1553-05 Groundwater VOCs and Perchlorate EPA-MW18A-09202012 PVI1553-06 Groundwater VOCs EB001-09202012 PVI1553-07 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW43A-09212012 PVI1553-08 Groundwater VOCs EPA-MW10C-09212012 PVI1553-09 Groundwater VOCs DUP001-09212012 PVI1553-10 Quality Control VOCs / Field Duplicate or primary sample

EPA-MW10C-09212012 EPA-MW9C-09212012 PVI1553-11 Groundwater VOCs EPA-MW10A-09212012 PVI1553-12 Groundwater VOCs EPA-MW38A-09212012 PVI1553-13 Groundwater VOCs EPA-MW16A-09212012 PVI1553-14 Groundwater VOCs EB001-09212012 PVI1553-15 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X No B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X



degrees Celsius on wet ice. This temperature is below the recommended minimum temperature of 2 degrees Celsius. No action is taken, as the samples were not frozen. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on September 20 and 21, 2012. The samples were analyzed by September 26, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.




3

Sample ID Qualified VOCs (ug/L) EPA-MW17C Chloroform = 0.63 J EPA-MW17C Carbon tetrachloride = 0.66 J EPA-MW54A Chloroform = 0.44 J EPA-MW54A TCE = 0.22 J EPA-MW18A PCE = 0.57 J EPA-MW18A TCE = 0.91 J EPA-MW10C Chloroform = 0.24 J DUP001 Chloroform = 0.21 J EPA-MW9C Chloroform = 0.21 J EPA-MW10A Chloroform = 0.23 J

EPA-MW38A Chloroform = 0.25 J EPA-MW16A Chloroform = 0.29 J

3) Results from one full suite method blank were provided in association with the groundwater sample analyses. Acetone was detected in the method blank at an estimated concentration of 5.88 ug/L. Acetone was not detected in the associated samples, and no action is required. Results from one trip blank were provided. No VOCs were detected in the trip blank. Results from two equipment blanks were provided. Chloroform was detected in the equipment blanks collected on September 20 and 21, 2012, at estimated concentrations of 0.70 ug/L and 0.90 ug/L, respectively. All chloroform detections for the groundwater samples are at concentration equal to or less than these in the equipment blanks. Due to potential blank contamination bias, ass chloroform results are qualified as U/non-detect at the concentrations reported, as follows.

Sample ID Qualified VOCs (ug/L) EPA-MW17C Chloroform = 0.63 U EPA-MW54A Chloroform = 0.44 U EPA-MW18A Chloroform = 2.4 U EPA-MW10C Chloroform = 0.24 U DUP001 Chloroform = 0.21 U EPA-MW9C Chloroform = 0.21 U EPA-MW10A Chloroform = 0.23 U EPA-MW38A Chloroform = 0.25 U EPA-MW16A Chloroform = 0.29 U


4







EPA-MW10C. TCE was detected in the primary or duplicate samples at concentrations of 4.4 ug/L and 4.6 ug/L, respectively. Precision between the TCE detections is acceptable, with an RPD of 4.4 percent. Chloroform was detected in both samples at estimated concentrations. Both chloroform results are qualified due to blank contamination, and precision for chloroform is not calculated. Field duplicate precision is determined to be acceptable.



5





DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only 9. Results Quantitation X X


The water samples were received chilled at a temperature of 0.6 degrees Celsius on wet ice. This temperature is below the recommended minimum temperature of 2 degrees Celsius. No action is taken, as the samples were not frozen. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by September 27, 2012, within prescribed holding times.




4) Results from continuing calibration analyses were not provided. 5-6) TestAmerica provided results from one set of batch specific MS and MSD analyses

in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were each 98 percent, with an RPD between MS and MSD recoveries of 0.4 percent.


6

7) TestAmerica provided results from one set of LCS and LCS duplicate analyses in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. Aqueous LCS recoveries were 105 and 106 percent. The RPD between LCS and LCSD results was acceptable at 2 percent.



TestAmerica provided results from one set of batch specific laboratory duplicate sample analyses. Laboratory duplicate precision is acceptable, with an RPD of 2.0 percent between primary and duplicate sample results.



7




Geomatrix Consultants, Inc. (Geomatrix) collected 11 groundwater samples and four associated quality control samples on September 20 and 211, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW17C-09202012 / Carbon tetrachloride EPA-MW54A-09202012 / TCE EPA-MW18A-09202012 / PCE EPA-MW18A-09202012 / TCE

J/Estimated




may be limited.

EPA-MW17C-09202012 / Chloroform EPA-MW54A-09202012 / Chloroform EPA-MW10C-09212012 / Chloroform DUP001-09212012 / Chloroform EPA-MW9C-09212012 / Chloroform EPA-MW18A-09202012 / Chloroform EPA-MW10A-09212012 / Chloroform EPA-MW38A-09212012 / Chloroform EPA-MW16A-09212012 / Chloroform

U/Non-detect at

the concentrations

reported

Chloroform was detected in the associated equipment blanks at concentrations within 5 times

those of the groundwater samples. Chloroform detections

may be the results of blank contamination bias.

SIGNATURE:

DATE:

October 9, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected eight groundwater samples and four associated quality control samples on September 24 and 25, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 26, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09242012 PVI1723-01 Quality Control VOCs / Trip Blank IR26A-09242012 PVI1723-02 Groundwater VOCs EPA-MW60A-09242012 PVI1723-03 Groundwater VOCs and Perchlorate EB001-09242012 PVI1723-04 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW44A-09252012 PVI1723-05 Groundwater VOCs and Perchlorate EPA-MW39C-09252012 PVI1723-06 Groundwater VOCs EPA-MW39A-09252012 PVI1723-07 Groundwater VOCs EPA-MW45A-09252012 PVI1723-08 Groundwater VOCs DUP001-09252012 PVI1723-09 Quality Control VOCs / Field Duplicate or primary sample

EPA-MW45A-09252012 EPA-MW40C-09252012 PVI1723-10 Groundwater VOCs and Perchlorate EPA-MW40A-09252012 PVI1723-11 Groundwater VOCs EB001-09252012 PVI1723-12 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X No 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X







IR26A Chloroform = 0.31 J EPA-MW60A Chloroform = 0.34 J


3


EPA-MW45A Chloroform = 0.38 J DUP001 Chloroform = 0.34 J

3) Results from one full suite VOC method blank were provided in association with the groundwater sample analyses. No VOCs were detected in any of the method blank. Results from one trip blank were provided. Acetone was detected in the trip blank at an estimated concentration of 4.6 ug/L. Results from two equipment blanks were provided. Acetone and chloroform were detected in both equipment blanks, as follows:

Sample ID Detected VOCs (ug/L) EB001-09242012 Chloroform = 3.8 EB001-09242012 Acetone = 5.6 J

EB001-09252012 Chloroform = 3.7 EB001-09252012 Acetone = 5.3 J

Acetone was not detected in any of the associated samples and no action is required. Chloroform was detected several samples at concentrations less than those reported in the equipment blanks. Due to potential blank contamination bias, the following chloroform results are qualified as U/non-detect at the concentration reported

Sample ID Qualified VOCs (ug/L) IR26A Chloroform = 0.31 U EPA-MW60A Chloroform = 0.34 U EPA-MW45A Chloroform = 0.38 U DUP001 Chloroform = 0.34 U

4-5) TestAmerica provided results from one set of laboratory control sample (LCS) and







4

9) Sample DUP001 was submitted as a blind field duplicate of primary sample EPA-MW45A. Chloroform was detected in both samples at estimated concentrations. Both chloroform detections were qualified due to blank contamination, and are not further evaluated with respect to precision. Field duplicate precision is determined to be acceptable.






DATA QUALIFIED -




#2. 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab Only 9. Results Quantitation X X




determined to be acceptable, with the following consideration. Perchlorate was detected in the following samples at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, this perchlorate result is qualified as J/Estimated.


5

Sample ID Qualified Perchlorate (ug/L) EPA-MW40C Perchlorate = 1.3 J 3) Results from two method blanks were provided in support of the groundwater sample



analyses (spike on project sample EPA-MW60A), and from one set of batch specific MS and MSD analyses in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries ranged from 98 to 99 percent, with a maximum RPD between MS and MSD recoveries of 0.7 percent.




samples under this chain-of-custody

Results from two sets of laboratory duplicate sample analyses were provided; one on project sample EPA-MW40C. Laboratory duplicate precision is acceptable, with a maximum RPD of 2 percent between duplicate results, or agreement within a reporting limit increment for the duplicate of project sample EPA-MW40C.



6




Geomatrix Consultants, Inc. (Geomatrix) collected eight groundwater samples and four associated quality control samples on September 24 and 25, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)



J/Estimated



IR26A-09242012, EPA-MW60A-09242012, EPA-MW45A-09252012, and DUP001-09252012 / Chloroform

U/Non-detect at





SIGNATURE:

DATE:

October 12, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 12 groundwater samples and three associated quality control samples on September 26, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 27, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09262012 PVI1822-01 Quality Control VOCs / Trip Blank EPA-MW59A-09262012 PVI1822-02 Groundwater VOCs and Perchlorate EPA-MW53A-09262012 PVI1822-03 Groundwater VOCs and Perchlorate EPA-MW52A-09262012 PVI1822-04 Groundwater VOCs and Perchlorate EPA-MW61A-09262012 PVI1822-05 Groundwater VOCs and Perchlorate EPA-MW20A-09262012 PVI1822-06 Groundwater VOCs COA18-09262012 PVI1822-07 Groundwater VOCs and Perchlorate EPA-MW21A-09262012 PVI1822-08 Groundwater VOCs and Perchlorate EPA-MW34A-09262012 PVI1822-09 Groundwater VOCs DUP001-09262012 PVI1822-10 Quality Control VOCs / Field Duplicate or primary sample

EPA-MW34A-09262012 EPA-MW31A-09262012 PVI1822-11 Groundwater VOCs EPA-MW30A-09262012 PVI1822-12 Groundwater VOCs EPA-MW50A-09262012 PVI1822-13 Groundwater VOCs COG03-09262012 PVI1822-14 Groundwater VOCs EB001-09262012 PVI1822-15 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X No 9. Field Duplicate Comparison X X 10. Results Quantitation X X







EPA-MW21A TCE = 0.47 J EPA-MW34A TCE = 0.89 J


3


DUP001-099262012 PCE = 0.69 J DUP001-099262012 TCE = 0.79 J EPA-MW31A PCE = 0.68 J EPA-MW30A Chloroform = 0.28 J EPA-MW50A Chloroform = 0.34 J

3) Results from two full suite VOC method blanks were provided in association with the groundwater sample analyses. No VOCs were detected in any of the method blanks. Results from one trip blank were provided. No VOCs were detected in the trip blanks. Results from one equipment blank were provided. Acetone and chloroform were detected in the equipment blank, as follows:

Sample ID Qualified VOCs (ug/L) EB001-09262012 Chloroform = 1.8 EB001-09262012 Acetone = 4.2 J

Acetone was not detected in any of the associated samples and no action is required. Chloroform was detected several samples at concentrations within 5 times that of the equipment blank. Due to potential blank contamination bias, the following chloroform results are qualified as U/non-detect at the concentration reported

Sample ID Qualified VOCs (ug/L) EPA-MW31A Chloroform = 5.5 U EPA-MW30A Chloroform = 0.28 U EPA-MW50A Chloroform = 0.34 U




(spike on project sample EPA-MW59A), and from one set of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable for all VOCs, with the following exception. The cis-1,2-DCE MSD recovery for the project spike was slightly high at


4

121 percent (upper control limit of 119 percent). No action is required, as the associated LCS recovery demonstrated acceptable accuracy.


analyses. Surrogate recoveries ranged from 105 to 126 percent, and were within prescribed control limits, with the following exceptions. The toluene-d8 surrogate was high in sample EPA-MW20A at 113 percent (upper control limit of 111 percent). No action is taken, as no VOCs were detected in the sample and no bias to the sample results is indicated. The 4-bromofluorobenzene surrogate was high in sample EPA-MW50A at 115 percent (upper control limit of 114 percent). No action is taken, for the slightly high surrogate recovery, given a 1 percent allowance for rounding issues.

9) Sample DUP001 was submitted as a field duplicate of primary sample EPA-

MW34A. Chloroform was detected in the primary and duplicate samples at concentrations of 9.8 ug/L and 9.5 ug/L, respectively. Precision between chloroform results is acceptable, with an RPD of 3.1 percent. TCE was detected in both samples at estimated concentrations between the MDL and RL. PCE was detected in the duplicate sample at an estimated concentration of 0.69 ug/L, but was not detected in the primary sample at <1.0 ug/L. Precision for TCE and PCE is acceptable, as all results agree within reporting limit increments.



5





DATA QUALIFIED -




#2. 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only 9. Results Quantitation X X



2) Sample EPA-MW21A was diluted by a factor of 2 times to quantitate perchlorate.

No other sample dilutions were required to quantitate perchlorate. Reporting limits are determined to be acceptable, with the following consideration. Perchlorate was detected in the following samples at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, this perchlorate result is qualified as J/Estimated.

Sample ID Qualified Perchlorate (ug/L) EPA-MW59A Perchlorate = 1.6 J COA18 Perchlorate = 1.5 J 3) Results from one method blank were provided in support of the groundwater sample



6


analyses (spike on project sample EPA-MW59A) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable. MS and MSD recoveries were each 99 percent, with an RPD between MS and MSD recoveries of 0.3 percent.




samples under this chain-of-custody Results from one set of batch specific laboratory duplicate samples were provided, with acceptable precision, as both results were in agreement within reporting limit increments.



7




Geomatrix Consultants, Inc. (Geomatrix) collected 12 groundwater samples and three associated quality control samples on September 26, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW21A-09262012 / TCE EPA-MW34A-09262012 / TCE DUP001-099262012 / PCE and TCE EPA-MW31A-09262012 / PCE

J/Estimated




EPA-MW31A-09262012, EPA-MW30A-09262012, and EPA-MW50A / Chloroform


reported




EPA-MW59A-09262012 / Perchlorate COA18-09262012 / Perchlorate

J/Estimated

Perchlorate was reported at



SIGNATURE:

DATE:

October 12, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected 14 groundwater samples and five associated quality control samples on September 27, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 27, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

TB001-09272012 PVI1869-01 Quality Control VOCs / Trip Blank MW18-09272012 PVI1869-02 Groundwater VOCs MW12-09272012 PVI1869-03 Groundwater VOCs EB001-09272012 PVI1869-04 Quality Control VOCs and Perchlorate / Equipment Blank EPA-MW35A-09272012 PVI1869-05 Groundwater VOCs IR34B-09272012 PVI1869-06 Groundwater VOCs GCLake-09272012 PVI1869-07 Groundwater VOCs IR3B-09272012 PVI1869-08 Groundwater VOCs MW16-09272012 PVI1869-09 Groundwater VOCs DUP001-09272012 PVI1869-10 Quality Control VOCs / Field Duplicate or primary sample

MW16-09272012 EA07-09272012 PVI1869-11 Groundwater VOCs MW15-09272012 PVI1869-12 Groundwater VOCs EPA-MW42A-09272012 PVI1869-13 Groundwater VOCs and Perchlorate EPA-MW26A-09272012 PVI1869-14 Groundwater VOCs MW25-09272012 PVI1869-15 Groundwater VOCs EPA-MW62A-09272012 PVI1869-16 Groundwater VOCs and Perchlorate DUP002-09272012 PVI1869-17 Quality Control VOCs and Perchlorate / Field duplicate or

primary sample EPA-MW62A-09272012 EPA-MW23A-09272012 PVI1869-18 Groundwater VOCs EB002-09272012 PVI1869-19 Quality Control VOCs and Perchlorate / Equipment Blank Samples were submitted for analysis of organic and inorganic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X Yes C. Trip Blanks X X Yes 4. Laboratory Control Sample (LCS) %R X X 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X See Note #8. 9. Field Duplicate Comparison X X 10. Results Quantitation X X




2) Sample MW12 was diluted by a factor of 20 times for TCE only. Samples EPA-

MW62A and DUP002-09272012 were diluted by factors of 5 times each for TCE only. No other sample dilutions were required to quantitate any VOCs. All reporting limits are acceptable with the following considerations. Some VOCs were reported at concentrations between the method detection limit (MDL) and the reporting limit. Due to limited accuracy in this portion of the calibration range, these VOC results are qualified as J/Estimated. The following results are qualified (pending the results of the blank evaluation).




3

Sample ID Qualified VOCs (ug/L) MW12 Chloroform = 0.78 J GCLake Chloroform = 0.22 J IR3B Chloroform = 0.32 J MW16 Chloroform = 0.24 J DUP001-09272012 Chloroform = 0.29 J EA07 Acetone = 4.2 J MW15 Chloroform = 0.31 J EPA-MW26A Chloroform = 0.50 J MW25 Chloroform = 0.38 J EPA-MW62A Chloroform = 0.44 J EPA-MW62A 1,1-DCE = 0.25 J EPA-MW62A Acetone = 3.8 J DUP002-09272012 Chloroform = 0.56 J DUP002-09272012 PCE = 0.23 J EPA-MW23A Chloroform = 0.35 J

3) Results from two full suite VOC method blanks were provided in association with the groundwater sample analyses. No VOCs were detected in any of the method blanks. Results from one trip blank were provided. Acetone was detected in the trip blank at an estimated concentration of 6.0 ug/L. Results from two equipment blanks were provided. Several VOCs were detected in the equipment blanks, as follows:

Sample ID Qualified VOCs (ug/L) EB001-09272012 Acetone = 5.4 EB001-09272012 Chloroform = 0.97 EB001-09272012 TCE = 0.35 EB002-09272012 Acetone = 4.2 J EB002-09272012 Chloroform = 1.5 J


4

Acetone was detected in several samples at concentrations within 10 times those of the associated equipment blanks. Due to potential blank contamination bias, the following Acetone results are qualified as U/non-detect at the concentration reported

Sample ID Qualified VOCs (ug/L) EA07 Acetone = 4.2 U EPA-MW62A Acetone = 3.8 U GCLake Acetone = 20 U

Chloroform was detected in several samples at concentrations within 5 times those of the associated equipment blanks. Due to potential blank contamination bias, the following Chloroform results are qualified as U/non-detect at the concentration reported

Sample ID Qualified VOCs (ug/L) MW18 Chloroform = 0.28 U MW12 Chloroform = 0.78 U GCLake Chloroform = 0.22 U IR3B Chloroform = 0.32 U MW16 Chloroform = 0.24 U DUP001-09272012 Chloroform = 0.29 U MW15 Chloroform = 0.31 U EPA-MW26A Chloroform = 0.50 U MW25 Chloroform = 0.38 U EPA-MW62A Chloroform = 0.44 U DUP002-09272012 Chloroform = 0.56 U EPA-MW23A Chloroform = 0.35 U

TCE was detected in one sample at a concentration within 5 times those of the associated equipment blank. Due to potential blank contamination bias, the following TCE results are qualified as U/non-detect at the concentration reported

Sample ID Qualified VOCs (ug/L) IR3B TCE = 1.4 U




(spike on project sample EPA-MW35A), and from one set of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable for all VOCs, with the following


5

exceptions. MSD recoveries in the project spike were high for cis-1,2-DCE, TCE, and trichlorofluoromethane. No action is required, as the associated LCS recoveries for these VOCs demonstrated acceptable accuracy.


analyses. Surrogate recoveries ranged from 102 to 129 percent, and were within prescribed control limits, with the following exceptions. The toluene-d8 surrogate was slightly high in the following samples (upper control limit of 111 percent):

Sample ID High Toluene-D8 Surrogate

GCLake 112 % MW15 112 % EPA-MW62A 113 % DUP002 113 % EPA-MW23A 112 %

No action is taken, for the slightly high surrogate recoveries at 112 percent, given a 1 percent allowance for rounding issues. VOCs detections in undiluted analyses for samples EPA-MW26A and it duplicate DUP002 are qualified as J/Estimated due to potential high bias. No additional data are qualified as all detections are either between the MDL and RL, or a qualified due to blank contamination.

9) Two sets of field duplicate samples were collected in support of the VOC analyses.

Sample DUP001 was submitted as a field duplicate of primary sample MW16. TCE was detected in the primary and duplicate samples at concentrations of 15 ug/L, each. Precision between TCE results is acceptable, with an RPD of 0 percent. Chloroform was detected in both samples at estimated concentrations between the MDL and RL. Chloroform is qualified due to equipment blank contamination, and is not further assessed in the precision evaluation.

Sample DUP002 was submitted as a field duplicate of primary sample EPA-MW62A. Precision between the duplicate sample results, measured as the relative percent difference (RPD) between the primary and duplicate sample results, is calculated in the following table. Results are presented in micrograms per liter (ug/L).

Sample ID 1,1-DCE Acetone Chloroform PCE TCE

EPA-MW62A 0.25 3.8 0.44 <1.0 210 DUP002 <1.0 <20 0.56 0.23 190 RPD (%) +/- RL NC NC +/- RL 10

+/- RL = Results agree within a reporting limit increment NC – Not calculated as acetone detection is qualified due to blank contamination. Precision between the duplicate sample results is very good, with a maximum RPD between duplicate results of 10 percent between TCE.


6






DATA QUALIFIED -



1. Holding times / Preservation X X 2. Detection limits / Dilutions X X 3. Blanks A. Method/Prep Blanks X X B. Equipment/Decon/Field Blanks X X 4. Initial and Continuing Calibration %R X X Not required 5. Matrix Spike (MS) %R X X 6. MS Duplicate (MSD) %R and RPD X X 7. LCS and LCSD %R and RPD X X 8. Field/Lab Duplicate Comparison (RPD) X X Lab only 9. Results Quantitation X X


The water samples were received chilled at a temperature of 2.1 degrees Celsius on wet ice. Holding times for perchlorate are 28 days. All perchlorate analyzes were performed by October 1 2012, within prescribed holding times.





analyses (spike on project sample EPA-MW62A) in support of the perchlorate analyses. Precision and accuracy, as demonstrated by these analyses is acceptable.


7

MS and MSD recoveries were 98 percent and 100 percent, with an RPD between MS and MSD recoveries of 2 percent.




samples under this chain-of-custody Results from one set of batch specific laboratory duplicate samples were provided, with acceptable precision, as both results were non-detect.



8




Geomatrix Consultants, Inc. (Geomatrix) collected 14 groundwater samples and five associated quality control samples on September 27, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic and Inorganic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


EPA-MW62A-09272012 / 1,1-DCE DUP002-09272012 / PCE

J/Estimated




MW18-09272012 , MW12-09272012 GCLake-09272012, IR3B-09272012 MW16-09272012 , DUP001-09272012-09272012 MW15-09272012 , EPA-MW26A-09272012 MW25-09272012, EPA-MW62A-09272012 DUP002-09272012, and EPA-MW23A-09272012 / Chloroform


reported




EA07-09272012, EPA-MW62A-09272012, GCLake-09272012 / Acetone

U/Non-detect at



associated equipment blanks at concentrations within 10 times those of the associated samples. Acetone


SIGNATURE:

DATE:

October 13, 2012


1




INTRODUCTION Geomatrix Consultants, Inc. (Geomatrix) collected two groundwater samples on September 27, 2012. The samples were hand delivered to TestAmerica Laboratory, located in Phoenix, Arizona on September 27, 2012. Sample identifications and requested analyses are listed below. Geomatrix Sample ID Lab ID Matrix Analyses Requested / Comments

IR27C-170-09272012 PVI1870-01 Groundwater VOCs / Passive Diffusion Bag Samples IR27C-258-09272012 PVI1870-02 Groundwater VOCs / Passive Diffusion Bag Samples Samples were submitted for analysis of organic compounds, as listed below. Volatile Organic Compounds (VOCs) – Project Specific Short List - EPA Method



2




REPORTED


DATA QUALIFIED -




#2 3. Blanks A. Laboratory Method Blanks X X B. Equipment/Decon/Field Blanks X X C. Trip Blanks X X 4. Laboratory Control Sample (LCS) %R X X No 5. LCS Duplicate %R and (RPD) X X 6. Matrix Spike (MS) %R X X No 7. MS Duplicate (MSD) %R and (RPD) X X No 8. Surrogate Recoveries (%R) X X 9. Field Duplicate Comparison X X 10. Results Quantitation X X



1.2 degrees Celsius on wet ice. The groundwater samples were properly preserved with hydrochloric acid at the time of collection on April 24, 2012. The samples were analyzed by May 1, 2012, within the prescribed 14-day holding time for preserved VOCs in groundwater.




3

Sample ID Qualified VOCs (ug/L) IR3B-170 2-Butanone = 1.8 J IR3B-170 Chloroform = 0.46 J IR3B-170 Acetone = 19 J IR3B-270 Chloroform = 0.40 J IR3B-270 Acetone = 17 J

IR27A-180 Acetone = 15 J IR27A-180 PCE = 0.41 J

IR27A-180 TCE = 0.58 J

IR27C-170 Acetone = 16 J IR27C-170 Benzene = 0.46 J IR27C-170 m/p-Xylenes = 0.83 J IR27C-170 o-Xylene = 0.38 J

IR27C-258 Acetone = 9.2 J 3) Results from three full suite method blanks were provided in association with the

groundwater sample analyses. No VOCs were detected in the method blanks. 4-5) TestAmerica provided results from three full sets of laboratory control sample (LCS)

and LCS duplicate (LCSD) analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. The acetone LCS recovery for batch 12D1214 was high at 155 percent (upper control limit of 153 percent). No acetone detections were associated with this batch, and no action is required. The trichlorofluoromethane LCS recovery for batch 12E0076 was high at 126 percent (upper control limit of 123 percent). No trichlorofluoromethane detections were associated with this batch, and no action is required.


(spike on project sample IR27C-258), and from two sets of batch specific MS and MSD analyses in support of the VOC analyses. Precision and accuracy, as demonstrated by these analyses is acceptable, with the following exceptions. MS recoveries were high for acetone, ethylbenzene, and trichlorofluoromethane in one f the batch spikes. Precision for both acetone and 2-butanone was poor in the project spike, and in one of the batch spikes. TCE has a slightly low MS recovery in one of the batch spikes. No action is taken for these excursions, as acceptable precision and accuracy for the associated batches was demonstrated by the results of the LCS and LCSD analyses.




4

9) Field duplicate samples were not collected with the samples under this chain-of-custody.




LABORATORY REPORT # PVD1832 DATED MAY 3, 2012

Geomatrix Consultants, Inc. (Geomatrix) collected five groundwater samples on April 24, 2012. The sample results have been validated in accordance with the EPA Functional Guidelines for Organic Data Review (EPA – most applicable versions), appropriate method requirements, Project QAPP requirements, and professional judgment of the data reviewer. The QC information evaluated has been described in the preceding pages. Based on this review, data provided for the groundwater samples collected are determined to be quantitative, with the exceptions noted in the following table. Sample Identification(s) / Analyte(s)

Data Qualifier(s)


IR3B-170 / 2-Butanone, Chloroform, and Acetone IR3B-270 / Chloroform and Acetone IR27A-180 / Acetone, PCE, and TCE IR27C-170 / Acetone, Benzene, m/p-Xylenes, o-Xylene IR27C-258 / Acetone

J/Estimated




limited.

SIGNATURE:

DATE:

May 24, 2012

Page:

1/15

MEMORANDUM

To:

Michael Dempsey, Matrix New World Engineering, Inc.

From:

William Huskie, Nankoweep Environmental Consulting, Golden, Colorado

Date:

January 10, 2013

Subject:

Phoenix Goodyear Airport North – Quality Control Evaluation – Fourth Quarter 2012 Groundwater Sampling

The purpose of this memorandum is to provide a summary evaluation of data quality associated with groundwater, waste water, and performance evaluation samples collected during the Fourth Quarter 2012 (includes samples collected in September, October, and November 2012) at the Phoenix-Goodyear Airport-North Superfund Site (PGAN). The review was conducted by a third party Data Validator, Mr. William Huskie, of Nankoweep Environmental Consulting. The review process included evaluation of both field and laboratory quality assurance and quality control (QA/QC) sample results reported. Evaluation criteria for the QA/QC review were based on a combination of SW-846 method requirements, EPA data validation guidance, the Quality Assurance Project Plan (QAPP) prepared for the project, and professional judgment of the third party Data Validator. Groundwater and waste water samples were submitted to TestAmerica Laboratory, located in Phoenix, AZ, for analysis of volatile organic compounds (VOCs) and perchlorate. Two additional laboratories analyzed PGAN samples during the fourth quarter 2012. One data package from each the September, October, and November 2012 sampling events was submitted to ESC laboratory (ESC) located in Mt. Juliet, Tennessee for analysis of VOCs and perchlorate. Similarly, one data package from each month in the fourth quarter was submitted to Accutest Laboratory, located in San Jose, California for analysis of VOCs and perchlorate. Additionally, all three laboratories performed analyses of blind Performance Evaluation (PE) samples (identified as field groundwater samples MW030 and MW031) during the fourth quarter 2012 (November sampling event). A project specific short list of 19 target VOCs was reported from the Method 8260B analyte list for all samples where VOC analysis was requested. Results of the fourth quarter 2012 groundwater sampling (including PE samples) were provided in 29 TestAmerica reports, four ESC reports, and four Accutest laboratory reports (referred to as sample delivery group (SDG) reports).

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Individual data validation reports were prepared by the Data Validator for each of the 37 SDGs to assess field and laboratory quality control for the fourth quarter 2012 groundwater sampling events. Standard laboratory quality control deliverables (i.e. Level 3 deliverables) were evaluated for each of the SDGs, as detailed herein. The validation reports were transmitted to Matrix New World Engineering for review and incorporation of data qualifiers into the project database. Validation procedures were used to evaluate the data in terms of accuracy, precision, sensitivity, and completeness. A summary of the validation effort and findings for the fourth quarter 2012 samples is presented in the following sections.

SAMPLE HOLDING TIME EVALUATION Sample holding time limits stipulate the time allowed between sample collection, sample preparation (if required), and sample analysis, when the specified sample preservation and storage procedures are followed (SW-846). The time interval from sample collection to sample analysis, for each sample and parameter tested, was evaluated to determine if the required holding times were met. Sample preservation, chain-of-custody documentation, and sample receipt documentation were also reviewed. All samples submitted for analysis of VOCs during the fourth quarter 2012 sampling events were properly preserved with hydrochloric acid, and were analyzed within prescribed holding time of 14 days. All samples submitted for analysis of perchlorate were analyzed within the required 28-day holding time. All samples were placed on wet ice in coolers at the time of sample collection. Samples were hand delivered to TestAmerica laboratory, usually on the day of sampling, or on the following day. Samples submitted to ESC and Accutest laboratories were shipped under proper chain-of-custody procedures. Samples should arrive at the laboratory chilled to a temperature of 4.0 degrees Celsius (+/- 2 degrees Celsius). No temperature exceedances were recorded. Some samples have been received at temperatures less than 2 degrees Celsius. No action was required, as no samples arrived at the laboratory frozen.

QUALITY ASSURANCE – FIELD SAMPLES Twenty-nine trip blanks and 44 equipment rinsate blanks were submitted from the field to the laboratories to evaluate potential contamination from sampling operations, field conditions, sample handling, decontamination procedures, and sample transport. Twenty-eight sets of blind field duplicate samples were submitted to monitor field and laboratory quality control with respect to analytical precision during the fourth quarter 2012 sampling event. Results of the field quality control sampling are discussed in detail in the following sections. FIELD DUPLICATES Twenty-eight sets of field duplicate samples were collected during the fourth quarter 2012 groundwater sampling events. Precision between the major constituents of concern for the groundwater monitoring program (trichloroethene (TCE) and perchlorate) was very good, with all RPDs less than the QAPP specified RPD precision control limit of 25 percent, with the following exceptions. TCE precision was poor between the following field duplicate samples analyzed by Accutest in one November 2012 SDG.

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SDG Sample(s) Affected C23118 EPA-MW3C and DUP001 Due to the poor precision, TCE results for these samples were qualified as J/Estimated. Perchlorate precision was poor between the following field duplicate samples analyzed by ESC in one November 2012 SDG. SDG Sample(s) Affected L605508 PZ01 and DUP001 Due to the poor precision, perchlorate results for these samples were qualified as J/Estimated. Precision for all remaining target analytes for the investigation was acceptable, with RPDs less than the project specified control limit of 25 percent between field duplicate results, or with duplicate results in agreement within a reporting limit increment. LABORATORY DUPLICATES TestAmerica and ESC provided results from batch specific and project specific laboratory duplicate analyses in support of the perchlorate results for each analytical batch. Laboratory duplicate precision for the perchlorate analyses was within laboratory-prescribed RPD control limits for each of the duplicate analyses, or was in agreement within the 2 ug/L reporting limit increment. TRIP BLANK ANALYSES A trip blank is defined as a sample of analyte-free water prepared at the laboratory, shipped to the sampling site, and returned to the laboratory unopened for analysis. The objective of a trip blank sample is to document potential contamination associated with sample shipping procedures, field and laboratory handling procedures, or other contamination associated with organic-free and deionized water provided by, and used within the laboratory. Trip blank samples are particularly useful in documenting VOC contamination from outside sources. Thirty-nine trip blanks were submitted to TestAmerica/ESC/Accutest laboratories in support of the fourth quarter 2012 VOC analyses. VOCs were not detected in the trip blanks, with the exceptions described below: Acetone, methylene chloride, and chloroform were detected in some trip blanks during the fourth quarter 2012 sampling events. In some cases, acetone was detected in trip blanks, but was not detected in the associated samples, and no action was required, as no bias to the sample results was indicated. In other cases, acetone, methylene chloride, or chloroform were detected in the associated groundwater samples at concentrations similar to the concentrations reported in the trip blanks, as described below. Acetone was detected in trip blanks from one September TestAmerica SDG, and from one October ESC SDG at concentrations within ten times those of associated groundwater samples (ten times rule for common laboratory contaminants – though actual sample concentrations were generally within a factor of two to three times the blank detections). The following acetone sample results were qualified as “U/non-detect at the concentrations reported” due to potential blank contamination bias.

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SDG Sample(s) Affected PVI0609 PH1-EFF, PH23-EFF, PH23-INF, 33A-EFF, 33A-201, EA08-EFF, EA08-INF,

EA06-EFF, and EA06-MID Acetone was also detected in the method blank associated with this SDG SDG Sample(s) Affected L600820 EPA-MW6A Chloroform was detected in the trip blank from one September 2012 ESC laboratory SDG, and from three November 2012 TestAmerica SDGs at concentrations within five times those of associated groundwater samples. The following Chloroform sample results were qualified as “U/non-detect at the concentrations reported” due to potential blank contamination bias. SDG Sample(s) Affected L596529 EPA-MW12A, DUP001-09182012, and EPA-MW13A Chloroform was also detected in the equipment blank associated with this SDG SDG Sample(s) Affected PVK1721 MW18, EPA-MW14C, EPA-MW31A, EPA-MW15, EPA-MW16,

EPA-MW25A and EPA-MW42A Chloroform was also detected in the equipment blank associated with this SDG SDG Sample(s) Affected PVK1630 MW26, EPA-MW54A, PSDW, APS-MW03, EPA-MW21A, and

EPA-MW34A Chloroform was also detected in the equipment blank associated with this SDG SDG Sample(s) Affected PVK1450 LPW-894, EPA-MW39C, EPA-MW39A, EPA-MW45A, EPA-MW16C

EPA-MW35A, EA02, EA07, EPA-MW16A, DUP001-11202012, EPA-MW62A, MW19, EPA-MW6C, and MW09

Chloroform was also detected in the equipment blank associated with this SDG Methylene chloride was detected in the trip blank from one November 2012 ESC laboratory SDG (for the analysis of PE samples) at a concentration within tent times those of associated groundwater samples. The following Methylene chloride sample results were qualified as “U/non-detect at the concentrations reported” due to potential blank contamination bias. SDG Sample(s) Affected L608220 MW030 and MW-031 EQUIPMENT BLANK ANALYSES Forty-four equipment rinsate blanks were collected during the fourth quarter 2012 sampling event. Field blanks were not collected. Some VOCs, including, acetone, chloroform, methylene chloride, and TCE were detected in the equipment blanks at low concentrations, typically between

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the method detection limit (MDL) and the standard reporting limit (RL). Chloroform, TCE, and acetone were detected in the associated groundwater samples. Due to potential blank contamination bias, the following VOC results were qualified. Chloroform was detected in equipment blanks from six SDGs submitted to TestAmerica. Chloroform in the equipment blanks was reported at a concentration within five times those of associated groundwater samples. The following chloroform sample results were qualified as “U/non-detect at the concentrations reported” due to potential blank contamination bias. SDG Sample(s) Affected PVI1869 MW18, MW12, GCLake, IR3B, MW16, DUP001-09272012, MW15,

EPA-MW26A, MW25, EPA-MW62A, DUP002-09272012, and EPA-MW23A SDG Sample(s) Affected PVI1882 EPA-MW31A, EPA-MW30A, and EPA-MW50A SDG Sample(s) Affected PVI1723 IR26A, EPA-MW60A, EPA-MW45A, and DUP001-09252012 SDG Sample(s) Affected PVI1553 EPA-MW17C, EPA-MW54A, EPA-MW10C, DUP001-09212012, EPA-MW9C, EPA-MW18A, EPA-MW10A, EPA-MW38A, and EPA-MW16A SDG Sample(s) Affected PVJ0513 EPA-MW10C, EPA-MW10A, EPA-MW36A, EPA-MW11A, and EPA-MW9C SDG Sample(s) Affected PVK1911 EPA-MW26A, MW25, IR3B, and EPA-MW38A TCE was detected in equipment blanks from one October 2012 SDG at a concentration within five times those of associated groundwater samples. The following TCE sample results were qualified as “U/non-detect at the concentrations reported” due to potential blank contamination bias. SDG Sample(s) Affected PVJ1065 EPA-MW21 Acetone was detected in the equipment blanks from one TestAmerica SDG and from one Accutest at concentration within ten times those of associated groundwater samples (ten times rule for common laboratory contaminants). The following acetone sample results were qualified as “U/non-detect at the concentrations reported” due to potential blank contamination bias. SDG Sample(s) Affected PVI1869 EA07, EPA-MW62A, and GCLake SDG Sample(s) Affected C24140 EPA-MW15C

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Perchlorate was detected in equipment blanks from two September, one October, and one November 2012 TestAmerica SDGs at concentrations within five times those of associated groundwater samples (often within 2 to 3 times the blank results). Due to potential blank contamination bias, the following perchlorate sample results were qualified as “U/non-detect at the concentrations reported”. SDG Sample(s) Affected PVI0290 EPA-MW10A (Sept) SDG Sample(s) Affected PVI1060 EPA-MW2C, EPA-MW19C, EPA-MW4C, and EPA-MW8C SDG Sample(s) Affected PVHJ1237 COA18 SDG Sample(s) Affected PVK1911 IR3B No other bias in the sampling program is indicated by the results of the equipment blank analyses.

DECONTAMINATION WATER BLANK ANALYSES Decontamination water blanks were not collected during the fourth quarter 2012 sampling event.

LABORATORY QUALITY ASSURANCE/QUALITY CONTROL DATA The laboratory QA/QC program included evaluation of results from method blanks, matrix spike samples, laboratory control samples, and surrogate spike samples. Inorganic and organic quality control sample results were evaluated using project specified control limits, guidelines specified in SW-846, and applicable laboratory prescribed control limits.

METHOD BLANK ANALYSES Method blanks are prepared from analyte-free water to which all reagents are added in the same volumes and proportions as used in the sample processing. The objective of method blank analysis is to determine the existence and magnitude of potential contamination associated with laboratory methodologies for analysis of inorganic and organic parameters. Target analytes should not be detected in method blanks at concentrations above standard laboratory reporting limits. Method blank analyses were performed by TestAmerica, ESC, and Accutest laboratories in support of each analytical method performed for each sample batch analyzed. Perchlorate was not detected in any method blanks. Some target VOCs were detected in the method blanks at estimated concentrations (between the MDL and RL). These included acetone, methylene chloride, and chloroform. Acetone was the only one of these VOCs that was detected

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in associated samples, resulting in data qualifications. Acetone was also detected in the associated equipment blanks. Data qualified for acetone blank detections are summarized in the equipment blank section descried in the preceding pages.

LABORATORY CONTROL SAMPLE EVALUATION A laboratory control sample (LCS) is a known matrix spiked with compounds representative of the target analytes. Laboratory control samples are used for assessing the accuracy of a method (including any preparation steps) in a controlled matrix for inorganic and organic parameters. A laboratory control sample meeting recovery criteria provides evidence that the method, exclusive of sample matrix considerations, is in control. Laboratory control sample duplicate (LCSD) analyses may also be performed to demonstrate method precision in a controlled matrix. TestAmerica, Accutest, and ESC laboratories provided LCS and/or LCS/LCSD results for each method performed for each sample batch analyzed. All of the target VOCs for the Method 8260 analyses were included in the LCS spikes for each batch. For the fourth quarter 2012 VOC analyses, some LCS and/or LCSD analyses had target compound recoveries that were outside control limits, and biased high. The magnitude of the LCS excursions was generally small, typically within 5 percent of the stated control limits. VOCs with high LCS recoveries included benzene, toluene, ethylbenzene, xylenes, trichlorofluoromethane, carbon tetrachloride, and 1,1,2,2-tetrachloroethane. No validation action was required for VOCs with high LCS recoveries, unless that VOC was detected in the associated samples, indicating potential high bias. Acetone was the only VOC qualified in the fourth quarter due to high LCS recoveries. Acetone data were qualified as J/Estimated for the following PE samples in one November 2012 SDG from TestAmerica due to high LCS recoveries, as follows. SDG Sample(s) Affected PVK1726 MW030 and MW031 Some fourth quarter LCS and/or LCSD analyses had target compound recoveries that were outside control limits, and biased low. These included methylene chloride, 1,2-dichloropropane, PCE, and vinyl chloride. A low LCS recovery typically impacts all samples of the associated batch, as results for both detections and non-detects are qualified due to potential low bias. Several SDGs had sample results qualified due to low LCS recoveries, as follows: Methylene chloride data were qualified as “UJ/Estimated and non-detect at the reporting limits stated” for the following samples in one September 2012 SDG due to low LCS recoveries SDG Sample(s) Affected PVI0290 COG03, EPA-MW10A, EPA-MW10C, and EPA-MW9C 1,2-Dichloropropane data were qualified as “UJ/Estimated and non-detect at the reporting limits stated” for the following samples in one September 2012 SDG due to low LCS recoveries, as follows. SDG Sample(s) Affected PVI0290 EA05-EFF, EA05-MID, and EA05

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Methylene chloride data were qualified as “UJ/Estimated and non-detect at the reporting limits stated” for the following samples in one October 2012 SDG due to low LCS recoveries, as follows. SDG Sample(s) Affected PVJ0682 33A-102, 33A-201, 33A-EFF, 33A, EA-05-EFF, EA-05, EA-05-MID, EA-06-EFF, EA-06-INF, EA-06-MID, EA-08-EFF, EA-08, EA-08-MID, PH1-EFF, PH1-INF, PH23-EFF, and PH23-INF Vinyl chloride data were qualified as “UJ/Estimated and non-detect at the reporting limits stated” for the following samples in three October 2012 SDGs due to low LCS recoveries, as follows. SDG Sample(s) Affected PVJ1577 EPA-MW30A, EPA-MW50A, EPA-MW42A, DUP001, and MW12 SDG Sample(s) Affected PVJ1575 IR27C-170 and IR27C-258 SDG Sample(s) Affected PVJ1475 EPA-MW39C, EPA-MW39A, EPA-MW45A, EPA-MW54A, EPA-MW35A,

IR3B, EA07, EPA-MW59A, EPA-MW61A, IR34B, DUP001, GCLake, MW25, and EPA-MW38A

PCE data were qualified as “UJ/Estimated and non-detect at the reporting limits stated” for the following samples in one November 2012 SDG due to low LCS recoveries, as follows. SDG Sample(s) Affected PVK1450 LPW894, EPA-MW22C, EPA-MW55A, EPA-MW39C, EPA-MW39A,

EPA-MW45A, EPA-MW16C, and EPA-MW35A

Precision between LCS and LCSD recoveries was poor for acetone and 2-butanone in a several SDGs. Acetone and 2-butanone were not detected in the associated samples. The magnitude of the poor precision was often small (based on an RPD precision control limit of 25 percent), and no bias to the associated sample results was indicated. The contract laboratories flagged all analytical results with associated LCS excursions on the analytical results pages. The flags noted the possible bias direction, as required by the Arizona Department of Environmental Quality. Acetone LCS results were flagged “E4” for some reports because the spike result was less than the 20 ug/L reporting limit for acetone, with the amount spiked of 25 ug/L. Acetone LCS recoveries, calculated using the “estimated” result below the 20 ug/L reporting limit were within control limits, and no bias to the sample results was indicated. For the fourth quarter 2012 perchlorate analyses, precision and accuracy, as demonstrated by the LCS and LCSD analyses were determined to be acceptable.

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MATRIX SPIKE ANALYSES A matrix spike (MS) is defined as an aliquot of sample spiked with a known concentration of selected target analytes. MS duplicates (MSD) are intra-laboratory split samples spiked with identical concentrations of target analytes. The spiking occurs prior to sample preparation and analysis. The purpose of the MS and MSD analyses is to assess the effect of the sample matrices on laboratory accuracy and precision for inorganic and organic parameters. Organic analysis MS recoveries are considered advisory, and no validation action was performed for the fourth quarter groundwater 2012 investigation based solely on the results of MS recoveries reported outside of QC limits. Poor spike recoveries do not necessarily represent an error in the analytical system. It is possible that unavoidable interferences from the sample spiked preclude efficient recoveries. Other samples spike in the same batch, may not have the same matrix characteristics. Therefore, the organic MS/MSD data were used in conjunction with other quality control data (specifically LCS/LCSD results) to determine the overall quality and usability of the data. Matrix New World designated several project specific samples for MS and MSD analysis during the course of the fourth quarter 2012 groundwater investigation. In many cases, results from batch specific MS and MSD analyses were also provided in the same SDGs. Precision and accuracy, as demonstrated by MS/MSD data reported in support of the fourth quarter 2012 VOC analyses were acceptable, with some exceptions. MS and/or MSD recoveries were out of control and biased high for the following VOCs in one or more SDGs: Cis-1,2-DCE, trichlorofluoromethane, TCE, acetone, ethylbenzene, toluene, 1,1,2,2-tetrachloroethane, carbon tetrachloride, and chloroform. In the few cases where these VOCs were detected in the associated samples, the detections were often at concentrations between the MDL and RL, and the data were already qualified. Acceptable precision and accuracy for these VOCs was also demonstrated by the results of the LCS and LCSD analyses. MS and/or MSD recoveries were out of control and biased low for the following VOCs in one or more SDGs: Methylene chloride, m/p-xylenes, and ethylbenzene. The magnitude of the low recoveries was generally small, within 5 of the lower laboratory recovery control limit. In cases with low MS and MSD recoveries, the associated LCS and LCSD recoveries typically demonstrated acceptable precision and accuracy, and the VOC data were not qualified (one exception was for methylene chloride, where the associated LCS recoveries were also low and the methylene chloride results were qualified). For one SDG, TCE spike recoveries were out of control, where the TCE concentration in the sample spiked was more than four times greater than the spike added amount. No action was taken in these cases, as the representativeness of the spike recovery is diminished in this scenario. MS and MSD recoveries for perchlorate were within prescribed control limits of 75 to 125 percent for all fourth quarter 2012 analyses.

SURROGATE SPIKE ANALYSIS A surrogate is an organic compound which is similar to method target analytes in chemical composition and behavior in the analytical process, but which is not normally found in groundwater samples. For all VOC analyses and dilution analyses, each field sample, QC sample, and blank was

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spiked with three surrogate compounds prior to purging or extraction. Surrogate recoveries were calculated to evaluate the ability of the analytical procedures to recover the true amount of a known compound in the sample matrix. Surrogate recoveries were reported in support of all VOC analyses performed for the fourth quarter 2012 groundwater monitoring event. Surrogate recoveries were within laboratory-prescribed control limits, with the following exceptions. Surrogate recoveries for three samples in two ESC SDGs were low for samples where no VOCs were detected. VOC results for these samples were qualified as “UJ/Estimated and non-detect at the reporting limits stated” due to potential low bias, as follows: SDG Sample(s) Affected L596529 (ESC) DUP001-09182012 and EPA-MW13A (all VOCs = UJ) SDG Sample(s) Affected L600820 (ESC) EPA-MW12C (all VOCs = UJ) During late October 2012, and during all of November 2012, TestAmerica reported high surrogates for nearly all samples in nearly all SDGs. Many 4-bromofluorobenzene (4-BFB) surrogates were high, exceeding the 114 percent upper project control limit. Many toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit. One dibromofluoromethane surrogate was high, exceeding 130 percent. VOCs detected in these samples were qualified as J/Estimated due to potential high bias. In nearly all of these cases, the surrogates in question were well within current statistically-derived TestAmerica laboratory control limits. Therefore, the laboratory did not perform any corrective actions for these SDGs, based on the exceedences of the project control limits. It is noted, that during December 2012, TestAmerica regained control of these surrogates to levels again meeting project control limits. Therefore, these potential high biases are generally limited to the November 2012 timeframe. The following SDGs and samples had qualified VOC results due to high surrogates. SDG Sample(s) Affected PVJ1577 MW12 (PCE = J) SDG Sample(s) Affected PVK1375 MW13, EPA-MW17C, EPA-MW18A, EA06, and EPA-MW23A

(Chloroform = J) EPA-MW53A (Acetone = J) EPA-MW18A (PCE = J)

EA06, EPA-MW23A, DUP002 (TCE = J) SDG Sample(s) Affected PVK1288 EPA-MW41A (Chloroform = J) SDG Sample(s) Affected PVK1286 EA06-EFF, EA06-MID, EA06-INF, EA08-EFF, EA08-MID, and

EA08-INF (Chloroform = J) EA06-MID, EA06-INF, EA08-MID, and EA08-INF (TCE = J)

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SDG Sample(s) Affected PVK1220 EPA-MW44A, MW17, EPA-MW20A, and EPA-MW37A (Chloroform =J)

EPA-MW20A (TCE and PCE= J) SDG Sample(s) Affected PVK0684 EPA-MW11A, EPA-MW58A, EPA-MW10A and DUP001 (PCE = J)

EPA-MW58A, EPA-MW10C, EPA-MW9C, EPA-MW10A and DUP001 (TCE = J)

SDG Sample(s) Affected PVK0632 PH1-INF, PH23-INF, EA05-MID, EA05-INF, EA06-MID, EA06-INF and

33A-INF (TCE = J) EA06-MID, EA06-INF and 33A-202 (Chloroform = J)

SDG Sample(s) Affected PVK1912 IR27C-170 and IR27C-258 (Chloroform and TCE = J) IR27A-180 (Chloroform and PCE = J) SDG Sample(s) Affected PVK1911 EPA-MW60A, IR26A, EPA-MW30A, and MW12 (Chloroform and TCE = J)

DUP001, EPA-MW49C, GCLake (Chloroform = J) EPA-MW50A (PCE = J) IR3B and EPA-MW38A (TCE = J)

SDG Sample(s) Affected PVK1726 MW031 (Acetone, Chloroform, PCE, and TCE = J) SDG Sample(s) Affected PVK1721 MW18, EPA-MW31A, MW15, MW16, EPA-MW25A, and

EPA-MW42A (TCE = J) EPA-MW31A (PCE = J) SDG Sample(s) Affected PVK1630 APS-MW03, EPA-MW21A, DUP001, and EPA-MW34A (TCE = J) SDG Sample(s) Affected PVK1450 EPA-MW35A, EA02, EA07, EPA-MW16A, DUP001, EPA-MW62A, MW19 and MW09 (TCE = J) EA02 (Toluene and Acetone = J)

RESULTS QUANTITATION Sample results were evaluated to determine if sample dilutions were appropriate, and to evaluate sample reporting limits in terms of sensitivity DQOs. For the VOC analyses, several dilutions were required to bring target VOCs into linear range for quantitation. In general, only the VOCs exceeding the undiluted calibration range (200 ug/L for most VOCs) were reported from dilutions. The sensitivity DQO for the VOC analyses was satisfied, with the following considerations.

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Beginning with the second quarter 2007 sampling event, the contract laboratory was required to report all VOC detections quantified between the MDL and the RL. Reporting to the MDL was performed for a selected set of 19 target VOCs. These VOCs were noted with an “E8” flag in the TestAmerica reports. Any detections between the MDL and standard RL were flagged with an “E4” qualifier by TestAmerica or a “J” qualifier by ESC and Accutest Laboratories. Several VOCs were reported as detections in this range, and all of these were qualified as J/Estimated due to potential limited accuracy in this portion of the calibration range (some of the VOCs detected in this range were then superceded by the “U/non-detect” qualifier in SDGs, where blank contamination was also associated with the sample detections). Chloroform (93 samples), TCE (23 samples), PCE (23 samples), 1,1-DCE (16 samples), acetone (6 samples), and carbon tetrachloride (4 samples) were the most common VOCs detected at concentrations between the MDL and RL. Other VOCs detected one or more times between the MDL and RL included cis-1,2-DCE, toluene, and 2-butanone. For many of the fourth quarter 2012 laboratory reports, perchlorate detections were reported at concentrations less than the standard 2 ug/L TestAmerica reporting limit (which is also the project sensitivity goal of 2 ug/L), but at concentrations greater than the MDL. TestAmerica laboratory noted each case and flagged the perchlorate results with an “E4”. Due to limited accuracy in this portion of the calibration curve, 14 perchlorate sample results were qualified as J/Estimated. ESC laboratory performed nearly all perchlorate analyses at dilutions, due to stated matrix interferences. In most of these samples, no perchlorate was detected. A five times dilution from ESC results in a reporting limit of 2.5 ug/L for perchlorate (compared to the 2.0 ug/L TestAmerica reporting limit with no dilution).

DATA QUALIFICATION DISCUSSION During the fourth quarter 2012, many VOC data were qualified as a result of high surrogate recoveries reported during November 2012. The laboratory did not perform corrective action for the surrogate excursions, as the recoveries were well within laboratory derived control limits. The high recoveries exceeded project specific control limits for surrogates toluene-d8 (upper control limit of 111 percent) and 4-bromofluorobenzene (upper control limit of 114 percent). By comparison, only one sample exceeded the dibromofluoromethane surrogate project control limit of 130 percent. Results for samples reviewed from December 2012, indicated that TestAmerica was again in control, with respect to project specified surrogate control limits for all three surrogates. TestAmerica continues to note that some MDLs have changed relative to project requirements, due to updates from ongoing MDL studies. A large portion of the VOC detections for PGAN groundwater samples are at concentrations between the MDL and the standard laboratory reporting limits. If current study-derived laboratory MDLs are higher then the required project MDLs, then some of the VOC detections reported as “J” or “E4” values may be more statistically valid as non-detects. The blank evaluation is nominally based on “factors of safety” such that VOC detections in groundwater samples within five times those in associated blanks (or ten times for common laboratory contaminants acetone and methylene chloride), are qualified as “U/non-detect at the concentration reported.” Such factors of safety prevent false positive data points from being incorporated into the site evaluation. In practice, for the PGAN project, these five and ten times

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outer limits for data evaluation against blank contamination were rarely tested. It was far more common that blank detections were at concentrations within a factor of 2 to 3 times those of the associated qualified groundwater sample results. In some cases, blank detections were reported at concentrations higher than those of the samples in question. Many VOCs results qualified due to associated blank contamination, already had initially lower data quality, as they were reported at concentrations between the MDL an RL of the analysis. LEVEL 4 DATA EVALUATION Results from eight level 4 (full quality control deliverables) data packages were evaluated for SDGs from September, October, and November 2012. One level 4 SDG from November 2012 will be re-submitted in the 1st Quarter 2013, due to missing data in the initial delivery.

The level 4 data packages were evaluated for each of the Level 3 QC elements described above, with the addition of the following:

Gas chromatography/Mass spectroscopy instrument tuning (VOCs) Initial calibration and initial calibration verification Continuing calibration verification Internal standards, area and retention times (VOCs) Chromatogram review Raw data review GCMS instrument use Standards Preparation

VOCs – GC/MS tunes were reported in the raw data at frequencies such that all water sample analyses and QC sample analyses were bracketed by successful tunes every 12 hours. Results from nine-point initial calibrations were provided in support of all VOC analyses. For the data packages reviewed, one or two initial calibrations were associated with the samples in each SDG. Up to four continuing calibrations were provided with each initial calibration. Initial calibrations and sample analyses were performed by TestAmerica on GC/MS instruments #2, #4, #7, and #9. No bias was noted based on comparison of sample results and quality control results between the different instruments used on the PGAN project. Response factors and percent relative standard deviations (%RSD) were evaluated for each calibration. Based on the level 4 data review, groundwater sample results for 2-butanone were qualified in the approximately half of the data sets reviewed due to low response factors. The initial calibration response factors for 2-butanone were less than the minimum criteria of 0.05 used for all other project target VOCs. Continuing calibration response factors for 2-butanone were also low for the SDGs where the initial calibration response was low. 2-Butanone was not detected in the associated groundwater samples, and 2-butanone results for these SDGs were qualified as R/Rejected. 2-Butanone in known to be a poor performing calibration constituent due to low purge efficiency. As such, a lower response factor of 0.01 is allowed by the method for 2-butanone (and other poor performers) in the initial and continuing calibrations so that the calibrations can pass. However, for data validation purposes, the 2-butanone results are evaluated against the same calibration criteria as those for the other target VOCs, so that the data quality comparison is equivalent.

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For VOCs with %RSDs greater than 15 percent, linear or quadratic calibrations were performed. Associated linear correlation coefficients were determined to be acceptable with correlation coefficients greater than 0.995. Quadratic curves for acetone and 2-butanone were evaluated against a calibration coefficient of greater than 0.99 The initial calibrations were acceptable for all other short list VOC target compounds. It is noted that two to four of the low level calibration standards for acetone and/or 2-butanone were omitted from the calibration curves in order to improve response factors and RSDs. This resulted in an elevated reporting limit provided for acetone (20 ug/L) in the data packages. Results from initial calibration verifications (ICV - second source standards at concentrations of 25 ug/L and 20 ug/L) were provided with each initial calibration. ICV recoveries were within prescribed control limits for each calibration. Percent deviations between average response in the initial calibration and those in the second source standards were less than 25 percent. Continuing calibrations were evaluated for each day of groundwater sample analysis. Continuing calibration standard recoveries were within specified laboratory control limits for all target VOCs. Percent differences between responses factors in initial and continuing calibrations were less than 25 percent for target VOCs, with the exception of acetone in one SDG. These VOCs were qualified as “UJ/Estimated and non-detect at the reporting limits stated” due to the high percent differences. Response factors for VOCs in continuing calibrations were greater than 0.05, with some exceptions for 2-butanone. In each of these cases, 2-butanone was qualified due to the initial calibration. The raw data for each sample was reviewed. Ion chromatograms and GC/MS specta were checked for VOC target compound detections. Results quantitation was determined to be acceptable, based on these reviews. Final reported concentrations matched the raw data values and sample dilutions were properly accounted for. Perchlorate – All groundwater perchlorate results were quantified based on a 5-point initial calibration. Initial calibrations dated May 29, 2012 and September 26, 2012 were referenced for most perchlorate analyses reported for the fourth quarter 2012. The linearity for each of the initial calibrations was acceptable, and no data were qualified based on calibrations. Correlation coefficients for each 5-point calibration were greater than 0.995. Initial calibration check standards (ICCS), continuing/ending calibrations check standard (CCCS/ECCS), and instrument performance check (IPC) standards, and second source standards were analyzed at various concentrations within each analytical batch (typically 2 ug/L, 25 ug/L, and 40 ug/L). The calibration standard recoveries were evaluated based on 85 to 115 percent recovery criteria. IPC standards were evaluated at 80 to 120 percent. ICCS standards were evaluated based on control limits of 75 to 125 percent. No perchlorate data required qualification based on the results of the continuing calibration analyses. It was noted that in some SDGs, several ICCS had recoveries of greater than 125 percent, and several analyses were required to obtain an acceptable ICCS. All ion chromatograms were reviewed and raw data were checked against the final reported values. Final reported concentrations matched the raw data values. No other data quality issues were identified based on the results of the level 4 validation review.

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DATA USABILITY There were no significant data usability issues noted for the fourth quarter 2012 groundwater sampling events, with the following considerations. For samples collected in November 2012, all VOC detections from TestAmerica laboratory were qualified due to elevated surrogate recoveries. Many 4-bromofluorobenzene surrogate recoveries were high, exceeding the 114 percent upper project control limit. Many toluene-d8 surrogate recoveries were also high, exceeding the 111 percent upper control limit. VOCs detected in these samples were qualified as J/Estimated due to potential high bias. In nearly all of these cases, the surrogates in question were well within current statistically-derived TestAmerica laboratory control limits. Therefore, the laboratory did not perform any corrective actions for these SDGs, based on the exceedences of the project control limits. A review of several SDGs from December 2012 indicates that these surrogate recoveries were back in control, relative to project specific control limits.

DATA QUALITY SUMMARY Based on the review of the analytical reports provided by TestAmerica, Accutest, and ESC laboratories, the data reported for the fourth quarter 2012 groundwater sampling events at the PGA North site are determined to be quantitative and usable, with the considerations noted herein and detailed in the SDG-specific validation reports. Completeness objectives for the analyses performed during the fourth quarter 2012 meet the project DQOs for data usability, with the possible exception of that for 2-butanone. 2-Butanone results were qualified as R/Rejected for non-detect concentrations in over half of the level 4 data packages evaluated due to poor responses in the initial calibrations and continuing. Removal of the lowest concentration calibration points (up to four points) for acetone and 2-butanone in the initial calibrations often improved the average response to acceptable levels, though with increased reporting limits.

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LCS %R1,1,1-Trichloroethane

Limits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0235-BS1 29.9 1202511/7/12 83.2-12011/7/12 CQC

12K0286-BS1 25.4 1022511/8/12 83.2-12011/8/12 CQC

12K0341-BS1 24.4 982511/9/12 83.2-12011/9/12

12K0415-BS1 23.8 952511/12/12 83.2-12011/12/12 CQC

12K0462-BS1 27.6 1102511/13/12 83.2-12011/13/12 CQC

12K0522-BS1 28.2 1132511/14/12 83.2-12011/14/12 CQC

12K0803-BS1 26.7 1072511/21/12 83.2-12011/21/12 CQC

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LCS/LCSD RPD1,1,1-Trichloroethane

%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

11528.82511/7/1211/7/1212K0235-BSD1 29.9 120 4 25 CQC

10025.12511/8/1211/8/1212K0286-BSD1 25.4 102 1 25 CQC

9824.62511/9/1211/9/1212K0341-BSD1 24.4 98 0.8 25

9423.62511/12/1211/12/1212K0415-BSD1 23.8 95 0.9 25 CQC

11528.82511/13/1211/13/1212K0462-BSD1 27.6 110 5 25 CQC

11328.32511/14/1211/14/1212K0522-BSD1 28.2 113 0.1 25 CQC

112282511/21/1211/21/1212K0803-BSD1 26.7 107 5 25 CQC

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MS %R1,1,1-Trichloroethane

Source%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC,PSL81.4-125PVK0237-0112631.512K0235-MS1 11/7/12 11/7/12 25

CQC81.4-125PVK0555-0412130.312K0286-MS1 11/8/12 11/8/12 25

81.4-125PVK0649-069924.712K0341-MS1 11/9/12 11/9/12 25

CQC81.4-125PVK0756-019824.612K0415-MS1 11/12/12 11/12/12 25

CQC81.4-125PVK0793-0211629.112K0462-MS1 11/13/12 11/13/12 25

CQC81.4-125PVK0281-0111328.212K0522-MS1 11/14/12 11/14/12 25

CQC81.4-125PVK1220-0211428.412K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPD1,1,1-Trichloroethane

%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

12932.22511/7/1211/7/1212K0235-MSD1 CQC,PSL25212631.5 PVK0237-01

11428.52511/8/1211/8/1212K0286-MSD1 CQC25612130.3 PVK0555-04

10025.12511/9/1211/9/1212K0341-MSD1 2529924.7 PVK0649-06

9924.82511/12/1211/12/1212K0415-MSD1 CQC250.69824.6 PVK0756-01

11428.52511/13/1211/13/1212K0462-MSD1 CQC25211629.1 PVK0793-02

116292511/14/1211/14/1212K0522-MSD1 CQC25311328.2 PVK0281-01

12330.62511/21/1211/21/1212K0803-MSD1 CQC25811428.4 PVK1220-02

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BLK1,1,1-Trichloroethane

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Analyzed By:

LCS %R1,1,2,2-Tetrachloroethane


12I0005-BS1 26.6 106259/1/12 70.5-1259/1/12 CQC

12I0028-BS1 24.1 96259/4/12 70.5-1259/4/12 CQC

12I0081-BS1 24.9 100259/5/12 70.5-1259/5/12 CQC

12I0215-BS1 23.1 92259/7/12 70.5-1259/7/12 CQC

12I0352-BS1 25.1 100259/12/12 70.5-1259/12/12 CQC

12I0394-BS1 22.3 89259/12/12 70.5-1259/12/12 CQC

12I0598-BS1 29.3 117259/18/12 70.5-1259/18/12 CQC

12I0648-BS1 27.4 110259/18/12 70.5-1259/18/12 CQC

12I0926-BS1 28.4 114259/25/12 70.5-1259/25/12 CQC

12I0925-BS1 28.7 115259/25/12 70.5-1259/25/12 CQC

12I1065-BS1 26.1 104259/28/12 70.5-1259/28/12 CQC

12I1095-BS1 23.7 95259/28/12 70.5-1259/28/12 CQC

12I1107-BS1 26.1 104259/29/12 70.5-1259/29/12 CQC

12J0008-BS1 26.9 1072510/1/12 70.5-12510/1/12 CQC

12J0298-BS1 25.5 1022510/8/12 70.5-12510/8/12

12J0389-BS1 26.1 1042510/10/12 70.5-12510/10/12

12J0445-BS1 26.8 1072510/11/12 70.5-12510/11/12 CQC

12J0620-BS1 22.6 912510/16/12 70.5-12510/16/12 CQC

12J0736-BS1 22.5 902510/18/12 70.5-12510/18/12 CQC

12J0821-BS1 27.4 1102510/20/12 70.5-12510/20/12 CQC

12J0850-BS1 24.9 1002510/22/12 70.5-12510/22/12 CQC

12J0972-BS1 26.4 1052510/24/12 70.5-12510/24/12 CQC

12J1010-BS1 25.1 1002510/25/12 70.5-12510/25/12 CQC

12J1038-BS1 27.1 1092510/25/12 70.5-12510/25/12 CQC

12J1059-BS1 27.2 1092510/26/12 70.5-12510/26/12 CQC

12K0235-BS1 31 1242511/7/12 70.5-12511/7/12 CQC

12K0286-BS1 25.4 1022511/8/12 70.5-12511/8/12 CQC

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LCS %R1,1,2,2-TetrachloroethaneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 22.8 912511/9/12 70.5-12511/9/12

12K0415-BS1 21.2 852511/12/12 70.5-12511/12/12 CQC

12K0462-BS1 26.8 1072511/13/12 70.5-12511/13/12 CQC

12K0522-BS1 32 1282511/14/12 70.5-12511/14/12 CQC,L

12K0553-BS1 26.5 1062511/14/12 70.5-12511/14/12 CQC

12K0552-BS1 24.5 982511/14/12 70.5-12511/14/12 CQC

12K0581-BS1 27 1082511/15/12 70.5-12511/15/12 CQC

12K0740-BS1 29 1162511/20/12 70.5-12511/20/12 CQC

12K0751-BS1 25.6 1022511/20/12 70.5-12511/20/12 CQC

12K0789-BS1 29.3 1172511/20/12 70.5-12511/20/12

12K0803-BS1 26.8 1072511/21/12 70.5-12511/21/12 CQC

12K0836-BS1 28.9 1152511/21/12 70.5-12511/21/12 CQC

12K0855-BS1 28.2 1132511/23/12 70.5-12511/23/12 CQC

12K0865-BS1 25.9 1042511/23/12 70.5-12511/23/12 CQC

12K0897-BS1 30.6 1232511/24/12 70.5-12511/24/12 CQC

12K0905-BS1 29.4 1182511/25/12 70.5-12511/25/12 CQC

12K1134-BS1 25 1002511/30/12 70.5-12511/30/12 CQC

12K1135-BS1 26.8 1072511/30/12 70.5-12511/30/12 CQC

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LCS/LCSD RPD1,1,2,2-Tetrachloroethane


9122.8259/1/129/1/1212I0005-BSD1 26.6 106 15 25 CQC

10325.7259/4/129/4/1212I0028-BSD1 24.1 96 7 25 CQC

8621.6259/5/129/5/1212I0081-BSD1 24.9 100 14 25 CQC

9022.6259/7/129/7/1212I0215-BSD1 23.1 92 2 25 CQC

10626.6259/12/129/12/1212I0352-BSD1 25.1 100 6 25 CQC

10125.2259/12/129/12/1212I0394-BSD1 22.3 89 12 25 CQC

12230.6259/18/129/18/1212I0598-BSD1 29.3 117 4 25 CQC

10526.3259/18/129/18/1212I0648-BSD1 27.4 110 4 25 CQC

10325.8259/25/129/25/1212I0926-BSD1 28.4 114 10 25 CQC

10826.9259/25/129/25/1212I0925-BSD1 28.7 115 7 25 CQC

9724.3259/28/129/28/1212I1065-BSD1 26.1 104 7 25 CQC

10526.3259/28/129/28/1212I1095-BSD1 23.7 95 10 25 CQC

9624259/29/129/29/1212I1107-BSD1 26.1 104 8 25 CQC

11328.32510/1/1210/1/1212J0008-BSD1 26.9 107 5 25 CQC

10125.22510/8/1210/8/1212J0298-BSD1 25.5 102 1 25

10426.12510/10/1210/10/1212J0389-BSD1 26.1 104 0.2 25

10826.92510/11/1210/11/1212J0445-BSD1 26.8 107 0.3 25 CQC

9924.82510/16/1210/16/1212J0620-BSD1 22.6 91 9 25 CQC

9022.42510/18/1210/18/1212J0736-BSD1 22.5 90 0.4 25 CQC

10024.92510/20/1210/20/1212J0821-BSD1 27.4 110 10 25 CQC

9323.22510/22/1210/22/1212J0850-BSD1 24.9 100 7 25 CQC

9423.52510/24/1210/24/1212J0972-BSD1 26.4 105 11 25 CQC

10526.32510/25/1210/25/1212J1010-BSD1 25.1 100 5 25 CQC

10927.22510/25/1210/25/1212J1038-BSD1 27.1 109 0.07 25 CQC

10726.82510/26/1210/26/1212J1059-BSD1 27.2 109 2 25 CQC

11428.42511/7/1211/7/1212K0235-BSD1 31 124 9 25 CQC

10626.52511/8/1211/8/1212K0286-BSD1 25.4 102 4 25 CQC

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LCS/LCSD RPD1,1,2,2-Tetrachloroethane%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

9323.42511/9/1211/9/1212K0341-BSD1 22.8 91 3 25

8521.42511/12/1211/12/1212K0415-BSD1 21.2 85 0.8 25 CQC

11227.92511/13/1211/13/1212K0462-BSD1 26.8 107 4 25 CQC

13132.92511/14/1211/14/1212K0522-BSD1X 32 128 3 25 CQC,L

9523.82511/14/1211/14/1212K0553-BSD1 26.5 106 11 25 CQC

9924.92511/14/1211/14/1212K0552-BSD1 24.5 98 1 25 CQC

10726.72511/15/1211/15/1212K0581-BSD1 27 108 1 25 CQC

11228.12511/20/1211/20/1212K0740-BSD1 29 116 3 25 CQC

10125.22511/20/1211/20/1212K0751-BSD1 25.6 102 1 25 CQC

116292511/20/1211/20/1212K0789-BSD1 29.3 117 1 25

11829.62511/21/1211/21/1212K0803-BSD1 26.8 107 10 25 CQC

10426.12511/21/1211/21/1212K0836-BSD1 28.9 115 10 25 CQC

12731.72511/23/1211/23/1212K0855-BSD1 28.2 113 12 25 CQC,PSL

100252511/23/1211/23/1212K0865-BSD1 25.9 104 4 25 CQC

12130.32511/24/1211/24/1212K0897-BSD1 30.6 123 1 25 CQC

11328.42511/25/1211/25/1212K0905-BSD1 29.4 118 4 25 CQC

10526.32511/30/1211/30/1212K1134-BSD1 25 100 5 25 CQC

10526.22511/30/1211/30/1212K1135-BSD1 26.8 107 2 25 CQC

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MS %R1,1,2,2-Tetrachloroethane


CQC70.4-124PVH2309-0210225.412I0005-MS1 9/1/12 9/1/12 25

CQC70.4-124PVH2309-1110927.312I0028-MS1 9/4/12 9/4/12 25

CQC70.4-124PVH2037-078120.212I0081-MS1 9/5/12 9/5/12 25

CQC70.4-124PVI0290-039924.712I0215-MS1 9/7/12 9/7/12 25

CQC70.4-124PVI0609-0910125.212I0352-MS1 9/12/12 9/12/12 25

CQC70.4-124PVI0525-069423.412I0394-MS1 9/12/12 9/12/12 25

CQC70.4-124PVI0894-0612029.912I0598-MS1 9/18/12 9/18/12 25

CQC70.4-124PVI1060-029924.812I0648-MS1 9/18/12 9/18/12 25

CQC70.4-124PVI1553-081002512I0925-MS1 9/25/12 9/25/12 25

CQC70.4-124PVI1510-0810125.312I0926-MS1 9/25/12 9/25/12 25

CQC70.4-124PVI1723-0310626.512I1065-MS1 9/28/12 9/28/12 25

CQC70.4-124PVI1822-029924.712I1095-MS1 9/28/12 9/28/12 25

CQC70.4-124PVI1869-0510426.112I1107-MS1 9/29/12 9/29/12 25

CQC70.4-124PVI1575-0110927.212J0008-MS1 10/1/12 10/1/12 25

70.4-124PVJ0513-039824.412J0298-MS1 10/8/12 10/8/12 25

70.4-124PVJ0682-0110325.712J0389-MS1 10/10/12 10/10/12 25

CQC70.4-124PVJ0682-179824.512J0445-MS1 10/11/12 10/11/12 25

CQC70.4-124PVJ1065-028922.212J0620-MS1 10/16/12 10/16/12 25

CQC70.4-124PVJ1237-029122.812J0736-MS1 10/18/12 10/18/12 25

CQC70.4-124PVJ1405-0211127.712J0821-MS1 10/20/12 10/20/12 25

CQC70.4-124PVJ1405-179423.612J0850-MS1 10/22/12 10/22/12 25

CQC70.4-124PVJ1577-029724.212J0972-MS1 10/24/12 10/24/12 25

CQC70.4-124PVJ1627-018420912J1010-MS1 10/25/12 10/25/12 250

CQC70.4-124PVJ1600-029924.812J1038-MS1 10/25/12 10/25/12 25

CQC70.4-124PVJ1577-18RE111027412J1059-MS1 10/26/12 10/26/12 250

CQC70.4-124PVK0237-0110927.212K0235-MS1 11/7/12 11/7/12 25

CQC70.4-124PVK0555-041082712K0286-MS1 11/8/12 11/8/12 25

70.4-124PVK0649-0610225.512K0341-MS1 11/9/12 11/9/12 25

CQC70.4-124PVK0756-019523.812K0415-MS1 11/12/12 11/12/12 25

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MS %R1,1,2,2-TetrachloroethaneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC70.4-124PVK0793-0210225.512K0462-MS1 11/13/12 11/13/12 25

CQC70.4-124PVK0281-0110827.1X 12K0522-MS1 11/14/12 11/14/12 25

CQC70.4-124PVK0632-099924.812K0553-MS1 11/14/12 11/14/12 25

CQC70.4-124PVK0684-02962412K0552-MS1 11/14/12 11/14/12 25

CQC70.4-124PVK0696-011042612K0581-MS1 11/15/12 11/15/12 25

CQC70.4-124PVK0934-0110325.812K0740-MS1 11/20/12 11/20/12 25

CQC70.4-124PVK0768-0211127.712K0751-MS1 11/20/12 11/20/12 25

CQC70.4-124PVK1220-0211729.4X 12K0803-MS1 11/21/12 11/21/12 25

CQC70.4-124PVK1288-0311829.412K0836-MS1 11/21/12 11/21/12 25

CQC70.4-124PVK1375-089924.812K0865-MS1 11/23/12 11/23/12 25

CQC,M1470.4-124PVK1375-0213032.412K0855-MS1 11/23/12 11/23/12 25

CQC70.4-124PVK0988-0311328.212K0897-MS1 11/24/12 11/24/12 25

CQC70.4-124PVK1006-0112531.212K0905-MS1 11/25/12 11/25/12 25

CQC70.4-124PVK1450-109924.812K1135-MS1 11/30/12 11/30/12 25

CQC70.4-124PVK1450-0311929.712K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPD1,1,2,2-Tetrachloroethane


10225.5259/1/129/1/1212I0005-MSD1 CQC250.110225.4 PVH2309-02

11228259/4/129/4/1212I0028-MSD1 CQC25310927.3 PVH2309-11

9323.2259/5/129/5/1212I0081-MSD1 CQC25148120.2 PVH2037-07

9824.6259/7/129/7/1212I0215-MSD1 CQC250.49924.7 PVI0290-03

10827259/12/129/12/1212I0352-MSD1 CQC25710125.2 PVI0609-09

9824.6259/12/129/12/1212I0394-MSD1 CQC2559423.4 PVI0525-06

11929.8259/18/129/18/1212I0598-MSD1 CQC250.512029.9 PVI0894-06

9523.7259/18/129/18/1212I0648-MSD1 CQC2549924.8 PVI1060-02

9924.8259/25/129/25/1212I0925-MSD1 CQC250.710025 PVI1553-08

10325.7259/25/129/25/1212I0926-MSD1 CQC25210125.3 PVI1510-08

10325.8259/28/129/28/1212I1065-MSD1 CQC25310626.5 PVI1723-03

11228259/28/129/28/1212I1095-MSD1 CQC25129924.7 PVI1822-02

11729.4259/29/129/29/1212I1107-MSD1 CQC251210426.1 PVI1869-05

11127.82510/1/1210/1/1212J0008-MSD1 CQC25210927.2 PVI1575-01

10025.12510/8/1210/8/1212J0298-MSD1 2539824.4 PVJ0513-03

9824.42510/10/1210/10/1212J0389-MSD1 25510325.7 PVJ0682-01

9423.52510/11/1210/11/1212J0445-MSD1 CQC2549824.5 PVJ0682-17

8521.42510/16/1210/16/1212J0620-MSD1 CQC2548922.2 PVJ1065-02

9222.92510/18/1210/18/1212J0736-MSD1 CQC250.69122.8 PVJ1237-02

11528.82510/20/1210/20/1212J0821-MSD1 CQC25411127.7 PVJ1405-02

100252510/22/1210/22/1212J0850-MSD1 CQC2569423.6 PVJ1405-17

11027.42510/24/1210/24/1212J0972-MSD1 CQC25129724.2 PVJ1577-02

9223025010/25/1210/25/1212J1010-MSD1 CQC25984209 PVJ1627-01

10425.92510/25/1210/25/1212J1038-MSD1 CQC2549924.8 PVJ1600-02

11528825010/26/1210/26/1212J1059-MSD1 CQC255110274 PVJ1577-18RE1

11528.72511/7/1211/7/1212K0235-MSD1 CQC25610927.2 PVK0237-01

10927.32511/8/1211/8/1212K0286-MSD1 CQC25110827 PVK0555-04

96242511/9/1211/9/1212K0341-MSD1 25610225.5 PVK0649-06

9523.72511/12/1211/12/1212K0415-MSD1 CQC250.49523.8 PVK0756-01

12531.22511/13/1211/13/1212K0462-MSD1 CQC,M7252010225.5 PVK0793-02

11629.12511/14/1211/14/1212K0522-MSD1X CQC25710827.1 PVK0281-01

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MS/MSD RPD1,1,2,2-Tetrachloroethane%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

108272511/14/1211/14/1212K0553-MSD1 CQC2599924.8 PVK0632-09

10325.82511/14/1211/14/1212K0552-MSD1 CQC2579624 PVK0684-02

10325.82511/15/1211/15/1212K0581-MSD1 CQC250.410426 PVK0696-01

10726.72511/20/1211/20/1212K0740-MSD1 CQC25410325.8 PVK0934-01

11027.52511/20/1211/20/1212K0751-MSD1 CQC250.711127.7 PVK0768-02

11528.82511/21/1211/21/1212K0803-MSD1X CQC25211729.4 PVK1220-02

11929.82511/21/1211/21/1212K0836-MSD1 CQC25111829.4 PVK1288-03

9423.62511/23/1211/23/1212K0865-MSD1 CQC2559924.8 PVK1375-08

11127.82511/23/1211/23/1212K0855-MSD1 CQC251513032.4 PVK1375-02

12330.82511/24/1211/24/1212K0897-MSD1 CQC25911328.2 PVK0988-03

120302511/25/1211/25/1212K0905-MSD1 CQC25412531.2 PVK1006-01

10125.22511/30/1211/30/1212K1135-MSD1 CQC2519924.8 PVK1450-10

11528.72512/1/1211/30/1212K1134-MSD1 CQC25411929.7 PVK1450-03

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BLK1,1,2,2-Tetrachloroethane

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0.0 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

Plotted: 44

MDL: 0.12

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

3s: 0

4s: 0

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LCS %R1,1,2-Trichloroethane


12K0235-BS1 30.4 1222511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 26.6 1062511/8/12 85-11511/8/12 CQC

12K0341-BS1 24.5 982511/9/12 85-11511/9/12

12K0415-BS1 26.1 1042511/12/12 85-11511/12/12 CQC

12K0462-BS1 28 1122511/13/12 85-11511/13/12 CQC

12K0522-BS1 26.3 1052511/14/12 85-11511/14/12 CQC

12K0803-BS1 22.6 902511/21/12 85-11511/21/12 CQC

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LCS/LCSD RPD1,1,2-Trichloroethane


11729.22511/7/1211/7/1212K0235-BSD1 30.4 122 4 25 CQC,PSL

10726.62511/8/1211/8/1212K0286-BSD1 26.6 106 0.1 25 CQC

9824.52511/9/1211/9/1212K0341-BSD1 24.5 98 0.1 25

100252511/12/1211/12/1212K0415-BSD1 26.1 104 4 25 CQC

10726.82511/13/1211/13/1212K0462-BSD1 28 112 4 25 CQC

10726.72511/14/1211/14/1212K0522-BSD1 26.3 105 2 25 CQC

10024.92511/21/1211/21/1212K0803-BSD1 22.6 90 10 25 CQC

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MS %R1,1,2-Trichloroethane


CQC,PSL77.5-118PVK0237-0112631.512K0235-MS1 11/7/12 11/7/12 25

CQC77.5-118PVK0555-0411629.112K0286-MS1 11/8/12 11/8/12 25

77.5-118PVK0649-0610125.412K0341-MS1 11/9/12 11/9/12 25

CQC77.5-118PVK0756-011042612K0415-MS1 11/12/12 11/12/12 25

CQC77.5-118PVK0793-0211027.512K0462-MS1 11/13/12 11/13/12 25

CQC77.5-118PVK0281-019924.712K0522-MS1 11/14/12 11/14/12 25

CQC77.5-118PVK1220-029624.112K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPD1,1,2-Trichloroethane


12932.22511/7/1211/7/1212K0235-MSD1 CQC,PSL25212631.5 PVK0237-01

11528.92511/8/1211/8/1212K0286-MSD1 CQC250.811629.1 PVK0555-04

9423.62511/9/1211/9/1212K0341-MSD1 25710125.4 PVK0649-06

10826.92511/12/1211/12/1212K0415-MSD1 CQC25310426 PVK0756-01

10726.82511/13/1211/13/1212K0462-MSD1 CQC25211027.5 PVK0793-02

104262511/14/1211/14/1212K0522-MSD1 CQC2559924.7 PVK0281-01

10225.52511/21/1211/21/1212K0803-MSD1 CQC2569624.1 PVK1220-02

01/02/13 15:46

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BLK1,1,2-Trichloroethane2.0,-------------------------~

1.8

1.6

1.4

Plotted: 7

MDL: 0.19

MRL: 1

1.2 j-. _· ~· ~·_:·_·~:....:_~~~~.:...:.~...:...:~:....:_~~_:_:....:....:...:.~...:...:~:....:_~~_:_:....:....:...:.~...:...:~:....:_~_j Rejected: 0 1.0 Stdv: 0.321

0.8 r~~~~~~~~~~~~~~~~~~~~~-7,,..,.-,~~~~~~~~~~l Mean: 0.179

0.6 ...... ............. ··A······......... 2s:0.821

0.4 ............. ·~· . . . . . . . . . . . . . . . . . !:::: 0.2 r------:7"'c:;_ __ ___:::"":::::_""7''-----~~-----l

/ "-...../ '\. 0.0 ~--....¢:.:__ ____ ~,£_ _____ _:,~ __ -J 3 4 5 6 7

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LCS %R1,1-Dichloroethane


12K0235-BS1 28.6 1142511/7/12 78.8-12211/7/12 CQC

12K0286-BS1 24.1 962511/8/12 78.8-12211/8/12 CQC

12K0341-BS1 20.4 822511/9/12 78.8-12211/9/12

12K0415-BS1 23.6 952511/12/12 78.8-12211/12/12 CQC

12K0462-BS1 26.2 1052511/13/12 78.8-12211/13/12 CQC

12K0522-BS1 26.1 1042511/14/12 78.8-12211/14/12 CQC

12K0803-BS1 25.1 1002511/21/12 78.8-12211/21/12 CQC

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LCS/LCSD RPD1,1-Dichloroethane


