Guidel ines for Chemical Dr ink inq Water Qual i tv as of Auqust 2012

ParameterA luminum

Heal th Guidel ine

0.0060.01

10 .005

n nn6v , v v v

iChloratecniorioe <250Chlori teChromium 0.05Colour

CyanidgCyanobacterial toxins - microcystin-LREthylbenzeneFluor ide

<1 5 TCU1

02o.oor s

<6 oozq1 . 5

l ron <0.3Lead 0.01Manganese <0.05MercuryNitrate

0.001_tryo_us4 s9 x)

N itritebHSelen iumSoOium

3.2 (1 mg/L as N)6 5 - 8 . 5

<200<500<0.05<0.024

rola I D 19s9lyq9ls9!4ls (rDS ) <500Trih_alomethanes (Tgtg!i._....,. _ 0.1Turbidity" 1,0lttu'Uranium 0.02xytdnes (roiat) iO.aZinc

Guidelines for Microbiolooical Parameters

The MAC tor total coliforms and Escherichia coli, in public, semi-public and private drinking water systems is nonedetectable per 100 mL. No MAC is specified fot heterotrophic plate count (HPC) bacteria. However, increasesin HPC concentrations above baseline levels are considered undesirable.

Saturation Index (Sl)

Saturation /tdex is used to evaluate the need for corrosion control.(a) A positive Sl indicates scaling tendencies, but non-corrosive water(b) A negative Sl indicates non-scaling tendencies, but corrosive water

< lgss lhan or equgllg _1" TUtb_,9tty vg!,Lte !$e,Q_o1s_lgy srlq or !g!qrnggg_q_Us__9-q4! "!l!E!g!,Guidel ines for Canadian Drinking Water Quali ty are provided courtesy of Health Canada. August 2012.http://www.hc-sc.gc.calewh-semt/alt_formats/pdf/pubs/water-eau12012-sum_guide-res_recoml2012-sum_guide-res_recom-eng.pdf

wsHi:

Lobs(1ee2) ff id.38518 - 21 Street N.E. * Calgary, Alberta, Canada * T2E 6T5

Phone: 403-250-9164 n Fax: 403-291-4597 € www.wshlabs.com

Cor ix Ut i l i t ies Inc.#2, 8515 - 48 St . SECalgary, AB T2C 2PB

Sample Info: Emerald BayTreated

Phone :Fax:

Emai l :

(403) 273-8676(403) 273-7382

Lab Number: 73620

PO Number:

Sampled By:Date Sampled:Date Received:Date Reported:

CK9t27 t20139t27 t20131011712A13

Analyte Uni ts Res u lt Canadian Dr ink ing Water Guidel ine MaximumCalc iumlronMagnes iumManganesePotassiumSod iumBicarbonatesBromidesCarbonatesChlor idesFluor idesNitrates as NNitr i tes as NNO, + NO, as NSulfates

Parameter

mg/Lmg/Lmgi Lmgi Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

Uni ts

t J . o0 , 0 51 2 . 6

<0 .011 91 3 8332< 0 . 1

013.20 5 30 .2

<0.020 . 21 0 3

Result

No Gu ide l inen ?

No Gu ide l ine0 0 5

No Guidel ine20Q

No Guidel ineNo Guidel ineNo Guidel ine

2501 51 0

At

No Guidel ine500

Canadian Dr ink ing Water Guidel ine MaximumElectr ical Cond uctivi tvpHHardness (as CaCOr)Total Alkal inity (as CaCO.)P-Alkal in i ty (as CaCO3)Hydroxide (as CaCOr)Total Dissolved Solids (calculated)Sulf ides as SColorAmmonia Ni t rogenTotal Organic CarbonCyanideBromateChloraminesChlorateChlori te

Microbio logy

pS/cmp H

mg/Lmg/Lmg/Lmg/Lmg/Lmg/LTCUmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmgi L

Uni ts

728B 1 81 1 1272

00

456<0.03

<5< 0 . 91 5

<0 .05< 0 . 0 1 0

0 . 10 .33

< 0 . 1 0

Result

No Gu ide l ine6 5 - 8 . 5

No Gu ide l ineNo Gu ide l ineNo Guidel ineNo Guidel ine

5000 .051 5

No Guidel ineNo Gu ide l ine

0 .20 . 0 1

34I

1

Canadian Dr ink ing Water Guidel ine MaximumMicrocystin-LR pg/L < 0 . 1 4 1 . 5

Sum of Cat ionsSum of Anions

lon Balance

8 2 6 TDS / EC RatioSodium Adsorption Ratio

Saturation lndex

0 .638 0 0 5 .70' i . 03 0.53 Page 1

" *

Lsbs (t 992! ttd.

Cor ix Ut i l i t ies lnc.#2 ,8515 - 48 S t . SECalgary, AB TzC zPB

Sample Info: Emerald BayTreated

A luminumChromiumCopperZ incArsenicSeleniumSi lverCadmiumAnt imonyBar iumMercuryLeadUran ium

Accredited by CALA to ISO/IEC 17025 for specif ic tests< denotes less than detection l imit.

Cont ro l No: WSH-BKW041 409-Rev1.0

38518 - 21 Street N.E. ' Calgary, Alberta, Canada * T2E 6T5Phone: 403-250-9164 e Fax: 403-291-4SgT € www.wshlabs.com

Phone: (403) 273-8676 Lab Number:Fax: (403) 273-7382

Emai l : PO Number :

Sampled By:

1 0 050

1 0005000

1 01 0

No Guidel ineRv

o1 000

1t

1 020

73620

CKDate Sampled: 912712013Date Received: 9 127 12013Date Reported: 1011T12013

Trace Metals Units Result Canadian Drinkinq Water Guideline MaximumBoron pg/L 44.4 5000-

trg/L 3 6Lrgi L 0.2trg/Lug/Lpgi Lpg/Lpg/Lpg/Lpgi Lpg/Lpg/L

49.41 2 . 60 30 .2

<0.04<0 .05< 0 . 324 1<0 .05

pgi l 1 2pg/L 0.5

WSH Labs (1992) Ltd. as per:

The results above are related only to the i tems analyzed.

