Page No.01

TH MS TQ TW PR LW LQ

MAX MIN MAX MIN MAX MIN MAX MIN MAX MIN MAX MIN MAX MIN

70 2270 2270 2270 2270 22- -- -- -

20 -20 -20 -20 -20 -- -- -- --

10 -10 -10 -10 -10 -- -- -- --

- -- -- -- -- -- -- -- --

- -- -30 930 930 930 9- -- -

- -- -20 -20 -20 -20 -- -- --

- -- -- -- -- -- -50 -50 --

4 -4 -4 24 24 2- 2- 2- 2

100100150150150505050

SUBJECT CODETHEORY PRACTICAL

CREDIT TOTALTH- THEORY MS-MID SEM

TW- THEORY TERMWORKPR- PRACTICALLW- LAB WORKPQ- PRACTICALQUIZ G - GRADEGP- GRADE POINT

F$-ABSENT#-GRACE

70 2270 2270 2270 2270 22- -- -- -

20 -20 -20 -20 -20 -- -- -- --

10 -10 -10 -10 -10 -- -- -- --

- -- -- -- -- -- -- -- --

- -- -20 -20 -20 -20 -- -- --

- -- -- -- -- -- -50 -50 --

4 -4 -4 24 24 2- 2- 2- 2

100100150150150505050

TH- THEORY MS-MID SEM

TW- THEORY TERMWORKPR- PRACTICALLW- LAB WORKPQ- PRACTICALQUIZ G - GRADEGP- GRADE POINT

F$-ABSENT#-GRACE

SUBJECTMass Transfer Operation –IIChemical Process Industries-IIProcess Equipment Design-IPollution Control & Safety ManagementComputer Aided Process SynthesisSoftware lab-IVSELF STUDY (INTERNAL ASSESMENT)

SEMINAR / GROUP DISCUSSION (INTERNAL ASSESSMENT)

TH PR MAXBT-601CH-602CH-603CH-604CH-605CH-606CH-607CH-608

SCHEME OF B.TECH CHEMICAL SEM- VISUBJECT CODE

BT-601CH-602CH-603CH-604CH-605CH-606CH-607CH-608

- -- -30 930 930 930 -- -- -

B.Tech. Chemical Engg.Semester -VI

Sr.No Course Content Total

Hrs.1. Distillation:

Binary System: Introduction, Vapor-liquid Equilibria, P-x-y T-x-ydiagrams,concept of volatility and effect of P and T on equilibrium data, Idealsolutions, Raoult's Law as applied to distillation operations, Deviation fromideality, Minimum and maximum boiling azeotropic mixtures, Enthalpy-concentration diagrams, their characteristics. Flash distillation, steamdistillation, simple distillation, continuous rectification, Batch fractionationetc., Determination of number of stages by Ponchon and Severit methodand McCabe-Thiele method, Concept of minimum, total and optimumreflux ratio, Reboilers, Use of open steam, , Partial condensers, cold hotcirculating reflux etc.Azeotropic Distillation,Extractive Distillation

25

2. Humidification and dehumidification:Vapour liquid Equilibria, Enthalpy of saturated and unsaturated vapourliquid mixtures, adiabatic saturation curves, concept of wet bulb and drybulb temp. Lewis relation, water-cooling with air, Dehumidification of air-water vapour, Various types of cooling tower & their selection criteria,wetbulb approach & range of cooling tower,Cooling tower fillings,Calculationsof make-up water requirement of cooling tower.

10

3. Adsorption and ion exchange:Types of adsorption, Nature of adsorbents, adsorption Equilibria,adsorption of single gas/vapour from gaseous mixture, dilute andconcentrated liquid solutions, fixed bed, ion-bed adsorbers, principles ofion exchange. Equilibria and rate of ion exchange.

09

Swami Vivekanand University,Sironja Sagar (M.P.)

Page No.05

Subject Name: Mass Transfer Operation-II

B.Tech. Chemical Engg.Semester -VI

Sr.No Course Content Total

Hrs.1. Dyes and Intermediates:

Classification of dyes according to constitution and application, variousdyes such as Azo dyes, Anthroquione dyes, Triamyl dyes, dispersed dyes,Misc. Dyes such as azine, oxazines, thiazines, thiazoles, nitro dyes etc.Various dye intermediates based on unit processes ,ManufacturingProcesses of Crome blue black,H-acid,Koch acid,Vinyl sulphone,Wetdyes,Nitro benzene,Aniline,etc.

14

2. Drugs and Pharmaceuticals:Classification of various drugs and pharmaceuticals, Introduction ofAntibiotics such as penicillin, streptomycin,erithromycin ,Introduction ofvitamins,Manufacturing processes of Aspirine,Vitamin-C,Insulin,Ascorbicacid,Barbital & Pheno Barbital

14

3. Sugar, Paints, Pigments:Manufacturing of Sugar, Paints, different types of pigments such as white,blue, red, yellow, green, brown, etc , Varnishes, Indsrial Coatings, printinginks, Polishes etc

14

4. Fermentation industries :Industrial alcohol, absolute alcohol, beers wines and liquors,Manufacturing of Butyl alcohol & Citric acid by Fermentation

12

Practical and Term-work:

Experiments based on the above topics for the testing, identification, analysis andpreparations etc. should be given to the students.