11027.42511/7/1211/7/1212K0235-BSD1 28.6 114 4 25 CQC

9323.32511/8/1211/8/1212K0286-BSD1 24.1 96 3 25 CQC

8120.42511/9/1211/9/1212K0341-BSD1 20.4 82 0.3 25

96242511/12/1211/12/1212K0415-BSD1 23.6 95 1 25 CQC

10426.12511/13/1211/13/1212K0462-BSD1 26.2 105 0.3 25 CQC

108272511/14/1211/14/1212K0522-BSD1 26.1 104 3 25 CQC

10325.82511/21/1211/21/1212K0803-BSD1 25.1 100 3 25 CQC

01/02/13 15:46

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MS %R1,1-Dichloroethane


CQC75.7-126PVK0237-0112330.712K0235-MS1 11/7/12 11/7/12 25

CQC75.7-126PVK0555-0411328.312K0286-MS1 11/8/12 11/8/12 25

75.7-126PVK0649-06842112K0341-MS1 11/9/12 11/9/12 25

CQC75.7-126PVK0756-011002512K0415-MS1 11/12/12 11/12/12 25

CQC75.7-126PVK0793-0211228.112K0462-MS1 11/13/12 11/13/12 25

CQC75.7-126PVK0281-0110626.612K0522-MS1 11/14/12 11/14/12 25

CQC75.7-126PVK1220-0211127.812K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPD1,1-Dichloroethane


12631.42511/7/1211/7/1212K0235-MSD1 CQC25212330.7 PVK0237-01

10726.82511/8/1211/8/1212K0286-MSD1 CQC25511328.3 PVK0555-04

8621.52511/9/1211/9/1212K0341-MSD1 2528421 PVK0649-06

10325.62511/12/1211/12/1212K0415-MSD1 CQC25210025 PVK0756-01

112282511/13/1211/13/1212K0462-MSD1 CQC250.411228.1 PVK0793-02

10827.12511/14/1211/14/1212K0522-MSD1 CQC25210626.6 PVK0281-01

11929.72511/21/1211/21/1212K0803-MSD1 CQC25711127.8 PVK1220-02

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BLK1,1-Dichloroethane

01/02/13 15:46

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LCS %R1,1-Dichloroethene


12I0005-BS1 26.8 107259/1/12 81.7-1229/1/12 CQC

12I0028-BS1 23.6 95259/4/12 81.7-1229/4/12 CQC

12I0081-BS1 24.6 98259/5/12 81.7-1229/5/12 CQC

12I0215-BS1 22.7 91259/7/12 81.7-1229/7/12 CQC

12I0352-BS1 27.3 109259/12/12 81.7-1229/12/12 CQC

12I0394-BS1 25.4 102259/12/12 81.7-1229/12/12 CQC

12I0598-BS1 28 112259/18/12 81.7-1229/18/12 CQC

12I0648-BS1 24.9 100259/18/12 81.7-1229/18/12 CQC

12I0926-BS1 25 100259/25/12 81.7-1229/25/12 CQC

12I0925-BS1 25.9 104259/25/12 81.7-1229/25/12 CQC

12I1065-BS1 27.6 111259/28/12 81.7-1229/28/12 CQC

12I1095-BS1 27.1 108259/28/12 81.7-1229/28/12 CQC

12I1107-BS1 27 108259/29/12 81.7-1229/29/12 CQC

12J0008-BS1 27.7 1112510/1/12 81.7-12210/1/12 CQC

12J0298-BS1 23.1 922510/8/12 81.7-12210/8/12

12J0389-BS1 22.9 922510/10/12 81.7-12210/10/12

12J0445-BS1 22.8 912510/11/12 81.7-12210/11/12 CQC

12J0620-BS1 25.2 1012510/16/12 81.7-12210/16/12 CQC

12J0736-BS1 23.7 952510/18/12 81.7-12210/18/12 CQC

12J0821-BS1 23.7 952510/20/12 81.7-12210/20/12 CQC

12J0850-BS1 22.8 912510/22/12 81.7-12210/22/12 CQC

12J0972-BS1 25 1002510/24/12 81.7-12210/24/12 CQC

12J1010-BS1 23.8 952510/25/12 81.7-12210/25/12 CQC

12J1038-BS1 23.9 962510/25/12 81.7-12210/25/12 CQC

12J1059-BS1 24 962510/26/12 81.7-12210/26/12 CQC

12K0235-BS1 31.1 1242511/7/12 81.7-12211/7/12 CQC,PSL

12K0286-BS1 25.9 1042511/8/12 81.7-12211/8/12 CQC

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LCS %R1,1-DichloroetheneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 20.1 812511/9/12 81.7-12211/9/12

12K0415-BS1 24.6 982511/12/12 81.7-12211/12/12 CQC

12K0462-BS1 27.1 1082511/13/12 81.7-12211/13/12 CQC

12K0522-BS1 27.8 111X 2511/14/12 81.7-12211/14/12 CQC

12K0553-BS1 23 922511/14/12 81.7-12211/14/12 CQC

12K0552-BS1 25 1002511/14/12 81.7-12211/14/12 CQC

12K0581-BS1 23.8 952511/15/12 81.7-12211/15/12 CQC

12K0740-BS1 23.8 952511/20/12 81.7-12211/20/12 CQC

12K0751-BS1 26.5 1062511/20/12 81.7-12211/20/12 CQC

12K0789-BS1 27.1 1082511/20/12 81.7-12211/20/12

12K0803-BS1 22.8 912511/21/12 81.7-12211/21/12 CQC

12K0836-BS1 24.1 962511/21/12 81.7-12211/21/12 CQC

12K0855-BS1 24 962511/23/12 81.7-12211/23/12 CQC

12K0865-BS1 25.5 1022511/23/12 81.7-12211/23/12 CQC

12K0897-BS1 22.2 892511/24/12 81.7-12211/24/12 CQC

12K0905-BS1 23.3 932511/25/12 81.7-12211/25/12 CQC

12K1134-BS1 20.8 832511/30/12 81.7-12211/30/12 CQC

12K1135-BS1 24.2 972511/30/12 81.7-12211/30/12 CQC

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LCS/LCSD RPD1,1-Dichloroethene


9223259/1/129/1/1212I0005-BSD1 26.8 107 15 25 CQC

10426.1259/4/129/4/1212I0028-BSD1 23.6 95 10 25 CQC

9323.4259/5/129/5/1212I0081-BSD1 24.6 98 5 25 CQC

9022.6259/7/129/7/1212I0215-BSD1 22.7 91 0.6 25 CQC

10325.8259/12/129/12/1212I0352-BSD1 27.3 109 6 25 CQC

10426259/12/129/12/1212I0394-BSD1 25.4 102 2 25 CQC

11228.1259/18/129/18/1212I0598-BSD1 28 112 0.5 25 CQC

10125.3259/18/129/18/1212I0648-BSD1 24.9 100 2 25 CQC

9523.7259/25/129/25/1212I0926-BSD1 25 100 5 25 CQC

10225.4259/25/129/25/1212I0925-BSD1 25.9 104 2 25 CQC

11027.4259/28/129/28/1212I1065-BSD1 27.6 111 0.9 25 CQC

10927.2259/28/129/28/1212I1095-BSD1 27.1 108 0.7 25 CQC

9824.6259/29/129/29/1212I1107-BSD1 27 108 9 25 CQC

11328.32510/1/1210/1/1212J0008-BSD1 27.7 111 2 25 CQC

9323.42510/8/1210/8/1212J0298-BSD1 23.1 92 1 25

9222.92510/10/1210/10/1212J0389-BSD1 22.9 92 0 25

9423.62510/11/1210/11/1212J0445-BSD1 22.8 91 3 25 CQC

10225.62510/16/1210/16/1212J0620-BSD1 25.2 101 2 25 CQC

9323.12510/18/1210/18/1212J0736-BSD1 23.7 95 2 25 CQC

9323.22510/20/1210/20/1212J0821-BSD1 23.7 95 2 25 CQC

8922.42510/22/1210/22/1212J0850-BSD1 22.8 91 2 25 CQC

9323.22510/24/1210/24/1212J0972-BSD1 25 100 7 25 CQC

92232510/25/1210/25/1212J1010-BSD1 23.8 95 4 25 CQC

104262510/25/1210/25/1212J1038-BSD1 23.9 96 9 25 CQC

9624.12510/26/1210/26/1212J1059-BSD1 24 96 0.4 25 CQC

11929.92511/7/1211/7/1212K0235-BSD1 31.1 124 4 25 CQC

10425.92511/8/1211/8/1212K0286-BSD1 25.9 104 0 25 CQC

01/02/13 15:46

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LCS/LCSD RPD1,1-Dichloroethene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

88222511/9/1211/9/1212K0341-BSD1 20.1 81 9 25

9824.52511/12/1211/12/1212K0415-BSD1 24.6 98 0.5 25 CQC

11127.72511/13/1211/13/1212K0462-BSD1 27.1 108 2 25 CQC

11227.92511/14/1211/14/1212K0522-BSD1X 27.8 111 0.5 25 CQC

10526.22511/14/1211/14/1212K0553-BSD1 23 92 13 25 CQC

10225.52511/14/1211/14/1212K0552-BSD1 25 100 2 25 CQC

96242511/15/1211/15/1212K0581-BSD1 23.8 95 1 25 CQC

9724.22511/20/1211/20/1212K0740-BSD1 23.8 95 2 25 CQC

10125.32511/20/1211/20/1212K0751-BSD1 26.5 106 5 25 CQC

10125.32511/20/1211/20/1212K0789-BSD1 27.1 108 7 25

9924.82511/21/1211/21/1212K0803-BSD1X 22.8 91 8 25 CQC

9122.82511/21/1211/21/1212K0836-BSD1 24.1 96 5 25 CQC

9824.52511/23/1211/23/1212K0855-BSD1 24 96 2 25 CQC

10125.22511/23/1211/23/1212K0865-BSD1 25.5 102 0.9 25 CQC

8922.22511/24/1211/24/1212K0897-BSD1 22.2 89 0.1 25 CQC

9724.32511/25/1211/25/1212K0905-BSD1 23.3 93 4 25 CQC

88222511/30/1211/30/1212K1134-BSD1 20.8 83 5 25 CQC

11127.92511/30/1211/30/1212K1135-BSD1 24.2 97 14 25 CQC

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MS %R1,1-Dichloroethene


CQC82.1-126PVH2309-029724.212I0005-MS1 9/1/12 9/1/12 25

CQC82.1-126PVH2309-1110726.612I0028-MS1 9/4/12 9/4/12 25

CQC82.1-126PVH2037-079724.412I0081-MS1 9/5/12 9/5/12 25

CQC82.1-126PVI0290-039924.712I0215-MS1 9/7/12 9/7/12 25

CQC82.1-126PVI0609-0910927.112I0352-MS1 9/12/12 9/12/12 25

CQC82.1-126PVI0525-06 (2.06)11230.112I0394-MS1 9/12/12 9/12/12 25

CQC82.1-126PVI0894-06 (3.12)11431.612I0598-MS1 9/18/12 9/18/12 25

CQC82.1-126PVI1060-0210325.612I0648-MS1 9/18/12 9/18/12 25

CQC82.1-126PVI1553-0810225.612I0925-MS1 9/25/12 9/25/12 25

CQC82.1-126PVI1510-089423.612I0926-MS1 9/25/12 9/25/12 25

CQC82.1-126PVI1723-0311528.712I1065-MS1 9/28/12 9/28/12 25

CQC82.1-126PVI1822-0210526.212I1095-MS1 9/28/12 9/28/12 25

CQC82.1-126PVI1869-0511127.712I1107-MS1 9/29/12 9/29/12 25

CQC82.1-126PVI1575-0110927.212J0008-MS1 10/1/12 10/1/12 25

82.1-126PVJ0513-039724.212J0298-MS1 10/8/12 10/8/12 25

82.1-126PVJ0682-01962412J0389-MS1 10/10/12 10/10/12 25

CQC82.1-126PVJ0682-17 (0.3)8521.512J0445-MS1 10/11/12 10/11/12 25

CQC82.1-126PVJ1065-029824.512J0620-MS1 10/16/12 10/16/12 25

CQC82.1-126PVJ1237-029122.812J0736-MS1 10/18/12 10/18/12 25

CQC82.1-126PVJ1405-0210225.612J0821-MS1 10/20/12 10/20/12 25

CQC82.1-126PVJ1405-179122.812J0850-MS1 10/22/12 10/22/12 25

CQC82.1-126PVJ1577-029523.812J0972-MS1 10/24/12 10/24/12 25

CQC82.1-126PVJ1627-018721712J1010-MS1 10/25/12 10/25/12 250

CQC82.1-126PVJ1600-021002512J1038-MS1 10/25/12 10/25/12 25

CQC82.1-126PVJ1577-18RE110927212J1059-MS1 10/26/12 10/26/12 250

CQC82.1-126PVK0237-0112531.212K0235-MS1 11/7/12 11/7/12 25

CQC82.1-126PVK0555-041162912K0286-MS1 11/8/12 11/8/12 25

82.1-126PVK0649-068822.112K0341-MS1 11/9/12 11/9/12 25

CQC82.1-126PVK0756-0110125.412K0415-MS1 11/12/12 11/12/12 25

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MS %R1,1-DichloroetheneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC82.1-126PVK0793-021122812K0462-MS1 11/13/12 11/13/12 25

CQC82.1-126PVK0281-0110826.9X 12K0522-MS1 11/14/12 11/14/12 25

CQC82.1-126PVK0632-0910826.912K0553-MS1 11/14/12 11/14/12 25

CQC82.1-126PVK0684-0210726.812K0552-MS1 11/14/12 11/14/12 25

CQC82.1-126PVK0696-019423.412K0581-MS1 11/15/12 11/15/12 25

CQC82.1-126PVK0934-019423.412K0740-MS1 11/20/12 11/20/12 25

CQC82.1-126PVK0768-0211528.812K0751-MS1 11/20/12 11/20/12 25

CQC82.1-126PVK1220-029824.4X 12K0803-MS1 11/21/12 11/21/12 25

CQC82.1-126PVK1288-0310125.312K0836-MS1 11/21/12 11/21/12 25

CQC82.1-126PVK1375-0810325.712K0865-MS1 11/23/12 11/23/12 25

CQC82.1-126PVK1375-0210526.412K0855-MS1 11/23/12 11/23/12 25

CQC82.1-126PVK0988-039423.412K0897-MS1 11/24/12 11/24/12 25

CQC82.1-126PVK1006-0110025.112K0905-MS1 11/25/12 11/25/12 25

CQC82.1-126PVK1450-109724.312K1135-MS1 11/30/12 11/30/12 25

CQC82.1-126PVK1450-0310225.612K1134-MS1 11/30/12 12/1/12 25

01/02/13 15:46

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Analyzed By:

MS/MSD RPD1,1-Dichloroethene


10225.4259/1/129/1/1212I0005-MSD1 CQC2559724.2 PVH2309-02

10425.9259/4/129/4/1212I0028-MSD1 CQC25310726.6 PVH2309-11

9824.5259/5/129/5/1212I0081-MSD1 CQC250.79724.4 PVH2037-07

9724.3259/7/129/7/1212I0215-MSD1 CQC2529924.7 PVI0290-03

10325.7259/12/129/12/1212I0352-MSD1 CQC25610927.1 PVI0609-09

11029.6259/12/129/12/1212I0394-MSD1 CQC25211230.1 PVI0525-06 (2.06)

11431.7259/18/129/18/1212I0598-MSD1 CQC250.0311431.6 PVI0894-06 (3.12)

9624.1259/18/129/18/1212I0648-MSD1 CQC25610325.6 PVI1060-02

10225.6259/25/129/25/1212I0925-MSD1 CQC250.0410225.6 PVI1553-08

9724.4259/25/129/25/1212I0926-MSD1 CQC2539423.6 PVI1510-08

11027.5259/28/129/28/1212I1065-MSD1 CQC25411528.7 PVI1723-03

11528.7259/28/129/28/1212I1095-MSD1 CQC25910526.2 PVI1822-02

12230.6259/29/129/29/1212I1107-MSD1 CQC251011127.7 PVI1869-05

11127.72510/1/1210/1/1212J0008-MSD1 CQC25210927.2 PVI1575-01

9523.82510/8/1210/8/1212J0298-MSD1 2529724.2 PVJ0513-03

9724.22510/10/1210/10/1212J0389-MSD1 250.69624 PVJ0682-01

8521.62510/11/1210/11/1212J0445-MSD1 CQC250.28521.5 PVJ0682-17 (0.3)

10125.22510/16/1210/16/1212J0620-MSD1 CQC2539824.5 PVJ1065-02

9724.22510/18/1210/18/1212J0736-MSD1 CQC2569122.8 PVJ1237-02

11428.52510/20/1210/20/1212J0821-MSD1 CQC251110225.6 PVJ1405-02

9022.62510/22/1210/22/1212J0850-MSD1 CQC250.89122.8 PVJ1405-17

10025.12510/24/1210/24/1212J0972-MSD1 CQC2559523.8 PVJ1577-02

8922225010/25/1210/25/1212J1010-MSD1 CQC25287217 PVJ1627-01

10125.32510/25/1210/25/1212J1038-MSD1 CQC25110025 PVJ1600-02

11027625010/26/1210/26/1212J1059-MSD1 CQC251109272 PVJ1577-18RE1

128322511/7/1211/7/1212K0235-MSD1 CQC,PSL25212531.2 PVK0237-01

10826.92511/8/1211/8/1212K0286-MSD1 CQC25711629 PVK0555-04

9022.52511/9/1211/9/1212K0341-MSD1 2528822.1 PVK0649-06

10225.52511/12/1211/12/1212K0415-MSD1 CQC250.610125.4 PVK0756-01

11027.52511/13/1211/13/1212K0462-MSD1 CQC25211228 PVK0793-02

112282511/14/1211/14/1212K0522-MSD1X CQC25410826.9 PVK0281-01

01/02/13 15:46

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MS/MSD RPD1,1-Dichloroethene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

9523.82511/14/1211/14/1212K0553-MSD1 CQC251210826.9 PVK0632-09

11127.72511/14/1211/14/1212K0552-MSD1 CQC25310726.8 PVK0684-02

10125.22511/15/1211/15/1212K0581-MSD1 CQC2579423.4 PVK0696-01

9624.12511/20/1211/20/1212K0740-MSD1 CQC2539423.4 PVK0934-01

11528.72511/20/1211/20/1212K0751-MSD1 CQC250.211528.8 PVK0768-02

10726.62511/21/1211/21/1212K0803-MSD1X CQC2599824.4 PVK1220-02

10125.42511/21/1211/21/1212K0836-MSD1 CQC250.410125.3 PVK1288-03

10526.22511/23/1211/23/1212K0865-MSD1 CQC25210325.7 PVK1375-08

9523.72511/23/1211/23/1212K0855-MSD1 CQC251010526.4 PVK1375-02

10024.92511/24/1211/24/1212K0897-MSD1 CQC2569423.4 PVK0988-03

9724.32511/25/1211/25/1212K0905-MSD1 CQC25310025.1 PVK1006-01

10526.32511/30/1211/30/1212K1135-MSD1 CQC2589724.3 PVK1450-10

96242512/1/1211/30/1212K1134-MSD1 CQC25610225.6 PVK1450-03

01/02/13 15:46

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BLK1,1-Dichloroethene

1.0 r-------------------------------------------------------~

0.9

0.8

0.7

0.6

0.5

0.4

03 .......... .

Plotted: 44

MDL: 0.23

MRL: 1

Rejected: 2

Stdv: 0.0428

Mean: 0.0148

2s: 0.1

l----------------------------------1 3s: 0.143 0.2 · · · · · · 0 · 4s: 0.186

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %R1,1-Dichloropropene


12K0235-BS1 27.5 1102511/7/12 82.3-11911/7/12 CQC

12K0286-BS1 23 922511/8/12 82.3-11911/8/12 CQC

12K0341-BS1 23 922511/9/12 82.3-11911/9/12

12K0415-BS1 22.1 882511/12/12 82.3-11911/12/12 CQC

12K0462-BS1 23.7 952511/13/12 82.3-11911/13/12 CQC

12K0522-BS1 25.1 1002511/14/12 82.3-11911/14/12 CQC

12K0803-BS1 23.6 942511/21/12 82.3-11911/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPD1,1-Dichloropropene


11027.42511/7/1211/7/1212K0235-BSD1 27.5 110 0.5 25 CQC

96242511/8/1211/8/1212K0286-BSD1 23 92 4 25 CQC

9323.32511/9/1211/9/1212K0341-BSD1 23 92 1 25

9022.42511/12/1211/12/1212K0415-BSD1 22.1 88 2 25 CQC

9724.22511/13/1211/13/1212K0462-BSD1 23.7 95 2 25 CQC

9824.52511/14/1211/14/1212K0522-BSD1 25.1 100 2 25 CQC

9724.42511/21/1211/21/1212K0803-BSD1 23.6 94 3 25 CQC

01/02/13 15:46

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MS %R1,1-Dichloropropene


CQC81.4-123PVK0237-0111127.812K0235-MS1 11/7/12 11/7/12 25

CQC81.4-123PVK0555-0410425.912K0286-MS1 11/8/12 11/8/12 25

81.4-123PVK0649-069022.612K0341-MS1 11/9/12 11/9/12 25

CQC81.4-123PVK0756-019423.512K0415-MS1 11/12/12 11/12/12 25

CQC81.4-123PVK0793-02962412K0462-MS1 11/13/12 11/13/12 25

CQC81.4-123PVK0281-019523.612K0522-MS1 11/14/12 11/14/12 25

CQC81.4-123PVK1220-028922.212K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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MS/MSD RPD1,1-Dichloropropene


11428.52511/7/1211/7/1212K0235-MSD1 CQC25311127.8 PVK0237-01

100252511/8/1211/8/1212K0286-MSD1 CQC25410425.9 PVK0555-04

9022.62511/9/1211/9/1212K0341-MSD1 250.39022.6 PVK0649-06

9222.92511/12/1211/12/1212K0415-MSD1 CQC2529423.5 PVK0756-01

96242511/13/1211/13/1212K0462-MSD1 CQC250.29624 PVK0793-02

10125.22511/14/1211/14/1212K0522-MSD1 CQC2579523.6 PVK0281-01

9924.62511/21/1211/21/1212K0803-MSD1 CQC25108922.2 PVK1220-02

01/02/13 15:46

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BLK1,1-Dichloropropene

01/02/13 15:46

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LCS %R1,2,3-Trichlorobenzene


12K0235-BS1 34.7 1392511/7/12 60.4-17111/7/12 CQC

12K0286-BS1 28.3 1132511/8/12 60.4-17111/8/12 CQC

12K0341-BS1 34.6 1382511/9/12 60.4-17111/9/12

12K0415-BS1 29.7 1192511/12/12 60.4-17111/12/12 CQC

12K0462-BS1 29.8 1192511/13/12 60.4-17111/13/12 CQC

12K0522-BS1 30.9 1232511/14/12 60.4-17111/14/12 CQC

12K0803-BS1 22.2 892511/21/12 60.4-17111/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPD1,2,3-Trichlorobenzene


132332511/7/1211/7/1212K0235-BSD1 34.7 139 5 25 CQC

12330.82511/8/1211/8/1212K0286-BSD1 28.3 113 9 25 CQC

13232.92511/9/1211/9/1212K0341-BSD1 34.6 138 5 25

12330.72511/12/1211/12/1212K0415-BSD1 29.7 119 3 25 CQC

11929.82511/13/1211/13/1212K0462-BSD1 29.8 119 0.03 25 CQC

116292511/14/1211/14/1212K0522-BSD1 30.9 123 6 25 CQC

9623.92511/21/1211/21/1212K0803-BSD1 22.2 89 7 25 CQC

01/02/13 15:46

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MS %R1,2,3-Trichlorobenzene


CQC,PSL32.3-117PVK0237-0113934.912K0235-MS1 11/7/12 11/7/12 25

CQC,M732.3-117PVK0555-0413934.812K0286-MS1 11/8/12 11/8/12 25

32.3-117PVK0649-0612330.712K0341-MS1 11/9/12 11/9/12 25

CQC,M732.3-117PVK0756-0113533.712K0415-MS1 11/12/12 11/12/12 25

CQC32.3-117PVK0793-0211127.812K0462-MS1 11/13/12 11/13/12 25

CQC32.3-117PVK0281-0110325.712K0522-MS1 11/14/12 11/14/12 25

CQC32.3-117PVK1220-029223.112K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPD1,2,3-Trichlorobenzene


14536.32511/7/1211/7/1212K0235-MSD1 CQC,M725413934.9 PVK0237-01

13233.12511/8/1211/8/1212K0286-MSD1 CQC,M725513934.8 PVK0555-04

12030.12511/9/1211/9/1212K0341-MSD1 25212330.7 PVK0649-06

11729.32511/12/1211/12/1212K0415-MSD1 CQC251413533.7 PVK0756-01

12932.12511/13/1211/13/1212K0462-MSD1 CQC,M7251411127.8 PVK0793-02

10726.72511/14/1211/14/1212K0522-MSD1 CQC25410325.7 PVK0281-01

10225.62511/21/1211/21/1212K0803-MSD1 CQC25109223.1 PVK1220-02

01/02/13 15:46

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BLK1,2,3-Trichlorobenzene

Plotted: 7

MDL: 0.27

MRL: 2

Rejected: 0

Stdv: 0.0631

Mean: 0.221

2s: 0.348

~;;~~~~~~~~~~~~~~~~3~~;;~~;;;;~~~;;;;;;;~~ 3s: 0.411 T 4s: 0.474

3 4 5 6 7

01/02/13 15:46

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LCS %R1,2,3-Trichloropropane


12K0235-BS1 29.6 1192511/7/12 76.3-12511/7/12 CQC

12K0286-BS1 23.8 952511/8/12 76.3-12511/8/12 CQC

12K0341-BS1 23.8 952511/9/12 76.3-12511/9/12

12K0415-BS1 23 922511/12/12 76.3-12511/12/12 CQC

12K0462-BS1 26 1042511/13/12 76.3-12511/13/12 CQC

12K0522-BS1 30 1202511/14/12 76.3-12511/14/12 CQC

12K0803-BS1 23.4 932511/21/12 76.3-12511/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPD1,2,3-Trichloropropane


11428.52511/7/1211/7/1212K0235-BSD1 29.6 119 4 25 CQC

9924.62511/8/1211/8/1212K0286-BSD1 23.8 95 4 25 CQC

10125.32511/9/1211/9/1212K0341-BSD1 23.8 95 6 25

8922.22511/12/1211/12/1212K0415-BSD1 23 92 3 25 CQC

10426.12511/13/1211/13/1212K0462-BSD1 26 104 0.2 25 CQC

11929.82511/14/1211/14/1212K0522-BSD1 30 120 0.5 25 CQC

10325.92511/21/1211/21/1212K0803-BSD1 23.4 93 10 25 CQC

01/02/13 15:46

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MS %R1,2,3-Trichloropropane


CQC69.8-124PVK0237-0110426.112K0235-MS1 11/7/12 11/7/12 25

CQC69.8-124PVK0555-04962412K0286-MS1 11/8/12 11/8/12 25

69.8-124PVK0649-061042612K0341-MS1 11/9/12 11/9/12 25

CQC69.8-124PVK0756-01962412K0415-MS1 11/12/12 11/12/12 25

CQC69.8-124PVK0793-029724.412K0462-MS1 11/13/12 11/13/12 25

CQC69.8-124PVK0281-0111428.512K0522-MS1 11/14/12 11/14/12 25

CQC69.8-124PVK1220-0210325.812K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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MS/MSD RPD1,2,3-Trichloropropane


10626.62511/7/1211/7/1212K0235-MSD1 CQC25210426.1 PVK0237-01

10325.72511/8/1211/8/1212K0286-MSD1 CQC2579624 PVK0555-04

10024.92511/9/1211/9/1212K0341-MSD1 25410426 PVK0649-06

9724.22511/12/1211/12/1212K0415-MSD1 CQC2519624 PVK0756-01

11328.32511/13/1211/13/1212K0462-MSD1 CQC25159724.4 PVK0793-02

11027.62511/14/1211/14/1212K0522-MSD1 CQC25311428.5 PVK0281-01

9924.82511/21/1211/21/1212K0803-MSD1 CQC25410325.8 PVK1220-02

01/02/13 15:46

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BLK1,2,3-Trichloropropane

Plotted: 7

MDL: 0.31

MRL: 2

Rejected: 0

Stdv: 0

Mean: 0

2s: 0

3s: 0

r--------------~~...:...:....:...:..:....:...~~...:...:..:....:...~~...:...:.~ 4s: 0

4 5 6 7

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LCS %R1,2,4-Trichlorobenzene


12K0235-BS1 34.8 1392511/7/12 71-13611/7/12 CQC,L

12K0286-BS1 30.3 1212511/8/12 71-13611/8/12 CQC

12K0341-BS1 35.7 1432511/9/12 71-13611/9/12

12K0415-BS1 26.5 1062511/12/12 71-13611/12/12 CQC

12K0462-BS1 28.8 1152511/13/12 71-13611/13/12 CQC

12K0522-BS1 30.2 1212511/14/12 71-13611/14/12 CQC

12K0803-BS1 23.4 932511/21/12 71-13611/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPD1,2,4-Trichlorobenzene


13834.42511/7/1211/7/1212K0235-BSD1 34.8 139 1 25 CQC,L

12831.92511/8/1211/8/1212K0286-BSD1 30.3 121 5 25 CQC

13132.72511/9/1211/9/1212K0341-BSD1 35.7 143 9 25

10426.12511/12/1211/12/1212K0415-BSD1 26.5 106 2 25 CQC

11829.42511/13/1211/13/1212K0462-BSD1 28.8 115 2 25 CQC

11628.92511/14/1211/14/1212K0522-BSD1 30.2 121 4 25 CQC

100252511/21/1211/21/1212K0803-BSD1 23.4 93 7 25 CQC

01/02/13 15:46

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MS %R1,2,4-Trichlorobenzene


CQC52.9-145PVK0237-0114235.412K0235-MS1 11/7/12 11/7/12 25

CQC,M752.9-145PVK0555-0414636.412K0286-MS1 11/8/12 11/8/12 25

52.9-145PVK0649-0612731.812K0341-MS1 11/9/12 11/9/12 25

CQC52.9-145PVK0756-0111428.612K0415-MS1 11/12/12 11/12/12 25

CQC52.9-145PVK0793-0211328.312K0462-MS1 11/13/12 11/13/12 25

CQC52.9-145PVK0281-0110225.512K0522-MS1 11/14/12 11/14/12 25

CQC52.9-145PVK1220-029323.312K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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Analyzed By:

MS/MSD RPD1,2,4-Trichlorobenzene


15037.42511/7/1211/7/1212K0235-MSD1 CQC,M1425514235.4 PVK0237-01

13533.82511/8/1211/8/1212K0286-MSD1 CQC25714636.4 PVK0555-04

12932.32511/9/1211/9/1212K0341-MSD1 25212731.8 PVK0649-06

10526.22511/12/1211/12/1212K0415-MSD1 CQC25911428.6 PVK0756-01

13433.42511/13/1211/13/1212K0462-MSD1 CQC251611328.3 PVK0793-02

10526.22511/14/1211/14/1212K0522-MSD1 CQC25310225.5 PVK0281-01

10827.12511/21/1211/21/1212K0803-MSD1 CQC25159323.3 PVK1220-02

01/02/13 15:46

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BLK1,2,4-Trichlorobenzene

1.o r -----------------------, 0.9

0.8

0.7 ..... .

0.6 ..... .

0.5 ..... .

0.4 ..... .

Plotted: 7

MDL: 0.18

MRL: 1

Rejected: 0

Stdv: 0.109

Mean: 0.136

:: F.· =· =·=·=·;;· ;;. ;;. =· ~· :·~·~·==· =· =· =· =· =·=·=·==· ~· ;. ;;:· ~·~=·=·=·=· :· =· =· =· =·=·=·~~:;;:::::::::::::::::::::::;~d ;: ~:;~ :: ~---·. _· .. ·_·. ·_· ·~-· · ----==· .. ~/_· . ·_·. ·_·. ·_·. ·_· .. _· .. _"<______:·. ·~·. ·.c__7'_· . __J.

2 3 4 5 6 7

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Analyzed By:

LCS %R1,2,4-Trimethylbenzene


12K0235-BS1 29.7 1192511/7/12 78.1-12011/7/12 CQC

12K0286-BS1 25.5 1022511/8/12 78.1-12011/8/12 CQC

12K0341-BS1 27 1082511/9/12 78.1-12011/9/12

12K0415-BS1 23.2 932511/12/12 78.1-12011/12/12 CQC

12K0462-BS1 24.9 1002511/13/12 78.1-12011/13/12 CQC

12K0522-BS1 27.4 1092511/14/12 78.1-12011/14/12 CQC

12K0803-BS1 25.8 1032511/21/12 78.1-12011/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPD1,2,4-Trimethylbenzene


11829.42511/7/1211/7/1212K0235-BSD1 29.7 119 0.9 25 CQC

10626.42511/8/1211/8/1212K0286-BSD1 25.5 102 3 25 CQC

10425.92511/9/1211/9/1212K0341-BSD1 27 108 4 25

9523.82511/12/1211/12/1212K0415-BSD1 23.2 93 3 25 CQC

10726.82511/13/1211/13/1212K0462-BSD1 24.9 100 7 25 CQC

11127.72511/14/1211/14/1212K0522-BSD1 27.4 109 1 25 CQC

10626.42511/21/1211/21/1212K0803-BSD1 25.8 103 2 25 CQC

01/02/13 15:46

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MS %R1,2,4-Trimethylbenzene


CQC75.2-120PVK0237-0111929.812K0235-MS1 11/7/12 11/7/12 25

CQC75.2-120PVK0555-0411929.812K0286-MS1 11/8/12 11/8/12 25

75.2-120PVK0649-0610726.912K0341-MS1 11/9/12 11/9/12 25

CQC75.2-120PVK0756-019624.112K0415-MS1 11/12/12 11/12/12 25

CQC75.2-120PVK0793-0210726.812K0462-MS1 11/13/12 11/13/12 25

CQC75.2-120PVK0281-01 (40.2)10766.912K0522-MS1 11/14/12 11/14/12 25

CQC75.2-120PVK1220-0210526.212K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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MS/MSD RPD1,2,4-Trimethylbenzene


12531.22511/7/1211/7/1212K0235-MSD1 CQC,PSL25411929.8 PVK0237-01

11027.52511/8/1211/8/1212K0286-MSD1 CQC25811929.8 PVK0555-04

10426.12511/9/1211/9/1212K0341-MSD1 25310726.9 PVK0649-06

9724.22511/12/1211/12/1212K0415-MSD1 CQC250.49624.1 PVK0756-01

11027.62511/13/1211/13/1212K0462-MSD1 CQC25310726.8 PVK0793-02

8962.52511/14/1211/14/1212K0522-MSD1 CQC25710766.9 PVK0281-01 (40.2)

11528.72511/21/1211/21/1212K0803-MSD1 CQC25910526.2 PVK1220-02

01/02/13 15:46

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BLK1,2,4-Trimethylbenzene

01/02/13 15:46

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LCS %R1,2-Dibromoethane (EDB)


12K0235-BS1 30.8 1232511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 25.9 1042511/8/12 85-11511/8/12 CQC

12K0341-BS1 25.5 1022511/9/12 85-11511/9/12

12K0415-BS1 25.3 1012511/12/12 85-11511/12/12 CQC

12K0462-BS1 28.5 1142511/13/12 85-11511/13/12 CQC

12K0522-BS1 27.7 1112511/14/12 85-11511/14/12 CQC

12K0803-BS1 25.3 1012511/21/12 85-11511/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPD1,2-Dibromoethane (EDB)


12531.22511/7/1211/7/1212K0235-BSD1 30.8 123 1 25 CQC,PSL

10626.42511/8/1211/8/1212K0286-BSD1 25.9 104 2 25 CQC

10225.42511/9/1211/9/1212K0341-BSD1 25.5 102 0.5 25

9523.82511/12/1211/12/1212K0415-BSD1 25.3 101 6 25 CQC

11127.62511/13/1211/13/1212K0462-BSD1 28.5 114 3 25 CQC

11328.22511/14/1211/14/1212K0522-BSD1 27.7 111 2 25 CQC

10426.12511/21/1211/21/1212K0803-BSD1 25.3 101 3 25 CQC

01/02/13 15:46

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MS %R1,2-Dibromoethane (EDB)


CQC76.5-120PVK0237-0111729.112K0235-MS1 11/7/12 11/7/12 25

CQC76.5-120PVK0555-0411328.212K0286-MS1 11/8/12 11/8/12 25

76.5-120PVK0649-0610125.212K0341-MS1 11/9/12 11/9/12 25

CQC76.5-120PVK0756-011042612K0415-MS1 11/12/12 11/12/12 25

CQC76.5-120PVK0793-0211127.612K0462-MS1 11/13/12 11/13/12 25

CQC76.5-120PVK0281-0110626.512K0522-MS1 11/14/12 11/14/12 25

CQC76.5-120PVK1220-0210526.312K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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MS/MSD RPD1,2-Dibromoethane (EDB)


12230.52511/7/1211/7/1212K0235-MSD1 CQC,PSL25511729.1 PVK0237-01

11528.62511/8/1211/8/1212K0286-MSD1 CQC25111328.2 PVK0555-04

9924.82511/9/1211/9/1212K0341-MSD1 25210125.2 PVK0649-06

11228.12511/12/1211/12/1212K0415-MSD1 CQC25810426 PVK0756-01

11428.42511/13/1211/13/1212K0462-MSD1 CQC25311127.6 PVK0793-02

11027.52511/14/1211/14/1212K0522-MSD1 CQC25310626.5 PVK0281-01

10325.72511/21/1211/21/1212K0803-MSD1 CQC25210526.3 PVK1220-02

01/02/13 15:46

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BLK1,2-Dibromoethane (EDB)

01/02/13 15:46

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LCS %R1,2-Dichlorobenzene


12K0235-BS1 30.2 1212511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 26.1 1042511/8/12 85-11511/8/12 CQC

12K0341-BS1 27.6 1102511/9/12 85-11511/9/12

12K0415-BS1 24.8 992511/12/12 85-11511/12/12 CQC

12K0462-BS1 25.7 1032511/13/12 85-11511/13/12 CQC

12K0522-BS1 27.4 1092511/14/12 85-11511/14/12 CQC

12K0803-BS1 25.4 1022511/21/12 85-11511/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPD1,2-Dichlorobenzene


12030.12511/7/1211/7/1212K0235-BSD1 30.2 121 0.5 25 CQC,PSL

10726.72511/8/1211/8/1212K0286-BSD1 26.1 104 2 25 CQC

10626.62511/9/1211/9/1212K0341-BSD1 27.6 110 3 25

10125.22511/12/1211/12/1212K0415-BSD1 24.8 99 2 25 CQC

10827.12511/13/1211/13/1212K0462-BSD1 25.7 103 5 25 CQC

11027.42511/14/1211/14/1212K0522-BSD1 27.4 109 0.1 25 CQC

10626.52511/21/1211/21/1212K0803-BSD1 25.4 102 4 25 CQC

01/02/13 15:46

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MS %R1,2-Dichlorobenzene


CQC,PSL80.6-114PVK0237-0112030.112K0235-MS1 11/7/12 11/7/12 25

CQC,M780.6-114PVK0555-041243112K0286-MS1 11/8/12 11/8/12 25

80.6-114PVK0649-0610626.412K0341-MS1 11/9/12 11/9/12 25

CQC80.6-114PVK0756-019924.812K0415-MS1 11/12/12 11/12/12 25

CQC80.6-114PVK0793-0210726.812K0462-MS1 11/13/12 11/13/12 25

CQC80.6-114PVK0281-011002512K0522-MS1 11/14/12 11/14/12 25

CQC80.6-114PVK1220-0210927.312K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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MS/MSD RPD1,2-Dichlorobenzene


13032.52511/7/1211/7/1212K0235-MSD1 CQC,PSL25812030.1 PVK0237-01

11929.92511/8/1211/8/1212K0286-MSD1 CQC,M725412431 PVK0555-04

10626.52511/9/1211/9/1212K0341-MSD1 250.510626.4 PVK0649-06

10125.22511/12/1211/12/1212K0415-MSD1 CQC2529924.8 PVK0756-01

11628.92511/13/1211/13/1212K0462-MSD1 CQC,M725810726.8 PVK0793-02

10225.62511/14/1211/14/1212K0522-MSD1 CQC25210025 PVK0281-01

11428.52511/21/1211/21/1212K0803-MSD1 CQC25410927.3 PVK1220-02

01/02/13 15:46

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BLK1,2-Dichlorobenzene

01/02/13 15:46

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LCS %R1,2-Dichloroethane


12K0235-BS1 27.7 1112511/7/12 79.1-12411/7/12 CQC

12K0286-BS1 22.6 912511/8/12 79.1-12411/8/12 CQC

12K0341-BS1 21.9 882511/9/12 79.1-12411/9/12

12K0415-BS1 25.1 1002511/12/12 79.1-12411/12/12 CQC

12K0462-BS1 28.5 1142511/13/12 79.1-12411/13/12 CQC

12K0522-BS1 27.6 1112511/14/12 79.1-12411/14/12 CQC

12K0803-BS1 26.7 1072511/21/12 79.1-12411/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPD1,2-Dichloroethane


10526.42511/7/1211/7/1212K0235-BSD1 27.7 111 5 25 CQC

9223.12511/8/1211/8/1212K0286-BSD1 22.6 91 2 25 CQC

8821.92511/9/1211/9/1212K0341-BSD1 21.9 88 0.1 25

9724.22511/12/1211/12/1212K0415-BSD1 25.1 100 3 25 CQC

11328.22511/13/1211/13/1212K0462-BSD1 28.5 114 1 25 CQC

11528.62511/14/1211/14/1212K0522-BSD1 27.6 111 4 25 CQC

11729.12511/21/1211/21/1212K0803-BSD1 26.7 107 9 25 CQC

01/02/13 15:46

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MS %R1,2-Dichloroethane


CQC69.4-129PVK0237-0112130.312K0235-MS1 11/7/12 11/7/12 25

CQC69.4-129PVK0555-0410927.212K0286-MS1 11/8/12 11/8/12 25

69.4-129PVK0649-069122.712K0341-MS1 11/9/12 11/9/12 25

CQC69.4-129PVK0756-019724.212K0415-MS1 11/12/12 11/12/12 25

CQC69.4-129PVK0793-0211829.412K0462-MS1 11/13/12 11/13/12 25

CQC69.4-129PVK0281-0111328.212K0522-MS1 11/14/12 11/14/12 25

CQC69.4-129PVK1220-0211929.912K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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MS/MSD RPD1,2-Dichloroethane


12230.62511/7/1211/7/1212K0235-MSD1 CQC250.912130.3 PVK0237-01

10325.62511/8/1211/8/1212K0286-MSD1 CQC25610927.2 PVK0555-04

8821.92511/9/1211/9/1212K0341-MSD1 2549122.7 PVK0649-06

10025.12511/12/1211/12/1212K0415-MSD1 CQC2549724.2 PVK0756-01

11929.72511/13/1211/13/1212K0462-MSD1 CQC250.811829.4 PVK0793-02

11629.12511/14/1211/14/1212K0522-MSD1 CQC25311328.2 PVK0281-01

11729.32511/21/1211/21/1212K0803-MSD1 CQC25211929.9 PVK1220-02

01/02/13 15:46

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Analyzed By:

BLK1,2-Dichloroethane

01/02/13 15:46

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LCS %R1,2-Dichloropropane


12I0005-BS1 24.8 99259/1/12 85-1159/1/12 CQC

12I0028-BS1 23.8 95259/4/12 85-1159/4/12 CQC

12I0081-BS1 20.2 81259/5/12 85-1159/5/12 CQC,PSL

12I0215-BS1 23.1 92259/7/12 85-1159/7/12 CQC

12I0352-BS1 25.1 100259/12/12 85-1159/12/12 CQC

12I0394-BS1 19.8 79259/12/12 85-1159/12/12 CQC,PSL

12I0598-BS1 26.6 106259/18/12 85-1159/18/12 CQC

12I0648-BS1 23.8 95259/18/12 85-1159/18/12 CQC

12I0926-BS1 23.7 95259/25/12 85-1159/25/12 CQC

12I0925-BS1 22.1 89259/25/12 85-1159/25/12 CQC

12I1065-BS1 24.2 97259/28/12 85-1159/28/12 CQC

12I1095-BS1 24.1 96259/28/12 85-1159/28/12 CQC

12I1107-BS1 24.8 99259/29/12 85-1159/29/12 CQC

12J0008-BS1 24.6 982510/1/12 85-11510/1/12 CQC

12J0298-BS1 22.4 892510/8/12 85-11510/8/12

12J0389-BS1 22.1 882510/10/12 85-11510/10/12

12J0445-BS1 22.7 912510/11/12 85-11510/11/12 CQC

12J0620-BS1 22.4 892510/16/12 85-11510/16/12 CQC

12J0736-BS1 23.6 952510/18/12 85-11510/18/12 CQC

12J0821-BS1 24.1 962510/20/12 85-11510/20/12 CQC

12J0850-BS1 22.3 892510/22/12 85-11510/22/12 CQC

12J0972-BS1 23.4 942510/24/12 85-11510/24/12 CQC

12J1010-BS1 22.6 902510/25/12 85-11510/25/12 CQC

12J1038-BS1 23.2 932510/25/12 85-11510/25/12 CQC

12J1059-BS1 23.6 952510/26/12 85-11510/26/12 CQC

12K0235-BS1 26.8 1072511/7/12 85-11511/7/12 CQC

12K0286-BS1 24 962511/8/12 85-11511/8/12 CQC

01/02/13 15:46

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LCS %R1,2-DichloropropaneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 22.7 912511/9/12 85-11511/9/12

12K0415-BS1 23.4 932511/12/12 85-11511/12/12 CQC

12K0462-BS1 24.7 992511/13/12 85-11511/13/12 CQC

12K0522-BS1 24.5 982511/14/12 85-11511/14/12 CQC

12K0553-BS1 25.4 1022511/14/12 85-11511/14/12 CQC

12K0552-BS1 23.9 962511/14/12 85-11511/14/12 CQC

12K0581-BS1 26.2 1052511/15/12 85-11511/15/12 CQC

12K0740-BS1 22.9 912511/20/12 85-11511/20/12 CQC

12K0751-BS1 25.2 1012511/20/12 85-11511/20/12 CQC

12K0789-BS1 26.5 1062511/20/12 85-11511/20/12

12K0803-BS1 24.1 96X 2511/21/12 85-11511/21/12 CQC

12K0836-BS1 25.3 1012511/21/12 85-11511/21/12 CQC

12K0855-BS1 25.5 1022511/23/12 85-11511/23/12 CQC

12K0865-BS1 25.3 1012511/23/12 85-11511/23/12 CQC

12K0897-BS1 26.4 1062511/24/12 85-11511/24/12 CQC

12K0905-BS1 28.1 1132511/25/12 85-11511/25/12 CQC

12K1134-BS1 24.2 972511/30/12 85-11511/30/12 CQC

12K1135-BS1 23.9 962511/30/12 85-11511/30/12 CQC

01/02/13 15:46

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Analyzed By:

LCS/LCSD RPD1,2-Dichloropropane


8721.7259/1/129/1/1212I0005-BSD1 24.8 99 14 25 CQC

9824.5259/4/129/4/1212I0028-BSD1 23.8 95 3 25 CQC

8220.5259/5/129/5/1212I0081-BSD1 20.2 81 2 25 CQC,PSL

8822.1259/7/129/7/1212I0215-BSD1 23.1 92 4 25 CQC

9824.5259/12/129/12/1212I0352-BSD1 25.1 100 2 25 CQC

8320.7259/12/129/12/1212I0394-BSD1 19.8 79 5 25 CQC,PSL

10626.5259/18/129/18/1212I0598-BSD1 26.6 106 0.3 25 CQC

9523.6259/18/129/18/1212I0648-BSD1 23.8 95 0.7 25 CQC

8821.9259/25/129/25/1212I0926-BSD1 23.7 95 8 25 CQC

9022.5259/25/129/25/1212I0925-BSD1 22.1 89 1 25 CQC

10025259/28/129/28/1212I1065-BSD1 24.2 97 3 25 CQC

9523.8259/28/129/28/1212I1095-BSD1 24.1 96 1 25 CQC

9223259/29/129/29/1212I1107-BSD1 24.8 99 8 25 CQC

10225.62510/1/1210/1/1212J0008-BSD1 24.6 98 4 25 CQC

9122.72510/8/1210/8/1212J0298-BSD1 22.4 89 1 25

8922.22510/10/1210/10/1212J0389-BSD1 22.1 88 0.6 25

9222.92510/11/1210/11/1212J0445-BSD1 22.7 91 1 25 CQC

9122.92510/16/1210/16/1212J0620-BSD1 22.4 89 2 25 CQC

92232510/18/1210/18/1212J0736-BSD1 23.6 95 3 25 CQC

9323.12510/20/1210/20/1212J0821-BSD1 24.1 96 4 25 CQC

88222510/22/1210/22/1212J0850-BSD1 22.3 89 1 25 CQC

8922.22510/24/1210/24/1212J0972-BSD1 23.4 94 6 25 CQC

9323.32510/25/1210/25/1212J1010-BSD1 22.6 90 3 25 CQC

9122.82510/25/1210/25/1212J1038-BSD1 23.2 93 2 25 CQC

9724.32510/26/1210/26/1212J1059-BSD1 23.6 95 3 25 CQC

11127.82511/7/1211/7/1212K0235-BSD1 26.8 107 4 25 CQC

9724.22511/8/1211/8/1212K0286-BSD1 24 96 0.9 25 CQC

01/02/13 15:46

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LCS/LCSD RPD1,2-Dichloropropane%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

88222511/9/1211/9/1212K0341-BSD1 22.7 91 3 25

9323.32511/12/1211/12/1212K0415-BSD1 23.4 93 0.2 25 CQC

10225.42511/13/1211/13/1212K0462-BSD1 24.7 99 3 25 CQC

100252511/14/1211/14/1212K0522-BSD1X 24.5 98 2 25 CQC

9022.52511/14/1211/14/1212K0553-BSD1 25.4 102 12 25 CQC

9523.72511/14/1211/14/1212K0552-BSD1 23.9 96 0.9 25 CQC

10626.42511/15/1211/15/1212K0581-BSD1 26.2 105 0.6 25 CQC

9724.22511/20/1211/20/1212K0740-BSD1 22.9 91 6 25 CQC

96242511/20/1211/20/1212K0751-BSD1 25.2 101 5 25 CQC

10425.92511/20/1211/20/1212K0789-BSD1 26.5 106 2 25

10125.32511/21/1211/21/1212K0803-BSD1 24.1 96 5 25 CQC

9824.62511/21/1211/21/1212K0836-BSD1 25.3 101 3 25 CQC

10225.62511/23/1211/23/1212K0865-BSD1 25.3 101 1 25 CQC

10526.22511/23/1211/23/1212K0855-BSD1 25.5 102 3 25 CQC

10827.12511/24/1211/24/1212K0897-BSD1 26.4 106 2 25 CQC

11528.72511/25/1211/25/1212K0905-BSD1 28.1 113 2 25 CQC

9724.22511/30/1211/30/1212K1134-BSD1 24.2 97 0.2 25 CQC

10325.92511/30/1211/30/1212K1135-BSD1 23.9 96 8 25 CQC

01/02/13 15:46

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MS %R1,2-Dichloropropane


CQC81.1-116PVH2309-029323.412I0005-MS1 9/1/12 9/1/12 25

CQC81.1-116PVH2309-1110526.212I0028-MS1 9/4/12 9/4/12 25

CQC,PSL81.1-116PVH2037-077719.212I0081-MS1 9/5/12 9/5/12 25

CQC81.1-116PVI0290-039924.812I0215-MS1 9/7/12 9/7/12 25

CQC81.1-116PVI0609-099924.812I0352-MS1 9/12/12 9/12/12 25

CQC81.1-116PVI0525-069022.512I0394-MS1 9/12/12 9/12/12 25

CQC81.1-116PVI0894-0610726.812I0598-MS1 9/18/12 9/18/12 25

CQC81.1-116PVI1060-029624.112I0648-MS1 9/18/12 9/18/12 25

CQC81.1-116PVI1553-088922.312I0925-MS1 9/25/12 9/25/12 25

CQC81.1-116PVI1510-088922.312I0926-MS1 9/25/12 9/25/12 25

CQC81.1-116PVI1723-0310626.412I1065-MS1 9/28/12 9/28/12 25

CQC81.1-116PVI1822-029724.212I1095-MS1 9/28/12 9/28/12 25

CQC81.1-116PVI1869-051042612I1107-MS1 9/29/12 9/29/12 25

CQC81.1-116PVI1575-0110726.612J0008-MS1 10/1/12 10/1/12 25

81.1-116PVJ0513-039122.712J0298-MS1 10/8/12 10/8/12 25

81.1-116PVJ0682-019122.812J0389-MS1 10/10/12 10/10/12 25

CQC81.1-116PVJ0682-178721.812J0445-MS1 10/11/12 10/11/12 25

CQC81.1-116PVJ1065-02882212J0620-MS1 10/16/12 10/16/12 25

CQC81.1-116PVJ1237-029323.212J0736-MS1 10/18/12 10/18/12 25

CQC81.1-116PVJ1405-0210526.312J0821-MS1 10/20/12 10/20/12 25

CQC81.1-116PVJ1405-178922.312J0850-MS1 10/22/12 10/22/12 25

CQC81.1-116PVJ1577-029222.912J0972-MS1 10/24/12 10/24/12 25

CQC81.1-116PVJ1627-019323112J1010-MS1 10/25/12 10/25/12 250

CQC81.1-116PVJ1600-029423.512J1038-MS1 10/25/12 10/25/12 25

CQC81.1-116PVJ1577-18RE110025012J1059-MS1 10/26/12 10/26/12 250

CQC,PSL81.1-116PVK0237-0112230.412K0235-MS1 11/7/12 11/7/12 25

CQC81.1-116PVK0555-0411328.312K0286-MS1 11/8/12 11/8/12 25

81.1-116PVK0649-068822.112K0341-MS1 11/9/12 11/9/12 25

CQC81.1-116PVK0756-0110025.112K0415-MS1 11/12/12 11/12/12 25

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MS %R1,2-DichloropropaneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC81.1-116PVK0793-0210726.812K0462-MS1 11/13/12 11/13/12 25

CQC81.1-116PVK0281-0110125.112K0522-MS1 11/14/12 11/14/12 25

CQC81.1-116PVK0632-091002512K0553-MS1 11/14/12 11/14/12 25

CQC81.1-116PVK0684-029924.812K0552-MS1 11/14/12 11/14/12 25

CQC81.1-116PVK0696-0110526.412K0581-MS1 11/15/12 11/15/12 25

CQC81.1-116PVK0934-019423.612K0740-MS1 11/20/12 11/20/12 25

CQC81.1-116PVK0768-0210927.312K0751-MS1 11/20/12 11/20/12 25

CQC81.1-116PVK1220-029824.5X 12K0803-MS1 11/21/12 11/21/12 25

CQC81.1-116PVK1288-0310726.812K0836-MS1 11/21/12 11/21/12 25

CQC81.1-116PVK1375-0810225.612K0865-MS1 11/23/12 11/23/12 25

CQC81.1-116PVK1375-0210225.512K0855-MS1 11/23/12 11/23/12 25

CQC81.1-116PVK0988-0311328.412K0897-MS1 11/24/12 11/24/12 25

CQC81.1-116PVK1006-011162912K0905-MS1 11/25/12 11/25/12 25

CQC81.1-116PVK1450-1010526.312K1135-MS1 11/30/12 11/30/12 25

CQC81.1-116PVK1450-0311528.912K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPD1,2-Dichloropropane


9222.9259/1/129/1/1212I0005-MSD1 CQC2529323.4 PVH2309-02

10325.7259/4/129/4/1212I0028-MSD1 CQC25210526.2 PVH2309-11

8220.6259/5/129/5/1212I0081-MSD1 CQC2577719.2 PVH2037-07

9824.4259/7/129/7/1212I0215-MSD1 CQC2519924.8 PVI0290-03

9924.6259/12/129/12/1212I0352-MSD1 CQC250.79924.8 PVI0609-09

8922.2259/12/129/12/1212I0394-MSD1 CQC2519022.5 PVI0525-06

10826.9259/18/129/18/1212I0598-MSD1 CQC250.610726.8 PVI0894-06

9824.6259/18/129/18/1212I0648-MSD1 CQC2529624.1 PVI1060-02

9122.8259/25/129/25/1212I0925-MSD1 CQC2528922.3 PVI1553-08

9523.7259/25/129/25/1212I0926-MSD1 CQC2568922.3 PVI1510-08

10325.8259/28/129/28/1212I1065-MSD1 CQC25310626.4 PVI1723-03

10125.3259/28/129/28/1212I1095-MSD1 CQC2549724.2 PVI1822-02

11528.9259/29/129/29/1212I1107-MSD1 CQC251010426 PVI1869-05

10626.62510/1/1210/1/1212J0008-MSD1 CQC250.310726.6 PVI1575-01

9323.12510/8/1210/8/1212J0298-MSD1 2529122.7 PVJ0513-03

9022.62510/10/1210/10/1212J0389-MSD1 2519122.8 PVJ0682-01

8621.52510/11/1210/11/1212J0445-MSD1 CQC2518721.8 PVJ0682-17

9323.22510/16/1210/16/1212J0620-MSD1 CQC2558822 PVJ1065-02

9724.22510/18/1210/18/1212J0736-MSD1 CQC2549323.2 PVJ1237-02

11127.82510/20/1210/20/1212J0821-MSD1 CQC25610526.3 PVJ1405-02

9022.62510/22/1210/22/1212J0850-MSD1 CQC2518922.3 PVJ1405-17

96242510/24/1210/24/1212J0972-MSD1 CQC2559222.9 PVJ1577-02

9323325010/25/1210/25/1212J1010-MSD1 CQC250.693231 PVJ1627-01

9824.62510/25/1210/25/1212J1038-MSD1 CQC2549423.5 PVJ1600-02

10325825010/26/1210/26/1212J1059-MSD1 CQC254100250 PVJ1577-18RE1

120302511/7/1211/7/1212K0235-MSD1 CQC,PSL25212230.4 PVK0237-01

10927.22511/8/1211/8/1212K0286-MSD1 CQC25411328.3 PVK0555-04

8521.22511/9/1211/9/1212K0341-MSD1 2548822.1 PVK0649-06

10125.32511/12/1211/12/1212K0415-MSD1 CQC250.910025.1 PVK0756-01

104262511/13/1211/13/1212K0462-MSD1 CQC25310726.8 PVK0793-02

10225.62511/14/1211/14/1212K0522-MSD1 CQC25210125.1 PVK0281-01

01/02/13 15:46

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MS/MSD RPD1,2-Dichloropropane%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

10325.72511/14/1211/14/1212K0553-MSD1 CQC25310025 PVK0632-09

10626.52511/14/1211/14/1212K0552-MSD1 CQC2569924.8 PVK0684-02

10726.72511/15/1211/15/1212K0581-MSD1 CQC25110526.4 PVK0696-01

9724.32511/20/1211/20/1212K0740-MSD1 CQC2539423.6 PVK0934-01

11027.62511/20/1211/20/1212K0751-MSD1 CQC25110927.3 PVK0768-02

10626.62511/21/1211/21/1212K0803-MSD1 CQC2589824.5 PVK1220-02

10626.52511/21/1211/21/1212K0836-MSD1 CQC250.910726.8 PVK1288-03

10325.92511/23/1211/23/1212K0865-MSD1 CQC25110225.6 PVK1375-08

10526.32511/23/1211/23/1212K0855-MSD1 CQC25310225.5 PVK1375-02

11127.82511/24/1211/24/1212K0897-MSD1 CQC25211328.4 PVK0988-03

11829.62511/25/1211/25/1212K0905-MSD1 CQC,PSL25211629 PVK1006-01

10726.82511/30/1211/30/1212K1135-MSD1 CQC25210526.3 PVK1450-10

11328.32512/1/1211/30/1212K1134-MSD1 CQC25211528.9 PVK1450-03

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BLK1,2-Dichloropropane

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

~------------------------------------------~ 0.1

0.0 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

Plotted: 44

MDL: 0.15

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

3s: 0

4s: 0

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LCS %R1,3,5-Trimethylbenzene


12K0235-BS1 30.3 1212511/7/12 80.1-11911/7/12 CQC,PSL

12K0286-BS1 25.1 1012511/8/12 80.1-11911/8/12 CQC

12K0341-BS1 26.4 1062511/9/12 80.1-11911/9/12

12K0415-BS1 23.5 942511/12/12 80.1-11911/12/12 CQC

12K0462-BS1 24 962511/13/12 80.1-11911/13/12 CQC

12K0522-BS1 29.4 1172511/14/12 80.1-11911/14/12 CQC

12K0803-BS1 26.4 1062511/21/12 80.1-11911/21/12 CQC

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LCS/LCSD RPD1,3,5-Trimethylbenzene


116292511/7/1211/7/1212K0235-BSD1 30.3 121 4 25 CQC

10526.22511/8/1211/8/1212K0286-BSD1 25.1 101 4 25 CQC

10626.62511/9/1211/9/1212K0341-BSD1 26.4 106 0.5 25

10024.92511/12/1211/12/1212K0415-BSD1 23.5 94 6 25 CQC

104262511/13/1211/13/1212K0462-BSD1 24 96 8 25 CQC

12230.42511/14/1211/14/1212K0522-BSD1 29.4 117 4 25 CQC,L

11027.52511/21/1211/21/1212K0803-BSD1 26.4 106 4 25 CQC

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MS %R1,3,5-Trimethylbenzene


CQC75.1-123PVK0237-0111829.412K0235-MS1 11/7/12 11/7/12 25

CQC75.1-123PVK0555-0411729.312K0286-MS1 11/8/12 11/8/12 25

75.1-123PVK0649-061082712K0341-MS1 11/9/12 11/9/12 25

CQC75.1-123PVK0756-0110125.212K0415-MS1 11/12/12 11/12/12 25

CQC75.1-123PVK0793-0210526.212K0462-MS1 11/13/12 11/13/12 25

CQC75.1-123PVK0281-01 (10.5)1063712K0522-MS1 11/14/12 11/14/12 25

CQC75.1-123PVK1220-0211027.612K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPD1,3,5-Trimethylbenzene


12230.42511/7/1211/7/1212K0235-MSD1 CQC25311829.4 PVK0237-01

11027.52511/8/1211/8/1212K0286-MSD1 CQC25611729.3 PVK0555-04

10927.22511/9/1211/9/1212K0341-MSD1 25110827 PVK0649-06

9624.12511/12/1211/12/1212K0415-MSD1 CQC25510125.2 PVK0756-01

116292511/13/1211/13/1212K0462-MSD1 CQC251010526.2 PVK0793-02

10336.32511/14/1211/14/1212K0522-MSD1 CQC25210637 PVK0281-01 (10.5)

12130.32511/21/1211/21/1212K0803-MSD1 CQC25911027.6 PVK1220-02

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BLK1,3,5-Trimethylbenzene

01/02/13 15:46

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12K0235-BS1 29.4 1182511/7/12 83.9-11411/7/12 CQC,PSL

12K0286-BS1 26.2 1052511/8/12 83.9-11411/8/12 CQC

12K0341-BS1 26.8 1072511/9/12 83.9-11411/9/12

12K0415-BS1 24.7 992511/12/12 83.9-11411/12/12 CQC

12K0462-BS1 25.8 1032511/13/12 83.9-11411/13/12 CQC

12K0522-BS1 26.9 1072511/14/12 83.9-11411/14/12 CQC

12K0803-BS1 24.6 982511/21/12 83.9-11411/21/12 CQC

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11929.72511/7/1211/7/1212K0235-BSD1 29.4 118 0.8 25 CQC,PSL

10726.72511/8/1211/8/1212K0286-BSD1 26.2 105 2 25 CQC

10526.42511/9/1211/9/1212K0341-BSD1 26.8 107 2 25

10025.12511/12/1211/12/1212K0415-BSD1 24.7 99 2 25 CQC

10526.32511/13/1211/13/1212K0462-BSD1 25.8 103 2 25 CQC

10726.62511/14/1211/14/1212K0522-BSD1 26.9 107 0.8 25 CQC

10025.12511/21/1211/21/1212K0803-BSD1 24.6 98 2 25 CQC

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CQC,PSL80.4-114PVK0237-011243112K0235-MS1 11/7/12 11/7/12 25

CQC,M780.4-114PVK0555-0412330.812K0286-MS1 11/8/12 11/8/12 25

80.4-114PVK0649-0610526.412K0341-MS1 11/9/12 11/9/12 25

CQC80.4-114PVK0756-0110526.212K0415-MS1 11/12/12 11/12/12 25

CQC80.4-114PVK0793-021082712K0462-MS1 11/13/12 11/13/12 25

CQC80.4-114PVK0281-0110526.412K0522-MS1 11/14/12 11/14/12 25

CQC80.4-114PVK1220-029924.912K0803-MS1 11/21/12 11/21/12 25

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128322511/7/1211/7/1212K0235-MSD1 CQC,PSL25312431 PVK0237-01

116292511/8/1211/8/1212K0286-MSD1 CQC,M725612330.8 PVK0555-04

10826.92511/9/1211/9/1212K0341-MSD1 25210526.4 PVK0649-06

10125.32511/12/1211/12/1212K0415-MSD1 CQC25310526.2 PVK0756-01

10726.72511/13/1211/13/1212K0462-MSD1 CQC25110827 PVK0793-02

10526.32511/14/1211/14/1212K0522-MSD1 CQC250.110526.4 PVK0281-01

11027.62511/21/1211/21/1212K0803-MSD1 CQC25109924.9 PVK1220-02

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01/02/13 15:46

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Analyzed By:



12K0235-BS1 29.5 1182511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 24.9 1002511/8/12 85-11511/8/12 CQC

12K0341-BS1 24.2 972511/9/12 85-11511/9/12

12K0415-BS1 23.2 932511/12/12 85-11511/12/12 CQC

12K0462-BS1 26.7 1072511/13/12 85-11511/13/12 CQC

12K0522-BS1 26.8 1072511/14/12 85-11511/14/12 CQC

12K0803-BS1 25.4 1022511/21/12 85-11511/21/12 CQC

01/02/13 15:46

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12029.92511/7/1211/7/1212K0235-BSD1 29.5 118 1 25 CQC,PSL

10225.62511/8/1211/8/1212K0286-BSD1 24.9 100 3 25 CQC

9423.52511/9/1211/9/1212K0341-BSD1 24.2 97 3 25

8922.32511/12/1211/12/1212K0415-BSD1 23.2 93 4 25 CQC

104262511/13/1211/13/1212K0462-BSD1 26.7 107 2 25 CQC

11127.82511/14/1211/14/1212K0522-BSD1 26.8 107 4 25 CQC

10726.72511/21/1211/21/1212K0803-BSD1 25.4 102 5 25 CQC

01/02/13 15:46

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CQC77.1-119PVK0237-0111428.412K0235-MS1 11/7/12 11/7/12 25

CQC77.1-119PVK0555-0411127.612K0286-MS1 11/8/12 11/8/12 25

77.1-119PVK0649-069824.612K0341-MS1 11/9/12 11/9/12 25

CQC77.1-119PVK0756-019724.312K0415-MS1 11/12/12 11/12/12 25

CQC77.1-119PVK0793-0211027.512K0462-MS1 11/13/12 11/13/12 25

CQC77.1-119PVK0281-011042612K0522-MS1 11/14/12 11/14/12 25

CQC77.1-119PVK1220-029824.612K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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12030.12511/7/1211/7/1212K0235-MSD1 CQC25611428.4 PVK0237-01

112282511/8/1211/8/1212K0286-MSD1 CQC25111127.6 PVK0555-04

9624.12511/9/1211/9/1212K0341-MSD1 2529824.6 PVK0649-06

10125.22511/12/1211/12/1212K0415-MSD1 CQC2539724.3 PVK0756-01

11127.72511/13/1211/13/1212K0462-MSD1 CQC250.811027.5 PVK0793-02

10626.42511/14/1211/14/1212K0522-MSD1 CQC25110426 PVK0281-01

96242511/21/1211/21/1212K0803-MSD1 CQC2529824.6 PVK1220-02

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2.0,-------------------------~

1 .8 Plotted: 7

1.6 j-:--:-;--:-;--:-;--:-;--:-;--:-;--:-;--:-;--:-;--:-;--:-;--:-;--:-;--:-;--:-;--:-;--:-;---------------l MDL: 0.18

MRL: 1 1.4 ..... .

1.2 ..... . Rejected: 0

1.0 j------------------------------1 Stdv: 0.371

0.8 · · · · · · -" . . . . . . . . . . . A . . Mean: 0.541

o.6 t----·-·-·- ·- ·- ·_·_· _· _· _· _· _· _· ~~-· ..:.· ~·~· ..:....:..:....:..:....:..:....:..:....:.:..· .:._· .:,1-/. ::.·..:.·..:.·..:.· '....:·.:::!·~·:--·.:._·.:._· .:._. :.... :... . .:._ • .:._· .:._· .:.· .:.· ..:.·..:.·..;./L ·...:·I 2s: 1.28

:: ·······················~·····/ ·······~·····/ · !::~: 0.0 \---------""'~./>;£_ _____ '\.....¥./ __ _J

2 3 4 5 6 7

01/02/13 15:46

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12K0235-BS1 29.2 1172511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 25.8 1032511/8/12 85-11511/8/12 CQC

12K0341-BS1 25.9 1042511/9/12 85-11511/9/12

12K0415-BS1 24.6 982511/12/12 85-11511/12/12 CQC

12K0462-BS1 25 1002511/13/12 85-11511/13/12 CQC

12K0522-BS1 25.4 1012511/14/12 85-11511/14/12 CQC

12K0803-BS1 24.2 972511/21/12 85-11511/21/12 CQC

01/02/13 15:46

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11428.52511/7/1211/7/1212K0235-BSD1 29.2 117 2 25 CQC

10626.52511/8/1211/8/1212K0286-BSD1 25.8 103 3 25 CQC

10225.62511/9/1211/9/1212K0341-BSD1 25.9 104 1 25

10025.12511/12/1211/12/1212K0415-BSD1 24.6 98 2 25 CQC

10125.42511/13/1211/13/1212K0462-BSD1 25 100 1 25 CQC

10526.22511/14/1211/14/1212K0522-BSD1 25.4 101 3 25 CQC

10024.92511/21/1211/21/1212K0803-BSD1 24.2 97 3 25 CQC

01/02/13 15:46

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CQC,PSL81.3-110PVK0237-011203012K0235-MS1 11/7/12 11/7/12 25

CQC,M781.3-110PVK0555-0411829.612K0286-MS1 11/8/12 11/8/12 25

81.3-110PVK0649-0610225.612K0341-MS1 11/9/12 11/9/12 25

CQC81.3-110PVK0756-0110125.312K0415-MS1 11/12/12 11/12/12 25

CQC81.3-110PVK0793-021042612K0462-MS1 11/13/12 11/13/12 25

CQC81.3-110PVK0281-019924.712K0522-MS1 11/14/12 11/14/12 25

CQC81.3-110PVK1220-0210024.912K0803-MS1 11/21/12 11/21/12 25

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12531.32511/7/1211/7/1212K0235-MSD1 CQC,PSL25412030 PVK0237-01

11328.22511/8/1211/8/1212K0286-MSD1 CQC,M725511829.6 PVK0555-04

10125.22511/9/1211/9/1212K0341-MSD1 25110225.6 PVK0649-06

10426.12511/12/1211/12/1212K0415-MSD1 CQC25310125.3 PVK0756-01

104262511/13/1211/13/1212K0462-MSD1 CQC250.310426 PVK0793-02

10325.82511/14/1211/14/1212K0522-MSD1 CQC2549924.7 PVK0281-01

10827.12511/21/1211/21/1212K0803-MSD1 CQC25910024.9 PVK1220-02

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01/02/13 15:46

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12K0235-BS1 41.3 1652511/7/12 70.8-12811/7/12 CQC,L

12K0286-BS1 39.2 1572511/8/12 70.8-12811/8/12 CQC,C,L

12K0341-BS1 38.4 1542511/9/12 70.8-12811/9/12 C

12K0415-BS1 24.2 972511/12/12 70.8-12811/12/12 CQC

12K0462-BS1 25.8 1032511/13/12 70.8-12811/13/12 CQC

12K0522-BS1 27 1082511/14/12 70.8-12811/14/12 CQC

12K0803-BS1 26.2 1052511/21/12 70.8-12811/21/12 CQC

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15338.22511/7/1211/7/1212K0235-BSD1 41.3 165 8 25 CQC,L

16039.92511/8/1211/8/1212K0286-BSD1 39.2 157 2 25 CQC,C,L

14937.32511/9/1211/9/1212K0341-BSD1 38.4 154 3 25 C

9022.42511/12/1211/12/1212K0415-BSD1 24.2 97 8 25 CQC

10526.32511/13/1211/13/1212K0462-BSD1 25.8 103 2 25 CQC

11127.72511/14/1211/14/1212K0522-BSD1 27 108 3 25 CQC

10827.12511/21/1211/21/1212K0803-BSD1 26.2 105 3 25 CQC

01/02/13 15:46

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CQC,M1466.5-134PVK0237-0117543.912K0235-MS1 11/7/12 11/7/12 25

CQC,C,M1466.5-134PVK0555-0418145.212K0286-MS1 11/8/12 11/8/12 25

C66.5-134PVK0649-0615438.612K0341-MS1 11/9/12 11/9/12 25

CQC66.5-134PVK0756-019824.512K0415-MS1 11/12/12 11/12/12 25

CQC66.5-134PVK0793-0210425.912K0462-MS1 11/13/12 11/13/12 25

CQC66.5-134PVK0281-0110626.412K0522-MS1 11/14/12 11/14/12 25

CQC66.5-134PVK1220-029724.312K0803-MS1 11/21/12 11/21/12 25

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176442511/7/1211/7/1212K0235-MSD1 CQC,M14250.417543.9 PVK0237-01

17443.42511/8/1211/8/1212K0286-MSD1 CQC,C,M1425418145.2 PVK0555-04

15037.52511/9/1211/9/1212K0341-MSD1 C25315438.6 PVK0649-06

9724.22511/12/1211/12/1212K0415-MSD1 CQC2519824.5 PVK0756-01

10425.92511/13/1211/13/1212K0462-MSD1 CQC250.210425.9 PVK0793-02

11027.42511/14/1211/14/1212K0522-MSD1 CQC25410626.4 PVK0281-01

10325.72511/21/1211/21/1212K0803-MSD1 CQC2569724.3 PVK1220-02

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4 5 6 7

Plotted: 7

MDL: 0.18

MRL: 2

Rejected: 0

Stdv: 0

Mean: 0

2s: 0

3s: 0

4s: 0

01/02/13 15:46

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LCS %R2-Butanone (MEK)


12I0005-BS1 28.6 115259/1/12 45.6-1419/1/12 CQC

12I0028-BS1 25.4 101259/4/12 45.6-1419/4/12 CQC

12I0081-BS1 24.1 96259/5/12 45.6-1419/5/12 CQC

12I0215-BS1 22.8 91259/7/12 45.6-1419/7/12 CQC

12I0352-BS1 23 92259/12/12 45.6-1419/12/12 CQC

12I0394-BS1 23.6 94259/12/12 45.6-1419/12/12 CQC

12I0598-BS1 29.3 117259/18/12 45.6-1419/18/12 CQC

12I0648-BS1 31.4 126259/18/12 45.6-1419/18/12 CQC

12I0926-BS1 22.8 91259/25/12 45.6-1419/25/12 CQC

12I0925-BS1 28.4 114259/25/12 45.6-1419/25/12 CQC

12I1065-BS1 26.8 107259/28/12 45.6-1419/28/12 CQC

12I1095-BS1 25.8 103259/28/12 45.6-1419/28/12 CQC

12I1107-BS1 27 108259/29/12 45.6-1419/29/12 CQC

12J0008-BS1 29.3 1172510/1/12 45.6-14110/1/12 CQC

12J0298-BS1 23 922510/8/12 45.6-14110/8/12

12J0389-BS1 26.1 1042510/10/12 45.6-14110/10/12

12J0445-BS1 29.6 1182510/11/12 45.6-14110/11/12 CQC

12J0620-BS1 21.8 872510/16/12 45.6-14110/16/12 CQC

12J0736-BS1 25.2 1012510/18/12 45.6-14110/18/12 CQC

12J0821-BS1 28.2 1132510/20/12 45.6-14110/20/12 CQC

12J0850-BS1 27.4 1102510/22/12 45.6-14110/22/12 CQC

12J0972-BS1 33.2 1332510/24/12 45.6-14110/24/12 CQC

12J1010-BS1 21.5 862510/25/12 45.6-14110/25/12 CQC

12J1038-BS1 19 762510/25/12 45.6-14110/25/12 CQC

12J1059-BS1 28.5 1142510/26/12 45.6-14110/26/12 CQC

12K0235-BS1 27.7 1112511/7/12 45.6-14111/7/12 CQC

12K0286-BS1 24.1 962511/8/12 45.6-14111/8/12 CQC

01/02/13 15:46

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LCS %R2-Butanone (MEK)Limits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 18.8 752511/9/12 45.6-14111/9/12

12K0415-BS1 21.5 862511/12/12 45.6-14111/12/12 CQC

12K0462-BS1 23.2 932511/13/12 45.6-14111/13/12 CQC

12K0522-BS1 32.8 131X 2511/14/12 45.6-14111/14/12 CQC

12K0553-BS1 25.7 1032511/14/12 45.6-14111/14/12 CQC

12K0552-BS1 23.6 952511/14/12 45.6-14111/14/12 CQC

12K0581-BS1 27.2 1092511/15/12 45.6-14111/15/12 CQC

12K0740-BS1 26.8 1072511/20/12 45.6-14111/20/12 CQC

12K0751-BS1 27.2 1092511/20/12 45.6-14111/20/12 CQC

12K0789-BS1 33.3 1332511/20/12 45.6-14111/20/12

12K0803-BS1 23.6 942511/21/12 45.6-14111/21/12 CQC

12K0836-BS1 31.9 1282511/21/12 45.6-14111/21/12 CQC

12K0855-BS1 29.9 1202511/23/12 45.6-14111/23/12 CQC

12K0865-BS1 28.7 1152511/23/12 45.6-14111/23/12 CQC

12K0897-BS1 29.2 1172511/24/12 45.6-14111/24/12 CQC

12K0905-BS1 37.2 1492511/25/12 45.6-14111/25/12 CQC,PSL

12K1134-BS1 21.7 872511/30/12 45.6-14111/30/12 CQC

12K1135-BS1 25.4 1012511/30/12 45.6-14111/30/12 CQC

01/02/13 15:46

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Analyzed By:

LCS/LCSD RPD2-Butanone (MEK)


9623.9259/1/129/1/1212I0005-BSD1 28.6 115 18 25 CQC

10826.9259/4/129/4/1212I0028-BSD1 25.4 101 6 25 CQC

6917.2259/5/129/5/1212I0081-BSD1 24.1 96 34 25 CQC,R-7

8521.2259/7/129/7/1212I0215-BSD1 22.8 91 7 25 CQC

10426.1259/12/129/12/1212I0352-BSD1 23 92 12 25 CQC

8320.8259/12/129/12/1212I0394-BSD1 23.6 94 12 25 CQC

10927.2259/18/129/18/1212I0598-BSD1 29.3 117 7 25 CQC

12130.1259/18/129/18/1212I0648-BSD1 31.4 126 4 25 CQC

9724.2259/25/129/25/1212I0926-BSD1 22.8 91 6 25 CQC

10626.5259/25/129/25/1212I0925-BSD1 28.4 114 7 25 CQC

10325.7259/28/129/28/1212I1065-BSD1 26.8 107 4 25 CQC

10125.4259/28/129/28/1212I1095-BSD1 25.8 103 2 25 CQC

10526.4259/29/129/29/1212I1107-BSD1 27 108 2 25 CQC

12230.42510/1/1210/1/1212J0008-BSD1 29.3 117 4 25 CQC

10425.92510/8/1210/8/1212J0298-BSD1 23 92 12 25

9724.32510/10/1210/10/1212J0389-BSD1 26.1 104 7 25

11528.72510/11/1210/11/1212J0445-BSD1 29.6 118 3 25 CQC

8421.12510/16/1210/16/1212J0620-BSD1 21.8 87 3 25 CQC

92232510/18/1210/18/1212J0736-BSD1 25.2 101 9 25 CQC

10526.32510/20/1210/20/1212J0821-BSD1 28.2 113 7 25 CQC

10125.32510/22/1210/22/1212J0850-BSD1 27.4 110 8 25 CQC

8019.92510/24/1210/24/1212J0972-BSD1 33.2 133 50 25 CQC,R-7

7518.82510/25/1210/25/1212J1010-BSD1 21.5 86 13 25 CQC

7819.62510/25/1210/25/1212J1038-BSD1 19 76 3 25 CQC

10225.62510/26/1210/26/1212J1059-BSD1 28.5 114 11 25 CQC

100252511/7/1211/7/1212K0235-BSD1 27.7 111 10 25 CQC

92232511/8/1211/8/1212K0286-BSD1 24.1 96 5 25 CQC

01/02/13 15:46

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LCS/LCSD RPD2-Butanone (MEK)%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

7518.92511/9/1211/9/1212K0341-BSD1 18.8 75 0.6 25

7518.72511/12/1211/12/1212K0415-BSD1 21.5 86 14 25 CQC

10125.32511/13/1211/13/1212K0462-BSD1 23.2 93 9 25 CQC

108272511/14/1211/14/1212K0522-BSD1 32.8 131 19 25 CQC

9223.12511/14/1211/14/1212K0553-BSD1 25.7 103 11 25 CQC

8721.82511/14/1211/14/1212K0552-BSD1 23.6 95 8 25 CQC

11127.72511/15/1211/15/1212K0581-BSD1 27.2 109 2 25 CQC

8822.12511/20/1211/20/1212K0740-BSD1 26.8 107 19 25 CQC

7719.32511/20/1211/20/1212K0751-BSD1 27.2 109 34 25 CQC,R-7

11528.72511/20/1211/20/1212K0789-BSD1 33.3 133 15 25

11027.42511/21/1211/21/1212K0803-BSD1X 23.6 94 15 25 CQC

9924.72511/21/1211/21/1212K0836-BSD1 31.9 128 25 25 CQC

14135.32511/23/1211/23/1212K0855-BSD1 29.9 120 16 25 CQC

11328.42511/23/1211/23/1212K0865-BSD1 28.7 115 1 25 CQC

140352511/24/1211/24/1212K0897-BSD1 29.2 117 18 25 CQC

12531.22511/25/1211/25/1212K0905-BSD1 37.2 149 17 25 CQC

9824.62511/30/1211/30/1212K1134-BSD1 21.7 87 13 25 CQC

92232511/30/1211/30/1212K1135-BSD1 25.4 101 10 25 CQC

01/02/13 15:46

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Analyzed By:

MS %R2-Butanone (MEK)


CQC41.6-130PVH2309-028320.812I0005-MS1 9/1/12 9/1/12 25

CQC41.6-130PVH2309-118320.812I0028-MS1 9/4/12 9/4/12 25

CQC41.6-130PVH2037-077017.612I0081-MS1 9/5/12 9/5/12 25

CQC41.6-130PVI0290-039924.912I0215-MS1 9/7/12 9/7/12 25

CQC41.6-130PVI0609-097719.212I0352-MS1 9/12/12 9/12/12 25

CQC41.6-130PVI0525-067017.512I0394-MS1 9/12/12 9/12/12 25

CQC41.6-130PVI0894-069122.712I0598-MS1 9/18/12 9/18/12 25

CQC41.6-130PVI1060-0211027.412I0648-MS1 9/18/12 9/18/12 25

CQC41.6-130PVI1553-088120.212I0925-MS1 9/25/12 9/25/12 25

CQC41.6-130PVI1510-087618.912I0926-MS1 9/25/12 9/25/12 25

CQC41.6-130PVI1723-0311127.712I1065-MS1 9/28/12 9/28/12 25

CQC41.6-130PVI1822-0210626.512I1095-MS1 9/28/12 9/28/12 25

CQC41.6-130PVI1869-0510325.812I1107-MS1 9/29/12 9/29/12 25

CQC41.6-130PVI1575-0110526.312J0008-MS1 10/1/12 10/1/12 25

41.6-130PVJ0513-038020.112J0298-MS1 10/8/12 10/8/12 25

41.6-130PVJ0682-018721.812J0389-MS1 10/10/12 10/10/12 25

CQC41.6-130PVJ0682-178220.612J0445-MS1 10/11/12 10/11/12 25

CQC41.6-130PVJ1065-026917.312J0620-MS1 10/16/12 10/16/12 25

CQC41.6-130PVJ1237-028120.412J0736-MS1 10/18/12 10/18/12 25

CQC41.6-130PVJ1405-027919.712J0821-MS1 10/20/12 10/20/12 25

CQC41.6-130PVJ1405-177518.812J0850-MS1 10/22/12 10/22/12 25

CQC41.6-130PVJ1577-027819.512J0972-MS1 10/24/12 10/24/12 25

CQC41.6-130PVJ1627-016616412J1010-MS1 10/25/12 10/25/12 250

CQC41.6-130PVJ1600-026215.612J1038-MS1 10/25/12 10/25/12 25

CQC41.6-130PVJ1577-18RE17518812J1059-MS1 10/26/12 10/26/12 250

CQC41.6-130PVK0237-0110225.512K0235-MS1 11/7/12 11/7/12 25

CQC41.6-130PVK0555-04 (6.27)10532.512K0286-MS1 11/8/12 11/8/12 25

41.6-130PVK0649-06 (6.75)7024.312K0341-MS1 11/9/12 11/9/12 25

CQC41.6-130PVK0756-01 (9)8931.212K0415-MS1 11/12/12 11/12/12 25

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MS %R2-Butanone (MEK)Source%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC41.6-130PVK0793-027719.412K0462-MS1 11/13/12 11/13/12 25