Page 2

rVf a {;i^rrlYour P.O. #: 7OO7Your C.O.C. #: NA

@WSH Labs3851 B - 21 St NECalgary , ABT2E 6T5

Report Date: 2O13l1Ol1 1

Received : 201 311 0102. 1 0:52

Sample Matrix: Water# Samples Received: 1

Date Date MethodAlalvse! ,, = Quanti ReferenceDiuron, Guthion, Temephos t ZOtSnOlO4 2otgfiO/o7 CAt\4 SOP-OO EpA 532Glyphosate 1 2o13l1oto7 2o13l1o/oa cAM sop-oo3os HpLc in-house merhodHaloacetic Acids in Water (1) | 2Ot3/10/09 2Ot3/10/11 ATLSOPOO|29 Based on EpA552.2Nitrilotriacetic Acid (NTA) 1 2O1gnOtO4 2O'tgt1OIO7 CAM SOp-OO4i l EpA 490.1OC Peslicides (Selected) &PCB@ 1 2013/tO/03 2O1At1OtO9 CA|VI SOP-OO3O7 SW846 8081.8082oc Pesticides summed Paramele6 1 N/A 2olc/to/07 cAM sop-oo3o7 swg46 8081, 8082oDWs - Semi-volatlles 1 2o13hon4 2o1gt1oto5 cAM sop-oo3ol EpA 8270 modified

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

(1) This test was performed by Bedford(2) Chlordane ( Total) = Alpha Chlordane + Gamma Chlordane

Encryption Key,/2 --. , James Aspin

,:/ti'4?-*_2.->>- 12 Oct 201319:58:32 -04:00

Please direct all qr"iion" regarding this Certificate of Analysis to your Project Manager.

James Aspin, Senior Project ManagerEmail: JAspin @ maxxam.caPhone# (905) 817-5771

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5'10'2 of ISO/IEC 17025:20O5(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Total cover pages: 1

Page 't of 15

|v |axx fAna|yncsh6nat i rna |c . rporanono/a l \ | !a l r fAm|yn6674ocfpobe| |oRoad 'M|$ |ssa 'omdio ,L$1€

, / jlVf a XXa rrlr ' /

WSH LabsMaxxam Job #: 83G6957Report Date: 2O13l1O/1 1

Your P.O. #:7007

RESULTS OF ANALYSES OF WATER

Vlaxxam lD TH6034iampling Date 2013109127

14:30IOC Number NA

Units /3620(EMERALDBAYI

]DL lC Batch

\tliscel laneous ParametersNTA mg/L ND c.05 3374487

\D = lrlel detectediDL = Reportable Detection Limitf,C Batch = Quality Control Batch

Page 2 of 15

I\,brxmAnal!nica|mernanonalcorpdariono/aMd1amArElytiB674ocdnpobe||oBosd'M|s6|ssa|lga'onio'[$18

. /1twlayarr l

Maxxam Job #: 83G6957 wsH Labs

Report Date: 201311011 1Your P.O. #:7O07

HALOACETTC ACTDS By GC-ECD (WATER)

Vlaxxam lD TH6034Sampling Date 2013/09/27

14:30IOC Number NA

Units 73620(EMERALDBAY}

IDL lC Batch

Mliscel laneous ParametersVlonochloroacetic Acid (MCAA) ug/L ND 5.0 3379157Monobromoacetic Acid (MBAA) ug/L ND 5.0 3379157Dichloroacetic Acid (DCAA) ug/L ND 5.0 3379157frichloroacetic Acid (TCAA) ug/L ND 5.0 33791573romochloroacetic Acid (BCAA) ug/L ND 5.0 3379157Jibromoacetic Acid (DBAA) ug/L ND 5.0 3379157Iotal haloacetic acids ug/L ND 5.0 3379157Surrogate Recovery (%)2,3-Dibromopropionic Acid o//o 87 N/A 3379157

ND = Not detected\/A = Not Applicable3DL = Reportable Detection Limitf,C Batch = Quality Control Batch

Page 3 of 15

A/ 'a fxmAna|y i |cs | fe rna t iona |@rpor f |ono/aMdramAm|yr l66740cfpobe| |oRoad.M|$ lssa la 'omaio '18

_ -/ilV la#arr l

Maxxam Job #: 83G6957 wsH Labs

Repoft Date: 2013/1011iYour P.O. #:7007

SEM!-VOLAT|LE ORGANTCS By cc-MS (WATER)

Vlaxxam lD TH6034Sampling Date 2013t09t27

14:30IOC Number NA

Units 73620(EMERALDBAY)

