Parts and Equipment Guide for Ion Sources and Mass ... · Turbo VTM Ion Source Operator Guide....

Parts and Equipment Guide

for Ion Sources and Mass Spectrometers

February 2019RUO-IDV-05-6233-E

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for Ion Sources and Mass SpectrometersParts and Equipment GuideRUO-IDV-05-6233-E2 / 20

1 Introduction..............................................................................................................................................4

2 Spare Parts................................................................................................................................................5Mass Spectrometer............................................................................................................................................................5

Mass Spectrometer Power Cables................................................................................................................................5Roughing Pump ................................................................................................................................................................6Turbo VTM, IonDriveTM Turbo V, and DuoSprayTM Ion Sources...........................................................................................6OptiFlowTM Turbo V Ion Source.........................................................................................................................................8NanoSpray

® Ion Source......................................................................................................................................................9

3 Consumables..........................................................................................................................................10Mass Spectrometer..........................................................................................................................................................10Roughing Pump...............................................................................................................................................................11Turbo VTM and IonDriveTM Turbo V Ion Sources...............................................................................................................12OptiFlowTM Turbo V Ion Source.......................................................................................................................................15DuoSprayTM Ion Source....................................................................................................................................................16NanoSpray

® Ion Source....................................................................................................................................................17

Calibrant Delivery System (CDS, TripleTOF®

Systems)......................................................................................................19Calibration Solutions..................................................................................................................................................20

Parts and Equipment Guidefor Ion Sources and Mass Spectrometers3 / 20RUO-IDV-05-6233-E

Contents

Note: Only parts and equipment listed in this guide are serviceable by the customer. Contact a Field ServiceEmployee (FSE) for information about other parts.

This guide applies to non-MD systems, including:

• 3200 series systems

• SCIEX Triple QuadTM 3500 systems




• SCIEX Triple QuadTM 5500+ systems

• 6500 and 6500+ series systems

• TripleTOF® 4600 systems

• TripleTOF® 5600 and 5600+ systems

• TripleTOF® 6600 and 6600+ systems

• SCIEX X500 QTOF systems

Ion sources detailed in the guide include:

• Turbo VTM ion source

• IonDriveTM Turbo V ion source

• OptiFlowTM Turbo V ion source

• DuoSprayTM ion source

• NanoSpray® ion source


1Introduction

WARNING! Personal Injury Hazard. Use SCIEX-recommended parts only. Use of partsnot recommended by SCIEX or use of parts for any purpose other than their intendedpurpose can put the user at risk of harm or negatively impact system performance.

Mass Spectrometer

Table 2-1 Mass Spectrometer Spares

RemarkDescriptionPart Number

Refer to the Qualified MaintenancePerson Guide.

Orifice plate interface heater kit.1040121

(X500 QTOF systems) Refer to the DevicesSetup Guide.

Contact closure cable for CTC PAL systems5065277


Contact closure cable for ExionLCTM,Shimadzu, Waters, and Gilson systems

5065278


Contact closure cable for Agilent systems5065279

Mass Spectrometer Power Cables

Table 2-2 Mass Spectrometer Power Cable Spares


Refer to the Site Planning Guide.North America001461

Refer to the Site Planning Guide.United Kingdom5027349

Refer to the Site Planning Guide.Switzerland5027461

Refer to the Site Planning Guide.Italy5027503

Refer to the Site Planning Guide.Central Europe5027841


2Spare Parts

Table 2-2 Mass Spectrometer Power Cable Spares (continued)


Refer to the Site Planning Guide.South Korea5028400

Refer to the Site Planning Guide.Australia5028431

Refer to the Site Planning Guide.Japan5029429

Refer to the Site Planning Guide.China5029431

Refer to the Site Planning Guide.India5044093

Roughing PumpTable 2-3 Roughing Pump Spares


For 3200, 4000, and 5000 series systems.Refer to the Qualified MaintenancePerson Guide.

Roughing pump oil return line for the HS602roughing pump.

028685

For 6500 and 6500+ series systems.Exhaust filter cartridge for the MS roughingpump.

1034438

Contact an FSE.

Note: Not for use with the HS602roughing pump.

Roughing pump oil change kit. The kitcontains a roughing pump oil extractionsystem that simplifies and speeds up the oilchange process.

5037860

For 3200, 4000, and 5000 series systems.Refer to the Qualified MaintenancePerson Guide.

Roughing pump oil exhaust filter for theHS602 roughing pump.

9499342

Turbo VTM, IonDriveTM Turbo V, and DuoSprayTM IonSourcesFor maintenance procedures, refer to the documentation that comes with the ion source.