CQC41.6-130PVK0281-017117.8X 12K0522-MS1 11/14/12 11/14/12 25

CQC41.6-130PVK0632-096516.212K0553-MS1 11/14/12 11/14/12 25

CQC41.6-130PVK0684-027919.812K0552-MS1 11/14/12 11/14/12 25

CQC41.6-130PVK0696-016115.212K0581-MS1 11/15/12 11/15/12 25

CQC41.6-130PVK0934-017518.812K0740-MS1 11/20/12 11/20/12 25

CQC41.6-130PVK0768-02922312K0751-MS1 11/20/12 11/20/12 25

CQC41.6-130PVK1220-028320.812K0803-MS1 11/21/12 11/21/12 25

CQC41.6-130PVK1288-039022.412K0836-MS1 11/21/12 11/21/12 25

CQC41.6-130PVK1375-088421.112K0865-MS1 11/23/12 11/23/12 25

CQC41.6-130PVK1375-0210024.912K0855-MS1 11/23/12 11/23/12 25

CQC41.6-130PVK0988-038020.112K0897-MS1 11/24/12 11/24/12 25

CQC41.6-130PVK1006-019222.912K0905-MS1 11/25/12 11/25/12 25

CQC41.6-130PVK1450-108320.712K1135-MS1 11/30/12 11/30/12 25

CQC41.6-130PVK1450-039222.912K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPD2-Butanone (MEK)


8621.4259/1/129/1/1212I0005-MSD1 CQC2538320.8 PVH2309-02

9222.9259/4/129/4/1212I0028-MSD1 CQC25108320.8 PVH2309-11

6516.3259/5/129/5/1212I0081-MSD1 CQC2587017.6 PVH2037-07

9222.9259/7/129/7/1212I0215-MSD1 CQC2589924.9 PVI0290-03

8421.1259/12/129/12/1212I0352-MSD1 CQC2597719.2 PVI0609-09

7919.7259/12/129/12/1212I0394-MSD1 CQC25127017.5 PVI0525-06

9223259/18/129/18/1212I0598-MSD1 CQC2529122.7 PVI0894-06

11127.8259/18/129/18/1212I0648-MSD1 CQC25111027.4 PVI1060-02

9122.8259/25/129/25/1212I0925-MSD1 CQC25128120.2 PVI1553-08

7719.2259/25/129/25/1212I0926-MSD1 CQC2517618.9 PVI1510-08

10225.4259/28/129/28/1212I1065-MSD1 CQC25911127.7 PVI1723-03

11428.4259/28/129/28/1212I1095-MSD1 CQC25710626.5 PVI1822-02

12030259/29/129/29/1212I1107-MSD1 CQC251510325.8 PVI1869-05

120302510/1/1210/1/1212J0008-MSD1 CQC251310526.3 PVI1575-01

84212510/8/1210/8/1212J0298-MSD1 2558020.1 PVJ0513-03

8320.72510/10/1210/10/1212J0389-MSD1 2558721.8 PVJ0682-01

7819.52510/11/1210/11/1212J0445-MSD1 CQC2568220.6 PVJ0682-17

6716.72510/16/1210/16/1212J0620-MSD1 CQC2546917.3 PVJ1065-02

7719.32510/18/1210/18/1212J0736-MSD1 CQC2558120.4 PVJ1237-02

8220.62510/20/1210/20/1212J0821-MSD1 CQC2547919.7 PVJ1405-02

9022.52510/22/1210/22/1212J0850-MSD1 CQC25187518.8 PVJ1405-17

8721.82510/24/1210/24/1212J0972-MSD1 CQC25117819.5 PVJ1577-02

8220425010/25/1210/25/1212J1010-MSD1 CQC252266164 PVJ1627-01

7217.92510/25/1210/25/1212J1038-MSD1 CQC25146215.6 PVJ1600-02

7518625010/26/1210/26/1212J1059-MSD1 CQC250.975188 PVJ1577-18RE1

9423.52511/7/1211/7/1212K0235-MSD1 CQC25810225.5 PVK0237-01

10532.62511/8/1211/8/1212K0286-MSD1 CQC250.210532.5 PVK0555-04 (6.27)

73252511/9/1211/9/1212K0341-MSD1 2537024.3 PVK0649-06 (6.75)

8730.72511/12/1211/12/1212K0415-MSD1 CQC2528931.2 PVK0756-01 (9)

7318.22511/13/1211/13/1212K0462-MSD1 CQC2567719.4 PVK0793-02

7117.72511/14/1211/14/1212K0522-MSD1X CQC250.47117.8 PVK0281-01

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MS/MSD RPD2-Butanone (MEK)%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

6014.92511/14/1211/14/1212K0553-MSD1 CQC2586516.2 PVK0632-09

9122.82511/14/1211/14/1212K0552-MSD1 CQC25147919.8 PVK0684-02

5714.22511/15/1211/15/1212K0581-MSD1 CQC2576115.2 PVK0696-01

72182511/20/1211/20/1212K0740-MSD1 CQC2547518.8 PVK0934-01

8220.42511/20/1211/20/1212K0751-MSD1 CQC25129223 PVK0768-02

9122.82511/21/1211/21/1212K0803-MSD1X CQC2598320.8 PVK1220-02

9924.72511/21/1211/21/1212K0836-MSD1 CQC25109022.4 PVK1288-03

7618.92511/23/1211/23/1212K0865-MSD1 CQC25118421.1 PVK1375-08

8721.92511/23/1211/23/1212K0855-MSD1 CQC251310024.9 PVK1375-02

9924.72511/24/1211/24/1212K0897-MSD1 CQC25208020.1 PVK0988-03

9824.62511/25/1211/25/1212K0905-MSD1 CQC2579222.9 PVK1006-01

10726.82511/30/1211/30/1212K1135-MSD1 CQC,R-725268320.7 PVK1450-10

7117.72512/1/1211/30/1212K1134-MSD1 CQC,R-725269222.9 PVK1450-03

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BLK2-Butanone (MEK)

5

Plotted: 44

4 MDL: 1.8

MRL: 5

3 Rejected: 2

Stdv: 0.0485

2 Mean: O.Q1 05

2s: 0.107

3s: 0.156

4s: 0.204

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %R2-Chlorotoluene


12K0235-BS1 28.8 1152511/7/12 78.6-12011/7/12 CQC

12K0286-BS1 24.4 982511/8/12 78.6-12011/8/12 CQC

12K0341-BS1 24.9 1002511/9/12 78.6-12011/9/12

12K0415-BS1 22.4 902511/12/12 78.6-12011/12/12 CQC

12K0462-BS1 23.5 942511/13/12 78.6-12011/13/12 CQC

12K0522-BS1 28.3 1132511/14/12 78.6-12011/14/12 CQC

12K0803-BS1 25.3 1012511/21/12 78.6-12011/21/12 CQC

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LCS/LCSD RPD2-Chlorotoluene


11127.92511/7/1211/7/1212K0235-BSD1 28.8 115 3 25 CQC

10024.92511/8/1211/8/1212K0286-BSD1 24.4 98 2 25 CQC

9924.62511/9/1211/9/1212K0341-BSD1 24.9 100 1 25

9724.12511/12/1211/12/1212K0415-BSD1 22.4 90 7 25 CQC

9724.12511/13/1211/13/1212K0462-BSD1 23.5 94 2 25 CQC

11528.62511/14/1211/14/1212K0522-BSD1 28.3 113 1 25 CQC

10626.52511/21/1211/21/1212K0803-BSD1 25.3 101 5 25 CQC

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MS %R2-Chlorotoluene


CQC75.2-122PVK0237-0111428.612K0235-MS1 11/7/12 11/7/12 25

CQC75.2-122PVK0555-041162912K0286-MS1 11/8/12 11/8/12 25

75.2-122PVK0649-0610425.912K0341-MS1 11/9/12 11/9/12 25

CQC75.2-122PVK0756-01962412K0415-MS1 11/12/12 11/12/12 25

CQC75.2-122PVK0793-021002512K0462-MS1 11/13/12 11/13/12 25

CQC75.2-122PVK0281-0111127.712K0522-MS1 11/14/12 11/14/12 25

CQC75.2-122PVK1220-0210626.412K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPD2-Chlorotoluene


11729.22511/7/1211/7/1212K0235-MSD1 CQC25211428.6 PVK0237-01

10927.32511/8/1211/8/1212K0286-MSD1 CQC25611629 PVK0555-04

10025.12511/9/1211/9/1212K0341-MSD1 25310425.9 PVK0649-06

9724.12511/12/1211/12/1212K0415-MSD1 CQC250.79624 PVK0756-01

11228.12511/13/1211/13/1212K0462-MSD1 CQC251210025 PVK0793-02

11428.62511/14/1211/14/1212K0522-MSD1 CQC25311127.7 PVK0281-01

11628.92511/21/1211/21/1212K0803-MSD1 CQC25910626.4 PVK1220-02

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BLK2-Chlorotoluene

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LCS %R2-Hexanone


12K0235-BS1 32.8 1312511/7/12 58.5-13511/7/12 CQC

12K0286-BS1 27.5 1102511/8/12 58.5-13511/8/12 CQC

12K0341-BS1 24.1 962511/9/12 58.5-13511/9/12

12K0415-BS1 24.4 982511/12/12 58.5-13511/12/12 CQC

12K0462-BS1 25.2 1012511/13/12 58.5-13511/13/12 CQC

12K0522-BS1 31.7 1272511/14/12 58.5-13511/14/12 CQC

12K0803-BS1 28.2 1132511/21/12 58.5-13511/21/12 CQC

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LCS/LCSD RPD2-Hexanone


12531.22511/7/1211/7/1212K0235-BSD1 32.8 131 5 25 CQC

108272511/8/1211/8/1212K0286-BSD1 27.5 110 2 25 CQC

10526.22511/9/1211/9/1212K0341-BSD1 24.1 96 8 25

7518.82511/12/1211/12/1212K0415-BSD1 24.4 98 26 25 CQC,R-7

10125.42511/13/1211/13/1212K0462-BSD1 25.2 101 0.6 25 CQC

10827.12511/14/1211/14/1212K0522-BSD1 31.7 127 15 25 CQC

11829.52511/21/1211/21/1212K0803-BSD1 28.2 113 4 25 CQC

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MS %R2-Hexanone


CQC57.9-118PVK0237-0111127.712K0235-MS1 11/7/12 11/7/12 25

CQC,M757.9-118PVK0555-0412230.612K0286-MS1 11/8/12 11/8/12 25

57.9-118PVK0649-0611929.712K0341-MS1 11/9/12 11/9/12 25

CQC57.9-118PVK0756-01 (2.58)9025.112K0415-MS1 11/12/12 11/12/12 25

CQC57.9-118PVK0793-028721.712K0462-MS1 11/13/12 11/13/12 25

CQC57.9-118PVK0281-018621.412K0522-MS1 11/14/12 11/14/12 25

CQC57.9-118PVK1220-02922312K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPD2-Hexanone


11428.52511/7/1211/7/1212K0235-MSD1 CQC25311127.7 PVK0237-01

13032.62511/8/1211/8/1212K0286-MSD1 CQC,M725612230.6 PVK0555-04

104262511/9/1211/9/1212K0341-MSD1 251311929.7 PVK0649-06

8924.92511/12/1211/12/1212K0415-MSD1 CQC250.89025.1 PVK0756-01 (2.58)

88222511/13/1211/13/1212K0462-MSD1 CQC2518721.7 PVK0793-02

88222511/14/1211/14/1212K0522-MSD1 CQC2538621.4 PVK0281-01

9423.42511/21/1211/21/1212K0803-MSD1 CQC2529223 PVK1220-02

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BLK2-Hexanone

Plotted: 7

MDL: 0.31

MRL: 5

Rejected: 0

Stdv: 0.386

Mean: 0.146

2s: 0.917

3s: 1.3

4s: 1.69

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%R in BLK4-Bromofluorobenzene

Limits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

12I0005-BLK1 24.5259/1/12 98 86.5-1149/1/12 CQC

12I0028-BLK1 23.1259/4/12 92 86.5-1149/4/12 CQC

12I0081-BLK1 26.1259/5/12 104 86.5-1149/5/12 CQC

12I0215-BLK1 25259/7/12 100 86.5-1149/7/12 CQC

12I0352-BLK1 23.2259/12/12 93 86.5-1149/12/12 CQC

12I0394-BLK1 25.7259/12/12 103 86.5-1149/12/12 CQC

12I0598-BLK1 23.7259/18/12 95 86.5-1149/18/12 CQC

12I0648-BLK1 24.2259/18/12 97 86.5-1149/18/12 CQC

12I0926-BLK1 22.6259/25/12 90 86.5-1149/25/12 CQC

12I0925-BLK1 25259/25/12 100 86.5-1149/25/12 CQC

12I1065-BLK1 26.5259/28/12 106 86.5-1149/28/12 CQC

12I1095-BLK1 27.3259/28/12 109 86.5-1149/28/12 CQC

12I1107-BLK1 27.6259/29/12 110 86.5-1149/29/12 CQC

12J0008-BLK1 27.12510/1/12 109 86.5-11410/1/12 CQC

12J0298-BLK1 25.62510/8/12 102 86.5-11410/8/12

12J0389-BLK1 252510/10/12 100 86.5-11410/10/12

12J0445-BLK1 25.42510/11/12 102 86.5-11410/11/12 CQC

12J0620-BLK1 25.82510/16/12 103 86.5-11410/16/12 CQC

12J0736-BLK1 27.22510/18/12 109 86.5-11410/18/12 CQC

12J0821-BLK1 24.72510/20/12 99 86.5-11410/20/12 CQC

12J0850-BLK1 26.52510/22/12 106 86.5-11410/22/12 CQC

12J0972-BLK1 262510/24/12 104 86.5-11410/24/12 CQC

12J1010-BLK1 282510/25/12 112 86.5-11410/25/12 CQC

12J1038-BLK1 28.82510/25/12 115 86.5-11410/25/12 CQC,PSL

12J1059-BLK1 28.62510/26/12 114 86.5-11410/26/12 CQC

12K0235-BLK1 28.72511/7/12 115 86.5-11411/7/12 CQC,PSL

12K0286-BLK1 27.22511/8/12 109 86.5-11411/8/12 CQC

12K0341-BLK1 28.22511/9/12 113 86.5-11411/9/12

12K0415-BLK1 30.52511/12/12 122 86.5-11411/12/12 CQC,PSL

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%R in BLK4-BromofluorobenzeneLimits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

12K0462-BLK1 30.72511/13/12 123 86.5-11411/13/12 CQC,PSL

X 12K0522-BLK1 29.82511/14/12 119 86.5-11411/14/12 CQC,PGA,Z1

12K0552-BLK1 29.22511/14/12 117 86.5-11411/14/12 CQC,PSL

12K0553-BLK1 30.32511/14/12 121 86.5-11411/14/12 CQC,PSL

12K0581-BLK1 31.92511/15/12 128 86.5-11411/15/12 CQC,PSL

12K0740-BLK1 29.62511/20/12 119 86.5-11411/20/12 CQC,PSL

12K0751-BLK1 28.82511/20/12 115 86.5-11411/20/12 CQC,PSL

12K0803-BLK1 31.42511/21/12 126 86.5-11411/21/12 CQC,PSL

12K0836-BLK1 29.92511/21/12 119 86.5-11411/21/12 CQC,PSL

12K0865-BLK1 29.42511/23/12 118 86.5-11411/23/12 CQC,PSL

12K0855-BLK1 30.32511/23/12 121 86.5-11411/23/12 CQC,PSL

12K0897-BLK1 31.42511/24/12 125 86.5-11411/24/12 CQC,PSL

12K0905-BLK1 32.22511/25/12 129 86.5-11411/25/12 CQC

12K1134-BLK1 31.32511/30/12 125 86.5-11411/30/12 CQC,PSL

12K1135-BLK1 27.72511/30/12 111 86.5-11411/30/12 CQC

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%R In BS/BSD4-Bromofluorobenzene


12I0005-BS1 24.9259/1/12 99 86.5-1149/1/12 CQC

12I0005-BSD1 24.8259/1/12 99 86.5-1149/1/12 CQC

12I0028-BS1 24259/4/12 96 86.5-1149/4/12 CQC

12I0028-BSD1 23.6259/4/12 94 86.5-1149/4/12 CQC

12I0081-BS1 27.7259/5/12 111 86.5-1149/5/12 CQC

12I0081-BSD1 26.4259/5/12 106 86.5-1149/5/12 CQC

12I0215-BS1 25.2259/7/12 101 86.5-1149/7/12 CQC

12I0215-BSD1 25259/7/12 100 86.5-1149/7/12 CQC

12I0352-BS1 24.3259/12/12 97 86.5-1149/12/12 CQC

12I0352-BSD1 24.6259/12/12 98 86.5-1149/12/12 CQC

12I0394-BS1 27.3259/12/12 109 86.5-1149/12/12 CQC

12I0394-BSD1 26.3259/12/12 105 86.5-1149/12/12 CQC

12I0598-BS1 24.9259/18/12 100 86.5-1149/18/12 CQC

12I0598-BSD1 23.7259/18/12 95 86.5-1149/18/12 CQC

12I0648-BS1 23259/18/12 92 86.5-1149/18/12 CQC

12I0648-BSD1 24.5259/18/12 98 86.5-1149/18/12 CQC

12I0926-BS1 23.2259/25/12 93 86.5-1149/25/12 CQC

12I0925-BS1 24.9259/25/12 100 86.5-1149/25/12 CQC

12I0926-BSD1 22.8259/25/12 91 86.5-1149/25/12 CQC

12I0925-BSD1 26.6259/25/12 106 86.5-1149/25/12 CQC

12I1065-BS1 26.6259/28/12 106 86.5-1149/28/12 CQC

12I1065-BSD1 26.8259/28/12 107 86.5-1149/28/12 CQC

12I1095-BS1 26.8259/28/12 107 86.5-1149/28/12 CQC

12I1095-BSD1 27259/28/12 108 86.5-1149/28/12 CQC

12I1107-BS1 27.3259/29/12 109 86.5-1149/29/12 CQC

12I1107-BSD1 27.5259/29/12 110 86.5-1149/29/12 CQC

12J0008-BS1 27.92510/1/12 111 86.5-11410/1/12 CQC

12J0008-BSD1 28.62510/1/12 114 86.5-11410/1/12 CQC

12J0298-BS1 26.62510/8/12 106 86.5-11410/8/12

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%R In BS/BSD4-BromofluorobenzeneLimits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

12J0298-BSD1 25.72510/8/12 103 86.5-11410/8/12

12J0389-BS1 25.62510/10/12 103 86.5-11410/10/12

12J0389-BSD1 25.32510/10/12 101 86.5-11410/10/12

12J0445-BS1 262510/11/12 104 86.5-11410/11/12 CQC

12J0445-BSD1 26.22510/11/12 105 86.5-11410/11/12 CQC

12J0620-BS1 25.72510/16/12 103 86.5-11410/16/12 CQC

12J0620-BSD1 24.42510/16/12 97 86.5-11410/16/12 CQC

12J0736-BS1 26.72510/18/12 107 86.5-11410/18/12 CQC

12J0736-BSD1 26.12510/18/12 104 86.5-11410/18/12 CQC

12J0821-BS1 25.32510/20/12 101 86.5-11410/20/12 CQC

12J0821-BSD1 25.42510/20/12 102 86.5-11410/20/12 CQC

12J0850-BS1 27.12510/22/12 108 86.5-11410/22/12 CQC

12J0850-BSD1 27.12510/22/12 108 86.5-11410/22/12 CQC

12J0972-BS1 26.62510/24/12 106 86.5-11410/24/12 CQC

12J0972-BSD1 26.62510/24/12 106 86.5-11410/24/12 CQC

12J1010-BS1 26.32510/25/12 105 86.5-11410/25/12 CQC

12J1010-BSD1 28.22510/25/12 113 86.5-11410/25/12 CQC

12J1038-BS1 26.82510/25/12 107 86.5-11410/25/12 CQC

12J1038-BSD1 27.12510/25/12 108 86.5-11410/25/12 CQC

12J1059-BS1 28.12510/26/12 112 86.5-11410/26/12 CQC

12J1059-BSD1 28.42510/26/12 114 86.5-11410/26/12 CQC

12K0235-BS1 26.62511/7/12 106 86.5-11411/7/12 CQC

12K0235-BSD1 28.22511/7/12 113 86.5-11411/7/12 CQC

12K0286-BS1 26.92511/8/12 108 86.5-11411/8/12 CQC

12K0286-BSD1 26.82511/8/12 107 86.5-11411/8/12 CQC

12K0341-BSD1 27.42511/9/12 110 86.5-11411/9/12

12K0341-BS1 26.62511/9/12 106 86.5-11411/9/12

12K0415-BS1 31.32511/12/12 125 86.5-11411/12/12 CQC,PSL

12K0415-BSD1 30.62511/12/12 122 86.5-11411/12/12 CQC,PSL

12K0462-BS1 30.12511/13/12 120 86.5-11411/13/12 CQC,PSL

12K0462-BSD1 29.12511/13/12 117 86.5-11411/13/12 CQC,PSL

12K0522-BS1 26.72511/14/12 107 86.5-11411/14/12 CQC

X 12K0522-BSD1 27.62511/14/12 110 86.5-11411/14/12 CQC

12K0553-BS1 26.52511/14/12 106 86.5-11411/14/12 CQC

12K0552-BS1 30.22511/14/12 121 86.5-11411/14/12 CQC,PSL

12K0553-BSD1 27.42511/14/12 110 86.5-11411/14/12 CQC

12K0552-BSD1 30.22511/14/12 121 86.5-11411/14/12 CQC,PSL

12K0581-BS1 26.72511/15/12 107 86.5-11411/15/12 CQC

12K0581-BSD1 26.32511/15/12 105 86.5-11411/15/12 CQC

12K0740-BS1 30.12511/20/12 120 86.5-11411/20/12 CQC,PSL

12K0751-BS1 29.82511/20/12 119 86.5-11411/20/12 CQC,PSL

12K0740-BSD1 30.42511/20/12 122 86.5-11411/20/12 CQC,PSL

12K0751-BSD1 29.52511/20/12 118 86.5-11411/20/12 CQC,PSL

12K0789-BS1 30.12511/20/12 120 86.5-11411/20/12

12K0789-BSD1 302511/20/12 120 86.5-11411/20/12

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%R In BS/BSD4-BromofluorobenzeneLimits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

12K0803-BS1 31.22511/21/12 125 86.5-11411/21/12 CQC,PSL

X 12K0803-BSD1 30.52511/21/12 122 86.5-11411/21/12 CQC,PSL

12K0836-BS1 30.62511/21/12 122 86.5-11411/21/12 CQC,PSL

12K0836-BSD1 30.92511/21/12 124 86.5-11411/21/12 CQC,PSL

12K0855-BS1 30.12511/23/12 120 86.5-11411/23/12 CQC,PSL

12K0865-BS1 292511/23/12 116 86.5-11411/23/12 CQC,PSL

12K0855-BSD1 30.32511/23/12 121 86.5-11411/23/12 CQC,PSL

12K0865-BSD1 29.42511/23/12 118 86.5-11411/23/12 CQC,PSL

12K0897-BS1 31.62511/24/12 126 86.5-11411/24/12 CQC,PSL

12K0897-BSD1 322511/24/12 128 86.5-11411/24/12 CQC,PSL

12K0905-BS1 32.52511/25/12 130 86.5-11411/25/12 CQC,PSL

12K0905-BSD1 32.72511/25/12 131 86.5-11411/25/12 CQC,Z1

12K1134-BS1 31.92511/30/12 127 86.5-11411/30/12 CQC,PSL

12K1134-BSD1 32.52511/30/12 130 86.5-11411/30/12 CQC,PSL

12K1135-BS1 30.72511/30/12 123 86.5-11411/30/12 CQC,PSL

12K1135-BSD1 292511/30/12 116 86.5-11411/30/12 CQC,PSL

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%R in MS/MSD4-Bromofluorobenzene

Source QualifiersLimitsSample ID Prepared Spike Level Result %RRjct Analyzed

10225.5259/1/1212I0005-MS1 CQC86.5-114PVH2309-029/1/12

9924.9259/1/1212I0005-MSD1X CQC86.5-114PVH2309-029/1/12

9423.6259/4/1212I0028-MS1 CQC86.5-114PVH2309-119/4/12

9624.1259/4/1212I0028-MSD1X CQC86.5-114PVH2309-119/4/12

10726.7259/5/1212I0081-MS1 CQC86.5-114PVH2037-079/5/12

10726.8259/5/1212I0081-MSD1X CQC86.5-114PVH2037-079/5/12

10024.9259/7/1212I0215-MS1 CQC86.5-114PVI0290-039/7/12

10025259/7/1212I0215-MSD1X CQC86.5-114PVI0290-039/7/12

9724.4259/12/1212I0352-MS1 CQC86.5-114PVI0609-099/12/12

9724.3259/12/1212I0352-MSD1X CQC86.5-114PVI0609-099/12/12

10726.7259/12/1212I0394-MS1 CQC86.5-114PVI0525-069/12/12

10927.2259/12/1212I0394-MSD1X CQC86.5-114PVI0525-069/12/12

9724.1259/18/1212I0598-MS1 CQC86.5-114PVI0894-069/18/12

9824.4259/18/1212I0598-MSD1X CQC86.5-114PVI0894-069/18/12

9423.5259/18/1212I0648-MS1 CQC86.5-114PVI1060-029/18/12

9223259/18/1212I0648-MSD1X CQC86.5-114PVI1060-029/18/12

10225.6259/25/1212I0925-MS1 CQC86.5-114PVI1553-089/25/12

10225.4259/25/1212I0925-MSD1X CQC86.5-114PVI1553-089/25/12

9523.6259/25/1212I0926-MS1 CQC86.5-114PVI1510-089/25/12

9523.8259/25/1212I0926-MSD1X CQC86.5-114PVI1510-089/25/12

10726.7259/28/1212I1065-MS1 CQC86.5-114PVI1723-039/28/12

10827.1259/28/1212I1065-MSD1X CQC86.5-114PVI1723-039/28/12

11227.9259/28/1212I1095-MS1 CQC86.5-114PVI1822-029/28/12

10726.7259/28/1212I1095-MSD1X CQC86.5-114PVI1822-029/28/12

11328.3259/29/1212I1107-MS1 CQC86.5-114PVI1869-059/29/12

11228.1259/29/1212I1107-MSD1X CQC86.5-114PVI1869-059/29/12

11328.32510/1/1212J0008-MS1 CQC86.5-114PVI1575-0110/1/12

11528.72510/1/1212J0008-MSD1X CQC,PSL86.5-114PVI1575-0110/1/12

10325.82510/8/1212J0298-MS1 86.5-114PVJ0513-0310/8/12

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%R in MS/MSD4-BromofluorobenzeneSource QualifiersLimitsSample ID Prepared Spike Level Result %RRjct Analyzed

10225.52510/8/1212J0298-MSD1X 86.5-114PVJ0513-0310/8/12

10125.32510/10/1212J0389-MS1 86.5-114PVJ0682-0110/10/12

10425.92510/10/1212J0389-MSD1X 86.5-114PVJ0682-0110/10/12

9523.72510/11/1212J0445-MS1 CQC86.5-114PVJ0682-1710/11/12

9423.52510/11/1212J0445-MSD1X CQC86.5-114PVJ0682-1710/11/12

10125.12510/16/1212J0620-MS1 CQC86.5-114PVJ1065-0210/16/12

9924.72510/16/1212J0620-MSD1X CQC86.5-114PVJ1065-0210/16/12

10024.92510/18/1212J0736-MS1 CQC86.5-114PVJ1237-0210/18/12

10325.82510/18/1212J0736-MSD1X CQC86.5-114PVJ1237-0210/18/12

10025.12510/20/1212J0821-MS1 CQC86.5-114PVJ1405-0210/20/12

10426.12510/20/1212J0821-MSD1X CQC86.5-114PVJ1405-0210/20/12

10526.22510/22/1212J0850-MS1 CQC86.5-114PVJ1405-1710/22/12

11027.62510/22/1212J0850-MSD1X CQC86.5-114PVJ1405-1710/22/12

10726.62510/24/1212J0972-MS1 CQC86.5-114PVJ1577-0210/24/12

10726.82510/24/1212J0972-MSD1X CQC86.5-114PVJ1577-0210/24/12

11528.92510/25/1212J1010-MS1 CQC,PSL86.5-114PVJ1627-0110/25/12

11428.52510/25/1212J1010-MSD1X CQC86.5-114PVJ1627-0110/25/12

11127.62510/25/1212J1038-MS1 CQC86.5-114PVJ1600-0210/25/12

10726.82510/25/1212J1038-MSD1X CQC86.5-114PVJ1600-0210/25/12

10927.32510/26/1212J1059-MS1 CQC86.5-114PVJ1577-18RE110/26/12

11127.92510/26/1212J1059-MSD1X CQC86.5-114PVJ1577-18RE110/26/12

10927.42511/7/1212K0235-MS1 CQC86.5-114PVK0237-0111/7/12

11328.12511/7/1212K0235-MSD1X CQC86.5-114PVK0237-0111/7/12

10726.72511/8/1212K0286-MS1 CQC86.5-114PVK0555-0411/8/12

11428.42511/8/1212K0286-MSD1X CQC86.5-114PVK0555-0411/8/12

10726.72511/9/1212K0341-MS1 86.5-114PVK0649-0611/9/12

10726.62511/9/1212K0341-MSD1X 86.5-114PVK0649-0611/9/12

12631.42511/12/1212K0415-MS1 CQC,PSL86.5-114PVK0756-0111/12/12

12531.32511/12/1212K0415-MSD1X CQC,PSL86.5-114PVK0756-0111/12/12

12130.32511/13/1212K0462-MS1 CQC,PSL86.5-114PVK0793-0211/13/12

11528.62511/13/1212K0462-MSD1X CQC,PSL86.5-114PVK0793-0211/13/12

10726.82511/14/1212K0522-MS1 CQC86.5-114PVK0281-0111/14/12

10125.12511/14/1212K0522-MSD1X CQC86.5-114PVK0281-0111/14/12

11428.52511/14/1212K0553-MS1 CQC86.5-114PVK0632-0911/14/12

12029.92511/14/1212K0552-MS1 CQC,PSL86.5-114PVK0684-0211/14/12

10526.22511/14/1212K0553-MSD1X CQC86.5-114PVK0632-0911/14/12

120302511/14/1212K0552-MSD1X CQC,PSL86.5-114PVK0684-0211/14/12

11528.72511/15/1212K0581-MS1 CQC,PSL86.5-114PVK0696-0111/15/12

11528.92511/15/1212K0581-MSD1X CQC,PSL86.5-114PVK0696-0111/15/12

12130.32511/20/1212K0740-MS1 CQC,PSL86.5-114PVK0934-0111/20/12

11729.32511/20/1212K0740-MSD1X CQC,PSL86.5-114PVK0934-0111/20/12

11528.92511/20/1212K0751-MS1 CQC,PSL86.5-114PVK0768-0211/20/12

11729.32511/20/1212K0751-MSD1X CQC,PSL86.5-114PVK0768-0211/20/12

11929.82511/21/1212K0803-MS1 CQC,PSL86.5-114PVK1220-0211/21/12

120302511/21/1212K0803-MSD1X CQC,PSL86.5-114PVK1220-0211/21/12

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%R in MS/MSD4-BromofluorobenzeneSource QualifiersLimitsSample ID Prepared Spike Level Result %RRjct Analyzed

11929.72511/21/1212K0836-MS1 CQC,PSL86.5-114PVK1288-0311/21/12

12531.22511/21/1212K0836-MSD1X CQC,PSL86.5-114PVK1288-0311/21/12

12030.12511/23/1212K0865-MS1 CQC,PSL86.5-114PVK1375-0811/23/12

11629.12511/23/1212K0865-MSD1X CQC,PSL86.5-114PVK1375-0811/23/12

11629.12511/23/1212K0855-MS1 CQC,PSL86.5-114PVK1375-0211/23/12

124312511/23/1212K0855-MSD1X CQC,PSL86.5-114PVK1375-0211/23/12

124312511/24/1212K0897-MS1 CQC,PSL86.5-114PVK0988-0311/24/12

12932.32511/24/1212K0897-MSD1X CQC,PSL86.5-114PVK0988-0311/24/12

13132.82511/25/1212K0905-MS1 CQC,Z186.5-114PVK1006-0111/25/12

13032.62511/25/1212K0905-MSD1X CQC,PSL86.5-114PVK1006-0111/25/12

12130.32511/30/1212K1135-MS1 CQC,PSL86.5-114PVK1450-1011/30/12

11929.72511/30/1212K1135-MSD1X CQC,PSL86.5-114PVK1450-1011/30/12

12731.82511/30/1212K1134-MS1 CQC,PSL86.5-114PVK1450-0312/1/12

13032.52511/30/1212K1134-MSD1X CQC,PSL86.5-114PVK1450-0312/1/12

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%R in Samples4-Bromofluorobenzene


PVH2309-01 24259/1/12 96 86.5-1149/1/12 CQC,PGA

PVH2309-02 24.9259/1/12 100 86.5-1149/1/12 CQC,PGA

PVH2309-03 24.1259/1/12 97 86.5-1149/1/12 CQC,PGA

PVH2309-04 24.3259/1/12 97 86.5-1149/1/12 CQC,PGA

PVH2309-05 25259/1/12 100 86.5-1149/1/12 CQC,PGA

PVH2309-06 25.1259/1/12 100 86.5-1149/1/12 CQC,PGA

PVH2309-07 24.4259/1/12 98 86.5-1149/1/12 CQC,PGA

PVH2309-08 24.5259/1/12 98 86.5-1149/1/12 CQC,PGA

PVH2309-09 24.7259/1/12 99 86.5-1149/1/12 CQC,PGA

PVH2309-10 23.3259/4/12 93 86.5-1149/4/12 CQC,PGA

PVH2309-11 23259/4/12 92 86.5-1149/4/12 CQC,PGA

PVH2309-12 23.9259/4/12 96 86.5-1149/4/12 CQC,PGA

PVH2309-13 23.2259/4/12 93 86.5-1149/4/12 CQC,PGA

PVH2309-14 22.7259/4/12 91 86.5-1149/4/12 CQC,PGA

PVH2318-01 23.2259/4/12 93 86.5-1149/4/12 CQC,PGA

PVH2318-02 22.4259/4/12 90 86.5-1149/4/12 CQC,PGA

PVH2318-03 23.2259/4/12 93 86.5-1149/4/12 CQC,PGA

PVH2309-12RE1 24.9259/5/12 100 86.5-1149/5/12 CQC,PGA

PVH2309-13RE1 25.3259/5/12 101 86.5-1149/5/12 CQC,PGA

PVH2037-07 9/5/12 86.5-1149/5/12

PVI0290-01 25.4259/7/12 102 86.5-1149/7/12 CQC,PGA

PVI0290-06 24.2259/7/12 97 86.5-1149/7/12 CQC,PGA

PVI0290-02 24.1259/7/12 97 86.5-1149/7/12 CQC,PGA

PVI0290-03 24.6259/7/12 99 86.5-1149/7/12 CQC,PGA

PVI0290-04 24.6259/7/12 98 86.5-1149/7/12 CQC,PGA

PVI0290-05 24.5259/7/12 98 86.5-1149/7/12 CQC,PGA

PVI0609-08 24.1259/12/12 97 86.5-1149/12/12 CQC,PGA

PVI0609-01 24259/12/12 96 86.5-1149/12/12 CQC,PGA

PVI0609-02 24.1259/12/12 97 86.5-1149/12/12 CQC,PGA

01/02/13 15:46

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%R in Samples4-BromofluorobenzeneLimits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

PVI0609-03 23.1259/12/12 92 86.5-1149/12/12 CQC,PGA

PVI0609-04 23.4259/12/12 94 86.5-1149/12/12 CQC,PGA

PVI0609-09 23.3259/12/12 93 86.5-1149/12/12 CQC,PGA

PVI0609-10 23.9259/12/12 96 86.5-1149/12/12 CQC,PGA

PVI0609-11 23.3259/12/12 93 86.5-1149/12/12 CQC,PGA

PVI0609-12 23.6259/12/12 94 86.5-1149/12/12 CQC,PGA

PVI0609-13 24259/12/12 96 86.5-1149/12/12 CQC,PGA

PVI0609-14 23.2259/12/12 93 86.5-1149/12/12 CQC,PGA

PVI0609-15 23.3259/12/12 93 86.5-1149/12/12 CQC,PGA

PVI0609-16 23259/12/12 92 86.5-1149/12/12 CQC,PGA

PVI0609-17 23.8259/12/12 95 86.5-1149/12/12 CQC,PGA

PVI0609-18 23.8259/12/12 95 86.5-1149/12/12 CQC,PGA

PVI0525-06 9/12/12 86.5-1149/12/12 CQC,PGA

PVI0609-19 25.9259/12/12 104 86.5-1149/13/12 CQC,PGA

PVI0609-20 25.7259/12/12 103 86.5-1149/13/12 CQC,PGA

PVI0609-21 25259/12/12 100 86.5-1149/13/12 CQC,PGA

PVI1059-01 24259/18/12 96 86.5-1149/18/12 CQC,PGA

PVI1059-02 24.4259/18/12 97 86.5-1149/18/12 CQC,PGA

PVI1059-03 24.6259/18/12 98 86.5-1149/18/12 CQC,PGA

PVI0894-06 9/18/12 86.5-1149/18/12

PVI1060-01 23.4259/18/12 94 86.5-1149/18/12 CQC,PGA

PVI1060-03 24.4259/18/12 98 86.5-1149/18/12 CQC,PGA

PVI1060-04 23.7259/18/12 95 86.5-1149/18/12 CQC,PGA

PVI1060-05 24259/18/12 96 86.5-1149/18/12 CQC,PGA

PVI1060-06 23.5259/18/12 94 86.5-1149/18/12 CQC,PGA

PVI1060-02 23.5259/18/12 94 86.5-1149/18/12 CQC,PGA

PVI1060-07 23.3259/18/12 93 86.5-1149/18/12 CQC,PGA

PVI1060-08 23.5259/18/12 94 86.5-1149/18/12 CQC,PGA

PVI1060-09 23.5259/18/12 94 86.5-1149/18/12 CQC,PGA

PVI1553-01 23.8259/25/12 95 86.5-1149/25/12 CQC,PGA

PVI1510-08 9/25/12 86.5-1149/25/12 CQC,PGA

PVI1553-02 24.9259/25/12 100 86.5-1149/25/12 CQC,PGA

PVI1553-03 24.4259/25/12 98 86.5-1149/25/12 CQC,PGA

PVI1554-02 23.4259/25/12 94 86.5-1149/25/12 CQC,PGA

PVI1553-04 23.8259/25/12 95 86.5-1149/25/12 CQC,PGA

PVI1554-03 23.2259/25/12 93 86.5-1149/25/12 CQC,PGA

PVI1553-05 25.4259/25/12 102 86.5-1149/25/12 CQC,PGA

PVI1553-06 25.5259/25/12 102 86.5-1149/25/12 CQC,PGA

PVI1553-07 24.8259/25/12 99 86.5-1149/25/12 CQC,PGA

PVI1553-08 23.5259/25/12 94 86.5-1149/26/12 CQC,PGA

PVI1553-09 24.4259/25/12 98 86.5-1149/26/12 CQC,PGA

PVI1553-10 25.6259/25/12 102 86.5-1149/26/12 CQC,PGA

PVI1553-11 25259/25/12 100 86.5-1149/26/12 CQC,PGA

PVI1553-12 24.6259/25/12 98 86.5-1149/26/12 CQC,PGA

PVI1553-13 24.8259/25/12 99 86.5-1149/26/12 CQC,PGA

01/02/13 15:46

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8260 (PGA), 8260 (PGA) Short

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Analyzed By:


PVI1553-14 24.7259/25/12 99 86.5-1149/26/12 CQC,PGA

PVI1553-15 24.2259/25/12 97 86.5-1149/26/12 CQC,PGA

PVI1554-01 25259/25/12 100 86.5-1149/26/12 CQC,PGA

PVI1723-01 25.9259/28/12 104 86.5-1149/28/12 CQC,PGA

PVI1723-02 26.4259/28/12 106 86.5-1149/28/12 CQC,PGA

PVI1723-03 26.4259/28/12 106 86.5-1149/28/12 CQC,PGA

PVI1723-04 25.8259/28/12 103 86.5-1149/28/12 CQC,PGA

PVI1723-05 27.6259/28/12 111 86.5-1149/28/12 CQC,PGA

PVI1723-06 26.7259/28/12 107 86.5-1149/28/12 CQC,PGA

PVI1723-07 26.7259/28/12 107 86.5-1149/28/12 CQC,PGA

PVI1723-08 26.4259/28/12 106 86.5-1149/28/12 CQC,PGA

PVI1723-09 26.3259/28/12 105 86.5-1149/28/12 CQC,PGA

PVI1723-10 26.1259/28/12 104 86.5-1149/28/12 CQC,PGA

PVI1723-11 26.2259/28/12 105 86.5-1149/28/12 CQC,PGA

PVI1723-12 25.6259/28/12 103 86.5-1149/28/12 CQC,PGA

PVI1822-01 27.6259/28/12 110 86.5-1149/28/12 CQC,PGA

PVI1822-02 27.5259/28/12 110 86.5-1149/28/12 CQC,PGA

PVI1822-03 27.1259/28/12 108 86.5-1149/28/12 CQC,PGA

PVI1822-04 27.5259/28/12 110 86.5-1149/28/12 CQC,PGA

PVI1822-05 26.8259/28/12 107 86.5-1149/28/12 CQC,PGA

PVI1822-06 27.8259/28/12 111 86.5-1149/28/12 CQC,PGA

PVI1822-07 28.3259/28/12 113 86.5-1149/28/12 CQC,PGA

PVI1822-08 28.4259/28/12 114 86.5-1149/28/12 CQC,PGA

PVI1822-09 27.7259/28/12 111 86.5-1149/28/12 CQC,PGA

PVI1822-10 27.3259/28/12 109 86.5-1149/29/12 CQC,PGA

PVI1822-11 26.8259/28/12 107 86.5-1149/29/12 CQC,PGA

PVI1822-12 28259/28/12 112 86.5-1149/29/12 CQC,PGA

PVI1822-13 28.8259/28/12 115 86.5-1149/29/12 CQC,PGA,PSL

PVI1822-14 28.6259/28/12 114 86.5-1149/29/12 CQC,PGA

PVI1822-15 22259/28/12 88 86.5-1149/29/12 CQC,PGA

PVI1870-01 27.7259/28/12 111 86.5-1149/29/12 CQC,PGA

PVI1870-02 27259/28/12 108 86.5-1149/29/12 CQC,PGA

PVI1869-01 27.4259/29/12 110 86.5-1149/29/12 CQC,PGA

PVI1869-02 27.9259/29/12 112 86.5-1149/29/12 CQC,PGA

PVI1869-03 27.1259/29/12 108 86.5-1149/29/12 CQC,PGA

PVI1869-04 27.6259/29/12 110 86.5-1149/29/12 CQC,PGA

PVI1869-05 26.8259/29/12 107 86.5-1149/29/12 CQC,PGA

PVI1869-06 27.3259/29/12 109 86.5-1149/29/12 CQC,PGA

PVI1869-07 28.1259/29/12 113 86.5-1149/29/12 CQC,PGA

PVI1869-08 27.2259/29/12 109 86.5-1149/29/12 CQC,PGA

PVI1869-09 27.6259/29/12 111 86.5-1149/29/12 CQC,PGA

PVI1869-10 27.1259/29/12 108 86.5-1149/29/12 CQC,PGA

PVI1869-11 28.4259/29/12 114 86.5-1149/29/12 CQC,PGA

PVI1869-12 27.8259/29/12 111 86.5-1149/29/12 CQC,PGA

PVI1869-13 26.8259/29/12 107 86.5-1149/29/12 CQC,PGA

01/02/13 15:46

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8260 (PGA), 8260 (PGA) Short

Water

All Extractions

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All Extractionists

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Printed:

Client:

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Matrices:

Extractions:

Instruments:

Prepared By:

Analyzed By:


PVI1869-14 27.5259/29/12 110 86.5-1149/29/12 CQC,PGA

PVI1869-15 27.5259/29/12 110 86.5-1149/29/12 CQC,PGA

PVI1869-16 27.5259/29/12 110 86.5-1149/29/12 CQC,PGA

PVI1869-17 27.2259/29/12 109 86.5-1149/29/12 CQC,PGA

PVI1822-15RE1 26.82510/1/12 107 86.5-11410/1/12 CQC,PGA

PVI1869-03RE1 27.32510/1/12 109 86.5-11410/1/12 CQC,PGA

PVI1869-16RE1 28.22510/1/12 113 86.5-11410/1/12 CQC,PGA

PVI1869-17RE1 28.22510/1/12 113 86.5-11410/1/12 CQC,PGA

PVI1869-18 27.82510/1/12 111 86.5-11410/1/12 CQC,PGA

PVI1869-19 27.52510/1/12 110 86.5-11410/1/12 CQC,PGA

PVI1575-01 10/1/12 86.5-11410/1/12 CQC,PGA

PVJ0513-01 25.32510/8/12 101 86.5-11410/8/12 CQC,PGA

PVJ0513-02 25.62510/8/12 102 86.5-11410/8/12 CQC,PGA

PVJ0513-03 26.42510/8/12 106 86.5-11410/8/12 CQC,PGA

PVJ0513-04 26.22510/8/12 105 86.5-11410/8/12 CQC,PGA

PVJ0513-05 25.82510/8/12 103 86.5-11410/8/12 CQC,PGA

PVJ0513-06 25.72510/8/12 103 86.5-11410/8/12 CQC,PGA

PVJ0513-07 24.92510/8/12 100 86.5-11410/8/12 CQC,PGA

PVJ0513-08 25.92510/8/12 104 86.5-11410/8/12 CQC,PGA

PVJ0513-09 25.52510/8/12 102 86.5-11410/8/12 CQC,PGA

PVJ0513-10 24.92510/8/12 99 86.5-11410/8/12 CQC,PGA

PVJ0513-11 25.42510/8/12 102 86.5-11410/8/12 CQC,PGA

PVJ0513-12 25.12510/8/12 100 86.5-11410/8/12 CQC,PGA

PVJ0513-13 25.72510/8/12 103 86.5-11410/8/12 CQC,PGA

PVJ0513-14 25.52510/8/12 102 86.5-11410/8/12 CQC,PGA

PVJ0513-15 25.42510/8/12 102 86.5-11410/8/12 CQC,PGA

PVJ0682-01 24.42510/10/12 98 86.5-11410/10/12 CQC,PGA

PVJ0682-02 25.22510/10/12 101 86.5-11410/10/12 CQC,PGA

PVJ0682-03 25.32510/10/12 101 86.5-11410/10/12 CQC,PGA

PVJ0682-04 25.22510/10/12 101 86.5-11410/10/12 CQC,PGA

PVJ0682-05 25.22510/10/12 101 86.5-11410/10/12 CQC,PGA

PVJ0682-06 25.12510/10/12 100 86.5-11410/10/12 CQC,PGA

PVJ0682-07 25.52510/10/12 102 86.5-11410/10/12 CQC,PGA

PVJ0682-08 25.72510/10/12 103 86.5-11410/10/12 CQC,PGA

PVJ0682-09 25.62510/10/12 102 86.5-11410/10/12 CQC,PGA

PVJ0682-10 25.82510/10/12 103 86.5-11410/10/12 CQC,PGA

PVJ0682-11 25.12510/10/12 100 86.5-11410/10/12 CQC,PGA

PVJ0682-12 25.82510/10/12 103 86.5-11410/10/12 CQC,PGA

PVJ0682-13 25.42510/10/12 102 86.5-11410/10/12 CQC,PGA

PVJ0682-14 25.42510/10/12 102 86.5-11410/10/12 CQC,PGA

PVJ0682-15 24.92510/10/12 99 86.5-11410/10/12 CQC,PGA

PVJ0682-16 25.32510/10/12 101 86.5-11410/10/12 CQC,PGA

PVJ0682-17 242510/11/12 96 86.5-11410/11/12 CQC,PGA

PVJ0682-21 24.12510/11/12 96 86.5-11410/11/12 CQC,PGA

PVJ1065-01 24.92510/16/12 99 86.5-11410/16/12 CQC,PGA

01/02/13 15:46

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8260 (PGA), 8260 (PGA) Short

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PVJ1065-02 24.82510/16/12 99 86.5-11410/16/12 CQC,PGA

PVJ1065-03 24.92510/16/12 100 86.5-11410/16/12 CQC,PGA

PVJ1065-04 252510/16/12 100 86.5-11410/16/12 CQC,PGA

PVJ1065-05 24.82510/16/12 99 86.5-11410/16/12 CQC,PGA

PVJ1065-06 25.22510/16/12 101 86.5-11410/16/12 CQC,PGA

PVJ1065-07 24.32510/16/12 97 86.5-11410/16/12 CQC,PGA

PVJ1065-08 24.52510/16/12 98 86.5-11410/16/12 CQC,PGA

PVJ1065-09 25.52510/16/12 102 86.5-11410/16/12 CQC,PGA

PVJ1065-10 25.32510/16/12 101 86.5-11410/16/12 CQC,PGA

PVJ1237-01 24.32510/18/12 97 86.5-11410/18/12 CQC,PGA

PVJ1237-02 252510/18/12 100 86.5-11410/18/12 CQC,PGA

PVJ1237-03 24.42510/18/12 97 86.5-11410/18/12 CQC,PGA

PVJ1237-04 23.82510/18/12 95 86.5-11410/18/12 CQC,PGA

PVJ1237-05 24.22510/18/12 97 86.5-11410/18/12 CQC,PGA

PVJ1237-06 24.52510/18/12 98 86.5-11410/18/12 CQC,PGA

PVJ1237-07 23.82510/18/12 95 86.5-11410/18/12 CQC,PGA

PVJ1237-08 24.22510/18/12 97 86.5-11410/18/12 CQC,PGA

PVJ1237-09 23.82510/18/12 95 86.5-11410/18/12 CQC,PGA

PVJ1237-10 24.82510/18/12 99 86.5-11410/18/12 CQC,PGA

PVJ1237-11 23.42510/18/12 94 86.5-11410/18/12 CQC,PGA

PVJ1237-12 24.32510/18/12 97 86.5-11410/18/12 CQC,PGA

PVJ1237-13 23.92510/18/12 96 86.5-11410/18/12 CQC,PGA

PVJ1237-14 24.32510/18/12 97 86.5-11410/18/12 CQC,PGA

PVJ1405-01 24.92510/20/12 100 86.5-11410/20/12 CQC,PGA

PVJ1405-02 24.72510/20/12 99 86.5-11410/20/12 CQC,PGA

PVJ1405-03 24.82510/20/12 99 86.5-11410/20/12 CQC,PGA

PVJ1405-04 25.22510/20/12 101 86.5-11410/20/12 CQC,PGA

PVJ1405-05 24.42510/20/12 97 86.5-11410/20/12 CQC,PGA

PVJ1405-06 242510/20/12 96 86.5-11410/20/12 CQC,PGA

PVJ1405-07 24.62510/20/12 98 86.5-11410/20/12 CQC,PGA

PVJ1405-08 252510/20/12 100 86.5-11410/20/12 CQC,PGA

PVJ1405-09 23.92510/20/12 96 86.5-11410/20/12 CQC,PGA

PVJ1405-10 25.22510/20/12 101 86.5-11410/20/12 CQC,PGA

PVJ1405-11 24.82510/20/12 99 86.5-11410/20/12 CQC,PGA

PVJ1405-12 24.72510/20/12 99 86.5-11410/20/12 CQC,PGA

PVJ1405-13 23.92510/20/12 96 86.5-11410/20/12 CQC,PGA

PVJ1405-14 24.32510/20/12 97 86.5-11410/20/12 CQC,PGA

PVJ1405-15 25.32510/20/12 101 86.5-11410/20/12 CQC,PGA

PVJ1405-16 24.62510/20/12 98 86.5-11410/20/12 CQC,PGA

PVJ1405-17 26.72510/22/12 107 86.5-11410/22/12 CQC,PGA

PVJ1405-18 272510/22/12 108 86.5-11410/22/12 CQC,PGA

PVJ1577-01 26.22510/24/12 105 86.5-11410/24/12 CQC,PGA

PVJ1577-02 26.42510/24/12 106 86.5-11410/24/12 CQC,PGA

PVJ1577-03 26.12510/24/12 105 86.5-11410/24/12 CQC,PGA

PVJ1577-04 26.22510/24/12 105 86.5-11410/24/12 CQC,PGA

01/02/13 15:46

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8260 (PGA), 8260 (PGA) Short

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Printed:

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Extractions:

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Prepared By:

Analyzed By:


PVJ1577-05 25.92510/24/12 103 86.5-11410/24/12 CQC,PGA

PVJ1577-06 26.42510/24/12 105 86.5-11410/24/12 CQC,PGA

PVJ1577-07 25.82510/24/12 103 86.5-11410/25/12 CQC,PGA

PVJ1577-08 26.82510/24/12 107 86.5-11410/25/12 CQC,PGA

PVJ1577-09 25.82510/24/12 103 86.5-11410/25/12 CQC,PGA

PVJ1577-10 25.72510/24/12 103 86.5-11410/25/12 CQC,PGA

PVJ1577-11 25.62510/24/12 102 86.5-11410/25/12 CQC,PGA

PVJ1577-12 26.52510/24/12 106 86.5-11410/25/12 CQC,PGA

PVJ1577-13 25.52510/24/12 102 86.5-11410/25/12 CQC,PGA

PVJ1577-14 02510/24/12 86.5-11410/25/12

PVJ1575-01 02510/24/12 86.5-11410/25/12

PVJ1575-01RE1 282510/24/12 112 86.5-11410/25/12 CQC,PGA

PVJ1577-14RE1 28.12510/24/12 112 86.5-11410/25/12 CQC,PGA

PVJ1627-01 10/25/12 86.5-11410/25/12 CQC,PGA

PVJ1575-02 27.72510/25/12 111 86.5-11410/25/12 CQC,PGA

PVJ1577-15 28.42510/25/12 114 86.5-11410/25/12 CQC,PGA

PVJ1577-16 27.62510/25/12 111 86.5-11410/25/12 CQC,PGA

PVJ1577-17 26.92510/25/12 108 86.5-11410/25/12 CQC,PGA

PVJ1577-18 26.92510/25/12 108 86.5-11410/25/12 CQC,PGA

PVJ1600-02 10/25/12 86.5-11410/25/12 CQC,PGA

PVJ1577-19 28.82510/25/12 115 86.5-11410/25/12 CQC,PGA,PSL

PVJ1577-19RE1 28.72510/26/12 115 86.5-11410/26/12 CQC,PGA,PSL

PVJ1577-18RE1 29.62510/26/12 118 86.5-11410/26/12 CQC,PGA,PSL

PVK0411-02 28.32511/7/12 113 86.5-11411/7/12 CQC,PGA

PVK0411-03 27.92511/7/12 112 86.5-11411/7/12 CQC,PGA

PVK0237-01 11/7/12 86.5-11411/7/12

PVK0555-02 27.62511/8/12 110 86.5-11411/8/12 CQC,PGA

PVK0555-01 28.12511/8/12 112 86.5-11411/8/12 CQC,PGA

PVK0555-03 27.22511/8/12 109 86.5-11411/8/12 CQC,PGA

PVK0555-04 27.92511/8/12 112 86.5-11411/8/12 CQC,PGA

PVK0555-05 28.52511/8/12 114 86.5-11411/8/12 CQC,PGA

PVK0649-03 28.22511/9/12 113 86.5-11411/9/12

PVK0649-04 27.82511/9/12 111 86.5-11411/9/12

PVK0649-05 27.22511/9/12 109 86.5-11411/9/12

PVK0649-06 27.62511/9/12 110 86.5-11411/9/12

PVK0756-03 292511/12/12 116 86.5-11411/12/12 PSL,CQC,PGA

PVK0756-01 29.82511/12/12 119 86.5-11411/12/12 CQC,PGA,PSL

PVK0756-02 31.32511/12/12 125 86.5-11411/12/12 CQC,PGA,PSL

PVK0756-04 30.12511/12/12 120 86.5-11411/12/12 QC,PGA,E8,PS

PVK0756-05 30.42511/12/12 122 86.5-11411/12/12 CQC,PGA,PSL

PVK0411-01 30.32511/12/12 121 86.5-11411/12/12 CQC,PGA,PSL

PVK0411-02RE1 30.52511/12/12 122 86.5-11411/12/12 CQC,PGA,PSL

PVK0411-03RE1 30.82511/12/12 123 86.5-11411/12/12 QC,N1,PGA,PS

PVK0649-01 31.22511/12/12 125 86.5-11411/12/12 CQC,PGA,PSL

PVK0649-02 29.82511/12/12 119 86.5-11411/12/12 CQC,PGA,PSL

01/02/13 15:46

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8260 (PGA), 8260 (PGA) Short

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Printed:

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Prepared By:

Analyzed By:


PVK0649-03RE1 312511/12/12 124 86.5-11411/12/12 PSL,CQC,PGA

PVK0649-04RE1 29.82511/12/12 119 86.5-11411/12/12 CQC,PGA,PSL

PVK0649-05RE1 30.62511/12/12 122 86.5-11411/12/12 CQC,PGA,PSL

PVK0649-06RE1 30.52511/12/12 122 86.5-11411/12/12 CQC,PGA,PSL

PVK0828-02 29.52511/13/12 118 86.5-11411/13/12 CQC,PGA,PSL

PVK0828-03 30.62511/13/12 122 86.5-11411/13/12 CQC,PGA,PSL

PVK0828-05 29.72511/13/12 119 86.5-11411/13/12 CQC,PGA,PSL

PVK0793-02 11/13/12 86.5-11411/13/12 CQC,PGA

PVK0828-01 30.52511/13/12 122 86.5-11411/13/12 PSL,CQC,PGA

PVK0828-04 29.32511/13/12 117 86.5-11411/13/12 PSL,CQC,PGA

PVK0411-02RE2 292511/13/12 116 86.5-11411/13/12 CQC,PGA,PSL

PVK0892-03 29.92511/14/12 120 86.5-11411/14/12 CQC,PGA,PSL

X PVK0281-01 11/14/12 86.5-11411/14/12

PVK0892-01 29.72511/14/12 119 86.5-11411/14/12 CQC,PGA,PSL

PVK0892-02 30.72511/14/12 123 86.5-11411/14/12 PSL,CQC,PGA

PVK0632-01 29.92511/14/12 119 86.5-11411/14/12 CQC,PGA,PSL

PVK0632-02 30.62511/14/12 123 86.5-11411/14/12 CQC,PGA,PSL

PVK0632-03 29.82511/14/12 119 86.5-11411/14/12 CQC,PGA,PSL

PVK0632-04 30.42511/14/12 122 86.5-11411/14/12 CQC,PGA,PSL

PVK0632-08 29.42511/14/12 118 86.5-11411/14/12 CQC,PGA,PSL

PVK0632-09 29.32511/14/12 117 86.5-11411/14/12 CQC,PGA,PSL

PVK0684-01 28.22511/14/12 113 86.5-11411/14/12 CQC,PGA

PVK0632-10 30.62511/14/12 122 86.5-11411/14/12 CQC,PGA,PSL

PVK0684-02 292511/14/12 116 86.5-11411/14/12 CQC,PGA,PSL

PVK0632-11 30.62511/14/12 122 86.5-11411/14/12 CQC,PGA,PSL

PVK0684-03 28.82511/14/12 115 86.5-11411/14/12 CQC,PGA,PSL

PVK0632-12 30.62511/14/12 123 86.5-11411/14/12 CQC,PGA,PSL

PVK0684-04 29.82511/14/12 119 86.5-11411/15/12 CQC,PGA,PSL

PVK0684-05 28.82511/14/12 115 86.5-11411/15/12 CQC,PGA,PSL

PVK0632-13 30.52511/14/12 122 86.5-11411/15/12 CQC,PGA,PSL

PVK0684-06 28.72511/14/12 115 86.5-11411/15/12 CQC,PGA,PSL

PVK0632-14 30.32511/14/12 121 86.5-11411/15/12 CQC,PGA,PSL

PVK0684-07 28.12511/14/12 112 86.5-11411/15/12 CQC,PGA

PVK0632-15 31.12511/14/12 124 86.5-11411/15/12 CQC,PGA,PSL

PVK0684-08 28.82511/14/12 115 86.5-11411/15/12 CQC,PGA,PSL

PVK0632-16 30.52511/14/12 122 86.5-11411/15/12 CQC,PGA,PSL

PVK0684-09 30.12511/14/12 120 86.5-11411/15/12 CQC,PGA,PSL

PVK0632-17 30.72511/14/12 123 86.5-11411/15/12 CQC,PGA,PSL

PVK0632-18 30.72511/14/12 123 86.5-11411/15/12 CQC,PGA,PSL

PVK0684-10 31.62511/15/12 126 86.5-11411/15/12 CQC,PGA,PSL

PVK0684-08RE1 30.32511/15/12 121 86.5-11411/15/12 CQC,PGA,PSL

PVK0696-01 11/15/12 86.5-11411/15/12 CQC,PGA

PVK1220-01 28.92511/20/12 116 86.5-11411/20/12 CQC,PGA,PSL

PVK0768-02 11/20/12 86.5-11411/20/12

PVK1220-03 302511/20/12 120 86.5-11411/20/12 CQC,PGA,PSL

01/02/13 15:46

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PVK1220-04 302511/20/12 120 86.5-11411/20/12 CQC,PGA,PSL

PVK0934-01 11/20/12 86.5-11411/20/12 CQC,PGA

PVK1380-01 29.12511/21/12 116 86.5-11411/21/12 PSL,CQC,PGA

PVK1380-02 29.92511/21/12 120 86.5-11411/21/12 CQC,PGA,PSL

PVK1220-02 29.22511/21/12 117 86.5-11411/21/12 CQC,PGA,PSL

PVK1220-06 302511/21/12 120 86.5-11411/21/12 CQC,PGA,PSL

PVK1220-07 29.22511/21/12 117 86.5-11411/21/12 CQC,PGA,PSL

PVK1220-08 30.22511/21/12 121 86.5-11411/21/12 CQC,PGA,PSL

PVK1220-09 29.32511/21/12 117 86.5-11411/21/12 CQC,PGA,PSL

PVK1220-10 30.42511/21/12 122 86.5-11411/21/12 CQC,PGA,PSL

PVK1220-11 29.92511/21/12 120 86.5-11411/21/12 CQC,PGA,PSL

PVK1220-12 30.32511/21/12 121 86.5-11411/21/12 CQC,PGA,PSL

PVK1220-13 28.42511/21/12 113 86.5-11411/21/12 CQC,PGA

PVK1220-14 30.42511/21/12 122 86.5-11411/21/12 CQC,PGA,PSL

PVK1288-01 30.22511/21/12 121 86.5-11411/21/12 CQC,PGA,PSL

PVK1288-02 31.12511/21/12 124 86.5-11411/21/12 CQC,PGA,PSL

PVK1288-03 30.12511/21/12 121 86.5-11411/21/12 CQC,PGA,PSL

PVK1288-04 302511/21/12 120 86.5-11411/21/12 CQC,PGA,PSL

PVK1288-05 30.12511/21/12 121 86.5-11411/21/12 CQC,PGA,PSL

PVK1288-06 31.42511/21/12 126 86.5-11411/21/12 CQC,PGA,PSL

PVK1288-07 29.92511/21/12 120 86.5-11411/21/12 CQC,PGA,PSL

PVK1286-01 29.92511/21/12 119 86.5-11411/22/12 CQC,PGA,PSL

PVK1286-02 29.62511/21/12 118 86.5-11411/22/12 CQC,PGA,PSL

PVK1286-03 29.92511/21/12 120 86.5-11411/22/12 CQC,PGA,PSL

PVK1286-04 30.52511/21/12 122 86.5-11411/22/12 CQC,PGA,PSL

PVK1286-05 29.72511/21/12 119 86.5-11411/22/12 CQC,PGA,PSL

PVK1286-06 30.22511/21/12 121 86.5-11411/22/12 CQC,PGA,PSL

PVK1220-15 29.32511/21/12 117 86.5-11411/22/12 CQC,PGA,PSL

PVK1220-17 29.72511/21/12 119 86.5-11411/22/12 CQC,PGA,PSL

PVK1220-16 28.32511/23/12 113 86.5-11411/23/12 CQC,PGA

PVK1375-08 29.52511/23/12 118 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-09 28.72511/23/12 115 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-01 30.92511/23/12 124 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-10 292511/23/12 116 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-02 302511/23/12 120 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-11 28.82511/23/12 115 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-12 29.42511/23/12 117 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-13 292511/23/12 116 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-03 29.32511/23/12 117 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-14 29.62511/23/12 119 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-04 30.42511/23/12 122 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-15 29.42511/23/12 118 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-05 29.42511/23/12 117 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-06 29.82511/23/12 119 86.5-11411/23/12 CQC,PGA,PSL

PVK1375-07 29.62511/23/12 118 86.5-11411/23/12 CQC,PGA,PSL

01/02/13 15:46

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PVK1375-16 33.22511/24/12 133 86.5-11411/24/12 CQC,PGA,Z2

PVK0988-03 11/24/12 86.5-11411/24/12

PVK1006-01 11/24/12 86.5-11411/25/12

PVK1375-16RE1 32.42511/25/12 130 86.5-11411/26/12 CQC,PGA,PSL

PVK1450-20 29.12511/30/12 116 86.5-11411/30/12 CQC,PGA,PSL

PVK1450-10 29.12511/30/12 117 86.5-11411/30/12 CQC,PGA,PSL

PVK1450-11 28.92511/30/12 116 86.5-11411/30/12 CQC,PGA,PSL

PVK1450-12 292511/30/12 116 86.5-11411/30/12 CQC,PGA,PSL

PVK1450-01 312511/30/12 124 86.5-11411/30/12 CQC,PGA,PSL

PVK1450-13 29.12511/30/12 116 86.5-11411/30/12 CQC,PGA,PSL

PVK1450-02 32.12511/30/12 129 86.5-11411/30/12 CQC,PGA,PSL

PVK1450-14 28.42511/30/12 114 86.5-11411/30/12 CQC,PGA

PVK1450-03 312511/30/12 124 86.5-11412/1/12 CQC,PGA,PSL

PVK1450-15 28.12511/30/12 112 86.5-11412/1/12 CQC,PGA

PVK1450-16 28.72511/30/12 115 86.5-11412/1/12 CQC,PGA,PSL

PVK1450-17 28.42511/30/12 114 86.5-11412/1/12 CQC,PGA

PVK1450-18 28.72511/30/12 115 86.5-11412/1/12 CQC,PGA,PSL

PVK1450-04 30.62511/30/12 122 86.5-11412/1/12 CQC,PGA,PSL

PVK1450-19 28.22511/30/12 113 86.5-11412/1/12 CQC,PGA

PVK1450-05 32.82511/30/12 131 86.5-11412/1/12 CQC,PGA,Z2

PVK1450-06 31.92511/30/12 127 86.5-11412/1/12 CQC,PGA,PSL

PVK1450-07 32.42511/30/12 130 86.5-11412/1/12 CQC,PGA,PSL

PVK1450-08 31.82511/30/12 127 86.5-11412/1/12 CQC,PGA,PSL

PVK1450-09 31.32511/30/12 125 86.5-11412/1/12 CQC,PGA,PSL

01/02/13 15:46

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LCS %R4-Chlorotoluene


12K0235-BS1 28.9 1162511/7/12 80.3-11911/7/12 CQC

12K0286-BS1 24.5 982511/8/12 80.3-11911/8/12 CQC

12K0341-BS1 25.4 1022511/9/12 80.3-11911/9/12

12K0415-BS1 23.3 932511/12/12 80.3-11911/12/12 CQC

12K0462-BS1 24.5 982511/13/12 80.3-11911/13/12 CQC

12K0522-BS1 28.5 1142511/14/12 80.3-11911/14/12 CQC

12K0803-BS1 25.7 1032511/21/12 80.3-11911/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPD4-Chlorotoluene


11528.82511/7/1211/7/1212K0235-BSD1 28.9 116 0.4 25 CQC

10425.92511/8/1211/8/1212K0286-BSD1 24.5 98 6 25 CQC

10225.52511/9/1211/9/1212K0341-BSD1 25.4 102 0.2 25

9323.42511/12/1211/12/1212K0415-BSD1 23.3 93 0.4 25 CQC

9924.62511/13/1211/13/1212K0462-BSD1 24.5 98 0.6 25 CQC

11729.22511/14/1211/14/1212K0522-BSD1 28.5 114 2 25 CQC

10526.32511/21/1211/21/1212K0803-BSD1 25.7 103 2 25 CQC

01/02/13 15:46

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MS %R4-Chlorotoluene


CQC76.8-120PVK0237-0111729.212K0235-MS1 11/7/12 11/7/12 25

CQC76.8-120PVK0555-0411428.612K0286-MS1 11/8/12 11/8/12 25

76.8-120PVK0649-0610626.512K0341-MS1 11/9/12 11/9/12 25

CQC76.8-120PVK0756-019624.112K0415-MS1 11/12/12 11/12/12 25

CQC76.8-120PVK0793-0210526.212K0462-MS1 11/13/12 11/13/12 25

CQC76.8-120PVK0281-0111428.612K0522-MS1 11/14/12 11/14/12 25

CQC76.8-120PVK1220-0210325.912K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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MS/MSD RPD4-Chlorotoluene


12230.52511/7/1211/7/1212K0235-MSD1 CQC,PSL25511729.2 PVK0237-01

11127.72511/8/1211/8/1212K0286-MSD1 CQC25311428.6 PVK0555-04

11027.52511/9/1211/9/1212K0341-MSD1 25410626.5 PVK0649-06

9423.52511/12/1211/12/1212K0415-MSD1 CQC2539624.1 PVK0756-01

11629.12511/13/1211/13/1212K0462-MSD1 CQC251110526.2 PVK0793-02

11829.42511/14/1211/14/1212K0522-MSD1 CQC25311428.6 PVK0281-01

11228.12511/21/1211/21/1212K0803-MSD1 CQC25810325.9 PVK1220-02

01/02/13 15:46

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BLK4-Chlorotoluene

01/02/13 15:46

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LCS %R4-Methyl-2-pentanone (MIBK)


12K0235-BS1 31.6 1262511/7/12 72-12911/7/12 CQC

12K0286-BS1 25.2 1012511/8/12 72-12911/8/12 CQC

12K0341-BS1 22.7 912511/9/12 72-12911/9/12

12K0415-BS1 21.5 862511/12/12 72-12911/12/12 CQC

12K0462-BS1 28.2 1132511/13/12 72-12911/13/12 CQC

12K0522-BS1 28.2 1132511/14/12 72-12911/14/12 CQC

12K0803-BS1 26.8 1072511/21/12 72-12911/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPD4-Methyl-2-pentanone (MIBK)


11528.62511/7/1211/7/1212K0235-BSD1 31.6 126 10 25 CQC

10325.62511/8/1211/8/1212K0286-BSD1 25.2 101 2 25 CQC

9423.42511/9/1211/9/1212K0341-BSD1 22.7 91 3 25

8120.42511/12/1211/12/1212K0415-BSD1 21.5 86 6 25 CQC

10726.72511/13/1211/13/1212K0462-BSD1 28.2 113 6 25 CQC

10927.32511/14/1211/14/1212K0522-BSD1 28.2 113 3 25 CQC

12230.52511/21/1211/21/1212K0803-BSD1 26.8 107 13 25 CQC

01/02/13 15:46

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MS %R4-Methyl-2-pentanone (MIBK)


CQC65.6-127PVK0237-0111328.412K0235-MS1 11/7/12 11/7/12 25

CQC65.6-127PVK0555-04 (0.82)1173012K0286-MS1 11/8/12 11/8/12 25

65.6-127PVK0649-06 (0.57)9223.612K0341-MS1 11/9/12 11/9/12 25

CQC65.6-127PVK0756-019824.412K0415-MS1 11/12/12 11/12/12 25

CQC65.6-127PVK0793-0210325.712K0462-MS1 11/13/12 11/13/12 25

CQC65.6-127PVK0281-01962412K0522-MS1 11/14/12 11/14/12 25

CQC65.6-127PVK1220-0210726.712K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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MS/MSD RPD4-Methyl-2-pentanone (MIBK)


11328.22511/7/1211/7/1212K0235-MSD1 CQC250.511328.4 PVK0237-01

10627.22511/8/1211/8/1212K0286-MSD1 CQC251011730 PVK0555-04 (0.82)

86222511/9/1211/9/1212K0341-MSD1 2579223.6 PVK0649-06 (0.57)

9724.32511/12/1211/12/1212K0415-MSD1 CQC250.59824.4 PVK0756-01

10325.82511/13/1211/13/1212K0462-MSD1 CQC250.310325.7 PVK0793-02

10626.42511/14/1211/14/1212K0522-MSD1 CQC25109624 PVK0281-01

108272511/21/1211/21/1212K0803-MSD1 CQC25110726.7 PVK1220-02

01/02/13 15:46

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BLK4-Methyl-2-pentanone (MIBK)

01/02/13 15:46

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LCS %RAcetone


12I0005-BS1 26.5 106259/1/12 22.4-1539/1/12 CQC

12I0028-BS1 24 96259/4/12 22.4-1539/4/12 CQC

12I0081-BS1 26.8 107259/5/12 22.4-1539/5/12 CQC

12I0215-BS1 19.6 78259/7/12 22.4-1539/7/12 CQC

12I0352-BS1 19.4 77259/12/12 22.4-1539/12/12 CQC

12I0394-BS1 30.5 122259/12/12 22.4-1539/12/12 CQC

12I0598-BS1 25.3 101259/18/12 22.4-1539/18/12 CQC

12I0648-BS1 30.8 123259/18/12 22.4-1539/18/12 CQC

12I0926-BS1 22.9 91259/25/12 22.4-1539/25/12 CQC

12I0925-BS1 30.3 121259/25/12 22.4-1539/25/12 CQC

12I1065-BS1 28.8 115259/28/12 22.4-1539/28/12 CQC

12I1095-BS1 27.6 110259/28/12 22.4-1539/28/12 CQC

12I1107-BS1 27.5 110259/29/12 22.4-1539/29/12 CQC

12J0008-BS1 31.8 1272510/1/12 22.4-15310/1/12 CQC

12J0298-BS1 24.7 992510/8/12 22.4-15310/8/12

12J0389-BS1 27.8 1112510/10/12 22.4-15310/10/12

12J0445-BS1 28.4 1142510/11/12 22.4-15310/11/12 CQC

12J0620-BS1 19.9 792510/16/12 22.4-15310/16/12 CQC

12J0736-BS1 27.9 1122510/18/12 22.4-15310/18/12 CQC

12J0821-BS1 23.5 942510/20/12 22.4-15310/20/12 CQC

12J0850-BS1 29.3 1172510/22/12 22.4-15310/22/12 CQC

12J0972-BS1 38 1522510/24/12 22.4-15310/24/12 CQC

12J1010-BS1 19.5 782510/25/12 22.4-15310/25/12 CQC

12J1038-BS1 15.4 622510/25/12 22.4-15310/25/12 CQC

12J1059-BS1 29.4 1182510/26/12 22.4-15310/26/12 CQC

12K0235-BS1 28.5 1142511/7/12 22.4-15311/7/12 CQC

12K0286-BS1 20.4 822511/8/12 22.4-15311/8/12 CQC

01/02/13 15:46

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LCS %RAcetoneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 9.45 382511/9/12 22.4-15311/9/12

12K0415-BS1 22.3 892511/12/12 22.4-15311/12/12 CQC

12K0462-BS1 22.7 912511/13/12 22.4-15311/13/12 CQC

12K0522-BS1 34 1362511/14/12 22.4-15311/14/12 CQC

12K0553-BS1 31 1242511/14/12 22.4-15311/14/12 CQC

12K0552-BS1 25.4 1022511/14/12 22.4-15311/14/12 CQC

12K0581-BS1 30.3 1212511/15/12 22.4-15311/15/12 CQC

12K0740-BS1 25.5 1022511/20/12 22.4-15311/20/12 CQC,C

12K0751-BS1 29.5 1182511/20/12 22.4-15311/20/12 CQC

12K0789-BS1 36.9 1482511/20/12 22.4-15311/20/12

12K0803-BS1 26 104X 2511/21/12 22.4-15311/21/12 CQC

12K0836-BS1 34.7 1392511/21/12 22.4-15311/21/12 CQC

12K0855-BS1 33.5 1342511/23/12 22.4-15311/23/12 CQC

12K0865-BS1 28.9 1162511/23/12 22.4-15311/23/12 CQC

12K0897-BS1 23.1 922511/24/12 22.4-15311/24/12 CQC

12K0905-BS1 34.8 1392511/25/12 22.4-15311/25/12 CQC

12K1134-BS1 22.7 912511/30/12 22.4-15311/30/12 CQC

12K1135-BS1 25.3 1012511/30/12 22.4-15311/30/12 CQC

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LCS/LCSD RPDAcetone


9624259/1/129/1/1212I0005-BSD1 26.5 106 10 25 CQC

10025.1259/4/129/4/1212I0028-BSD1 24 96 4 25 CQC

8420.9259/5/129/5/1212I0081-BSD1 26.8 107 25 25 CQC

7619.1259/7/129/7/1212I0215-BSD1 19.6 78 3 25 CQC

9423.6259/12/129/12/1212I0352-BSD1 19.4 77 20 25 CQC

7117.8259/12/129/12/1212I0394-BSD1 30.5 122 52 25 CQC,R-7

9824.5259/18/129/18/1212I0598-BSD1 25.3 101 3 25 CQC

11729.4259/18/129/18/1212I0648-BSD1 30.8 123 5 25 CQC

11027.6259/25/129/25/1212I0926-BSD1 22.9 91 19 25 CQC

9523.7259/25/129/25/1212I0925-BSD1 30.3 121 24 25 CQC

10526.2259/28/129/28/1212I1065-BSD1 28.8 115 10 25 CQC

11829.4259/28/129/28/1212I1095-BSD1 27.6 110 7 25 CQC

10726.7259/29/129/29/1212I1107-BSD1 27.5 110 3 25 CQC

13032.42510/1/1210/1/1212J0008-BSD1 31.8 127 2 25 CQC

10726.82510/8/1210/8/1212J0298-BSD1 24.7 99 8 25

96242510/10/1210/10/1212J0389-BSD1 27.8 111 14 25

9724.32510/11/1210/11/1212J0445-BSD1 28.4 114 16 25 CQC

7518.72510/16/1210/16/1212J0620-BSD1 19.9 79 6 25 CQC

9924.72510/18/1210/18/1212J0736-BSD1 27.9 112 12 25 CQC

9323.42510/20/1210/20/1212J0821-BSD1 23.5 94 0.6 25 CQC

10125.42510/22/1210/22/1212J0850-BSD1 29.3 117 14 25 CQC

6917.32510/24/1210/24/1212J0972-BSD1 38 152 75 25 CQC,R-7

6516.22510/25/1210/25/1212J1010-BSD1 19.5 78 19 25 CQC

68172510/25/1210/25/1212J1038-BSD1 15.4 62 10 25 CQC

11729.12510/26/1210/26/1212J1059-BSD1 29.4 118 1 25 CQC

8521.22511/7/1211/7/1212K0235-BSD1 28.5 114 29 25 CQC,R-7

6816.92511/8/1211/8/1212K0286-BSD1 20.4 82 19 25 CQC

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LCS/LCSD RPDAcetone%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

4110.22511/9/1211/9/1212K0341-BSD1 9.45 38 8 25

68172511/12/1211/12/1212K0415-BSD1 22.3 89 27 25 CQC,R-7

9523.62511/13/1211/13/1212K0462-BSD1 22.7 91 4 25 CQC

11127.82511/14/1211/14/1212K0522-BSD1 34 136 20 25 CQC

10325.62511/14/1211/14/1212K0553-BSD1 31 124 19 25 CQC

88222511/14/1211/14/1212K0552-BSD1 25.4 102 14 25 CQC

12030.12511/15/1211/15/1212K0581-BSD1 30.3 121 0.7 25 CQC

7017.62511/20/1211/20/1212K0740-BSD1 25.5 102 37 25 CQC,C,R-7

7619.12511/20/1211/20/1212K0751-BSD1 29.5 118 43 25 CQC,R-7

11328.32511/20/1211/20/1212K0789-BSD1 36.9 148 27 25

9523.72511/21/1211/21/1212K0803-BSD1X 26 104 9 25 CQC

10526.32511/21/1211/21/1212K0836-BSD1 34.7 139 28 25 CQC,R-7

14034.92511/23/1211/23/1212K0855-BSD1 33.5 134 4 25 CQC

11127.72511/23/1211/23/1212K0865-BSD1 28.9 116 4 25 CQC

14435.92511/24/1211/24/1212K0897-BSD1 23.1 92 43 25 CQC,R-7

12130.32511/25/1211/25/1212K0905-BSD1 34.8 139 14 25 CQC

11929.82511/30/1211/30/1212K1134-BSD1 22.7 91 27 25 CQC,R-7

9523.72511/30/1211/30/1212K1135-BSD1 25.3 101 7 25 CQC

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MS %RAcetone


CQC19.7-131PVH2309-026115.412I0005-MS1 9/1/12 9/1/12 25

CQC19.7-131PVH2309-11 (4.78)411512I0028-MS1 9/4/12 9/4/12 25

CQC19.7-131PVH2037-076716.712I0081-MS1 9/5/12 9/5/12 25

CQC19.7-131PVI0290-034711.812I0215-MS1 9/7/12 9/7/12 25

CQC19.7-131PVI0609-09 (4.67)5418.212I0352-MS1 9/12/12 9/12/12 25

CQC19.7-131PVI0525-066315.612I0394-MS1 9/12/12 9/12/12 25

CQC19.7-131PVI0894-066516.212I0598-MS1 9/18/12 9/18/12 25

CQC19.7-131PVI1060-027719.212I0648-MS1 9/18/12 9/18/12 25

CQC19.7-131PVI1553-087418.412I0925-MS1 9/25/12 9/25/12 25

CQC19.7-131PVI1510-086014.912I0926-MS1 9/25/12 9/25/12 25

CQC19.7-131PVI1723-039523.812I1065-MS1 9/28/12 9/28/12 25

CQC19.7-131PVI1822-029222.912I1095-MS1 9/28/12 9/28/12 25

CQC19.7-131PVI1869-051002512I1107-MS1 9/29/12 9/29/12 25

CQC19.7-131PVI1575-0110325.612J0008-MS1 10/1/12 10/1/12 25

19.7-131PVJ0513-036616.612J0298-MS1 10/8/12 10/8/12 25

19.7-131PVJ0682-01 (7.54)6824.612J0389-MS1 10/10/12 10/10/12 25

CQC19.7-131PVJ0682-175513.712J0445-MS1 10/11/12 10/11/12 25

CQC19.7-131PVJ1065-025714.212J0620-MS1 10/16/12 10/16/12 25

CQC19.7-131PVJ1237-026115.212J0736-MS1 10/18/12 10/18/12 25

CQC19.7-131PVJ1405-025613.912J0821-MS1 10/20/12 10/20/12 25

CQC19.7-131PVJ1405-177418.512J0850-MS1 10/22/12 10/22/12 25

CQC19.7-131PVJ1577-025814.412J0972-MS1 10/24/12 10/24/12 25

CQC19.7-131PVJ1627-0112631512J1010-MS1 10/25/12 10/25/12 250

CQC19.7-131PVJ1600-025212.912J1038-MS1 10/25/12 10/25/12 25

CQC19.7-131PVJ1577-18RE16015012J1059-MS1 10/26/12 10/26/12 250

CQC19.7-131PVK0237-017418.412K0235-MS1 11/7/12 11/7/12 25

CQC19.7-131PVK0555-04 (31.3)8753.112K0286-MS1 11/8/12 11/8/12 25

19.7-131PVK0649-06 (20.9)5735.212K0341-MS1 11/9/12 11/9/12 25

CQC19.7-131PVK0756-01 (38.9)5652.812K0415-MS1 11/12/12 11/12/12 25

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MS %RAcetoneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC19.7-131PVK0793-026115.412K0462-MS1 11/13/12 11/13/12 25