RDL lC Batch

Semivolatile Organics2,3, 4, 6-Tetrach loroph en ol ug/L ND 0.50 33741822,4,5-T ug/L ND 1 . 0 33741822,4,6-Trichloroph enol ug/L ND 0,50 33741822,4-D ug/L ND 1 . 0 33741822,4-Dichlorophenol ug/L ND 0.50 3374182Alachlor ug/L ND 0.50 3374182Aldicarb ug/L ND 5.0 3374182{trazine ug/L ND 0.50 3374182Des-ethyl atrazine ugil ND 0.50 3374182Atrazine + Desethyl-atrazine ug/L ND 1 . 0 33741823endiocarb ug/L ND 2.0 3374182Bromoxynil ug/L ND 0.50 3374182Sarbaryl ug/L ND 5.0 3374182larbofuran ug/L ND 5.0 3374182)h lorpyrifos (Du rsban) ug/L ND 1 . 0 3374182Oyanazine (Bladex) ugil ND 1 . 0 3374182)iazinon ug/L ND 1 . 0 3374182Dicamba ug/L ND 1 . 0 3374182)iclofop-methyl ug/L ND 0.90 3374182)imethoate ug/L ND 2.5 3374182Dinoseb ug/L ND 1 . 0 3374182Vlalathion ug/L ND 5.0 3374182Metolachlor ug/L ND 0.50 3374182Metribuzin (Sencor) ug/L ND 5.0 3374182Ethyl Parathion ug/L ND 1 . 0 3374182)entachlorophenol ug/L ND 0.50 3374182Phorate ug/L ND 0.s0 3374182ricloram ug/L ND 5.0 3374182Prometryne ug/L ND 0.25 3374182Simazine ug/L ND 1 , 0 3374182

ND = ryel detectedRDL = Reporlable Detection LimitQC Batch = Quality Control Batch

Page 4 of 15

|uaxramAna|}nbsherm0ona|corpdanono/aMaumArE]yt|66-74ocfpoDe|loRod',

_ -/1f\^/f ^a -{J-a lTtr v r i ( , _ r y .

WSH LabsMaxxam Job #:83G6957Report Date: 2013110/11

Your P.O. #:7007

sEMr-voLATtLE ORGAN|CS By GC-MS (WATER)

Vlaxxam lD TH6034Sampling Date 2013/09/27

14:30OC Number NA

Units 73620(EMERALDBAYI

RDL )C Batch

Page 5 of 15

l \ , | a l t a m A n a | ! d i c a l n t * n a n o n a | c d p . r a r b n o / a | J l a r r f A m l y n 6 6 - ' 4 0 c o p o b e | | o F @ d ' M | s h q E , , o n i o . 1 8

ferbufos ug/L ND 0.50 3374182Iriallate ug/L ND 1 . 0 3374182lrifluralin ugil ND 1 . 0 33741823enzo(a)pyrene ug/L N D 1.0090 3374182Methyl parathion ug/L ND 1 . 0 3374182iurrogate Recovery (%)2,4,6-Tribromophenol o//o B9 N/A 33741822,4-Dichlorophenyl Acetic Acid o//o 106 N/A 33741822-Fluorobiphenyl o//o 82 N/A 3374182)14-Terphenyl (FS) o/ 1 1 1 N/A 3374182)5-Nitrobenzene % 82 N/A 3374182

ND = flel detectedN/A = Not ApplicableRDL = Reoortable Detection LimitQC Batch = Quality Control Batch

. /7lVf a#arr lWSH Labs

Maxxam Job #:83G6957Report Date: 201311011 1

Your P.O. #:7007

PESTTCTDES & HERBTCTDES BY HPLC (WATER)

vlaxxam lu TH6034Sampling Date 2013109127

14:30IOC Number NA

Units 13620(EMERALDBAY)

tDL lC Batch

resticides & HerbicidesSlyphosate ug/L ND 1 0 33771 38)iuron ug/L ND 1 0 3374057Suthion (Azinphos-methyl)ug/L ND 2 3374057femeohos ug/L ND 1 0 3374057

tlD = Not detectedfDL = Reportable Detection Limitf,C Batch = Quality Control Batch

Page 6 of l5

MdxamAnaly1ics|l16nationalcorporariono/aMa!rdAE|yrbs6740can0obe||oRoad'M|s|s3allga'onl4io'L5N

- / ilVf a#arTlWSH Labs

Maxxam Job #:83G6957Report Date: 2013/1011 1

Your P.O. #:7OO7

oRGANOCHLORTNATED PESTICIDES BY GC-ECD (WATER)

Vlaxxam lD TH60343ampling Date 2013109127

14:30IOC Number NA

Units 73620(EMERALDBAY)

RDL lC Batch

lalculated Parameters\ ldrin + Dieldrin ug/L ND 1.006 3372849

lhlordane (Total) ug/L ND 1.006 3372849-{eptachlor + Heptachlor epoxide ug/L ND 1.006 3372849

r,p-DDT + p,p-DDT ug/L ND ).006 3372849

fotal PCB ug/L ND 0.05 3372849resticides & Herbicides-indane ug/L ND ).006 3372570

leptachlor ug/L ND ).006 3372570

\ldrin ugil ND 1.006 3372570"leptachlor epoxide ug/L ND ).006 3372570

)xychlordane ug/L ND 1.006 3372570

;-Chlordane ug/L ND 1.006 3372570

l-Chlordane ug/L ND 1.006 3372570

l ,p -DDE ug/L ND 1.006 3372570)ieldrin ug/L ND 1.006 3372570

l ,p -DDD ug/L ND 1.006 3372570

l,p-DDT ug/L ND 1.006 3372570

l,p-DDT ug/L ND 1.006 3372570

Vlethoxychlor ug/L ND o.o2 3372570

\roclor 1016 ug/L ND 0.05 3372570\roclor 1221 ug/L ND 0.05 3372570Aroclor 1232 ug/L ND 0.05 3372570

\roclor 1242 ug/L ND 0.05 3372570Aroclor 1248 ug/L ND 0.05 3372570

Aroclor 1254 ug/L ND 0.05 3372570Aroclor 1260 ug/L ND 0.05 3372570

Surrogate Recovery (%)2,4,5,6-Tetrachloro-m-xylene o/ 98 N/A 3372570lecachlorobiphenyl "/" 117 N/A 3372570

\D = Not detected\/A = Not ApplicablelDL = Reportable Detection Limitf,C Batch = Quality Control Batch

Page 7 of 15

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_ ./)lV la#arr lWSH Labs

Maxxam Job #: 83G6957Report Date: 201311011 1

Your P.O. #:7007

GENERAL COMMENTS

Total haloacetic acids refers to the total of monochloroacetic acid. dichloroacetic acid. trichloroacetic acid, monobromoacetic acid anddibromoacetic acid..