Swami Vivekanand University,Sironja Sagar (M.P.)

Page No.11

Subject Name: Chemical Process Industries – II

Text Book:

1. Shreve’s chemical process industries- George Austin.2. DRYDENS outlines of chemical technology for the 21st century, third edition by

M Gopalarao & Marsal Sitting, pub East-West Press

Reference Books:1. Biotechnology, Chemical feedstock and Energy utilization-D. F. Gibbs.

Swami Vivekanand University,Sironja Sagar (M.P.)

Page No.12

4. Drying: 10Equilibrium relationship, Drying operations and equipments, Equilibriummoisture, Bound moisture, unbound moisture, free moistureetc.,Hysteresis in Drying, Batch drying, rate of drying, time of drying,Cross-circulation drying, concept of NoG and HoG, Drying at lowtemperature, Freeze drying etc. Mechanism of various dryingoperations,Batch & continuous drying equipments-Tray dryer,Tunneldryer, Rotary dryers, Spray dryers,Fluidized bed dryer, etc.

Practical and Term-work:

Experiments based on the above topics

Text Book:

“Mass transfer operation"by R.E.Treybal, Mc-Graw Hill international

Reference Books:

1 “Mass Transfer” by Sherwood,Pigford & Wilke, Mc-Graw Hill international2 “Chemical Engineering”,Volume-2 ,4th edition by Coulson & Richardson3 Perry’s Chemical Engineers handbook,7th edition by Perry & Green, Mc-Graw

Hill international4 Unit Operations of Chemical Engg. By W.L. McCabe , J. C. Smith & Harriott,6th

edition Mc-Graw Hill international

Swami Vivekanand University,Sironja Sagar (M.P.)

Page No.06

B.Tech. Chemical Engg.Semester -VI

Sr.No Course Content Total

Hrs.1. Process design of piping, Fluid moving devices and Flow meters:

Introduction, Process design of piping,NPSHA &NPSHR,Power requiredby pump, evaluation of Centrifugal pump performance when handlingviscous liquids, Power required in Fan, Blower and adiabatic compressor,flow meters, Process design of Orifice meter, Rotameter etc.

10

2. Process design of Heat exchangers:Shell & Tube heat exchangers, Funcion of various parts of shell & TubeHeat exchaner, General design method of shell & tube heat exchanger,Criteria of selection among Fixed Tubesheet,U Tube & Floating Headheatexchanger,Process design of without phase changeheatexchanger,Process design of condenser, Horizontal and verticalcondenser, Condensation with non-condensable, Multi-componentcondensation, Process design of Kettle type &Thermosyphon Reboilersand vaporizes, Tinker’s flow model, Air cooled heat exchangers and airheaters, plate heat exchangers, etc.

20

3. Process design of Distillation Column:Introduction, Criteria of selection, Selection of equipment for distillation,Distillation column design, Selection of key components formulticomponent distillation,Determination of operating pressure fordistillaion column,Advantages & disadvantages of vacuum distillation,Determination of nos. of theoretical stages for binary distillation byMeCabe Thiele method & Ponchon-Savarit method, Determination of nos.of theoretical stages for multicomponent distillation by Fenskey-Underwood-Gilliland’s method,Selection of trays,Calculations for towerdiameter & pressure drop of sieve tray tower, Cheking of conditions forweeping,downcomer flooding,liquid entrainment,etc, tray efficiency,JetFlooding & downcomer Flooding,Different types of weirs & downcomers oftray tower, their selection criteria,Process design of Batchdistillation,simple batch distillation & batch distillaion with rectification.

18

Swami Vivekanand University,Sironja Sagar (M.P.)

Page No.09

Subject Name: Process Equipment Design – I

4. Process design of Absorbers:Introduction, Criteria for selection among different types of absorptionequipment, Process Design of packed tower type absorber: Determinationof actual amount of solvet, Selection of packing, Determination of towerdiameter & pressure drop, Detrmiation of NtoG, HtoG & height of packing,Process design & selection criteria of liquid distributors,redisributors &packing support, Process design of Spray chamber or spray tower typeabsorber, Venturi Scrubber, Process design of falling film absorber.

12

5. Process design of Extactor:Indutrial applications of liquid-liquid extraction,choice of solvent,Processdesign of counter current multistage extractor, Selection criteria amongdifferent types of extactor, Process design of mixer-settler type extractor& packed tower type extractor, Guidelines for the design of other types ofextractors

12

Text Book:

1. “Introduction to Process Engineering and Design” by S B Thakore and B I Bhatt,Tata McGraw Hill, 1st Edition, 2007.

Reference Books:

1. Coulson & Richardson’s Chemical Engineering - Vol. 6 by R.K.Sinnott,AsianBook Pvt. Ltd. (publisher)

2. Applied Process Design for Chemical and Petrochemical plants,Vol. 1to 3 byE.E.Ludwig, Gulf Publishing Company

Swami Vivekanand University,Sironja Sagar (M.P.)