CQC19.7-131PVK0281-015614.1X 12K0522-MS1 11/14/12 11/14/12 25

CQC19.7-131PVK0632-095413.612K0553-MS1 11/14/12 11/14/12 25

CQC19.7-131PVK0684-027117.712K0552-MS1 11/14/12 11/14/12 25

CQC19.7-131PVK0696-015313.312K0581-MS1 11/15/12 11/15/12 25

CQC,C19.7-131PVK0934-016516.212K0740-MS1 11/20/12 11/20/12 25

CQC19.7-131PVK0768-027318.312K0751-MS1 11/20/12 11/20/12 25

CQC19.7-131PVK1220-026917.4X 12K0803-MS1 11/21/12 11/21/12 25

CQC19.7-131PVK1288-036917.212K0836-MS1 11/21/12 11/21/12 25

CQC19.7-131PVK1375-08 (4.2)6219.612K0865-MS1 11/23/12 11/23/12 25

CQC19.7-131PVK1375-028320.812K0855-MS1 11/23/12 11/23/12 25

CQC19.7-131PVK0988-036817.112K0897-MS1 11/24/12 11/24/12 25

CQC19.7-131PVK1006-017518.712K0905-MS1 11/25/12 11/25/12 25

CQC19.7-131PVK1450-10 (7.16)6623.812K1135-MS1 11/30/12 11/30/12 25

CQC19.7-131PVK1450-038621.412K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDAcetone


6816.9259/1/129/1/1212I0005-MSD1 CQC2596115.4 PVH2309-02

4415.8259/4/129/4/1212I0028-MSD1 CQC2564115 PVH2309-11 (4.78)

7017.5259/5/129/5/1212I0081-MSD1 CQC2546716.7 PVH2037-07

5213.1259/7/129/7/1212I0215-MSD1 CQC25114711.8 PVI0290-03

6220.1259/12/129/12/1212I0352-MSD1 CQC25105418.2 PVI0609-09 (4.67)

7017.6259/12/129/12/1212I0394-MSD1 CQC25126315.6 PVI0525-06

6616.4259/18/129/18/1212I0598-MSD1 CQC2516516.2 PVI0894-06

8220.5259/18/129/18/1212I0648-MSD1 CQC2567719.2 PVI1060-02

7618.9259/25/129/25/1212I0925-MSD1 CQC2527418.4 PVI1553-08

6215.5259/25/129/25/1212I0926-MSD1 CQC2546014.9 PVI1510-08

9523.8259/28/129/28/1212I1065-MSD1 CQC250.089523.8 PVI1723-03

10826.9259/28/129/28/1212I1095-MSD1 CQC25169222.9 PVI1822-02

10726.8259/29/129/29/1212I1107-MSD1 CQC25710025 PVI1869-05

10927.22510/1/1210/1/1212J0008-MSD1 CQC25610325.6 PVI1575-01

6516.22510/8/1210/8/1212J0298-MSD1 2526616.6 PVJ0513-03

6924.72510/10/1210/10/1212J0389-MSD1 250.36824.6 PVJ0682-01 (7.54)

5513.82510/11/1210/11/1212J0445-MSD1 CQC250.55513.7 PVJ0682-17

5012.52510/16/1210/16/1212J0620-MSD1 CQC25125714.2 PVJ1065-02

60152510/18/1210/18/1212J0736-MSD1 CQC2516115.2 PVJ1237-02

5814.52510/20/1210/20/1212J0821-MSD1 CQC2545613.9 PVJ1405-02

60152510/22/1210/22/1212J0850-MSD1 CQC25217418.5 PVJ1405-17

72182510/24/1210/24/1212J0972-MSD1 CQC25225814.4 PVJ1577-02

14335825010/25/1210/25/1212J1010-MSD1 CQC,M12513126315 PVJ1627-01

52132510/25/1210/25/1212J1038-MSD1 CQC250.45212.9 PVJ1600-02

6616525010/26/1210/26/1212J1059-MSD1 CQC251060150 PVJ1577-18RE1

7619.12511/7/1211/7/1212K0235-MSD1 CQC2537418.4 PVK0237-01

8151.52511/8/1211/8/1212K0286-MSD1 CQC2538753.1 PVK0555-04 (31.3)

61362511/9/1211/9/1212K0341-MSD1 2525735.2 PVK0649-06 (20.9)

3848.42511/12/1211/12/1212K0415-MSD1 CQC2595652.8 PVK0756-01 (38.9)

6115.22511/13/1211/13/1212K0462-MSD1 CQC2516115.4 PVK0793-02

5814.62511/14/1211/14/1212K0522-MSD1 CQC2535614.1 PVK0281-01

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MS/MSD RPDAcetone%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

4912.22511/14/1211/14/1212K0553-MSD1 CQC25115413.6 PVK0632-09

7719.42511/14/1211/14/1212K0552-MSD1 CQC2597117.7 PVK0684-02

6516.42511/15/1211/15/1212K0581-MSD1 CQC25215313.3 PVK0696-01

5413.42511/20/1211/20/1212K0740-MSD1 CQC,C25196516.2 PVK0934-01

7619.12511/20/1211/20/1212K0751-MSD1 CQC2547318.3 PVK0768-02

6616.52511/21/1211/21/1212K0803-MSD1 CQC2556917.4 PVK1220-02

7919.82511/21/1211/21/1212K0836-MSD1 CQC25146917.2 PVK1288-03

6721.12511/23/1211/23/1212K0865-MSD1 CQC2576219.6 PVK1375-08 (4.2)

6716.72511/23/1211/23/1212K0855-MSD1 CQC25228320.8 PVK1375-02

8320.72511/24/1211/24/1212K0897-MSD1 CQC25196817.1 PVK0988-03

76192511/25/1211/25/1212K0905-MSD1 CQC2517518.7 PVK1006-01

6924.52511/30/1211/30/1212K1135-MSD1 CQC2536623.8 PVK1450-10 (7.16)

8019.92512/1/1211/30/1212K1134-MSD1 CQC2588621.4 PVK1450-03

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BLKAcetone

20

18

16

14

12

10 ~-----------------*------------------------~ 8 ...... . ............................. . ~--------------~~~+4-------------------------------l

Plotted: 44

MDL: 3.8

MRL: 20

Rejected: 2

Stdv: 2.52

Mean: 2.5

2s: 7.54 6 }\ M \A }\~ 3s 10.1 4 ~+ /\ -+~ h. '""'/f-W~\~A=--++H+->4-~+-"~\------j}~-----""""'i 4s: 12.6

: vy v~ ll l7w- \ A j 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %RBenzene


12I0005-BS1 26.9 108259/1/12 80.7-1209/1/12 CQC

12I0028-BS1 25.5 102259/4/12 80.7-1209/4/12 CQC

12I0081-BS1 21.8 87259/5/12 80.7-1209/5/12 CQC

12I0215-BS1 23.6 94259/7/12 80.7-1209/7/12 CQC

12I0352-BS1 26.4 106259/12/12 80.7-1209/12/12 CQC

12I0394-BS1 22.4 90259/12/12 80.7-1209/12/12 CQC

12I0598-BS1 27.6 110259/18/12 80.7-1209/18/12 CQC

12I0648-BS1 24.1 96259/18/12 80.7-1209/18/12 CQC

12I0926-BS1 24.4 98259/25/12 80.7-1209/25/12 CQC

12I0925-BS1 23.3 93259/25/12 80.7-1209/25/12 CQC

12I1065-BS1 25 100259/28/12 80.7-1209/28/12 CQC

12I1095-BS1 24.6 99259/28/12 80.7-1209/28/12 CQC

12I1107-BS1 26 104259/29/12 80.7-1209/29/12 CQC

12J0008-BS1 25.9 1042510/1/12 80.7-12010/1/12 CQC

12J0298-BS1 22.8 912510/8/12 80.7-12010/8/12

12J0389-BS1 22.8 912510/10/12 80.7-12010/10/12

12J0445-BS1 23.3 932510/11/12 80.7-12010/11/12 CQC

12J0620-BS1 24 962510/16/12 80.7-12010/16/12 CQC

12J0736-BS1 23.4 942510/18/12 80.7-12010/18/12 CQC

12J0821-BS1 25 1002510/20/12 80.7-12010/20/12 CQC

12J0850-BS1 22.8 912510/22/12 80.7-12010/22/12 CQC

12J0972-BS1 25.2 1012510/24/12 80.7-12010/24/12 CQC

12J1010-BS1 24.7 992510/25/12 80.7-12010/25/12 CQC

12J1038-BS1 25.3 1012510/25/12 80.7-12010/25/12 CQC

12J1059-BS1 25.2 1012510/26/12 80.7-12010/26/12 CQC

12K0235-BS1 28.5 1142511/7/12 80.7-12011/7/12 CQC

12K0286-BS1 24.5 982511/8/12 80.7-12011/8/12 CQC

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LCS %RBenzeneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 24 962511/9/12 80.7-12011/9/12

12K0415-BS1 24.2 972511/12/12 80.7-12011/12/12 CQC

12K0462-BS1 26.1 1042511/13/12 80.7-12011/13/12 CQC

12K0522-BS1 27.1 1082511/14/12 80.7-12011/14/12 CQC

12K0553-BS1 26.9 1082511/14/12 80.7-12011/14/12 CQC

12K0552-BS1 24.8 992511/14/12 80.7-12011/14/12 CQC

12K0581-BS1 26.8 1072511/15/12 80.7-12011/15/12 CQC

12K0740-BS1 23.6 952511/20/12 80.7-12011/20/12 CQC

12K0751-BS1 25.1 1012511/20/12 80.7-12011/20/12 CQC

12K0789-BS1 26 1042511/20/12 80.7-12011/20/12

12K0803-BS1 24.3 97X 2511/21/12 80.7-12011/21/12 CQC

12K0836-BS1 24.8 992511/21/12 80.7-12011/21/12 CQC

12K0855-BS1 24.7 992511/23/12 80.7-12011/23/12 CQC

12K0865-BS1 25 1002511/23/12 80.7-12011/23/12 CQC

12K0897-BS1 25.7 1032511/24/12 80.7-12011/24/12 CQC

12K0905-BS1 27.3 1092511/25/12 80.7-12011/25/12 CQC

12K1134-BS1 24.6 982511/30/12 80.7-12011/30/12 CQC

12K1135-BS1 23.7 952511/30/12 80.7-12011/30/12 CQC

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LCS/LCSD RPDBenzene


9523.7259/1/129/1/1212I0005-BSD1 26.9 108 13 25 CQC

10726.9259/4/129/4/1212I0028-BSD1 25.5 102 5 25 CQC

9022.6259/5/129/5/1212I0081-BSD1 21.8 87 4 25 CQC

9122.8259/7/129/7/1212I0215-BSD1 23.6 94 3 25 CQC

10225.4259/12/129/12/1212I0352-BSD1 26.4 106 4 25 CQC

9423.4259/12/129/12/1212I0394-BSD1 22.4 90 4 25 CQC

11127.7259/18/129/18/1212I0598-BSD1 27.6 110 0.3 25 CQC

9523.7259/18/129/18/1212I0648-BSD1 24.1 96 1 25 CQC

9323.3259/25/129/25/1212I0926-BSD1 24.4 98 4 25 CQC

9223259/25/129/25/1212I0925-BSD1 23.3 93 1 25 CQC

10526.3259/28/129/28/1212I1065-BSD1 25 100 5 25 CQC

10425.9259/28/129/28/1212I1095-BSD1 24.6 99 5 25 CQC

9724.4259/29/129/29/1212I1107-BSD1 26 104 7 25 CQC

10726.92510/1/1210/1/1212J0008-BSD1 25.9 104 4 25 CQC

9122.82510/8/1210/8/1212J0298-BSD1 22.8 91 0.04 25

9122.82510/10/1210/10/1212J0389-BSD1 22.8 91 0 25

96242510/11/1210/11/1212J0445-BSD1 23.3 93 3 25 CQC

9724.42510/16/1210/16/1212J0620-BSD1 24 96 2 25 CQC

9323.22510/18/1210/18/1212J0736-BSD1 23.4 94 0.8 25 CQC

9824.52510/20/1210/20/1212J0821-BSD1 25 100 2 25 CQC

9122.62510/22/1210/22/1212J0850-BSD1 22.8 91 1 25 CQC

9323.22510/24/1210/24/1212J0972-BSD1 25.2 101 8 25 CQC

10325.62510/25/1210/25/1212J1010-BSD1 24.7 99 4 25 CQC

10526.32510/25/1210/25/1212J1038-BSD1 25.3 101 4 25 CQC

10927.12510/26/1210/26/1212J1059-BSD1 25.2 101 7 25 CQC

11428.42511/7/1211/7/1212K0235-BSD1 28.5 114 0.1 25 CQC

9924.72511/8/1211/8/1212K0286-BSD1 24.5 98 0.6 25 CQC

01/02/13 15:46

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LCS/LCSD RPDBenzene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

9423.52511/9/1211/9/1212K0341-BSD1 24 96 2 25

9724.32511/12/1211/12/1212K0415-BSD1 24.2 97 0.5 25 CQC

10726.82511/13/1211/13/1212K0462-BSD1 26.1 104 3 25 CQC

10626.42511/14/1211/14/1212K0522-BSD1 27.1 108 2 25 CQC

9824.52511/14/1211/14/1212K0553-BSD1 26.9 108 9 25 CQC

9924.62511/14/1211/14/1212K0552-BSD1 24.8 99 0.6 25 CQC

10927.32511/15/1211/15/1212K0581-BSD1 26.8 107 2 25 CQC

9724.22511/20/1211/20/1212K0740-BSD1 23.6 95 3 25 CQC

9824.52511/20/1211/20/1212K0751-BSD1 25.1 101 2 25 CQC

10425.92511/20/1211/20/1212K0789-BSD1 26 104 0.2 25

10025.12511/21/1211/21/1212K0803-BSD1X 24.3 97 3 25 CQC

9323.22511/21/1211/21/1212K0836-BSD1 24.8 99 7 25 CQC

9924.82511/23/1211/23/1212K0855-BSD1 24.7 99 0.4 25 CQC

10125.22511/23/1211/23/1212K0865-BSD1 25 100 0.7 25 CQC

10726.62511/24/1211/24/1212K0897-BSD1 25.7 103 4 25 CQC

11328.22511/25/1211/25/1212K0905-BSD1 27.3 109 3 25 CQC

9623.92511/30/1211/30/1212K1134-BSD1 24.6 98 3 25 CQC

10426.12511/30/1211/30/1212K1135-BSD1 23.7 95 10 25 CQC

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MS %RBenzene


CQC78.4-127PVH2309-021002512I0005-MS1 9/1/12 9/1/12 25

CQC78.4-127PVH2309-1111127.812I0028-MS1 9/4/12 9/4/12 25

CQC78.4-127PVH2037-078721.912I0081-MS1 9/5/12 9/5/12 25

CQC78.4-127PVI0290-039924.812I0215-MS1 9/7/12 9/7/12 25

CQC78.4-127PVI0609-0910626.512I0352-MS1 9/12/12 9/12/12 25

CQC78.4-127PVI0525-069724.312I0394-MS1 9/12/12 9/12/12 25

CQC78.4-127PVI0894-0611127.812I0598-MS1 9/18/12 9/18/12 25

CQC78.4-127PVI1060-029623.912I0648-MS1 9/18/12 9/18/12 25

CQC78.4-127PVI1553-089523.712I0925-MS1 9/25/12 9/25/12 25

CQC78.4-127PVI1510-089323.312I0926-MS1 9/25/12 9/25/12 25

CQC78.4-127PVI1723-031082712I1065-MS1 9/28/12 9/28/12 25

CQC78.4-127PVI1822-029724.412I1095-MS1 9/28/12 9/28/12 25

CQC78.4-127PVI1869-051042612I1107-MS1 9/29/12 9/29/12 25

CQC78.4-127PVI1575-0110626.412J0008-MS1 10/1/12 10/1/12 25

78.4-127PVJ0513-039423.512J0298-MS1 10/8/12 10/8/12 25

78.4-127PVJ0682-019423.512J0389-MS1 10/10/12 10/10/12 25

CQC78.4-127PVJ0682-178822.112J0445-MS1 10/11/12 10/11/12 25

CQC78.4-127PVJ1065-029323.212J0620-MS1 10/16/12 10/16/12 25

CQC78.4-127PVJ1237-029423.412J0736-MS1 10/18/12 10/18/12 25

CQC78.4-127PVJ1405-0210726.812J0821-MS1 10/20/12 10/20/12 25

CQC78.4-127PVJ1405-179022.512J0850-MS1 10/22/12 10/22/12 25

CQC78.4-127PVJ1577-029623.912J0972-MS1 10/24/12 10/24/12 25

CQC78.4-127PVJ1627-01 (189)9843512J1010-MS1 10/25/12 10/25/12 250

CQC78.4-127PVJ1600-02 (0.32)10125.512J1038-MS1 10/25/12 10/25/12 25

CQC78.4-127PVJ1577-18RE110626612J1059-MS1 10/26/12 10/26/12 250

CQC78.4-127PVK0237-0112330.712K0235-MS1 11/7/12 11/7/12 25

CQC78.4-127PVK0555-041162912K0286-MS1 11/8/12 11/8/12 25

78.4-127PVK0649-069423.612K0341-MS1 11/9/12 11/9/12 25

CQC78.4-127PVK0756-01 (0.18)10225.812K0415-MS1 11/12/12 11/12/12 25

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MS %RBenzeneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC78.4-127PVK0793-02 (2.2)1072912K0462-MS1 11/13/12 11/13/12 25

CQC78.4-127PVK0281-01 (7.22)10433.112K0522-MS1 11/14/12 11/14/12 25

CQC78.4-127PVK0632-0910325.712K0553-MS1 11/14/12 11/14/12 25

CQC78.4-127PVK0684-0210125.412K0552-MS1 11/14/12 11/14/12 25

CQC78.4-127PVK0696-0111127.612K0581-MS1 11/15/12 11/15/12 25

CQC78.4-127PVK0934-01 (5.19)9529.112K0740-MS1 11/20/12 11/20/12 25

CQC78.4-127PVK0768-0210726.812K0751-MS1 11/20/12 11/20/12 25

CQC78.4-127PVK1220-0210125.2X 12K0803-MS1 11/21/12 11/21/12 25

CQC78.4-127PVK1288-0310426.112K0836-MS1 11/21/12 11/21/12 25

CQC78.4-127PVK1375-0810325.812K0865-MS1 11/23/12 11/23/12 25

CQC78.4-127PVK1375-021042612K0855-MS1 11/23/12 11/23/12 25

CQC78.4-127PVK0988-0311027.512K0897-MS1 11/24/12 11/24/12 25

CQC78.4-127PVK1006-0111528.612K0905-MS1 11/25/12 11/25/12 25

CQC78.4-127PVK1450-101002512K1135-MS1 11/30/12 11/30/12 25

CQC78.4-127PVK1450-0311829.512K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDBenzene


10125.2259/1/129/1/1212I0005-MSD1 CQC25110025 PVH2309-02

10826.9259/4/129/4/1212I0028-MSD1 CQC25311127.8 PVH2309-11

9022.4259/5/129/5/1212I0081-MSD1 CQC2538721.9 PVH2037-07

9924.7259/7/129/7/1212I0215-MSD1 CQC250.59924.8 PVI0290-03

10325.7259/12/129/12/1212I0352-MSD1 CQC25310626.5 PVI0609-09

9022.4259/12/129/12/1212I0394-MSD1 CQC2589724.3 PVI0525-06

11027.5259/18/129/18/1212I0598-MSD1 CQC25111127.8 PVI0894-06

10125.1259/18/129/18/1212I0648-MSD1 CQC2559623.9 PVI1060-02

9523.7259/25/129/25/1212I0925-MSD1 CQC2509523.7 PVI1553-08

9824.6259/25/129/25/1212I0926-MSD1 CQC2569323.3 PVI1510-08

10626.4259/28/129/28/1212I1065-MSD1 CQC25210827 PVI1723-03

10325.8259/28/129/28/1212I1095-MSD1 CQC2569724.4 PVI1822-02

11829.5259/29/129/29/1212I1107-MSD1 CQC251210426 PVI1869-05

10726.92510/1/1210/1/1212J0008-MSD1 CQC25210626.4 PVI1575-01

9323.22510/8/1210/8/1212J0298-MSD1 2519423.5 PVJ0513-03

9323.32510/10/1210/10/1212J0389-MSD1 250.99423.5 PVJ0682-01

8721.82510/11/1210/11/1212J0445-MSD1 CQC2518822.1 PVJ0682-17

9624.12510/16/1210/16/1212J0620-MSD1 CQC2549323.2 PVJ1065-02

9523.82510/18/1210/18/1212J0736-MSD1 CQC2529423.4 PVJ1237-02

11428.62510/20/1210/20/1212J0821-MSD1 CQC25610726.8 PVJ1405-02

8922.32510/22/1210/22/1212J0850-MSD1 CQC250.89022.5 PVJ1405-17

10125.32510/24/1210/24/1212J0972-MSD1 CQC2569623.9 PVJ1577-02

10144225010/25/1210/25/1212J1010-MSD1 CQC25198435 PVJ1627-01 (189)

10727.12510/25/1210/25/1212J1038-MSD1 CQC25610125.5 PVJ1600-02 (0.32)

10726825010/26/1210/26/1212J1059-MSD1 CQC250.7106266 PVJ1577-18RE1

12631.62511/7/1211/7/1212K0235-MSD1 CQC25312330.7 PVK0237-01

11127.72511/8/1211/8/1212K0286-MSD1 CQC25511629 PVK0555-04

9423.42511/9/1211/9/1212K0341-MSD1 250.79423.6 PVK0649-06

10325.82511/12/1211/12/1212K0415-MSD1 CQC250.310225.8 PVK0756-01 (0.18)

111302511/13/1211/13/1212K0462-MSD1 CQC25310729 PVK0793-02 (2.2)

11235.22511/14/1211/14/1212K0522-MSD1 CQC25610433.1 PVK0281-01 (7.22)

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MS/MSD RPDBenzene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

108272511/14/1211/14/1212K0553-MSD1 CQC25510325.7 PVK0632-09

104262511/14/1211/14/1212K0552-MSD1 CQC25210125.4 PVK0684-02

10726.72511/15/1211/15/1212K0581-MSD1 CQC25311127.6 PVK0696-01

9729.42511/20/1211/20/1212K0740-MSD1 CQC2519529.1 PVK0934-01 (5.19)

11328.22511/20/1211/20/1212K0751-MSD1 CQC25510726.8 PVK0768-02

10726.82511/21/1211/21/1212K0803-MSD1X CQC25610125.2 PVK1220-02

10325.82511/21/1211/21/1212K0836-MSD1 CQC250.910426.1 PVK1288-03

10425.92511/23/1211/23/1212K0865-MSD1 CQC250.310325.8 PVK1375-08

10425.92511/23/1211/23/1212K0855-MSD1 CQC250.510426 PVK1375-02

11027.42511/24/1211/24/1212K0897-MSD1 CQC250.0411027.5 PVK0988-03

11528.82511/25/1211/25/1212K0905-MSD1 CQC250.511528.6 PVK1006-01

10626.52511/30/1211/30/1212K1135-MSD1 CQC25610025 PVK1450-10

11528.92512/1/1211/30/1212K1134-MSD1 CQC25211829.5 PVK1450-03

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BLKBenzene

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

~------------------------------------------~ 0.1

0.0 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

Plotted: 44

MDL: 0.15

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

3s: 0

4s: 0

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LCS %RBromobenzene


12K0235-BS1 28.6 1152511/7/12 83.3-11611/7/12 CQC

12K0286-BS1 25.4 1012511/8/12 83.3-11611/8/12 CQC

12K0341-BS1 28.2 1132511/9/12 83.3-11611/9/12

12K0415-BS1 23.8 952511/12/12 83.3-11611/12/12 CQC

12K0462-BS1 25.4 1012511/13/12 83.3-11611/13/12 CQC

12K0522-BS1 31.2 1252511/14/12 83.3-11611/14/12 CQC,L

12K0803-BS1 23.3 932511/21/12 83.3-11611/21/12 CQC

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LCS/LCSD RPDBromobenzene


11729.12511/7/1211/7/1212K0235-BSD1 28.6 115 2 25 CQC,PSL

10325.72511/8/1211/8/1212K0286-BSD1 25.4 101 1 25 CQC

108272511/9/1211/9/1212K0341-BSD1 28.2 113 4 25

9824.42511/12/1211/12/1212K0415-BSD1 23.8 95 2 25 CQC

10426.12511/13/1211/13/1212K0462-BSD1 25.4 101 3 25 CQC

12330.82511/14/1211/14/1212K0522-BSD1 31.2 125 1 25 CQC,L

9824.52511/21/1211/21/1212K0803-BSD1 23.3 93 5 25 CQC

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MS %RBromobenzene


CQC,PSL79.4-116PVK0237-0111729.112K0235-MS1 11/7/12 11/7/12 25

CQC,M779.4-116PVK0555-0412330.712K0286-MS1 11/8/12 11/8/12 25

79.4-116PVK0649-0611729.212K0341-MS1 11/9/12 11/9/12 25

CQC79.4-116PVK0756-0110225.412K0415-MS1 11/12/12 11/12/12 25

CQC79.4-116PVK0793-0211127.912K0462-MS1 11/13/12 11/13/12 25

CQC,M1479.4-116PVK0281-0112330.712K0522-MS1 11/14/12 11/14/12 25

CQC79.4-116PVK1220-0210225.512K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDBromobenzene


12230.62511/7/1211/7/1212K0235-MSD1 CQC,PSL25511729.1 PVK0237-01

11929.72511/8/1211/8/1212K0286-MSD1 CQC,M725312330.7 PVK0555-04

11929.82511/9/1211/9/1212K0341-MSD1 25211729.2 PVK0649-06

10025.12511/12/1211/12/1212K0415-MSD1 CQC25110225.4 PVK0756-01

12531.32511/13/1211/13/1212K0462-MSD1 CQC,M7251211127.9 PVK0793-02

13032.42511/14/1211/14/1212K0522-MSD1 CQC,M1425512330.7 PVK0281-01

10726.62511/21/1211/21/1212K0803-MSD1 CQC25410225.5 PVK1220-02

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BLKBromobenzene

01/02/13 15:46

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LCS %RBromochloromethane


12K0235-BS1 30.2 1212511/7/12 83-12211/7/12 CQC

12K0286-BS1 25.3 1012511/8/12 83-12211/8/12 CQC

12K0341-BS1 23.1 922511/9/12 83-12211/9/12

12K0415-BS1 27 1082511/12/12 83-12211/12/12 CQC

12K0462-BS1 28.9 1162511/13/12 83-12211/13/12 CQC

12K0522-BS1 28 1122511/14/12 83-12211/14/12 CQC

12K0803-BS1 23.6 952511/21/12 83-12211/21/12 CQC

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LCS/LCSD RPDBromochloromethane


11528.82511/7/1211/7/1212K0235-BSD1 30.2 121 5 25 CQC

10325.72511/8/1211/8/1212K0286-BSD1 25.3 101 1 25 CQC

9423.42511/9/1211/9/1212K0341-BSD1 23.1 92 1 25

10425.92511/12/1211/12/1212K0415-BSD1 27 108 4 25 CQC

11228.12511/13/1211/13/1212K0462-BSD1 28.9 116 3 25 CQC

11127.72511/14/1211/14/1212K0522-BSD1 28 112 0.9 25 CQC

10626.42511/21/1211/21/1212K0803-BSD1 23.6 95 11 25 CQC

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MS %RBromochloromethane


CQC,PSL75.5-125PVK0237-0113132.812K0235-MS1 11/7/12 11/7/12 25

CQC75.5-125PVK0555-0412130.212K0286-MS1 11/8/12 11/8/12 25

75.5-125PVK0649-069824.412K0341-MS1 11/9/12 11/9/12 25

CQC75.5-125PVK0756-0110626.512K0415-MS1 11/12/12 11/12/12 25

CQC75.5-125PVK0793-0211929.812K0462-MS1 11/13/12 11/13/12 25

CQC75.5-125PVK0281-0110726.712K0522-MS1 11/14/12 11/14/12 25

CQC75.5-125PVK1220-021082712K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDBromochloromethane


13132.82511/7/1211/7/1212K0235-MSD1 CQC,PSL250.213132.8 PVK0237-01

11528.92511/8/1211/8/1212K0286-MSD1 CQC25512130.2 PVK0555-04

9724.22511/9/1211/9/1212K0341-MSD1 2519824.4 PVK0649-06

10626.42511/12/1211/12/1212K0415-MSD1 CQC250.310626.5 PVK0756-01

11929.82511/13/1211/13/1212K0462-MSD1 CQC250.111929.8 PVK0793-02

11629.12511/14/1211/14/1212K0522-MSD1 CQC25810726.7 PVK0281-01

10927.32511/21/1211/21/1212K0803-MSD1 CQC25110827 PVK1220-02

01/02/13 15:46

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BLKBromochloromethane

01/02/13 15:46

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LCS %RBromodichloromethane


12K0235-BS1 28.7 1152511/7/12 84-11711/7/12 CQC

12K0286-BS1 26 1042511/8/12 84-11711/8/12 CQC

12K0341-BS1 25.6 1032511/9/12 84-11711/9/12

12K0415-BS1 25.1 1012511/12/12 84-11711/12/12 CQC

12K0462-BS1 28.1 1132511/13/12 84-11711/13/12 CQC

12K0522-BS1 28.1 1132511/14/12 84-11711/14/12 CQC

12K0803-BS1 25.2 1012511/21/12 84-11711/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPDBromodichloromethane


11829.52511/7/1211/7/1212K0235-BSD1 28.7 115 3 25 CQC,PSL

10325.92511/8/1211/8/1212K0286-BSD1 26 104 0.3 25 CQC

100252511/9/1211/9/1212K0341-BSD1 25.6 103 3 25

9924.72511/12/1211/12/1212K0415-BSD1 25.1 101 2 25 CQC

11027.52511/13/1211/13/1212K0462-BSD1 28.1 113 2 25 CQC

11027.52511/14/1211/14/1212K0522-BSD1 28.1 113 2 25 CQC

10827.12511/21/1211/21/1212K0803-BSD1 25.2 101 7 25 CQC

01/02/13 15:46

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MS %RBromodichloromethane


CQC,PSL78.1-118PVK0237-0112731.712K0235-MS1 11/7/12 11/7/12 25

CQC,M778.1-118PVK0555-041203012K0286-MS1 11/8/12 11/8/12 25

78.1-118PVK0649-061042612K0341-MS1 11/9/12 11/9/12 25

CQC78.1-118PVK0756-0110726.812K0415-MS1 11/12/12 11/12/12 25

CQC78.1-118PVK0793-0211829.412K0462-MS1 11/13/12 11/13/12 25

CQC78.1-118PVK0281-0111027.512K0522-MS1 11/14/12 11/14/12 25

CQC78.1-118PVK1220-0210726.812K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDBromodichloromethane


13232.92511/7/1211/7/1212K0235-MSD1 CQC,PSL25412731.7 PVK0237-01

11628.92511/8/1211/8/1212K0286-MSD1 CQC25412030 PVK0555-04

10125.22511/9/1211/9/1212K0341-MSD1 25310426 PVK0649-06

10626.42511/12/1211/12/1212K0415-MSD1 CQC25110726.8 PVK0756-01

11729.32511/13/1211/13/1212K0462-MSD1 CQC250.511829.4 PVK0793-02

11528.82511/14/1211/14/1212K0522-MSD1 CQC25511027.5 PVK0281-01

11729.32511/21/1211/21/1212K0803-MSD1 CQC25910726.8 PVK1220-02

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BLKBromodichloromethane

01/02/13 15:46

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LCS %RBromoform


12K0235-BS1 23.7 952511/7/12 71.9-13111/7/12 CQC

12K0286-BS1 20.6 832511/8/12 71.9-13111/8/12 CQC

12K0341-BS1 24.2 972511/9/12 71.9-13111/9/12

12K0415-BS1 23.6 942511/12/12 71.9-13111/12/12 CQC

12K0462-BS1 22.6 902511/13/12 71.9-13111/13/12 CQC

12K0522-BS1 27.1 1082511/14/12 71.9-13111/14/12 CQC

12K0803-BS1 21.3 852511/21/12 71.9-13111/21/12 CQC

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LCS/LCSD RPDBromoform


9323.32511/7/1211/7/1212K0235-BSD1 23.7 95 2 25 CQC

8621.52511/8/1211/8/1212K0286-BSD1 20.6 83 4 25 CQC

9223.12511/9/1211/9/1212K0341-BSD1 24.2 97 5 25

9724.32511/12/1211/12/1212K0415-BSD1 23.6 94 3 25 CQC

9022.62511/13/1211/13/1212K0462-BSD1 22.6 90 0.3 25 CQC

10827.12511/14/1211/14/1212K0522-BSD1 27.1 108 0.04 25 CQC

9222.92511/21/1211/21/1212K0803-BSD1 21.3 85 7 25 CQC

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MS %RBromoform


CQC63.7-129PVK0237-01922312K0235-MS1 11/7/12 11/7/12 25

CQC63.7-129PVK0555-049323.212K0286-MS1 11/8/12 11/8/12 25

63.7-129PVK0649-069924.812K0341-MS1 11/9/12 11/9/12 25

CQC63.7-129PVK0756-0110726.812K0415-MS1 11/12/12 11/12/12 25

CQC63.7-129PVK0793-029122.612K0462-MS1 11/13/12 11/13/12 25

CQC63.7-129PVK0281-0110325.712K0522-MS1 11/14/12 11/14/12 25

CQC63.7-129PVK1220-02922312K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDBromoform


9323.22511/7/1211/7/1212K0235-MSD1 CQC250.99223 PVK0237-01

9222.92511/8/1211/8/1212K0286-MSD1 CQC2519323.2 PVK0555-04

9824.62511/9/1211/9/1212K0341-MSD1 250.89924.8 PVK0649-06

108272511/12/1211/12/1212K0415-MSD1 CQC250.810726.8 PVK0756-01

10526.22511/13/1211/13/1212K0462-MSD1 CQC25159122.6 PVK0793-02

10726.82511/14/1211/14/1212K0522-MSD1 CQC25410325.7 PVK0281-01

9122.82511/21/1211/21/1212K0803-MSD1 CQC2519223 PVK1220-02

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BLKBromoform

01/02/13 15:46

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LCS %RBromomethane


12K0235-BS1 29.6 1182511/7/12 56.3-14511/7/12 CQC

12K0286-BS1 24.7 992511/8/12 56.3-14511/8/12 CQC

12K0341-BS1 18.7 752511/9/12 56.3-14511/9/12

12K0415-BS1 21.8 872511/12/12 56.3-14511/12/12 CQC

12K0462-BS1 27.7 1112511/13/12 56.3-14511/13/12 CQC

12K0522-BS1 24.6 982511/14/12 56.3-14511/14/12 CQC

12K0803-BS1 24.6 982511/21/12 56.3-14511/21/12 CQC

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LCS/LCSD RPDBromomethane


11328.22511/7/1211/7/1212K0235-BSD1 29.6 118 5 25 CQC

9924.82511/8/1211/8/1212K0286-BSD1 24.7 99 0.2 25 CQC

8120.32511/9/1211/9/1212K0341-BSD1 18.7 75 8 25

8922.32511/12/1211/12/1212K0415-BSD1 21.8 87 2 25 CQC

10526.22511/13/1211/13/1212K0462-BSD1 27.7 111 6 25 CQC

10025.12511/14/1211/14/1212K0522-BSD1 24.6 98 2 25 CQC

10225.52511/21/1211/21/1212K0803-BSD1 24.6 98 4 25 CQC

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MS %RBromomethane


CQC44.2-155PVK0237-0111829.512K0235-MS1 11/7/12 11/7/12 25

CQC44.2-155PVK0555-0411729.412K0286-MS1 11/8/12 11/8/12 25

44.2-155PVK0649-069122.712K0341-MS1 11/9/12 11/9/12 25

CQC44.2-155PVK0756-019022.612K0415-MS1 11/12/12 11/12/12 25

CQC44.2-155PVK0793-0211428.512K0462-MS1 11/13/12 11/13/12 25

CQC44.2-155PVK0281-011002512K0522-MS1 11/14/12 11/14/12 25

CQC44.2-155PVK1220-029423.412K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDBromomethane


12631.52511/7/1211/7/1212K0235-MSD1 CQC25711829.5 PVK0237-01

11428.42511/8/1211/8/1212K0286-MSD1 CQC25311729.4 PVK0555-04

8621.62511/9/1211/9/1212K0341-MSD1 2559122.7 PVK0649-06

9423.52511/12/1211/12/1212K0415-MSD1 CQC2549022.6 PVK0756-01

11227.92511/13/1211/13/1212K0462-MSD1 CQC25211428.5 PVK0793-02

9824.62511/14/1211/14/1212K0522-MSD1 CQC25210025 PVK0281-01

9623.92511/21/1211/21/1212K0803-MSD1 CQC2529423.4 PVK1220-02

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BLKBromomethane

2.0

1.8

1.6

1.4

1.2

1.0

0.8

0.6

0.4

0.2

0.0

Plotted: 7

MDL: 0.22

MRL: 2

Rejected: 0

Stdv: 0.0783

Mean: 0.14

2s: 0.297

3s: 0.375

E~~~~~~~~~~~~~~§~~~--~~~ 4s:0.453

2 3 4 5 6 7

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LCS %RCarbon tetrachloride


12I0005-BS1 27.4 110259/1/12 82.5-1239/1/12 CQC

12I0028-BS1 25 100259/4/12 82.5-1239/4/12 CQC

12I0081-BS1 29.4 118259/5/12 82.5-1239/5/12 CQC

12I0215-BS1 24.2 97259/7/12 82.5-1239/7/12 CQC

12I0352-BS1 25.2 101259/12/12 82.5-1239/12/12 CQC

12I0394-BS1 29.9 120259/12/12 82.5-1239/12/12 CQC

12I0598-BS1 26.8 107259/18/12 82.5-1239/18/12 CQC

12I0648-BS1 23 92259/18/12 82.5-1239/18/12 CQC

12I0926-BS1 23.9 96259/25/12 82.5-1239/25/12 CQC

12I0925-BS1 24 96259/25/12 82.5-1239/25/12 CQC

12I1065-BS1 24.2 97259/28/12 82.5-1239/28/12 CQC

12I1095-BS1 24.2 97259/28/12 82.5-1239/28/12 CQC

12I1107-BS1 24.9 99259/29/12 82.5-1239/29/12 CQC

12J0008-BS1 24.5 982510/1/12 82.5-12310/1/12 CQC

12J0298-BS1 24.9 1002510/8/12 82.5-12310/8/12

12J0389-BS1 24.2 972510/10/12 82.5-12310/10/12

12J0445-BS1 25 1002510/11/12 82.5-12310/11/12 CQC

12J0620-BS1 23.2 932510/16/12 82.5-12310/16/12 CQC

12J0736-BS1 23.9 962510/18/12 82.5-12310/18/12 CQC

12J0821-BS1 24.3 972510/20/12 82.5-12310/20/12 CQC

12J0850-BS1 24.8 992510/22/12 82.5-12310/22/12 CQC

12J0972-BS1 28.8 1152510/24/12 82.5-12310/24/12 CQC

12J1010-BS1 26.9 1082510/25/12 82.5-12310/25/12 CQC

12J1038-BS1 27.3 1092510/25/12 82.5-12310/25/12 CQC

12J1059-BS1 28.4 1132510/26/12 82.5-12310/26/12 CQC

12K0235-BS1 33.3 1332511/7/12 82.5-12311/7/12 CQC,PSL

12K0286-BS1 28 1122511/8/12 82.5-12311/8/12 CQC

01/02/13 15:46

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LCS %RCarbon tetrachlorideLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 30.7 1232511/9/12 82.5-12311/9/12

12K0415-BS1 25 1002511/12/12 82.5-12311/12/12 CQC

12K0462-BS1 27.5 1102511/13/12 82.5-12311/13/12 CQC

12K0522-BS1 27.8 111X 2511/14/12 82.5-12311/14/12 CQC

12K0553-BS1 29.4 1182511/14/12 82.5-12311/14/12 CQC

12K0552-BS1 26.2 1052511/14/12 82.5-12311/14/12 CQC

12K0581-BS1 30.1 1202511/15/12 82.5-12311/15/12 CQC

12K0740-BS1 26 1042511/20/12 82.5-12311/20/12 CQC

12K0751-BS1 27.4 1102511/20/12 82.5-12311/20/12 CQC

12K0789-BS1 29 1162511/20/12 82.5-12311/20/12

12K0803-BS1 26.3 105X 2511/21/12 82.5-12311/21/12 CQC

12K0836-BS1 26.8 1072511/21/12 82.5-12311/21/12 CQC

12K0855-BS1 28 1122511/23/12 82.5-12311/23/12 CQC

12K0865-BS1 28 1122511/23/12 82.5-12311/23/12 CQC

12K0897-BS1 28.5 1142511/24/12 82.5-12311/24/12 CQC

12K0905-BS1 31.8 1272511/25/12 82.5-12311/25/12 CQC,PSL

12K1134-BS1 27.5 1102511/30/12 82.5-12311/30/12 CQC

12K1135-BS1 26 1042511/30/12 82.5-12311/30/12 CQC

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LCS/LCSD RPDCarbon tetrachloride


9924.6259/1/129/1/1212I0005-BSD1 27.4 110 11 25 CQC

10726.7259/4/129/4/1212I0028-BSD1 25 100 7 25 CQC

11929.8259/5/129/5/1212I0081-BSD1 29.4 118 1 25 CQC

9624.1259/7/129/7/1212I0215-BSD1 24.2 97 0.6 25 CQC

9824.5259/12/129/12/1212I0352-BSD1 25.2 101 3 25 CQC

11829.6259/12/129/12/1212I0394-BSD1 29.9 120 1 25 CQC

10726.8259/18/129/18/1212I0598-BSD1 26.8 107 0.1 25 CQC

9122.7259/18/129/18/1212I0648-BSD1 23 92 2 25 CQC

9323.4259/25/129/25/1212I0926-BSD1 23.9 96 2 25 CQC

9423.5259/25/129/25/1212I0925-BSD1 24 96 2 25 CQC

9824.6259/28/129/28/1212I1065-BSD1 24.2 97 2 25 CQC

10125.2259/28/129/28/1212I1095-BSD1 24.2 97 4 25 CQC

9122.7259/29/129/29/1212I1107-BSD1 24.9 99 9 25 CQC

10125.32510/1/1210/1/1212J0008-BSD1 24.5 98 3 25 CQC

9924.72510/8/1210/8/1212J0298-BSD1 24.9 100 0.8 25

9924.82510/10/1210/10/1212J0389-BSD1 24.2 97 3 25

104262510/11/1210/11/1212J0445-BSD1 25 100 4 25 CQC

9223.12510/16/1210/16/1212J0620-BSD1 23.2 93 0.6 25 CQC

10024.92510/18/1210/18/1212J0736-BSD1 23.9 96 4 25 CQC

9323.12510/20/1210/20/1212J0821-BSD1 24.3 97 5 25 CQC

9824.52510/22/1210/22/1212J0850-BSD1 24.8 99 1 25 CQC

104262510/24/1210/24/1212J0972-BSD1 28.8 115 10 25 CQC

11628.92510/25/1210/25/1212J1010-BSD1 26.9 108 7 25 CQC

11227.92510/25/1210/25/1212J1038-BSD1 27.3 109 2 25 CQC

12029.92510/26/1210/26/1212J1059-BSD1 28.4 113 5 25 CQC

13032.42511/7/1211/7/1212K0235-BSD1 33.3 133 3 25 CQC,PSL

11628.92511/8/1211/8/1212K0286-BSD1 28 112 3 25 CQC

01/02/13 15:46

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LCS/LCSD RPDCarbon tetrachloride%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

12330.62511/9/1211/9/1212K0341-BSD1 30.7 123 0.2 25

9724.32511/12/1211/12/1212K0415-BSD1 25 100 3 25 CQC

11027.42511/13/1211/13/1212K0462-BSD1 27.5 110 0.3 25 CQC

11328.32511/14/1211/14/1212K0522-BSD1 27.8 111 2 25 CQC

112282511/14/1211/14/1212K0553-BSD1 29.4 118 5 25 CQC

10526.22511/14/1211/14/1212K0552-BSD1 26.2 105 0.04 25 CQC

12631.52511/15/1211/15/1212K0581-BSD1 30.1 120 4 25 CQC,PSL

10726.72511/20/1211/20/1212K0740-BSD1 26 104 3 25 CQC

108272511/20/1211/20/1212K0751-BSD1 27.4 110 2 25 CQC

11428.62511/20/1211/20/1212K0789-BSD1 29 116 2 25

108272511/21/1211/21/1212K0803-BSD1X 26.3 105 3 25 CQC

10526.22511/21/1211/21/1212K0836-BSD1 26.8 107 2 25 CQC

11027.42511/23/1211/23/1212K0855-BSD1 28 112 2 25 CQC

11127.92511/23/1211/23/1212K0865-BSD1 28 112 0.6 25 CQC

120302511/24/1211/24/1212K0897-BSD1 28.5 114 5 25 CQC

13132.72511/25/1211/25/1212K0905-BSD1 31.8 127 3 25 CQC,PSL

11027.62511/30/1211/30/1212K1134-BSD1 27.5 110 0.1 25 CQC

12130.42511/30/1211/30/1212K1135-BSD1 26 104 15 25 CQC

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Analyzed By:

MS %RCarbon tetrachloride


CQC80.7-128PVH2309-029824.612I0005-MS1 9/1/12 9/1/12 25

CQC80.7-128PVH2309-1111027.512I0028-MS1 9/4/12 9/4/12 25

CQC80.7-128PVH2037-0711528.812I0081-MS1 9/5/12 9/5/12 25

CQC80.7-128PVI0290-039624.112I0215-MS1 9/7/12 9/7/12 25

CQC80.7-128PVI0609-0910325.812I0352-MS1 9/12/12 9/12/12 25

CQC80.7-128PVI0525-0611829.612I0394-MS1 9/12/12 9/12/12 25

CQC80.7-128PVI0894-0610726.812I0598-MS1 9/18/12 9/18/12 25

CQC80.7-128PVI1060-029223.112I0648-MS1 9/18/12 9/18/12 25

CQC80.7-128PVI1553-089523.912I0925-MS1 9/25/12 9/25/12 25

CQC80.7-128PVI1510-089122.712I0926-MS1 9/25/12 9/25/12 25

CQC80.7-128PVI1723-0310325.712I1065-MS1 9/28/12 9/28/12 25

CQC80.7-128PVI1822-028922.312I1095-MS1 9/28/12 9/28/12 25

CQC80.7-128PVI1869-05922312I1107-MS1 9/29/12 9/29/12 25

CQC80.7-128PVI1575-01962412J0008-MS1 10/1/12 10/1/12 25

80.7-128PVJ0513-0310125.212J0298-MS1 10/8/12 10/8/12 25

80.7-128PVJ0682-0110225.512J0389-MS1 10/10/12 10/10/12 25

CQC80.7-128PVJ0682-179623.912J0445-MS1 10/11/12 10/11/12 25

CQC80.7-128PVJ1065-028922.312J0620-MS1 10/16/12 10/16/12 25

CQC80.7-128PVJ1237-029724.412J0736-MS1 10/18/12 10/18/12 25

CQC80.7-128PVJ1405-0210125.212J0821-MS1 10/20/12 10/20/12 25

CQC80.7-128PVJ1405-179724.112J0850-MS1 10/22/12 10/22/12 25

CQC80.7-128PVJ1577-0211328.312J0972-MS1 10/24/12 10/24/12 25

CQC80.7-128PVJ1627-0111127612J1010-MS1 10/25/12 10/25/12 250

CQC80.7-128PVJ1600-0210626.412J1038-MS1 10/25/12 10/25/12 25

CQC80.7-128PVJ1577-18RE111629012J1059-MS1 10/26/12 10/26/12 250

CQC,PSL80.7-128PVK0237-0113333.212K0235-MS1 11/7/12 11/7/12 25

CQC,M780.7-128PVK0555-0412932.312K0286-MS1 11/8/12 11/8/12 25

80.7-128PVK0649-061203012K0341-MS1 11/9/12 11/9/12 25

CQC80.7-128PVK0756-0110726.712K0415-MS1 11/12/12 11/12/12 25

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MS %RCarbon tetrachlorideSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC80.7-128PVK0793-0211227.912K0462-MS1 11/13/12 11/13/12 25

CQC80.7-128PVK0281-0110426X 12K0522-MS1 11/14/12 11/14/12 25

CQC80.7-128PVK0632-0911628.912K0553-MS1 11/14/12 11/14/12 25

CQC80.7-128PVK0684-0210526.212K0552-MS1 11/14/12 11/14/12 25

CQC80.7-128PVK0696-0112130.312K0581-MS1 11/15/12 11/15/12 25

CQC80.7-128PVK0934-0110726.712K0740-MS1 11/20/12 11/20/12 25

CQC80.7-128PVK0768-021122812K0751-MS1 11/20/12 11/20/12 25

CQC80.7-128PVK1220-0210626.512K0803-MS1 11/21/12 11/21/12 25

CQC80.7-128PVK1288-0311328.212K0836-MS1 11/21/12 11/21/12 25

CQC80.7-128PVK1375-0811127.612K0865-MS1 11/23/12 11/23/12 25

CQC80.7-128PVK1375-0211729.312K0855-MS1 11/23/12 11/23/12 25

CQC80.7-128PVK0988-031203012K0897-MS1 11/24/12 11/24/12 25

CQC,PSL80.7-128PVK1006-0113132.812K0905-MS1 11/25/12 11/25/12 25

CQC80.7-128PVK1450-1010626.412K1135-MS1 11/30/12 11/30/12 25

CQC,M780.7-128PVK1450-0313734.312K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDCarbon tetrachloride


9824.4259/1/129/1/1212I0005-MSD1 CQC250.79824.6 PVH2309-02

10526.2259/4/129/4/1212I0028-MSD1 CQC25511027.5 PVH2309-11

11528.7259/5/129/5/1212I0081-MSD1 CQC250.211528.8 PVH2037-07

9624259/7/129/7/1212I0215-MSD1 CQC250.29624.1 PVI0290-03

9824.5259/12/129/12/1212I0352-MSD1 CQC25510325.8 PVI0609-09

11729.3259/12/129/12/1212I0394-MSD1 CQC25111829.6 PVI0525-06

10626.5259/18/129/18/1212I0598-MSD1 CQC25110726.8 PVI0894-06

9724.2259/18/129/18/1212I0648-MSD1 CQC2559223.1 PVI1060-02

9323.2259/25/129/25/1212I0925-MSD1 CQC2539523.9 PVI1553-08

9323.2259/25/129/25/1212I0926-MSD1 CQC2529122.7 PVI1510-08

10125.3259/28/129/28/1212I1065-MSD1 CQC25210325.7 PVI1723-03

9523.6259/28/129/28/1212I1095-MSD1 CQC2568922.3 PVI1822-02

10927.2259/29/129/29/1212I1107-MSD1 CQC25179223 PVI1869-05

9824.52510/1/1210/1/1212J0008-MSD1 CQC2529624 PVI1575-01

9724.32510/8/1210/8/1212J0298-MSD1 25410125.2 PVJ0513-03

10225.62510/10/1210/10/1212J0389-MSD1 250.510225.5 PVJ0682-01

9423.42510/11/1210/11/1212J0445-MSD1 CQC2529623.9 PVJ0682-17

9423.42510/16/1210/16/1212J0620-MSD1 CQC2558922.3 PVJ1065-02

9924.62510/18/1210/18/1212J0736-MSD1 CQC2519724.4 PVJ1237-02

108272510/20/1210/20/1212J0821-MSD1 CQC25710125.2 PVJ1405-02

9323.22510/22/1210/22/1212J0850-MSD1 CQC2549724.1 PVJ1405-17

12030.12510/24/1210/24/1212J0972-MSD1 CQC25611328.3 PVJ1577-02

11127825010/25/1210/25/1212J1010-MSD1 CQC250.5111276 PVJ1627-01

112282510/25/1210/25/1212J1038-MSD1 CQC25610626.4 PVJ1600-02

12230425010/26/1210/26/1212J1059-MSD1 CQC255116290 PVJ1577-18RE1

14135.32511/7/1211/7/1212K0235-MSD1 CQC,PSL25613333.2 PVK0237-01

12731.82511/8/1211/8/1212K0286-MSD1 CQC25212932.3 PVK0555-04

12130.22511/9/1211/9/1212K0341-MSD1 250.512030 PVK0649-06

10626.42511/12/1211/12/1212K0415-MSD1 CQC25110726.7 PVK0756-01

10927.22511/13/1211/13/1212K0462-MSD1 CQC25211227.9 PVK0793-02

11227.92511/14/1211/14/1212K0522-MSD1X CQC25710426 PVK0281-01

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MS/MSD RPDCarbon tetrachloride%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

12030.12511/14/1211/14/1212K0553-MSD1 CQC25411628.9 PVK0632-09

10526.32511/14/1211/14/1212K0552-MSD1 CQC250.610526.2 PVK0684-02

12230.52511/15/1211/15/1212K0581-MSD1 CQC250.512130.3 PVK0696-01

10726.62511/20/1211/20/1212K0740-MSD1 CQC250.310726.7 PVK0934-01

11628.92511/20/1211/20/1212K0751-MSD1 CQC25311228 PVK0768-02

11528.82511/21/1211/21/1212K0803-MSD1 CQC25810626.5 PVK1220-02

112282511/21/1211/21/1212K0836-MSD1 CQC250.911328.2 PVK1288-03

11027.42511/23/1211/23/1212K0865-MSD1 CQC250.911127.6 PVK1375-08

11328.32511/23/1211/23/1212K0855-MSD1 CQC25411729.3 PVK1375-02

11729.22511/24/1211/24/1212K0897-MSD1 CQC25312030 PVK0988-03

13032.42511/25/1211/25/1212K0905-MSD1 CQC,PSL25113132.8 PVK1006-01

10726.72511/30/1211/30/1212K1135-MSD1 CQC25110626.4 PVK1450-10

13934.82512/1/1211/30/1212K1134-MSD1 CQC,M725113734.3 PVK1450-03

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BLKCarbon tetrachloride

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0.0

Plotted: 44

MDL: 0.19

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

3s: 0 ~------------------------------------------------------------~4.:0

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %RChlorobenzene


12K0235-BS1 29.4 1182511/7/12 82.5-12311/7/12 CQC

12K0286-BS1 25.9 1032511/8/12 82.5-12311/8/12 CQC

12K0341-BS1 26.9 1082511/9/12 82.5-12311/9/12

12K0415-BS1 24.8 992511/12/12 82.5-12311/12/12 CQC

12K0462-BS1 25.5 1022511/13/12 82.5-12311/13/12 CQC

12K0522-BS1 26.3 1052511/14/12 82.5-12311/14/12 CQC

12K0803-BS1 24.5 982511/21/12 82.5-12311/21/12 CQC

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LCS/LCSD RPDChlorobenzene


11929.82511/7/1211/7/1212K0235-BSD1 29.4 118 1 25 CQC

10225.62511/8/1211/8/1212K0286-BSD1 25.9 103 1 25 CQC

10526.22511/9/1211/9/1212K0341-BSD1 26.9 108 3 25

9724.22511/12/1211/12/1212K0415-BSD1 24.8 99 2 25 CQC

10526.32511/13/1211/13/1212K0462-BSD1 25.5 102 3 25 CQC

10626.42511/14/1211/14/1212K0522-BSD1 26.3 105 0.4 25 CQC

10225.42511/21/1211/21/1212K0803-BSD1 24.5 98 4 25 CQC

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MS %RChlorobenzene


CQC,PSL84.6-110PVK0237-0112330.712K0235-MS1 11/7/12 11/7/12 25

CQC,M784.6-110PVK0555-0412030.112K0286-MS1 11/8/12 11/8/12 25

84.6-110PVK0649-0610526.212K0341-MS1 11/9/12 11/9/12 25

CQC84.6-110PVK0756-0110325.712K0415-MS1 11/12/12 11/12/12 25

CQC84.6-110PVK0793-0211027.412K0462-MS1 11/13/12 11/13/12 25

CQC84.6-110PVK0281-0110526.412K0522-MS1 11/14/12 11/14/12 25

CQC84.6-110PVK1220-029924.712K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDChlorobenzene


12731.62511/7/1211/7/1212K0235-MSD1 CQC,PSL25312330.7 PVK0237-01

12130.12511/8/1211/8/1212K0286-MSD1 CQC,M7250.0712030.1 PVK0555-04

10726.82511/9/1211/9/1212K0341-MSD1 25210526.2 PVK0649-06

10526.42511/12/1211/12/1212K0415-MSD1 CQC25310325.7 PVK0756-01

10927.42511/13/1211/13/1212K0462-MSD1 CQC250.111027.4 PVK0793-02

10426.12511/14/1211/14/1212K0522-MSD1 CQC250.910526.4 PVK0281-01

10827.12511/21/1211/21/1212K0803-MSD1 CQC2599924.7 PVK1220-02

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BLKChlorobenzene

01/02/13 15:46

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LCS %RChloroethane


12K0235-BS1 29 1162511/7/12 69.5-13211/7/12 CQC

12K0286-BS1 24.6 992511/8/12 69.5-13211/8/12 CQC

12K0341-BS1 16.5 662511/9/12 69.5-13211/9/12

12K0415-BS1 21.1 842511/12/12 69.5-13211/12/12 CQC

12K0462-BS1 26.8 1072511/13/12 69.5-13211/13/12 CQC

12K0522-BS1 24.1 972511/14/12 69.5-13211/14/12 CQC

12K0803-BS1 23.9 962511/21/12 69.5-13211/21/12 CQC

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LCS/LCSD RPDChloroethane


10927.32511/7/1211/7/1212K0235-BSD1 29 116 6 25 CQC

9523.62511/8/1211/8/1212K0286-BSD1 24.6 99 4 25 CQC

7318.22511/9/1211/9/1212K0341-BSD1 16.5 66 10 25

8320.72511/12/1211/12/1212K0415-BSD1 21.1 84 2 25 CQC

10426.12511/13/1211/13/1212K0462-BSD1 26.8 107 2 25 CQC

10024.92511/14/1211/14/1212K0522-BSD1 24.1 97 3 25 CQC

9924.82511/21/1211/21/1212K0803-BSD1 23.9 96 4 25 CQC

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MS %RChloroethane


CQC68.9-136PVK0237-0111729.212K0235-MS1 11/7/12 11/7/12 25

CQC68.9-136PVK0555-0411027.612K0286-MS1 11/8/12 11/8/12 25

68.9-136PVK0649-068120.212K0341-MS1 11/9/12 11/9/12 25

CQC68.9-136PVK0756-01882212K0415-MS1 11/12/12 11/12/12 25

CQC68.9-136PVK0793-0211228.112K0462-MS1 11/13/12 11/13/12 25

CQC68.9-136PVK0281-0110325.612K0522-MS1 11/14/12 11/14/12 25

CQC68.9-136PVK1220-029523.812K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDChloroethane


12230.62511/7/1211/7/1212K0235-MSD1 CQC25511729.2 PVK0237-01

10626.62511/8/1211/8/1212K0286-MSD1 CQC25411027.6 PVK0555-04

76192511/9/1211/9/1212K0341-MSD1 2568120.2 PVK0649-06

8922.32511/12/1211/12/1212K0415-MSD1 CQC2518822 PVK0756-01

11127.72511/13/1211/13/1212K0462-MSD1 CQC25111228.1 PVK0793-02

10025.12511/14/1211/14/1212K0522-MSD1 CQC25210325.6 PVK0281-01

9824.62511/21/1211/21/1212K0803-MSD1 CQC2539523.8 PVK1220-02

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BLKChloroethane

01/02/13 15:46

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LCS %RChloroform


12I0005-BS1 25.3 101259/1/12 80.7-1199/1/12 CQC

12I0028-BS1 24.5 98259/4/12 80.7-1199/4/12 CQC

12I0081-BS1 23.2 93259/5/12 80.7-1199/5/12 CQC

12I0215-BS1 22.3 89259/7/12 80.7-1199/7/12 CQC

12I0352-BS1 24.8 99259/12/12 80.7-1199/12/12 CQC

12I0394-BS1 21.4 86259/12/12 80.7-1199/12/12 CQC

12I0598-BS1 25.8 103259/18/12 80.7-1199/18/12 CQC

12I0648-BS1 22.2 89259/18/12 80.7-1199/18/12 CQC

12I0926-BS1 23.2 93259/25/12 80.7-1199/25/12 CQC

12I0925-BS1 22.8 91259/25/12 80.7-1199/25/12 CQC

12I1065-BS1 25.2 101259/28/12 80.7-1199/28/12 CQC

12I1095-BS1 25.1 100259/28/12 80.7-1199/28/12 CQC

12I1107-BS1 24.9 100259/29/12 80.7-1199/29/12 CQC

12J0008-BS1 24.7 992510/1/12 80.7-11910/1/12 CQC

12J0298-BS1 21.5 862510/8/12 80.7-11910/8/12

12J0389-BS1 20.4 822510/10/12 80.7-11910/10/12

12J0445-BS1 21.6 862510/11/12 80.7-11910/11/12 CQC

12J0620-BS1 21.7 872510/16/12 80.7-11910/16/12 CQC

12J0736-BS1 22.4 902510/18/12 80.7-11910/18/12 CQC

12J0821-BS1 23.6 942510/20/12 80.7-11910/20/12 CQC

12J0850-BS1 21.5 862510/22/12 80.7-11910/22/12 CQC

12J0972-BS1 23.9 962510/24/12 80.7-11910/24/12 CQC

12J1010-BS1 24.4 982510/25/12 80.7-11910/25/12 CQC

12J1038-BS1 23.6 952510/25/12 80.7-11910/25/12 CQC

12J1059-BS1 27.2 1092510/26/12 80.7-11910/26/12 CQC

12K0235-BS1 26.9 1072511/7/12 80.7-11911/7/12 CQC

12K0286-BS1 23.2 932511/8/12 80.7-11911/8/12 CQC

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LCS %RChloroformLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 20.8 832511/9/12 80.7-11911/9/12

12K0415-BS1 23.1 922511/12/12 80.7-11911/12/12 CQC

12K0462-BS1 26.2 1052511/13/12 80.7-11911/13/12 CQC

12K0522-BS1 25.6 102X 2511/14/12 80.7-11911/14/12 CQC

12K0553-BS1 26.2 1052511/14/12 80.7-11911/14/12 CQC

12K0552-BS1 24.4 972511/14/12 80.7-11911/14/12 CQC

12K0581-BS1 26.5 1062511/15/12 80.7-11911/15/12 CQC

12K0740-BS1 24.5 982511/20/12 80.7-11911/20/12 CQC

12K0751-BS1 25 1002511/20/12 80.7-11911/20/12 CQC

12K0789-BS1 28.2 1132511/20/12 80.7-11911/20/12

12K0803-BS1 25.1 1002511/21/12 80.7-11911/21/12 CQC

12K0836-BS1 26.4 1052511/21/12 80.7-11911/21/12 CQC

12K0855-BS1 26.2 1052511/23/12 80.7-11911/23/12 CQC

12K0865-BS1 24.8 992511/23/12 80.7-11911/23/12 CQC

12K0897-BS1 27 1082511/24/12 80.7-11911/24/12 CQC

12K0905-BS1 28.4 1142511/25/12 80.7-11911/25/12 CQC

12K1134-BS1 25.4 1012511/30/12 80.7-11911/30/12 CQC

12K1135-BS1 23.1 922511/30/12 80.7-11911/30/12 CQC

01/02/13 15:46

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LCS/LCSD RPDChloroform


8822259/1/129/1/1212I0005-BSD1 25.3 101 14 25 CQC

10426.1259/4/129/4/1212I0028-BSD1 24.5 98 6 25 CQC

8922.2259/5/129/5/1212I0081-BSD1 23.2 93 5 25 CQC

8421.1259/7/129/7/1212I0215-BSD1 22.3 89 6 25 CQC

9724.2259/12/129/12/1212I0352-BSD1 24.8 99 3 25 CQC

9223.1259/12/129/12/1212I0394-BSD1 21.4 86 8 25 CQC

10426259/18/129/18/1212I0598-BSD1 25.8 103 0.8 25 CQC

9022.6259/18/129/18/1212I0648-BSD1 22.2 89 2 25 CQC

8621.4259/25/129/25/1212I0926-BSD1 23.2 93 8 25 CQC

9022.6259/25/129/25/1212I0925-BSD1 22.8 91 0.8 25 CQC

9924.6259/28/129/28/1212I1065-BSD1 25.2 101 2 25 CQC

9523.8259/28/129/28/1212I1095-BSD1 25.1 100 6 25 CQC

9323.2259/29/129/29/1212I1107-BSD1 24.9 100 7 25 CQC

10125.22510/1/1210/1/1212J0008-BSD1 24.7 99 2 25 CQC

8621.42510/8/1210/8/1212J0298-BSD1 21.5 86 0.4 25

8220.42510/10/1210/10/1212J0389-BSD1 20.4 82 0.05 25

8621.42510/11/1210/11/1212J0445-BSD1 21.6 86 0.7 25 CQC

8922.32510/16/1210/16/1212J0620-BSD1 21.7 87 3 25 CQC

8922.22510/18/1210/18/1212J0736-BSD1 22.4 90 1 25 CQC

9323.22510/20/1210/20/1212J0821-BSD1 23.6 94 1 25 CQC

8420.92510/22/1210/22/1212J0850-BSD1 21.5 86 3 25 CQC

88222510/24/1210/24/1212J0972-BSD1 23.9 96 8 25 CQC

9423.62510/25/1210/25/1212J1010-BSD1 24.4 98 3 25 CQC

10125.22510/25/1210/25/1212J1038-BSD1 23.6 95 6 25 CQC

10425.92510/26/1210/26/1212J1059-BSD1 27.2 109 5 25 CQC

10526.32511/7/1211/7/1212K0235-BSD1 26.9 107 2 25 CQC

9022.62511/8/1211/8/1212K0286-BSD1 23.2 93 2 25 CQC

01/02/13 15:46

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LCS/LCSD RPDChloroform%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

8320.92511/9/1211/9/1212K0341-BSD1 20.8 83 0.5 25

9223.12511/12/1211/12/1212K0415-BSD1 23.1 92 0.2 25 CQC

10726.82511/13/1211/13/1212K0462-BSD1 26.2 105 2 25 CQC

10626.62511/14/1211/14/1212K0522-BSD1 25.6 102 4 25 CQC

9523.82511/14/1211/14/1212K0553-BSD1 26.2 105 10 25 CQC

9724.42511/14/1211/14/1212K0552-BSD1 24.4 97 0.08 25 CQC

10726.82511/15/1211/15/1212K0581-BSD1 26.5 106 1 25 CQC

100252511/20/1211/20/1212K0740-BSD1 24.5 98 2 25 CQC

9623.92511/20/1211/20/1212K0751-BSD1 25 100 4 25 CQC

10726.82511/20/1211/20/1212K0789-BSD1 28.2 113 5 25

108272511/21/1211/21/1212K0803-BSD1X 25.1 100 7 25 CQC

10225.52511/21/1211/21/1212K0836-BSD1 26.4 105 3 25 CQC

10827.12511/23/1211/23/1212K0855-BSD1 26.2 105 3 25 CQC

10125.32511/23/1211/23/1212K0865-BSD1 24.8 99 2 25 CQC

11027.42511/24/1211/24/1212K0897-BSD1 27 108 2 25 CQC

11628.92511/25/1211/25/1212K0905-BSD1 28.4 114 2 25 CQC

108272511/30/1211/30/1212K1134-BSD1 25.4 101 6 25 CQC

100252511/30/1211/30/1212K1135-BSD1 23.1 92 8 25 CQC

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MS %RChloroform


CQC77.6-122PVH2309-029423.512I0005-MS1 9/1/12 9/1/12 25

CQC77.6-122PVH2309-1110927.412I0028-MS1 9/4/12 9/4/12 25

CQC77.6-122PVH2037-07 (6.85)9029.412I0081-MS1 9/5/12 9/5/12 25

CQC77.6-122PVI0290-03 (0.19)10025.212I0215-MS1 9/7/12 9/7/12 25

CQC77.6-122PVI0609-09 (0.62)9825.212I0352-MS1 9/12/12 9/12/12 25

CQC77.6-122PVI0525-06 (2.36)10227.812I0394-MS1 9/12/12 9/12/12 25

CQC77.6-122PVI0894-06 (5.06)1083212I0598-MS1 9/18/12 9/18/12 25

CQC77.6-122PVI1060-02 (0.52)9123.312I0648-MS1 9/18/12 9/18/12 25

CQC77.6-122PVI1553-089222.912I0925-MS1 9/25/12 9/25/12 25

CQC77.6-122PVI1510-088922.112I0926-MS1 9/25/12 9/25/12 25

CQC77.6-122PVI1723-03 (0.34)10827.412I1065-MS1 9/28/12 9/28/12 25

CQC77.6-122PVI1822-029623.912I1095-MS1 9/28/12 9/28/12 25

CQC77.6-122PVI1869-0510826.912I1107-MS1 9/29/12 9/29/12 25

CQC77.6-122PVI1575-0110726.812J0008-MS1 10/1/12 10/1/12 25

77.6-122PVJ0513-039122.812J0298-MS1 10/8/12 10/8/12 25

77.6-122PVJ0682-018822.112J0389-MS1 10/10/12 10/10/12 25

CQC77.6-122PVJ0682-17 (0.2)832112J0445-MS1 10/11/12 10/11/12 25

CQC77.6-122PVJ1065-028621.512J0620-MS1 10/16/12 10/16/12 25

CQC77.6-122PVJ1237-028922.212J0736-MS1 10/18/12 10/18/12 25

CQC77.6-122PVJ1405-0210325.612J0821-MS1 10/20/12 10/20/12 25

CQC77.6-122PVJ1405-17 (0.28)8621.712J0850-MS1 10/22/12 10/22/12 25

CQC77.6-122PVJ1577-02 (0.23)8822.412J0972-MS1 10/24/12 10/24/12 25

CQC77.6-122PVJ1627-019523712J1010-MS1 10/25/12 10/25/12 250

CQC77.6-122PVJ1600-029924.712J1038-MS1 10/25/12 10/25/12 25

CQC77.6-122PVJ1577-18RE111127612J1059-MS1 10/26/12 10/26/12 250

CQC77.6-122PVK0237-0112130.212K0235-MS1 11/7/12 11/7/12 25

CQC77.6-122PVK0555-0411127.812K0286-MS1 11/8/12 11/8/12 25

77.6-122PVK0649-068621.512K0341-MS1 11/9/12 11/9/12 25

CQC77.6-122PVK0756-019824.612K0415-MS1 11/12/12 11/12/12 25

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MS %RChloroformSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC77.6-122PVK0793-0211328.212K0462-MS1 11/13/12 11/13/12 25

CQC77.6-122PVK0281-0110626.612K0522-MS1 11/14/12 11/14/12 25

CQC77.6-122PVK0632-0910726.812K0553-MS1 11/14/12 11/14/12 25

CQC77.6-122PVK0684-0210726.712K0552-MS1 11/14/12 11/14/12 25

CQC77.6-122PVK0696-0111328.212K0581-MS1 11/15/12 11/15/12 25

CQC77.6-122PVK0934-011042612K0740-MS1 11/20/12 11/20/12 25

CQC77.6-122PVK0768-021162912K0751-MS1 11/20/12 11/20/12 25

CQC77.6-122PVK1220-02 (0.72)11028.212K0803-MS1 11/21/12 11/21/12 25

CQC77.6-122PVK1288-0311328.212K0836-MS1 11/21/12 11/21/12 25

CQC77.6-122PVK1375-0810526.212K0865-MS1 11/23/12 11/23/12 25

CQC77.6-122PVK1375-0211127.712K0855-MS1 11/23/12 11/23/12 25

CQC77.6-122PVK0988-0311729.412K0897-MS1 11/24/12 11/24/12 25

CQC,PSL77.6-122PVK1006-0112531.412K0905-MS1 11/25/12 11/25/12 25

CQC77.6-122PVK1450-10 (1.37)10427.312K1135-MS1 11/30/12 11/30/12 25

CQC,M777.6-122PVK1450-0312932.312K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDChloroform


9624259/1/129/1/1212I0005-MSD1 CQC2529423.5 PVH2309-02

10726.6259/4/129/4/1212I0028-MSD1 CQC25310927.4 PVH2309-11

9330259/5/129/5/1212I0081-MSD1 CQC2529029.4 PVH2037-07 (6.85)

9925259/7/129/7/1212I0215-MSD1 CQC250.810025.2 PVI0290-03 (0.19)

9724.8259/12/129/12/1212I0352-MSD1 CQC2529825.2 PVI0609-09 (0.62)

9826.9259/12/129/12/1212I0394-MSD1 CQC25310227.8 PVI0525-06 (2.36)

10731.8259/18/129/18/1212I0598-MSD1 CQC250.310832 PVI0894-06 (5.06)

8922.8259/18/129/18/1212I0648-MSD1 CQC2529123.3 PVI1060-02 (0.52)

9122.8259/25/129/25/1212I0925-MSD1 CQC250.59222.9 PVI1553-08

9423.6259/25/129/25/1212I0926-MSD1 CQC2578922.1 PVI1510-08

10426.3259/28/129/28/1212I1065-MSD1 CQC25410827.4 PVI1723-03 (0.34)

11027.5259/28/129/28/1212I1095-MSD1 CQC25149623.9 PVI1822-02

11528.8259/29/129/29/1212I1107-MSD1 CQC25710826.9 PVI1869-05

10626.52510/1/1210/1/1212J0008-MSD1 CQC25110726.8 PVI1575-01

92232510/8/1210/8/1212J0298-MSD1 2519122.8 PVJ0513-03

8721.82510/10/1210/10/1212J0389-MSD1 2518822.1 PVJ0682-01

8220.82510/11/1210/11/1212J0445-MSD1 CQC250.78321 PVJ0682-17 (0.2)

9122.72510/16/1210/16/1212J0620-MSD1 CQC2558621.5 PVJ1065-02

96242510/18/1210/18/1212J0736-MSD1 CQC2588922.2 PVJ1237-02

11027.52510/20/1210/20/1212J0821-MSD1 CQC25710325.6 PVJ1405-02

8621.82510/22/1210/22/1212J0850-MSD1 CQC250.58621.7 PVJ1405-17 (0.28)

9423.82510/24/1210/24/1212J0972-MSD1 CQC2568822.4 PVJ1577-02 (0.23)

10025025010/25/1210/25/1212J1010-MSD1 CQC25595237 PVJ1627-01

10426.12510/25/1210/25/1212J1038-MSD1 CQC2559924.7 PVJ1600-02

11328225010/26/1210/26/1212J1059-MSD1 CQC252111276 PVJ1577-18RE1

12130.32511/7/1211/7/1212K0235-MSD1 CQC250.412130.2 PVK0237-01

10526.12511/8/1211/8/1212K0286-MSD1 CQC25611127.8 PVK0555-04

8621.62511/9/1211/9/1212K0341-MSD1 250.78621.5 PVK0649-06

9924.72511/12/1211/12/1212K0415-MSD1 CQC250.49824.6 PVK0756-01

11228.12511/13/1211/13/1212K0462-MSD1 CQC250.211328.2 PVK0793-02

11127.82511/14/1211/14/1212K0522-MSD1X CQC25510626.6 PVK0281-01

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MS/MSD RPDChloroform%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

10726.92511/14/1211/14/1212K0553-MSD1 CQC250.0710726.8 PVK0632-09

11628.92511/14/1211/14/1212K0552-MSD1 CQC25810726.7 PVK0684-02

11328.22511/15/1211/15/1212K0581-MSD1 CQC250.0411328.2 PVK0696-01

104262511/20/1211/20/1212K0740-MSD1 CQC250.110426 PVK0934-01

11629.12511/20/1211/20/1212K0751-MSD1 CQC250.311629 PVK0768-02

11529.42511/21/1211/21/1212K0803-MSD1 CQC25411028.2 PVK1220-02 (0.72)

11528.82511/21/1211/21/1212K0836-MSD1 CQC25211328.2 PVK1288-03

10827.12511/23/1211/23/1212K0865-MSD1 CQC25310526.2 PVK1375-08

11528.72511/23/1211/23/1212K0855-MSD1 CQC25311127.7 PVK1375-02

12130.22511/24/1211/24/1212K0897-MSD1 CQC25311729.4 PVK0988-03

12531.32511/25/1211/25/1212K0905-MSD1 CQC,PSL250.212531.4 PVK1006-01

10828.22511/30/1211/30/1212K1135-MSD1 CQC25310427.3 PVK1450-10 (1.37)

12330.62512/1/1211/30/1212K1134-MSD1 CQC,M725512932.3 PVK1450-03

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BLKChloroform

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0.0

Plotted: 44

MDL: 0.16

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

3s: 0

~------------------------------------------------------------__,4•:0

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %RChloromethane


12K0235-BS1 29.9 1202511/7/12 70.9-12311/7/12 CQC

12K0286-BS1 24.5 982511/8/12 70.9-12311/8/12 CQC

12K0341-BS1 18.4 732511/9/12 70.9-12311/9/12

12K0415-BS1 22.6 902511/12/12 70.9-12311/12/12 CQC

12K0462-BS1 28.8 1152511/13/12 70.9-12311/13/12 CQC

12K0522-BS1 26.8 1072511/14/12 70.9-12311/14/12 CQC

12K0803-BS1 25.8 1032511/21/12 70.9-12311/21/12 CQC

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LCS/LCSD RPDChloromethane


11027.42511/7/1211/7/1212K0235-BSD1 29.9 120 9 25 CQC

96242511/8/1211/8/1212K0286-BSD1 24.5 98 2 25 CQC

7418.42511/9/1211/9/1212K0341-BSD1 18.4 73 0.2 25

9423.52511/12/1211/12/1212K0415-BSD1 22.6 90 4 25 CQC

11328.32511/13/1211/13/1212K0462-BSD1 28.8 115 2 25 CQC

10626.52511/14/1211/14/1212K0522-BSD1 26.8 107 1 25 CQC

11127.62511/21/1211/21/1212K0803-BSD1 25.8 103 7 25 CQC

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MS %RChloromethane


CQC64.1-135PVK0237-0111628.912K0235-MS1 11/7/12 11/7/12 25

CQC64.1-135PVK0555-0411027.412K0286-MS1 11/8/12 11/8/12 25

64.1-135PVK0649-06 (0.22)8120.512K0341-MS1 11/9/12 11/9/12 25

CQC64.1-135PVK0756-019824.512K0415-MS1 11/12/12 11/12/12 25

CQC64.1-135PVK0793-0212230.412K0462-MS1 11/13/12 11/13/12 25

CQC64.1-135PVK0281-0110425.912K0522-MS1 11/14/12 11/14/12 25

CQC64.1-135PVK1220-029724.212K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDChloromethane


12230.62511/7/1211/7/1212K0235-MSD1 CQC25611628.9 PVK0237-01

10726.82511/8/1211/8/1212K0286-MSD1 CQC25211027.4 PVK0555-04

7819.82511/9/1211/9/1212K0341-MSD1 2538120.5 PVK0649-06 (0.22)

9924.82511/12/1211/12/1212K0415-MSD1 CQC2519824.5 PVK0756-01

11428.42511/13/1211/13/1212K0462-MSD1 CQC25712230.4 PVK0793-02

9924.82511/14/1211/14/1212K0522-MSD1 CQC25510425.9 PVK0281-01

10125.22511/21/1211/21/1212K0803-MSD1 CQC2549724.2 PVK1220-02

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BLKChloromethane

01/02/13 15:46

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LCS %Rcis-1,2-Dichloroethene


12I0005-BS1 26.3 105259/1/12 83.3-1179/1/12 CQC

12I0028-BS1 25 100259/4/12 83.3-1179/4/12 CQC

12I0081-BS1 21.8 87259/5/12 83.3-1179/5/12 CQC

12I0215-BS1 23 92259/7/12 83.3-1179/7/12 CQC

12I0352-BS1 28.1 113259/12/12 83.3-1179/12/12 CQC

12I0394-BS1 21.8 87259/12/12 83.3-1179/12/12 CQC

12I0598-BS1 29 116259/18/12 83.3-1179/18/12 CQC

12I0648-BS1 25.6 102259/18/12 83.3-1179/18/12 CQC

12I0926-BS1 25.8 103259/25/12 83.3-1179/25/12 CQC

12I0925-BS1 25.7 103259/25/12 83.3-1179/25/12 CQC

12I1065-BS1 27.8 111259/28/12 83.3-1179/28/12 CQC

12I1095-BS1 27.9 112259/28/12 83.3-1179/28/12 CQC

12I1107-BS1 27.7 111259/29/12 83.3-1179/29/12 CQC

12J0008-BS1 26.9 1082510/1/12 83.3-11710/1/12 CQC

12J0298-BS1 23.2 932510/8/12 83.3-11710/8/12

12J0389-BS1 23.2 932510/10/12 83.3-11710/10/12

12J0445-BS1 24 962510/11/12 83.3-11710/11/12 CQC

12J0620-BS1 23.8 952510/16/12 83.3-11710/16/12 CQC

12J0736-BS1 24.5 982510/18/12 83.3-11710/18/12 CQC

12J0821-BS1 26.3 1052510/20/12 83.3-11710/20/12 CQC

12J0850-BS1 23.6 942510/22/12 83.3-11710/22/12 CQC

12J0972-BS1 24.7 992510/24/12 83.3-11710/24/12 CQC

12J1010-BS1 25 1002510/25/12 83.3-11710/25/12 CQC

12J1038-BS1 23.5 942510/25/12 83.3-11710/25/12 CQC

12J1059-BS1 26.4 1062510/26/12 83.3-11710/26/12 CQC

12K0235-BS1 28.8 1152511/7/12 83.3-11711/7/12 CQC

12K0286-BS1 24.4 982511/8/12 83.3-11711/8/12 CQC

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LCS %Rcis-1,2-DichloroetheneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 22.5 902511/9/12 83.3-11711/9/12

12K0415-BS1 24 962511/12/12 83.3-11711/12/12 CQC

12K0462-BS1 26.5 1062511/13/12 83.3-11711/13/12 CQC

12K0522-BS1 26.8 107X 2511/14/12 83.3-11711/14/12 CQC

12K0553-BS1 25.2 1012511/14/12 83.3-11711/14/12 CQC

12K0552-BS1 24.8 992511/14/12 83.3-11711/14/12 CQC

12K0581-BS1 26 1042511/15/12 83.3-11711/15/12 CQC

12K0740-BS1 24.2 972511/20/12 83.3-11711/20/12 CQC

12K0751-BS1 25.6 1032511/20/12 83.3-11711/20/12 CQC

12K0789-BS1 27.7 1112511/20/12 83.3-11711/20/12

12K0803-BS1 24.1 96X 2511/21/12 83.3-11711/21/12 CQC

12K0836-BS1 25.1 1002511/21/12 83.3-11711/21/12 CQC

12K0855-BS1 25.3 1012511/23/12 83.3-11711/23/12 CQC

12K0865-BS1 24.8 992511/23/12 83.3-11711/23/12 CQC

12K0897-BS1 24.9 1002511/24/12 83.3-11711/24/12 CQC

12K0905-BS1 26.6 1062511/25/12 83.3-11711/25/12 CQC

12K1134-BS1 22.6 902511/30/12 83.3-11711/30/12 CQC

12K1135-BS1 23.4 942511/30/12 83.3-11711/30/12 CQC

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LCS/LCSD RPDcis-1,2-Dichloroethene


9223259/1/129/1/1212I0005-BSD1 26.3 105 13 25 CQC

10526.2259/4/129/4/1212I0028-BSD1 25 100 5 25 CQC

8421259/5/129/5/1212I0081-BSD1 21.8 87 4 25 CQC

8922.2259/7/129/7/1212I0215-BSD1 23 92 4 25 CQC

11027.4259/12/129/12/1212I0352-BSD1 28.1 113 3 25 CQC

9223259/12/129/12/1212I0394-BSD1 21.8 87 5 25 CQC

11528.9259/18/129/18/1212I0598-BSD1 29 116 0.4 25 CQC

10526.3259/18/129/18/1212I0648-BSD1 25.6 102 3 25 CQC

9523.8259/25/129/25/1212I0926-BSD1 25.8 103 8 25 CQC

10025259/25/129/25/1212I0925-BSD1 25.7 103 3 25 CQC

11328.3259/28/129/28/1212I1065-BSD1 27.8 111 2 25 CQC

10726.7259/28/129/28/1212I1095-BSD1 27.9 112 4 25 CQC

10426259/29/129/29/1212I1107-BSD1 27.7 111 6 25 CQC

11328.22510/1/1210/1/1212J0008-BSD1 26.9 108 5 25 CQC

9423.42510/8/1210/8/1212J0298-BSD1 23.2 93 0.9 25

9122.62510/10/1210/10/1212J0389-BSD1 23.2 93 3 25

9423.42510/11/1210/11/1212J0445-BSD1 24 96 2 25 CQC

9824.42510/16/1210/16/1212J0620-BSD1 23.8 95 3 25 CQC

9623.92510/18/1210/18/1212J0736-BSD1 24.5 98 2 25 CQC

10325.62510/20/1210/20/1212J0821-BSD1 26.3 105 2 25 CQC

9223.12510/22/1210/22/1212J0850-BSD1 23.6 94 2 25 CQC

8922.22510/24/1210/24/1212J0972-BSD1 24.7 99 11 25 CQC

9523.72510/25/1210/25/1212J1010-BSD1 25 100 5 25 CQC

10024.92510/25/1210/25/1212J1038-BSD1 23.5 94 6 25 CQC

10325.62510/26/1210/26/1212J1059-BSD1 26.4 106 3 25 CQC

11428.42511/7/1211/7/1212K0235-BSD1 28.8 115 1 25 CQC

9724.22511/8/1211/8/1212K0286-BSD1 24.4 98 1 25 CQC

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LCS/LCSD RPDcis-1,2-Dichloroethene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