Results relate onlv to the items tested.

Page 8 of 15

MaxxmAta]},1l:csmdnationa|cqporariono/aMd4AB|yI|66740cfFbe]|oB€d,M|$issa!ga,omaio.L5N:l

lVf a #arTtWSH LabsAttention: Bil l WongClient Project #:P.O. #: 7007Site Location:

Quality Assurance ReportMaxxam Job Number: M83G6957

QA/QCBatchNum ln i t

DateAnalyzed

Parameter /dd Value Limits337257A JZ Matrix Spike 2,4,5,6-Tetrachloro-m-xylene

DecachlorobiphenylLindaneHeptachlorAldrinHeptachlor epoxideOxychlordaneg-Chlordanea-ChlordaneP,P-DDEDieldrinP,P-DDDo,p-DDTP,P-DDTMethoxychlor2,4,5,6-T elrachlo ro-m -xylen eDecachlorobiphenylLindaneLindaneHeptachlorHeptachlorAldrinAldrinHeptachlor epoxideHeptachlor epoxideOxychlordaneOxychlordaneg-Chlordaneg-Chlordanea-Chlordanea-ChlordaneP,P-DDEP,P-DDEDieldrinDieldrinP,P-DDDP,P-DDDo,p-DDTo,p-DDTP,P.DDTp,p-DDTMethoxychlor2,4,5,6-Tetrachloro-m-xyleneDecachlorobiphenylLindaneHeptachlorAldrinHeptachlor epoxideOxychlordaneg-Chlordanea-ChlordaneP,P-DDEDieldrinP,P-DDDo,p-DDT

2013/101092013/101092013/10/092013/10/092013/101092013/101092013/10/092013110/092013110/092013/10/092013110/092013110/092013110/092013/101092013/101092013t10/092013110/O920't3/10/09201 3/1 0/092013110/092013110/092013110/09201 3/1 0/092013t10t092013110/O9201 3/1 0/092013110/092A131101092013110/0920131101o92013/10/O92013110/092013110/O92013/101092A131101092013i10/092013110/092013/101092013110/O920131101092013110/092013110109201311010920131101092013110/O92013/101092013h010s2013/10/0920131101092013110109201311010920131101o920131101092013t10/O92013/10/O9

7B12487B17B94BO9490B5

1049289879990

12895

B9

90

106

91

107

"/"o//o

Y"Yoo//oo//o

"/"/o

o//oo //oo //o

%/o

o//o

/oo //o

"/"o/^

o//oo//o

%Voo//oo//o

"/"o//o'/o

o // oo//oo//oo//o

"/"o//o

%/o

/o

/oo/

%"/"o//oo//oo//o

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

30 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 130

4030 - 130

4030 - 130

4030 - 130

4030 - 130

4030 - 130

4030 - 130

4030 - 130

4A30 - 130

4030 - 130

4030 - 130

4030 - 130

4040

30 - 13030 - 130

Spiked Blank

RPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPD

Method Blank

2 .1

5.8

5.7

1 , 9

3.4

2,8

2.0

2.2

1 . 7

1

103

94

120

105

971 . 0

914.5NC

80120

ND, RDL=0.006ND, RDL=0.006ND, RDL=0.006ND, RDL=0.006ND, RDL=0.006ND, RDL=0.006ND, RDL=0.006ND, RDL=0.006ND, RDL=0.006ND, RDL=0.006ND, RDL=0.006

Page I of 15

l!ldrfAna]yncshterEnona|cdporarionoraMd:dArEIyli36740c€mpobe||oBoad.M65is9l-EE'omdio'L5N28

lVf a SarTlWSH LabsAttention: Bill WongClient Project #:P.O. #:7007Site Location:

Quality Assurance Report (Continued)Maxxam Job Number: M83G6957

QA/QCBatch

lnit OC T3372570 JZ Method Blank

3374057 JLE Matrix Spike

Spiked Blank

Method Blank

RPD

3374182 WZ Matrix Soike

ParameterP,P-DDTMethoxychlorAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260DiuronGuthion (Azinphos-methyl)TemephosDiuronGuthion (Azinphos-methyl)TemephosDiuronGuthion (Azinphos-methyl)TemeohosDiuronGuthion (Azinphos-methyl)Temephos2,4,6-Tribromophenol2,4-Dichlorophenyl Acetic Acid2-FluorobiphenylD14-Terphenyl (FS)D5-Nitrobenzene2,3,4,6-Tetrachlorophenol2,4,5-T2,4,6-Trichlorophenol2,4-D2,4-DichlorophenolAlachlorAldicarbAtrazineDes-ethyl atrazineAtrazine + Desethyl-atrazineBendiocarbBromoxynilCarbarylCarbofuranChlorpyrifos (Dursban)Cyanazine (Bladex)DiazinonDicambaDiclofop-methylDimethoateDinosebMalathionMetolachlorMetribuzin (Sencor)Ethyl ParathionPentachlorophenolPhoratePicloramPrometryne