Page No.10

B.Tech. Chemical Engg.Semester -VI

Sr.No Course Content Total

Hrs.a. Environmental Protection:

Concept of environment and ecology, various natural cycles in environmentand ecology, effect of human activities on environment and ecology. Varioustypes of environmental pollution in general and in chemical and allied industryin particular, sources and causes of environmental pollution, effect of pollutionon environment, environmental impact assessment and EIS, methodologiesfor environmental pollution prevention (including process technology upgradation, development, Invention etc.), control, abatement and treatment andwaste disposal. Rules, regulations, laws etc. regarding environmentalprotection, pollution prevention and control, waste disposal etc. Role ofgovernment, semi/quasi govt. and voluntary organizations. Current trends andtopics

18

b. Introduction to Industrial laws, Industries Factory act, Energy audit,Environment Audit, Trade union, Labour laws and acts. Industrial Electricityrules, Industrial Dispute Acts, Workmen compensation Act, ESIC Act,Payment and Wages act, Minimum Wages act, Payment of Bonus act, Recenttrends and practices in Safe industrial practices

9

c. Safety Management:Current practices and topics in safety management, rules, regulations,laws etc. for safety management in industry.

1. General IntroductionHistorical Background, Grown of Safety Science, Aims of SafetyScience, Safety and the Organization.

2. Basic Concepts of Safety Science.Hazard, Risk, Nature of the accident process, Use of EngineeringFundamentals in safety science.

3. Techniques of Hazard IdentificationHazard and Operatbility Studies (HAZOP), Safety Audits, HazardAnalysis.

8

Swami Vivekanand University,Sironja Sagar (M.P.)

Page No.07

Subject Name: Pollution Control & Safety Management

4. Fault and Event Tree Analysis for Risk Prediction5. Source Models

Models of Accidental Release of Toxic/Flammable liquids and vapors,Models of flow of liquids and vapors through pipes.

6. Dispersion Models:Mathematical Models for prediction of Dispersion patterns fortoxic/flammable materials released into atmosphere, various types of"plume" and "puff" models of dispersion.

9

7. Nature of fires and explosionCalculation of Blast damage due to over-pressure, prevention of firesand explosions.

8. Control of Major Chemical Hazards, Emergency Control and disasterplanning.

9. Introduction to various personal protective equipments10. Instruments for safety : Pressure safety valve, Rupture disc , Interlocks

etc..

10

Text Books:

1. Frank P Lees, "Loss Prevention in Process Industries" Volume 1, 2 & 32. Industrial Organization and Economics by T.R. Banga & S.C. Sharma

Reference Books:

1. Environment Engg. by Metcalf and Eddy2. Enviornmental Pollution Control Engineering By C.S.Rao

Swami Vivekanand University,Sironja Sagar (M.P.)

Page No.08

B.Tech. Chemical Engg.Semester -VI

Subject Name: Computer Aided Process Synthesis

Detailed Process Synthesis - Algorithmic Methods:

Sr.No Course Content Total

Hrs.1. The Design Process-

Design Opportunities, Steps in Product Process Design, EnvironmentalProtection, Safety Considerations, Engineering Ethics, Role of Computers.Reactor Design and Reactor Network Synthesis- Objectives, Reactor Models,Reactor Design for Complex Configurations, Reactor Network Design Usingthe Attainable Region.

12

2. Synthesis of Separation Trains-Objectives, Criteria for Selection of Separation Methods, Selection ofEquipment, Sequencing of Ordinary Distillation for the Separation of NearlyIdeal Fluid Mixtures, Sequencing of Operations for the Separation of Non-ideal Fluid Mixtures, Separation Systems for Gas Mixtures, SeparationSequencing for Solid-Fluid Systems.

15

3. Heat and Power Integration-Objectives, Minimum Utility Targets, Networks for Maximum EnergyRecovery, Minimum Number of Heat Exchangers, Threshold ApproachTemperature, Optimum Approach Temperature, Superstructures forMinimization of Annual Costs, Multiple Utilities, Heat-integrated DistillationTrains, Heat Engines and Heat Pumps.

30

4. Optimal Design and Scheduling of Batch Processes-Objectives, Introduction, Design of Batch Process Units, Design of Reactor-separator Processes, Design of Single Product Processing Sequences,Design of Multi-Product Processing Sequencing.

15

Swami Vivekanand University,Sironja Sagar (M.P.)

Page No.03

Text Books:

1. Warren D. Seider, J. D. Seader, Daniel R. Lewin, “Product and Process DesignPrinciples: Synthesis, Analysis, and Evaluation”, 2nd Edition, Wiley(2003)

2. Systematic Methods of Chemical Process Design by Lorens T Biegler, E. I. GnacioGrossmann Arthur W Westerberg, PHI International.

Reference Books:1. T.F. Edgar and D.M. Himmelblau, “Optimization of Chemical Processes”, Chemical

Engg. Series, McGraw Hill2. Richard G. Brereton, “Chemometrics: Data Analysis for the Laboratory and Chemical

Plant”, April 2003 Wiley

Swami Vivekanand University,Sironja Sagar (M.P.)

Page No.04