88222511/9/1211/9/1212K0341-BSD1 22.5 90 3 25

9323.42511/12/1211/12/1212K0415-BSD1 24 96 2 25 CQC

10726.72511/13/1211/13/1212K0462-BSD1 26.5 106 0.9 25 CQC

11027.42511/14/1211/14/1212K0522-BSD1X 26.8 107 2 25 CQC

9523.82511/14/1211/14/1212K0553-BSD1 25.2 101 6 25 CQC

9924.92511/14/1211/14/1212K0552-BSD1 24.8 99 0.08 25 CQC

10426.12511/15/1211/15/1212K0581-BSD1 26 104 0.3 25 CQC

10125.22511/20/1211/20/1212K0740-BSD1 24.2 97 4 25 CQC

9824.42511/20/1211/20/1212K0751-BSD1 25.6 103 5 25 CQC

10626.62511/20/1211/20/1212K0789-BSD1 27.7 111 4 25

104262511/21/1211/21/1212K0803-BSD1 24.1 96 8 25 CQC

9523.82511/21/1211/21/1212K0836-BSD1 25.1 100 5 25 CQC

10225.62511/23/1211/23/1212K0855-BSD1 25.3 101 1 25 CQC

10225.62511/23/1211/23/1212K0865-BSD1 24.8 99 3 25 CQC

10325.82511/24/1211/24/1212K0897-BSD1 24.9 100 3 25 CQC

10626.52511/25/1211/25/1212K0905-BSD1 26.6 106 0.3 25 CQC

9523.72511/30/1211/30/1212K1134-BSD1 22.6 90 5 25 CQC

10125.32511/30/1211/30/1212K1135-BSD1 23.4 94 8 25 CQC

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MS %Rcis-1,2-Dichloroethene


CQC80.1-119PVH2309-029824.612I0005-MS1 9/1/12 9/1/12 25

CQC80.1-119PVH2309-1111328.212I0028-MS1 9/4/12 9/4/12 25

CQC80.1-119PVH2037-078521.112I0081-MS1 9/5/12 9/5/12 25

CQC80.1-119PVI0290-0310125.412I0215-MS1 9/7/12 9/7/12 25

CQC80.1-119PVI0609-0911127.812I0352-MS1 9/12/12 9/12/12 25

CQC80.1-119PVI0525-06 (6.52)1023212I0394-MS1 9/12/12 9/12/12 25

CQC80.1-119PVI0894-06 (8.32)11837.912I0598-MS1 9/18/12 9/18/12 25

CQC80.1-119PVI1060-0210325.712I0648-MS1 9/18/12 9/18/12 25

CQC80.1-119PVI1553-089924.712I0925-MS1 9/25/12 9/25/12 25

CQC80.1-119PVI1510-081002512I0926-MS1 9/25/12 9/25/12 25

CQC80.1-119PVI1723-031162912I1065-MS1 9/28/12 9/28/12 25

CQC80.1-119PVI1822-0210626.612I1095-MS1 9/28/12 9/28/12 25

CQC80.1-119PVI1869-051122812I1107-MS1 9/29/12 9/29/12 25

CQC80.1-119PVI1575-0111328.212J0008-MS1 10/1/12 10/1/12 25

80.1-119PVJ0513-039924.612J0298-MS1 10/8/12 10/8/12 25

80.1-119PVJ0682-019523.712J0389-MS1 10/10/12 10/10/12 25

CQC80.1-119PVJ0682-179122.712J0445-MS1 10/11/12 10/11/12 25

CQC80.1-119PVJ1065-029323.312J0620-MS1 10/16/12 10/16/12 25

CQC80.1-119PVJ1237-029724.112J0736-MS1 10/18/12 10/18/12 25

CQC80.1-119PVJ1405-0211428.412J0821-MS1 10/20/12 10/20/12 25

CQC80.1-119PVJ1405-179523.612J0850-MS1 10/22/12 10/22/12 25

CQC80.1-119PVJ1577-029122.612J0972-MS1 10/24/12 10/24/12 25

CQC80.1-119PVJ1627-019924712J1010-MS1 10/25/12 10/25/12 250

CQC80.1-119PVJ1600-029824.612J1038-MS1 10/25/12 10/25/12 25

CQC80.1-119PVJ1577-18RE110726812J1059-MS1 10/26/12 10/26/12 250

CQC,PSL80.1-119PVK0237-0112631.612K0235-MS1 11/7/12 11/7/12 25

CQC80.1-119PVK0555-0411729.212K0286-MS1 11/8/12 11/8/12 25

80.1-119PVK0649-069122.812K0341-MS1 11/9/12 11/9/12 25

CQC80.1-119PVK0756-019924.812K0415-MS1 11/12/12 11/12/12 25

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MS %Rcis-1,2-DichloroetheneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC80.1-119PVK0793-0211127.612K0462-MS1 11/13/12 11/13/12 25

CQC80.1-119PVK0281-0110526.312K0522-MS1 11/14/12 11/14/12 25

CQC80.1-119PVK0632-0910526.212K0553-MS1 11/14/12 11/14/12 25

CQC80.1-119PVK0684-021082712K0552-MS1 11/14/12 11/14/12 25

CQC80.1-119PVK0696-0110726.812K0581-MS1 11/15/12 11/15/12 25

CQC80.1-119PVK0934-0110225.612K0740-MS1 11/20/12 11/20/12 25

CQC80.1-119PVK0768-021162912K0751-MS1 11/20/12 11/20/12 25

CQC80.1-119PVK1220-0210927.212K0803-MS1 11/21/12 11/21/12 25

CQC80.1-119PVK1288-0310626.512K0836-MS1 11/21/12 11/21/12 25

CQC80.1-119PVK1375-0810325.712K0865-MS1 11/23/12 11/23/12 25

CQC80.1-119PVK1375-0210225.412K0855-MS1 11/23/12 11/23/12 25

CQC80.1-119PVK0988-0310526.412K0897-MS1 11/24/12 11/24/12 25

CQC80.1-119PVK1006-0111027.612K0905-MS1 11/25/12 11/25/12 25

CQC80.1-119PVK1450-1010626.412K1135-MS1 11/30/12 11/30/12 25

CQC80.1-119PVK1450-0311127.812K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDcis-1,2-Dichloroethene


10125.3259/1/129/1/1212I0005-MSD1 CQC2539824.6 PVH2309-02

11027.5259/4/129/4/1212I0028-MSD1 CQC25311328.2 PVH2309-11

8621.6259/5/129/5/1212I0081-MSD1 CQC2528521.1 PVH2037-07

10325.8259/7/129/7/1212I0215-MSD1 CQC25210125.4 PVI0290-03

10927.2259/12/129/12/1212I0352-MSD1 CQC25211127.8 PVI0609-09

9831259/12/129/12/1212I0394-MSD1 CQC25310232 PVI0525-06 (6.52)

11737.6259/18/129/18/1212I0598-MSD1 CQC250.911837.9 PVI0894-06 (8.32)

10225.5259/18/129/18/1212I0648-MSD1 CQC250.910325.7 PVI1060-02

9824.5259/25/129/25/1212I0925-MSD1 CQC250.59924.7 PVI1553-08

10426259/25/129/25/1212I0926-MSD1 CQC25410025 PVI1510-08

11428.5259/28/129/28/1212I1065-MSD1 CQC25211629 PVI1723-03

12130.3259/28/129/28/1212I1095-MSD1 CQC,PSL251310626.6 PVI1822-02

12130.4259/29/129/29/1212I1107-MSD1 CQC,PSL25811228 PVI1869-05

116292510/1/1210/1/1212J0008-MSD1 CQC25311328.2 PVI1575-01

9824.52510/8/1210/8/1212J0298-MSD1 250.49924.6 PVJ0513-03

9523.72510/10/1210/10/1212J0389-MSD1 250.049523.7 PVJ0682-01

8822.12510/11/1210/11/1212J0445-MSD1 CQC2539122.7 PVJ0682-17

9924.72510/16/1210/16/1212J0620-MSD1 CQC2569323.3 PVJ1065-02

10426.12510/18/1210/18/1212J0736-MSD1 CQC2589724.1 PVJ1237-02

12130.22510/20/1210/20/1212J0821-MSD1 CQC,PSL25611428.4 PVJ1405-02

9423.42510/22/1210/22/1212J0850-MSD1 CQC250.99523.6 PVJ1405-17

9824.62510/24/1210/24/1212J0972-MSD1 CQC2589122.6 PVJ1577-02

9924825010/25/1210/25/1212J1010-MSD1 CQC250.599247 PVJ1627-01

104262510/25/1210/25/1212J1038-MSD1 CQC2569824.6 PVJ1600-02

10726625010/26/1210/26/1212J1059-MSD1 CQC250.4107268 PVJ1577-18RE1

12932.22511/7/1211/7/1212K0235-MSD1 CQC,M725212631.6 PVK0237-01

11528.82511/8/1211/8/1212K0286-MSD1 CQC25111729.2 PVK0555-04

9223.12511/9/1211/9/1212K0341-MSD1 2519122.8 PVK0649-06

100252511/12/1211/12/1212K0415-MSD1 CQC250.99924.8 PVK0756-01

11127.72511/13/1211/13/1212K0462-MSD1 CQC250.311127.6 PVK0793-02

11227.92511/14/1211/14/1212K0522-MSD1 CQC25610526.3 PVK0281-01

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MS/MSD RPDcis-1,2-Dichloroethene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

10526.12511/14/1211/14/1212K0553-MSD1 CQC250.310526.2 PVK0632-09

11528.82511/14/1211/14/1212K0552-MSD1 CQC25610827 PVK0684-02

10726.82511/15/1211/15/1212K0581-MSD1 CQC25010726.8 PVK0696-01

10325.62511/20/1211/20/1212K0740-MSD1 CQC250.110225.6 PVK0934-01

11528.82511/20/1211/20/1212K0751-MSD1 CQC250.711629 PVK0768-02

11428.52511/21/1211/21/1212K0803-MSD1 CQC25510927.2 PVK1220-02

10726.72511/21/1211/21/1212K0836-MSD1 CQC250.910626.5 PVK1288-03

10526.32511/23/1211/23/1212K0865-MSD1 CQC25210325.7 PVK1375-08

104262511/23/1211/23/1212K0855-MSD1 CQC25210225.4 PVK1375-02

11127.82511/24/1211/24/1212K0897-MSD1 CQC25510526.4 PVK0988-03

10927.22511/25/1211/25/1212K0905-MSD1 CQC25211027.6 PVK1006-01

11227.92511/30/1211/30/1212K1135-MSD1 CQC25510626.4 PVK1450-10

10726.62512/1/1211/30/1212K1134-MSD1 CQC25411127.8 PVK1450-03

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BLKcis-1,2-Dichloroethene

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0.0

Plotted: 44

MDL: 0.18

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

3s: 0 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~4s:O

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %Rcis-1,3-Dichloropropene


12K0235-BS1 27.4 1102511/7/12 85-11511/7/12 CQC

12K0286-BS1 23.9 962511/8/12 85-11511/8/12 CQC

12K0341-BS1 23.5 942511/9/12 85-11511/9/12

12K0415-BS1 24.2 972511/12/12 85-11511/12/12 CQC

12K0462-BS1 26.3 1052511/13/12 85-11511/13/12 CQC

12K0522-BS1 25.9 1042511/14/12 85-11511/14/12 CQC

12K0803-BS1 25 1002511/21/12 85-11511/21/12 CQC

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LCS/LCSD RPDcis-1,3-Dichloropropene


108272511/7/1211/7/1212K0235-BSD1 27.4 110 2 25 CQC

9523.62511/8/1211/8/1212K0286-BSD1 23.9 96 1 25 CQC

8922.22511/9/1211/9/1212K0341-BSD1 23.5 94 6 25

9824.42511/12/1211/12/1212K0415-BSD1 24.2 97 0.8 25 CQC

10426.12511/13/1211/13/1212K0462-BSD1 26.3 105 1 25 CQC

104262511/14/1211/14/1212K0522-BSD1 25.9 104 0.3 25 CQC

11027.42511/21/1211/21/1212K0803-BSD1 25 100 9 25 CQC

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MS %Rcis-1,3-Dichloropropene


CQC78.6-118PVK0237-0111829.512K0235-MS1 11/7/12 11/7/12 25

CQC78.6-118PVK0555-0410726.912K0286-MS1 11/8/12 11/8/12 25

78.6-118PVK0649-06962412K0341-MS1 11/9/12 11/9/12 25

CQC78.6-118PVK0756-019824.512K0415-MS1 11/12/12 11/12/12 25

CQC78.6-118PVK0793-0210726.812K0462-MS1 11/13/12 11/13/12 25

CQC78.6-118PVK0281-0110125.212K0522-MS1 11/14/12 11/14/12 25

CQC78.6-118PVK1220-029423.612K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDcis-1,3-Dichloropropene


12330.72511/7/1211/7/1212K0235-MSD1 CQC,PSL25411829.5 PVK0237-01

10726.82511/8/1211/8/1212K0286-MSD1 CQC250.310726.9 PVK0555-04

9223.12511/9/1211/9/1212K0341-MSD1 2549624 PVK0649-06

10325.82511/12/1211/12/1212K0415-MSD1 CQC2559824.5 PVK0756-01

10626.42511/13/1211/13/1212K0462-MSD1 CQC25110726.8 PVK0793-02

10626.52511/14/1211/14/1212K0522-MSD1 CQC25510125.2 PVK0281-01

10125.32511/21/1211/21/1212K0803-MSD1 CQC2579423.6 PVK1220-02

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BLKcis-1,3-Dichloropropene

1.o r -----------------------, 0.9

0.8

0.7 ..... .

0.6 ..... .

0.5 ..... .

Plotted: 7

MDL: 0.17

MRL: 1

Rejected: 0

Stdv: 0.132

r-------------------------~~ 0.4 Mean: 0.05

0.3 p.~~~ .. ~ .. ~~~~~~~~~~~~~~~~~~~~~~~~~-1 2s: 0.315 3s: 0.447

0.2 r---~~----~~~~~~~~~~~~~~~~~~~~~~~~~~ 0

.1

..... "" . 4s: 0.579

0.0 t===~"s;:====::;:=====;::====:;:====::;:::::::::::J 2 3 4 5 6 7

01/02/13 15:46

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LCS %RDibromochloromethane


12K0235-BS1 30.4 1212511/7/12 83.2-12311/7/12 CQC

12K0286-BS1 26.8 1072511/8/12 83.2-12311/8/12 CQC

12K0341-BS1 29 1162511/9/12 83.2-12311/9/12

12K0415-BS1 24.8 992511/12/12 83.2-12311/12/12 CQC

12K0462-BS1 27.9 1112511/13/12 83.2-12311/13/12 CQC

12K0522-BS1 27.4 1102511/14/12 83.2-12311/14/12 CQC

12K0803-BS1 27.3 1092511/21/12 83.2-12311/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPDDibromochloromethane


12631.52511/7/1211/7/1212K0235-BSD1 30.4 121 4 25 CQC,PSL

10726.72511/8/1211/8/1212K0286-BSD1 26.8 107 0.5 25 CQC

11127.82511/9/1211/9/1212K0341-BSD1 29 116 4 25

9724.22511/12/1211/12/1212K0415-BSD1 24.8 99 2 25 CQC

10927.32511/13/1211/13/1212K0462-BSD1 27.9 111 2 25 CQC

11227.92511/14/1211/14/1212K0522-BSD1 27.4 110 2 25 CQC

11027.62511/21/1211/21/1212K0803-BSD1 27.3 109 1 25 CQC

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MS %RDibromochloromethane


CQC,PSL75.2-123PVK0237-0112531.412K0235-MS1 11/7/12 11/7/12 25

CQC75.2-123PVK0555-0412130.212K0286-MS1 11/8/12 11/8/12 25

75.2-123PVK0649-0611428.412K0341-MS1 11/9/12 11/9/12 25

CQC75.2-123PVK0756-0110526.312K0415-MS1 11/12/12 11/12/12 25

CQC75.2-123PVK0793-021162912K0462-MS1 11/13/12 11/13/12 25

CQC75.2-123PVK0281-0111027.612K0522-MS1 11/14/12 11/14/12 25

CQC75.2-123PVK1220-0210626.512K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDDibromochloromethane


12832.12511/7/1211/7/1212K0235-MSD1 CQC,PSL25212531.4 PVK0237-01

12130.32511/8/1211/8/1212K0286-MSD1 CQC250.312130.2 PVK0555-04

11227.92511/9/1211/9/1212K0341-MSD1 25211428.4 PVK0649-06

108272511/12/1211/12/1212K0415-MSD1 CQC25310526.3 PVK0756-01

11328.42511/13/1211/13/1212K0462-MSD1 CQC25211629 PVK0793-02

11228.12511/14/1211/14/1212K0522-MSD1 CQC25211027.6 PVK0281-01

11127.82511/21/1211/21/1212K0803-MSD1 CQC25510626.5 PVK1220-02

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BLKDibromochloromethane

01/02/13 15:46

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%R in BLKDibromofluoromethane


12I0005-BLK1 25.6259/1/12 102 80.3-1309/1/12 CQC

12I0028-BLK1 21.8259/4/12 87 80.3-1309/4/12 CQC

12I0081-BLK1 25.4259/5/12 102 80.3-1309/5/12 CQC

12I0215-BLK1 24259/7/12 96 80.3-1309/7/12 CQC

12I0352-BLK1 24.5259/12/12 98 80.3-1309/12/12 CQC

12I0394-BLK1 26.1259/12/12 104 80.3-1309/12/12 CQC

12I0598-BLK1 25.5259/18/12 102 80.3-1309/18/12 CQC

12I0648-BLK1 24259/18/12 96 80.3-1309/18/12 CQC

12I0926-BLK1 23.4259/25/12 94 80.3-1309/25/12 CQC

12I0925-BLK1 24.4259/25/12 98 80.3-1309/25/12 CQC

12I1065-BLK1 28.1259/28/12 113 80.3-1309/28/12 CQC

12I1095-BLK1 28259/28/12 112 80.3-1309/28/12 CQC

12I1107-BLK1 28.3259/29/12 113 80.3-1309/29/12 CQC

12J0008-BLK1 27.42510/1/12 110 80.3-13010/1/12 CQC

12J0298-BLK1 262510/8/12 104 80.3-13010/8/12

12J0389-BLK1 242510/10/12 96 80.3-13010/10/12

12J0445-BLK1 25.52510/11/12 102 80.3-13010/11/12 CQC

12J0620-BLK1 25.82510/16/12 103 80.3-13010/16/12 CQC

12J0736-BLK1 25.82510/18/12 103 80.3-13010/18/12 CQC

12J0821-BLK1 25.82510/20/12 103 80.3-13010/20/12 CQC

12J0850-BLK1 27.82510/22/12 111 80.3-13010/22/12 CQC

12J0972-BLK1 26.62510/24/12 107 80.3-13010/24/12 CQC

12J1010-BLK1 28.12510/25/12 112 80.3-13010/25/12 CQC

12J1038-BLK1 28.52510/25/12 114 80.3-13010/25/12 CQC

12J1059-BLK1 29.22510/26/12 117 80.3-13010/26/12 CQC

12K0235-BLK1 24.72511/7/12 99 80.3-13011/7/12 CQC

12K0286-BLK1 252511/8/12 100 80.3-13011/8/12 CQC

12K0341-BLK1 22.52511/9/12 90 80.3-13011/9/12

12K0415-BLK1 29.12511/12/12 117 80.3-13011/12/12 CQC

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%R in BLKDibromofluoromethaneLimits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

12K0462-BLK1 28.62511/13/12 114 80.3-13011/13/12 CQC

12K0522-BLK1 292511/14/12 116 80.3-13011/14/12 CQC

12K0552-BLK1 302511/14/12 120 80.3-13011/14/12 CQC

12K0553-BLK1 29.52511/14/12 118 80.3-13011/14/12 CQC

12K0581-BLK1 30.42511/15/12 122 80.3-13011/15/12 CQC

12K0740-BLK1 292511/20/12 116 80.3-13011/20/12 CQC

12K0751-BLK1 312511/20/12 124 80.3-13011/20/12 CQC

X 12K0803-BLK1 28.52511/21/12 114 80.3-13011/21/12 CQC

12K0836-BLK1 29.12511/21/12 117 80.3-13011/21/12 CQC

12K0865-BLK1 30.62511/23/12 123 80.3-13011/23/12 CQC

12K0855-BLK1 29.52511/23/12 118 80.3-13011/23/12 CQC

12K0897-BLK1 28.42511/24/12 114 80.3-13011/24/12 CQC

12K0905-BLK1 27.12511/25/12 108 80.3-13011/25/12 CQC

12K1134-BLK1 292511/30/12 116 80.3-13011/30/12 CQC

12K1135-BLK1 27.92511/30/12 112 80.3-13011/30/12 CQC

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%R In BS/BSDDibromofluoromethane


12I0005-BS1 25.4259/1/12 102 80.3-1309/1/12 CQC

12I0005-BSD1 24.8259/1/12 99 80.3-1309/1/12 CQC

12I0028-BS1 24.4259/4/12 98 80.3-1309/4/12 CQC

12I0028-BSD1 25259/4/12 100 80.3-1309/4/12 CQC

12I0081-BS1 25.3259/5/12 101 80.3-1309/5/12 CQC

12I0081-BSD1 25.2259/5/12 101 80.3-1309/5/12 CQC

12I0215-BS1 24.4259/7/12 98 80.3-1309/7/12 CQC

12I0215-BSD1 23.4259/7/12 94 80.3-1309/7/12 CQC

12I0352-BS1 27.1259/12/12 109 80.3-1309/12/12 CQC

12I0352-BSD1 26259/12/12 104 80.3-1309/12/12 CQC

12I0394-BS1 24.2259/12/12 97 80.3-1309/12/12 CQC

12I0394-BSD1 25259/12/12 100 80.3-1309/12/12 CQC

12I0598-BS1 26.2259/18/12 105 80.3-1309/18/12 CQC

12I0598-BSD1 25.3259/18/12 101 80.3-1309/18/12 CQC

12I0648-BS1 24.6259/18/12 98 80.3-1309/18/12 CQC

12I0648-BSD1 24.5259/18/12 98 80.3-1309/18/12 CQC

12I0926-BS1 24.9259/25/12 100 80.3-1309/25/12 CQC

12I0925-BS1 24.9259/25/12 100 80.3-1309/25/12 CQC

12I0926-BSD1 23.4259/25/12 94 80.3-1309/25/12 CQC

12I0925-BSD1 25.1259/25/12 100 80.3-1309/25/12 CQC

12I1065-BS1 29.1259/28/12 116 80.3-1309/28/12 CQC

12I1065-BSD1 28.9259/28/12 115 80.3-1309/28/12 CQC

12I1095-BS1 28.6259/28/12 115 80.3-1309/28/12 CQC

12I1095-BSD1 26.7259/28/12 107 80.3-1309/28/12 CQC

12I1107-BS1 29.1259/29/12 117 80.3-1309/29/12 CQC

12I1107-BSD1 28.5259/29/12 114 80.3-1309/29/12 CQC

12J0008-BS1 28.92510/1/12 115 80.3-13010/1/12 CQC

12J0008-BSD1 27.52510/1/12 110 80.3-13010/1/12 CQC

12J0298-BS1 25.72510/8/12 103 80.3-13010/8/12

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%R In BS/BSDDibromofluoromethaneLimits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

12J0298-BSD1 26.42510/8/12 106 80.3-13010/8/12

12J0389-BS1 24.92510/10/12 100 80.3-13010/10/12

12J0389-BSD1 24.72510/10/12 99 80.3-13010/10/12

12J0445-BS1 25.52510/11/12 102 80.3-13010/11/12 CQC

12J0445-BSD1 24.92510/11/12 100 80.3-13010/11/12 CQC

12J0620-BS1 25.12510/16/12 100 80.3-13010/16/12 CQC

12J0620-BSD1 25.82510/16/12 103 80.3-13010/16/12 CQC

12J0736-BS1 26.52510/18/12 106 80.3-13010/18/12 CQC

12J0736-BSD1 24.82510/18/12 99 80.3-13010/18/12 CQC

12J0821-BS1 252510/20/12 100 80.3-13010/20/12 CQC

12J0821-BSD1 25.72510/20/12 103 80.3-13010/20/12 CQC

12J0850-BS1 26.42510/22/12 106 80.3-13010/22/12 CQC

12J0850-BSD1 26.32510/22/12 105 80.3-13010/22/12 CQC

12J0972-BS1 27.22510/24/12 109 80.3-13010/24/12 CQC

12J0972-BSD1 26.72510/24/12 107 80.3-13010/24/12 CQC

12J1010-BS1 27.52510/25/12 110 80.3-13010/25/12 CQC

12J1010-BSD1 26.42510/25/12 105 80.3-13010/25/12 CQC

12J1038-BS1 26.72510/25/12 107 80.3-13010/25/12 CQC

12J1038-BSD1 272510/25/12 108 80.3-13010/25/12 CQC

12J1059-BS1 28.32510/26/12 113 80.3-13010/26/12 CQC

12J1059-BSD1 28.12510/26/12 112 80.3-13010/26/12 CQC

12K0235-BS1 24.92511/7/12 100 80.3-13011/7/12 CQC

12K0235-BSD1 24.92511/7/12 100 80.3-13011/7/12 CQC

12K0286-BS1 24.22511/8/12 97 80.3-13011/8/12 CQC

12K0286-BSD1 23.62511/8/12 94 80.3-13011/8/12 CQC

12K0341-BSD1 21.72511/9/12 87 80.3-13011/9/12

12K0341-BS1 22.42511/9/12 90 80.3-13011/9/12

12K0415-BS1 30.12511/12/12 120 80.3-13011/12/12 CQC

12K0415-BSD1 29.82511/12/12 119 80.3-13011/12/12 CQC

12K0462-BS1 29.92511/13/12 120 80.3-13011/13/12 CQC

12K0462-BSD1 29.52511/13/12 118 80.3-13011/13/12 CQC

12K0522-BS1 28.12511/14/12 112 80.3-13011/14/12 CQC

12K0522-BSD1 28.72511/14/12 115 80.3-13011/14/12 CQC

12K0553-BS1 28.82511/14/12 115 80.3-13011/14/12 CQC

12K0552-BS1 302511/14/12 120 80.3-13011/14/12 CQC

12K0553-BSD1 28.12511/14/12 112 80.3-13011/14/12 CQC

12K0552-BSD1 302511/14/12 120 80.3-13011/14/12 CQC

12K0581-BS1 29.12511/15/12 116 80.3-13011/15/12 CQC

12K0581-BSD1 28.32511/15/12 113 80.3-13011/15/12 CQC

12K0740-BS1 28.12511/20/12 112 80.3-13011/20/12 CQC

12K0751-BS1 31.22511/20/12 125 80.3-13011/20/12 CQC

12K0740-BSD1 27.92511/20/12 112 80.3-13011/20/12 CQC

12K0751-BSD1 29.12511/20/12 116 80.3-13011/20/12 CQC

12K0789-BS1 29.32511/20/12 117 80.3-13011/20/12

12K0789-BSD1 29.42511/20/12 117 80.3-13011/20/12

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%R In BS/BSDDibromofluoromethaneLimits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

12K0803-BS1 28.62511/21/12 114 80.3-13011/21/12 CQC

12K0803-BSD1 29.62511/21/12 118 80.3-13011/21/12 CQC

12K0836-BS1 302511/21/12 120 80.3-13011/21/12 CQC

12K0836-BSD1 29.42511/21/12 117 80.3-13011/21/12 CQC

12K0855-BS1 28.32511/23/12 113 80.3-13011/23/12 CQC

12K0865-BS1 30.22511/23/12 121 80.3-13011/23/12 CQC

12K0865-BSD1 30.72511/23/12 123 80.3-13011/23/12 CQC

12K0855-BSD1 28.92511/23/12 116 80.3-13011/23/12 CQC

12K0897-BS1 28.62511/24/12 114 80.3-13011/24/12 CQC

12K0897-BSD1 27.82511/24/12 111 80.3-13011/24/12 CQC

12K0905-BS1 27.62511/25/12 110 80.3-13011/25/12 CQC

12K0905-BSD1 27.92511/25/12 112 80.3-13011/25/12 CQC

12K1134-BS1 29.62511/30/12 118 80.3-13011/30/12 CQC

12K1134-BSD1 29.12511/30/12 117 80.3-13011/30/12 CQC

12K1135-BS1 29.92511/30/12 120 80.3-13011/30/12 CQC

12K1135-BSD1 28.12511/30/12 112 80.3-13011/30/12 CQC

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%R in MS/MSDDibromofluoromethane


10526.2259/1/1212I0005-MS1 CQC80.3-130PVH2309-029/1/12

11027.4259/1/1212I0005-MSD1X CQC80.3-130PVH2309-029/1/12

10425.9259/4/1212I0028-MS1 CQC80.3-130PVH2309-119/4/12

10225.6259/4/1212I0028-MSD1X CQC80.3-130PVH2309-119/4/12

10426259/5/1212I0081-MS1 CQC80.3-130PVH2037-079/5/12

10626.5259/5/1212I0081-MSD1X CQC80.3-130PVH2037-079/5/12

11127.7259/7/1212I0215-MS1 CQC80.3-130PVI0290-039/7/12

10726.6259/7/1212I0215-MSD1X CQC80.3-130PVI0290-039/7/12

10325.8259/12/1212I0352-MS1 CQC80.3-130PVI0609-099/12/12

10626.5259/12/1212I0352-MSD1X CQC80.3-130PVI0609-099/12/12

10626.5259/12/1212I0394-MS1 CQC80.3-130PVI0525-069/12/12

10726.8259/12/1212I0394-MSD1X CQC80.3-130PVI0525-069/12/12

10927.1259/18/1212I0598-MS1 CQC80.3-130PVI0894-069/18/12

10726.7259/18/1212I0598-MSD1X CQC80.3-130PVI0894-069/18/12

9924.8259/18/1212I0648-MS1 CQC80.3-130PVI1060-029/18/12

9724.2259/18/1212I0648-MSD1X CQC80.3-130PVI1060-029/18/12

10325.9259/25/1212I0925-MS1 CQC80.3-130PVI1553-089/25/12

10225.5259/25/1212I0925-MSD1X CQC80.3-130PVI1553-089/25/12

10125.2259/25/1212I0926-MS1 CQC80.3-130PVI1510-089/25/12

10325.7259/25/1212I0926-MSD1X CQC80.3-130PVI1510-089/25/12

11528.8259/28/1212I1065-MS1 CQC80.3-130PVI1723-039/28/12

11628.9259/28/1212I1065-MSD1X CQC80.3-130PVI1723-039/28/12

11729.2259/28/1212I1095-MS1 CQC80.3-130PVI1822-029/28/12

12330.8259/28/1212I1095-MSD1X CQC80.3-130PVI1822-029/28/12

12230.5259/29/1212I1107-MS1 CQC80.3-130PVI1869-059/29/12

12130.2259/29/1212I1107-MSD1X CQC80.3-130PVI1869-059/29/12

12230.42510/1/1212J0008-MS1 CQC80.3-130PVI1575-0110/1/12

11929.82510/1/1212J0008-MSD1X CQC80.3-130PVI1575-0110/1/12

11027.52510/8/1212J0298-MS1 80.3-130PVJ0513-0310/8/12

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%R in MS/MSDDibromofluoromethaneSource QualifiersLimitsSample ID Prepared Spike Level Result %RRjct Analyzed

11127.82510/8/1212J0298-MSD1X 80.3-130PVJ0513-0310/8/12

10225.52510/10/1212J0389-MS1 80.3-130PVJ0682-0110/10/12

10125.22510/10/1212J0389-MSD1X 80.3-130PVJ0682-0110/10/12

9824.42510/11/1212J0445-MS1 CQC80.3-130PVJ0682-1710/11/12

96242510/11/1212J0445-MSD1X CQC80.3-130PVJ0682-1710/11/12

10425.92510/16/1212J0620-MS1 CQC80.3-130PVJ1065-0210/16/12

10526.32510/16/1212J0620-MSD1X CQC80.3-130PVJ1065-0210/16/12

100252510/18/1212J0736-MS1 CQC80.3-130PVJ1237-0210/18/12

10526.22510/18/1212J0736-MSD1X CQC80.3-130PVJ1237-0210/18/12

10726.72510/20/1212J0821-MS1 CQC80.3-130PVJ1405-0210/20/12

10526.32510/20/1212J0821-MSD1X CQC80.3-130PVJ1405-0210/20/12

108272510/22/1212J0850-MS1 CQC80.3-130PVJ1405-1710/22/12

10626.62510/22/1212J0850-MSD1X CQC80.3-130PVJ1405-1710/22/12

10425.92510/24/1212J0972-MS1 CQC80.3-130PVJ1577-0210/24/12

10726.82510/24/1212J0972-MSD1X CQC80.3-130PVJ1577-0210/24/12

104262510/25/1212J1010-MS1 CQC80.3-130PVJ1627-0110/25/12

108272510/25/1212J1010-MSD1X CQC80.3-130PVJ1627-0110/25/12

11127.72510/25/1212J1038-MS1 CQC80.3-130PVJ1600-0210/25/12

11027.62510/25/1212J1038-MSD1X CQC80.3-130PVJ1600-0210/25/12

11829.52510/26/1212J1059-MS1 CQC80.3-130PVJ1577-18RE110/26/12

11428.62510/26/1212J1059-MSD1X CQC80.3-130PVJ1577-18RE110/26/12

10726.72511/7/1212K0235-MS1 CQC80.3-130PVK0237-0111/7/12

10325.62511/7/1212K0235-MSD1X CQC80.3-130PVK0237-0111/7/12

10325.82511/8/1212K0286-MS1 CQC80.3-130PVK0555-0411/8/12

9924.72511/8/1212K0286-MSD1X CQC80.3-130PVK0555-0411/8/12

9122.62511/9/1212K0341-MS1 80.3-130PVK0649-0611/9/12

8922.32511/9/1212K0341-MSD1X 80.3-130PVK0649-0611/9/12

11629.12511/12/1212K0415-MS1 CQC80.3-130PVK0756-0111/12/12

11829.52511/12/1212K0415-MSD1X CQC80.3-130PVK0756-0111/12/12

12531.32511/13/1212K0462-MS1 CQC80.3-130PVK0793-0211/13/12

12330.62511/13/1212K0462-MSD1X CQC80.3-130PVK0793-0211/13/12

11428.62511/14/1212K0522-MS1X CQC80.3-130PVK0281-0111/14/12

11729.22511/14/1212K0522-MSD1X CQC80.3-130PVK0281-0111/14/12

116292511/14/1212K0553-MS1 CQC80.3-130PVK0632-0911/14/12

12330.82511/14/1212K0552-MS1 CQC80.3-130PVK0684-0211/14/12

11127.82511/14/1212K0553-MSD1X CQC80.3-130PVK0632-0911/14/12

13233.12511/14/1212K0552-MSD1X CQC,Z180.3-130PVK0684-0211/14/12

12230.42511/15/1212K0581-MS1 CQC80.3-130PVK0696-0111/15/12

11629.12511/15/1212K0581-MSD1X CQC80.3-130PVK0696-0111/15/12

11629.12511/20/1212K0740-MS1 CQC80.3-130PVK0934-0111/20/12

116292511/20/1212K0740-MSD1X CQC80.3-130PVK0934-0111/20/12

12731.92511/20/1212K0751-MS1 CQC80.3-130PVK0768-0211/20/12

12330.62511/20/1212K0751-MSD1X CQC80.3-130PVK0768-0211/20/12

12631.42511/21/1212K0803-MS1X CQC80.3-130PVK1220-0211/21/12

11629.12511/21/1212K0803-MSD1X CQC80.3-130PVK1220-0211/21/12

01/02/13 15:46

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%R in MS/MSDDibromofluoromethaneSource QualifiersLimitsSample ID Prepared Spike Level Result %RRjct Analyzed

11929.92511/21/1212K0836-MS1 CQC80.3-130PVK1288-0311/21/12

12330.82511/21/1212K0836-MSD1X CQC80.3-130PVK1288-0311/21/12

12330.62511/23/1212K0865-MS1 CQC80.3-130PVK1375-0811/23/12

12731.72511/23/1212K0865-MSD1X CQC80.3-130PVK1375-0811/23/12

11127.92511/23/1212K0855-MS1 CQC80.3-130PVK1375-0211/23/12

11829.52511/23/1212K0855-MSD1X CQC80.3-130PVK1375-0211/23/12

11729.32511/24/1212K0897-MS1 CQC80.3-130PVK0988-0311/24/12

12430.92511/24/1212K0897-MSD1X CQC80.3-130PVK0988-0311/24/12

11829.42511/25/1212K0905-MS1 CQC80.3-130PVK1006-0111/25/12

11829.52511/25/1212K0905-MSD1X CQC80.3-130PVK1006-0111/25/12

12631.42511/30/1212K1135-MS1 CQC80.3-130PVK1450-1011/30/12

12731.62511/30/1212K1135-MSD1X CQC80.3-130PVK1450-1011/30/12

11528.72511/30/1212K1134-MS1 CQC80.3-130PVK1450-0312/1/12

11328.32511/30/1212K1134-MSD1X CQC80.3-130PVK1450-0312/1/12

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%R in SamplesDibromofluoromethane


PVH2309-01 27.1259/1/12 108 80.3-1309/1/12 CQC,PGA

PVH2309-02 26.6259/1/12 106 80.3-1309/1/12 CQC,PGA

PVH2309-03 26259/1/12 104 80.3-1309/1/12 CQC,PGA

PVH2309-04 27.4259/1/12 110 80.3-1309/1/12 CQC,PGA

PVH2309-05 27.8259/1/12 111 80.3-1309/1/12 CQC,PGA

PVH2309-06 25.9259/1/12 104 80.3-1309/1/12 CQC,PGA

PVH2309-07 27259/1/12 108 80.3-1309/1/12 CQC,PGA

PVH2309-08 25.9259/1/12 104 80.3-1309/1/12 CQC,PGA

PVH2309-09 26259/1/12 104 80.3-1309/1/12 CQC,PGA

PVH2309-10 24.6259/4/12 99 80.3-1309/4/12 CQC,PGA

PVH2309-11 24.9259/4/12 100 80.3-1309/4/12 CQC,PGA

PVH2309-12 26.4259/4/12 106 80.3-1309/4/12 CQC,PGA

PVH2309-13 24.6259/4/12 99 80.3-1309/4/12 CQC,PGA

PVH2309-14 24259/4/12 96 80.3-1309/4/12 CQC,PGA

PVH2318-01 25259/4/12 100 80.3-1309/4/12 CQC,PGA

PVH2318-02 24.2259/4/12 97 80.3-1309/4/12 CQC,PGA

PVH2318-03 25.1259/4/12 100 80.3-1309/4/12 CQC,PGA

PVH2309-12RE1 24.7259/5/12 99 80.3-1309/5/12 CQC,PGA

PVH2309-13RE1 25.2259/5/12 101 80.3-1309/5/12 CQC,PGA

PVH2037-07 9/5/12 80.3-1309/5/12

PVI0290-01 24.8259/7/12 99 80.3-1309/7/12 CQC,PGA

PVI0290-06 24.8259/7/12 99 80.3-1309/7/12 CQC,PGA

PVI0290-02 25.4259/7/12 101 80.3-1309/7/12 CQC,PGA

PVI0290-03 24.9259/7/12 100 80.3-1309/7/12 CQC,PGA

PVI0290-04 25.1259/7/12 100 80.3-1309/7/12 CQC,PGA

PVI0290-05 25.1259/7/12 100 80.3-1309/7/12 CQC,PGA

PVI0609-08 25.5259/12/12 102 80.3-1309/12/12 CQC,PGA

PVI0609-01 25.8259/12/12 103 80.3-1309/12/12 CQC,PGA

PVI0609-02 26.1259/12/12 104 80.3-1309/12/12 CQC,PGA

01/02/13 15:46

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%R in SamplesDibromofluoromethaneLimits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

PVI0609-03 26.2259/12/12 105 80.3-1309/12/12 CQC,PGA

PVI0609-04 25.6259/12/12 102 80.3-1309/12/12 CQC,PGA

PVI0609-09 27.5259/12/12 110 80.3-1309/12/12 CQC,PGA

PVI0609-10 26.4259/12/12 106 80.3-1309/12/12 CQC,PGA

PVI0609-11 26.5259/12/12 106 80.3-1309/12/12 CQC,PGA

PVI0609-12 25.7259/12/12 103 80.3-1309/12/12 CQC,PGA

PVI0609-13 27.2259/12/12 109 80.3-1309/12/12 CQC,PGA

PVI0609-14 26.4259/12/12 106 80.3-1309/12/12 CQC,PGA

PVI0609-15 26.8259/12/12 107 80.3-1309/12/12 CQC,PGA

PVI0609-16 26.6259/12/12 107 80.3-1309/12/12 CQC,PGA

PVI0609-17 27259/12/12 108 80.3-1309/12/12 CQC,PGA

PVI0609-18 26259/12/12 104 80.3-1309/12/12 CQC,PGA

PVI0525-06 9/12/12 80.3-1309/12/12 CQC,PGA

PVI0609-19 27.6259/12/12 110 80.3-1309/13/12 CQC,PGA

PVI0609-20 26.8259/12/12 107 80.3-1309/13/12 CQC,PGA

PVI0609-21 26.7259/12/12 107 80.3-1309/13/12 CQC,PGA

PVI1059-01 26.4259/18/12 106 80.3-1309/18/12 CQC,PGA

PVI1059-02 26.8259/18/12 107 80.3-1309/18/12 CQC,PGA

PVI1059-03 26.6259/18/12 107 80.3-1309/18/12 CQC,PGA

PVI0894-06 9/18/12 80.3-1309/18/12

PVI1060-01 26259/18/12 104 80.3-1309/18/12 CQC,PGA

PVI1060-03 26.6259/18/12 107 80.3-1309/18/12 CQC,PGA

PVI1060-04 27.3259/18/12 109 80.3-1309/18/12 CQC,PGA

PVI1060-05 27.8259/18/12 111 80.3-1309/18/12 CQC,PGA

PVI1060-06 26.7259/18/12 107 80.3-1309/18/12 CQC,PGA

PVI1060-02 24.4259/18/12 98 80.3-1309/18/12 CQC,PGA

PVI1060-07 25.1259/18/12 100 80.3-1309/18/12 CQC,PGA

PVI1060-08 24.4259/18/12 98 80.3-1309/18/12 CQC,PGA

PVI1060-09 24.8259/18/12 99 80.3-1309/18/12 CQC,PGA

PVI1553-01 25.1259/25/12 100 80.3-1309/25/12 CQC,PGA

PVI1510-08 9/25/12 80.3-1309/25/12 CQC,PGA

PVI1553-02 26.1259/25/12 104 80.3-1309/25/12 CQC,PGA

PVI1553-03 25.1259/25/12 100 80.3-1309/25/12 CQC,PGA

PVI1554-02 23.9259/25/12 96 80.3-1309/25/12 CQC,PGA

PVI1553-04 25.8259/25/12 103 80.3-1309/25/12 CQC,PGA

PVI1554-03 24.3259/25/12 97 80.3-1309/25/12 CQC,PGA

PVI1553-05 24.2259/25/12 97 80.3-1309/25/12 CQC,PGA

PVI1553-06 25.8259/25/12 103 80.3-1309/25/12 CQC,PGA

PVI1553-07 24.6259/25/12 98 80.3-1309/25/12 CQC,PGA

PVI1553-08 25259/25/12 100 80.3-1309/26/12 CQC,PGA

PVI1553-09 25.4259/25/12 102 80.3-1309/26/12 CQC,PGA

PVI1553-10 25.3259/25/12 101 80.3-1309/26/12 CQC,PGA

PVI1553-11 26.2259/25/12 105 80.3-1309/26/12 CQC,PGA

PVI1553-12 26.3259/25/12 105 80.3-1309/26/12 CQC,PGA

PVI1553-13 25.7259/25/12 103 80.3-1309/26/12 CQC,PGA

01/02/13 15:46

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PVI1553-14 24.7259/25/12 99 80.3-1309/26/12 CQC,PGA

PVI1553-15 26.2259/25/12 105 80.3-1309/26/12 CQC,PGA

PVI1554-01 27259/25/12 108 80.3-1309/26/12 CQC,PGA

PVI1723-01 27.5259/28/12 110 80.3-1309/28/12 CQC,PGA

PVI1723-02 27259/28/12 108 80.3-1309/28/12 CQC,PGA

PVI1723-03 27.6259/28/12 111 80.3-1309/28/12 CQC,PGA

PVI1723-04 27.6259/28/12 110 80.3-1309/28/12 CQC,PGA

PVI1723-05 27.5259/28/12 110 80.3-1309/28/12 CQC,PGA

PVI1723-06 28.1259/28/12 112 80.3-1309/28/12 CQC,PGA

PVI1723-07 28.9259/28/12 115 80.3-1309/28/12 CQC,PGA

PVI1723-08 28.3259/28/12 113 80.3-1309/28/12 CQC,PGA

PVI1723-09 28.6259/28/12 114 80.3-1309/28/12 CQC,PGA

PVI1723-10 28.7259/28/12 115 80.3-1309/28/12 CQC,PGA

PVI1723-11 28.2259/28/12 113 80.3-1309/28/12 CQC,PGA

PVI1723-12 28.4259/28/12 114 80.3-1309/28/12 CQC,PGA

PVI1822-01 28.1259/28/12 112 80.3-1309/28/12 CQC,PGA

PVI1822-02 29.2259/28/12 117 80.3-1309/28/12 CQC,PGA

PVI1822-03 29259/28/12 116 80.3-1309/28/12 CQC,PGA

PVI1822-04 30.3259/28/12 121 80.3-1309/28/12 CQC,PGA

PVI1822-05 29.4259/28/12 118 80.3-1309/28/12 CQC,PGA

PVI1822-06 29.4259/28/12 118 80.3-1309/28/12 CQC,PGA

PVI1822-07 29.9259/28/12 120 80.3-1309/28/12 CQC,PGA

PVI1822-08 30.2259/28/12 121 80.3-1309/28/12 CQC,PGA

PVI1822-09 29.4259/28/12 118 80.3-1309/28/12 CQC,PGA

PVI1822-10 29.2259/28/12 117 80.3-1309/29/12 CQC,PGA

PVI1822-11 30.1259/28/12 121 80.3-1309/29/12 CQC,PGA

PVI1822-12 30259/28/12 120 80.3-1309/29/12 CQC,PGA

PVI1822-13 31.4259/28/12 126 80.3-1309/29/12 CQC,PGA

PVI1822-14 30.2259/28/12 121 80.3-1309/29/12 CQC,PGA

PVI1822-15 24.5259/28/12 98 80.3-1309/29/12 CQC,PGA

PVI1870-01 28.8259/28/12 115 80.3-1309/29/12 CQC,PGA

PVI1870-02 30.2259/28/12 121 80.3-1309/29/12 CQC,PGA

PVI1869-01 28.2259/29/12 113 80.3-1309/29/12 CQC,PGA

PVI1869-02 28.9259/29/12 116 80.3-1309/29/12 CQC,PGA

PVI1869-03 29.5259/29/12 118 80.3-1309/29/12 CQC,PGA

PVI1869-04 28.9259/29/12 116 80.3-1309/29/12 CQC,PGA

PVI1869-05 29259/29/12 116 80.3-1309/29/12 CQC,PGA

PVI1869-06 27.6259/29/12 110 80.3-1309/29/12 CQC,PGA

PVI1869-07 29259/29/12 116 80.3-1309/29/12 CQC,PGA

PVI1869-08 30259/29/12 120 80.3-1309/29/12 CQC,PGA

PVI1869-09 32.4259/29/12 129 80.3-1309/29/12 CQC,PGA

PVI1869-10 30259/29/12 120 80.3-1309/29/12 CQC,PGA

PVI1869-11 29.7259/29/12 119 80.3-1309/29/12 CQC,PGA

PVI1869-12 29.8259/29/12 119 80.3-1309/29/12 CQC,PGA

PVI1869-13 30.7259/29/12 123 80.3-1309/29/12 CQC,PGA

01/02/13 15:46

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PVI1869-14 30.8259/29/12 123 80.3-1309/29/12 CQC,PGA

PVI1869-15 30.4259/29/12 121 80.3-1309/29/12 CQC,PGA

PVI1869-16 31259/29/12 124 80.3-1309/29/12 CQC,PGA

PVI1869-17 30259/29/12 120 80.3-1309/29/12 CQC,PGA

PVI1822-15RE1 27.92510/1/12 112 80.3-13010/1/12 CQC,PGA

PVI1869-03RE1 26.82510/1/12 107 80.3-13010/1/12 CQC,PGA

PVI1869-16RE1 28.42510/1/12 113 80.3-13010/1/12 CQC,PGA

PVI1869-17RE1 28.52510/1/12 114 80.3-13010/1/12 CQC,PGA

PVI1869-18 29.42510/1/12 118 80.3-13010/1/12 CQC,PGA

PVI1869-19 29.82510/1/12 119 80.3-13010/1/12 CQC,PGA

PVI1575-01 10/1/12 80.3-13010/1/12 CQC,PGA

PVJ0513-01 26.22510/8/12 105 80.3-13010/8/12 CQC,PGA

PVJ0513-02 26.62510/8/12 107 80.3-13010/8/12 CQC,PGA

PVJ0513-03 26.62510/8/12 107 80.3-13010/8/12 CQC,PGA

PVJ0513-04 27.12510/8/12 108 80.3-13010/8/12 CQC,PGA

PVJ0513-05 27.22510/8/12 109 80.3-13010/8/12 CQC,PGA

PVJ0513-06 26.42510/8/12 106 80.3-13010/8/12 CQC,PGA

PVJ0513-07 27.22510/8/12 109 80.3-13010/8/12 CQC,PGA

PVJ0513-08 25.82510/8/12 103 80.3-13010/8/12 CQC,PGA

PVJ0513-09 26.72510/8/12 107 80.3-13010/8/12 CQC,PGA

PVJ0513-10 27.82510/8/12 111 80.3-13010/8/12 CQC,PGA

PVJ0513-11 26.52510/8/12 106 80.3-13010/8/12 CQC,PGA

PVJ0513-12 262510/8/12 104 80.3-13010/8/12 CQC,PGA

PVJ0513-13 26.72510/8/12 107 80.3-13010/8/12 CQC,PGA

PVJ0513-14 27.52510/8/12 110 80.3-13010/8/12 CQC,PGA

PVJ0513-15 27.22510/8/12 109 80.3-13010/8/12 CQC,PGA

PVJ0682-01 25.82510/10/12 103 80.3-13010/10/12 CQC,PGA

PVJ0682-02 262510/10/12 104 80.3-13010/10/12 CQC,PGA

PVJ0682-03 27.22510/10/12 109 80.3-13010/10/12 CQC,PGA

PVJ0682-04 25.82510/10/12 103 80.3-13010/10/12 CQC,PGA

PVJ0682-05 26.32510/10/12 105 80.3-13010/10/12 CQC,PGA

PVJ0682-06 262510/10/12 104 80.3-13010/10/12 CQC,PGA

PVJ0682-07 26.72510/10/12 107 80.3-13010/10/12 CQC,PGA

PVJ0682-08 25.82510/10/12 103 80.3-13010/10/12 CQC,PGA

PVJ0682-09 26.92510/10/12 108 80.3-13010/10/12 CQC,PGA

PVJ0682-10 27.42510/10/12 110 80.3-13010/10/12 CQC,PGA

PVJ0682-11 27.42510/10/12 110 80.3-13010/10/12 CQC,PGA

PVJ0682-12 26.22510/10/12 105 80.3-13010/10/12 CQC,PGA

PVJ0682-13 27.42510/10/12 110 80.3-13010/10/12 CQC,PGA

PVJ0682-14 26.92510/10/12 108 80.3-13010/10/12 CQC,PGA

PVJ0682-15 26.82510/10/12 107 80.3-13010/10/12 CQC,PGA

PVJ0682-16 25.22510/10/12 101 80.3-13010/10/12 CQC,PGA

PVJ0682-17 23.62510/11/12 95 80.3-13010/11/12 CQC,PGA

PVJ0682-21 252510/11/12 100 80.3-13010/11/12 CQC,PGA

PVJ1065-01 262510/16/12 104 80.3-13010/16/12 CQC,PGA

01/02/13 15:46

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PVJ1065-02 26.62510/16/12 106 80.3-13010/16/12 CQC,PGA

PVJ1065-03 26.22510/16/12 105 80.3-13010/16/12 CQC,PGA

PVJ1065-04 25.52510/16/12 102 80.3-13010/16/12 CQC,PGA

PVJ1065-05 26.82510/16/12 107 80.3-13010/16/12 CQC,PGA

PVJ1065-06 27.22510/16/12 109 80.3-13010/16/12 CQC,PGA

PVJ1065-07 27.62510/16/12 110 80.3-13010/16/12 CQC,PGA

PVJ1065-08 272510/16/12 108 80.3-13010/16/12 CQC,PGA

PVJ1065-09 27.42510/16/12 110 80.3-13010/16/12 CQC,PGA

PVJ1065-10 272510/16/12 108 80.3-13010/16/12 CQC,PGA

PVJ1237-01 252510/18/12 100 80.3-13010/18/12 CQC,PGA

PVJ1237-02 25.42510/18/12 102 80.3-13010/18/12 CQC,PGA

PVJ1237-03 25.52510/18/12 102 80.3-13010/18/12 CQC,PGA

PVJ1237-04 25.42510/18/12 102 80.3-13010/18/12 CQC,PGA

PVJ1237-05 24.82510/18/12 99 80.3-13010/18/12 CQC,PGA

PVJ1237-06 25.12510/18/12 100 80.3-13010/18/12 CQC,PGA

PVJ1237-07 25.52510/18/12 102 80.3-13010/18/12 CQC,PGA

PVJ1237-08 25.22510/18/12 101 80.3-13010/18/12 CQC,PGA

PVJ1237-09 24.62510/18/12 99 80.3-13010/18/12 CQC,PGA

PVJ1237-10 25.72510/18/12 103 80.3-13010/18/12 CQC,PGA

PVJ1237-11 25.72510/18/12 103 80.3-13010/18/12 CQC,PGA

PVJ1237-12 24.92510/18/12 100 80.3-13010/18/12 CQC,PGA

PVJ1237-13 24.62510/18/12 99 80.3-13010/18/12 CQC,PGA

PVJ1237-14 24.92510/18/12 100 80.3-13010/18/12 CQC,PGA

PVJ1405-01 25.92510/20/12 104 80.3-13010/20/12 CQC,PGA

PVJ1405-02 26.42510/20/12 106 80.3-13010/20/12 CQC,PGA

PVJ1405-03 25.52510/20/12 102 80.3-13010/20/12 CQC,PGA

PVJ1405-04 26.52510/20/12 106 80.3-13010/20/12 CQC,PGA

PVJ1405-05 26.62510/20/12 107 80.3-13010/20/12 CQC,PGA

PVJ1405-06 26.42510/20/12 106 80.3-13010/20/12 CQC,PGA

PVJ1405-07 26.62510/20/12 106 80.3-13010/20/12 CQC,PGA

PVJ1405-08 27.32510/20/12 109 80.3-13010/20/12 CQC,PGA

PVJ1405-09 26.62510/20/12 107 80.3-13010/20/12 CQC,PGA

PVJ1405-10 26.42510/20/12 106 80.3-13010/20/12 CQC,PGA

PVJ1405-11 25.82510/20/12 103 80.3-13010/20/12 CQC,PGA

PVJ1405-12 26.72510/20/12 107 80.3-13010/20/12 CQC,PGA

PVJ1405-13 26.42510/20/12 106 80.3-13010/20/12 CQC,PGA

PVJ1405-14 26.62510/20/12 106 80.3-13010/20/12 CQC,PGA

PVJ1405-15 27.52510/20/12 110 80.3-13010/20/12 CQC,PGA

PVJ1405-16 27.52510/20/12 110 80.3-13010/20/12 CQC,PGA

PVJ1405-17 272510/22/12 108 80.3-13010/22/12 CQC,PGA

PVJ1405-18 26.92510/22/12 108 80.3-13010/22/12 CQC,PGA

PVJ1577-01 272510/24/12 108 80.3-13010/24/12 CQC,PGA

PVJ1577-02 28.22510/24/12 113 80.3-13010/24/12 CQC,PGA

PVJ1577-03 26.62510/24/12 107 80.3-13010/24/12 CQC,PGA

PVJ1577-04 26.62510/24/12 106 80.3-13010/24/12 CQC,PGA

01/02/13 15:46

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8260 (PGA), 8260 (PGA) Short

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PVJ1577-05 26.52510/24/12 106 80.3-13010/24/12 CQC,PGA

PVJ1577-06 28.52510/24/12 114 80.3-13010/24/12 CQC,PGA

PVJ1577-07 27.42510/24/12 110 80.3-13010/25/12 CQC,PGA

PVJ1577-08 262510/24/12 104 80.3-13010/25/12 CQC,PGA

PVJ1577-09 27.22510/24/12 109 80.3-13010/25/12 CQC,PGA

PVJ1577-10 26.92510/24/12 108 80.3-13010/25/12 CQC,PGA

PVJ1577-11 27.62510/24/12 110 80.3-13010/25/12 CQC,PGA

PVJ1577-12 26.12510/24/12 104 80.3-13010/25/12 CQC,PGA

PVJ1577-13 272510/24/12 108 80.3-13010/25/12 CQC,PGA

PVJ1577-14 02510/24/12 80.3-13010/25/12

PVJ1575-01 02510/24/12 80.3-13010/25/12

PVJ1575-01RE1 272510/24/12 108 80.3-13010/25/12 CQC,PGA

PVJ1577-14RE1 28.12510/24/12 112 80.3-13010/25/12 CQC,PGA

PVJ1627-01 10/25/12 80.3-13010/25/12 CQC,PGA

PVJ1575-02 27.92510/25/12 111 80.3-13010/25/12 CQC,PGA

PVJ1577-15 292510/25/12 116 80.3-13010/25/12 CQC,PGA

PVJ1577-16 28.12510/25/12 112 80.3-13010/25/12 CQC,PGA

PVJ1577-17 28.62510/25/12 114 80.3-13010/25/12 CQC,PGA

PVJ1577-18 28.32510/25/12 113 80.3-13010/25/12 CQC,PGA

PVJ1600-02 10/25/12 80.3-13010/25/12 CQC,PGA

PVJ1577-19 26.42510/25/12 105 80.3-13010/25/12 CQC,PGA

PVJ1577-19RE1 28.62510/26/12 115 80.3-13010/26/12 CQC,PGA

PVJ1577-18RE1 29.82510/26/12 119 80.3-13010/26/12 CQC,PGA

PVK0411-02 26.12511/7/12 105 80.3-13011/7/12 CQC,PGA

PVK0411-03 26.62511/7/12 106 80.3-13011/7/12 CQC,PGA

PVK0237-01 11/7/12 80.3-13011/7/12

PVK0555-02 252511/8/12 100 80.3-13011/8/12 CQC,PGA

PVK0555-01 25.12511/8/12 100 80.3-13011/8/12 CQC,PGA

PVK0555-03 26.32511/8/12 105 80.3-13011/8/12 CQC,PGA

PVK0555-04 25.42511/8/12 102 80.3-13011/8/12 CQC,PGA

PVK0555-05 26.42511/8/12 106 80.3-13011/8/12 CQC,PGA

PVK0649-03 21.62511/9/12 86 80.3-13011/9/12

PVK0649-04 22.22511/9/12 89 80.3-13011/9/12

PVK0649-05 22.62511/9/12 90 80.3-13011/9/12

PVK0649-06 22.92511/9/12 91 80.3-13011/9/12

PVK0756-03 29.72511/12/12 119 80.3-13011/12/12 CQC,PGA

PVK0756-01 29.82511/12/12 119 80.3-13011/12/12 CQC,PGA

PVK0756-02 28.82511/12/12 115 80.3-13011/12/12 CQC,PGA

PVK0756-04 29.32511/12/12 117 80.3-13011/12/12 CQC,PGA

PVK0756-05 302511/12/12 120 80.3-13011/12/12 CQC,PGA

PVK0411-01 30.52511/12/12 122 80.3-13011/12/12 CQC,PGA

PVK0411-02RE1 29.42511/12/12 118 80.3-13011/12/12 CQC,PGA

PVK0411-03RE1 28.62511/12/12 114 80.3-13011/12/12 CQC,N1,PGA

PVK0649-01 30.82511/12/12 123 80.3-13011/12/12 CQC,PGA

PVK0649-02 30.62511/12/12 122 80.3-13011/12/12 CQC,PGA

01/02/13 15:46

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PVK0649-03RE1 30.72511/12/12 123 80.3-13011/12/12 CQC,PGA

PVK0649-04RE1 29.92511/12/12 120 80.3-13011/12/12 CQC,PGA

PVK0649-05RE1 29.52511/12/12 118 80.3-13011/12/12 CQC,PGA

PVK0649-06RE1 29.62511/12/12 118 80.3-13011/12/12 CQC,PGA

PVK0828-02 29.92511/13/12 120 80.3-13011/13/12 CQC,PGA

PVK0828-03 28.82511/13/12 115 80.3-13011/13/12 CQC,PGA

PVK0828-05 28.62511/13/12 114 80.3-13011/13/12 CQC,PGA

PVK0793-02 11/13/12 80.3-13011/13/12 CQC,PGA

PVK0828-01 30.62511/13/12 122 80.3-13011/13/12 CQC,PGA

PVK0828-04 30.12511/13/12 120 80.3-13011/13/12 CQC,PGA

PVK0411-02RE2 29.72511/13/12 119 80.3-13011/13/12 CQC,PGA

PVK0892-03 29.62511/14/12 119 80.3-13011/14/12 CQC,PGA

PVK0281-01 11/14/12 80.3-13011/14/12

PVK0892-01 29.22511/14/12 117 80.3-13011/14/12 CQC,PGA

PVK0892-02 29.92511/14/12 120 80.3-13011/14/12 CQC,PGA

PVK0632-01 29.42511/14/12 117 80.3-13011/14/12 CQC,PGA

PVK0632-02 29.82511/14/12 119 80.3-13011/14/12 CQC,PGA

PVK0632-03 30.42511/14/12 122 80.3-13011/14/12 CQC,PGA

PVK0632-04 29.82511/14/12 119 80.3-13011/14/12 CQC,PGA

PVK0632-08 30.42511/14/12 121 80.3-13011/14/12 CQC,PGA

PVK0632-09 29.12511/14/12 117 80.3-13011/14/12 CQC,PGA

PVK0684-01 30.22511/14/12 121 80.3-13011/14/12 CQC,PGA

PVK0632-10 30.12511/14/12 120 80.3-13011/14/12 CQC,PGA

PVK0684-02 32.42511/14/12 129 80.3-13011/14/12 CQC,PGA

PVK0632-11 292511/14/12 116 80.3-13011/14/12 CQC,PGA

PVK0684-03 322511/14/12 128 80.3-13011/14/12 CQC,PGA

PVK0632-12 29.82511/14/12 119 80.3-13011/14/12 CQC,PGA

PVK0684-04 32.32511/14/12 129 80.3-13011/15/12 CQC,PGA

PVK0684-05 30.92511/14/12 124 80.3-13011/15/12 CQC,PGA

PVK0632-13 30.32511/14/12 121 80.3-13011/15/12 CQC,PGA

PVK0684-06 30.72511/14/12 123 80.3-13011/15/12 CQC,PGA

PVK0632-14 30.42511/14/12 121 80.3-13011/15/12 CQC,PGA

PVK0684-07 32.32511/14/12 129 80.3-13011/15/12 CQC,PGA

PVK0632-15 302511/14/12 120 80.3-13011/15/12 CQC,PGA

PVK0684-08 33.22511/14/12 133 80.3-13011/15/12 CQC,PGA

PVK0632-16 30.42511/14/12 122 80.3-13011/15/12 CQC,PGA

PVK0684-09 31.42511/14/12 125 80.3-13011/15/12 CQC,PGA

PVK0632-17 30.62511/14/12 123 80.3-13011/15/12 CQC,PGA

PVK0632-18 30.62511/14/12 122 80.3-13011/15/12 CQC,PGA

PVK0684-10 28.92511/15/12 116 80.3-13011/15/12 CQC,PGA

PVK0684-08RE1 29.42511/15/12 118 80.3-13011/15/12 CQC,PGA

PVK0696-01 11/15/12 80.3-13011/15/12 CQC,PGA

PVK1220-01 31.12511/20/12 124 80.3-13011/20/12 CQC,PGA

PVK0768-02 11/20/12 80.3-13011/20/12

PVK1220-03 27.82511/20/12 111 80.3-13011/20/12 CQC,PGA

01/02/13 15:46

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PVK1220-04 29.12511/20/12 116 80.3-13011/20/12 CQC,PGA

PVK0934-01 11/20/12 80.3-13011/20/12 CQC,PGA

PVK1380-01 29.12511/21/12 116 80.3-13011/21/12 CQC,PGA

PVK1380-02 29.12511/21/12 117 80.3-13011/21/12 CQC,PGA

PVK1220-02 31.22511/21/12 125 80.3-13011/21/12 CQC,PGA

PVK1220-06 302511/21/12 120 80.3-13011/21/12 CQC,PGA

PVK1220-07 29.22511/21/12 117 80.3-13011/21/12 CQC,PGA

PVK1220-08 29.22511/21/12 117 80.3-13011/21/12 CQC,PGA

PVK1220-09 292511/21/12 116 80.3-13011/21/12 CQC,PGA

PVK1220-10 30.72511/21/12 123 80.3-13011/21/12 CQC,PGA

PVK1220-11 31.92511/21/12 128 80.3-13011/21/12 CQC,PGA

PVK1220-12 292511/21/12 116 80.3-13011/21/12 CQC,PGA

PVK1220-13 31.92511/21/12 128 80.3-13011/21/12 CQC,PGA

PVK1220-14 29.82511/21/12 119 80.3-13011/21/12 CQC,PGA

PVK1288-01 292511/21/12 116 80.3-13011/21/12 CQC,PGA

PVK1288-02 29.22511/21/12 117 80.3-13011/21/12 CQC,PGA

PVK1288-03 29.82511/21/12 119 80.3-13011/21/12 CQC,PGA

PVK1288-04 28.82511/21/12 115 80.3-13011/21/12 CQC,PGA

PVK1288-05 30.22511/21/12 121 80.3-13011/21/12 CQC,PGA

PVK1288-06 28.82511/21/12 115 80.3-13011/21/12 CQC,PGA

PVK1288-07 312511/21/12 124 80.3-13011/21/12 CQC,PGA

PVK1286-01 29.32511/21/12 117 80.3-13011/22/12 CQC,PGA

PVK1286-02 28.72511/21/12 115 80.3-13011/22/12 CQC,PGA

PVK1286-03 29.62511/21/12 119 80.3-13011/22/12 CQC,PGA

PVK1286-04 31.32511/21/12 125 80.3-13011/22/12 CQC,PGA

PVK1286-05 312511/21/12 124 80.3-13011/22/12 CQC,PGA

PVK1286-06 31.52511/21/12 126 80.3-13011/22/12 CQC,PGA

PVK1220-15 28.52511/21/12 114 80.3-13011/22/12 CQC,PGA

PVK1220-17 28.32511/21/12 113 80.3-13011/22/12 CQC,PGA

PVK1220-16 30.42511/23/12 121 80.3-13011/23/12 CQC,PGA

PVK1375-08 30.22511/23/12 121 80.3-13011/23/12 CQC,PGA

PVK1375-09 31.12511/23/12 124 80.3-13011/23/12 CQC,PGA

PVK1375-01 302511/23/12 120 80.3-13011/23/12 CQC,PGA

PVK1375-10 31.92511/23/12 128 80.3-13011/23/12 CQC,PGA

PVK1375-02 29.52511/23/12 118 80.3-13011/23/12 CQC,PGA

PVK1375-11 30.12511/23/12 121 80.3-13011/23/12 CQC,PGA

PVK1375-12 31.52511/23/12 126 80.3-13011/23/12 CQC,PGA

PVK1375-13 31.52511/23/12 126 80.3-13011/23/12 CQC,PGA

PVK1375-03 29.42511/23/12 118 80.3-13011/23/12 CQC,PGA

PVK1375-14 31.32511/23/12 125 80.3-13011/23/12 CQC,PGA

PVK1375-04 30.22511/23/12 121 80.3-13011/23/12 CQC,PGA

PVK1375-15 322511/23/12 128 80.3-13011/23/12 CQC,PGA

PVK1375-05 31.22511/23/12 125 80.3-13011/23/12 CQC,PGA

PVK1375-06 29.62511/23/12 118 80.3-13011/23/12 CQC,PGA

PVK1375-07 30.22511/23/12 121 80.3-13011/23/12 CQC,PGA

01/02/13 15:46

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PVK1375-16 29.52511/24/12 118 80.3-13011/24/12 CQC,PGA

PVK0988-03 11/24/12 80.3-13011/24/12

PVK1006-01 11/24/12 80.3-13011/25/12

PVK1375-16RE1 29.72511/25/12 119 80.3-13011/26/12 CQC,PGA

PVK1450-20 30.92511/30/12 124 80.3-13011/30/12 CQC,PGA

PVK1450-10 31.22511/30/12 125 80.3-13011/30/12 CQC,PGA

PVK1450-11 32.52511/30/12 130 80.3-13011/30/12 CQC,PGA

PVK1450-12 32.12511/30/12 128 80.3-13011/30/12 CQC,PGA

PVK1450-01 27.72511/30/12 111 80.3-13011/30/12 CQC,PGA

PVK1450-13 31.22511/30/12 125 80.3-13011/30/12 CQC,PGA

PVK1450-02 29.22511/30/12 117 80.3-13011/30/12 CQC,PGA

PVK1450-14 32.92511/30/12 132 80.3-13011/30/12 CQC,PGA,Z1

PVK1450-03 282511/30/12 112 80.3-13012/1/12 CQC,PGA

PVK1450-15 32.62511/30/12 130 80.3-13012/1/12 CQC,PGA

PVK1450-16 30.62511/30/12 122 80.3-13012/1/12 CQC,PGA

PVK1450-17 332511/30/12 132 80.3-13012/1/12 CQC,PGA,Z1

PVK1450-18 31.12511/30/12 124 80.3-13012/1/12 CQC,PGA

PVK1450-04 28.52511/30/12 114 80.3-13012/1/12 CQC,PGA

PVK1450-19 322511/30/12 128 80.3-13012/1/12 CQC,PGA

PVK1450-05 28.82511/30/12 115 80.3-13012/1/12 CQC,PGA

PVK1450-06 29.92511/30/12 120 80.3-13012/1/12 CQC,PGA

PVK1450-07 28.92511/30/12 116 80.3-13012/1/12 CQC,PGA

PVK1450-08 29.62511/30/12 118 80.3-13012/1/12 CQC,PGA

PVK1450-09 30.52511/30/12 122 80.3-13012/1/12 CQC,PGA

01/02/13 15:46

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LCS %RDichlorodifluoromethane


12K0235-BS1 34.4 1382511/7/12 72.8-13011/7/12 CQC,PSL

12K0286-BS1 25.4 1022511/8/12 72.8-13011/8/12 CQC

12K0341-BS1 20.9 842511/9/12 72.8-13011/9/12

12K0415-BS1 23.1 922511/12/12 72.8-13011/12/12 CQC

12K0462-BS1 30.4 1222511/13/12 72.8-13011/13/12 CQC

12K0522-BS1 28.2 1132511/14/12 72.8-13011/14/12 CQC

12K0803-BS1 24.6 982511/21/12 72.8-13011/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPDDichlorodifluoromethane


12631.52511/7/1211/7/1212K0235-BSD1 34.4 138 9 25 CQC

9824.52511/8/1211/8/1212K0286-BSD1 25.4 102 4 25 CQC

8922.22511/9/1211/9/1212K0341-BSD1 20.9 84 6 25

9423.42511/12/1211/12/1212K0415-BSD1 23.1 92 1 25 CQC

11929.82511/13/1211/13/1212K0462-BSD1 30.4 122 2 25 CQC

112282511/14/1211/14/1212K0522-BSD1 28.2 113 0.7 25 CQC

10325.82511/21/1211/21/1212K0803-BSD1 24.6 98 5 25 CQC

01/02/13 15:46

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MS %RDichlorodifluoromethane


CQC71-138PVK0237-0113132.712K0235-MS1 11/7/12 11/7/12 25

CQC71-138PVK0555-0411227.912K0286-MS1 11/8/12 11/8/12 25

71-138PVK0649-068821.912K0341-MS1 11/9/12 11/9/12 25

CQC71-138PVK0756-0110125.312K0415-MS1 11/12/12 11/12/12 25

CQC71-138PVK0793-0212531.212K0462-MS1 11/13/12 11/13/12 25

CQC71-138PVK0281-0111328.212K0522-MS1 11/14/12 11/14/12 25

CQC71-138PVK1220-02802012K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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MS/MSD RPDDichlorodifluoromethane


13533.92511/7/1211/7/1212K0235-MSD1 CQC25413132.7 PVK0237-01

104262511/8/1211/8/1212K0286-MSD1 CQC25711227.9 PVK0555-04

8822.12511/9/1211/9/1212K0341-MSD1 250.98821.9 PVK0649-06

10125.22511/12/1211/12/1212K0415-MSD1 CQC250.410125.3 PVK0756-01

11629.12511/13/1211/13/1212K0462-MSD1 CQC25712531.2 PVK0793-02

10927.12511/14/1211/14/1212K0522-MSD1 CQC25411328.2 PVK0281-01

8521.22511/21/1211/21/1212K0803-MSD1 CQC2568020 PVK1220-02

01/02/13 15:46

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BLKDichlorodifluoromethane

01/02/13 15:46

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LCS %REthylbenzene


12I0005-BS1 26.6 106259/1/12 85-1159/1/12 CQC

12I0028-BS1 25.4 102259/4/12 85-1159/4/12 CQC

12I0081-BS1 24.9 99259/5/12 85-1159/5/12 CQC

12I0215-BS1 24.7 99259/7/12 85-1159/7/12 CQC

12I0352-BS1 25.1 100259/12/12 85-1159/12/12 CQC

12I0394-BS1 24 96259/12/12 85-1159/12/12 CQC

12I0598-BS1 26.7 107259/18/12 85-1159/18/12 CQC

12I0648-BS1 24.8 99259/18/12 85-1159/18/12 CQC

12I0926-BS1 24.3 97259/25/12 85-1159/25/12 CQC

12I0925-BS1 24.3 97259/25/12 85-1159/25/12 CQC

12I1065-BS1 24.6 99259/28/12 85-1159/28/12 CQC

12I1095-BS1 24.2 97259/28/12 85-1159/28/12 CQC

12I1107-BS1 24.6 99259/29/12 85-1159/29/12 CQC

12J0008-BS1 25.4 1022510/1/12 85-11510/1/12 CQC

12J0298-BS1 23.9 962510/8/12 85-11510/8/12

12J0389-BS1 24 962510/10/12 85-11510/10/12

12J0445-BS1 24.6 982510/11/12 85-11510/11/12 CQC

12J0620-BS1 25.5 1022510/16/12 85-11510/16/12 CQC

12J0736-BS1 24.1 962510/18/12 85-11510/18/12 CQC

12J0821-BS1 26 1042510/20/12 85-11510/20/12 CQC

12J0850-BS1 24.2 972510/22/12 85-11510/22/12 CQC

12J0972-BS1 25.9 1032510/24/12 85-11510/24/12 CQC

12J1010-BS1 26.2 1052510/25/12 85-11510/25/12 CQC

12J1038-BS1 25.5 1022510/25/12 85-11510/25/12 CQC

12J1059-BS1 27.2 1092510/26/12 85-11510/26/12 CQC

12K0235-BS1 30.5 1222511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 27.6 1112511/8/12 85-11511/8/12 CQC

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LCS %REthylbenzeneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 28 1122511/9/12 85-11511/9/12

12K0415-BS1 23.9 962511/12/12 85-11511/12/12 CQC

12K0462-BS1 27.1 1092511/13/12 85-11511/13/12 CQC

12K0522-BS1 27.4 1102511/14/12 85-11511/14/12 CQC

12K0553-BS1 27.6 1102511/14/12 85-11511/14/12 CQC

12K0552-BS1 25 1002511/14/12 85-11511/14/12 CQC

12K0581-BS1 26.2 1052511/15/12 85-11511/15/12 CQC

12K0740-BS1 26.4 1062511/20/12 85-11511/20/12 CQC

12K0751-BS1 25.7 1032511/20/12 85-11511/20/12 CQC

12K0789-BS1 28.6 1142511/20/12 85-11511/20/12

12K0803-BS1 27.4 1102511/21/12 85-11511/21/12 CQC

12K0836-BS1 26.8 1072511/21/12 85-11511/21/12 CQC

12K0855-BS1 27.8 1112511/23/12 85-11511/23/12 CQC

12K0865-BS1 25.1 1012511/23/12 85-11511/23/12 CQC

12K0897-BS1 28.8 1152511/24/12 85-11511/24/12 CQC

12K0905-BS1 30 1202511/25/12 85-11511/25/12 CQC,PSL

12K1134-BS1 24.9 1002511/30/12 85-11511/30/12 CQC

12K1135-BS1 24.6 992511/30/12 85-11511/30/12 CQC

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LCS/LCSD RPDEthylbenzene


9323.1259/1/129/1/1212I0005-BSD1 26.6 106 14 25 CQC

10626.4259/4/129/4/1212I0028-BSD1 25.4 102 4 25 CQC

9724.3259/5/129/5/1212I0081-BSD1 24.9 99 2 25 CQC

10125.2259/7/129/7/1212I0215-BSD1 24.7 99 2 25 CQC

9624259/12/129/12/1212I0352-BSD1 25.1 100 5 25 CQC

10025.1259/12/129/12/1212I0394-BSD1 24 96 4 25 CQC

10827259/18/129/18/1212I0598-BSD1 26.7 107 0.9 25 CQC

9924.8259/18/129/18/1212I0648-BSD1 24.8 99 0 25 CQC

9223259/25/129/25/1212I0926-BSD1 24.3 97 5 25 CQC

9624259/25/129/25/1212I0925-BSD1 24.3 97 2 25 CQC

10225.6259/28/129/28/1212I1065-BSD1 24.6 99 4 25 CQC

10425.9259/28/129/28/1212I1095-BSD1 24.2 97 7 25 CQC

9523.8259/29/129/29/1212I1107-BSD1 24.6 99 3 25 CQC

10626.42510/1/1210/1/1212J0008-BSD1 25.4 102 4 25 CQC

96242510/8/1210/8/1212J0298-BSD1 23.9 96 0.4 25

9523.82510/10/1210/10/1212J0389-BSD1 24 96 1 25

10125.22510/11/1210/11/1212J0445-BSD1 24.6 98 3 25 CQC

9523.82510/16/1210/16/1212J0620-BSD1 25.5 102 7 25 CQC

9824.52510/18/1210/18/1212J0736-BSD1 24.1 96 2 25 CQC

10125.22510/20/1210/20/1212J0821-BSD1 26 104 3 25 CQC

9323.32510/22/1210/22/1212J0850-BSD1 24.2 97 4 25 CQC

9523.62510/24/1210/24/1212J0972-BSD1 25.9 103 9 25 CQC

10927.32510/25/1210/25/1212J1010-BSD1 26.2 105 4 25 CQC

11127.82510/25/1210/25/1212J1038-BSD1 25.5 102 9 25 CQC

11127.82510/26/1210/26/1212J1059-BSD1 27.2 109 2 25 CQC

12731.72511/7/1211/7/1212K0235-BSD1 30.5 122 4 25 CQC,PSL

10927.22511/8/1211/8/1212K0286-BSD1 27.6 111 2 25 CQC

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LCS/LCSD RPDEthylbenzene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

11227.92511/9/1211/9/1212K0341-BSD1 28 112 0.4 25

9624.12511/12/1211/12/1212K0415-BSD1 23.9 96 0.7 25 CQC

108272511/13/1211/13/1212K0462-BSD1 27.1 109 0.5 25 CQC

11127.72511/14/1211/14/1212K0522-BSD1X 27.4 110 0.9 25 CQC

9824.62511/14/1211/14/1212K0553-BSD1 27.6 110 12 25 CQC

10225.62511/14/1211/14/1212K0552-BSD1 25 100 2 25 CQC

10125.32511/15/1211/15/1212K0581-BSD1 26.2 105 3 25 CQC

10827.12511/20/1211/20/1212K0740-BSD1 26.4 106 2 25 CQC

9924.82511/20/1211/20/1212K0751-BSD1 25.7 103 3 25 CQC

10726.92511/20/1211/20/1212K0789-BSD1 28.6 114 6 25

10626.52511/21/1211/21/1212K0803-BSD1X 27.4 110 3 25 CQC

10325.82511/21/1211/21/1212K0836-BSD1 26.8 107 4 25 CQC

11328.22511/23/1211/23/1212K0855-BSD1 27.8 111 1 25 CQC

9824.62511/23/1211/23/1212K0865-BSD1 25.1 101 2 25 CQC

11929.72511/24/1211/24/1212K0897-BSD1 28.8 115 3 25 CQC,PSL

128322511/25/1211/25/1212K0905-BSD1 30 120 6 25 CQC,PSL

10626.42511/30/1211/30/1212K1134-BSD1 24.9 100 6 25 CQC

10927.32511/30/1211/30/1212K1135-BSD1 24.6 99 10 25 CQC

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MS %REthylbenzene


CQC83.4-116PVH2309-029724.212I0005-MS1 9/1/12 9/1/12 25

CQC83.4-116PVH2309-1110626.412I0028-MS1 9/4/12 9/4/12 25

CQC83.4-116PVH2037-079824.612I0081-MS1 9/5/12 9/5/12 25

CQC83.4-116PVI0290-0310025.112I0215-MS1 9/7/12 9/7/12 25

CQC83.4-116PVI0609-0910025.112I0352-MS1 9/12/12 9/12/12 25

CQC83.4-116PVI0525-069924.612I0394-MS1 9/12/12 9/12/12 25

CQC83.4-116PVI0894-0610526.112I0598-MS1 9/18/12 9/18/12 25

CQC83.4-116PVI1060-029924.712I0648-MS1 9/18/12 9/18/12 25

CQC83.4-116PVI1553-089523.712I0925-MS1 9/25/12 9/25/12 25

CQC83.4-116PVI1510-088922.312I0926-MS1 9/25/12 9/25/12 25

CQC83.4-116PVI1723-0310325.812I1065-MS1 9/28/12 9/28/12 25

CQC83.4-116PVI1822-029523.812I1095-MS1 9/28/12 9/28/12 25

CQC83.4-116PVI1869-059824.512I1107-MS1 9/29/12 9/29/12 25

CQC83.4-116PVI1575-019924.812J0008-MS1 10/1/12 10/1/12 25

83.4-116PVJ0513-03962412J0298-MS1 10/8/12 10/8/12 25

83.4-116PVJ0682-019724.112J0389-MS1 10/10/12 10/10/12 25

CQC83.4-116PVJ0682-179222.912J0445-MS1 10/11/12 10/11/12 25

CQC83.4-116PVJ1065-029624.112J0620-MS1 10/16/12 10/16/12 25

CQC83.4-116PVJ1237-029623.912J0736-MS1 10/18/12 10/18/12 25

CQC83.4-116PVJ1405-021082712J0821-MS1 10/20/12 10/20/12 25

CQC83.4-116PVJ1405-179223.112J0850-MS1 10/22/12 10/22/12 25

CQC83.4-116PVJ1577-0210225.612J0972-MS1 10/24/12 10/24/12 25

CQC,M183.4-116PVJ1627-01 (667)11796112J1010-MS1 10/25/12 10/25/12 250

CQC83.4-116PVJ1600-02 (0.22)10426.112J1038-MS1 10/25/12 10/25/12 25

CQC83.4-116PVJ1577-18RE111328212J1059-MS1 10/26/12 10/26/12 250

CQC,PSL83.4-116PVK0237-011283212K0235-MS1 11/7/12 11/7/12 25

CQC,M783.4-116PVK0555-0412230.412K0286-MS1 11/8/12 11/8/12 25

83.4-116PVK0649-061082712K0341-MS1 11/9/12 11/9/12 25

CQC83.4-116PVK0756-0110125.412K0415-MS1 11/12/12 11/12/12 25

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MS %REthylbenzeneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC83.4-116PVK0793-0211428.512K0462-MS1 11/13/12 11/13/12 25

CQC83.4-116PVK0281-01 (50.6)9774.8X 12K0522-MS1 11/14/12 11/14/12 25

CQC83.4-116PVK0632-0910626.512K0553-MS1 11/14/12 11/14/12 25

CQC83.4-116PVK0684-0210325.812K0552-MS1 11/14/12 11/14/12 25

CQC83.4-116PVK0696-0111027.512K0581-MS1 11/15/12 11/15/12 25

CQC83.4-116PVK0934-0110526.212K0740-MS1 11/20/12 11/20/12 25

CQC83.4-116PVK0768-0211428.412K0751-MS1 11/20/12 11/20/12 25

CQC83.4-116PVK1220-0210726.812K0803-MS1 11/21/12 11/21/12 25

CQC83.4-116PVK1288-0311328.312K0836-MS1 11/21/12 11/21/12 25

CQC83.4-116PVK1375-0810526.212K0865-MS1 11/23/12 11/23/12 25

CQC83.4-116PVK1375-0211428.412K0855-MS1 11/23/12 11/23/12 25

CQC83.4-116PVK0988-0311328.212K0897-MS1 11/24/12 11/24/12 25

CQC,PSL83.4-116PVK1006-0112430.912K0905-MS1 11/25/12 11/25/12 25

CQC83.4-116PVK1450-109924.712K1135-MS1 11/30/12 11/30/12 25

CQC,M783.4-116PVK1450-0312531.312K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDEthylbenzene


9523.8259/1/129/1/1212I0005-MSD1 CQC2529724.2 PVH2309-02

10325.7259/4/129/4/1212I0028-MSD1 CQC25310626.4 PVH2309-11

9724.3259/5/129/5/1212I0081-MSD1 CQC2519824.6 PVH2037-07

9924.7259/7/129/7/1212I0215-MSD1 CQC25210025.1 PVI0290-03

9624259/12/129/12/1212I0352-MSD1 CQC25410025.1 PVI0609-09

9824.6259/12/129/12/1212I0394-MSD1 CQC250.19924.6 PVI0525-06

10426.1259/18/129/18/1212I0598-MSD1 CQC250.210526.1 PVI0894-06

9724.3259/18/129/18/1212I0648-MSD1 CQC2519924.7 PVI1060-02

9122.7259/25/129/25/1212I0925-MSD1 CQC2559523.7 PVI1553-08

9223259/25/129/25/1212I0926-MSD1 CQC2538922.3 PVI1510-08

10626.6259/28/129/28/1212I1065-MSD1 CQC25310325.8 PVI1723-03

9924.8259/28/129/28/1212I1095-MSD1 CQC2549523.8 PVI1822-02

11127.7259/29/129/29/1212I1107-MSD1 CQC25129824.5 PVI1869-05

10125.32510/1/1210/1/1212J0008-MSD1 CQC2529924.8 PVI1575-01

9423.52510/8/1210/8/1212J0298-MSD1 2529624 PVJ0513-03

9924.82510/10/1210/10/1212J0389-MSD1 2539724.1 PVJ0682-01

9122.72510/11/1210/11/1212J0445-MSD1 CQC2519222.9 PVJ0682-17

9724.32510/16/1210/16/1212J0620-MSD1 CQC2519624.1 PVJ1065-02

9724.32510/18/1210/18/1212J0736-MSD1 CQC2529623.9 PVJ1237-02

11328.22510/20/1210/20/1212J0821-MSD1 CQC25410827 PVJ1405-02

9122.92510/22/1210/22/1212J0850-MSD1 CQC250.99223.1 PVJ1405-17

10526.22510/24/1210/24/1212J0972-MSD1 CQC25210225.6 PVJ1577-02

10492625010/25/1210/25/1212J1010-MSD1 CQC254117961 PVJ1627-01 (667)

11027.82510/25/1210/25/1212J1038-MSD1 CQC25610426.1 PVJ1600-02 (0.22)

11629125010/26/1210/26/1212J1059-MSD1 CQC253113282 PVJ1577-18RE1

132332511/7/1211/7/1212K0235-MSD1 CQC,PSL25312832 PVK0237-01

12330.72511/8/1211/8/1212K0286-MSD1 CQC,M7250.712230.4 PVK0555-04

10626.62511/9/1211/9/1212K0341-MSD1 25110827 PVK0649-06

104262511/12/1211/12/1212K0415-MSD1 CQC25310125.4 PVK0756-01

11228.12511/13/1211/13/1212K0462-MSD1 CQC25211428.5 PVK0793-02

7569.32511/14/1211/14/1212K0522-MSD1 CQC,M22589774.8 PVK0281-01 (50.6)

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MS/MSD RPDEthylbenzene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

11127.72511/14/1211/14/1212K0553-MSD1 CQC25510626.5 PVK0632-09

10526.22511/14/1211/14/1212K0552-MSD1 CQC25210325.8 PVK0684-02

11227.92511/15/1211/15/1212K0581-MSD1 CQC25111027.5 PVK0696-01

10325.62511/20/1211/20/1212K0740-MSD1 CQC25210526.2 PVK0934-01

11127.82511/20/1211/20/1212K0751-MSD1 CQC25211428.4 PVK0768-02

11629.12511/21/1211/21/1212K0803-MSD1 CQC25810726.8 PVK1220-02

112282511/21/1211/21/1212K0836-MSD1 CQC25111328.3 PVK1288-03

10325.72511/23/1211/23/1212K0865-MSD1 CQC25210526.2 PVK1375-08

11428.42511/23/1211/23/1212K0855-MSD1 CQC250.0711428.4 PVK1375-02

12130.32511/24/1211/24/1212K0897-MSD1 CQC,PSL25711328.2 PVK0988-03

11829.62511/25/1211/25/1212K0905-MSD1 CQC,PSL25412430.9 PVK1006-01

10425.92511/30/1211/30/1212K1135-MSD1 CQC2559924.7 PVK1450-10

13032.42512/1/1211/30/1212K1134-MSD1 CQC,M725412531.3 PVK1450-03

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BLKEthylbenzene

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0.0

Plotted: 44

MDL: 0.16

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

3s: 0

~------------------------------------------------------------__,4•:0

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %Rm,p-Xylenes


12I0005-BS1 26.2 105259/1/12 85-1159/1/12 CQC

12I0028-BS1 24.4 98259/4/12 85-1159/4/12 CQC

12I0081-BS1 24.4 98259/5/12 85-1159/5/12 CQC

12I0215-BS1 23.4 94259/7/12 85-1159/7/12 CQC

12I0352-BS1 25.2 101259/12/12 85-1159/12/12 CQC

12I0394-BS1 24.1 96259/12/12 85-1159/12/12 CQC

12I0598-BS1 26.1 104259/18/12 85-1159/18/12 CQC

12I0648-BS1 23.6 94259/18/12 85-1159/18/12 CQC

12I0926-BS1 23.2 93259/25/12 85-1159/25/12 CQC

12I0925-BS1 23.4 94259/25/12 85-1159/25/12 CQC

12I1065-BS1 24.8 99259/28/12 85-1159/28/12 CQC

12I1095-BS1 24 96259/28/12 85-1159/28/12 CQC

12I1107-BS1 24.2 97259/29/12 85-1159/29/12 CQC

12J0008-BS1 24.8 992510/1/12 85-11510/1/12 CQC

12J0298-BS1 23.3 932510/8/12 85-11510/8/12

12J0389-BS1 23.4 942510/10/12 85-11510/10/12

12J0445-BS1 23.8 952510/11/12 85-11510/11/12 CQC

12J0620-BS1 25.2 1012510/16/12 85-11510/16/12 CQC

12J0736-BS1 23.7 952510/18/12 85-11510/18/12 CQC

12J0821-BS1 25.7 1032510/20/12 85-11510/20/12 CQC

12J0850-BS1 23.6 942510/22/12 85-11510/22/12 CQC

12J0972-BS1 25.3 1012510/24/12 85-11510/24/12 CQC

12J1010-BS1 25.4 1012510/25/12 85-11510/25/12 CQC

12J1038-BS1 25.9 1042510/25/12 85-11510/25/12 CQC

12J1059-BS1 26.2 1052510/26/12 85-11510/26/12 CQC

12K0235-BS1 30.5 1222511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 26.8 1072511/8/12 85-11511/8/12 CQC

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LCS %Rm,p-XylenesLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 26.4 1062511/9/12 85-11511/9/12

12K0415-BS1 24.9 1002511/12/12 85-11511/12/12 CQC

12K0462-BS1 26.3 1052511/13/12 85-11511/13/12 CQC

12K0522-BS1 25.9 104X 2511/14/12 85-11511/14/12 CQC

12K0553-BS1 23.9 962511/14/12 85-11511/14/12 CQC

12K0552-BS1 25 1002511/14/12 85-11511/14/12 CQC

12K0581-BS1 24.4 982511/15/12 85-11511/15/12 CQC

12K0740-BS1 25.7 1032511/20/12 85-11511/20/12 CQC

12K0751-BS1 27.1 1082511/20/12 85-11511/20/12 CQC

12K0789-BS1 27.7 1112511/20/12 85-11511/20/12

12K0803-BS1 27.1 108X 2511/21/12 85-11511/21/12 CQC

12K0836-BS1 26.3 1052511/21/12 85-11511/21/12 CQC

12K0855-BS1 27.1 1082511/23/12 85-11511/23/12 CQC

12K0865-BS1 26.4 1062511/23/12 85-11511/23/12 CQC

12K0897-BS1 26.4 1062511/24/12 85-11511/24/12 CQC

12K0905-BS1 29.1 1172511/25/12 85-11511/25/12 CQC,PSL

12K1134-BS1 24.2 972511/30/12 85-11511/30/12 CQC

12K1135-BS1 25.1 1002511/30/12 85-11511/30/12 CQC

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LCS/LCSD RPDm,p-Xylenes


9223259/1/129/1/1212I0005-BSD1 26.2 105 13 25 CQC

10325.6259/4/129/4/1212I0028-BSD1 24.4 98 5 25 CQC

9323.4259/5/129/5/1212I0081-BSD1 24.4 98 4 25 CQC

9624.1259/7/129/7/1212I0215-BSD1 23.4 94 3 25 CQC

9523.7259/12/129/12/1212I0352-BSD1 25.2 101 6 25 CQC

9924.9259/12/129/12/1212I0394-BSD1 24.1 96 3 25 CQC

10325.8259/18/129/18/1212I0598-BSD1 26.1 104 1 25 CQC

9724.2259/18/129/18/1212I0648-BSD1 23.6 94 3 25 CQC

9122.7259/25/129/25/1212I0926-BSD1 23.2 93 2 25 CQC

9122.8259/25/129/25/1212I0925-BSD1 23.4 94 3 25 CQC

10225.4259/28/129/28/1212I1065-BSD1 24.8 99 3 25 CQC

10125.2259/28/129/28/1212I1095-BSD1 24 96 5 25 CQC

9022.5259/29/129/29/1212I1107-BSD1 24.2 97 7 25 CQC

10426.12510/1/1210/1/1212J0008-BSD1 24.8 99 5 25 CQC

9423.62510/8/1210/8/1212J0298-BSD1 23.3 93 1 25

9423.42510/10/1210/10/1212J0389-BSD1 23.4 94 0.2 25

9824.42510/11/1210/11/1212J0445-BSD1 23.8 95 3 25 CQC

9624.12510/16/1210/16/1212J0620-BSD1 25.2 101 5 25 CQC

96242510/18/1210/18/1212J0736-BSD1 23.7 95 1 25 CQC

100252510/20/1210/20/1212J0821-BSD1 25.7 103 3 25 CQC

9223.12510/22/1210/22/1212J0850-BSD1 23.6 94 2 25 CQC

9122.82510/24/1210/24/1212J0972-BSD1 25.3 101 10 25 CQC

10726.62510/25/1210/25/1212J1010-BSD1 25.4 101 5 25 CQC

11027.62510/25/1210/25/1212J1038-BSD1 25.9 104 6 25 CQC

10726.92510/26/1210/26/1212J1059-BSD1 26.2 105 3 25 CQC

12531.22511/7/1211/7/1212K0235-BSD1 30.5 122 2 25 CQC,PSL

10726.82511/8/1211/8/1212K0286-BSD1 26.8 107 0.07 25 CQC

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LCS/LCSD RPDm,p-Xylenes%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

10826.92511/9/1211/9/1212K0341-BSD1 26.4 106 2 25

9824.52511/12/1211/12/1212K0415-BSD1 24.9 100 2 25 CQC

10726.82511/13/1211/13/1212K0462-BSD1 26.3 105 2 25 CQC

10626.52511/14/1211/14/1212K0522-BSD1X 25.9 104 2 25 CQC

92232511/14/1211/14/1212K0553-BSD1 23.9 96 4 25 CQC

10225.62511/14/1211/14/1212K0552-BSD1 25 100 2 25 CQC

9523.82511/15/1211/15/1212K0581-BSD1 24.4 98 2 25 CQC

10626.42511/20/1211/20/1212K0740-BSD1 25.7 103 3 25 CQC

10325.82511/20/1211/20/1212K0751-BSD1 27.1 108 5 25 CQC

10526.42511/20/1211/20/1212K0789-BSD1 27.7 111 5 25

10526.32511/21/1211/21/1212K0803-BSD1 27.1 108 3 25 CQC

10125.22511/21/1211/21/1212K0836-BSD1 26.3 105 4 25 CQC

10927.22511/23/1211/23/1212K0855-BSD1 27.1 108 0.4 25 CQC

10426.12511/23/1211/23/1212K0865-BSD1 26.4 106 1 25 CQC

11027.52511/24/1211/24/1212K0897-BSD1 26.4 106 4 25 CQC

12130.32511/25/1211/25/1212K0905-BSD1 29.1 117 4 25 CQC,PSL

9824.52511/30/1211/30/1212K1134-BSD1 24.2 97 1 25 CQC

11328.32511/30/1211/30/1212K1135-BSD1 25.1 100 12 25 CQC

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MS %Rm,p-Xylenes


CQC70.8-132PVH2309-029724.312I0005-MS1 9/1/12 9/1/12 25

CQC70.8-132PVH2309-1110425.912I0028-MS1 9/4/12 9/4/12 25

CQC70.8-132PVH2037-079824.512I0081-MS1 9/5/12 9/5/12 25

CQC70.8-132PVI0290-039824.512I0215-MS1 9/7/12 9/7/12 25

CQC70.8-132PVI0609-091002512I0352-MS1 9/12/12 9/12/12 25

CQC70.8-132PVI0525-069824.412I0394-MS1 9/12/12 9/12/12 25

CQC70.8-132PVI0894-061042612I0598-MS1 9/18/12 9/18/12 25

CQC70.8-132PVI1060-029624.112I0648-MS1 9/18/12 9/18/12 25

CQC70.8-132PVI1553-089022.512I0925-MS1 9/25/12 9/25/12 25

CQC70.8-132PVI1510-08882212I0926-MS1 9/25/12 9/25/12 25

CQC70.8-132PVI1723-0310225.512I1065-MS1 9/28/12 9/28/12 25

CQC70.8-132PVI1822-029323.212I1095-MS1 9/28/12 9/28/12 25

CQC70.8-132PVI1869-059523.712I1107-MS1 9/29/12 9/29/12 25

CQC70.8-132PVI1575-019523.812J0008-MS1 10/1/12 10/1/12 25

70.8-132PVJ0513-039323.312J0298-MS1 10/8/12 10/8/12 25

70.8-132PVJ0682-019523.612J0389-MS1 10/10/12 10/10/12 25

CQC70.8-132PVJ0682-178922.212J0445-MS1 10/11/12 10/11/12 25

CQC70.8-132PVJ1065-029824.612J0620-MS1 10/16/12 10/16/12 25

CQC70.8-132PVJ1237-029423.512J0736-MS1 10/18/12 10/18/12 25

CQC70.8-132PVJ1405-021082712J0821-MS1 10/20/12 10/20/12 25

CQC70.8-132PVJ1405-179122.812J0850-MS1 10/22/12 10/22/12 25

CQC70.8-132PVJ1577-029824.612J0972-MS1 10/24/12 10/24/12 25

CQC70.8-132PVJ1627-01 (2370)123267012J1010-MS1 10/25/12 10/25/12 250

CQC70.8-132PVJ1600-0210626.412J1038-MS1 10/25/12 10/25/12 25

CQC70.8-132PVJ1577-18RE110927212J1059-MS1 10/26/12 10/26/12 250

CQC70.8-132PVK0237-0112631.412K0235-MS1 11/7/12 11/7/12 25

CQC70.8-132PVK0555-0412330.812K0286-MS1 11/8/12 11/8/12 25

70.8-132PVK0649-0610726.712K0341-MS1 11/9/12 11/9/12 25

CQC70.8-132PVK0756-0110626.612K0415-MS1 11/12/12 11/12/12 25

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MS %Rm,p-XylenesSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC70.8-132PVK0793-0211027.612K0462-MS1 11/13/12 11/13/12 25

CQC,M270.8-132PVK0281-01 (70.2)6887.112K0522-MS1 11/14/12 11/14/12 25

CQC70.8-132PVK0632-099924.812K0553-MS1 11/14/12 11/14/12 25

CQC70.8-132PVK0684-0210826.912K0552-MS1 11/14/12 11/14/12 25

CQC70.8-132PVK0696-0110225.612K0581-MS1 11/15/12 11/15/12 25

CQC70.8-132PVK0934-01 (1.08)10527.312K0740-MS1 11/20/12 11/20/12 25

CQC70.8-132PVK0768-0211528.612K0751-MS1 11/20/12 11/20/12 25

CQC70.8-132PVK1220-0210325.912K0803-MS1 11/21/12 11/21/12 25

CQC70.8-132PVK1288-0310927.312K0836-MS1 11/21/12 11/21/12 25

CQC70.8-132PVK1375-0810827.112K0865-MS1 11/23/12 11/23/12 25

CQC70.8-132PVK1375-021082712K0855-MS1 11/23/12 11/23/12 25

CQC70.8-132PVK0988-031082712K0897-MS1 11/24/12 11/24/12 25

CQC70.8-132PVK1006-0112230.412K0905-MS1 11/25/12 11/25/12 25

CQC70.8-132PVK1450-1010325.812K1135-MS1 11/30/12 11/30/12 25

CQC70.8-132PVK1450-0311829.512K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDm,p-Xylenes


9523.7259/1/129/1/1212I0005-MSD1 CQC2539724.3 PVH2309-02

10125.2259/4/129/4/1212I0028-MSD1 CQC25310425.9 PVH2309-11

9924.7259/5/129/5/1212I0081-MSD1 CQC2519824.5 PVH2037-07

9824.6259/7/129/7/1212I0215-MSD1 CQC250.59824.5 PVI0290-03

9624.1259/12/129/12/1212I0352-MSD1 CQC25410025 PVI0609-09

9423.4259/12/129/12/1212I0394-MSD1 CQC2549824.4 PVI0525-06

10526.2259/18/129/18/1212I0598-MSD1 CQC25110426 PVI0894-06

9223.1259/18/129/18/1212I0648-MSD1 CQC2549624.1 PVI1060-02

9022.6259/25/129/25/1212I0925-MSD1 CQC250.39022.5 PVI1553-08

8922.3259/25/129/25/1212I0926-MSD1 CQC2518822 PVI1510-08

10125.3259/28/129/28/1212I1065-MSD1 CQC250.610225.5 PVI1723-03

9523.9259/28/129/28/1212I1095-MSD1 CQC2539323.2 PVI1822-02

10626.5259/29/129/29/1212I1107-MSD1 CQC25119523.7 PVI1869-05

9222.92510/1/1210/1/1212J0008-MSD1 CQC2549523.8 PVI1575-01

9323.42510/8/1210/8/1212J0298-MSD1 250.099323.3 PVJ0513-03

9724.22510/10/1210/10/1212J0389-MSD1 2539523.6 PVJ0682-01

8922.32510/11/1210/11/1212J0445-MSD1 CQC250.58922.2 PVJ0682-17

9824.42510/16/1210/16/1212J0620-MSD1 CQC250.49824.6 PVJ1065-02

96242510/18/1210/18/1212J0736-MSD1 CQC2529423.5 PVJ1237-02

116292510/20/1210/20/1212J0821-MSD1 CQC25710827 PVJ1405-02

92232510/22/1210/22/1212J0850-MSD1 CQC250.89122.8 PVJ1405-17

10125.12510/24/1210/24/1212J0972-MSD1 CQC2529824.6 PVJ1577-02

87258025010/25/1210/25/1212J1010-MSD1 CQC2531232670 PVJ1627-01 (2370)

10827.12510/25/1210/25/1212J1038-MSD1 CQC25210626.4 PVJ1600-02

11127925010/26/1210/26/1212J1059-MSD1 CQC252109272 PVJ1577-18RE1

13132.72511/7/1211/7/1212K0235-MSD1 CQC25412631.4 PVK0237-01

12130.32511/8/1211/8/1212K0286-MSD1 CQC25212330.8 PVK0555-04

104262511/9/1211/9/1212K0341-MSD1 25310726.7 PVK0649-06

10826.92511/12/1211/12/1212K0415-MSD1 CQC25110626.6 PVK0756-01

10526.32511/13/1211/13/1212K0462-MSD1 CQC25511027.6 PVK0793-02

5383.42511/14/1211/14/1212K0522-MSD1X CQC,M22546887.1 PVK0281-01 (70.2)

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MS/MSD RPDm,p-Xylenes%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

10024.92511/14/1211/14/1212K0553-MSD1 CQC250.39924.8 PVK0632-09

10626.62511/14/1211/14/1212K0552-MSD1 CQC25110826.9 PVK0684-02

10225.42511/15/1211/15/1212K0581-MSD1 CQC250.810225.6 PVK0696-01

10126.42511/20/1211/20/1212K0740-MSD1 CQC25410527.3 PVK0934-01 (1.08)

11428.42511/20/1211/20/1212K0751-MSD1 CQC250.811528.6 PVK0768-02

11428.42511/21/1211/21/1212K0803-MSD1 CQC251010325.9 PVK1220-02

10927.22511/21/1211/21/1212K0836-MSD1 CQC250.610927.3 PVK1288-03

10425.92511/23/1211/23/1212K0865-MSD1 CQC25510827.1 PVK1375-08

108272511/23/1211/23/1212K0855-MSD1 CQC250.110827 PVK1375-02

11729.32511/24/1211/24/1212K0897-MSD1 CQC25810827 PVK0988-03

11027.62511/25/1211/25/1212K0905-MSD1 CQC251012230.4 PVK1006-01

11127.72511/30/1211/30/1212K1135-MSD1 CQC25710325.8 PVK1450-10

12330.82512/1/1211/30/1212K1134-MSD1 CQC25411829.5 PVK1450-03

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BLKm,p-Xylenes

2.0

1.8

1.6

1.4

1.2

1.0

0.8

0.6

0.4

0.2

0.0

Plotted: 44

MDL: 0.35

MRL: 2

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

3s: 0

~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~4s:O

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %RMethylene Chloride


12I0005-BS1 25.8 103259/1/12 79.7-1179/1/12 CQC

12I0028-BS1 24 96259/4/12 79.7-1179/4/12 CQC

12I0081-BS1 21.5 86259/5/12 79.7-1179/5/12 CQC

12I0215-BS1 21.8 87259/7/12 79.7-1179/7/12 CQC

12I0352-BS1 25.5 102259/12/12 79.7-1179/12/12 CQC

12I0394-BS1 22.6 90259/12/12 79.7-1179/12/12 CQC

12I0598-BS1 26.9 108259/18/12 79.7-1179/18/12 CQC

12I0648-BS1 22.9 92259/18/12 79.7-1179/18/12 CQC

12I0926-BS1 22.9 91259/25/12 79.7-1179/25/12 CQC

12I0925-BS1 22 88259/25/12 79.7-1179/25/12 CQC

12I1065-BS1 23.7 95259/28/12 79.7-1179/28/12 CQC

12I1095-BS1 24.3 97259/28/12 79.7-1179/28/12 CQC

12I1107-BS1 24.6 98259/29/12 79.7-1179/29/12 CQC

12J0008-BS1 22.8 912510/1/12 79.7-11710/1/12 CQC

12J0298-BS1 20.5 822510/8/12 79.7-11710/8/12

12J0389-BS1 20.2 812510/10/12 79.7-11710/10/12

12J0445-BS1 19.6 782510/11/12 79.7-11710/11/12 CQC,PSL

12J0620-BS1 21.1 842510/16/12 79.7-11710/16/12 CQC

12J0736-BS1 21.9 882510/18/12 79.7-11710/18/12 CQC

12J0821-BS1 21.2 852510/20/12 79.7-11710/20/12 CQC

12J0850-BS1 20.9 832510/22/12 79.7-11710/22/12 CQC

12J0972-BS1 23.4 932510/24/12 79.7-11710/24/12 CQC

12J1010-BS1 21.8 872510/25/12 79.7-11710/25/12 CQC

12J1038-BS1 23.2 932510/25/12 79.7-11710/25/12 CQC

12J1059-BS1 21.9 882510/26/12 79.7-11710/26/12 CQC

12K0235-BS1 28.5 1142511/7/12 79.7-11711/7/12 CQC

12K0286-BS1 24.7 992511/8/12 79.7-11711/8/12 CQC

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LCS %RMethylene ChlorideLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 19.3 772511/9/12 79.7-11711/9/12

12K0415-BS1 21.7 872511/12/12 79.7-11711/12/12 CQC

12K0462-BS1 25 1002511/13/12 79.7-11711/13/12 CQC

12K0522-BS1 24.7 99X 2511/14/12 79.7-11711/14/12 CQC

12K0553-BS1 20.5 822511/14/12 79.7-11711/14/12 CQC

12K0552-BS1 22.4 892511/14/12 79.7-11711/14/12 CQC

12K0581-BS1 21.1 842511/15/12 79.7-11711/15/12 CQC

12K0740-BS1 23.2 932511/20/12 79.7-11711/20/12 CQC

12K0751-BS1 23.1 922511/20/12 79.7-11711/20/12 CQC

12K0789-BS1 25.6 1022511/20/12 79.7-11711/20/12

12K0803-BS1 22.8 91X 2511/21/12 79.7-11711/21/12 CQC

12K0836-BS1 24.5 982511/21/12 79.7-11711/21/12 CQC

12K0855-BS1 24 962511/23/12 79.7-11711/23/12 CQC

12K0865-BS1 23 922511/23/12 79.7-11711/23/12 CQC

12K0897-BS1 21.4 852511/24/12 79.7-11711/24/12 CQC

12K0905-BS1 22.8 912511/25/12 79.7-11711/25/12 CQC

12K1134-BS1 20.3 812511/30/12 79.7-11711/30/12 CQC

12K1135-BS1 22.4 902511/30/12 79.7-11711/30/12 CQC

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LCS/LCSD RPDMethylene Chloride


8521.4259/1/129/1/1212I0005-BSD1 25.8 103 19 25 CQC

10225.5259/4/129/4/1212I0028-BSD1 24 96 6 25 CQC

9223259/5/129/5/1212I0081-BSD1 21.5 86 7 25 CQC

7819.5259/7/129/7/1212I0215-BSD1 21.8 87 11 25 CQC,PSL

9824.5259/12/129/12/1212I0352-BSD1 25.5 102 4 25 CQC

9724.3259/12/129/12/1212I0394-BSD1 22.6 90 7 25 CQC

10426259/18/129/18/1212I0598-BSD1 26.9 108 3 25 CQC

8922.3259/18/129/18/1212I0648-BSD1 22.9 92 3 25 CQC

8521.3259/25/129/25/1212I0926-BSD1 22.9 91 7 25 CQC

8621.4259/25/129/25/1212I0925-BSD1 22 88 2 25 CQC

9122.8259/28/129/28/1212I1065-BSD1 23.7 95 4 25 CQC

8821.9259/28/129/28/1212I1095-BSD1 24.3 97 10 25 CQC

8721.7259/29/129/29/1212I1107-BSD1 24.6 98 13 25 CQC

9724.22510/1/1210/1/1212J0008-BSD1 22.8 91 6 25 CQC

8220.42510/8/1210/8/1212J0298-BSD1 20.5 82 0.3 25

7919.72510/10/1210/10/1212J0389-BSD1 20.2 81 2 25 PSL

7819.62510/11/1210/11/1212J0445-BSD1 19.6 78 0 25 CQC,PSL

9122.82510/16/1210/16/1212J0620-BSD1 21.1 84 8 25 CQC

8421.12510/18/1210/18/1212J0736-BSD1 21.9 88 4 25 CQC

8521.32510/20/1210/20/1212J0821-BSD1 21.2 85 0.5 25 CQC

8120.22510/22/1210/22/1212J0850-BSD1 20.9 83 3 25 CQC

8420.92510/24/1210/24/1212J0972-BSD1 23.4 93 11 25 CQC

8120.42510/25/1210/25/1212J1010-BSD1 21.8 87 7 25 CQC

9523.82510/25/1210/25/1212J1038-BSD1 23.2 93 3 25 CQC

9323.12510/26/1210/26/1212J1059-BSD1 21.9 88 5 25 CQC

11027.42511/7/1211/7/1212K0235-BSD1 28.5 114 4 25 CQC

9824.52511/8/1211/8/1212K0286-BSD1 24.7 99 0.7 25 CQC

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LCS/LCSD RPDMethylene Chloride%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

8220.52511/9/1211/9/1212K0341-BSD1 19.3 77 6 25

8922.22511/12/1211/12/1212K0415-BSD1 21.7 87 2 25 CQC

9724.12511/13/1211/13/1212K0462-BSD1 25 100 3 25 CQC

9724.12511/14/1211/14/1212K0522-BSD1X 24.7 99 2 25 CQC

9523.72511/14/1211/14/1212K0553-BSD1 20.5 82 15 25 CQC

88222511/14/1211/14/1212K0552-BSD1 22.4 89 2 25 CQC

8521.22511/15/1211/15/1212K0581-BSD1 21.1 84 0.5 25 CQC

9222.92511/20/1211/20/1212K0740-BSD1 23.2 93 1 25 CQC

8721.62511/20/1211/20/1212K0751-BSD1 23.1 92 6 25 CQC

9824.52511/20/1211/20/1212K0789-BSD1 25.6 102 4 25

10024.92511/21/1211/21/1212K0803-BSD1 22.8 91 9 25 CQC

9423.52511/21/1211/21/1212K0836-BSD1 24.5 98 4 25 CQC

9824.52511/23/1211/23/1212K0855-BSD1 24 96 2 25 CQC

9824.52511/23/1211/23/1212K0865-BSD1 23 92 6 25 CQC

8922.22511/24/1211/24/1212K0897-BSD1 21.4 85 4 25 CQC

9623.92511/25/1211/25/1212K0905-BSD1 22.8 91 5 25 CQC

8922.22511/30/1211/30/1212K1134-BSD1 20.3 81 9 25 CQC

9523.82511/30/1211/30/1212K1135-BSD1 22.4 90 6 25 CQC

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MS %RMethylene Chloride


CQC74.6-119PVH2309-029724.212I0005-MS1 9/1/12 9/1/12 25

CQC74.6-119PVH2309-1110927.112I0028-MS1 9/4/12 9/4/12 25

CQC74.6-119PVH2037-079423.512I0081-MS1 9/5/12 9/5/12 25

CQC74.6-119PVI0290-039924.712I0215-MS1 9/7/12 9/7/12 25

CQC74.6-119PVI0609-099924.712I0352-MS1 9/12/12 9/12/12 25

CQC74.6-119PVI0525-0610325.812I0394-MS1 9/12/12 9/12/12 25

CQC74.6-119PVI0894-0610827.112I0598-MS1 9/18/12 9/18/12 25

CQC74.6-119PVI1060-029122.712I0648-MS1 9/18/12 9/18/12 25

CQC74.6-119PVI1553-088621.512I0925-MS1 9/25/12 9/25/12 25

CQC74.6-119PVI1510-089022.412I0926-MS1 9/25/12 9/25/12 25

CQC74.6-119PVI1723-0310626.612I1065-MS1 9/28/12 9/28/12 25

CQC74.6-119PVI1822-029423.612I1095-MS1 9/28/12 9/28/12 25

CQC74.6-119PVI1869-05962412I1107-MS1 9/29/12 9/29/12 25

CQC74.6-119PVI1575-019724.412J0008-MS1 10/1/12 10/1/12 25

74.6-119PVJ0513-038320.912J0298-MS1 10/8/12 10/8/12 25

74.6-119PVJ0682-01842112J0389-MS1 10/10/12 10/10/12 25

CQC,PSL74.6-119PVJ0682-177418.512J0445-MS1 10/11/12 10/11/12 25

CQC74.6-119PVJ1065-028521.312J0620-MS1 10/16/12 10/16/12 25

CQC74.6-119PVJ1237-028621.412J0736-MS1 10/18/12 10/18/12 25

CQC74.6-119PVJ1405-029523.612J0821-MS1 10/20/12 10/20/12 25

CQC74.6-119PVJ1405-178120.312J0850-MS1 10/22/12 10/22/12 25

CQC74.6-119PVJ1577-028721.812J0972-MS1 10/24/12 10/24/12 25

CQC74.6-119PVJ1627-018120312J1010-MS1 10/25/12 10/25/12 250

CQC74.6-119PVJ1600-029523.812J1038-MS1 10/25/12 10/25/12 25

CQC74.6-119PVJ1577-18RE110325712J1059-MS1 10/26/12 10/26/12 250

CQC,PSL74.6-119PVK0237-011243112K0235-MS1 11/7/12 11/7/12 25

CQC74.6-119PVK0555-0411829.512K0286-MS1 11/8/12 11/8/12 25

74.6-119PVK0649-068721.712K0341-MS1 11/9/12 11/9/12 25

CQC74.6-119PVK0756-019122.912K0415-MS1 11/12/12 11/12/12 25

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MS %RMethylene ChlorideSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC74.6-119PVK0793-0211127.712K0462-MS1 11/13/12 11/13/12 25

CQC74.6-119PVK0281-019824.5X 12K0522-MS1 11/14/12 11/14/12 25

CQC74.6-119PVK0632-099423.412K0553-MS1 11/14/12 11/14/12 25

CQC74.6-119PVK0684-0210024.912K0552-MS1 11/14/12 11/14/12 25

CQC74.6-119PVK0696-01922312K0581-MS1 11/15/12 11/15/12 25

CQC74.6-119PVK0934-01922312K0740-MS1 11/20/12 11/20/12 25

CQC74.6-119PVK0768-0210927.312K0751-MS1 11/20/12 11/20/12 25

CQC74.6-119PVK1220-0210025.1X 12K0803-MS1 11/21/12 11/21/12 25

CQC74.6-119PVK1288-031042612K0836-MS1 11/21/12 11/21/12 25

CQC74.6-119PVK1375-08962412K0865-MS1 11/23/12 11/23/12 25

CQC74.6-119PVK1375-029624.112K0855-MS1 11/23/12 11/23/12 25

CQC74.6-119PVK0988-039423.612K0897-MS1 11/24/12 11/24/12 25

CQC74.6-119PVK1006-019824.612K0905-MS1 11/25/12 11/25/12 25

CQC74.6-119PVK1450-101002512K1135-MS1 11/30/12 11/30/12 25

CQC74.6-119PVK1450-0310125.312K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDMethylene Chloride


10025259/1/129/1/1212I0005-MSD1 CQC2539724.2 PVH2309-02

10827259/4/129/4/1212I0028-MSD1 CQC250.510927.1 PVH2309-11

9824.6259/5/129/5/1212I0081-MSD1 CQC2549423.5 PVH2037-07

9222.9259/7/129/7/1212I0215-MSD1 CQC2579924.7 PVI0290-03

9924.7259/12/129/12/1212I0352-MSD1 CQC250.29924.7 PVI0609-09

10425.9259/12/129/12/1212I0394-MSD1 CQC250.510325.8 PVI0525-06

10726.6259/18/129/18/1212I0598-MSD1 CQC25210827.1 PVI0894-06

8721.7259/18/129/18/1212I0648-MSD1 CQC2559122.7 PVI1060-02

9022.4259/25/129/25/1212I0925-MSD1 CQC2548621.5 PVI1553-08

9423.4259/25/129/25/1212I0926-MSD1 CQC2549022.4 PVI1510-08

10125.4259/28/129/28/1212I1065-MSD1 CQC25510626.6 PVI1723-03

10325.8259/28/129/28/1212I1095-MSD1 CQC2599423.6 PVI1822-02

10827.1259/29/129/29/1212I1107-MSD1 CQC25129624 PVI1869-05

10024.92510/1/1210/1/1212J0008-MSD1 CQC2529724.4 PVI1575-01

8621.42510/8/1210/8/1212J0298-MSD1 2538320.9 PVJ0513-03

8220.52510/10/1210/10/1212J0389-MSD1 2538421 PVJ0682-01

7418.62510/11/1210/11/1212J0445-MSD1 CQC,PSL250.37418.5 PVJ0682-17

8721.72510/16/1210/16/1212J0620-MSD1 CQC2528521.3 PVJ1065-02

9323.32510/18/1210/18/1212J0736-MSD1 CQC2588621.4 PVJ1237-02

10125.22510/20/1210/20/1212J0821-MSD1 CQC2579523.6 PVJ1405-02

8120.22510/22/1210/22/1212J0850-MSD1 CQC250.48120.3 PVJ1405-17

9122.82510/24/1210/24/1212J0972-MSD1 CQC2558721.8 PVJ1577-02

8421025010/25/1210/25/1212J1010-MSD1 CQC25381203 PVJ1627-01

9624.12510/25/1210/25/1212J1038-MSD1 CQC2519523.8 PVJ1600-02

10125425010/26/1210/26/1212J1059-MSD1 CQC251103257 PVJ1577-18RE1

12731.82511/7/1211/7/1212K0235-MSD1 CQC,PSL25312431 PVK0237-01

10826.92511/8/1211/8/1212K0286-MSD1 CQC25911829.5 PVK0555-04

88222511/9/1211/9/1212K0341-MSD1 2528721.7 PVK0649-06

9423.42511/12/1211/12/1212K0415-MSD1 CQC2529122.9 PVK0756-01

10626.52511/13/1211/13/1212K0462-MSD1 CQC25411127.7 PVK0793-02

10426.12511/14/1211/14/1212K0522-MSD1X CQC2569824.5 PVK0281-01

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MS/MSD RPDMethylene Chloride%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

8521.22511/14/1211/14/1212K0553-MSD1 CQC25109423.4 PVK0632-09

10826.92511/14/1211/14/1212K0552-MSD1 CQC25810024.9 PVK0684-02

9623.92511/15/1211/15/1212K0581-MSD1 CQC2549223 PVK0696-01

9223.12511/20/1211/20/1212K0740-MSD1 CQC250.79223 PVK0934-01

10626.52511/20/1211/20/1212K0751-MSD1 CQC25310927.3 PVK0768-02

10325.92511/21/1211/21/1212K0803-MSD1 CQC25310025.1 PVK1220-02

10526.22511/21/1211/21/1212K0836-MSD1 CQC250.710426 PVK1288-03

10125.22511/23/1211/23/1212K0865-MSD1 CQC2559624 PVK1375-08

96242511/23/1211/23/1212K0855-MSD1 CQC250.049624.1 PVK1375-02

9924.92511/24/1211/24/1212K0897-MSD1 CQC2559423.6 PVK0988-03

9624.12511/25/1211/25/1212K0905-MSD1 CQC2529824.6 PVK1006-01

104262511/30/1211/30/1212K1135-MSD1 CQC25410025 PVK1450-10

9623.92512/1/1211/30/1212K1134-MSD1 CQC25610125.3 PVK1450-03

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BLKMethylene Chloride

2.0 r-------------------------------------------------------~

1.8

1.6

1.4

1.2

1.0

OB · · · · · · · · · · · · · · · · ·

Plotted: 44

MDL: 0.5

MRL: 2

Rejected: 2

Stdv: 0.142

Mean: 0.121

2s: 0.406 0

·6 ]::::::1~·=· =· =· 1· t. =· ~· ~· =· =· =·=·=·====================~3s: 0.548

0.4 \ A ~ . . . . 1\. . . 4s: 0.691 o.2 · · I V \ · · · · · A _y:r · ~ · · · · o: · h · · · A I ' t;.;;:;Jtj~~=Jt::~t\;/'.,z:;;;,.;rZ,~~::=::::~~\.=~.Jt:.:-:v::;\ 2A~Z,.Pt::\.;;;./4~~_J 0.0 .,..

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %RMethyl-tert-butyl Ether (MTBE)


12K0235-BS1 29.3 1172511/7/12 81.8-11811/7/12 CQC

12K0286-BS1 26 1042511/8/12 81.8-11811/8/12 CQC

12K0341-BS1 23.7 952511/9/12 81.8-11811/9/12

12K0415-BS1 23.5 942511/12/12 81.8-11811/12/12 CQC

12K0462-BS1 26.3 1052511/13/12 81.8-11811/13/12 CQC

12K0522-BS1 25.4 1022511/14/12 81.8-11811/14/12 CQC

12K0803-BS1 25.8 1032511/21/12 81.8-11811/21/12 CQC

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LCS/LCSD RPDMethyl-tert-butyl Ether (MTBE)


11127.72511/7/1211/7/1212K0235-BSD1 29.3 117 5 25 CQC

10325.72511/8/1211/8/1212K0286-BSD1 26 104 1 25 CQC

9323.22511/9/1211/9/1212K0341-BSD1 23.7 95 2 25

9122.72511/12/1211/12/1212K0415-BSD1 23.5 94 3 25 CQC

10125.42511/13/1211/13/1212K0462-BSD1 26.3 105 4 25 CQC

10726.82511/14/1211/14/1212K0522-BSD1 25.4 102 5 25 CQC

11629.12511/21/1211/21/1212K0803-BSD1 25.8 103 12 25 CQC

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MS %RMethyl-tert-butyl Ether (MTBE)


CQC68.8-126PVK0237-0112631.612K0235-MS1 11/7/12 11/7/12 25

CQC68.8-126PVK0555-0411729.312K0286-MS1 11/8/12 11/8/12 25

68.8-126PVK0649-069724.312K0341-MS1 11/9/12 11/9/12 25

CQC68.8-126PVK0756-019423.512K0415-MS1 11/12/12 11/12/12 25

CQC68.8-126PVK0793-0211127.912K0462-MS1 11/13/12 11/13/12 25

CQC68.8-126PVK0281-01 (37.1)926012K0522-MS1 11/14/12 11/14/12 25

CQC68.8-126PVK1220-0211328.312K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDMethyl-tert-butyl Ether (MTBE)


12430.92511/7/1211/7/1212K0235-MSD1 CQC25212631.6 PVK0237-01

116292511/8/1211/8/1212K0286-MSD1 CQC25111729.3 PVK0555-04

96242511/9/1211/9/1212K0341-MSD1 2519724.3 PVK0649-06

9924.72511/12/1211/12/1212K0415-MSD1 CQC2559423.5 PVK0756-01

10927.22511/13/1211/13/1212K0462-MSD1 CQC25211127.9 PVK0793-02

100622511/14/1211/14/1212K0522-MSD1 CQC2539260 PVK0281-01 (37.1)

11127.82511/21/1211/21/1212K0803-MSD1 CQC25211328.3 PVK1220-02

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BLKMethyl-tert-butyl Ether (MTBE)

01/02/13 15:46

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LCS %Rn-Butylbenzene


12K0235-BS1 30.7 1232511/7/12 74-12111/7/12 CQC,PSL

12K0286-BS1 26.3 1052511/8/12 74-12111/8/12 CQC

12K0341-BS1 26.1 1042511/9/12 74-12111/9/12

12K0415-BS1 23.4 932511/12/12 74-12111/12/12 CQC

12K0462-BS1 24.5 982511/13/12 74-12111/13/12 CQC

12K0522-BS1 27.7 1112511/14/12 74-12111/14/12 CQC

12K0803-BS1 27.4 1102511/21/12 74-12111/21/12 CQC

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LCS/LCSD RPDn-Butylbenzene


12030.12511/7/1211/7/1212K0235-BSD1 30.7 123 2 25 CQC

10927.32511/8/1211/8/1212K0286-BSD1 26.3 105 4 25 CQC

10025.12511/9/1211/9/1212K0341-BSD1 26.1 104 4 25

9523.82511/12/1211/12/1212K0415-BSD1 23.4 93 2 25 CQC

11027.42511/13/1211/13/1212K0462-BSD1 24.5 98 11 25 CQC

10927.22511/14/1211/14/1212K0522-BSD1 27.7 111 2 25 CQC

11227.92511/21/1211/21/1212K0803-BSD1 27.4 110 2 25 CQC

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MS %Rn-Butylbenzene


CQC,PSL70.4-119PVK0237-011203012K0235-MS1 11/7/12 11/7/12 25

CQC70.4-119PVK0555-0411929.912K0286-MS1 11/8/12 11/8/12 25

70.4-119PVK0649-069423.412K0341-MS1 11/9/12 11/9/12 25

CQC70.4-119PVK0756-019724.212K0415-MS1 11/12/12 11/12/12 25

CQC70.4-119PVK0793-0210726.812K0462-MS1 11/13/12 11/13/12 25

CQC70.4-119PVK0281-011082712K0522-MS1 11/14/12 11/14/12 25

CQC70.4-119PVK1220-021082712K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDn-Butylbenzene


128322511/7/1211/7/1212K0235-MSD1 CQC,PSL25612030 PVK0237-01

11127.72511/8/1211/8/1212K0286-MSD1 CQC25811929.9 PVK0555-04

9724.22511/9/1211/9/1212K0341-MSD1 2539423.4 PVK0649-06

8421.12511/12/1211/12/1212K0415-MSD1 CQC25149724.2 PVK0756-01

108272511/13/1211/13/1212K0462-MSD1 CQC250.610726.8 PVK0793-02

11428.42511/14/1211/14/1212K0522-MSD1 CQC25510827 PVK0281-01

12330.62511/21/1211/21/1212K0803-MSD1 CQC,M7251310827 PVK1220-02

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BLKn-Butylbenzene

01/02/13 15:46

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LCS %Rn-Propylbenzene


12K0235-BS1 30.1 1202511/7/12 79.4-12011/7/12 CQC

12K0286-BS1 26 1042511/8/12 79.4-12011/8/12 CQC

12K0341-BS1 26.3 1052511/9/12 79.4-12011/9/12

12K0415-BS1 23.3 932511/12/12 79.4-12011/12/12 CQC

12K0462-BS1 24.7 992511/13/12 79.4-12011/13/12 CQC

12K0522-BS1 30.8 1232511/14/12 79.4-12011/14/12 CQC,L

12K0803-BS1 26.4 1062511/21/12 79.4-12011/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPDn-Propylbenzene


11729.22511/7/1211/7/1212K0235-BSD1 30.1 120 3 25 CQC

10626.62511/8/1211/8/1212K0286-BSD1 26 104 2 25 CQC

10125.22511/9/1211/9/1212K0341-BSD1 26.3 105 4 25

9824.42511/12/1211/12/1212K0415-BSD1 23.3 93 5 25 CQC

10626.52511/13/1211/13/1212K0462-BSD1 24.7 99 7 25 CQC

12430.92511/14/1211/14/1212K0522-BSD1 30.8 123 0.2 25 CQC,L

10827.12511/21/1211/21/1212K0803-BSD1 26.4 106 2 25 CQC

01/02/13 15:46

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MS %Rn-Propylbenzene


CQC76-124PVK0237-0111929.812K0235-MS1 11/7/12 11/7/12 25

CQC76-124PVK0555-0411929.712K0286-MS1 11/8/12 11/8/12 25

76-124PVK0649-0610526.312K0341-MS1 11/9/12 11/9/12 25

CQC76-124PVK0756-019924.812K0415-MS1 11/12/12 11/12/12 25

CQC76-124PVK0793-021042612K0462-MS1 11/13/12 11/13/12 25

CQC76-124PVK0281-01 (9.01)11938.712K0522-MS1 11/14/12 11/14/12 25

CQC76-124PVK1220-0211127.812K0803-MS1 11/21/12 11/21/12 25

01/02/13 15:46

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MS/MSD RPDn-Propylbenzene


12130.22511/7/1211/7/1212K0235-MSD1 CQC25111929.8 PVK0237-01

11428.62511/8/1211/8/1212K0286-MSD1 CQC25411929.7 PVK0555-04

10225.52511/9/1211/9/1212K0341-MSD1 25310526.3 PVK0649-06

9824.42511/12/1211/12/1212K0415-MSD1 CQC2519924.8 PVK0756-01

11729.32511/13/1211/13/1212K0462-MSD1 CQC251210426 PVK0793-02

11838.42511/14/1211/14/1212K0522-MSD1 CQC250.611938.7 PVK0281-01 (9.01)

12230.42511/21/1211/21/1212K0803-MSD1 CQC25911127.8 PVK1220-02

01/02/13 15:46

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BLKn-Propylbenzene

01/02/13 15:46

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LCS %Ro-Xylene


12I0005-BS1 26.8 107259/1/12 85-1159/1/12 CQC

12I0028-BS1 25.4 101259/4/12 85-1159/4/12 CQC

12I0081-BS1 23.8 95259/5/12 85-1159/5/12 CQC

12I0215-BS1 24 96259/7/12 85-1159/7/12 CQC

12I0352-BS1 26.2 105259/12/12 85-1159/12/12 CQC

12I0394-BS1 24.2 97259/12/12 85-1159/12/12 CQC

12I0598-BS1 27.6 110259/18/12 85-1159/18/12 CQC

12I0648-BS1 25.4 101259/18/12 85-1159/18/12 CQC

12I0926-BS1 24 96259/25/12 85-1159/25/12 CQC

12I0925-BS1 24.4 98259/25/12 85-1159/25/12 CQC

12I1065-BS1 25.3 101259/28/12 85-1159/28/12 CQC

12I1095-BS1 24.3 97259/28/12 85-1159/28/12 CQC

12I1107-BS1 25.3 101259/29/12 85-1159/29/12 CQC

12J0008-BS1 25.7 1032510/1/12 85-11510/1/12 CQC

12J0298-BS1 23.9 962510/8/12 85-11510/8/12

12J0389-BS1 24.3 972510/10/12 85-11510/10/12

12J0445-BS1 25 1002510/11/12 85-11510/11/12 CQC

12J0620-BS1 26.3 1052510/16/12 85-11510/16/12 CQC

12J0736-BS1 25.1 1012510/18/12 85-11510/18/12 CQC

12J0821-BS1 27.2 1092510/20/12 85-11510/20/12 CQC

12J0850-BS1 24.5 982510/22/12 85-11510/22/12 CQC

12J0972-BS1 26.3 1052510/24/12 85-11510/24/12 CQC

12J1010-BS1 25.4 1022510/25/12 85-11510/25/12 CQC

12J1038-BS1 25.6 1032510/25/12 85-11510/25/12 CQC

12J1059-BS1 26.6 1072510/26/12 85-11510/26/12 CQC

12K0235-BS1 30.9 1242511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 27.3 1092511/8/12 85-11511/8/12 CQC

01/02/13 15:46

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LCS %Ro-XyleneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 25.9 1032511/9/12 85-11511/9/12

12K0415-BS1 26 1042511/12/12 85-11511/12/12 CQC

12K0462-BS1 26.1 1042511/13/12 85-11511/13/12 CQC

12K0522-BS1 26 104X 2511/14/12 85-11511/14/12 CQC

12K0553-BS1 23.4 932511/14/12 85-11511/14/12 CQC

12K0552-BS1 27.1 1082511/14/12 85-11511/14/12 CQC

12K0581-BS1 23.7 952511/15/12 85-11511/15/12 CQC

12K0740-BS1 26.4 1062511/20/12 85-11511/20/12 CQC

12K0751-BS1 27.6 1102511/20/12 85-11511/20/12 CQC

12K0789-BS1 28.3 1132511/20/12 85-11511/20/12

12K0803-BS1 27.7 111X 2511/21/12 85-11511/21/12 CQC

12K0836-BS1 27.7 1112511/21/12 85-11511/21/12 CQC

12K0855-BS1 27.6 1102511/23/12 85-11511/23/12 CQC

12K0865-BS1 26.8 1072511/23/12 85-11511/23/12 CQC

12K0897-BS1 27.3 1092511/24/12 85-11511/24/12 CQC

12K0905-BS1 29.4 1182511/25/12 85-11511/25/12 CQC,PSL

12K1134-BS1 24.3 972511/30/12 85-11511/30/12 CQC

12K1135-BS1 26.6 1062511/30/12 85-11511/30/12 CQC

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LCS/LCSD RPDo-Xylene


9523.8259/1/129/1/1212I0005-BSD1 26.8 107 12 25 CQC

10626.5259/4/129/4/1212I0028-BSD1 25.4 101 4 25 CQC

9222.9259/5/129/5/1212I0081-BSD1 23.8 95 4 25 CQC

9724.2259/7/129/7/1212I0215-BSD1 24 96 0.7 25 CQC

9924.8259/12/129/12/1212I0352-BSD1 26.2 105 5 25 CQC

10125.4259/12/129/12/1212I0394-BSD1 24.2 97 5 25 CQC

10927.3259/18/129/18/1212I0598-BSD1 27.6 110 1 25 CQC

10325.8259/18/129/18/1212I0648-BSD1 25.4 101 2 25 CQC

9022.6259/25/129/25/1212I0926-BSD1 24 96 6 25 CQC

9824.5259/25/129/25/1212I0925-BSD1 24.4 98 0.3 25 CQC

10726.7259/28/129/28/1212I1065-BSD1 25.3 101 5 25 CQC

10325.8259/28/129/28/1212I1095-BSD1 24.3 97 6 25 CQC

9423.6259/29/129/29/1212I1107-BSD1 25.3 101 7 25 CQC

10726.82510/1/1210/1/1212J0008-BSD1 25.7 103 4 25 CQC

9724.32510/8/1210/8/1212J0298-BSD1 23.9 96 2 25

96242510/10/1210/10/1212J0389-BSD1 24.3 97 0.9 25

9924.82510/11/1210/11/1212J0445-BSD1 25 100 0.9 25 CQC

9824.62510/16/1210/16/1212J0620-BSD1 26.3 105 7 25 CQC

9924.82510/18/1210/18/1212J0736-BSD1 25.1 101 1 25 CQC

10526.32510/20/1210/20/1212J0821-BSD1 27.2 109 3 25 CQC

9924.62510/22/1210/22/1212J0850-BSD1 24.5 98 0.7 25 CQC

9523.82510/24/1210/24/1212J0972-BSD1 26.3 105 10 25 CQC

11027.62510/25/1210/25/1212J1010-BSD1 25.4 102 8 25 CQC

108272510/25/1210/25/1212J1038-BSD1 25.6 103 5 25 CQC

11027.52510/26/1210/26/1212J1059-BSD1 26.6 107 3 25 CQC

12731.72511/7/1211/7/1212K0235-BSD1 30.9 124 3 25 CQC,PSL

108272511/8/1211/8/1212K0286-BSD1 27.3 109 1 25 CQC

01/02/13 15:46

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LCS/LCSD RPDo-Xylene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

10626.42511/9/1211/9/1212K0341-BSD1 25.9 103 2 25

10325.92511/12/1211/12/1212K0415-BSD1 26 104 0.5 25 CQC

10726.72511/13/1211/13/1212K0462-BSD1 26.1 104 2 25 CQC

104262511/14/1211/14/1212K0522-BSD1 26 104 0.2 25 CQC

9022.62511/14/1211/14/1212K0553-BSD1 23.4 93 3 25 CQC

10927.32511/14/1211/14/1212K0552-BSD1 27.1 108 0.8 25 CQC

9323.22511/15/1211/15/1212K0581-BSD1 23.7 95 2 25 CQC

10927.22511/20/1211/20/1212K0740-BSD1 26.4 106 3 25 CQC

10826.92511/20/1211/20/1212K0751-BSD1 27.6 110 2 25 CQC

11127.72511/20/1211/20/1212K0789-BSD1 28.3 113 2 25

11027.62511/21/1211/21/1212K0803-BSD1X 27.7 111 0.4 25 CQC

104262511/21/1211/21/1212K0836-BSD1 27.7 111 6 25 CQC

112282511/23/1211/23/1212K0855-BSD1 27.6 110 2 25 CQC

10827.12511/23/1211/23/1212K0865-BSD1 26.8 107 1 25 CQC

11328.42511/24/1211/24/1212K0897-BSD1 27.3 109 4 25 CQC

12330.62511/25/1211/25/1212K0905-BSD1 29.4 118 4 25 CQC,PSL

10325.82511/30/1211/30/1212K1134-BSD1 24.3 97 6 25 CQC

11829.52511/30/1211/30/1212K1135-BSD1 26.6 106 10 25 CQC,PSL

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MS %Ro-Xylene


CQC77.5-122PVH2309-029824.512I0005-MS1 9/1/12 9/1/12 25

CQC77.5-122PVH2309-1110626.612I0028-MS1 9/4/12 9/4/12 25

CQC77.5-122PVH2037-079523.712I0081-MS1 9/5/12 9/5/12 25

CQC77.5-122PVI0290-039924.612I0215-MS1 9/7/12 9/7/12 25

CQC77.5-122PVI0609-0910426.112I0352-MS1 9/12/12 9/12/12 25

CQC77.5-122PVI0525-0610325.712I0394-MS1 9/12/12 9/12/12 25

CQC77.5-122PVI0894-0610626.612I0598-MS1 9/18/12 9/18/12 25

CQC77.5-122PVI1060-0210325.812I0648-MS1 9/18/12 9/18/12 25

CQC77.5-122PVI1553-089724.412I0925-MS1 9/25/12 9/25/12 25

CQC77.5-122PVI1510-089122.712I0926-MS1 9/25/12 9/25/12 25

CQC77.5-122PVI1723-0310426.112I1065-MS1 9/28/12 9/28/12 25

CQC77.5-122PVI1822-029724.312I1095-MS1 9/28/12 9/28/12 25

CQC77.5-122PVI1869-059724.412I1107-MS1 9/29/12 9/29/12 25

CQC77.5-122PVI1575-0110125.112J0008-MS1 10/1/12 10/1/12 25

77.5-122PVJ0513-039824.612J0298-MS1 10/8/12 10/8/12 25

77.5-122PVJ0682-019724.312J0389-MS1 10/10/12 10/10/12 25

CQC77.5-122PVJ0682-179423.512J0445-MS1 10/11/12 10/11/12 25

CQC77.5-122PVJ1065-0210225.412J0620-MS1 10/16/12 10/16/12 25

CQC77.5-122PVJ1237-029924.712J0736-MS1 10/18/12 10/18/12 25

CQC77.5-122PVJ1405-0211328.212J0821-MS1 10/20/12 10/20/12 25

CQC77.5-122PVJ1405-17962412J0850-MS1 10/22/12 10/22/12 25

CQC77.5-122PVJ1577-0210225.512J0972-MS1 10/24/12 10/24/12 25

CQC77.5-122PVJ1627-01 (1070)101132012J1010-MS1 10/25/12 10/25/12 250

CQC77.5-122PVJ1600-0210726.712J1038-MS1 10/25/12 10/25/12 25

CQC77.5-122PVJ1577-18RE111027612J1059-MS1 10/26/12 10/26/12 250

CQC,PSL77.5-122PVK0237-011283212K0235-MS1 11/7/12 11/7/12 25

CQC,M777.5-122PVK0555-0412531.312K0286-MS1 11/8/12 11/8/12 25

77.5-122PVK0649-0610526.412K0341-MS1 11/9/12 11/9/12 25

CQC77.5-122PVK0756-0110927.312K0415-MS1 11/12/12 11/12/12 25

01/02/13 15:46

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MS %Ro-XyleneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC77.5-122PVK0793-0210927.212K0462-MS1 11/13/12 11/13/12 25

CQC77.5-122PVK0281-01 (7.19)8929.5X 12K0522-MS1 11/14/12 11/14/12 25

CQC77.5-122PVK0632-0910125.212K0553-MS1 11/14/12 11/14/12 25

CQC77.5-122PVK0684-0211027.512K0552-MS1 11/14/12 11/14/12 25

CQC77.5-122PVK0696-0110526.312K0581-MS1 11/15/12 11/15/12 25

CQC77.5-122PVK0934-01 (1.55)11229.512K0740-MS1 11/20/12 11/20/12 25

CQC77.5-122PVK0768-0212130.312K0751-MS1 11/20/12 11/20/12 25

CQC77.5-122PVK1220-0210827X 12K0803-MS1 11/21/12 11/21/12 25

CQC77.5-122PVK1288-0311528.712K0836-MS1 11/21/12 11/21/12 25

CQC77.5-122PVK1375-081162912K0865-MS1 11/23/12 11/23/12 25

CQC77.5-122PVK1375-0211027.612K0855-MS1 11/23/12 11/23/12 25

CQC77.5-122PVK0988-0311328.312K0897-MS1 11/24/12 11/24/12 25

CQC,PSL77.5-122PVK1006-0112731.712K0905-MS1 11/25/12 11/25/12 25

CQC77.5-122PVK1450-1010927.212K1135-MS1 11/30/12 11/30/12 25

CQC77.5-122PVK1450-0312230.612K1134-MS1 11/30/12 12/1/12 25

01/02/13 15:46

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MS/MSD RPDo-Xylene


9824.6259/1/129/1/1212I0005-MSD1 CQC250.39824.5 PVH2309-02

10426259/4/129/4/1212I0028-MSD1 CQC25210626.6 PVH2309-11

9423.4259/5/129/5/1212I0081-MSD1 CQC2519523.7 PVH2037-07

10024.9259/7/129/7/1212I0215-MSD1 CQC2519924.6 PVI0290-03

10025.1259/12/129/12/1212I0352-MSD1 CQC25410426.1 PVI0609-09

9724.4259/12/129/12/1212I0394-MSD1 CQC25510325.7 PVI0525-06

10927.1259/18/129/18/1212I0598-MSD1 CQC25210626.6 PVI0894-06

10025259/18/129/18/1212I0648-MSD1 CQC25310325.8 PVI1060-02

9323.2259/25/129/25/1212I0925-MSD1 CQC2559724.4 PVI1553-08

9624.1259/25/129/25/1212I0926-MSD1 CQC2569122.7 PVI1510-08

10827259/28/129/28/1212I1065-MSD1 CQC25410426.1 PVI1723-03

10225.5259/28/129/28/1212I1095-MSD1 CQC2559724.3 PVI1822-02

11027.6259/29/129/29/1212I1107-MSD1 CQC25129724.4 PVI1869-05

100252510/1/1210/1/1212J0008-MSD1 CQC250.410125.1 PVI1575-01

9924.82510/8/1210/8/1212J0298-MSD1 250.69824.6 PVJ0513-03

10125.32510/10/1210/10/1212J0389-MSD1 2549724.3 PVJ0682-01

9122.72510/11/1210/11/1212J0445-MSD1 CQC2539423.5 PVJ0682-17

10225.42510/16/1210/16/1212J0620-MSD1 CQC250.0810225.4 PVJ1065-02

10325.72510/18/1210/18/1212J0736-MSD1 CQC2549924.7 PVJ1237-02

11829.52510/20/1210/20/1212J0821-MSD1 CQC25411328.2 PVJ1405-02

9724.32510/22/1210/22/1212J0850-MSD1 CQC2519624 PVJ1405-17

10225.52510/24/1210/24/1212J0972-MSD1 CQC250.310225.5 PVJ1577-02

83128025010/25/1210/25/1212J1010-MSD1 CQC2531011320 PVJ1627-01 (1070)

10726.62510/25/1210/25/1212J1038-MSD1 CQC250.210726.7 PVJ1600-02

10626625010/26/1210/26/1212J1059-MSD1 CQC254110276 PVJ1577-18RE1

13533.82511/7/1211/7/1212K0235-MSD1 CQC,PSL25512832 PVK0237-01

12431.12511/8/1211/8/1212K0286-MSD1 CQC,M7250.712531.3 PVK0555-04

10225.42511/9/1211/9/1212K0341-MSD1 25410526.4 PVK0649-06

11328.32511/12/1211/12/1212K0415-MSD1 CQC25410927.3 PVK0756-01

10827.12511/13/1211/13/1212K0462-MSD1 CQC250.310927.2 PVK0793-02

9029.72511/14/1211/14/1212K0522-MSD1 CQC250.98929.5 PVK0281-01 (7.19)

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MS/MSD RPDo-Xylene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

9924.82511/14/1211/14/1212K0553-MSD1 CQC25210125.2 PVK0632-09

10927.22511/14/1211/14/1212K0552-MSD1 CQC25111027.5 PVK0684-02

10125.32511/15/1211/15/1212K0581-MSD1 CQC25410526.3 PVK0696-01

10728.22511/20/1211/20/1212K0740-MSD1 CQC25411229.5 PVK0934-01 (1.55)

11829.52511/20/1211/20/1212K0751-MSD1 CQC25212130.3 PVK0768-02

11629.12511/21/1211/21/1212K0803-MSD1X CQC25710827 PVK1220-02

11428.52511/21/1211/21/1212K0836-MSD1 CQC250.911528.7 PVK1288-03

11127.72511/23/1211/23/1212K0865-MSD1 CQC25511629 PVK1375-08

11428.52511/23/1211/23/1212K0855-MSD1 CQC25311027.6 PVK1375-02

124312511/24/1211/24/1212K0897-MSD1 CQC,PSL25911328.3 PVK0988-03

11528.82511/25/1211/25/1212K0905-MSD1 CQC251012731.7 PVK1006-01

11528.92511/30/1211/30/1212K1135-MSD1 CQC25610927.2 PVK1450-10

12631.62512/1/1211/30/1212K1134-MSD1 CQC,M725312230.6 PVK1450-03

01/02/13 15:46

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BLKo-Xylene

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0.0

Plotted: 44

MDL: 0.19

MRL: 1

Rejected: 2

Stdv: 0.0181

Mean: 0.00273

2s: 0.0389

3s: 0.057

~-------------------------------l4s: 0.0751

A 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

01/02/13 15:46

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LCS %Rp-Isopropyltoluene


12K0235-BS1 29.3 1172511/7/12 75.5-11611/7/12 CQC,PSL

12K0286-BS1 25.3 1012511/8/12 75.5-11611/8/12 CQC

12K0341-BS1 25.5 1022511/9/12 75.5-11611/9/12

12K0415-BS1 23.3 932511/12/12 75.5-11611/12/12 CQC

12K0462-BS1 23.9 962511/13/12 75.5-11611/13/12 CQC

12K0522-BS1 25.7 1032511/14/12 75.5-11611/14/12 CQC

12K0803-BS1 25.9 1042511/21/12 75.5-11611/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPDp-Isopropyltoluene


11729.12511/7/1211/7/1212K0235-BSD1 29.3 117 0.6 25 CQC,PSL

10526.22511/8/1211/8/1212K0286-BSD1 25.3 101 4 25 CQC

10024.92511/9/1211/9/1212K0341-BSD1 25.5 102 2 25

9423.62511/12/1211/12/1212K0415-BSD1 23.3 93 1 25 CQC

10225.62511/13/1211/13/1212K0462-BSD1 23.9 96 7 25 CQC

10927.22511/14/1211/14/1212K0522-BSD1 25.7 103 6 25 CQC

10927.12511/21/1211/21/1212K0803-BSD1 25.9 104 5 25 CQC

01/02/13 15:46

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MS %Rp-Isopropyltoluene


CQC67.9-122PVK0237-0111729.212K0235-MS1 11/7/12 11/7/12 25

CQC67.9-122PVK0555-0411629.112K0286-MS1 11/8/12 11/8/12 25

67.9-122PVK0649-06922312K0341-MS1 11/9/12 11/9/12 25

CQC67.9-122PVK0756-019323.412K0415-MS1 11/12/12 11/12/12 25

CQC67.9-122PVK0793-029824.512K0462-MS1 11/13/12 11/13/12 25

CQC67.9-122PVK0281-01 (0.37)10225.812K0522-MS1 11/14/12 11/14/12 25

CQC67.9-122PVK1220-0210726.712K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDp-Isopropyltoluene


12029.92511/7/1211/7/1212K0235-MSD1 CQC25211729.2 PVK0237-01

10626.42511/8/1211/8/1212K0286-MSD1 CQC251011629.1 PVK0555-04

9423.42511/9/1211/9/1212K0341-MSD1 2519223 PVK0649-06

8421.12511/12/1211/12/1212K0415-MSD1 CQC25109323.4 PVK0756-01

10325.72511/13/1211/13/1212K0462-MSD1 CQC2559824.5 PVK0793-02

103262511/14/1211/14/1212K0522-MSD1 CQC250.910225.8 PVK0281-01 (0.37)

12030.12511/21/1211/21/1212K0803-MSD1 CQC251210726.7 PVK1220-02

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BLKp-Isopropyltoluene

01/02/13 15:46

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LCS %Rsec-Butylbenzene


12K0235-BS1 30.6 1222511/7/12 76.7-12111/7/12 CQC,PSL

12K0286-BS1 26.1 1042511/8/12 76.7-12111/8/12 CQC

12K0341-BS1 26.2 1052511/9/12 76.7-12111/9/12

12K0415-BS1 24 962511/12/12 76.7-12111/12/12 CQC

12K0462-BS1 24 962511/13/12 76.7-12111/13/12 CQC

12K0522-BS1 27.5 1102511/14/12 76.7-12111/14/12 CQC

12K0803-BS1 26.9 1082511/21/12 76.7-12111/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPDsec-Butylbenzene


11729.22511/7/1211/7/1212K0235-BSD1 30.6 122 5 25 CQC

10726.82511/8/1211/8/1212K0286-BSD1 26.1 104 3 25 CQC

10526.22511/9/1211/9/1212K0341-BSD1 26.2 105 0.3 25

9624.12511/12/1211/12/1212K0415-BSD1 24 96 0.4 25 CQC

104262511/13/1211/13/1212K0462-BSD1 24 96 8 25 CQC

11027.62511/14/1211/14/1212K0522-BSD1 27.5 110 0.4 25 CQC

112282511/21/1211/21/1212K0803-BSD1 26.9 108 4 25 CQC

01/02/13 15:46

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MS %Rsec-Butylbenzene


CQC73.7-125PVK0237-0112029.912K0235-MS1 11/7/12 11/7/12 25

CQC73.7-125PVK0555-0411829.512K0286-MS1 11/8/12 11/8/12 25

73.7-125PVK0649-06962412K0341-MS1 11/9/12 11/9/12 25

CQC73.7-125PVK0756-019824.612K0415-MS1 11/12/12 11/12/12 25

CQC73.7-125PVK0793-0210225.412K0462-MS1 11/13/12 11/13/12 25

CQC73.7-125PVK0281-01 (0.94)10226.512K0522-MS1 11/14/12 11/14/12 25

CQC73.7-125PVK1220-0211629.112K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDsec-Butylbenzene


12531.22511/7/1211/7/1212K0235-MSD1 CQC25412029.9 PVK0237-01

11428.62511/8/1211/8/1212K0286-MSD1 CQC25311829.5 PVK0555-04

9824.52511/9/1211/9/1212K0341-MSD1 2529624 PVK0649-06

8922.12511/12/1211/12/1212K0415-MSD1 CQC25119824.6 PVK0756-01

104262511/13/1211/13/1212K0462-MSD1 CQC25210225.4 PVK0793-02

10527.22511/14/1211/14/1212K0522-MSD1 CQC25310226.5 PVK0281-01 (0.94)

12531.32511/21/1211/21/1212K0803-MSD1 CQC25811629.1 PVK1220-02

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BLKsec-Butylbenzene

01/02/13 15:46

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LCS %RStyrene


12K0235-BS1 30.7 1232511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 27.8 1112511/8/12 85-11511/8/12 CQC

12K0341-BS1 27 1082511/9/12 85-11511/9/12

12K0415-BS1 25.6 1032511/12/12 85-11511/12/12 CQC

12K0462-BS1 27.2 1092511/13/12 85-11511/13/12 CQC

12K0522-BS1 27.3 1092511/14/12 85-11511/14/12 CQC

12K0803-BS1 27.2 1092511/21/12 85-11511/21/12 CQC

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LCS/LCSD RPDStyrene


12731.72511/7/1211/7/1212K0235-BSD1 30.7 123 3 25 CQC,PSL

11127.82511/8/1211/8/1212K0286-BSD1 27.8 111 0.04 25 CQC

11227.92511/9/1211/9/1212K0341-BSD1 27 108 3 25

9824.52511/12/1211/12/1212K0415-BSD1 25.6 103 5 25 CQC

10927.22511/13/1211/13/1212K0462-BSD1 27.2 109 0 25 CQC

10526.42511/14/1211/14/1212K0522-BSD1 27.3 109 3 25 CQC

11127.82511/21/1211/21/1212K0803-BSD1 27.2 109 2 25 CQC

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MS %RStyrene


CQC55-136PVK0237-011203012K0235-MS1 11/7/12 11/7/12 25

CQC55-136PVK0555-0411328.212K0286-MS1 11/8/12 11/8/12 25

55-136PVK0649-066816.912K0341-MS1 11/9/12 11/9/12 25

CQC55-136PVK0756-01882212K0415-MS1 11/12/12 11/12/12 25

CQC55-136PVK0793-0210726.712K0462-MS1 11/13/12 11/13/12 25

CQC55-136PVK0281-0110225.412K0522-MS1 11/14/12 11/14/12 25

CQC55-136PVK1220-028421.112K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDStyrene


12430.92511/7/1211/7/1212K0235-MSD1 CQC25312030 PVK0237-01

11228.12511/8/1211/8/1212K0286-MSD1 CQC250.411328.2 PVK0555-04

6115.32511/9/1211/9/1212K0341-MSD1 25106816.9 PVK0649-06

8521.12511/12/1211/12/1212K0415-MSD1 CQC2548822 PVK0756-01

10626.42511/13/1211/13/1212K0462-MSD1 CQC25110726.7 PVK0793-02

9624.12511/14/1211/14/1212K0522-MSD1 CQC25510225.4 PVK0281-01

9423.62511/21/1211/21/1212K0803-MSD1 CQC25118421.1 PVK1220-02

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BLKStyrene

01/02/13 15:46

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LCS %Rtert-Butylbenzene


12K0235-BS1 30.4 1212511/7/12 78.9-11711/7/12 CQC,PSL

12K0286-BS1 25.1 1012511/8/12 78.9-11711/8/12 CQC

12K0341-BS1 27.1 1092511/9/12 78.9-11711/9/12

12K0415-BS1 24 962511/12/12 78.9-11711/12/12 CQC

12K0462-BS1 25.2 1012511/13/12 78.9-11711/13/12 CQC

12K0522-BS1 29.2 1172511/14/12 78.9-11711/14/12 CQC

12K0803-BS1 26.7 1072511/21/12 78.9-11711/21/12 CQC

01/02/13 15:46

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LCS/LCSD RPDtert-Butylbenzene


11829.52511/7/1211/7/1212K0235-BSD1 30.4 121 3 25 CQC,PSL

10726.92511/8/1211/8/1212K0286-BSD1 25.1 101 7 25 CQC

10626.52511/9/1211/9/1212K0341-BSD1 27.1 109 2 25

9924.72511/12/1211/12/1212K0415-BSD1 24 96 3 25 CQC

10827.12511/13/1211/13/1212K0462-BSD1 25.2 101 7 25 CQC

12130.22511/14/1211/14/1212K0522-BSD1 29.2 117 3 25 CQC,L

10927.32511/21/1211/21/1212K0803-BSD1 26.7 107 2 25 CQC

01/02/13 15:46

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MS %Rtert-Butylbenzene


CQC76.8-119PVK0237-0111729.212K0235-MS1 11/7/12 11/7/12 25

CQC,M776.8-119PVK0555-0412130.312K0286-MS1 11/8/12 11/8/12 25

76.8-119PVK0649-0611027.512K0341-MS1 11/9/12 11/9/12 25

CQC76.8-119PVK0756-0110325.912K0415-MS1 11/12/12 11/12/12 25

CQC76.8-119PVK0793-0210626.512K0462-MS1 11/13/12 11/13/12 25

CQC76.8-119PVK0281-0110827.112K0522-MS1 11/14/12 11/14/12 25

CQC76.8-119PVK1220-021122812K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDtert-Butylbenzene


12531.32511/7/1211/7/1212K0235-MSD1 CQC,PSL25711729.2 PVK0237-01

116292511/8/1211/8/1212K0286-MSD1 CQC25512130.3 PVK0555-04

10626.42511/9/1211/9/1212K0341-MSD1 25411027.5 PVK0649-06

9623.92511/12/1211/12/1212K0415-MSD1 CQC25810325.9 PVK0756-01

11829.62511/13/1211/13/1212K0462-MSD1 CQC251110626.5 PVK0793-02

10826.92511/14/1211/14/1212K0522-MSD1 CQC250.410827.1 PVK0281-01

12330.92511/21/1211/21/1212K0803-MSD1 CQC,M7251011228 PVK1220-02

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BLKtert-Butylbenzene

01/02/13 15:46

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LCS %RTetrachloroethene


12I0005-BS1 26.2 105259/1/12 85-1159/1/12 CQC

12I0028-BS1 23.1 92259/4/12 85-1159/4/12 CQC

12I0081-BS1 23.3 93259/5/12 85-1159/5/12 CQC

12I0215-BS1 23.3 93259/7/12 85-1159/7/12 CQC

12I0352-BS1 24.5 98259/12/12 85-1159/12/12 CQC

12I0394-BS1 23.9 96259/12/12 85-1159/12/12 CQC

12I0598-BS1 25.6 103259/18/12 85-1159/18/12 CQC

12I0648-BS1 24.6 98259/18/12 85-1159/18/12 CQC

12I0926-BS1 24.3 97259/25/12 85-1159/25/12 CQC

12I0925-BS1 23.5 94259/25/12 85-1159/25/12 CQC

12I1065-BS1 24.9 99259/28/12 85-1159/28/12 CQC

12I1095-BS1 24.8 99259/28/12 85-1159/28/12 CQC

12I1107-BS1 24.7 99259/29/12 85-1159/29/12 CQC

12J0008-BS1 24.3 972510/1/12 85-11510/1/12 CQC

12J0298-BS1 25 1002510/8/12 85-11510/8/12

12J0389-BS1 24.7 992510/10/12 85-11510/10/12

12J0445-BS1 26 1042510/11/12 85-11510/11/12 CQC

12J0620-BS1 26.4 1062510/16/12 85-11510/16/12 CQC

12J0736-BS1 25 1002510/18/12 85-11510/18/12 CQC

12J0821-BS1 25.8 1032510/20/12 85-11510/20/12 CQC

12J0850-BS1 25.3 1012510/22/12 85-11510/22/12 CQC

12J0972-BS1 28.6 1142510/24/12 85-11510/24/12 CQC

12J1010-BS1 26.3 1052510/25/12 85-11510/25/12 CQC

12J1038-BS1 25.4 1022510/25/12 85-11510/25/12 CQC

12J1059-BS1 24.2 972510/26/12 85-11510/26/12 CQC

12K0235-BS1 32.3 1292511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 26.9 1082511/8/12 85-11511/8/12 CQC

01/02/13 15:46

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LCS %RTetrachloroetheneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 30.8 1232511/9/12 85-11511/9/12

12K0415-BS1 24.7 992511/12/12 85-11511/12/12 CQC

12K0462-BS1 25.4 1022511/13/12 85-11511/13/12 CQC

12K0522-BS1 26.8 1072511/14/12 85-11511/14/12 CQC

12K0553-BS1 27 1082511/14/12 85-11511/14/12 CQC

12K0552-BS1 24.6 982511/14/12 85-11511/14/12 CQC

12K0581-BS1 27.6 1112511/15/12 85-11511/15/12 CQC

12K0740-BS1 23.3 932511/20/12 85-11511/20/12 CQC

12K0751-BS1 24.4 972511/20/12 85-11511/20/12 CQC

12K0789-BS1 25.3 1012511/20/12 85-11511/20/12

12K0803-BS1 23.3 932511/21/12 85-11511/21/12 CQC

12K0836-BS1 22.8 912511/21/12 85-11511/21/12 CQC

12K0855-BS1 23.4 942511/23/12 85-11511/23/12 CQC

12K0865-BS1 24.1 962511/23/12 85-11511/23/12 CQC

12K0897-BS1 23.9 962511/24/12 85-11511/24/12 CQC

12K0905-BS1 25.1 1002511/25/12 85-11511/25/12 CQC

12K1134-BS1 20.8 832511/30/12 85-11511/30/12 CQC,PSL

12K1135-BS1 23.8 952511/30/12 85-11511/30/12 CQC

01/02/13 15:46

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LCS/LCSD RPDTetrachloroethene


9222.9259/1/129/1/1212I0005-BSD1 26.2 105 13 25 CQC

9724.3259/4/129/4/1212I0028-BSD1 23.1 92 5 25 CQC

9323.2259/5/129/5/1212I0081-BSD1 23.3 93 0.6 25 CQC

9724.2259/7/129/7/1212I0215-BSD1 23.3 93 4 25 CQC

9423.6259/12/129/12/1212I0352-BSD1 24.5 98 4 25 CQC

9724.1259/12/129/12/1212I0394-BSD1 23.9 96 0.9 25 CQC

10426259/18/129/18/1212I0598-BSD1 25.6 103 1 25 CQC

9724.4259/18/129/18/1212I0648-BSD1 24.6 98 0.7 25 CQC

9222.9259/25/129/25/1212I0926-BSD1 24.3 97 6 25 CQC

9423.6259/25/129/25/1212I0925-BSD1 23.5 94 0.6 25 CQC

10225.4259/28/129/28/1212I1065-BSD1 24.9 99 2 25 CQC

10325.9259/28/129/28/1212I1095-BSD1 24.8 99 4 25 CQC

9222.9259/29/129/29/1212I1107-BSD1 24.7 99 8 25 CQC

10225.62510/1/1210/1/1212J0008-BSD1 24.3 97 5 25 CQC

9924.82510/8/1210/8/1212J0298-BSD1 25 100 0.6 25

10325.72510/10/1210/10/1212J0389-BSD1 24.7 99 4 25

10626.52510/11/1210/11/1212J0445-BSD1 26 104 2 25 CQC

9924.82510/16/1210/16/1212J0620-BSD1 26.4 106 6 25 CQC

10125.22510/18/1210/18/1212J0736-BSD1 25 100 0.7 25 CQC

9924.62510/20/1210/20/1212J0821-BSD1 25.8 103 5 25 CQC

10225.42510/22/1210/22/1212J0850-BSD1 25.3 101 0.4 25 CQC

10325.82510/24/1210/24/1212J0972-BSD1 28.6 114 10 25 CQC

10927.32510/25/1210/25/1212J1010-BSD1 26.3 105 4 25 CQC

11328.22510/25/1210/25/1212J1038-BSD1 25.4 102 11 25 CQC

108272510/26/1210/26/1212J1059-BSD1 24.2 97 11 25 CQC

12731.92511/7/1211/7/1212K0235-BSD1 32.3 129 1 25 CQC,PSL

11127.82511/8/1211/8/1212K0286-BSD1 26.9 108 3 25 CQC

01/02/13 15:46

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LCS/LCSD RPDTetrachloroethene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

12029.92511/9/1211/9/1212K0341-BSD1 30.8 123 3 25

9523.82511/12/1211/12/1212K0415-BSD1 24.7 99 4 25 CQC

10325.72511/13/1211/13/1212K0462-BSD1 25.4 102 1 25 CQC

10927.22511/14/1211/14/1212K0522-BSD1X 26.8 107 1 25 CQC

9824.52511/14/1211/14/1212K0553-BSD1 27 108 10 25 CQC

10325.72511/14/1211/14/1212K0552-BSD1 24.6 98 4 25 CQC

10626.62511/15/1211/15/1212K0581-BSD1 27.6 111 4 25 CQC

96242511/20/1211/20/1212K0740-BSD1 23.3 93 3 25 CQC

96242511/20/1211/20/1212K0751-BSD1 24.4 97 1 25 CQC

9523.82511/20/1211/20/1212K0789-BSD1 25.3 101 6 25

9122.82511/21/1211/21/1212K0803-BSD1X 23.3 93 3 25 CQC

8721.62511/21/1211/21/1212K0836-BSD1 22.8 91 5 25 CQC

9724.22511/23/1211/23/1212K0855-BSD1 23.4 94 3 25 CQC

9724.32511/23/1211/23/1212K0865-BSD1 24.1 96 1 25 CQC

9523.92511/24/1211/24/1212K0897-BSD1 23.9 96 0.3 25 CQC

104262511/25/1211/25/1212K0905-BSD1 25.1 100 4 25 CQC

8822.12511/30/1211/30/1212K1134-BSD1 20.8 83 6 25 CQC

10927.22511/30/1211/30/1212K1135-BSD1 23.8 95 13 25 CQC

01/02/13 15:46

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MS %RTetrachloroethene


CQC77.8-119PVH2309-029423.612I0005-MS1 9/1/12 9/1/12 25

CQC77.8-119PVH2309-1110125.312I0028-MS1 9/4/12 9/4/12 25

CQC77.8-119PVH2037-079122.812I0081-MS1 9/5/12 9/5/12 25

CQC77.8-119PVI0290-039423.512I0215-MS1 9/7/12 9/7/12 25

CQC77.8-119PVI0609-0910125.312I0352-MS1 9/12/12 9/12/12 25

CQC77.8-119PVI0525-06 (7.54)9731.912I0394-MS1 9/12/12 9/12/12 25

CQC77.8-119PVI0894-06 (8.54)10334.312I0598-MS1 9/18/12 9/18/12 25

CQC77.8-119PVI1060-02 (0.46)9825.112I0648-MS1 9/18/12 9/18/12 25

CQC77.8-119PVI1553-089122.712I0925-MS1 9/25/12 9/25/12 25

CQC77.8-119PVI1510-088621.512I0926-MS1 9/25/12 9/25/12 25

CQC77.8-119PVI1723-0310526.212I1065-MS1 9/28/12 9/28/12 25

CQC77.8-119PVI1822-029122.812I1095-MS1 9/28/12 9/28/12 25

CQC77.8-119PVI1869-059523.812I1107-MS1 9/29/12 9/29/12 25

CQC77.8-119PVI1575-019423.412J0008-MS1 10/1/12 10/1/12 25

77.8-119PVJ0513-03 (3.79)1012912J0298-MS1 10/8/12 10/8/12 25

77.8-119PVJ0682-0110125.212J0389-MS1 10/10/12 10/10/12 25

CQC77.8-119PVJ0682-179724.212J0445-MS1 10/11/12 10/11/12 25

CQC77.8-119PVJ1065-021002512J0620-MS1 10/16/12 10/16/12 25

CQC77.8-119PVJ1237-029824.412J0736-MS1 10/18/12 10/18/12 25

CQC77.8-119PVJ1405-0210325.812J0821-MS1 10/20/12 10/20/12 25

CQC77.8-119PVJ1405-179924.912J0850-MS1 10/22/12 10/22/12 25

CQC77.8-119PVJ1577-0211027.412J0972-MS1 10/24/12 10/24/12 25

CQC77.8-119PVJ1627-0111328212J1010-MS1 10/25/12 10/25/12 250

CQC77.8-119PVJ1600-0210526.312J1038-MS1 10/25/12 10/25/12 25

CQC77.8-119PVJ1577-18RE110626612J1059-MS1 10/26/12 10/26/12 250

CQC,PSL77.8-119PVK0237-0112631.412K0235-MS1 11/7/12 11/7/12 25

CQC,M777.8-119PVK0555-0412531.212K0286-MS1 11/8/12 11/8/12 25

77.8-119PVK0649-0611628.912K0341-MS1 11/9/12 11/9/12 25

CQC77.8-119PVK0756-0110626.512K0415-MS1 11/12/12 11/12/12 25

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MS %RTetrachloroetheneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC77.8-119PVK0793-0210325.812K0462-MS1 11/13/12 11/13/12 25