DateAnalyzed

2013/10t092013/101092013/10/092013110/092013/10t092013/101092013/101092013/10/092013/10/092013/10/072013110/072013/10/072013/10/072013/101072013/101072013/101072013/1010720't3/101072013/101072013/10/072013/10/072013/10/042013/10/042013/10/0420't3nola42013/101042013/10/042013110/042013/10/042013/10/0420't3/101042013/101042013/10/042013110/042013/10/042013/1010420't3/10/042013/101042013/101042013/10/042013/10/042013/10/042013/10/042013/101042013/1010420131101042013110/042013/10/042013/101042A13/10/0420131101042013110/0420131101o42013/'t0/042013/10104

ValueND, RDL=0.006ND, RDL=0.02ND, RDL=0.05ND, RDL=0.05ND, RDL=0.05ND, RDL=0.05ND, RDL=0.05ND, RDL=0.05ND, RDL=0.05

921027390

10365

ND, RDL=10ND, RDL=2ND, RDL=10NCNCNC

B310475

1057197

1 1 1B3

1 0 1789690604854

10' l'1031121051 0 1609993

1 1 679

100B8

1 0 165

100938B58

1 1 1

ug/Lugilug/Lug/Lug/Lug/Lug/Lug/Lug/L

o//oo //o

%-/o

/o

%ug/Lug/Lug/L

/oo/

%%o//o

%Y"o/

o// o

%/o

%o/^

%

o/

o/

%o//o

%o//o

/o

%o//o

/o

%o//oo/

/o

%%o//oo/

%o//o

"/o

%

40 - 13040 - 13040 - 13040 - 13040 - 13040 - 130

404040

30 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13040 - 13070 - 13030 - 13030 - 13030 - 13040 - 13040 - 13040 - 13040 - 13040 - 13040 - 13040 - 13030 - 13040 - 13040 - 13040 - 13040 - 13040 - 13040 - 13040 - 13025 - 13040 - 1301 0 - 1 3 030 - 130

Page l0 of 15

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fVf a SarrrWSH LabsAttention: Bill WongClient Project #:P.O. #:7007Site Location:

Quality Assurance Report (Continued)Maxxam Job Number: MB3G6957

Page 11 of 15

iJraxx4Ana|yn .3merna i |on . lcorpdar iono/aMaxmAE|y l l66740cfpDbe| ,oBoad 'M|sbs .onE|o 'L$48

OfuOCBatchNum ln i t

3374182 WZ

DateAnalyzed

rameter

1 , 9

3.7

14.9

1 . 3

1 . 7

0.08

1 . 2

0 .1

1 . 1

tS40 - 13040 - 13040 - 13040 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 13030 - 130

4030 - 130

4030 - 130

4030 - 130

4A30 - 130

4040 - 130

4070 - 130

4030 - 130

4030 - 130

4030 - 130

4040 - 130

4040 - 130

4040 - 130

4040 - 130

4040 - 130

4040 - 130

4040 - 130

4030 - 130

4040 - 130

4040 - 130

4040 - 130

4040 - 130

40

Matrix Spike

Spiked Blank

RPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPD

2013/1010420131101042013nO/A4201s1101042013/101042013/1010420131101042013/101042013/10/042013t10t042013/1010420131101042013/10/042013/101042013/101042013/10/042013/10t0420131101042013/10/042013/10/042013/10t042013/101042013/10/042013/10/042013/10/042013/10/042013/10t042013/10/042013/10/042013/10/042013/10/042013/10/042013/10/042013/10/042013110/042013/10/042013/101042013/10/042013110/042U3nAl042013/10/042013t10/0420131101042013/10/042013/10/042013/10/042013/10/042013/10/042013/10/042013/10/042013/10/042013110/042013/101042013/10/042013110/04

SimazineTerbufosTriallateTrifluralinBenzo(a)pyreneMethyl parathion2,4,6-Tribromophenol2,4-Dichlorophenyl Acetic Acid2-FluorobiphenylD14-Terphenyl (FS)D5-Nitrobenzene2, 3, 4, 6-Tetrach I oro ph en ol2, 3, 4, 6-Tetrach loroph en ol2,4,5-T2,4,5-T2,4,6-Trich lorophenol2,4, 6-Trich lorophenol2,4-D2,4-D2,4-Dichlorophenol2,4-DichlorophenolAlachlorAlachlorAldicarbAldicarbAtrazineAtrazineDes-ethyl atrazineDes-ethyl atrazineAtrazine + Desethyl-atrazineAtrazine + Desethyl-atrazineBendiocarbBendiocarbBromoxynilBromoxynilCarbarylCarbarylCarbofuranCarbofuranChlorpyrifos (Dursban)Chlorpyrifos (Du rsban)Cyanazine (Bladex)Cyanazine (Bladex)DiazinonDiazinonDicambaDicambaDiclofop-methylDiclofop-methylDimethoateDimethoateDinosebDinosebMalathionMalathion

558790

1 1 01 1 0BBBB

102B4

1 0 977

103

%

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2 .1

3.6

2 .1

1 1 3

91

99

B6

102

100

51

57

104

106

1 1 1

105

5.0

1 . 7

1 . 5

3.2

1 , 6

1 . 4

1 , 5

1 . 7

0.6

1 . 4

103

79

102

92

120

103

91

lVf a #arrtWSH LabsAttention: Bill WongClient Project #:P.O. #:7007Site Location:

Quality Assurance Report (Continued)Maxxam Job Number: M83G6957

QA/QCBatchNum In i t

3374182 WZQ C TSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDSpiked BlankRPDMethod Blank

ParameterMetolachlorMetolachlorMetribuzin (Sencor)Metribuzin (Sencor)Ethyl ParathionEthyl ParathionPentachlorophenolPentachlorophenolPhoratePhoratePicloramPicloramPrometrynePrometryneSimazineSimazineTerbufosTerbufosTriallateTriallateTrifluralinTrifluralinBenzo(a)pyreneBenzo(a)pyreneMethyl parathionMethyl parathion2,4,6-Tribromophenol2,4-Dichlorophenyl Acetic Acid2-FluorobiphenylD14-Terphenyl (FS)D5-Nitrobenzene2,3, 4, 6-Tetrach loroph enol2,4,5-T2,4,6-Trich lorophenol2,4-D2,4-DichlorophenolAlachlorAldicarbAtrazineDes-ethyl alrazineAtrazine + Desethyl-atrazineBendiocarbBromoxynilCarbarylCarbofuranChlorpyrifos (Du rsban)Cyanazine (Bladex)DiazinonDicambaDiclofop-methylDimethoateDinosebMalathionMetolachlorMetribuzin (Sencor)

DateAnalyzed

2013/101O42013/10/042013/10/042013/10t0420131101042013/101042013/101042013/101042013/101042013/101042A13/101042013/101042013/10tO42013/10/042013/101042013/101042013/10/A42013110/0420131101042013/101042A13/101042A13/10/042013110/042013110/0420131101042013/1010420131101042013110/042013/10/042013110/042013110/042013/101042013110/04201311010420131101042013/101042013110/042013110/042013110/042013110/042013/10/042013/10/042013110/042013110104201311010420131101042013110/042013110/0420131101042013/10/042013110/042013n0/a42013nAt042A131101042013110104

1 . 91 0 1

0.0197

0.0496

2.657

12.7

1 . 5

0.2

2.5

0.8

0.02

1 , 890

1 . 879927B

10277

ND, RDL=0.50ND, RDL=1.0ND, RDL=0.50ND, RDL=1.0ND, RDL=0,50ND, RDL=0.50ND, RDL=5.0ND, RDL=0.50ND, RDL=0,50ND, RDL=1.0ND, RDL=2.0ND, RDL=0,50ND, RDL=5.0ND, RDL=5.0ND, RDL=1.011P, PlPl-=1.0ND, RDL=1.0ND, RDL=1.0ND, RDL=0.9011P, PPL=2.5ND, RDL=1,0ND, RDL=5.0ND, RDL=0.50ND, RDL=5.0

QC Limits40 - 130

4040 - 130

4040 - 130

4025 - 130

4040 - 130

401 0 - 1 3 0

4030 - 130

4040 - 130

4040 - 130

4040 - 130

4040 - 130

4030 - 130

4030 - 130

4030 - 13030 - 13030 - 13030 - 13030 - 130

Value

0.2105

67

Unitso//o

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ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

1 1 1

60

94

95

112

1 1 1

Page 12 of 15

I\,brx.mAna|!nbsfltsmdona|corpdabnoraMdlmAE|yl|cs674ocmpobelbBoad'M|sbsalga'omar'L5N18

lVf a #arrrWSH LabsAttention: Bill WongClient Project #:P.O. #: 7007Site Location:

Quality Assurance Report (Continued)Maxxam Job Number: M83G6957

Page 13 of 15

NtagfAna|y r ics |a ie rna t ioha lcdporar lono/aMdamAm|y l l cs674ocmpobe| |oBMd'M|sbsa.onafo 'L$18

DateAnalyzed

QA/QCBatchNum In i t QC T

3374487 EAX

3377138 HKL

3379157 HIN

Matrix SpikeSpiked BlankMethod BlankRPDMatrix SpikeSpiked BlankMethod BlankRPDMatrix Spike

2013/10/042013/10/042013110/042013hO/A42013/101042013/101042013110/042013/10/042013/10/042013/101042013/101042013/10/072013/10/072013/10/072013110/072013/101082013/10/082U3hA/oe2013/101082013/101112013110/112013/10/112013/10/112013/10/112013/10/112013/10/112013110/102013/10/102013/10/102013/10/102013/10/102013/10/102013/10/102013110/092013/10/092013/10/092013110/0920131101092A13/10/092013/10/092013/10/092U3hAh02013/101102013/10/102013/10/102013110/102013/10110

1

ND, RDL=1.0ND, RDL=0.50ND, RDL=0.50ND, RDL=5.0ND, RDL=0.25ND, RDL=1.0ND, RDL=0.50ND, RDL=1.0ND, RDL=1 .0ND, RDL=0.0090ND, RDL=1.0

1 1 1104

ND, RDL=0.05NC

1 0 1107

ND, RDL=10NC

79104B587809097B395B489B695

1028B

ND, RDL=5,0ND, RDL=5.0ND, RDL=5.0ND, RDL=5.0ND, RDL=5.0ND, RDL=5.0ND, RDL=5.0NCNC1 . 67.7NCNC1 . 6

3374182 WZ Method Blank Ethyl ParathionPentachlorophenolPhoratePicloramPrometryneSimazineTerbufosTriallateTrif lural inBenzo(a)pyreneMethyl parathionNTANTANTANTAGlyphosateGlyphosateGlyphosateGlyphosate2,3-Dibromopropionic AcidMonochloroacetic Acid (MCAA)Monobromoacetic Acid (MBAA)Dichloroacetic Acid (DCAA)Trichloroacetic Acid (TCAA)Bromochloroacetic Acid (BCAA)Dibromoacetic Acid (DBAA)2,3-Dibromopropionic AcidMonochloroacetic Acid (MCAA)Monobromoacetic Acid (MBAA)Dichloroacetic Acid (DCAA)Trichloroacetic Acid (TCAA)Bromochloroacetic Acid (BCAA)Dibromoacetic Acid (DBAA)2,3-Dibromopropionic AcidMonochloroacetic Acid (MCAA)Monobromoacetic Acid (MBAA)Dichloroacetic Acid (DCAA)Trichloroacetic Acid (TCAA)Bromochloroacetic Acid (BCAA)Dibromoacetic Acid (DBAA)Total haloacetic acidsMonochloroacetic Acid (MCAA)Monobromoacetic Acid (MBAA)Dichloroacetic Acid (DCAA)Trichloroacetic Acid (TCAA)Bromochloroacetic Acid (BCAA)Dibromoacetic Acid (DBAA)Total haloacetic acids