Spare Parts

Table 2-4 Turbo VTM, IonDriveTM Turbo V, and DuoSprayTM Ion Source Spares


Refer to the DuoSprayTM Ion SourceOperator Guide.

TurboIonSpray® probe assembly for the

DuoSprayTM ion source.1005100

For SCIEX X500 QTOF systems. Refer to theTurbo VTM Ion Source OperatorGuide.

Twin ESI probe assembly.5041898


Twin APCI probe assembly.5041899

For SCIEX Triple QuadTM, QTRAP®, and

TripleTOF® systems. Refer to the Operator

Guide for the ion source or the 3200Series of Instruments System UserGuide.

APCI probe assembly. Refer to Figure 2-2.5050135




TurboIonSpray® probe assembly. Refer to

Figure 2-1.5050136

Figure 2-1 TurboIonSpray® Probe Assembly (PN 5050136)


Spare Parts

Figure 2-2 APCI Probe Assembly (PN 5050135)

OptiFlowTM Turbo V Ion SourceFor maintenance procedures, refer to the documentation that comes with the ion source.

Table 2-5 OptiFlowTM Turbo V Ion Source Spares


Refer to the OptiFlowTM Turbo V Ion SourceOperator Guide.

SteadySpray ANALYTICALprobe. Flow rates greater than50 µL

5063236


SteadySpray MICRO probe.Flow rates between 1 µL and50 µL

5063235


SteadySpray NANO probe.Flow rates between 100 nLand 1000 nL

5065457


Spare Parts

Figure 2-3 SteadySpray MICRO, ANALYTICAL, or NANO Probe

NanoSpray® Ion Source

For maintenance procedures, refer to the documentation that comes with the ion source.

Table 2-6 Mains Supply Cables by Country

RemarkCountryPart Number

N/AAustralia5028431

N/AChina5029431

N/AEurope5027841

N/AItaly5027961

N/AJapan5029429

N/ANorth America400-00023

N/ASouth Korea5028400

N/ASwitzerland5027461

N/AUnited Kingdom5027349


Spare Parts

Mass SpectrometerFor maintenance procedures, refer to the documentation that comes with the mass spectrometer.

Table 3-1 Mass Spectrometer Consumables


Refer to the System User Guide.O-ring for the vacuum interface017819


Lint-free wipe018027

For 3200 series systems. Refer to theQualified Maintenance PersonGuide.

Card cage air filter1007740


Small poly swab, package of 121017396

For 3500, 4500, 5500, 5500+, 6500, and6500+ systems. Refer to the QualifiedMaintenance Person Guide.

Mass spectrometer air filter kit including fourair filters

1027708


Q0 cleaning tool1028234

For TripleTOF® systems. Refer to the

Qualified Maintenance PersonGuide.

Cooling fan filter1032854

Refer to the Customer FamiliarizationChecklist.

Triazine standard solution4376887

Refer to the Ion Source Tests,Specifications, and Data Log.

PPG MS chemical kit4406127


3Consumables

Table 3-1 Mass Spectrometer Consumables (continued)


Refer to the Qualified MaintenancePerson Guide.Contains the small poly swab, lint-free wipe,Q0 cleaning tool, straight QJet

® ion guide

cleaning brush, and Alconox packets.

Cleaning kit, 3200, 4000, 3500, 4500, 5000,and 5500 systems

5020761

Refer to the Qualified MaintenancePerson Guide.Contains the small poly swab, lint-free wipe,Q0 cleaning tool, tapered QJet

® ion guide

cleaning brush, and Alconox packets.

Cleaning kit, TripleTOF® systems5020763


Alconox packets5020893


Custom QJet® ion guide brush (straight),

3500, 4500, and 5500 systems5020894


Custom IonDriveTM QJet ion guide brush(straight), 5500+, 6500, 6500+, andTripleTOF

® systems

5020895

Refer to the Qualified MaintenancePerson Guide.Contains the small poly swab, lint-free wipe,Q0 cleaning tool, straight IonDriveTM QJetion guide cleaning brush, and Alconoxpackets.

Cleaning kit, 5500+, 6500, and 6500+ seriessystems

5021294

Roughing PumpFor maintenance procedures, refer to the documentation that comes with the mass spectrometer.


Consumables

Table 3-2 Roughing Pump Consumables


For 3200 series systems and 4000 and 5000series systems with the HS602 roughingpump. Refer to the QualifiedMaintenance Person Guide.

Roughing pump oil for the HS602 roughingpump, 1 L

010998

For 3500, 4500, 5500, 5500+, andTripleTOF

® systems without the long-life

pump. Refer to the QualifiedMaintenance Person Guide.

Note: Two bottles of oil might berequired.