CQC77.8-119PVK0281-0110325.712K0522-MS1 11/14/12 11/14/12 25

CQC77.8-119PVK0632-0910526.212K0553-MS1 11/14/12 11/14/12 25

CQC77.8-119PVK0684-02 (3.63)9928.312K0552-MS1 11/14/12 11/14/12 25

CQC77.8-119PVK0696-0110626.512K0581-MS1 11/15/12 11/15/12 25

CQC77.8-119PVK0934-019323.212K0740-MS1 11/20/12 11/20/12 25

CQC77.8-119PVK0768-02 (0.61)10927.812K0751-MS1 11/20/12 11/20/12 25

CQC77.8-119PVK1220-029323.1X 12K0803-MS1 11/21/12 11/21/12 25

CQC77.8-119PVK1288-039323.312K0836-MS1 11/21/12 11/21/12 25

CQC77.8-119PVK1375-081002512K0865-MS1 11/23/12 11/23/12 25

CQC77.8-119PVK1375-0210125.112K0855-MS1 11/23/12 11/23/12 25

CQC77.8-119PVK0988-039323.212K0897-MS1 11/24/12 11/24/12 25

CQC77.8-119PVK1006-0110125.312K0905-MS1 11/25/12 11/25/12 25

CQC77.8-119PVK1450-109323.312K1135-MS1 11/30/12 11/30/12 25

CQC77.8-119PVK1450-031002512K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDTetrachloroethene


9323.1259/1/129/1/1212I0005-MSD1 CQC2529423.6 PVH2309-02

9724.2259/4/129/4/1212I0028-MSD1 CQC25510125.3 PVH2309-11

8922.2259/5/129/5/1212I0081-MSD1 CQC2529122.8 PVH2037-07

9523.6259/7/129/7/1212I0215-MSD1 CQC250.79423.5 PVI0290-03

9624.1259/12/129/12/1212I0352-MSD1 CQC25510125.3 PVI0609-09

9531.2259/12/129/12/1212I0394-MSD1 CQC2529731.9 PVI0525-06 (7.54)

10133.8259/18/129/18/1212I0598-MSD1 CQC25210334.3 PVI0894-06 (8.54)

9624.5259/18/129/18/1212I0648-MSD1 CQC2529825.1 PVI1060-02 (0.46)

9122.6259/25/129/25/1212I0925-MSD1 CQC250.59122.7 PVI1553-08

8922.2259/25/129/25/1212I0926-MSD1 CQC2538621.5 PVI1510-08

10325.7259/28/129/28/1212I1065-MSD1 CQC25210526.2 PVI1723-03

9624259/28/129/28/1212I1095-MSD1 CQC2559122.8 PVI1822-02

10726.7259/29/129/29/1212I1107-MSD1 CQC25119523.8 PVI1869-05

9724.22510/1/1210/1/1212J0008-MSD1 CQC2539423.4 PVI1575-01

9828.22510/8/1210/8/1212J0298-MSD1 25310129 PVJ0513-03 (3.79)

10526.32510/10/1210/10/1212J0389-MSD1 25410125.2 PVJ0682-01

9724.32510/11/1210/11/1212J0445-MSD1 CQC250.59724.2 PVJ0682-17

100252510/16/1210/16/1212J0620-MSD1 CQC250.0810025 PVJ1065-02

10225.42510/18/1210/18/1212J0736-MSD1 CQC2549824.4 PVJ1237-02

11328.22510/20/1210/20/1212J0821-MSD1 CQC25910325.8 PVJ1405-02

9924.82510/22/1210/22/1212J0850-MSD1 CQC250.49924.9 PVJ1405-17

11528.72510/24/1210/24/1212J0972-MSD1 CQC25411027.4 PVJ1577-02

10826925010/25/1210/25/1212J1010-MSD1 CQC255113282 PVJ1627-01

108272510/25/1210/25/1212J1038-MSD1 CQC25310526.3 PVJ1600-02

11027425010/26/1210/26/1212J1059-MSD1 CQC253106266 PVJ1577-18RE1

12832.12511/7/1211/7/1212K0235-MSD1 CQC,PSL25212631.4 PVK0237-01

12029.92511/8/1211/8/1212K0286-MSD1 CQC,M725412531.2 PVK0555-04

11729.22511/9/1211/9/1212K0341-MSD1 25111628.9 PVK0649-06

10626.62511/12/1211/12/1212K0415-MSD1 CQC250.610626.5 PVK0756-01

10225.42511/13/1211/13/1212K0462-MSD1 CQC25110325.8 PVK0793-02

108272511/14/1211/14/1212K0522-MSD1 CQC25510325.7 PVK0281-01

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MS/MSD RPDTetrachloroethene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

11328.32511/14/1211/14/1212K0553-MSD1 CQC25810526.2 PVK0632-09

9727.82511/14/1211/14/1212K0552-MSD1 CQC2529928.3 PVK0684-02 (3.63)

10526.22511/15/1211/15/1212K0581-MSD1 CQC25110626.5 PVK0696-01

9122.82511/20/1211/20/1212K0740-MSD1 CQC2529323.2 PVK0934-01

10426.72511/20/1211/20/1212K0751-MSD1 CQC25410927.8 PVK0768-02 (0.61)

10225.52511/21/1211/21/1212K0803-MSD1 CQC25109323.1 PVK1220-02

8922.22511/21/1211/21/1212K0836-MSD1 CQC2559323.3 PVK1288-03

10025.12511/23/1211/23/1212K0865-MSD1 CQC250.310025 PVK1375-08

9423.52511/23/1211/23/1212K0855-MSD1 CQC25710125.1 PVK1375-02

9824.52511/24/1211/24/1212K0897-MSD1 CQC2559323.2 PVK0988-03

9623.92511/25/1211/25/1212K0905-MSD1 CQC25510125.3 PVK1006-01

9924.82511/30/1211/30/1212K1135-MSD1 CQC2569323.3 PVK1450-10

108272512/1/1211/30/1212K1134-MSD1 CQC25710025 PVK1450-03

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BLKTetrachloroethene

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0.0

Plotted: 44

MDL: 0.23

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

~------------------------------------------------------------~3•:0 4s: 0

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %RTetrahydrofuran


12K0235-BS1 26.1 1042511/7/12 59.7-14511/7/12 CQC

12K0286-BS1 22.1 892511/8/12 59.7-14511/8/12 CQC

12K0341-BS1 15.2 612511/9/12 59.7-14511/9/12

12K0415-BS1 16.9 672511/12/12 59.7-14511/12/12 CQC

12K0462-BS1 26.3 1052511/13/12 59.7-14511/13/12 CQC

12K0522-BS1 26.3 1052511/14/12 59.7-14511/14/12 CQC

12K0803-BS1 26.5 1062511/21/12 59.7-14511/21/12 CQC

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LCS/LCSD RPDTetrahydrofuran


92232511/7/1211/7/1212K0235-BSD1 26.1 104 13 25 CQC

80202511/8/1211/8/1212K0286-BSD1 22.1 89 10 25 CQC

7518.92511/9/1211/9/1212K0341-BSD1 15.2 61 22 25

72182511/12/1211/12/1212K0415-BSD1 16.9 67 6 25 CQC

9022.52511/13/1211/13/1212K0462-BSD1 26.3 105 16 25 CQC

9924.82511/14/1211/14/1212K0522-BSD1 26.3 105 6 25 CQC

116292511/21/1211/21/1212K0803-BSD1 26.5 106 9 25 CQC

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MS %RTetrahydrofuran


CQC55-148PVK0237-01922312K0235-MS1 11/7/12 11/7/12 25

CQC55-148PVK0555-048019.912K0286-MS1 11/8/12 11/8/12 25

55-148PVK0649-06681712K0341-MS1 11/9/12 11/9/12 25

CQC55-148PVK0756-018120.212K0415-MS1 11/12/12 11/12/12 25

CQC55-148PVK0793-029623.912K0462-MS1 11/13/12 11/13/12 25

CQC55-148PVK0281-018220.412K0522-MS1 11/14/12 11/14/12 25

CQC55-148PVK1220-02882212K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDTetrahydrofuran


9122.82511/7/1211/7/1212K0235-MSD1 CQC250.89223 PVK0237-01

8922.12511/8/1211/8/1212K0286-MSD1 CQC25118019.9 PVK0555-04

6014.92511/9/1211/9/1212K0341-MSD1 25136817 PVK0649-06

7819.62511/12/1211/12/1212K0415-MSD1 CQC2538120.2 PVK0756-01

9523.72511/13/1211/13/1212K0462-MSD1 CQC250.69623.9 PVK0793-02

8922.32511/14/1211/14/1212K0522-MSD1 CQC2598220.4 PVK0281-01

8621.42511/21/1211/21/1212K0803-MSD1 CQC2538822 PVK1220-02

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BLKTetrahydrofuran

01/02/13 15:46

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LCS %RToluene


12I0005-BS1 27.6 110259/1/12 85-1159/1/12 CQC

12I0028-BS1 26.2 105259/4/12 85-1159/4/12 CQC

12I0081-BS1 23.8 95259/5/12 85-1159/5/12 CQC

12I0215-BS1 24.1 96259/7/12 85-1159/7/12 CQC

12I0352-BS1 27.1 108259/12/12 85-1159/12/12 CQC

12I0394-BS1 23.8 95259/12/12 85-1159/12/12 CQC

12I0598-BS1 28.2 113259/18/12 85-1159/18/12 CQC

12I0648-BS1 24.9 100259/18/12 85-1159/18/12 CQC

12I0926-BS1 25.2 101259/25/12 85-1159/25/12 CQC

12I0925-BS1 23.4 94259/25/12 85-1159/25/12 CQC

12I1065-BS1 25.5 102259/28/12 85-1159/28/12 CQC

12I1095-BS1 25 100259/28/12 85-1159/28/12 CQC

12I1107-BS1 25.2 101259/29/12 85-1159/29/12 CQC

12J0008-BS1 24.9 1002510/1/12 85-11510/1/12 CQC

12J0298-BS1 22.8 912510/8/12 85-11510/8/12

12J0389-BS1 22.3 892510/10/12 85-11510/10/12

12J0445-BS1 22.8 912510/11/12 85-11510/11/12 CQC

12J0620-BS1 24.6 982510/16/12 85-11510/16/12 CQC

12J0736-BS1 23 922510/18/12 85-11510/18/12 CQC

12J0821-BS1 25.6 1032510/20/12 85-11510/20/12 CQC

12J0850-BS1 22.6 902510/22/12 85-11510/22/12 CQC

12J0972-BS1 24.4 982510/24/12 85-11510/24/12 CQC

12J1010-BS1 25.4 1022510/25/12 85-11510/25/12 CQC

12J1038-BS1 25.8 1032510/25/12 85-11510/25/12 CQC

12J1059-BS1 26.5 1062510/26/12 85-11510/26/12 CQC

12K0235-BS1 31.7 1272511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 26.9 1082511/8/12 85-11511/8/12 CQC

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LCS %RTolueneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 26.6 1062511/9/12 85-11511/9/12

12K0415-BS1 24.6 982511/12/12 85-11511/12/12 CQC

12K0462-BS1 25.8 1032511/13/12 85-11511/13/12 CQC

12K0522-BS1 26.3 1052511/14/12 85-11511/14/12 CQC

12K0553-BS1 26.8 1072511/14/12 85-11511/14/12 CQC

12K0552-BS1 25.8 1032511/14/12 85-11511/14/12 CQC

12K0581-BS1 25.7 1032511/15/12 85-11511/15/12 CQC

12K0740-BS1 24.9 992511/20/12 85-11511/20/12 CQC

12K0751-BS1 25.6 1022511/20/12 85-11511/20/12 CQC

12K0789-BS1 27.1 1092511/20/12 85-11511/20/12

12K0803-BS1 24.4 982511/21/12 85-11511/21/12 CQC

12K0836-BS1 25.1 1012511/21/12 85-11511/21/12 CQC

12K0855-BS1 26 1042511/23/12 85-11511/23/12 CQC

12K0865-BS1 25.6 1022511/23/12 85-11511/23/12 CQC

12K0897-BS1 27 1082511/24/12 85-11511/24/12 CQC

12K0905-BS1 28.7 1152511/25/12 85-11511/25/12 CQC

12K1134-BS1 24.7 992511/30/12 85-11511/30/12 CQC

12K1135-BS1 24.6 992511/30/12 85-11511/30/12 CQC

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LCS/LCSD RPDToluene


9724.3259/1/129/1/1212I0005-BSD1 27.6 110 13 25 CQC

11027.5259/4/129/4/1212I0028-BSD1 26.2 105 5 25 CQC

9724.2259/5/129/5/1212I0081-BSD1 23.8 95 2 25 CQC

9323.4259/7/129/7/1212I0215-BSD1 24.1 96 3 25 CQC

10526.3259/12/129/12/1212I0352-BSD1 27.1 108 3 25 CQC

9824.5259/12/129/12/1212I0394-BSD1 23.8 95 3 25 CQC

11328.2259/18/129/18/1212I0598-BSD1 28.2 113 0.1 25 CQC

9724.1259/18/129/18/1212I0648-BSD1 24.9 100 3 25 CQC

9523.7259/25/129/25/1212I0926-BSD1 25.2 101 6 25 CQC

9423.5259/25/129/25/1212I0925-BSD1 23.4 94 0.3 25 CQC

10526.4259/28/129/28/1212I1065-BSD1 25.5 102 3 25 CQC

10225.6259/28/129/28/1212I1095-BSD1 25 100 2 25 CQC

9824.5259/29/129/29/1212I1107-BSD1 25.2 101 3 25 CQC

10325.72510/1/1210/1/1212J0008-BSD1 24.9 100 3 25 CQC

9022.62510/8/1210/8/1212J0298-BSD1 22.8 91 1 25

9022.52510/10/1210/10/1212J0389-BSD1 22.3 89 0.9 25

9423.52510/11/1210/11/1212J0445-BSD1 22.8 91 3 25 CQC

100252510/16/1210/16/1212J0620-BSD1 24.6 98 2 25 CQC

9222.92510/18/1210/18/1212J0736-BSD1 23 92 0.6 25 CQC

10225.42510/20/1210/20/1212J0821-BSD1 25.6 103 1 25 CQC

9022.52510/22/1210/22/1212J0850-BSD1 22.6 90 0.4 25 CQC

9022.52510/24/1210/24/1212J0972-BSD1 24.4 98 8 25 CQC

10325.82510/25/1210/25/1212J1010-BSD1 25.4 102 2 25 CQC

10426.12510/25/1210/25/1212J1038-BSD1 25.8 103 1 25 CQC

9824.62510/26/1210/26/1212J1059-BSD1 26.5 106 8 25 CQC

12230.62511/7/1211/7/1212K0235-BSD1 31.7 127 4 25 CQC,PSL

11528.62511/8/1211/8/1212K0286-BSD1 26.9 108 6 25 CQC

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LCS/LCSD RPDToluene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

10526.32511/9/1211/9/1212K0341-BSD1 26.6 106 1 25

10225.52511/12/1211/12/1212K0415-BSD1 24.6 98 4 25 CQC

10526.22511/13/1211/13/1212K0462-BSD1 25.8 103 1 25 CQC

10426.12511/14/1211/14/1212K0522-BSD1X 26.3 105 0.8 25 CQC

8721.82511/14/1211/14/1212K0553-BSD1 26.8 107 21 25 CQC

10325.72511/14/1211/14/1212K0552-BSD1 25.8 103 0.2 25 CQC

9523.62511/15/1211/15/1212K0581-BSD1 25.7 103 8 25 CQC

10325.72511/20/1211/20/1212K0740-BSD1 24.9 99 3 25 CQC

9824.62511/20/1211/20/1212K0751-BSD1 25.6 102 4 25 CQC

10526.32511/20/1211/20/1212K0789-BSD1 27.1 109 3 25

10526.32511/21/1211/21/1212K0803-BSD1X 24.4 98 7 25 CQC

9924.72511/21/1211/21/1212K0836-BSD1 25.1 101 2 25 CQC

10526.22511/23/1211/23/1212K0855-BSD1 26 104 0.7 25 CQC

10225.62511/23/1211/23/1212K0865-BSD1 25.6 102 0.1 25 CQC

10626.52511/24/1211/24/1212K0897-BSD1 27 108 2 25 CQC

11528.72511/25/1211/25/1212K0905-BSD1 28.7 115 0.2 25 CQC

96242511/30/1211/30/1212K1134-BSD1 24.7 99 3 25 CQC

11127.82511/30/1211/30/1212K1135-BSD1 24.6 99 12 25 CQC

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MS %RToluene


CQC83-118PVH2309-0210425.912I0005-MS1 9/1/12 9/1/12 25

CQC83-118PVH2309-1111428.512I0028-MS1 9/4/12 9/4/12 25

CQC83-118PVH2037-079323.212I0081-MS1 9/5/12 9/5/12 25

CQC83-118PVI0290-0310325.812I0215-MS1 9/7/12 9/7/12 25

CQC83-118PVI0609-0910827.112I0352-MS1 9/12/12 9/12/12 25

CQC83-118PVI0525-0610025.112I0394-MS1 9/12/12 9/12/12 25

CQC83-118PVI0894-061122812I0598-MS1 9/18/12 9/18/12 25

CQC83-118PVI1060-029924.812I0648-MS1 9/18/12 9/18/12 25

CQC83-118PVI1553-089523.712I0925-MS1 9/25/12 9/25/12 25

CQC83-118PVI1510-089623.912I0926-MS1 9/25/12 9/25/12 25

CQC83-118PVI1723-0310927.212I1065-MS1 9/28/12 9/28/12 25

CQC83-118PVI1822-029724.212I1095-MS1 9/28/12 9/28/12 25

CQC83-118PVI1869-0510425.912I1107-MS1 9/29/12 9/29/12 25

CQC83-118PVI1575-0110225.512J0008-MS1 10/1/12 10/1/12 25

83-118PVJ0513-039122.712J0298-MS1 10/8/12 10/8/12 25

83-118PVJ0682-019323.312J0389-MS1 10/10/12 10/10/12 25

CQC83-118PVJ0682-178621.412J0445-MS1 10/11/12 10/11/12 25

CQC83-118PVJ1065-029724.112J0620-MS1 10/16/12 10/16/12 25

CQC83-118PVJ1237-029122.812J0736-MS1 10/18/12 10/18/12 25

CQC83-118PVJ1405-021122812J0821-MS1 10/20/12 10/20/12 25

CQC83-118PVJ1405-178922.312J0850-MS1 10/22/12 10/22/12 25

CQC83-118PVJ1577-029423.412J0972-MS1 10/24/12 10/24/12 25

CQC,M183-118PVJ1627-01 (1450)130177012J1010-MS1 10/25/12 10/25/12 250

CQC83-118PVJ1600-0210526.312J1038-MS1 10/25/12 10/25/12 25

CQC83-118PVJ1577-18RE111027612J1059-MS1 10/26/12 10/26/12 250

CQC,PSL83-118PVK0237-0112832.112K0235-MS1 11/7/12 11/7/12 25

CQC,M783-118PVK0555-0412631.612K0286-MS1 11/8/12 11/8/12 25

83-118PVK0649-0610626.412K0341-MS1 11/9/12 11/9/12 25

CQC83-118PVK0756-0110526.212K0415-MS1 11/12/12 11/12/12 25

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MS %RTolueneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC83-118PVK0793-0211227.912K0462-MS1 11/13/12 11/13/12 25

CQC83-118PVK0281-01 (0.44)10225.9X 12K0522-MS1 11/14/12 11/14/12 25

CQC83-118PVK0632-09922312K0553-MS1 11/14/12 11/14/12 25

CQC83-118PVK0684-0210125.112K0552-MS1 11/14/12 11/14/12 25

CQC83-118PVK0696-019323.412K0581-MS1 11/15/12 11/15/12 25

CQC83-118PVK0934-0110125.312K0740-MS1 11/20/12 11/20/12 25

CQC83-118PVK0768-0211328.312K0751-MS1 11/20/12 11/20/12 25

CQC83-118PVK1220-0210025.1X 12K0803-MS1 11/21/12 11/21/12 25

CQC83-118PVK1288-0310626.412K0836-MS1 11/21/12 11/21/12 25

CQC83-118PVK1375-081082712K0865-MS1 11/23/12 11/23/12 25

CQC83-118PVK1375-0210526.412K0855-MS1 11/23/12 11/23/12 25

CQC83-118PVK0988-031122812K0897-MS1 11/24/12 11/24/12 25

CQC83-118PVK1006-0111729.412K0905-MS1 11/25/12 11/25/12 25

CQC83-118PVK1450-10 (1.77)10327.412K1135-MS1 11/30/12 11/30/12 25

CQC,M783-118PVK1450-0311929.712K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDToluene


10425.9259/1/129/1/1212I0005-MSD1 CQC250.0410425.9 PVH2309-02

11127.7259/4/129/4/1212I0028-MSD1 CQC25311428.5 PVH2309-11

9824.4259/5/129/5/1212I0081-MSD1 CQC2559323.2 PVH2037-07

10025259/7/129/7/1212I0215-MSD1 CQC25310325.8 PVI0290-03

10426259/12/129/12/1212I0352-MSD1 CQC25410827.1 PVI0609-09

9624.1259/12/129/12/1212I0394-MSD1 CQC25410025.1 PVI0525-06

11228259/18/129/18/1212I0598-MSD1 CQC250.311228 PVI0894-06

10426259/18/129/18/1212I0648-MSD1 CQC2559924.8 PVI1060-02

9323.2259/25/129/25/1212I0925-MSD1 CQC2529523.7 PVI1553-08

9924.8259/25/129/25/1212I0926-MSD1 CQC2549623.9 PVI1510-08

10425.9259/28/129/28/1212I1065-MSD1 CQC25510927.2 PVI1723-03

10325.6259/28/129/28/1212I1095-MSD1 CQC2569724.2 PVI1822-02

11629.1259/29/129/29/1212I1107-MSD1 CQC251110425.9 PVI1869-05

10325.82510/1/1210/1/1212J0008-MSD1 CQC25110225.5 PVI1575-01

9122.82510/8/1210/8/1212J0298-MSD1 250.49122.7 PVJ0513-03

92232510/10/1210/10/1212J0389-MSD1 250.99323.3 PVJ0682-01

8621.52510/11/1210/11/1212J0445-MSD1 CQC250.78621.4 PVJ0682-17

10024.92510/16/1210/16/1212J0620-MSD1 CQC2539724.1 PVJ1065-02

9423.42510/18/1210/18/1212J0736-MSD1 CQC2539122.8 PVJ1237-02

12029.92510/20/1210/20/1212J0821-MSD1 CQC,PSL25711228 PVJ1405-02

88222510/22/1210/22/1212J0850-MSD1 CQC2518922.3 PVJ1405-17

10025.12510/24/1210/24/1212J0972-MSD1 CQC2579423.4 PVJ1577-02

121175025010/25/1210/25/1212J1010-MSD1 CQC,M12511301770 PVJ1627-01 (1450)

10927.32510/25/1210/25/1212J1038-MSD1 CQC25410526.3 PVJ1600-02

11127825010/26/1210/26/1212J1059-MSD1 CQC250.6110276 PVJ1577-18RE1

13934.82511/7/1211/7/1212K0235-MSD1 CQC,M725812832.1 PVK0237-01

12531.22511/8/1211/8/1212K0286-MSD1 CQC,M725112631.6 PVK0555-04

10225.42511/9/1211/9/1212K0341-MSD1 25410626.4 PVK0649-06

10526.22511/12/1211/12/1212K0415-MSD1 CQC250.0810526.2 PVK0756-01

10826.92511/13/1211/13/1212K0462-MSD1 CQC25411227.9 PVK0793-02

11128.12511/14/1211/14/1212K0522-MSD1X CQC25810225.9 PVK0281-01 (0.44)

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MS/MSD RPDToluene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

10927.22511/14/1211/14/1212K0553-MSD1 CQC25169223 PVK0632-09

11027.52511/14/1211/14/1212K0552-MSD1 CQC25910125.1 PVK0684-02

9423.62511/15/1211/15/1212K0581-MSD1 CQC250.99323.4 PVK0696-01

10225.52511/20/1211/20/1212K0740-MSD1 CQC25110125.3 PVK0934-01

11328.22511/20/1211/20/1212K0751-MSD1 CQC250.211328.3 PVK0768-02

11228.12511/21/1211/21/1212K0803-MSD1X CQC251110025.1 PVK1220-02

104262511/21/1211/21/1212K0836-MSD1 CQC25210626.4 PVK1288-03

10526.32511/23/1211/23/1212K0865-MSD1 CQC25310827 PVK1375-08

104262511/23/1211/23/1212K0855-MSD1 CQC25110526.4 PVK1375-02

11127.82511/24/1211/24/1212K0897-MSD1 CQC250.611228 PVK0988-03

116292511/25/1211/25/1212K0905-MSD1 CQC25111729.4 PVK1006-01

10828.92511/30/1211/30/1212K1135-MSD1 CQC25510327.4 PVK1450-10 (1.77)

11428.52512/1/1211/30/1212K1134-MSD1 CQC25411929.7 PVK1450-03

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BLKToluene

1.0 r-------------------------------------------------------~

0.9

0.8

0.7

0.6

0.5

Plotted: 44

MDL: 0.35

MRL: 1

Rejected: 2

Stdv: 0.02

Mean: 0.00432 0.4

0.3 l------------------------------------i 2s: 0.0444

3s: 0.0645

0.2 4s: 0.0845

0.1 · · · · · · A · · · · ·fi ·

0.0 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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%R in BLKToluene-d8


12I0005-BLK1 26.2259/1/12 105 88.4-1119/1/12 CQC

12I0028-BLK1 24.8259/4/12 99 88.4-1119/4/12 CQC

12I0081-BLK1 25.4259/5/12 101 88.4-1119/5/12 CQC

12I0215-BLK1 25.2259/7/12 101 88.4-1119/7/12 CQC

12I0352-BLK1 26.2259/12/12 105 88.4-1119/12/12 CQC

12I0394-BLK1 25.1259/12/12 100 88.4-1119/12/12 CQC

12I0598-BLK1 26.1259/18/12 104 88.4-1119/18/12 CQC

12I0648-BLK1 24259/18/12 96 88.4-1119/18/12 CQC

12I0926-BLK1 25.4259/25/12 102 88.4-1119/25/12 CQC

12I0925-BLK1 26.1259/25/12 104 88.4-1119/25/12 CQC

12I1065-BLK1 26259/28/12 104 88.4-1119/28/12 CQC

12I1095-BLK1 27.4259/28/12 110 88.4-1119/28/12 CQC

12I1107-BLK1 26.5259/29/12 106 88.4-1119/29/12 CQC

12J0008-BLK1 282510/1/12 112 88.4-11110/1/12 CQC,PSL

12J0298-BLK1 26.62510/8/12 106 88.4-11110/8/12

12J0389-BLK1 262510/10/12 104 88.4-11110/10/12

12J0445-BLK1 26.32510/11/12 105 88.4-11110/11/12 CQC

12J0620-BLK1 25.42510/16/12 101 88.4-11110/16/12 CQC

12J0736-BLK1 26.52510/18/12 106 88.4-11110/18/12 CQC

12J0821-BLK1 24.52510/20/12 98 88.4-11110/20/12 CQC

12J0850-BLK1 26.52510/22/12 106 88.4-11110/22/12 CQC

12J0972-BLK1 26.32510/24/12 105 88.4-11110/24/12 CQC

12J1010-BLK1 27.62510/25/12 110 88.4-11110/25/12 CQC

12J1038-BLK1 272510/25/12 108 88.4-11110/25/12 CQC

12J1059-BLK1 26.62510/26/12 107 88.4-11110/26/12 CQC

12K0235-BLK1 26.92511/7/12 108 88.4-11111/7/12 CQC

12K0286-BLK1 26.22511/8/12 105 88.4-11111/8/12 CQC

12K0341-BLK1 25.82511/9/12 103 88.4-11111/9/12

12K0415-BLK1 292511/12/12 116 88.4-11111/12/12 CQC,PSL

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%R in BLKToluene-d8Limits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

12K0462-BLK1 29.22511/13/12 117 88.4-11111/13/12 CQC,PSL

X 12K0522-BLK1 27.52511/14/12 110 88.4-11111/14/12 CQC

12K0552-BLK1 28.42511/14/12 114 88.4-11111/14/12 CQC,PSL

12K0553-BLK1 27.82511/14/12 111 88.4-11111/14/12 CQC

12K0581-BLK1 262511/15/12 104 88.4-11111/15/12 CQC

12K0740-BLK1 28.22511/20/12 113 88.4-11111/20/12 CQC,PSL

12K0751-BLK1 28.32511/20/12 113 88.4-11111/20/12 CQC,PSL

X 12K0803-BLK1 27.62511/21/12 110 88.4-11111/21/12 CQC

12K0836-BLK1 27.92511/21/12 111 88.4-11111/21/12 CQC

12K0865-BLK1 27.72511/23/12 111 88.4-11111/23/12 CQC

12K0855-BLK1 28.52511/23/12 114 88.4-11111/23/12 CQC,PSL

12K0897-BLK1 28.42511/24/12 114 88.4-11111/24/12 CQC,PSL

12K0905-BLK1 29.82511/25/12 119 88.4-11111/25/12 CQC

12K1134-BLK1 28.42511/30/12 114 88.4-11111/30/12 CQC,PSL

12K1135-BLK1 27.82511/30/12 111 88.4-11111/30/12 CQC

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%R In BS/BSDToluene-d8


12I0005-BS1 26.4259/1/12 105 88.4-1119/1/12 CQC

12I0005-BSD1 26.8259/1/12 107 88.4-1119/1/12 CQC

12I0028-BS1 25.5259/4/12 102 88.4-1119/4/12 CQC

12I0028-BSD1 25259/4/12 100 88.4-1119/4/12 CQC

12I0081-BS1 24.9259/5/12 100 88.4-1119/5/12 CQC

12I0081-BSD1 24.9259/5/12 99 88.4-1119/5/12 CQC

12I0215-BS1 24.2259/7/12 97 88.4-1119/7/12 CQC

12I0215-BSD1 24259/7/12 96 88.4-1119/7/12 CQC

12I0352-BS1 26.7259/12/12 107 88.4-1119/12/12 CQC

12I0352-BSD1 26.6259/12/12 106 88.4-1119/12/12 CQC

12I0394-BS1 24.8259/12/12 99 88.4-1119/12/12 CQC

12I0394-BSD1 26.3259/12/12 105 88.4-1119/12/12 CQC

12I0598-BS1 26.6259/18/12 106 88.4-1119/18/12 CQC

12I0598-BSD1 26.6259/18/12 106 88.4-1119/18/12 CQC

12I0648-BS1 24.1259/18/12 96 88.4-1119/18/12 CQC

12I0648-BSD1 23.4259/18/12 94 88.4-1119/18/12 CQC

12I0926-BS1 25.8259/25/12 103 88.4-1119/25/12 CQC

12I0925-BS1 25.2259/25/12 101 88.4-1119/25/12 CQC

12I0926-BSD1 25.6259/25/12 103 88.4-1119/25/12 CQC

12I0925-BSD1 25.8259/25/12 103 88.4-1119/25/12 CQC

12I1065-BS1 26.8259/28/12 107 88.4-1119/28/12 CQC

12I1065-BSD1 27.7259/28/12 111 88.4-1119/28/12 CQC

12I1095-BS1 27.1259/28/12 109 88.4-1119/28/12 CQC

12I1095-BSD1 26.8259/28/12 107 88.4-1119/28/12 CQC

12I1107-BS1 27259/29/12 108 88.4-1119/29/12 CQC

12I1107-BSD1 27.6259/29/12 110 88.4-1119/29/12 CQC

12J0008-BS1 272510/1/12 108 88.4-11110/1/12 CQC

12J0008-BSD1 27.42510/1/12 109 88.4-11110/1/12 CQC

12J0298-BS1 26.82510/8/12 107 88.4-11110/8/12

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%R In BS/BSDToluene-d8Limits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

12J0298-BSD1 26.52510/8/12 106 88.4-11110/8/12

12J0389-BS1 272510/10/12 108 88.4-11110/10/12

12J0389-BSD1 26.62510/10/12 106 88.4-11110/10/12

12J0445-BS1 26.22510/11/12 105 88.4-11110/11/12 CQC

12J0445-BSD1 26.82510/11/12 107 88.4-11110/11/12 CQC

12J0620-BS1 25.82510/16/12 103 88.4-11110/16/12 CQC

12J0620-BSD1 25.72510/16/12 103 88.4-11110/16/12 CQC

12J0736-BS1 26.62510/18/12 107 88.4-11110/18/12 CQC

12J0736-BSD1 26.52510/18/12 106 88.4-11110/18/12 CQC

12J0821-BS1 25.22510/20/12 101 88.4-11110/20/12 CQC

12J0821-BSD1 25.42510/20/12 102 88.4-11110/20/12 CQC

12J0850-BS1 26.82510/22/12 107 88.4-11110/22/12 CQC

12J0850-BSD1 272510/22/12 108 88.4-11110/22/12 CQC

12J0972-BS1 26.62510/24/12 106 88.4-11110/24/12 CQC

12J0972-BSD1 26.62510/24/12 106 88.4-11110/24/12 CQC

12J1010-BS1 27.12510/25/12 108 88.4-11110/25/12 CQC

12J1010-BSD1 27.12510/25/12 108 88.4-11110/25/12 CQC

12J1038-BS1 27.92510/25/12 111 88.4-11110/25/12 CQC

12J1038-BSD1 27.42510/25/12 110 88.4-11110/25/12 CQC

12J1059-BS1 272510/26/12 108 88.4-11110/26/12 CQC

12J1059-BSD1 26.62510/26/12 106 88.4-11110/26/12 CQC

12K0235-BS1 27.12511/7/12 108 88.4-11111/7/12 CQC

12K0235-BSD1 27.82511/7/12 111 88.4-11111/7/12 CQC

12K0286-BS1 26.42511/8/12 105 88.4-11111/8/12 CQC

12K0286-BSD1 272511/8/12 108 88.4-11111/8/12 CQC

12K0341-BSD1 25.42511/9/12 102 88.4-11111/9/12

12K0341-BS1 25.22511/9/12 101 88.4-11111/9/12

12K0415-BS1 29.22511/12/12 117 88.4-11111/12/12 CQC,PSL

12K0415-BSD1 29.72511/12/12 119 88.4-11111/12/12 CQC,PSL

12K0462-BS1 28.52511/13/12 114 88.4-11111/13/12 CQC,PSL

12K0462-BSD1 27.62511/13/12 110 88.4-11111/13/12 CQC

X 12K0522-BS1 26.32511/14/12 105 88.4-11111/14/12 CQC

X 12K0522-BSD1 26.72511/14/12 107 88.4-11111/14/12 CQC

12K0553-BS1 29.12511/14/12 116 88.4-11111/14/12 CQC,PSL

12K0552-BS1 29.42511/14/12 117 88.4-11111/14/12 CQC,PSL

12K0553-BSD1 25.82511/14/12 103 88.4-11111/14/12 CQC

12K0552-BSD1 282511/14/12 112 88.4-11111/14/12 CQC,PSL

12K0581-BS1 27.32511/15/12 109 88.4-11111/15/12 CQC

12K0581-BSD1 26.82511/15/12 107 88.4-11111/15/12 CQC

12K0740-BS1 292511/20/12 116 88.4-11111/20/12 CQC,PSL

12K0751-BS1 28.42511/20/12 114 88.4-11111/20/12 CQC,PSL

12K0740-BSD1 27.92511/20/12 112 88.4-11111/20/12 CQC,PSL

12K0751-BSD1 28.22511/20/12 113 88.4-11111/20/12 CQC,PSL

12K0789-BS1 28.22511/20/12 113 88.4-11111/20/12

12K0789-BSD1 28.62511/20/12 114 88.4-11111/20/12

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%R In BS/BSDToluene-d8Limits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

12K0803-BS1 28.52511/21/12 114 88.4-11111/21/12 CQC,PSL

X 12K0803-BSD1 28.52511/21/12 114 88.4-11111/21/12 CQC,PSL

12K0836-BS1 28.22511/21/12 113 88.4-11111/21/12 CQC,PSL

12K0836-BSD1 28.12511/21/12 112 88.4-11111/21/12 CQC,PSL

12K0855-BS1 27.92511/23/12 112 88.4-11111/23/12 CQC,PSL

12K0865-BS1 28.52511/23/12 114 88.4-11111/23/12 CQC,PSL

12K0855-BSD1 28.62511/23/12 114 88.4-11111/23/12 CQC,PSL

12K0865-BSD1 28.82511/23/12 115 88.4-11111/23/12 CQC,PSL

12K0897-BS1 30.12511/24/12 120 88.4-11111/24/12 CQC,PSL

12K0897-BSD1 28.92511/24/12 116 88.4-11111/24/12 CQC,PSL

12K0905-BS1 28.82511/25/12 115 88.4-11111/25/12 CQC

12K0905-BSD1 28.82511/25/12 115 88.4-11111/25/12 CQC

12K1134-BS1 29.32511/30/12 117 88.4-11111/30/12 CQC,PSL

12K1134-BSD1 28.42511/30/12 114 88.4-11111/30/12 CQC,PSL

12K1135-BS1 27.62511/30/12 110 88.4-11111/30/12 CQC

12K1135-BSD1 282511/30/12 112 88.4-11111/30/12 CQC,PSL

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%R in MS/MSDToluene-d8


10726.7259/1/1212I0005-MS1 CQC88.4-111PVH2309-029/1/12

10726.8259/1/1212I0005-MSD1X CQC88.4-111PVH2309-029/1/12

10225.4259/4/1212I0028-MS1 CQC88.4-111PVH2309-119/4/12

10125.4259/4/1212I0028-MSD1X CQC88.4-111PVH2309-119/4/12

10225.6259/5/1212I0081-MS1 CQC88.4-111PVH2037-079/5/12

10325.9259/5/1212I0081-MSD1X CQC88.4-111PVH2037-079/5/12

9724.2259/7/1212I0215-MS1 CQC88.4-111PVI0290-039/7/12

9824.6259/7/1212I0215-MSD1X CQC88.4-111PVI0290-039/7/12

10726.6259/12/1212I0352-MS1 CQC88.4-111PVI0609-099/12/12

10626.5259/12/1212I0352-MSD1X CQC88.4-111PVI0609-099/12/12

10125.3259/12/1212I0394-MS1 CQC88.4-111PVI0525-069/12/12

9924.8259/12/1212I0394-MSD1X CQC88.4-111PVI0525-069/12/12

10526.3259/18/1212I0598-MS1 CQC88.4-111PVI0894-069/18/12

10626.6259/18/1212I0598-MSD1X CQC88.4-111PVI0894-069/18/12

9423.5259/18/1212I0648-MS1 CQC88.4-111PVI1060-029/18/12

10025259/18/1212I0648-MSD1X CQC88.4-111PVI1060-029/18/12

10726.8259/25/1212I0925-MS1 CQC88.4-111PVI1553-089/25/12

10526.4259/25/1212I0925-MSD1X CQC88.4-111PVI1553-089/25/12

10325.7259/25/1212I0926-MS1 CQC88.4-111PVI1510-089/25/12

10426259/25/1212I0926-MSD1X CQC88.4-111PVI1510-089/25/12

10927.2259/28/1212I1065-MS1 CQC88.4-111PVI1723-039/28/12

10526.2259/28/1212I1065-MSD1X CQC88.4-111PVI1723-039/28/12

11027.4259/28/1212I1095-MS1 CQC88.4-111PVI1822-029/28/12

10927.3259/28/1212I1095-MSD1X CQC88.4-111PVI1822-029/28/12

11228259/29/1212I1107-MS1 CQC,PSL88.4-111PVI1869-059/29/12

11027.4259/29/1212I1107-MSD1X CQC88.4-111PVI1869-059/29/12

11328.22510/1/1212J0008-MS1 CQC,PSL88.4-111PVI1575-0110/1/12

10827.12510/1/1212J0008-MSD1X CQC88.4-111PVI1575-0110/1/12

10626.62510/8/1212J0298-MS1 88.4-111PVJ0513-0310/8/12

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%R in MS/MSDToluene-d8Source QualifiersLimitsSample ID Prepared Spike Level Result %RRjct Analyzed

10626.42510/8/1212J0298-MSD1X 88.4-111PVJ0513-0310/8/12

10526.32510/10/1212J0389-MS1 88.4-111PVJ0682-0110/10/12

10526.32510/10/1212J0389-MSD1X 88.4-111PVJ0682-0110/10/12

9824.52510/11/1212J0445-MS1 CQC88.4-111PVJ0682-1710/11/12

9824.62510/11/1212J0445-MSD1X CQC88.4-111PVJ0682-1710/11/12

10225.52510/16/1212J0620-MS1 CQC88.4-111PVJ1065-0210/16/12

10225.62510/16/1212J0620-MSD1X CQC88.4-111PVJ1065-0210/16/12

100252510/18/1212J0736-MS1 CQC88.4-111PVJ1237-0210/18/12

9924.72510/18/1212J0736-MSD1X CQC88.4-111PVJ1237-0210/18/12

10125.32510/20/1212J0821-MS1 CQC88.4-111PVJ1405-0210/20/12

10125.32510/20/1212J0821-MSD1X CQC88.4-111PVJ1405-0210/20/12

10526.32510/22/1212J0850-MS1 CQC88.4-111PVJ1405-1710/22/12

10626.62510/22/1212J0850-MSD1X CQC88.4-111PVJ1405-1710/22/12

10526.32510/24/1212J0972-MS1 CQC88.4-111PVJ1577-0210/24/12

10927.22510/24/1212J0972-MSD1X CQC88.4-111PVJ1577-0210/24/12

108272510/25/1212J1010-MS1 CQC88.4-111PVJ1627-0110/25/12

10626.62510/25/1212J1010-MSD1X CQC88.4-111PVJ1627-0110/25/12

10927.22510/25/1212J1038-MS1 CQC88.4-111PVJ1600-0210/25/12

11428.62510/25/1212J1038-MSD1X CQC,PSL88.4-111PVJ1600-0210/25/12

11127.82510/26/1212J1059-MS1 CQC88.4-111PVJ1577-18RE110/26/12

11328.22510/26/1212J1059-MSD1X CQC,PSL88.4-111PVJ1577-18RE110/26/12

10826.92511/7/1212K0235-MS1 CQC88.4-111PVK0237-0111/7/12

10927.32511/7/1212K0235-MSD1X CQC88.4-111PVK0237-0111/7/12

10827.12511/8/1212K0286-MS1 CQC88.4-111PVK0555-0411/8/12

10626.62511/8/1212K0286-MSD1X CQC88.4-111PVK0555-0411/8/12

10225.62511/9/1212K0341-MS1 88.4-111PVK0649-0611/9/12

9924.62511/9/1212K0341-MSD1X 88.4-111PVK0649-0611/9/12

11629.12511/12/1212K0415-MS1 CQC,PSL88.4-111PVK0756-0111/12/12

11729.32511/12/1212K0415-MSD1X CQC,PSL88.4-111PVK0756-0111/12/12

11729.12511/13/1212K0462-MS1 CQC,PSL88.4-111PVK0793-0211/13/12

11328.32511/13/1212K0462-MSD1X CQC,PSL88.4-111PVK0793-0211/13/12

11027.62511/14/1212K0522-MS1X CQC88.4-111PVK0281-0111/14/12

11328.22511/14/1212K0522-MSD1X CQC,PSL88.4-111PVK0281-0111/14/12

10726.72511/14/1212K0553-MS1 CQC88.4-111PVK0632-0911/14/12

11127.82511/14/1212K0552-MS1 CQC88.4-111PVK0684-0211/14/12

112282511/14/1212K0553-MSD1X CQC,PSL88.4-111PVK0632-0911/14/12

11528.72511/14/1212K0552-MSD1X CQC,PSL88.4-111PVK0684-0211/14/12

10025.12511/15/1212K0581-MS1 CQC88.4-111PVK0696-0111/15/12

9924.82511/15/1212K0581-MSD1X CQC88.4-111PVK0696-0111/15/12

11228.12511/20/1212K0740-MS1 CQC,PSL88.4-111PVK0934-0111/20/12

11428.42511/20/1212K0740-MSD1X CQC,PSL88.4-111PVK0934-0111/20/12

11027.42511/20/1212K0751-MS1 CQC88.4-111PVK0768-0211/20/12

11027.42511/20/1212K0751-MSD1X CQC88.4-111PVK0768-0211/20/12

116292511/21/1212K0803-MS1 CQC,PSL88.4-111PVK1220-0211/21/12

11328.32511/21/1212K0803-MSD1X CQC,PSL88.4-111PVK1220-0211/21/12

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%R in MS/MSDToluene-d8Source QualifiersLimitsSample ID Prepared Spike Level Result %RRjct Analyzed

112282511/21/1212K0836-MS1 CQC,PSL88.4-111PVK1288-0311/21/12

11328.32511/21/1212K0836-MSD1X CQC,PSL88.4-111PVK1288-0311/21/12

116292511/23/1212K0865-MS1 CQC,PSL88.4-111PVK1375-0811/23/12

11428.42511/23/1212K0865-MSD1X CQC,PSL88.4-111PVK1375-0811/23/12

11328.22511/23/1212K0855-MS1 CQC,PSL88.4-111PVK1375-0211/23/12

11528.82511/23/1212K0855-MSD1X CQC,PSL88.4-111PVK1375-0211/23/12

12130.42511/24/1212K0897-MS1 CQC,PSL88.4-111PVK0988-0311/24/12

11929.92511/24/1212K0897-MSD1X CQC,PSL88.4-111PVK0988-0311/24/12

11628.92511/25/1212K0905-MS1 CQC,PSL88.4-111PVK1006-0111/25/12

11929.82511/25/1212K0905-MSD1X CQC,PSL88.4-111PVK1006-0111/25/12

116292511/30/1212K1135-MS1 CQC,PSL88.4-111PVK1450-1011/30/12

112282511/30/1212K1135-MSD1X CQC,PSL88.4-111PVK1450-1011/30/12

11629.12511/30/1212K1134-MS1 CQC,PSL88.4-111PVK1450-0312/1/12

11428.42511/30/1212K1134-MSD1X CQC,PSL88.4-111PVK1450-0312/1/12

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%R in SamplesToluene-d8


PVH2309-01 26.4259/1/12 106 88.4-1119/1/12 CQC,PGA

PVH2309-02 26.3259/1/12 105 88.4-1119/1/12 CQC,PGA

PVH2309-03 26.3259/1/12 105 88.4-1119/1/12 CQC,PGA

PVH2309-04 26.4259/1/12 106 88.4-1119/1/12 CQC,PGA

PVH2309-05 26.6259/1/12 107 88.4-1119/1/12 CQC,PGA

PVH2309-06 26.4259/1/12 106 88.4-1119/1/12 CQC,PGA

PVH2309-07 26.5259/1/12 106 88.4-1119/1/12 CQC,PGA

PVH2309-08 26.6259/1/12 106 88.4-1119/1/12 CQC,PGA

PVH2309-09 26.3259/1/12 105 88.4-1119/1/12 CQC,PGA

PVH2309-10 25.1259/4/12 101 88.4-1119/4/12 CQC,PGA

PVH2309-11 25.3259/4/12 101 88.4-1119/4/12 CQC,PGA

PVH2309-12 25.4259/4/12 101 88.4-1119/4/12 CQC,PGA

PVH2309-13 25259/4/12 100 88.4-1119/4/12 CQC,PGA

PVH2309-14 25.1259/4/12 101 88.4-1119/4/12 CQC,PGA

PVH2318-01 25259/4/12 100 88.4-1119/4/12 CQC,PGA

PVH2318-02 25.3259/4/12 101 88.4-1119/4/12 CQC,PGA

PVH2318-03 25.3259/4/12 101 88.4-1119/4/12 CQC,PGA

PVH2309-12RE1 24.8259/5/12 99 88.4-1119/5/12 CQC,PGA

PVH2309-13RE1 24.9259/5/12 100 88.4-1119/5/12 CQC,PGA

PVH2037-07 9/5/12 88.4-1119/5/12

PVI0290-01 24.1259/7/12 96 88.4-1119/7/12 CQC,PGA

PVI0290-06 24.6259/7/12 98 88.4-1119/7/12 CQC,PGA

PVI0290-02 24.2259/7/12 97 88.4-1119/7/12 CQC,PGA

PVI0290-03 24.4259/7/12 97 88.4-1119/7/12 CQC,PGA

PVI0290-04 24.2259/7/12 97 88.4-1119/7/12 CQC,PGA

PVI0290-05 24259/7/12 96 88.4-1119/7/12 CQC,PGA

PVI0609-08 26259/12/12 104 88.4-1119/12/12 CQC,PGA

PVI0609-01 26.2259/12/12 105 88.4-1119/12/12 CQC,PGA

PVI0609-02 26.5259/12/12 106 88.4-1119/12/12 CQC,PGA

01/02/13 15:46

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%R in SamplesToluene-d8Limits Qualifiers%RResultSpike LevelPreparedSample IDRjct Analyzed

PVI0609-03 26.1259/12/12 105 88.4-1119/12/12 CQC,PGA

PVI0609-04 26.3259/12/12 105 88.4-1119/12/12 CQC,PGA

PVI0609-09 26.1259/12/12 104 88.4-1119/12/12 CQC,PGA

PVI0609-10 26.1259/12/12 104 88.4-1119/12/12 CQC,PGA

PVI0609-11 26.1259/12/12 104 88.4-1119/12/12 CQC,PGA

PVI0609-12 26.3259/12/12 105 88.4-1119/12/12 CQC,PGA

PVI0609-13 25.9259/12/12 103 88.4-1119/12/12 CQC,PGA

PVI0609-14 26259/12/12 104 88.4-1119/12/12 CQC,PGA

PVI0609-15 26259/12/12 104 88.4-1119/12/12 CQC,PGA

PVI0609-16 26.2259/12/12 105 88.4-1119/12/12 CQC,PGA

PVI0609-17 25.7259/12/12 103 88.4-1119/12/12 CQC,PGA

PVI0609-18 26.1259/12/12 105 88.4-1119/12/12 CQC,PGA

PVI0525-06 9/12/12 88.4-1119/12/12 CQC,PGA

PVI0609-19 24.8259/12/12 99 88.4-1119/13/12 CQC,PGA

PVI0609-20 24.9259/12/12 100 88.4-1119/13/12 CQC,PGA

PVI0609-21 24.5259/12/12 98 88.4-1119/13/12 CQC,PGA

PVI1059-01 27.1259/18/12 108 88.4-1119/18/12 CQC,PGA

PVI1059-02 27.4259/18/12 110 88.4-1119/18/12 CQC,PGA

PVI1059-03 26.9259/18/12 108 88.4-1119/18/12 CQC,PGA

PVI0894-06 9/18/12 88.4-1119/18/12

PVI1060-01 26.6259/18/12 106 88.4-1119/18/12 CQC,PGA

PVI1060-03 26.4259/18/12 106 88.4-1119/18/12 CQC,PGA

PVI1060-04 26.8259/18/12 107 88.4-1119/18/12 CQC,PGA

PVI1060-05 27259/18/12 108 88.4-1119/18/12 CQC,PGA

PVI1060-06 26.5259/18/12 106 88.4-1119/18/12 CQC,PGA

PVI1060-02 23.8259/18/12 95 88.4-1119/18/12 CQC,PGA

PVI1060-07 25.3259/18/12 101 88.4-1119/18/12 CQC,PGA

PVI1060-08 24.3259/18/12 97 88.4-1119/18/12 CQC,PGA

PVI1060-09 23.9259/18/12 96 88.4-1119/18/12 CQC,PGA

PVI1553-01 25.2259/25/12 101 88.4-1119/25/12 CQC,PGA

PVI1510-08 9/25/12 88.4-1119/25/12 CQC,PGA

PVI1553-02 25.9259/25/12 103 88.4-1119/25/12 CQC,PGA

PVI1553-03 25.9259/25/12 104 88.4-1119/25/12 CQC,PGA

PVI1554-02 25.6259/25/12 102 88.4-1119/25/12 CQC,PGA

PVI1553-04 26.3259/25/12 105 88.4-1119/25/12 CQC,PGA

PVI1554-03 25.8259/25/12 103 88.4-1119/25/12 CQC,PGA

PVI1553-05 26.5259/25/12 106 88.4-1119/25/12 CQC,PGA

PVI1553-06 26.4259/25/12 106 88.4-1119/25/12 CQC,PGA

PVI1553-07 25.7259/25/12 103 88.4-1119/25/12 CQC,PGA

PVI1553-08 25.5259/25/12 102 88.4-1119/26/12 CQC,PGA

PVI1553-09 26.1259/25/12 104 88.4-1119/26/12 CQC,PGA

PVI1553-10 26.3259/25/12 105 88.4-1119/26/12 CQC,PGA

PVI1553-11 25.1259/25/12 101 88.4-1119/26/12 CQC,PGA

PVI1553-12 26.5259/25/12 106 88.4-1119/26/12 CQC,PGA

PVI1553-13 26.1259/25/12 104 88.4-1119/26/12 CQC,PGA

01/02/13 15:46

All Clients

All Projects

8260 (PGA), 8260 (PGA) Short

Water

All Extractions

All Instruments

All Extractionists

All Analysts

Printed:

Client:

Project:

Analyses:

Matrices:

Extractions:

Instruments:

Prepared By:

Analyzed By:


PVI1553-14 24.9259/25/12 100 88.4-1119/26/12 CQC,PGA

PVI1553-15 26259/25/12 104 88.4-1119/26/12 CQC,PGA

PVI1554-01 26.3259/25/12 105 88.4-1119/26/12 CQC,PGA

PVI1723-01 25.6259/28/12 102 88.4-1119/28/12 CQC,PGA

PVI1723-02 26.3259/28/12 105 88.4-1119/28/12 CQC,PGA

PVI1723-03 26.3259/28/12 105 88.4-1119/28/12 CQC,PGA

PVI1723-04 26.4259/28/12 106 88.4-1119/28/12 CQC,PGA

PVI1723-05 26.1259/28/12 105 88.4-1119/28/12 CQC,PGA

PVI1723-06 26.3259/28/12 105 88.4-1119/28/12 CQC,PGA

PVI1723-07 26.3259/28/12 105 88.4-1119/28/12 CQC,PGA

PVI1723-08 27.1259/28/12 108 88.4-1119/28/12 CQC,PGA

PVI1723-09 26.3259/28/12 105 88.4-1119/28/12 CQC,PGA

PVI1723-10 27.2259/28/12 109 88.4-1119/28/12 CQC,PGA

PVI1723-11 26.9259/28/12 108 88.4-1119/28/12 CQC,PGA

PVI1723-12 26.9259/28/12 108 88.4-1119/28/12 CQC,PGA

PVI1822-01 27.5259/28/12 110 88.4-1119/28/12 CQC,PGA

PVI1822-02 27259/28/12 108 88.4-1119/28/12 CQC,PGA

PVI1822-03 26.6259/28/12 107 88.4-1119/28/12 CQC,PGA

PVI1822-04 26.4259/28/12 106 88.4-1119/28/12 CQC,PGA

PVI1822-05 26.9259/28/12 108 88.4-1119/28/12 CQC,PGA

PVI1822-06 28.2259/28/12 113 88.4-1119/28/12 CQC,PGA,PSL

PVI1822-07 27259/28/12 108 88.4-1119/28/12 CQC,PGA

PVI1822-08 27.1259/28/12 108 88.4-1119/28/12 CQC,PGA

PVI1822-09 27.8259/28/12 111 88.4-1119/28/12 CQC,PGA

PVI1822-10 27.2259/28/12 109 88.4-1119/29/12 CQC,PGA

PVI1822-11 27259/28/12 108 88.4-1119/29/12 CQC,PGA

PVI1822-12 27.4259/28/12 110 88.4-1119/29/12 CQC,PGA

PVI1822-13 27259/28/12 108 88.4-1119/29/12 CQC,PGA

PVI1822-14 26.9259/28/12 108 88.4-1119/29/12 CQC,PGA

PVI1822-15 21.5259/28/12 86 88.4-1119/29/12 CQC,PGA,PSL

PVI1870-01 27.2259/28/12 109 88.4-1119/29/12 CQC,PGA

PVI1870-02 27.1259/28/12 108 88.4-1119/29/12 CQC,PGA

PVI1869-01 25.5259/29/12 102 88.4-1119/29/12 CQC,PGA

PVI1869-02 26.8259/29/12 107 88.4-1119/29/12 CQC,PGA

PVI1869-03 27.4259/29/12 110 88.4-1119/29/12 CQC,PGA

PVI1869-04 27.6259/29/12 110 88.4-1119/29/12 CQC,PGA

PVI1869-05 27.6259/29/12 110 88.4-1119/29/12 CQC,PGA,PSL

PVI1869-06 27.8259/29/12 111 88.4-1119/29/12 CQC,PGA

PVI1869-07 28259/29/12 112 88.4-1119/29/12 CQC,PGA,PSL

PVI1869-08 27.4259/29/12 110 88.4-1119/29/12 CQC,PGA

PVI1869-09 27.4259/29/12 110 88.4-1119/29/12 CQC,PGA

PVI1869-10 27259/29/12 108 88.4-1119/29/12 CQC,PGA

PVI1869-11 27.1259/29/12 109 88.4-1119/29/12 CQC,PGA

PVI1869-12 27.9259/29/12 112 88.4-1119/29/12 CQC,PGA,PSL

PVI1869-13 27.7259/29/12 111 88.4-1119/29/12 CQC,PGA

01/02/13 15:46

All Clients

All Projects

8260 (PGA), 8260 (PGA) Short

Water

All Extractions

All Instruments

All Extractionists

All Analysts

Printed:

Client:

Project:

Analyses:

Matrices:

Extractions:

Instruments:

Prepared By:

Analyzed By:


PVI1869-14 27.7259/29/12 111 88.4-1119/29/12 CQC,PGA

PVI1869-15 27.7259/29/12 111 88.4-1119/29/12 CQC,PGA

PVI1869-16 28.2259/29/12 113 88.4-1119/29/12 CQC,PGA,PSL

PVI1869-17 28.2259/29/12 113 88.4-1119/29/12 PSL,CQC,PGA

PVI1822-15RE1 26.22510/1/12 105 88.4-11110/1/12 CQC,PGA

PVI1869-03RE1 26.72510/1/12 107 88.4-11110/1/12 CQC,PGA

PVI1869-16RE1 27.32510/1/12 109 88.4-11110/1/12 CQC,PGA

PVI1869-17RE1 27.32510/1/12 109 88.4-11110/1/12 CQC,PGA

PVI1869-18 27.92510/1/12 112 88.4-11110/1/12 CQC,PGA,PSL

PVI1869-19 272510/1/12 108 88.4-11110/1/12 CQC,PGA

PVI1575-01 10/1/12 88.4-11110/1/12 CQC,PGA

PVJ0513-01 26.42510/8/12 106 88.4-11110/8/12 CQC,PGA

PVJ0513-02 262510/8/12 104 88.4-11110/8/12 CQC,PGA

PVJ0513-03 26.52510/8/12 106 88.4-11110/8/12 CQC,PGA

PVJ0513-04 25.92510/8/12 104 88.4-11110/8/12 CQC,PGA

PVJ0513-05 26.52510/8/12 106 88.4-11110/8/12 CQC,PGA

PVJ0513-06 26.22510/8/12 105 88.4-11110/8/12 CQC,PGA

PVJ0513-07 26.22510/8/12 105 88.4-11110/8/12 CQC,PGA

PVJ0513-08 26.32510/8/12 105 88.4-11110/8/12 CQC,PGA

PVJ0513-09 26.12510/8/12 104 88.4-11110/8/12 CQC,PGA

PVJ0513-10 26.12510/8/12 105 88.4-11110/8/12 CQC,PGA

PVJ0513-11 26.62510/8/12 106 88.4-11110/8/12 CQC,PGA

PVJ0513-12 26.12510/8/12 104 88.4-11110/8/12 CQC,PGA

PVJ0513-13 26.42510/8/12 105 88.4-11110/8/12 CQC,PGA

PVJ0513-14 26.72510/8/12 107 88.4-11110/8/12 CQC,PGA

PVJ0513-15 25.92510/8/12 104 88.4-11110/8/12 CQC,PGA

PVJ0682-01 262510/10/12 104 88.4-11110/10/12 CQC,PGA

PVJ0682-02 25.92510/10/12 104 88.4-11110/10/12 CQC,PGA

PVJ0682-03 262510/10/12 104 88.4-11110/10/12 CQC,PGA

PVJ0682-04 25.82510/10/12 103 88.4-11110/10/12 CQC,PGA

PVJ0682-05 25.92510/10/12 104 88.4-11110/10/12 CQC,PGA

PVJ0682-06 26.22510/10/12 105 88.4-11110/10/12 CQC,PGA

PVJ0682-07 26.62510/10/12 106 88.4-11110/10/12 CQC,PGA

PVJ0682-08 26.12510/10/12 104 88.4-11110/10/12 CQC,PGA

PVJ0682-09 262510/10/12 104 88.4-11110/10/12 CQC,PGA

PVJ0682-10 26.52510/10/12 106 88.4-11110/10/12 CQC,PGA

PVJ0682-11 262510/10/12 104 88.4-11110/10/12 CQC,PGA

PVJ0682-12 26.12510/10/12 104 88.4-11110/10/12 CQC,PGA

PVJ0682-13 26.52510/10/12 106 88.4-11110/10/12 CQC,PGA

PVJ0682-14 26.52510/10/12 106 88.4-11110/10/12 CQC,PGA

PVJ0682-15 262510/10/12 104 88.4-11110/10/12 CQC,PGA

PVJ0682-16 26.72510/10/12 107 88.4-11110/10/12 CQC,PGA

PVJ0682-17 24.12510/11/12 96 88.4-11110/11/12 CQC,PGA

PVJ0682-21 24.92510/11/12 100 88.4-11110/11/12 CQC,PGA

PVJ1065-01 24.72510/16/12 99 88.4-11110/16/12 CQC,PGA

01/02/13 15:46

All Clients

All Projects

8260 (PGA), 8260 (PGA) Short

Water

All Extractions

All Instruments

All Extractionists

All Analysts

Printed:

Client:

Project:

Analyses:

Matrices:

Extractions:

Instruments:

Prepared By:

Analyzed By:


PVJ1065-02 24.72510/16/12 99 88.4-11110/16/12 CQC,PGA

PVJ1065-03 25.22510/16/12 101 88.4-11110/16/12 CQC,PGA

PVJ1065-04 25.92510/16/12 104 88.4-11110/16/12 CQC,PGA

PVJ1065-05 24.72510/16/12 99 88.4-11110/16/12 CQC,PGA

PVJ1065-06 25.22510/16/12 101 88.4-11110/16/12 CQC,PGA

PVJ1065-07 24.92510/16/12 100 88.4-11110/16/12 CQC,PGA

PVJ1065-08 25.22510/16/12 101 88.4-11110/16/12 CQC,PGA

PVJ1065-09 24.72510/16/12 99 88.4-11110/16/12 CQC,PGA

PVJ1065-10 25.42510/16/12 102 88.4-11110/16/12 CQC,PGA

PVJ1237-01 24.62510/18/12 98 88.4-11110/18/12 CQC,PGA

PVJ1237-02 24.72510/18/12 99 88.4-11110/18/12 CQC,PGA

PVJ1237-03 24.92510/18/12 100 88.4-11110/18/12 CQC,PGA

PVJ1237-04 24.52510/18/12 98 88.4-11110/18/12 CQC,PGA

PVJ1237-05 24.42510/18/12 98 88.4-11110/18/12 CQC,PGA

PVJ1237-06 24.62510/18/12 98 88.4-11110/18/12 CQC,PGA

PVJ1237-07 24.22510/18/12 97 88.4-11110/18/12 CQC,PGA

PVJ1237-08 24.62510/18/12 99 88.4-11110/18/12 CQC,PGA

PVJ1237-09 24.32510/18/12 97 88.4-11110/18/12 CQC,PGA

PVJ1237-10 25.12510/18/12 100 88.4-11110/18/12 CQC,PGA

PVJ1237-11 24.22510/18/12 97 88.4-11110/18/12 CQC,PGA

PVJ1237-12 24.32510/18/12 97 88.4-11110/18/12 CQC,PGA

PVJ1237-13 24.52510/18/12 98 88.4-11110/18/12 CQC,PGA

PVJ1237-14 24.72510/18/12 99 88.4-11110/18/12 CQC,PGA

PVJ1405-01 25.52510/20/12 102 88.4-11110/20/12 CQC,PGA

PVJ1405-02 25.52510/20/12 102 88.4-11110/20/12 CQC,PGA

PVJ1405-03 24.82510/20/12 99 88.4-11110/20/12 CQC,PGA

PVJ1405-04 24.92510/20/12 100 88.4-11110/20/12 CQC,PGA

PVJ1405-05 252510/20/12 100 88.4-11110/20/12 CQC,PGA

PVJ1405-06 25.22510/20/12 101 88.4-11110/20/12 CQC,PGA

PVJ1405-07 24.62510/20/12 99 88.4-11110/20/12 CQC,PGA

PVJ1405-08 24.92510/20/12 100 88.4-11110/20/12 CQC,PGA

PVJ1405-09 24.82510/20/12 99 88.4-11110/20/12 CQC,PGA

PVJ1405-10 25.12510/20/12 100 88.4-11110/20/12 CQC,PGA

PVJ1405-11 25.62510/20/12 103 88.4-11110/20/12 CQC,PGA

PVJ1405-12 252510/20/12 100 88.4-11110/20/12 CQC,PGA

PVJ1405-13 252510/20/12 100 88.4-11110/20/12 CQC,PGA

PVJ1405-14 24.72510/20/12 99 88.4-11110/20/12 CQC,PGA

PVJ1405-15 24.62510/20/12 98 88.4-11110/20/12 CQC,PGA

PVJ1405-16 25.32510/20/12 101 88.4-11110/20/12 CQC,PGA

PVJ1405-17 26.22510/22/12 105 88.4-11110/22/12 CQC,PGA

PVJ1405-18 26.42510/22/12 106 88.4-11110/22/12 CQC,PGA

PVJ1577-01 26.62510/24/12 106 88.4-11110/24/12 CQC,PGA

PVJ1577-02 26.92510/24/12 108 88.4-11110/24/12 CQC,PGA

PVJ1577-03 26.32510/24/12 105 88.4-11110/24/12 CQC,PGA

PVJ1577-04 26.42510/24/12 105 88.4-11110/24/12 CQC,PGA

01/02/13 15:46

All Clients

All Projects

8260 (PGA), 8260 (PGA) Short

Water

All Extractions

All Instruments

All Extractionists

All Analysts

Printed:

Client:

Project:

Analyses:

Matrices:

Extractions:

Instruments:

Prepared By:

Analyzed By:


PVJ1577-05 26.62510/24/12 106 88.4-11110/24/12 CQC,PGA

PVJ1577-06 26.62510/24/12 106 88.4-11110/24/12 CQC,PGA

PVJ1577-07 26.52510/24/12 106 88.4-11110/25/12 CQC,PGA

PVJ1577-08 26.62510/24/12 106 88.4-11110/25/12 CQC,PGA

PVJ1577-09 25.82510/24/12 103 88.4-11110/25/12 CQC,PGA

PVJ1577-10 26.32510/24/12 105 88.4-11110/25/12 CQC,PGA

PVJ1577-11 26.52510/24/12 106 88.4-11110/25/12 CQC,PGA

PVJ1577-12 262510/24/12 104 88.4-11110/25/12 CQC,PGA

PVJ1577-13 24.52510/24/12 98 88.4-11110/25/12 CQC,PGA

PVJ1577-14 02510/24/12 88.4-11110/25/12

PVJ1575-01 02510/24/12 88.4-11110/25/12

PVJ1575-01RE1 26.82510/24/12 107 88.4-11110/25/12 CQC,PGA

PVJ1577-14RE1 27.12510/24/12 108 88.4-11110/25/12 CQC,PGA

PVJ1627-01 10/25/12 88.4-11110/25/12 CQC,PGA

PVJ1575-02 26.62510/25/12 106 88.4-11110/25/12 CQC,PGA

PVJ1577-15 27.72510/25/12 111 88.4-11110/25/12 CQC,PGA

PVJ1577-16 27.32510/25/12 109 88.4-11110/25/12 CQC,PGA

PVJ1577-17 26.82510/25/12 107 88.4-11110/25/12 CQC,PGA

PVJ1577-18 282510/25/12 112 88.4-11110/25/12 CQC,PGA

PVJ1600-02 10/25/12 88.4-11110/25/12 CQC,PGA

PVJ1577-19 26.72510/25/12 107 88.4-11110/25/12 CQC,PGA

PVJ1577-19RE1 26.92510/26/12 108 88.4-11110/26/12 CQC,PGA

PVJ1577-18RE1 27.62510/26/12 110 88.4-11110/26/12 CQC,PGA

PVK0411-02 26.32511/7/12 105 88.4-11111/7/12 CQC,PGA

PVK0411-03 26.62511/7/12 106 88.4-11111/7/12 CQC,PGA

PVK0237-01 11/7/12 88.4-11111/7/12

PVK0555-02 26.92511/8/12 108 88.4-11111/8/12 CQC,PGA

PVK0555-01 26.22511/8/12 105 88.4-11111/8/12 CQC,PGA

PVK0555-03 25.92511/8/12 104 88.4-11111/8/12 CQC,PGA

PVK0555-04 27.12511/8/12 108 88.4-11111/8/12 CQC,PGA

PVK0555-05 26.52511/8/12 106 88.4-11111/8/12 CQC,PGA

PVK0649-03 26.72511/9/12 107 88.4-11111/9/12

PVK0649-04 25.42511/9/12 102 88.4-11111/9/12

PVK0649-05 25.42511/9/12 101 88.4-11111/9/12

PVK0649-06 25.52511/9/12 102 88.4-11111/9/12

PVK0756-03 29.22511/12/12 117 88.4-11111/12/12 PSL,CQC,PGA

PVK0756-01 30.32511/12/12 121 88.4-11111/12/12 CQC,PGA,PSL

PVK0756-02 29.12511/12/12 117 88.4-11111/12/12 CQC,PGA,PSL

PVK0756-04 29.42511/12/12 118 88.4-11111/12/12 PSL,CQC,PGA

PVK0756-05 29.32511/12/12 117 88.4-11111/12/12 CQC,PGA,PSL

PVK0411-01 28.52511/12/12 114 88.4-11111/12/12 CQC,PGA,PSL

PVK0411-02RE1 29.62511/12/12 118 88.4-11111/12/12 PSL,CQC,PGA

PVK0411-03RE1 29.22511/12/12 117 88.4-11111/12/12 QC,N1,PGA,PS

PVK0649-01 29.52511/12/12 118 88.4-11111/12/12 CQC,PGA,PSL

PVK0649-02 29.22511/12/12 117 88.4-11111/12/12 CQC,PGA,PSL

01/02/13 15:46

All Clients

All Projects

8260 (PGA), 8260 (PGA) Short

Water

All Extractions

All Instruments

All Extractionists

All Analysts

Printed:

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Project:

Analyses:

Matrices:

Extractions:

Instruments:

Prepared By:

Analyzed By:


PVK0649-03RE1 28.62511/12/12 115 88.4-11111/12/12 PSL,CQC,PGA

PVK0649-04RE1 29.52511/12/12 118 88.4-11111/12/12 CQC,PGA,PSL

PVK0649-05RE1 29.52511/12/12 118 88.4-11111/12/12 CQC,PGA,PSL

PVK0649-06RE1 29.42511/12/12 117 88.4-11111/12/12 CQC,PGA,PSL

PVK0828-02 27.52511/13/12 110 88.4-11111/13/12 CQC,PGA

PVK0828-03 27.42511/13/12 110 88.4-11111/13/12 CQC,PGA

PVK0828-05 28.52511/13/12 114 88.4-11111/13/12 CQC,PGA,PSL

PVK0793-02 11/13/12 88.4-11111/13/12 CQC,PGA

PVK0828-01 282511/13/12 112 88.4-11111/13/12 PSL,CQC,PGA

PVK0828-04 28.32511/13/12 113 88.4-11111/13/12 PSL,CQC,PGA

PVK0411-02RE2 28.42511/13/12 114 88.4-11111/13/12 CQC,PGA,PSL

PVK0892-03 28.22511/14/12 113 88.4-11111/14/12 PSL,CQC,PGA

PVK0281-01 11/14/12 88.4-11111/14/12

PVK0892-01 26.92511/14/12 108 88.4-11111/14/12 CQC,PGA

PVK0892-02 27.52511/14/12 110 88.4-11111/14/12 CQC,PGA

PVK0632-01 26.92511/14/12 108 88.4-11111/14/12 CQC,PGA

PVK0632-02 27.62511/14/12 111 88.4-11111/14/12 CQC,PGA

PVK0632-03 27.12511/14/12 108 88.4-11111/14/12 CQC,PGA

PVK0632-04 26.72511/14/12 107 88.4-11111/14/12 CQC,PGA

PVK0632-08 27.42511/14/12 109 88.4-11111/14/12 CQC,PGA

PVK0632-09 27.42511/14/12 109 88.4-11111/14/12 CQC,PGA

PVK0684-01 28.22511/14/12 113 88.4-11111/14/12 CQC,PGA,PSL

PVK0632-10 26.92511/14/12 108 88.4-11111/14/12 CQC,PGA

PVK0684-02 28.42511/14/12 114 88.4-11111/14/12 PSL,CQC,PGA

PVK0632-11 27.42511/14/12 110 88.4-11111/14/12 CQC,PGA

PVK0684-03 27.72511/14/12 111 88.4-11111/14/12 CQC,PGA

PVK0632-12 272511/14/12 108 88.4-11111/14/12 CQC,PGA

PVK0684-04 28.82511/14/12 115 88.4-11111/15/12 CQC,PGA,PSL

PVK0684-05 28.62511/14/12 114 88.4-11111/15/12 CQC,PGA,PSL

PVK0632-13 28.32511/14/12 113 88.4-11111/15/12 CQC,PGA,PSL

PVK0684-06 27.82511/14/12 111 88.4-11111/15/12 CQC,PGA

PVK0632-14 27.62511/14/12 110 88.4-11111/15/12 CQC,PGA

PVK0684-07 29.32511/14/12 117 88.4-11111/15/12 CQC,PGA,PSL

PVK0632-15 28.72511/14/12 115 88.4-11111/15/12 CQC,PGA,PSL

PVK0684-08 28.12511/14/12 112 88.4-11111/15/12 CQC,PGA,PSL

PVK0632-16 26.42511/14/12 106 88.4-11111/15/12 CQC,PGA

PVK0684-09 28.42511/14/12 114 88.4-11111/15/12 CQC,PGA,PSL

PVK0632-17 26.72511/14/12 107 88.4-11111/15/12 CQC,PGA

PVK0632-18 28.42511/14/12 114 88.4-11111/15/12 CQC,PGA,PSL

PVK0684-10 26.42511/15/12 106 88.4-11111/15/12 CQC,PGA

PVK0684-08RE1 28.32511/15/12 113 88.4-11111/15/12 CQC,PGA,PSL

PVK0696-01 11/15/12 88.4-11111/15/12 CQC,PGA

PVK1220-01 27.52511/20/12 110 88.4-11111/20/12 CQC,PGA

PVK0768-02 11/20/12 88.4-11111/20/12

PVK1220-03 27.42511/20/12 109 88.4-11111/20/12 CQC,PGA

01/02/13 15:46

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PVK1220-04 27.82511/20/12 111 88.4-11111/20/12 CQC,PGA

PVK0934-01 11/20/12 88.4-11111/20/12 CQC,PGA,PSL

PVK1380-01 27.92511/21/12 112 88.4-11111/21/12 PSL,CQC,PGA

PVK1380-02 28.62511/21/12 114 88.4-11111/21/12 CQC,PGA,PSL

PVK1220-02 11/21/12 88.4-11111/21/12 CQC,PGA,PSL

PVK1220-06 28.12511/21/12 112 88.4-11111/21/12 CQC,PGA,PSL

PVK1220-07 28.32511/21/12 113 88.4-11111/21/12 PSL,CQC,PGA

PVK1220-08 27.82511/21/12 111 88.4-11111/21/12 CQC,PGA

PVK1220-09 282511/21/12 112 88.4-11111/21/12 CQC,PGA,PSL

PVK1220-10 29.52511/21/12 118 88.4-11111/21/12 CQC,PGA,PSL

PVK1220-11 28.92511/21/12 116 88.4-11111/21/12 CQC,PGA,PSL

PVK1220-12 28.42511/21/12 114 88.4-11111/21/12 CQC,PGA,PSL

PVK1220-13 28.42511/21/12 114 88.4-11111/21/12 CQC,PGA,PSL

PVK1220-14 28.42511/21/12 113 88.4-11111/21/12 CQC,PGA,PSL

PVK1288-01 28.22511/21/12 113 88.4-11111/21/12 CQC,PGA,PSL

PVK1288-02 28.92511/21/12 116 88.4-11111/21/12 CQC,PGA,PSL

PVK1288-03 27.72511/21/12 111 88.4-11111/21/12 CQC,PGA

PVK1288-04 28.72511/21/12 115 88.4-11111/21/12 CQC,PGA,PSL

PVK1288-05 28.62511/21/12 115 88.4-11111/21/12 CQC,PGA,PSL

PVK1288-06 28.22511/21/12 113 88.4-11111/21/12 CQC,PGA,PSL

PVK1288-07 27.82511/21/12 111 88.4-11111/21/12 CQC,PGA

PVK1286-01 28.52511/21/12 114 88.4-11111/22/12 CQC,PGA,PSL

PVK1286-02 28.32511/21/12 113 88.4-11111/22/12 CQC,PGA,PSL

PVK1286-03 28.22511/21/12 113 88.4-11111/22/12 CQC,PGA,PSL

PVK1286-04 282511/21/12 112 88.4-11111/22/12 CQC,PGA,PSL

PVK1286-05 28.62511/21/12 114 88.4-11111/22/12 CQC,PGA,PSL

PVK1286-06 29.32511/21/12 117 88.4-11111/22/12 CQC,PGA,PSL

PVK1220-15 28.62511/21/12 114 88.4-11111/22/12 CQC,PGA,PSL

PVK1220-17 28.82511/21/12 115 88.4-11111/22/12 CQC,PGA,PSL

PVK1220-16 28.52511/23/12 114 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-08 29.12511/23/12 116 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-09 28.82511/23/12 115 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-01 27.92511/23/12 112 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-10 29.12511/23/12 116 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-02 27.82511/23/12 111 88.4-11111/23/12 CQC,PGA

PVK1375-11 28.62511/23/12 115 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-12 28.72511/23/12 115 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-13 292511/23/12 116 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-03 28.42511/23/12 114 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-14 29.12511/23/12 116 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-04 29.12511/23/12 116 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-15 28.62511/23/12 115 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-05 29.12511/23/12 116 88.4-11111/23/12 CQC,PGA,PSL

PVK1375-06 27.62511/23/12 110 88.4-11111/23/12 CQC,PGA

PVK1375-07 28.42511/23/12 113 88.4-11111/23/12 CQC,PGA,PSL

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PVK1375-16 282511/24/12 112 88.4-11111/24/12 CQC,PGA,PSL

PVK0988-03 11/24/12 88.4-11111/24/12

PVK1006-01 11/24/12 88.4-11111/25/12

PVK1375-16RE1 27.82511/25/12 111 88.4-11111/26/12 CQC,PGA

PVK1450-20 27.42511/30/12 109 88.4-11111/30/12 CQC,PGA,PSL

PVK1450-10 28.62511/30/12 114 88.4-11111/30/12 CQC,PGA,PSL

PVK1450-11 27.92511/30/12 112 88.4-11111/30/12 CQC,PGA,PSL

PVK1450-12 282511/30/12 112 88.4-11111/30/12 CQC,PGA,PSL

PVK1450-01 27.72511/30/12 111 88.4-11111/30/12 CQC,PGA

PVK1450-13 28.32511/30/12 113 88.4-11111/30/12 CQC,PGA,PSL

PVK1450-02 282511/30/12 112 88.4-11111/30/12 CQC,PGA,PSL

PVK1450-14 28.42511/30/12 114 88.4-11111/30/12 CQC,PGA,PSL

PVK1450-03 28.82511/30/12 115 88.4-11112/1/12 CQC,PGA,PSL

PVK1450-15 28.42511/30/12 113 88.4-11112/1/12 CQC,PGA,PSL

PVK1450-16 28.22511/30/12 113 88.4-11112/1/12 CQC,PGA,PSL

PVK1450-17 28.72511/30/12 115 88.4-11112/1/12 CQC,PGA,PSL

PVK1450-18 282511/30/12 112 88.4-11112/1/12 CQC,PGA,PSL

PVK1450-04 29.32511/30/12 117 88.4-11112/1/12 CQC,PGA,PSL

PVK1450-19 28.82511/30/12 115 88.4-11112/1/12 CQC,PGA,PSL

PVK1450-05 28.12511/30/12 112 88.4-11112/1/12 CQC,PGA,PSL

PVK1450-06 28.52511/30/12 114 88.4-11112/1/12 CQC,PGA,PSL

PVK1450-07 27.82511/30/12 111 88.4-11112/1/12 CQC,PGA

PVK1450-08 28.52511/30/12 114 88.4-11112/1/12 CQC,PGA,PSL

PVK1450-09 28.42511/30/12 114 88.4-11112/1/12 CQC,PGA,PSL

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LCS %Rtrans-1,2-Dichloroethene


12I0005-BS1 27 108259/1/12 82.3-1209/1/12 CQC

12I0028-BS1 25.1 100259/4/12 82.3-1209/4/12 CQC

12I0081-BS1 22.1 88259/5/12 82.3-1209/5/12 CQC

12I0215-BS1 23.2 93259/7/12 82.3-1209/7/12 CQC

12I0352-BS1 28 112259/12/12 82.3-1209/12/12 CQC

12I0394-BS1 21.2 85259/12/12 82.3-1209/12/12 CQC

12I0598-BS1 28.8 115259/18/12 82.3-1209/18/12 CQC

12I0648-BS1 26 104259/18/12 82.3-1209/18/12 CQC

12I0926-BS1 25.4 102259/25/12 82.3-1209/25/12 CQC

12I0925-BS1 25 100259/25/12 82.3-1209/25/12 CQC

12I1065-BS1 26.7 107259/28/12 82.3-1209/28/12 CQC

12I1095-BS1 25.6 103259/28/12 82.3-1209/28/12 CQC

12I1107-BS1 26.1 104259/29/12 82.3-1209/29/12 CQC

12J0008-BS1 25.8 1032510/1/12 82.3-12010/1/12 CQC

12J0298-BS1 23.2 932510/8/12 82.3-12010/8/12

12J0389-BS1 22.7 912510/10/12 82.3-12010/10/12

12J0445-BS1 24 962510/11/12 82.3-12010/11/12 CQC

12J0620-BS1 24 962510/16/12 82.3-12010/16/12 CQC

12J0736-BS1 24 962510/18/12 82.3-12010/18/12 CQC

12J0821-BS1 25.5 1022510/20/12 82.3-12010/20/12 CQC

12J0850-BS1 23.1 932510/22/12 82.3-12010/22/12 CQC

12J0972-BS1 25.1 1012510/24/12 82.3-12010/24/12 CQC

12J1010-BS1 25.1 1002510/25/12 82.3-12010/25/12 CQC

12J1038-BS1 23.9 962510/25/12 82.3-12010/25/12 CQC

12J1059-BS1 26.8 1072510/26/12 82.3-12010/26/12 CQC

12K0235-BS1 29.8 1192511/7/12 82.3-12011/7/12 CQC

12K0286-BS1 25.5 1022511/8/12 82.3-12011/8/12 CQC

01/02/13 15:46

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LCS %Rtrans-1,2-DichloroetheneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 22 882511/9/12 82.3-12011/9/12

12K0415-BS1 23.7 952511/12/12 82.3-12011/12/12 CQC

12K0462-BS1 27.1 1082511/13/12 82.3-12011/13/12 CQC

12K0522-BS1 27.5 1102511/14/12 82.3-12011/14/12 CQC

12K0553-BS1 26 1042511/14/12 82.3-12011/14/12 CQC

12K0552-BS1 24.4 982511/14/12 82.3-12011/14/12 CQC

12K0581-BS1 26.6 1062511/15/12 82.3-12011/15/12 CQC

12K0740-BS1 23.2 932511/20/12 82.3-12011/20/12 CQC

12K0751-BS1 25.6 1032511/20/12 82.3-12011/20/12 CQC

12K0789-BS1 26.8 1072511/20/12 82.3-12011/20/12

12K0803-BS1 23.6 94X 2511/21/12 82.3-12011/21/12 CQC

12K0836-BS1 24.6 982511/21/12 82.3-12011/21/12 CQC

12K0855-BS1 24.9 1002511/23/12 82.3-12011/23/12 CQC

12K0865-BS1 24.6 992511/23/12 82.3-12011/23/12 CQC

12K0897-BS1 24.4 982511/24/12 82.3-12011/24/12 CQC

12K0905-BS1 25.9 1042511/25/12 82.3-12011/25/12 CQC

12K1134-BS1 21.1 842511/30/12 82.3-12011/30/12 CQC

12K1135-BS1 22.9 922511/30/12 82.3-12011/30/12 CQC

01/02/13 15:46

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LCS/LCSD RPDtrans-1,2-Dichloroethene