Spiked Blank

Method Blank

RPD

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lugilug/Lug/Lug/L

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%/o

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75 - 12575 - 125

2550 - 13050 - 130

4070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 1307 0 - 1 3 0

40404040404040

icate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measuremenl.trix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.

piked Blank: A blank matrix sample to which a known amount of the analyte, usually from a second source, has been added. Ljsed to evaluate method

Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.urrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency.

(RPD)| The RPD was not calculated. The level of analyle detected in the parent sarnple and ils duplicate was not sufficiently signfficant lo p€rmit a

- / ilVf a#arrrWSH LabsAttention: Bill WongClient Project #:P.O. #:7O07Site Location:

Quality Assurance Report (Continued)Maxxam Job Number: MB3G6957

calculation.

Page 14 of 15

lJbxxamAna|y i i ca |n te rna t iona |c4porar iono/aMaxfAm|y t i j6740Gfpobe| |oRoad,Mt€i ss3 ta 'o& io 'L5N

lVf a #arrl

Maxxam Job #:83G6957

The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).

0u* Muin^e-Cristina Carriere, Scientitic Services

h ! lSd""F W*4

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature page.

Page 15 of 15

n/bt,mA.a|yncsmernaliona]cdporariono/ai,agnArElyli5674ocfpobel|oBdad'M|sbs4ga'otl&iJ'L5N

Senior Analyst, Semi-Volatiles

Analysts

ialist (Organics)

lVf a #arTtYour P.O. #: 70A7Your C.O.C. #: 4090989

@WSH Labs3851 B - 21 St NECalgary , ABT2E 6T5

Report Date: 2013110116

CERTIFICATE OF ANALYSIS

MAXXAM JOB #:B3H2132Received: 201 3/1 0/09, 09:58

Sample Matrix: Water# SamDles Received: 1

Date Daie MethodAnalvses Ouaniitv Extracted Analyzed Laboratory Method ReferenceVOCs (Drinking Water) 1 N/A 2013110/16 CAM SOP-00226 EPA 8260

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

EncryPtion KeY ,1 .ramesAspin

/,./*7* -"

-.ruv * 17 oct 2013 11:2Q:29 -04:00

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

James Aspin, Senior Project ManagerEmail: JAspin @ maxxam,caPhone# (905) 817-5771

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17O25:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Total cover pagesi I

Page 1 of 6

|'JIarxamAna|yncahrernaliona|corpqationo/aMdmAm|ylis674ocanpobe||oAoad'Mlsi$a,oa,om?rk)'L5Al

,/]lVl a ></a rrrL' /

WSH LabsMaxxam Job #:B,3H2132Report Date: 201 311 011 6

Your P.O. #:7007

VoLATTLE ORGANTCS BY GC/MS (WATER)

Vlaxxam lD TK3301Sampling Date 2013/10107

1 1 : 0 0IOC Number A090989

Units 73620-EMERALDBAY

lDL )C Batch

Page 2 of 6

lvaltmAna|ytcslntermtona|corporaiono/aMarxmAE|yrhs6740cm@be]IoFBd'M|$issaucE'onl4i''L5N2La

Volatile Organics1 ,1 -Dichloroethylene ugil ND ) . 1 0 33784381 ,2-Dichlorobenzene ug/L ND ).20 33784381 .2-Dichloroethane ug/L ND ).20 3378438,4-Dichlorobenzene ug/L ND ).20 3378438

3enzene ug/L ND . 1 0 3378438Sromodichloromethane ug/L 0.66 . 1 0 3378438Jromoform ug/L N D ).20 3378438larbon Tetrachloride ug/L ND 1 0 3378438lhlorobenzene ug/L ND 1 . 1 0 3378438lhloroform ug/L 1 1 . 8 1 0 3378438libromochloromethane ugil ND ).20 3378438Vlethylene Chloride( Dich loromethane)ug/L ND ).50 3378438

thylbenzene ug/L ND 1 0 3378438Vlethyl t-butyl ether (MTBE) ug/L ND ).20 3378438Ietrachloroethylene ug/L ND . 1 0 3378438foluene ug/L 1 .22 J.20 3378438frichloroethylene ug/L ND . 1 0 3378438Vinyl Chloride ug/L ND ).20 3378438r-Xylene ug/L ND 1 0 3378438r+m-Xylene ug/L ND ) . 1 0 3378438lotal Trihalomethanes ug/L 12.4 ) .20 3378438Surrogate Recovery (%)1-Bromofluorobenzene o/ 95 N/A 3378438)4-1,2-Dich loroethane V" 74 N/A 3378438)B-Toluene 106 N/A 3378438

\D = lrlel detectedtl/A = Slel ApplicablelDL = Reportable Detection LimitfC Batch = Quality Control Batch

/ iI \ r la { /arTt'/

wsH LabsMaxxam Job #: B,3H2132Report Date: 2013110116 your p.o. #:7oo7

GENERAL COMMENTS

Results relate onlv to the items tested.