Roughing pump oil for SV roughing pumps,1 L

Note: Not for use with long-life pumps.

1027317

For 6500 and 6500+ series systems. Referto the Qualified Maintenance PersonGuide.

Roughing pump oil for MS roughing pumps,1 L

1034433

For 4500 and TripleTOF® systems with the

long-life pump. Refer to the QualifiedMaintenance Person Guide.

Note: Two bottles of oil might berequired.

Roughing pump oil for long-life SV roughingpumps, 1 L

Note: Only for use with long-life pumps.

5043115

Turbo VTM and IonDriveTM Turbo V Ion SourcesFor maintenance procedures, refer to the documentation that comes with the ion source.

Table 3-3 Turbo VTM Ion Source and IonDriveTM Turbo V Ion Source Consumables


Refer to the Operator Guide for the ionsource or the 3200 Series ofInstruments System User Guide.

Corona discharge needle.5051034


Metal-encased turbo heater for the Turbo VTM

ion source.5051082


Consumables

Table 3-3 Turbo VTM Ion Source and IonDriveTM Turbo V Ion Source Consumables (continued)



TripleTOF® systems. Refer to theOperator


TurboIonSpray® electrode.5052616




APCI electrode.5053788


Ceramic-encased turbo heater for theTurbo VTM ion source.

5054421


Turbo heater for the IonDriveTM Turbo V ionsource without covers.

5054661


Twin ESI probe electrode.5049795


Twin APCI probe electrode.5054901


Turbo heater for the Turbo VTM ion sourcewith covers.

5058778

Sample tubing, 100 cm.Red PEEK tubing (0.005-inch bore), 100 cm016316

Sample tubing nut.Brown PEEK fitting, pack of 5016325

Specify order quantity in cm.Tan PEEK tubing (0.0025-inch bore)016485

Grounding union connection.Tee insert (0.25 mm bore)019675


Consumables

Figure 3-1 Red PEEK Tubing (SCIEX Triple QuadTM, QTRAP®, and TripleTOF

® systems)


Consumables

Figure 3-2 Red PEEK Tubing (SCIEX X500 QTOF systems)

OptiFlowTM Turbo V Ion SourceFor maintenance procedures, refer to the documentation that comes with the ion source.

Table 3-4 OptiFlowTM Turbo V Ion Source Consumables


Refer to the OptiFlowTM Turbo V IonSource Operator Guide.

SteadySpray LOW MICRO electrode. Flowrates between 1 µL and 10 µL. Pack of 5.

5061574


SteadySpray MICRO electrode. Flow ratesbetween 10 µL and 50 µL. Pack of 5.

5061575


Consumables

Table 3-4 OptiFlowTM Turbo V Ion Source Consumables (continued)



SteadySpray HIGH MICRO electrode. Flowrates between 50 µL and 200 µL. Pack of 2.

5061576


SteadySpray MICRO electrodes starter pack.Mixed pack of 5 electrodes.

5061577


SteadySpray NANO electrodes starter pack.Flow rates between 100nL and 1000 nL. Packof 5.

5070382


Stainless steel upper fitting used for thecolumn connection.

5060978


PEEK upper fitting used for the MICROcolumn connection.

5061373

N/APEEK ferrule for 1/16" OD tubing5053325

N/ALower probe O-ring, 10 mm ID x 1.5 mm5055764

N/AUpper probe O-ring, 4 mm ID x 1.0 mm5045265

This kit contains spare parts if required fora new installation.

Installation kit (MICRO)5060726

This kit contains NANO parts required tooperate the system with the SteadySprayNANO probe and column heater.

NANO upgrade kit5069262

DuoSprayTM Ion SourceFor maintenance procedures, refer to the documentation that comes with the ion source.

Table 3-5 DuoSprayTM Ion Source Consumables


N/ASpring for probe026626

N/ASpring for corona discharge needle027013

N/AGold-plated spring for HV connection027497


Corona discharge needle rod1006174


Consumables

Table 3-5 DuoSprayTM Ion Source Consumables (continued)



Corona discharge needle tip1006177


TurboIonSpray® electrode5052616


APCI electrode5053788

For TripleTOF® systems. Sample tubing. Refer

to the DuoSprayTM Ion SourceOperator Guide.

Red PEEK tubing (0.005-inch bore), 100 cm016316

Sample tubing nutsBrown PEEK fitting, pack of 5016325

For SCIEX Triple QuadTM and QTRAP®

systems. Refer to the DuoSprayTM IonSource Operator Guide.

PEEK tubing kit to connect toTurboIonSpray

®probe, 30 cm

1005601

For SCIEX Triple QuadTM and QTRAP®

systems. Refer to the DuoSprayTM IonSource Operator Guide.