9523.8259/1/129/1/1212I0005-BSD1 27 108 13 25 CQC

11127.7259/4/129/4/1212I0028-BSD1 25.1 100 10 25 CQC

8320.8259/5/129/5/1212I0081-BSD1 22.1 88 6 25 CQC

9223.1259/7/129/7/1212I0215-BSD1 23.2 93 0.6 25 CQC

10626.6259/12/129/12/1212I0352-BSD1 28 112 5 25 CQC

9523.8259/12/129/12/1212I0394-BSD1 21.2 85 12 25 CQC

11528.8259/18/129/18/1212I0598-BSD1 28.8 115 0.2 25 CQC

10325.7259/18/129/18/1212I0648-BSD1 26 104 1 25 CQC

9523.8259/25/129/25/1212I0926-BSD1 25.4 102 7 25 CQC

9423.6259/25/129/25/1212I0925-BSD1 25 100 6 25 CQC

10426259/28/129/28/1212I1065-BSD1 26.7 107 3 25 CQC

10325.7259/28/129/28/1212I1095-BSD1 25.6 103 0.2 25 CQC

9624.1259/29/129/29/1212I1107-BSD1 26.1 104 8 25 CQC

10726.72510/1/1210/1/1212J0008-BSD1 25.8 103 3 25 CQC

9223.12510/8/1210/8/1212J0298-BSD1 23.2 93 0.6 25

9223.12510/10/1210/10/1212J0389-BSD1 22.7 91 1 25

9724.22510/11/1210/11/1212J0445-BSD1 24 96 0.7 25 CQC

9724.42510/16/1210/16/1212J0620-BSD1 24 96 2 25 CQC

96242510/18/1210/18/1212J0736-BSD1 24 96 0.3 25 CQC

9824.62510/20/1210/20/1212J0821-BSD1 25.5 102 4 25 CQC

9022.52510/22/1210/22/1212J0850-BSD1 23.1 93 3 25 CQC

9122.82510/24/1210/24/1212J0972-BSD1 25.1 101 10 25 CQC

9724.22510/25/1210/25/1212J1010-BSD1 25.1 100 4 25 CQC

10225.52510/25/1210/25/1212J1038-BSD1 23.9 96 6 25 CQC

104262510/26/1210/26/1212J1059-BSD1 26.8 107 3 25 CQC

11127.82511/7/1211/7/1212K0235-BSD1 29.8 119 7 25 CQC

10024.92511/8/1211/8/1212K0286-BSD1 25.5 102 2 25 CQC

01/02/13 15:46

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LCS/LCSD RPDtrans-1,2-Dichloroethene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

9122.62511/9/1211/9/1212K0341-BSD1 22 88 3 25

92232511/12/1211/12/1212K0415-BSD1 23.7 95 3 25 CQC

10325.82511/13/1211/13/1212K0462-BSD1 27.1 108 5 25 CQC

11328.22511/14/1211/14/1212K0522-BSD1 27.5 110 3 25 CQC

9824.52511/14/1211/14/1212K0553-BSD1 26 104 6 25 CQC

9824.42511/14/1211/14/1212K0552-BSD1 24.4 98 0.2 25 CQC

10526.22511/15/1211/15/1212K0581-BSD1 26.6 106 2 25 CQC

9724.22511/20/1211/20/1212K0740-BSD1 23.2 93 4 25 CQC

9423.42511/20/1211/20/1212K0751-BSD1 25.6 103 9 25 CQC

10225.52511/20/1211/20/1212K0789-BSD1 26.8 107 5 25

100252511/21/1211/21/1212K0803-BSD1X 23.6 94 6 25 CQC

92232511/21/1211/21/1212K0836-BSD1 24.6 98 7 25 CQC

9924.72511/23/1211/23/1212K0855-BSD1 24.9 100 0.9 25 CQC

9624.12511/23/1211/23/1212K0865-BSD1 24.6 99 2 25 CQC

9724.22511/24/1211/24/1212K0897-BSD1 24.4 98 0.8 25 CQC

10025.12511/25/1211/25/1212K0905-BSD1 25.9 104 3 25 CQC

9022.62511/30/1211/30/1212K1134-BSD1 21.1 84 7 25 CQC

10225.62511/30/1211/30/1212K1135-BSD1 22.9 92 11 25 CQC

01/02/13 15:46

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MS %Rtrans-1,2-Dichloroethene


CQC81.3-123PVH2309-021002512I0005-MS1 9/1/12 9/1/12 25

CQC81.3-123PVH2309-1111428.512I0028-MS1 9/4/12 9/4/12 25

CQC81.3-123PVH2037-078220.512I0081-MS1 9/5/12 9/5/12 25

CQC81.3-123PVI0290-0310225.612I0215-MS1 9/7/12 9/7/12 25

CQC81.3-123PVI0609-0911027.612I0352-MS1 9/12/12 9/12/12 25

CQC81.3-123PVI0525-06962412I0394-MS1 9/12/12 9/12/12 25

CQC81.3-123PVI0894-0611929.712I0598-MS1 9/18/12 9/18/12 25

CQC81.3-123PVI1060-0210826.912I0648-MS1 9/18/12 9/18/12 25

CQC81.3-123PVI1553-089824.612I0925-MS1 9/25/12 9/25/12 25

CQC81.3-123PVI1510-089724.212I0926-MS1 9/25/12 9/25/12 25

CQC81.3-123PVI1723-0311328.112I1065-MS1 9/28/12 9/28/12 25

CQC81.3-123PVI1822-029924.712I1095-MS1 9/28/12 9/28/12 25

CQC81.3-123PVI1869-0510726.812I1107-MS1 9/29/12 9/29/12 25

CQC81.3-123PVI1575-011042612J0008-MS1 10/1/12 10/1/12 25

81.3-123PVJ0513-039724.312J0298-MS1 10/8/12 10/8/12 25

81.3-123PVJ0682-019624.112J0389-MS1 10/10/12 10/10/12 25

CQC81.3-123PVJ0682-178822.112J0445-MS1 10/11/12 10/11/12 25

CQC81.3-123PVJ1065-029423.512J0620-MS1 10/16/12 10/16/12 25

CQC81.3-123PVJ1237-029523.812J0736-MS1 10/18/12 10/18/12 25

CQC81.3-123PVJ1405-0210726.812J0821-MS1 10/20/12 10/20/12 25

CQC81.3-123PVJ1405-179423.412J0850-MS1 10/22/12 10/22/12 25

CQC81.3-123PVJ1577-029223.112J0972-MS1 10/24/12 10/24/12 25

CQC81.3-123PVJ1627-0110025112J1010-MS1 10/25/12 10/25/12 250

CQC81.3-123PVJ1600-029824.612J1038-MS1 10/25/12 10/25/12 25

CQC81.3-123PVJ1577-18RE110526212J1059-MS1 10/26/12 10/26/12 250

CQC81.3-123PVK0237-0112330.812K0235-MS1 11/7/12 11/7/12 25

CQC81.3-123PVK0555-0411729.212K0286-MS1 11/8/12 11/8/12 25

81.3-123PVK0649-069323.312K0341-MS1 11/9/12 11/9/12 25

CQC81.3-123PVK0756-019724.412K0415-MS1 11/12/12 11/12/12 25

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MS %Rtrans-1,2-DichloroetheneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC81.3-123PVK0793-021122812K0462-MS1 11/13/12 11/13/12 25

CQC81.3-123PVK0281-0110726.7X 12K0522-MS1 11/14/12 11/14/12 25

CQC81.3-123PVK0632-0910626.412K0553-MS1 11/14/12 11/14/12 25

CQC81.3-123PVK0684-021042612K0552-MS1 11/14/12 11/14/12 25

CQC81.3-123PVK0696-0111027.412K0581-MS1 11/15/12 11/15/12 25

CQC81.3-123PVK0934-019724.312K0740-MS1 11/20/12 11/20/12 25

CQC81.3-123PVK0768-0211127.812K0751-MS1 11/20/12 11/20/12 25

CQC81.3-123PVK1220-0210025.1X 12K0803-MS1 11/21/12 11/21/12 25

CQC81.3-123PVK1288-0310325.812K0836-MS1 11/21/12 11/21/12 25

CQC81.3-123PVK1375-0810125.212K0865-MS1 11/23/12 11/23/12 25

CQC81.3-123PVK1375-0210225.512K0855-MS1 11/23/12 11/23/12 25

CQC81.3-123PVK0988-0310024.912K0897-MS1 11/24/12 11/24/12 25

CQC81.3-123PVK1006-0110626.412K0905-MS1 11/25/12 11/25/12 25

CQC81.3-123PVK1450-10962412K1135-MS1 11/30/12 11/30/12 25

CQC81.3-123PVK1450-0310927.312K1134-MS1 11/30/12 12/1/12 25

01/02/13 15:46

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Analyzed By:

MS/MSD RPDtrans-1,2-Dichloroethene


10325.8259/1/129/1/1212I0005-MSD1 CQC25310025 PVH2309-02

11127.8259/4/129/4/1212I0028-MSD1 CQC25311428.5 PVH2309-11

8721.8259/5/129/5/1212I0081-MSD1 CQC2568220.5 PVH2037-07

10225.4259/7/129/7/1212I0215-MSD1 CQC250.710225.6 PVI0290-03

10927.1259/12/129/12/1212I0352-MSD1 CQC25211027.6 PVI0609-09

9022.4259/12/129/12/1212I0394-MSD1 CQC2579624 PVI0525-06

11729.2259/18/129/18/1212I0598-MSD1 CQC25211929.7 PVI0894-06

10024.9259/18/129/18/1212I0648-MSD1 CQC25810826.9 PVI1060-02

9724.4259/25/129/25/1212I0925-MSD1 CQC250.99824.6 PVI1553-08

10325.6259/25/129/25/1212I0926-MSD1 CQC2569724.2 PVI1510-08

11027.6259/28/129/28/1212I1065-MSD1 CQC25211328.1 PVI1723-03

11328.2259/28/129/28/1212I1095-MSD1 CQC25139924.7 PVI1822-02

11829.4259/29/129/29/1212I1107-MSD1 CQC25910726.8 PVI1869-05

11127.82510/1/1210/1/1212J0008-MSD1 CQC25710426 PVI1575-01

96242510/8/1210/8/1212J0298-MSD1 2519724.3 PVJ0513-03

96242510/10/1210/10/1212J0389-MSD1 250.39624.1 PVJ0682-01

8821.92510/11/1210/11/1212J0445-MSD1 CQC250.78822.1 PVJ0682-17

9724.32510/16/1210/16/1212J0620-MSD1 CQC2549423.5 PVJ1065-02

10025.12510/18/1210/18/1212J0736-MSD1 CQC2559523.8 PVJ1237-02

11328.22510/20/1210/20/1212J0821-MSD1 CQC25510726.8 PVJ1405-02

9122.82510/22/1210/22/1212J0850-MSD1 CQC2539423.4 PVJ1405-17

100252510/24/1210/24/1212J0972-MSD1 CQC2589223.1 PVJ1577-02

10125325010/25/1210/25/1212J1010-MSD1 CQC250.8100251 PVJ1627-01

10325.82510/25/1210/25/1212J1038-MSD1 CQC2559824.6 PVJ1600-02

10726825010/26/1210/26/1212J1059-MSD1 CQC253105262 PVJ1577-18RE1

12531.32511/7/1211/7/1212K0235-MSD1 CQC,PSL25212330.8 PVK0237-01

11328.22511/8/1211/8/1212K0286-MSD1 CQC25411729.2 PVK0555-04

9423.42511/9/1211/9/1212K0341-MSD1 250.69323.3 PVK0649-06

9824.52511/12/1211/12/1212K0415-MSD1 CQC250.49724.4 PVK0756-01

11127.62511/13/1211/13/1212K0462-MSD1 CQC25111228 PVK0793-02

11127.82511/14/1211/14/1212K0522-MSD1 CQC25410726.7 PVK0281-01

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MS/MSD RPDtrans-1,2-Dichloroethene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

10425.92511/14/1211/14/1212K0553-MSD1 CQC25210626.4 PVK0632-09

11027.52511/14/1211/14/1212K0552-MSD1 CQC25610426 PVK0684-02

10927.32511/15/1211/15/1212K0581-MSD1 CQC250.511027.4 PVK0696-01

9724.42511/20/1211/20/1212K0740-MSD1 CQC250.29724.3 PVK0934-01

11228.12511/20/1211/20/1212K0751-MSD1 CQC25111127.8 PVK0768-02

10726.82511/21/1211/21/1212K0803-MSD1X CQC25610025.1 PVK1220-02

10225.42511/21/1211/21/1212K0836-MSD1 CQC25210325.8 PVK1288-03

9924.82511/23/1211/23/1212K0865-MSD1 CQC25210125.2 PVK1375-08

10225.52511/23/1211/23/1212K0855-MSD1 CQC25010225.5 PVK1375-02

10526.42511/24/1211/24/1212K0897-MSD1 CQC25610024.9 PVK0988-03

10325.82511/25/1211/25/1212K0905-MSD1 CQC25310626.4 PVK1006-01

10526.22511/30/1211/30/1212K1135-MSD1 CQC2599624 PVK1450-10

10225.62512/1/1211/30/1212K1134-MSD1 CQC25610927.3 PVK1450-03

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BLKtrans-1,2-Dichloroethene

1.0 r-------------------------------------------------------~

0.9 0.8 0.7

0.6 0.5

Plotted: 44 MDL: 0.22 MRL: 1

Rejected: 2 Stdv: 0.0211 Mean: 0.00318 0.4 2s: 0.0454 0.3 3s: 0.0665

:: :;.~.;.;.~.;.;.~.;;. ~· ;. ~· ~· ;. ~· ~· ;. ~.;.;.~.~.;.~.;.;~. ~J\;. ;. ;. ;~;;~;;~;;~;;;;;;;;;;;;;;;;;;;;4s: 0.0876 00 -\- 3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %Rtrans-1,3-Dichloropropene


12K0235-BS1 26.8 1072511/7/12 82.2-12111/7/12 CQC

12K0286-BS1 25.1 1002511/8/12 82.2-12111/8/12 CQC

12K0341-BS1 24.7 992511/9/12 82.2-12111/9/12

12K0415-BS1 23.7 952511/12/12 82.2-12111/12/12 CQC

12K0462-BS1 26.5 1062511/13/12 82.2-12111/13/12 CQC

12K0522-BS1 25 1002511/14/12 82.2-12111/14/12 CQC

12K0803-BS1 24.6 982511/21/12 82.2-12111/21/12 CQC

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LCS/LCSD RPDtrans-1,3-Dichloropropene


10626.62511/7/1211/7/1212K0235-BSD1 26.8 107 0.8 25 CQC

100252511/8/1211/8/1212K0286-BSD1 25.1 100 0.3 25 CQC

9724.12511/9/1211/9/1212K0341-BSD1 24.7 99 2 25

9423.52511/12/1211/12/1212K0415-BSD1 23.7 95 1 25 CQC

10426.12511/13/1211/13/1212K0462-BSD1 26.5 106 2 25 CQC

104262511/14/1211/14/1212K0522-BSD1 25 100 4 25 CQC

10827.12511/21/1211/21/1212K0803-BSD1 24.6 98 10 25 CQC

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MS %Rtrans-1,3-Dichloropropene


CQC72.8-123PVK0237-0111528.712K0235-MS1 11/7/12 11/7/12 25

CQC72.8-123PVK0555-0411528.612K0286-MS1 11/8/12 11/8/12 25

72.8-123PVK0649-0610025.112K0341-MS1 11/9/12 11/9/12 25

CQC72.8-123PVK0756-019824.612K0415-MS1 11/12/12 11/12/12 25

CQC72.8-123PVK0793-0210826.912K0462-MS1 11/13/12 11/13/12 25

CQC72.8-123PVK0281-019623.912K0522-MS1 11/14/12 11/14/12 25

CQC72.8-123PVK1220-02962412K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDtrans-1,3-Dichloropropene


12330.72511/7/1211/7/1212K0235-MSD1 CQC25711528.7 PVK0237-01

10927.22511/8/1211/8/1212K0286-MSD1 CQC25511528.6 PVK0555-04

9523.72511/9/1211/9/1212K0341-MSD1 25510025.1 PVK0649-06

9924.72511/12/1211/12/1212K0415-MSD1 CQC250.69824.6 PVK0756-01

10726.72511/13/1211/13/1212K0462-MSD1 CQC250.910826.9 PVK0793-02

10726.82511/14/1211/14/1212K0522-MSD1 CQC25119623.9 PVK0281-01

9924.82511/21/1211/21/1212K0803-MSD1 CQC2539624 PVK1220-02

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BLKtrans-1,3-Dichloropropene

01/02/13 15:46

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LCS %RTrichloroethene


12I0005-BS1 27.4 110259/1/12 85-1159/1/12 CQC

12I0028-BS1 25.3 101259/4/12 85-1159/4/12 CQC

12I0081-BS1 22 88259/5/12 85-1159/5/12 CQC

12I0215-BS1 22.8 91259/7/12 85-1159/7/12 CQC

12I0352-BS1 27.5 110259/12/12 85-1159/12/12 CQC

12I0394-BS1 23.9 96259/12/12 85-1159/12/12 CQC

12I0598-BS1 28.5 114259/18/12 85-1159/18/12 CQC

12I0648-BS1 24 96259/18/12 85-1159/18/12 CQC

12I0926-BS1 25.7 103259/25/12 85-1159/25/12 CQC

12I0925-BS1 22.2 89259/25/12 85-1159/25/12 CQC

12I1065-BS1 27.6 110259/28/12 85-1159/28/12 CQC

12I1095-BS1 25.7 103259/28/12 85-1159/28/12 CQC

12I1107-BS1 26.2 105259/29/12 85-1159/29/12 CQC

12J0008-BS1 25.2 1012510/1/12 85-11510/1/12 CQC

12J0298-BS1 23.4 942510/8/12 85-11510/8/12

12J0389-BS1 23.8 952510/10/12 85-11510/10/12

12J0445-BS1 24 962510/11/12 85-11510/11/12 CQC

12J0620-BS1 24.4 982510/16/12 85-11510/16/12 CQC

12J0736-BS1 24 962510/18/12 85-11510/18/12 CQC

12J0821-BS1 25.8 1032510/20/12 85-11510/20/12 CQC

12J0850-BS1 23.8 952510/22/12 85-11510/22/12 CQC

12J0972-BS1 25 1002510/24/12 85-11510/24/12 CQC

12J1010-BS1 25.4 1022510/25/12 85-11510/25/12 CQC

12J1038-BS1 26.4 1062510/25/12 85-11510/25/12 CQC

12J1059-BS1 27 1082510/26/12 85-11510/26/12 CQC

12K0235-BS1 29.7 1192511/7/12 85-11511/7/12 CQC,PSL

12K0286-BS1 25.8 1032511/8/12 85-11511/8/12 CQC

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LCS %RTrichloroetheneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 25.9 1042511/9/12 85-11511/9/12

12K0415-BS1 23.7 952511/12/12 85-11511/12/12 CQC

12K0462-BS1 26 1042511/13/12 85-11511/13/12 CQC

12K0522-BS1 27.2 1092511/14/12 85-11511/14/12 CQC

12K0553-BS1 27.1 1092511/14/12 85-11511/14/12 CQC

12K0552-BS1 23.9 962511/14/12 85-11511/14/12 CQC

12K0581-BS1 26.6 1062511/15/12 85-11511/15/12 CQC

12K0740-BS1 23.9 962511/20/12 85-11511/20/12 CQC

12K0751-BS1 25.4 1022511/20/12 85-11511/20/12 CQC

12K0789-BS1 26 1042511/20/12 85-11511/20/12

12K0803-BS1 24 96X 2511/21/12 85-11511/21/12 CQC

12K0836-BS1 24.1 962511/21/12 85-11511/21/12 CQC

12K0855-BS1 24.6 982511/23/12 85-11511/23/12 CQC

12K0865-BS1 25.8 1032511/23/12 85-11511/23/12 CQC

12K0897-BS1 26.2 1052511/24/12 85-11511/24/12 CQC

12K0905-BS1 27.5 1102511/25/12 85-11511/25/12 CQC

12K1134-BS1 24 962511/30/12 85-11511/30/12 CQC

12K1135-BS1 24.2 972511/30/12 85-11511/30/12 CQC

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LCS/LCSD RPDTrichloroethene


9724.4259/1/129/1/1212I0005-BSD1 27.4 110 12 25 CQC

10827259/4/129/4/1212I0028-BSD1 25.3 101 7 25 CQC

8922.3259/5/129/5/1212I0081-BSD1 22 88 1 25 CQC

9222.9259/7/129/7/1212I0215-BSD1 22.8 91 0.2 25 CQC

10526.3259/12/129/12/1212I0352-BSD1 27.5 110 4 25 CQC

10025259/12/129/12/1212I0394-BSD1 23.9 96 5 25 CQC

11528.7259/18/129/18/1212I0598-BSD1 28.5 114 0.6 25 CQC

9022.5259/18/129/18/1212I0648-BSD1 24 96 6 25 CQC

9924.8259/25/129/25/1212I0926-BSD1 25.7 103 4 25 CQC

9223259/25/129/25/1212I0925-BSD1 22.2 89 3 25 CQC

10526.1259/28/129/28/1212I1065-BSD1 27.6 110 5 25 CQC

10626.5259/28/129/28/1212I1095-BSD1 25.7 103 3 25 CQC

9724.2259/29/129/29/1212I1107-BSD1 26.2 105 8 25 CQC

112282510/1/1210/1/1212J0008-BSD1 25.2 101 10 25 CQC

9423.42510/8/1210/8/1212J0298-BSD1 23.4 94 0.09 25

9523.82510/10/1210/10/1212J0389-BSD1 23.8 95 0.3 25

100252510/11/1210/11/1212J0445-BSD1 24 96 4 25 CQC

96242510/16/1210/16/1212J0620-BSD1 24.4 98 2 25 CQC

9523.82510/18/1210/18/1212J0736-BSD1 24 96 0.7 25 CQC

10225.62510/20/1210/20/1212J0821-BSD1 25.8 103 0.9 25 CQC

9223.12510/22/1210/22/1212J0850-BSD1 23.8 95 3 25 CQC

9423.42510/24/1210/24/1212J0972-BSD1 25 100 6 25 CQC

10325.82510/25/1210/25/1212J1010-BSD1 25.4 102 1 25 CQC

10626.62510/25/1210/25/1212J1038-BSD1 26.4 106 0.7 25 CQC

11127.62510/26/1210/26/1212J1059-BSD1 27 108 2 25 CQC

12130.22511/7/1211/7/1212K0235-BSD1 29.7 119 2 25 CQC,PSL

10425.92511/8/1211/8/1212K0286-BSD1 25.8 103 0.6 25 CQC

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LCS/LCSD RPDTrichloroethene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

10325.72511/9/1211/9/1212K0341-BSD1 25.9 104 0.9 25

9623.92511/12/1211/12/1212K0415-BSD1 23.7 95 0.8 25 CQC

10526.22511/13/1211/13/1212K0462-BSD1 26 104 0.6 25 CQC

10426.12511/14/1211/14/1212K0522-BSD1X 27.2 109 4 25 CQC

9724.42511/14/1211/14/1212K0553-BSD1 27.1 109 11 25 CQC

10024.92511/14/1211/14/1212K0552-BSD1 23.9 96 4 25 CQC

11228.12511/15/1211/15/1212K0581-BSD1 26.6 106 5 25 CQC

96242511/20/1211/20/1212K0740-BSD1 23.9 96 0.6 25 CQC

9724.42511/20/1211/20/1212K0751-BSD1 25.4 102 4 25 CQC

10325.92511/20/1211/20/1212K0789-BSD1 26 104 0.7 25

10125.22511/21/1211/21/1212K0803-BSD1X 24 96 5 25 CQC

9323.22511/21/1211/21/1212K0836-BSD1 24.1 96 4 25 CQC

10225.42511/23/1211/23/1212K0855-BSD1 24.6 98 3 25 CQC

10125.42511/23/1211/23/1212K0865-BSD1 25.8 103 2 25 CQC

10626.62511/24/1211/24/1212K0897-BSD1 26.2 105 1 25 CQC

112282511/25/1211/25/1212K0905-BSD1 27.5 110 2 25 CQC

9423.52511/30/1211/30/1212K1134-BSD1 24 96 2 25 CQC

108272511/30/1211/30/1212K1135-BSD1 24.2 97 11 25 CQC

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MS %RTrichloroethene


CQC77.3-120PVH2309-0210225.612I0005-MS1 9/1/12 9/1/12 25

CQC77.3-120PVH2309-11 (22.3)11350.712I0028-MS1 9/4/12 9/4/12 25

CQC77.3-120PVH2037-07882212I0081-MS1 9/5/12 9/5/12 25

CQC77.3-120PVI0290-03 (4.79)9628.812I0215-MS1 9/7/12 9/7/12 25

CQC77.3-120PVI0609-0910927.312I0352-MS1 9/12/12 9/12/12 25

CQC,PSL77.3-120PVI0525-06 (55.7)1258712I0394-MS1 9/12/12 9/12/12 25

CQC77.3-120PVI0894-06 (64.7)10590.912I0598-MS1 9/18/12 9/18/12 25

CQC77.3-120PVI1060-029523.812I0648-MS1 9/18/12 9/18/12 25

CQC77.3-120PVI1553-08 (1.56)9124.312I0925-MS1 9/25/12 9/25/12 25

CQC77.3-120PVI1510-089623.912I0926-MS1 9/25/12 9/25/12 25

CQC77.3-120PVI1723-0311328.312I1065-MS1 9/28/12 9/28/12 25

CQC77.3-120PVI1822-029824.512I1095-MS1 9/28/12 9/28/12 25

CQC77.3-120PVI1869-0510526.312I1107-MS1 9/29/12 9/29/12 25

CQC77.3-120PVI1575-01 (0.37)11027.812J0008-MS1 10/1/12 10/1/12 25

77.3-120PVJ0513-03 (2.1)9425.612J0298-MS1 10/8/12 10/8/12 25

77.3-120PVJ0682-01962412J0389-MS1 10/10/12 10/10/12 25

CQC77.3-120PVJ0682-17 (132)9115512J0445-MS1 10/11/12 10/11/12 25

CQC77.3-120PVJ1065-029323.412J0620-MS1 10/16/12 10/16/12 25

CQC77.3-120PVJ1237-029423.412J0736-MS1 10/18/12 10/18/12 25

CQC77.3-120PVJ1405-0210927.412J0821-MS1 10/20/12 10/20/12 25

CQC,PSL77.3-120PVJ1405-17 (94.2)7711412J0850-MS1 10/22/12 10/22/12 25

CQC77.3-120PVJ1577-02 (5.07)9528.812J0972-MS1 10/24/12 10/24/12 25

CQC77.3-120PVJ1627-0110626612J1010-MS1 10/25/12 10/25/12 250

CQC77.3-120PVJ1600-0210325.812J1038-MS1 10/25/12 10/25/12 25

CQC77.3-120PVJ1577-18RE1 (1180)120148012J1059-MS1 10/26/12 10/26/12 250

CQC,PSL77.3-120PVK0237-0112731.712K0235-MS1 11/7/12 11/7/12 25

CQC77.3-120PVK0555-04 (69.1)9292.112K0286-MS1 11/8/12 11/8/12 25

77.3-120PVK0649-06 (46.2)9168.912K0341-MS1 11/9/12 11/9/12 25

CQC,M877.3-120PVK0756-01 (86.1)6810312K0415-MS1 11/12/12 11/12/12 25

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MS %RTrichloroetheneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC77.3-120PVK0793-0211027.412K0462-MS1 11/13/12 11/13/12 25

CQC77.3-120PVK0281-0110025.112K0522-MS1 11/14/12 11/14/12 25

CQC77.3-120PVK0632-0910425.912K0553-MS1 11/14/12 11/14/12 25

CQC77.3-120PVK0684-029824.512K0552-MS1 11/14/12 11/14/12 25

CQC77.3-120PVK0696-01 (8.15)11135.912K0581-MS1 11/15/12 11/15/12 25

CQC77.3-120PVK0934-01962412K0740-MS1 11/20/12 11/20/12 25

CQC77.3-120PVK0768-0211127.712K0751-MS1 11/20/12 11/20/12 25

CQC77.3-120PVK1220-029624.1X 12K0803-MS1 11/21/12 11/21/12 25

CQC77.3-120PVK1288-0310225.612K0836-MS1 11/21/12 11/21/12 25

CQC77.3-120PVK1375-0810325.812K0865-MS1 11/23/12 11/23/12 25

CQC77.3-120PVK1375-0210225.412K0855-MS1 11/23/12 11/23/12 25

CQC77.3-120PVK0988-031082712K0897-MS1 11/24/12 11/24/12 25

CQC77.3-120PVK1006-0111127.912K0905-MS1 11/25/12 11/25/12 25

CQC77.3-120PVK1450-10 (21.4)10447.512K1135-MS1 11/30/12 11/30/12 25

CQC77.3-120PVK1450-0311629.112K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDTrichloroethene


10225.5259/1/129/1/1212I0005-MSD1 CQC250.410225.6 PVH2309-02

11450.9259/4/129/4/1212I0028-MSD1 CQC250.411350.7 PVH2309-11 (22.3)

9022.5259/5/129/5/1212I0081-MSD1 CQC2528822 PVH2037-07

9729259/7/129/7/1212I0215-MSD1 CQC250.49628.8 PVI0290-03 (4.79)

10626.4259/12/129/12/1212I0352-MSD1 CQC25310927.3 PVI0609-09

11383.9259/12/129/12/1212I0394-MSD1 CQC25412587 PVI0525-06 (55.7)

9087.2259/18/129/18/1212I0598-MSD1 CQC25410590.9 PVI0894-06 (64.7)

9423.6259/18/129/18/1212I0648-MSD1 CQC250.79523.8 PVI1060-02

9324.7259/25/129/25/1212I0925-MSD1 CQC2529124.3 PVI1553-08 (1.56)

9824.6259/25/129/25/1212I0926-MSD1 CQC2539623.9 PVI1510-08

11027.5259/28/129/28/1212I1065-MSD1 CQC25311328.3 PVI1723-03

10426.1259/28/129/28/1212I1095-MSD1 CQC2569824.5 PVI1822-02

12731.7259/29/129/29/1212I1107-MSD1 CQC,PSL251910526.3 PVI1869-05

10827.32510/1/1210/1/1212J0008-MSD1 CQC25211027.8 PVI1575-01 (0.37)

9325.42510/8/1210/8/1212J0298-MSD1 2519425.6 PVJ0513-03 (2.1)

9824.42510/10/1210/10/1212J0389-MSD1 2529624 PVJ0682-01

931552510/11/1210/11/1212J0445-MSD1 CQC250.391155 PVJ0682-17 (132)

9924.62510/16/1210/16/1212J0620-MSD1 CQC2559323.4 PVJ1065-02

9724.12510/18/1210/18/1212J0736-MSD1 CQC2539423.4 PVJ1237-02

11428.52510/20/1210/20/1212J0821-MSD1 CQC25410927.4 PVJ1405-02

661112510/22/1210/22/1212J0850-MSD1 CQC,PSL25277114 PVJ1405-17 (94.2)

10130.42510/24/1210/24/1212J0972-MSD1 CQC2559528.8 PVJ1577-02 (5.07)

10726625010/25/1210/25/1212J1010-MSD1 CQC250.1106266 PVJ1627-01

10927.32510/25/1210/25/1212J1038-MSD1 CQC25610325.8 PVJ1600-02

119148025010/26/1210/26/1212J1059-MSD1 CQC250.21201480 PVJ1577-18RE1 (1180)

12731.72511/7/1211/7/1212K0235-MSD1 CQC,PSL250.0612731.7 PVK0237-01

9693.12511/8/1211/8/1212K0286-MSD1 CQC2519292.1 PVK0555-04 (69.1)

9068.72511/9/1211/9/1212K0341-MSD1 250.29168.9 PVK0649-06 (46.2)

3394.22511/12/1211/12/1212K0415-MSD1 CQC,M825968103 PVK0756-01 (86.1)

10526.32511/13/1211/13/1212K0462-MSD1 CQC25411027.4 PVK0793-02

10826.92511/14/1211/14/1212K0522-MSD1X CQC25710025.1 PVK0281-01

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MS/MSD RPDTrichloroethene%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

10626.62511/14/1211/14/1212K0553-MSD1 CQC25310425.9 PVK0632-09

10526.22511/14/1211/14/1212K0552-MSD1 CQC2579824.5 PVK0684-02

11135.82511/15/1211/15/1212K0581-MSD1 CQC250.411135.9 PVK0696-01 (8.15)

9724.22511/20/1211/20/1212K0740-MSD1 CQC250.79624 PVK0934-01

11127.72511/20/1211/20/1212K0751-MSD1 CQC250.0711127.7 PVK0768-02

10426.12511/21/1211/21/1212K0803-MSD1 CQC2589624.1 PVK1220-02

10225.52511/21/1211/21/1212K0836-MSD1 CQC250.210225.6 PVK1288-03

10425.92511/23/1211/23/1212K0865-MSD1 CQC250.510325.8 PVK1375-08

10225.42511/23/1211/23/1212K0855-MSD1 CQC250.0410225.4 PVK1375-02

104262511/24/1211/24/1212K0897-MSD1 CQC25410827 PVK0988-03

11428.52511/25/1211/25/1212K0905-MSD1 CQC25211127.9 PVK1006-01

11249.52511/30/1211/30/1212K1135-MSD1 CQC25410447.5 PVK1450-10 (21.4)

11328.22512/1/1211/30/1212K1134-MSD1 CQC25311629.1 PVK1450-03

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BLKTrichloroethene

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0.0

Plotted: 44

MDL: 0.19

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

3s: 0 ~------------------------------------------------------------~4.:0

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %RTrichlorofluoromethane


12I0005-BS1 29.6 118259/1/12 84.5-1239/1/12 CQC

12I0028-BS1 26.4 106259/4/12 84.5-1239/4/12 CQC

12I0081-BS1 30.6 122259/5/12 84.5-1239/5/12 CQC

12I0215-BS1 26 104259/7/12 84.5-1239/7/12 CQC

12I0352-BS1 30.2 121259/12/12 84.5-1239/12/12 CQC

12I0394-BS1 32.4 130259/12/12 84.5-1239/12/12 CQC,PSL

12I0598-BS1 30.8 123259/18/12 84.5-1239/18/12 CQC

12I0648-BS1 27.6 110259/18/12 84.5-1239/18/12 CQC

12I0926-BS1 28 112259/25/12 84.5-1239/25/12 CQC

12I0925-BS1 26.5 106259/25/12 84.5-1239/25/12 CQC

12I1065-BS1 30 120259/28/12 84.5-1239/28/12 CQC

12I1095-BS1 28.7 115259/28/12 84.5-1239/28/12 CQC

12I1107-BS1 29.1 116259/29/12 84.5-1239/29/12 CQC

12J0008-BS1 29.8 1192510/1/12 84.5-12310/1/12 CQC

12J0298-BS1 26.5 1062510/8/12 84.5-12310/8/12

12J0389-BS1 26.8 1072510/10/12 84.5-12310/10/12

12J0445-BS1 26 1042510/11/12 84.5-12310/11/12 CQC

12J0620-BS1 26.6 1062510/16/12 84.5-12310/16/12 CQC

12J0736-BS1 27.8 1112510/18/12 84.5-12310/18/12 CQC

12J0821-BS1 26.2 1052510/20/12 84.5-12310/20/12 CQC

12J0850-BS1 26.8 1072510/22/12 84.5-12310/22/12 CQC

12J0972-BS1 30.3 1212510/24/12 84.5-12310/24/12 CQC

12J1010-BS1 27.7 1112510/25/12 84.5-12310/25/12 CQC

12J1038-BS1 29 1162510/25/12 84.5-12310/25/12 CQC

12J1059-BS1 31.4 1262510/26/12 84.5-12310/26/12 CQC,L

12K0235-BS1 33.6 1342511/7/12 84.5-12311/7/12 CQC,PSL

12K0286-BS1 28 1122511/8/12 84.5-12311/8/12 CQC

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LCS %RTrichlorofluoromethaneLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 24 962511/9/12 84.5-12311/9/12

12K0415-BS1 24.4 982511/12/12 84.5-12311/12/12 CQC

12K0462-BS1 30.3 1212511/13/12 84.5-12311/13/12 CQC

12K0522-BS1 30.4 1222511/14/12 84.5-12311/14/12 CQC

12K0553-BS1 31.6 1262511/14/12 84.5-12311/14/12 CQC,L

12K0552-BS1 25.9 1042511/14/12 84.5-12311/14/12 CQC

12K0581-BS1 30.5 1222511/15/12 84.5-12311/15/12 CQC

12K0740-BS1 25.9 1042511/20/12 84.5-12311/20/12 CQC

12K0751-BS1 27 1082511/20/12 84.5-12311/20/12 CQC

12K0789-BS1 29.4 1182511/20/12 84.5-12311/20/12

12K0803-BS1 29.1 117X 2511/21/12 84.5-12311/21/12 CQC

12K0836-BS1 30 1202511/21/12 84.5-12311/21/12 CQC

12K0855-BS1 30.1 1202511/23/12 84.5-12311/23/12 CQC

12K0865-BS1 28.9 1162511/23/12 84.5-12311/23/12 CQC

12K0897-BS1 29.7 1192511/24/12 84.5-12311/24/12 CQC

12K0905-BS1 31.2 1252511/25/12 84.5-12311/25/12 CQC,PSL

12K1134-BS1 28.3 1132511/30/12 84.5-12311/30/12 CQC

12K1135-BS1 29.2 1172511/30/12 84.5-12311/30/12 CQC

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Analyzed By:

LCS/LCSD RPDTrichlorofluoromethane


10426.1259/1/129/1/1212I0005-BSD1 29.6 118 13 25 CQC

11629.1259/4/129/4/1212I0028-BSD1 26.4 106 10 25 CQC

12030.1259/5/129/5/1212I0081-BSD1 30.6 122 2 25 CQC

10426259/7/129/7/1212I0215-BSD1 26 104 0.3 25 CQC

11328.3259/12/129/12/1212I0352-BSD1 30.2 121 6 25 CQC

13132.8259/12/129/12/1212I0394-BSD1 32.4 130 1 25 CQC,PSL

12631.5259/18/129/18/1212I0598-BSD1 30.8 123 2 25 CQC,L

11328.3259/18/129/18/1212I0648-BSD1 27.6 110 3 25 CQC

10426.1259/25/129/25/1212I0926-BSD1 28 112 7 25 CQC

10425.9259/25/129/25/1212I0925-BSD1 26.5 106 2 25 CQC

11929.7259/28/129/28/1212I1065-BSD1 30 120 1 25 CQC

12330.7259/28/129/28/1212I1095-BSD1 28.7 115 7 25 CQC

11227.9259/29/129/29/1212I1107-BSD1 29.1 116 4 25 CQC

12130.22510/1/1210/1/1212J0008-BSD1 29.8 119 1 25 CQC

10726.82510/8/1210/8/1212J0298-BSD1 26.5 106 1 25

10526.32510/10/1210/10/1212J0389-BSD1 26.8 107 2 25

11328.22510/11/1210/11/1212J0445-BSD1 26 104 8 25 CQC

11127.82510/16/1210/16/1212J0620-BSD1 26.6 106 4 25 CQC

10826.92510/18/1210/18/1212J0736-BSD1 27.8 111 3 25 CQC

10025.12510/20/1210/20/1212J0821-BSD1 26.2 105 4 25 CQC

10325.72510/22/1210/22/1212J0850-BSD1 26.8 107 4 25 CQC

11127.82510/24/1210/24/1212J0972-BSD1 30.3 121 9 25 CQC

11127.82510/25/1210/25/1212J1010-BSD1 27.7 111 0.5 25 CQC

11929.82510/25/1210/25/1212J1038-BSD1 29 116 3 25 CQC

12330.72510/26/1210/26/1212J1059-BSD1 31.4 126 2 25 CQC

12731.72511/7/1211/7/1212K0235-BSD1 33.6 134 6 25 CQC,PSL

11027.52511/8/1211/8/1212K0286-BSD1 28 112 2 25 CQC

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LCS/LCSD RPDTrichlorofluoromethane%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

10626.42511/9/1211/9/1212K0341-BSD1 24 96 9 25

10025.12511/12/1211/12/1212K0415-BSD1 24.4 98 3 25 CQC

12230.62511/13/1211/13/1212K0462-BSD1 30.3 121 0.9 25 CQC

12029.92511/14/1211/14/1212K0522-BSD1X 30.4 122 2 25 CQC

11929.82511/14/1211/14/1212K0553-BSD1 31.6 126 6 25 CQC

10927.42511/14/1211/14/1212K0552-BSD1 25.9 104 5 25 CQC

120302511/15/1211/15/1212K0581-BSD1 30.5 122 2 25 CQC

10826.92511/20/1211/20/1212K0740-BSD1 25.9 104 4 25 CQC

10426.12511/20/1211/20/1212K0751-BSD1 27 108 3 25 CQC

11428.42511/20/1211/20/1212K0789-BSD1 29.4 118 3 25

12130.32511/21/1211/21/1212K0803-BSD1X 29.1 117 4 25 CQC

11428.62511/21/1211/21/1212K0836-BSD1 30 120 5 25 CQC

12130.22511/23/1211/23/1212K0855-BSD1 30.1 120 0.1 25 CQC

11528.82511/23/1211/23/1212K0865-BSD1 28.9 116 0.5 25 CQC

11929.82511/24/1211/24/1212K0897-BSD1 29.7 119 0.1 25 CQC

13132.72511/25/1211/25/1212K0905-BSD1 31.2 125 5 25 CQC,PSL

12230.42511/30/1211/30/1212K1134-BSD1 28.3 113 7 25 CQC

12731.82511/30/1211/30/1212K1135-BSD1 29.2 117 9 25 CQC,PSL

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MS %RTrichlorofluoromethane


CQC82.4-132PVH2309-0210826.912I0005-MS1 9/1/12 9/1/12 25

CQC82.4-132PVH2309-1112230.512I0028-MS1 9/4/12 9/4/12 25

CQC82.4-132PVH2037-0712230.412I0081-MS1 9/5/12 9/5/12 25

CQC82.4-132PVI0290-0311027.412I0215-MS1 9/7/12 9/7/12 25

CQC82.4-132PVI0609-0912029.912I0352-MS1 9/12/12 9/12/12 25

CQC,PSL82.4-132PVI0525-06 (0.32)13634.412I0394-MS1 9/12/12 9/12/12 25

CQC82.4-132PVI0894-0613032.612I0598-MS1 9/18/12 9/18/12 25

CQC82.4-132PVI1060-0211328.312I0648-MS1 9/18/12 9/18/12 25

CQC82.4-132PVI1553-0810225.612I0925-MS1 9/25/12 9/25/12 25

CQC82.4-132PVI1510-0810526.312I0926-MS1 9/25/12 9/25/12 25

CQC82.4-132PVI1723-0312731.712I1065-MS1 9/28/12 9/28/12 25

CQC82.4-132PVI1822-0211328.212I1095-MS1 9/28/12 9/28/12 25

CQC82.4-132PVI1869-0511628.912I1107-MS1 9/29/12 9/29/12 25

CQC82.4-132PVI1575-0112030.112J0008-MS1 10/1/12 10/1/12 25

82.4-132PVJ0513-0311227.912J0298-MS1 10/8/12 10/8/12 25

82.4-132PVJ0682-0111328.112J0389-MS1 10/10/12 10/10/12 25

CQC82.4-132PVJ0682-1710426.112J0445-MS1 10/11/12 10/11/12 25

CQC82.4-132PVJ1065-0210626.612J0620-MS1 10/16/12 10/16/12 25

CQC82.4-132PVJ1237-0210827.112J0736-MS1 10/18/12 10/18/12 25

CQC82.4-132PVJ1405-0210726.812J0821-MS1 10/20/12 10/20/12 25

CQC82.4-132PVJ1405-1710325.712J0850-MS1 10/22/12 10/22/12 25

CQC82.4-132PVJ1577-0211528.812J0972-MS1 10/24/12 10/24/12 25

CQC82.4-132PVJ1627-0110726812J1010-MS1 10/25/12 10/25/12 250

CQC82.4-132PVJ1600-0211528.812J1038-MS1 10/25/12 10/25/12 25

CQC82.4-132PVJ1577-18RE112832012J1059-MS1 10/26/12 10/26/12 250

CQC82.4-132PVK0237-0113032.612K0235-MS1 11/7/12 11/7/12 25

CQC82.4-132PVK0555-0413032.412K0286-MS1 11/8/12 11/8/12 25

82.4-132PVK0649-0610826.912K0341-MS1 11/9/12 11/9/12 25

CQC82.4-132PVK0756-0110426.112K0415-MS1 11/12/12 11/12/12 25

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MS %RTrichlorofluoromethaneSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC82.4-132PVK0793-0212330.712K0462-MS1 11/13/12 11/13/12 25

CQC82.4-132PVK0281-0111729.3X 12K0522-MS1 11/14/12 11/14/12 25

CQC82.4-132PVK0632-0912430.912K0553-MS1 11/14/12 11/14/12 25

CQC82.4-132PVK0684-0211228.112K0552-MS1 11/14/12 11/14/12 25

CQC82.4-132PVK0696-0112130.312K0581-MS1 11/15/12 11/15/12 25

CQC82.4-132PVK0934-0110927.212K0740-MS1 11/20/12 11/20/12 25

CQC82.4-132PVK0768-0211929.712K0751-MS1 11/20/12 11/20/12 25

CQC82.4-132PVK1220-0211027.4X 12K0803-MS1 11/21/12 11/21/12 25

CQC82.4-132PVK1288-0312230.612K0836-MS1 11/21/12 11/21/12 25

CQC82.4-132PVK1375-0812230.412K0865-MS1 11/23/12 11/23/12 25

CQC82.4-132PVK1375-0213032.512K0855-MS1 11/23/12 11/23/12 25

CQC82.4-132PVK0988-0312330.712K0897-MS1 11/24/12 11/24/12 25

CQC82.4-132PVK1006-0113132.712K0905-MS1 11/25/12 11/25/12 25

CQC82.4-132PVK1450-1011628.912K1135-MS1 11/30/12 11/30/12 25

CQC,M782.4-132PVK1450-0314335.812K1134-MS1 11/30/12 12/1/12 25

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Analyzed By:

MS/MSD RPDTrichlorofluoromethane


11227.9259/1/129/1/1212I0005-MSD1 CQC25410826.9 PVH2309-02

11629.1259/4/129/4/1212I0028-MSD1 CQC25512230.5 PVH2309-11

12531.3259/5/129/5/1212I0081-MSD1 CQC25312230.4 PVH2037-07

10526.3259/7/129/7/1212I0215-MSD1 CQC25411027.4 PVI0290-03

11328.4259/12/129/12/1212I0352-MSD1 CQC25512029.9 PVI0609-09

13634.4259/12/129/12/1212I0394-MSD1 CQC,PSL250.113634.4 PVI0525-06 (0.32)

12832259/18/129/18/1212I0598-MSD1 CQC25213032.6 PVI0894-06

10626.4259/18/129/18/1212I0648-MSD1 CQC25711328.3 PVI1060-02

10426259/25/129/25/1212I0925-MSD1 CQC25210225.6 PVI1553-08

10927.2259/25/129/25/1212I0926-MSD1 CQC25310526.3 PVI1510-08

12531.4259/28/129/28/1212I1065-MSD1 CQC25112731.7 PVI1723-03

12531.3259/28/129/28/1212I1095-MSD1 CQC251011328.2 PVI1822-02

13333.2259/29/129/29/1212I1107-MSD1 CQC,PSL251411628.9 PVI1869-05

12330.72510/1/1210/1/1212J0008-MSD1 CQC25212030.1 PVI1575-01

112282510/8/1210/8/1212J0298-MSD1 250.411227.9 PVJ0513-03

11127.82510/10/1210/10/1212J0389-MSD1 25111328.1 PVJ0682-01

10125.32510/11/1210/11/1212J0445-MSD1 CQC25310426.1 PVJ0682-17

11027.62510/16/1210/16/1212J0620-MSD1 CQC25410626.6 PVJ1065-02

11328.22510/18/1210/18/1212J0736-MSD1 CQC25410827.1 PVJ1237-02

11829.42510/20/1210/20/1212J0821-MSD1 CQC25910726.8 PVJ1405-02

10526.32510/22/1210/22/1212J0850-MSD1 CQC25210325.7 PVJ1405-17

12531.12510/24/1210/24/1212J0972-MSD1 CQC25811528.8 PVJ1577-02

10526425010/25/1210/25/1212J1010-MSD1 CQC252107268 PVJ1627-01

11929.82510/25/1210/25/1212J1038-MSD1 CQC25311528.8 PVJ1600-02

13233125010/26/1210/26/1212J1059-MSD1 CQC253128320 PVJ1577-18RE1

13734.42511/7/1211/7/1212K0235-MSD1 CQC,PSL25513032.6 PVK0237-01

12230.62511/8/1211/8/1212K0286-MSD1 CQC25613032.4 PVK0555-04

10826.92511/9/1211/9/1212K0341-MSD1 250.0410826.9 PVK0649-06

10526.12511/12/1211/12/1212K0415-MSD1 CQC250.210426.1 PVK0756-01

12230.52511/13/1211/13/1212K0462-MSD1 CQC250.812330.7 PVK0793-02

12130.42511/14/1211/14/1212K0522-MSD1 CQC25411729.3 PVK0281-01

01/02/13 15:46

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MS/MSD RPDTrichlorofluoromethane%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

120302511/14/1211/14/1212K0553-MSD1 CQC25312430.9 PVK0632-09

11528.82511/14/1211/14/1212K0552-MSD1 CQC25211228.1 PVK0684-02

13834.42511/15/1211/15/1212K0581-MSD1 CQC,M7251312130.3 PVK0696-01

10626.62511/20/1211/20/1212K0740-MSD1 CQC25210927.2 PVK0934-01

12130.32511/20/1211/20/1212K0751-MSD1 CQC25211929.7 PVK0768-02

11929.82511/21/1211/21/1212K0803-MSD1 CQC25811027.4 PVK1220-02

120302511/21/1211/21/1212K0836-MSD1 CQC25212230.6 PVK1288-03

12029.92511/23/1211/23/1212K0865-MSD1 CQC25212230.4 PVK1375-08

12430.92511/23/1211/23/1212K0855-MSD1 CQC25513032.5 PVK1375-02

13132.72511/24/1211/24/1212K0897-MSD1 CQC25612330.7 PVK0988-03

13132.82511/25/1211/25/1212K0905-MSD1 CQC250.413132.7 PVK1006-01

12230.42511/30/1211/30/1212K1135-MSD1 CQC25511628.9 PVK1450-10

14135.22512/1/1211/30/1212K1134-MSD1 CQC,M725214335.8 PVK1450-03

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BLKTrichlorofluoromethane

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0.0

Plotted: 44

MDL: 0.17

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

3s: 0

~------------------------------------------------------------__,4.:0

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %RVinyl Acetate


12K0235-BS1 41.6 1662511/7/12 70.5-13411/7/12 CQC,L

12K0286-BS1 35.4 1422511/8/12 70.5-13411/8/12 CQC,L

12K0341-BS1 27.6 1112511/9/12 70.5-13411/9/12

12K0415-BS1 32.4 1302511/12/12 70.5-13411/12/12 CQC

12K0462-BS1 42.3 1692511/13/12 70.5-13411/13/12 CQC,L,N1

12K0522-BS1 39 1562511/14/12 70.5-13411/14/12 CQC,L,N1

12K0803-BS1 45 1802511/21/12 70.5-13411/21/12 CQC,L

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LCS/LCSD RPDVinyl Acetate


15538.62511/7/1211/7/1212K0235-BSD1 41.6 166 7 25 CQC,L

13533.62511/8/1211/8/1212K0286-BSD1 35.4 142 5 25 CQC,L

11027.52511/9/1211/9/1212K0341-BSD1 27.6 111 0.4 25

12631.42511/12/1211/12/1212K0415-BSD1 32.4 130 3 25 CQC

16140.32511/13/1211/13/1212K0462-BSD1 42.3 169 5 25 CQC,L,N1

15438.62511/14/1211/14/1212K0522-BSD1 39 156 1 25 CQC,L,N1

19348.22511/21/1211/21/1212K0803-BSD1 45 180 7 25 CQC,L

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MS %RVinyl Acetate


CQC,M1450-139PVK0237-011523812K0235-MS1 11/7/12 11/7/12 25

CQC50-139PVK0555-0413333.412K0286-MS1 11/8/12 11/8/12 25

50-139PVK0649-0610927.312K0341-MS1 11/9/12 11/9/12 25

CQC50-139PVK0756-0113533.812K0415-MS1 11/12/12 11/12/12 25

CQC,M14,N150-139PVK0793-0214335.812K0462-MS1 11/13/12 11/13/12 25

CQC,M14,N150-139PVK0281-0115137.812K0522-MS1 11/14/12 11/14/12 25

CQC50-139PVK1220-0210425.912K0803-MS1 11/21/12 11/21/12 25

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MS/MSD RPDVinyl Acetate


15538.82511/7/1211/7/1212K0235-MSD1 CQC,M1425215238 PVK0237-01

124312511/8/1211/8/1212K0286-MSD1 CQC25713333.4 PVK0555-04

10927.22511/9/1211/9/1212K0341-MSD1 250.710927.3 PVK0649-06

136342511/12/1211/12/1212K0415-MSD1 CQC250.713533.8 PVK0756-01

14736.82511/13/1211/13/1212K0462-MSD1 CQC,M14,N125314335.8 PVK0793-02

15639.12511/14/1211/14/1212K0522-MSD1 CQC,M14,N125315137.8 PVK0281-01

104262511/21/1211/21/1212K0803-MSD1 CQC250.610425.9 PVK1220-02

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BLKVinyl Acetate

01/02/13 15:46

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LCS %RVinyl chloride


12I0005-BS1 27.4 109259/1/12 80.9-1279/1/12 CQC

12I0028-BS1 25.2 101259/4/12 80.9-1279/4/12 CQC

12I0081-BS1 23.9 96259/5/12 80.9-1279/5/12 CQC

12I0215-BS1 22 88259/7/12 80.9-1279/7/12 CQC

12I0352-BS1 28.4 113259/12/12 80.9-1279/12/12 CQC

12I0394-BS1 25.5 102259/12/12 80.9-1279/12/12 CQC

12I0598-BS1 29.3 117259/18/12 80.9-1279/18/12 CQC

12I0648-BS1 26 104259/18/12 80.9-1279/18/12 CQC

12I0926-BS1 23.8 95259/25/12 80.9-1279/25/12 CQC

12I0925-BS1 22 88259/25/12 80.9-1279/25/12 CQC

12I1065-BS1 26 104259/28/12 80.9-1279/28/12 CQC

12I1095-BS1 24.9 99259/28/12 80.9-1279/28/12 CQC

12I1107-BS1 25.3 101259/29/12 80.9-1279/29/12 CQC

12J0008-BS1 25 1002510/1/12 80.9-12710/1/12 CQC

12J0298-BS1 22.4 902510/8/12 80.9-12710/8/12

12J0389-BS1 22.5 902510/10/12 80.9-12710/10/12

12J0445-BS1 22.7 912510/11/12 80.9-12710/11/12 CQC

12J0620-BS1 21.6 862510/16/12 80.9-12710/16/12 CQC

12J0736-BS1 22.9 922510/18/12 80.9-12710/18/12 CQC

12J0821-BS1 19.3 772510/20/12 80.9-12710/20/12 CQC,PSL

12J0850-BS1 21.8 872510/22/12 80.9-12710/22/12 CQC

12J0972-BS1 24.5 982510/24/12 80.9-12710/24/12 CQC

12J1010-BS1 19.3 772510/25/12 80.9-12710/25/12 CQC,PSL

12J1038-BS1 21.8 872510/25/12 80.9-12710/25/12 CQC

12J1059-BS1 20 802510/26/12 80.9-12710/26/12 CQC,PSL

12K0235-BS1 32.4 1302511/7/12 80.9-12711/7/12 CQC,PSL

12K0286-BS1 26.1 1042511/8/12 80.9-12711/8/12 CQC

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LCS %RVinyl chlorideLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K0341-BS1 17.5 702511/9/12 80.9-12711/9/12

12K0415-BS1 20.2 812511/12/12 80.9-12711/12/12 CQC

12K0462-BS1 25.6 1022511/13/12 80.9-12711/13/12 CQC

12K0522-BS1 23.6 942511/14/12 80.9-12711/14/12 CQC

12K0553-BS1 22.8 912511/14/12 80.9-12711/14/12 CQC

12K0552-BS1 21.6 862511/14/12 80.9-12711/14/12 CQC

12K0581-BS1 23.8 952511/15/12 80.9-12711/15/12 CQC

12K0740-BS1 22.3 892511/20/12 80.9-12711/20/12 CQC

12K0751-BS1 22.2 892511/20/12 80.9-12711/20/12 CQC

12K0789-BS1 25.6 1022511/20/12 80.9-12711/20/12

12K0803-BS1 24.6 982511/21/12 80.9-12711/21/12 CQC

12K0836-BS1 25.5 1022511/21/12 80.9-12711/21/12 CQC

12K0855-BS1 25.2 1012511/23/12 80.9-12711/23/12 CQC

12K0865-BS1 24.1 962511/23/12 80.9-12711/23/12 CQC

12K0897-BS1 22.7 912511/24/12 80.9-12711/24/12 CQC

12K0905-BS1 23.7 952511/25/12 80.9-12711/25/12 CQC

12K1134-BS1 21.1 852511/30/12 80.9-12711/30/12 CQC

12K1135-BS1 24.7 992511/30/12 80.9-12711/30/12 CQC

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LCS/LCSD RPDVinyl chloride


9523.8259/1/129/1/1212I0005-BSD1 27.4 109 14 25 CQC

10726.7259/4/129/4/1212I0028-BSD1 25.2 101 6 25 CQC

9523.7259/5/129/5/1212I0081-BSD1 23.9 96 0.8 25 CQC

8721.8259/7/129/7/1212I0215-BSD1 22 88 1 25 CQC

10726.7259/12/129/12/1212I0352-BSD1 28.4 113 6 25 CQC

9924.8259/12/129/12/1212I0394-BSD1 25.5 102 3 25 CQC

11729.3259/18/129/18/1212I0598-BSD1 29.3 117 0.03 25 CQC

10626.5259/18/129/18/1212I0648-BSD1 26 104 2 25 CQC

9223.1259/25/129/25/1212I0926-BSD1 23.8 95 3 25 CQC

8320.8259/25/129/25/1212I0925-BSD1 22 88 6 25 CQC

10225.6259/28/129/28/1212I1065-BSD1 26 104 2 25 CQC

10626.5259/28/129/28/1212I1095-BSD1 24.9 99 6 25 CQC

9323.3259/29/129/29/1212I1107-BSD1 25.3 101 8 25 CQC

10526.12510/1/1210/1/1212J0008-BSD1 25 100 4 25 CQC

9122.82510/8/1210/8/1212J0298-BSD1 22.4 90 2 25

9122.72510/10/1210/10/1212J0389-BSD1 22.5 90 0.8 25

9323.32510/11/1210/11/1212J0445-BSD1 22.7 91 3 25 CQC

9022.62510/16/1210/16/1212J0620-BSD1 21.6 86 4 25 CQC

9022.62510/18/1210/18/1212J0736-BSD1 22.9 92 1 25 CQC

7518.72510/20/1210/20/1212J0821-BSD1 19.3 77 3 25 CQC,PSL

8320.62510/22/1210/22/1212J0850-BSD1 21.8 87 6 25 CQC

9022.52510/24/1210/24/1212J0972-BSD1 24.5 98 9 25 CQC

7318.32510/25/1210/25/1212J1010-BSD1 19.3 77 5 25 CQC,PSL

8922.32510/25/1210/25/1212J1038-BSD1 21.8 87 2 25 CQC

8120.22510/26/1210/26/1212J1059-BSD1 20 80 0.8 25 CQC

120302511/7/1211/7/1212K0235-BSD1 32.4 130 8 25 CQC

10526.22511/8/1211/8/1212K0286-BSD1 26.1 104 0.4 25 CQC

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LCS/LCSD RPDVinyl chloride%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

8120.22511/9/1211/9/1212K0341-BSD1 17.5 70 14 25

8019.92511/12/1211/12/1212K0415-BSD1 20.2 81 2 25 CQC,PSL

10125.32511/13/1211/13/1212K0462-BSD1 25.6 102 1 25 CQC

9423.52511/14/1211/14/1212K0522-BSD1X 23.6 94 0.4 25 CQC

9924.72511/14/1211/14/1212K0553-BSD1 22.8 91 8 25 CQC

8922.32511/14/1211/14/1212K0552-BSD1 21.6 86 3 25 CQC

92232511/15/1211/15/1212K0581-BSD1 23.8 95 4 25 CQC

9022.62511/20/1211/20/1212K0740-BSD1 22.3 89 1 25 CQC

8621.42511/20/1211/20/1212K0751-BSD1 22.2 89 3 25 CQC

96242511/20/1211/20/1212K0789-BSD1 25.6 102 7 25

10325.82511/21/1211/21/1212K0803-BSD1 24.6 98 5 25 CQC

9724.22511/21/1211/21/1212K0836-BSD1 25.5 102 5 25 CQC

10125.32511/23/1211/23/1212K0855-BSD1 25.2 101 0.5 25 CQC

9523.92511/23/1211/23/1212K0865-BSD1 24.1 96 0.9 25 CQC

9223.12511/24/1211/24/1212K0897-BSD1 22.7 91 2 25 CQC

9824.52511/25/1211/25/1212K0905-BSD1 23.7 95 3 25 CQC

92232511/30/1211/30/1212K1134-BSD1 21.1 85 8 25 CQC

108272511/30/1211/30/1212K1135-BSD1 24.7 99 9 25 CQC

01/02/13 15:46

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MS %RVinyl chloride


CQC69.2-143PVH2309-029523.612I0005-MS1 9/1/12 9/1/12 25

CQC69.2-143PVH2309-1110927.212I0028-MS1 9/4/12 9/4/12 25

CQC69.2-143PVH2037-07882212I0081-MS1 9/5/12 9/5/12 25

CQC69.2-143PVI0290-038721.712I0215-MS1 9/7/12 9/7/12 25

CQC69.2-143PVI0609-0911027.512I0352-MS1 9/12/12 9/12/12 25

CQC69.2-143PVI0525-0610626.412I0394-MS1 9/12/12 9/12/12 25

CQC69.2-143PVI0894-061162912I0598-MS1 9/18/12 9/18/12 25

CQC69.2-143PVI1060-0210125.212I0648-MS1 9/18/12 9/18/12 25

CQC69.2-143PVI1553-088220.512I0925-MS1 9/25/12 9/25/12 25

CQC69.2-143PVI1510-088721.712I0926-MS1 9/25/12 9/25/12 25

CQC69.2-143PVI1723-0310526.312I1065-MS1 9/28/12 9/28/12 25

CQC69.2-143PVI1822-029724.212I1095-MS1 9/28/12 9/28/12 25

CQC69.2-143PVI1869-059924.712I1107-MS1 9/29/12 9/29/12 25

CQC69.2-143PVI1575-019824.412J0008-MS1 10/1/12 10/1/12 25

69.2-143PVJ0513-03922312J0298-MS1 10/8/12 10/8/12 25

69.2-143PVJ0682-01922312J0389-MS1 10/10/12 10/10/12 25

CQC69.2-143PVJ0682-178320.712J0445-MS1 10/11/12 10/11/12 25

CQC69.2-143PVJ1065-02882212J0620-MS1 10/16/12 10/16/12 25

CQC69.2-143PVJ1237-02882212J0736-MS1 10/18/12 10/18/12 25

CQC69.2-143PVJ1405-02842112J0821-MS1 10/20/12 10/20/12 25

CQC69.2-143PVJ1405-178020.112J0850-MS1 10/22/12 10/22/12 25

CQC69.2-143PVJ1577-029222.912J0972-MS1 10/24/12 10/24/12 25

CQC69.2-143PVJ1627-017117912J1010-MS1 10/25/12 10/25/12 250

CQC69.2-143PVJ1600-028821.912J1038-MS1 10/25/12 10/25/12 25

CQC69.2-143PVJ1577-18RE19824612J1059-MS1 10/26/12 10/26/12 250

CQC69.2-143PVK0237-0111729.212K0235-MS1 11/7/12 11/7/12 25

CQC69.2-143PVK0555-0411428.512K0286-MS1 11/8/12 11/8/12 25

69.2-143PVK0649-067318.312K0341-MS1 11/9/12 11/9/12 25

CQC69.2-143PVK0756-01802012K0415-MS1 11/12/12 11/12/12 25

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MS %RVinyl chlorideSource%RResultSpike LevelAnalyzedPreparedSample IDRjct QualifiersLimits

CQC69.2-143PVK0793-0210325.812K0462-MS1 11/13/12 11/13/12 25

CQC69.2-143PVK0281-019724.212K0522-MS1 11/14/12 11/14/12 25

CQC69.2-143PVK0632-099924.712K0553-MS1 11/14/12 11/14/12 25

CQC69.2-143PVK0684-029022.512K0552-MS1 11/14/12 11/14/12 25

CQC69.2-143PVK0696-018621.512K0581-MS1 11/15/12 11/15/12 25

CQC69.2-143PVK0934-019022.412K0740-MS1 11/20/12 11/20/12 25

CQC69.2-143PVK0768-029623.912K0751-MS1 11/20/12 11/20/12 25

CQC69.2-143PVK1220-029222.9X 12K0803-MS1 11/21/12 11/21/12 25

CQC69.2-143PVK1288-0310325.712K0836-MS1 11/21/12 11/21/12 25

CQC69.2-143PVK1375-08922312K0865-MS1 11/23/12 11/23/12 25

CQC69.2-143PVK1375-0211328.312K0855-MS1 11/23/12 11/23/12 25

CQC69.2-143PVK0988-039724.112K0897-MS1 11/24/12 11/24/12 25

CQC69.2-143PVK1006-0110225.412K0905-MS1 11/25/12 11/25/12 25

CQC69.2-143PVK1450-10962412K1135-MS1 11/30/12 11/30/12 25

CQC69.2-143PVK1450-0310626.512K1134-MS1 11/30/12 12/1/12 25

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MS/MSD RPDVinyl chloride


10025259/1/129/1/1212I0005-MSD1 CQC2569523.6 PVH2309-02

10225.6259/4/129/4/1212I0028-MSD1 CQC25610927.2 PVH2309-11

9122.8259/5/129/5/1212I0081-MSD1 CQC2548822 PVH2037-07

8822259/7/129/7/1212I0215-MSD1 CQC2518721.7 PVI0290-03

10325.8259/12/129/12/1212I0352-MSD1 CQC25611027.5 PVI0609-09

10626.5259/12/129/12/1212I0394-MSD1 CQC250.410626.4 PVI0525-06

11428.4259/18/129/18/1212I0598-MSD1 CQC25211629 PVI0894-06

9624.1259/18/129/18/1212I0648-MSD1 CQC25510125.2 PVI1060-02

8120.1259/25/129/25/1212I0925-MSD1 CQC2528220.5 PVI1553-08

9222.9259/25/129/25/1212I0926-MSD1 CQC2558721.7 PVI1510-08

9924.8259/28/129/28/1212I1065-MSD1 CQC25610526.3 PVI1723-03

10024.9259/28/129/28/1212I1095-MSD1 CQC2539724.2 PVI1822-02

10927.2259/29/129/29/1212I1107-MSD1 CQC25109924.7 PVI1869-05

10526.22510/1/1210/1/1212J0008-MSD1 CQC2579824.4 PVI1575-01

9022.62510/8/1210/8/1212J0298-MSD1 2529223 PVJ0513-03

9222.92510/10/1210/10/1212J0389-MSD1 250.099223 PVJ0682-01

8120.32510/11/1210/11/1212J0445-MSD1 CQC2528320.7 PVJ0682-17

8922.32510/16/1210/16/1212J0620-MSD1 CQC2528822 PVJ1065-02

9122.82510/18/1210/18/1212J0736-MSD1 CQC2548822 PVJ1237-02

8521.22510/20/1210/20/1212J0821-MSD1 CQC2518421 PVJ1405-02

80202510/22/1210/22/1212J0850-MSD1 CQC250.58020.1 PVJ1405-17

9824.52510/24/1210/24/1212J0972-MSD1 CQC2579222.9 PVJ1577-02

7117825010/25/1210/25/1212J1010-MSD1 CQC250.271179 PVJ1627-01

8821.92510/25/1210/25/1212J1038-MSD1 CQC250.098821.9 PVJ1600-02

9122725010/26/1210/26/1212J1059-MSD1 CQC25898246 PVJ1577-18RE1

12631.42511/7/1211/7/1212K0235-MSD1 CQC25711729.2 PVK0237-01

10927.22511/8/1211/8/1212K0286-MSD1 CQC25411428.5 PVK0555-04

6917.22511/9/1211/9/1212K0341-MSD1 2567318.3 PVK0649-06

7719.22511/12/1211/12/1212K0415-MSD1 CQC2548020 PVK0756-01

10125.22511/13/1211/13/1212K0462-MSD1 CQC25210325.8 PVK0793-02

9323.32511/14/1211/14/1212K0522-MSD1X CQC2549724.2 PVK0281-01

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MS/MSD RPDVinyl chloride%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup %RDup QualifiersLimitRPDSource

9222.92511/14/1211/14/1212K0553-MSD1 CQC2579924.7 PVK0632-09

9122.72511/14/1211/14/1212K0552-MSD1 CQC250.89022.5 PVK0684-02

10626.52511/15/1211/15/1212K0581-MSD1 CQC25218621.5 PVK0696-01

8922.22511/20/1211/20/1212K0740-MSD1 CQC2519022.4 PVK0934-01

10125.22511/20/1211/20/1212K0751-MSD1 CQC2559623.9 PVK0768-02

9724.12511/21/1211/21/1212K0803-MSD1X CQC2559222.9 PVK1220-02

10526.32511/21/1211/21/1212K0836-MSD1 CQC25210325.7 PVK1288-03

9523.82511/23/1211/23/1212K0865-MSD1 CQC2539223 PVK1375-08

96242511/23/1211/23/1212K0855-MSD1 CQC251611328.3 PVK1375-02

10325.72511/24/1211/24/1212K0897-MSD1 CQC2569724.1 PVK0988-03

9423.62511/25/1211/25/1212K0905-MSD1 CQC25710225.4 PVK1006-01

10125.32511/30/1211/30/1212K1135-MSD1 CQC2559624 PVK1450-10

10325.82512/1/1211/30/1212K1134-MSD1 CQC25310626.5 PVK1450-03

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BLKVinyl chloride

1.0

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0.0

Plotted: 44

MDL: 0.24

MRL: 1

Rejected: 2

Stdv: 0

Mean: 0

2s: 0

~------------------------------------------------------------~3•:0 4s: 0

3 5 7 9 11 13 15 17 19 21 23 25 27 29 31 33 35 37 39 41 43

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LCS %RPerchlorate


12I0049-BS1 21.4 86259/4/12 85-1159/4/12

12I0099-BS1 21.4 85259/5/12 85-1159/5/12

12I0279-BS1 0X 259/10/12 85-1159/10/12

12I0326-BS1 23.6 94259/11/12 85-1159/11/12

12I0426-BS1 23.2 93259/12/12 85-1159/12/12

12I0482-BS1 25.8 103259/13/12 85-1159/13/12

12I0623-BS1 23 92259/18/12 85-1159/18/12

12I0912-BS1 23.3 93259/25/12 85-1159/25/12

12I1035-BS1 26.1 105259/27/12 85-1159/27/12

12I1101-BS1 26.4 106259/28/12 85-1159/28/12

12J0037-BS1 26.5 1062510/1/12 85-11510/1/12

12J0317-BS1 26.6 1062510/8/12 85-11510/8/12

12J0372-BS1 27.2 1092510/9/12 85-11510/9/12

12J0427-BS1 27.1 1082510/10/12 85-11510/10/12

12J0662-BS1 25.9 1042510/16/12 85-11510/16/12

12J0751-BS1 26.2 1052510/17/12 85-11510/17/12

12J0760-BS1 25.8 1032510/18/12 85-11510/18/12

12J0865-BS1 25.1 1002510/22/12 85-11510/22/12

12J0980-BS1 26 1042510/24/12 85-11510/24/12

12K0270-BS1 27.4 1092511/7/12 85-11511/7/12

12K0434-BS1 28.3 1132511/12/12 85-11511/12/12

12K0505-BS1 27.4 1092511/13/12 85-11511/13/12

12K0719-BS1 25.3 1012511/19/12 85-11511/19/12

12K0783-BS1 26.9 1082511/20/12 85-11511/20/12

12K0838-BS1 25 1002511/21/12 85-11511/21/12

12K0888-BS1 25.3 1012511/23/12 85-11511/23/12

12K1019-BS1 24.9 992511/28/12 85-11511/28/12

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LCS %RPerchlorateLimits QualifiersSample ID Prepared Spike Level Result %RRjct Analyzed

12K1067-BS1 25.4 1012511/29/12 85-11511/29/12

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LCS/LCSD RPDPerchlorate


8821.9259/4/129/4/1212I0049-BSD1 21.4 86 2 15

8621.4259/5/129/5/1212I0099-BSD1 21.4 85 0.4 15

0259/10/129/10/1212I0279-BSD1X 0 15

8521.3259/11/129/11/1212I0326-BSD1 23.6 94 10 15

10025259/12/129/12/1212I0426-BSD1 23.2 93 7 15

9724.3259/13/129/13/1212I0482-BSD1 25.8 103 6 15

10225.6259/18/129/18/1212I0623-BSD1 23 92 11 15

10024.9259/25/129/25/1212I0912-BSD1 23.3 93 7 15

10626.6259/27/129/27/1212I1035-BSD1 26.1 105 2 15

10726.6259/28/129/28/1212I1101-BSD1 26.4 106 0.7 15

104262510/1/1210/1/1212J0037-BSD1 26.5 106 2 15

10827.12510/8/1210/8/1212J0317-BSD1 26.6 106 2 15

10927.42510/9/1210/9/1212J0372-BSD1 27.2 109 0.7 15

10927.22510/10/1210/10/1212J0427-BSD1 27.1 108 0.3 15

10927.32510/16/1210/16/1212J0662-BSD1 25.9 104 5 15

10125.22510/17/1210/17/1212J0751-BSD1 26.2 105 4 15

10626.52510/18/1210/18/1212J0760-BSD1 25.8 103 3 15

9724.32510/22/1210/22/1212J0865-BSD1 25.1 100 3 15

10225.42510/24/1210/24/1212J0980-BSD1 26 104 2 15

10927.22511/7/1211/7/1212K0270-BSD1 27.4 109 0.5 15

112282511/12/1211/12/1212K0434-BSD1 28.3 113 0.8 15

10726.72511/13/1211/13/1212K0505-BSD1 27.4 109 2 15

10626.52511/19/1211/19/1212K0719-BSD1 25.3 101 5 15

9924.72511/20/1211/20/1212K0783-BSD1 26.9 108 9 15

10325.72511/21/1211/21/1212K0838-BSD1 25 100 3 15

10526.22511/23/1211/23/1212K0888-BSD1 25.3 101 3 15

10726.72511/28/1211/28/1212K1019-BSD1 24.9 99 7 15

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LCS/LCSD RPDPerchlorate%RResultSpike LevelAnalyzedPreparedSample IDRjct Dup Dup %R RPD Limit Qualifiers

10325.82511/29/1211/29/1212K1067-BSD1 25.4 101 2 15

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MS %RPerchlorate


80-120PVH2309-02 (3.03)9125.912I0049-MS1 9/4/12 9/4/12 25

80-120PVH2238-01 (3.69)9326.912I0099-MS1 9/5/12 9/5/12 25

80-120PVI0290-050X 12I0279-MS1 9/10/12 9/10/12 25

80-120PVI0290-05RE1 (5.45)10932.712I0326-MS1 9/11/12 9/11/12 25

80-120PVI0609-15 (4.42)6721.212I0426-MS1 9/12/12 9/12/12 25

M880-120PVI0609-15RE1 (2.12)7721.312I0482-MS1 9/13/12 9/13/12 25

80-120PVI1060-03 (4.67)9127.312I0623-MS1 9/18/12 9/18/12 25

80-120PVI1553-05 (2.67)8724.312I0912-MS1 9/25/12 9/25/12 25

80-120PVI1723-03 (3.56)982812I1035-MS1 9/27/12 9/27/12 25

80-120PVI1822-02 (1.6)9926.312I1101-MS1 9/28/12 9/28/12 25

80-120PVI1869-16 (3.82)9828.312J0037-MS1 10/1/12 10/1/12 25

80-120PVJ0513-11 (1.9)10227.412J0317-MS1 10/8/12 10/8/12 25

80-120PVJ0513-12 (2.23)10227.712J0372-MS1 10/9/12 10/9/12 25

80-120PVJ0682-03 (4.51)10430.612J0427-MS1 10/10/12 10/10/12 25

80-120PVJ1065-02 (2.95)1002812J0662-MS1 10/16/12 10/16/12 25

80-120PVJ1065-09 (3.73)10028.612J0751-MS1 10/17/12 10/17/12 25

80-120PVJ1237-02 (2.3)10227.812J0760-MS1 10/18/12 10/18/12 25

80-120PVJ1405-10 (1.56)10126.812J0865-MS1 10/22/12 10/22/12 25

80-120PVJ1577-17 (3.64)9928.312J0980-MS1 10/24/12 10/24/12 25

E80-120PVK0411-02 (37.2)10663.612K0270-MS1 11/7/12 11/7/12 25

80-120PVK0632-11 (5.13)10932.412K0434-MS1 11/12/12 11/12/12 25

80-120PVK0684-02 (2.69)1052912K0505-MS1 11/13/12 11/13/12 25

80-120PVK1220-02 (2.38)10829.412K0719-MS1 11/19/12 11/19/12 25

80-120PVK1288-02 (1.62)1102912K0783-MS1 11/20/12 11/20/12 25

80-120PVK1375-02 (2.89)10930.112K0783-MS2 11/20/12 11/20/12 25

80-120PVK1375-04RE1 (1.5)10828.612K0838-MS1 11/21/12 11/21/12 25

80-120PVK1450-03 (2.45)10729.212K0888-MS1 11/23/12 11/23/12 25

80-120PVK1630-04 (4.7)1133312K1019-MS1 11/28/12 11/28/12 25

80-120PVK1721-09 (2.74)10428.812K1067-MS1 11/29/12 11/29/12 25

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MS/MSD RPDPerchlorate


8624.6259/4/129/4/1212I0049-MSD1 1559125.9 PVH2309-02 (3.03)

8926259/5/129/5/1212I0099-MSD1 1539326.9 PVH2238-01 (3.69)

0259/10/129/10/1212I0279-MSD1X 150 PVI0290-05

8727.1259/11/129/11/1212I0326-MSD1 R-9151910932.7 PVI0290-05RE1 (5.45)

8325.2259/12/129/12/1212I0426-MSD1 15176721.2 PVI0609-15 (4.42)

9525.9259/13/129/13/1212I0482-MSD1 R-715197721.3 PVI0609-15RE1 (2.12)

9127.5259/18/129/18/1212I0623-MSD1 150.59127.3 PVI1060-03 (4.67)

9125.5259/25/129/25/1212I0912-MSD1 1558724.3 PVI1553-05 (2.67)

9828.2259/27/129/27/1212I1035-MSD1 150.49828 PVI1723-03 (3.56)

9926.3259/28/129/28/1212I1101-MSD1 150.39926.3 PVI1822-02 (1.6)

10028.92510/1/1210/1/1212J0037-MSD1 1529828.3 PVI1869-16 (3.82)

10327.62510/8/1210/8/1212J0317-MSD1 150.710227.4 PVJ0513-11 (1.9)

10428.22510/9/1210/9/1212J0372-MSD1 15210227.7 PVJ0513-12 (2.23)

10330.22510/10/1210/10/1212J0427-MSD1 15110430.6 PVJ0682-03 (4.51)

9927.72510/16/1210/16/1212J0662-MSD1 15110028 PVJ1065-02 (2.95)

10028.62510/17/1210/17/1212J0751-MSD1 150.0410028.6 PVJ1065-09 (3.73)

9325.52510/18/1210/18/1212J0760-MSD1 15810227.8 PVJ1237-02 (2.3)

10126.82510/22/1210/22/1212J0865-MSD1 150.110126.8 PVJ1405-10 (1.56)

9828.12510/24/1210/24/1212J0980-MSD1 150.89928.3 PVJ1577-17 (3.64)

10964.52511/7/1211/7/1212K0270-MSD1 E15110663.6 PVK0411-02 (37.2)

10832.12511/12/1211/12/1212K0434-MSD1 150.810932.4 PVK0632-11 (5.13)

10729.52511/13/1211/13/1212K0505-MSD1 15210529 PVK0684-02 (2.69)

10428.52511/19/1211/19/1212K0719-MSD1 15310829.4 PVK1220-02 (2.38)

10728.42511/20/1211/20/1212K0783-MSD1 15211029 PVK1288-02 (1.62)

11030.32511/20/1211/20/1212K0783-MSD2 150.710930.1 PVK1375-02 (2.89)

10728.22511/21/1211/21/1212K0838-MSD1 15110828.6 PVK1375-04RE1 (1.5)

10528.82511/23/1211/23/1212K0888-MSD1 15210729.2 PVK1450-03 (2.45)

10831.62511/28/1211/28/1212K1019-MSD1 15411333 PVK1630-04 (4.7)

10328.42511/29/1211/29/1212K1067-MSD1 15110428.8 PVK1721-09 (2.74)

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DUP RPDPerchlorate

ResultAnalyzedPreparedSample IDRjct Dup Source RPD Limit Qualifiers

20 15 R-92.19 1.79 PVH2309-03 (1.79)12I0049-DUP1 9/4/12 9/4/12

150 PVH2276-01X 12I0099-DUP1 9/5/12 9/5/12

150 PVI0160-01X 12I0279-DUP1 9/10/12 9/10/12

3 153.28 3.18 PVI0160-01RE1 (3.18)12I0326-DUP1 9/11/12 9/11/12

151.84 PVI0609-05X 12I0426-DUP1 9/12/12 9/12/12

15 E80 PVI0609-05RE1X 12I0482-DUP1 9/13/12 9/13/12

43 15 R-93.18 2.06 PVI1060-06 (2.06)12I0623-DUP1 9/18/12 9/18/12

3 15 R-91.34 1.37 PVI1417-01 (1.37)12I0912-DUP1 9/25/12 9/25/12

2 153.13 3.18 PVI1555-01RE1 (3.18)12I1035-DUP1 9/27/12 9/27/12

21 15 R-41.04 1.29 PVI1723-10 (1.29)12I1101-DUP1 9/28/12 9/28/12

150 PVI1918-01X 12J0037-DUP1 10/1/12 10/1/12

0.2 15435 435 PVJ0271-17RE1 (435)12J0317-DUP1 10/8/12 10/8/12

15 E80 PVJ0448-01X 12J0372-DUP1 10/9/12 10/9/12

7 153.48 3.73 PVJ0682-06 (3.73)12J0427-DUP1 10/10/12 10/10/12

5 152.07 1.96 PVJ1065-03 (1.96)12J0662-DUP1 10/16/12 10/16/12

10 153.37 3.73 PVJ1065-09 (3.73)12J0751-DUP1 10/17/12 10/17/12

3 152.81 2.73 PVJ1245-01 (2.73)12J0760-DUP1 10/18/12 10/18/12

150 PVJ1404-01X 12J0865-DUP1 10/22/12 10/22/12

25 15 R-93.63 2.82 PVJ1577-16 (2.82)12J0980-DUP1 10/24/12 10/24/12

1 1513.4 13.2 PVK0411-03 (13.2)12K0270-DUP1 11/7/12 11/7/12

3 154.93 5.07 PVK0684-03 (5.07)12K0434-DUP1 11/12/12 11/12/12

5 159.02 9.52 PVK0632-07RE1 (9.52)12K0505-DUP1 11/13/12 11/13/12

47 15 R-91.36 2.21 PVK1220-05 (2.21)12K0719-DUP1 11/19/12 11/19/12

3 154.65 4.49 PVK1286-06 (4.49)12K0783-DUP1 11/20/12 11/20/12

150 PVK1393-01X 12K0838-DUP1 11/21/12 11/21/12

0.4 151.62 1.62 PVK1450-02 (1.62)12K0888-DUP1 11/23/12 11/23/12

1 151.49 1.51 PVK1630-05 (1.51)12K1019-DUP1 11/28/12 11/28/12

150.458 PVK1721-10X 12K1067-DUP1 11/29/12 11/29/12

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BLKPerchlorate

2.0 r-------------------------------------------------------~ 1.8

1.6

1.4

1.2

1.0

Plotted: 28

MDL: 0.47

MRL: 2

Rejected: 0

Stdv: 0

Mean: 0 0.8

2s: 0 0.6

~------------------------------------------------------------__,3•:0 OA go

0.2

o.o +-4-~~~~~_.-+~~~~~~~~+-4-~~~~~_.-+~~~ 3 5 7 9 11 13 15 17 19 21 23 25 27

PGA NORTH – GROUNDWATER SAMPLING VALIDATION OF …DUP001-09142012 EB001-09142012 The calibration...

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