Page 3 of 6

[9 : ImAna| !n ica |n t rMnona|corpda l iono ' /aMagmA.Ety ' l |6674oGmpoDe| |oR@d.Mbs iss | . 'o io ,L5N18

N/f a #atTlWSH LabsAttention: Bil l WongClient Project #:P.O. #: 7007Site Location:

Qual ity Assu rance ReporlMaxxam Job Number: M83H2132

Page 4 of 6

MaxxanAna|yrica|rfernatbna|Gorporario.o/aMdd|Am|yl|6674ocfpobe||oBoad.Mlsbg.Ea'omeb.L5N2La

QA/OCBatchNum lnit QC Tvoe Para

DateAnalyzed

3378438 EAY Matrix Spike

Spiked Blank

Method Blank

4-BromofluorobenzeneD4-1,2-DichloroethaneDB-Toluene1 ,1-Dichloroethylene1 ,2-Dichlorobenzene1 .2-Dichloroethane1 ,4-DichlorobenzeneBenzeneBromodichloromethaneBromoformCarbon TetrachlorideChlorobenzeneChloroformDibromochloromethaneMethylene Chloride(Dichloromethane)EthylbenzeneMethyl t-butyl ether (MTBE)TetrachloroethyleneTolueneTrichloroethyleneVinyl Chlorideo-Xylenep+m-Xylene4-BromofluorobenzeneD4-1,2-DichloroethaneD8-Toluene1 ,1-Dichloroethylene1 ,2-Dichlorobenzene1 ,2-Dichloroethane1 ,4-DichlorobenzeneBenzeneBromodichloromethaneBromoformCarbon TetrachlorideChlorobenzeneChloroformDibromochloromethaneMethylene Chloride(Dichloromethane)EthylbenzeneMethyl t-butyl ether (MTBE)TetrachloroethyleneTolueneTrichloroethyleneVinyl Chlorideo-Xylenep+m-Xylene4-BromofluorobenzeneD4-1,2-DichloroethaneD8-Toluene1 ,1-Dichloroethylene1 ,2-Dichlorobenzene1 ,2-Dichloroethane1 ,4-DichlorobenzeneBenzeneBromodichloromethane

20131101152013/10115201311011520131101152013110115201311011520131101152A13nOn520131101152013110115201311011520131101152013/101152013/1011520131101152013/1011520131101152013/1011520131101152013/1011520131101152013/1011520131101152013110115201311011520131101152013/10/152A13/101152013110/15201311011520131101152013/10/1s2013/101152013/101152013/10/152013110/152013/10/152013/10/1520131101152013/101152013/101152013/101152013/101152013/101152A13/101152013/10/152A13/101152013/10/152013/10/152013/10/152A13/101152013/10/152013110/152013110/152013/10/15

1 0 177

1081 0 19B909892

NC10299

100NC103B999B9

1071 0 196919697

1 0 177

1079B948B9490BB99979BB5998796BB

1049693B993959578

105ND, RDL=0.10ND, RDL=0.20ND, RDL=0.20ND, RDL=0.20ND, RDL=O.10ND, RDL=0,10

o/

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ug/Lug/Lug/Lug/Lug/Lug/L

70 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 13070 - 130

lVf a SarrrWSH LAbSAttention: Bil l WongClient Project #:P.O. #:7007Site Location:

Quality Assurance Report (Continued)Maxxam Job Number: MB3H2132

Page 5 of 6

I !bxxmAnaly r ic i lmFnat |ona |corporanono/aNIagmAE|y l iB6740cm! .be | |oRoad 'Mt6 i9s38 'on la ib '$N48

QA/QCBatch

ln i t3378438 EAY Method Blank

RPD

ParameterBromoformCarbon TeirachlorideChlorobenzeneChloroformDibromochloromethaneMethylene Chloride(Dichloromethane)EthylbenzeneMethyl t-butyl ether (MTBE)TetrachloroethyleneTolueneTrichloroethyleneVinylChlorideo-Xylenep+m-XyleneTotal TrihalomethanesBromodichloromethaneBromoformChloroformDibromochloromethaneTotal Trihalomethanes

DateAnalyzed

/mm/dd20131101152A13110/1520131101152013110/152013110/152013110/152013110/152013110/1520131101152013110/152013110115201311011520131101152013110/152013/1011520131101162013/101162013/10t162013/101162013110116

ND, RDL=0.20ND, RDL=0.10ND, RDL=O.10ND, RDL=0.10ND, RDL=0.20ND, RDL=0,50ND, RDL=0.10ND, RDL=0.20ND, RDL=0.10ND, RDL=0.20ND, RDL=O,10ND, RDL=0.20ND, RDL=0.10ND, RDL=0.10ND, RDL=0.204.9NC4 .1NC4

V Unitsug/Lug/Lug/Lug/Lug/Lug/LuglLugilug/Lug/Lugilug/Lug/Lug/Lug/L%v/^

o/^

o //oo //o

oc

3030303030

te: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.

Diked Blank: A blank mairix sample to which a known amount of the analyte, usually from a second source, has been added. Used to evaluate method, 'Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination,

urrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency.(Matrix Spike)t The recovery in the malrix spike was not calculated. The relative difference belween lhe concentration in the parent sample and the

amount was not sufficiently significant to permit a reliable recovery calculation.(BPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicale was not sufficiently significanl to permit a

iable calculation.1 ) POTENTIAL EXCEEDENCE FOR PARAMETER

rVf a {;i^rrl

Maxxam Job #:83H2132

The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).

A,'lu lailh,^e-Cristina Carriere, Scientific Services

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.1O.2 ofISO/IEC 11025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Paoe 6 of 6

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