PEEK tubing kit to connect to APCI probe,45 cm

1005602

N/APEEK Graph-tite fitting, Black, 1/16 inch,pack of 2

5041723

N/APEEK union in probe5045984

NanoSpray® Ion Source

For maintenance procedures, refer to the documentation that comes with the ion source.

Table 3-6 NanoSpray® Ion Source Consumables


Refer to the NanoSpray® Ion Source

Operator Guide.Fused silica cutter200-00096


Operator Guide.Fitting and ferrule used at the nebulizer gasport

200-00213


Operator Guide.Stainless steel union, 1/16 inches on oneend, 1/32 inches on the other

200-00303


Consumables

Table 3-6 NanoSpray® Ion Source Consumables (continued)



Operator Guide.PEEK fitting for 360 uM OD tubing200-00408

Includes the fittings, sleeves, adapter blockand union and emitters. Refer to theNanoSpray

® Ion Source Operator

Guide.

Adapter kit for the NanoSpray® III ion source910-00112


Operator Guide.Syringe for the infusion test1003988


Operator Guide.395 μm (0.0155 inch) i.d., 1/16 inch o.d.green FEP sleeve, 1.6 inch length, for usewith the sprayer fitting.

1006547


Operator Guide.Optional Tee union with the makeup flow1034697


Operator Guide.Precut (7 cm) uncoated emitter tips with 20µm i.d., 10 µm at the tip

1035752


Operator Guide.O-ring at the front of the rail, for thenebulizer gas connection

1035770


Operator Guide.Finger-tight PEEK hex nut for the sprayerside of the straight union

5015860


Operator Guide.Syringe union for use with fused silica tubing5015886


Operator Guide.Syringe union for use with red PEEK-linefused silica tubing

5015900

Can also be ordered with the union holder,fittings, and thumbscrew. Refer to PN5016361.

Straight union5015902

The complete union assembly, including theholder, union, fittings, and unionthumbscrew. Refer to the NanoSpray

® Ion

Source Operator Guide.

Straight union and holder5016361


Consumables

Table 3-6 NanoSpray® Ion Source Consumables (continued)



Operator Guide.PEEK fitting to connect the sample line(fused silica or PEEK-lined fused silica) to theunion on the rail.

5017932


Operator Guide.Consumables kit5052735

Calibrant Delivery System (CDS, TripleTOF® Systems)

Table 3-7 Calibrant Delivery System Consumables

Upchurch PartNumber

QuantityDescriptionPartNumber

LT-1151NUT, PEEK, SHORT, 1/4-285008141

P-2602FERRULE, PEEK, SUPER FLANGELESS5008152

F1301FITTING, PEEK, NAT, LONG,5008157

U-467BLK1PLUG, ACETAL, BLACK5008232

PM-1960B1TUBING, PEEK, BLUE, 1/16x.010x40CM5008296

PM-1945R1TUBING, PEEK, RED, 1/16x.125x40CM5002985

PM1820G1TUBING, PEEK, GREEN, 1/16x.030x16CM5008298

PM10005TUBING, FEP, NAT, 1/16x.030x60CMN/A

PM10001TUBING, FEP, NAT, 1/16x.030x17CMN/A

PM1000G2TUBING, FEP, GREEN, 1/16x.030x60CM5008302

A-4532FILTER ASSY, PEEK, BOB, 1/16,10um,GL-385008303

N/A5CAP ASSY, BOTTLE, 1/16,GL-38N/A

N/A11FITTINGS, KNOB, BLACKN/A

N/A11FERRULE, PEEKN/A

N/A11NUT, RHEFLEXN/A


Consumables

Calibration Solutions

Table 3-8 Calibration Solution Consumables

QuantityDescriptionPart Number

100 mLAPCI Positive Calibration Solution for the SCIEX TripleTOF® 5600

System4460131

100 mLAPCI Negative Calibration Solution for the SCIEX TripleTOF® 5600

System4460134

5 × 100 mLAPCI Positive Calibration Solution for the SCIEX TripleTOF® 5600

System (5-pack)4460136

5 × 100 mLAPCI Negative Calibration Solution for the SCIEX TripleTOF® 5600


100 mLESI Positive Calibration Solution for the SCIEX TripleTOF® 5600

System4463272

5 × 100 mLESI Positive Calibration Solution for the SCIEX TripleTOF® 5600


5 × 100 mLESI Negative Calibration Solution for the SCIEX TripleTOF® 5600


100 mLESI Negative Calibration Solution for the SCIEX TripleTOF® 5600

System4463277


Consumables

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