Origination: The OK Cannabis Program UBI #: Inventory #: … · 2019. 5. 28. · Strain:Soulshine...
4
THCmax (a.k.a. Total THC) = THC + ( THC-A * 0.877 ) CBDmax (a.k.a. Total CBD) = CBD + ( CBD-A * 0.877 ) Total Cannabinoid is a raw sum of all measured cannabinoids In Traceability, Total Cannabinoid is a sum of THCmax and CBDmax Figures may differ slightly from traceability due to rounding ND = Not Detected NE = Not Examined Unk = Unknown Analytical Methods Used Cannabinoids: HPLC-UV Microbial: Plate Counting Terpenes: HS-GC-FID Solvents: HS-GC-MS Trace Residue: UHPLC-MSMS Water Activity: HYGROMER® Page 1 of 4 Official Test Results for Laboratory Sample # 6051344 Origination: The OK Cannabis Program UBI #: Inventory #: 20190516AJT0007 Strain: Soulshine Cannabis - Loopy Fruit License #: QA #: 20190516AJT0007 Type: Flower Harvest Date: Unknown Result #: Unlisted Address: 2310 E Union St, Seattle Date of Receipt: 2019-05-16 Approved By: N. Mosely, CEO Seattle, WA 98112 Date of Testing: 2019-05-20 S. Stevens, LDR PASS/FAIL Foreign Matter+Seeds PASS LossOnDrying(Moisture) PASS Water Activity PASS Microbiological PASS Mycotoxins PASS Pesticides PASS Chemical Profile (units in percent by weight) THC max CBD max Myrcene 19 raw sum: 22 0.041 raw sum: 0.046 0.67 THCA 20 THC 1.1 Caryophy CBDA 0.046 CBD ND 0.17 CBGA 0.44 CBG 0.15 CBC 0.046 CBN ND a-Pinene THCVA 0.12 THCV ND 0.14 D8THC ND CBDV ND CBT ND Terp total: 1.6 Total Cannabinoids (raw sum): 22 100 10 1 0.1 0.01 THC CBD CBG CBC CBN THCV D8- CBDV CBT Shelf Stability Loss-On-Drying 5.7% Water Activity: 0.5373 Terpene Fingerprint (units in percent by weight) 10 1 0.1 0.01 0.001 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 T ref# Name % 6 Myrcene 0.67 34 Caryophyllene 0.17 2 a-Pinene 0.14 12 Limonene 0.1 5 b-Pinene 0.092 36 Humulene 0.088 19 trans-Ocimene 0.076 21 Linalool 0.056 42* pseudo-Valence 0.048 43* Selinadiene 0.027 ref# Name % 41* b-Maaliene 0.026 23 Fenchol 0.023 33* Farnesene 0.019 26 Terpineol 0.012 15* Eucalyptol 0.006 3* Camphene 0.004 49 Bisabolol 0.0039 17 g-Terpinene 0.0022 18 Terpinolene 0.0019 10* a-Terpinene 0.0017 ref# Name % 8* Carene 0.0013 T Total 1.6 Most Volatile Least Volatile *Compounds identified using a spectral library. These testing results are certified by scientific examination of a single sample provided by the Producer/Processor. Confidence Analytics and its agents did not observe or participate in the sample selection process, and cannot confirm the authenticity of the sample or its representativeness of the associated lot/batch. The sample, as received, was homogenized before subsamples were drawn for specific analyses. This report is supplemental to any other reports with the same analytic sample number. Authenticity Verification: MPTPYMQDb6OpJZfOfnvbVk 2019-05-28 08:22:42 19 .041 .54 .046 .11 69% MONO TERPENES 6% MONO TERPENOIDS 23% SESQUI TERPENES 0% SESQUI TERPENOIDS
Transcript of Origination: The OK Cannabis Program UBI #: Inventory #: … · 2019. 5. 28. · Strain:Soulshine...
THCmax (a.k.a. Total THC) = THC + ( THC-A * 0.877 )CBDmax (a.k.a. Total CBD) = CBD + ( CBD-A * 0.877 )
Total Cannabinoid is a raw sum of all measured cannabinoidsIn Traceability, Total Cannabinoid is a sum of THCmax and CBDmax
Figures may differ slightly from traceability due to rounding
ND = Not DetectedNE = NotExamined
Unk = Unknown
Analytical Methods UsedCannabinoids: HPLC-UVMicrobial: Plate Counting
Terpenes: HS-GC-FIDSolvents: HS-GC-MS
Trace Residue: UHPLC-MSMSWater Activity: HYGROMER®
Page 1 of 4
Official Test Results for Laboratory Sample # 6051344Origination: The OK Cannabis Program UBI #: Inventory #: 20190516AJT0007
Strain: Soulshine Cannabis - Loopy Fruit License #: QA #: 20190516AJT0007Type: Flower Harvest Date: Unknown Result #: Unlisted
Address: 2310 E Union St, Seattle Date of Receipt: 2019-05-16 Approved By: N. Mosely, CEOSeattle, WA 98112 Date of Testing: 2019-05-20 S. Stevens, LDR
PASS/FAILForeign Matter+Seeds PASS
LossOnDrying(Moisture) PASSWater Activity PASS
Microbiological PASSMycotoxins PASSPesticides PASS
Chemical Profile (units in percent by weight)
THC max CBD max Myrcene19
raw sum: 220.041
raw sum: 0.046 0.67
THCA 20 THC 1.1 CaryophyCBDA 0.046 CBD ND
0.17CBGA 0.44 CBG 0.15CBC 0.046 CBN ND a-PineneTHCVA 0.12 THCV ND
0.14D8THC ND CBDV NDCBT ND Terp total: 1.6
Total Cannabinoids (raw sum): 22
100
10
1
0.1
0.01THC CBD CBG CBC CBN THCV D8- CBDV CBT
Shelf Stability
Loss-On-Drying 5.7%Water Activity: 0.5373
Terpene Fingerprint (units in percent by weight)10
1
0.1
0.01
0.0011 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 T
ref# Name %6 Myrcene 0.6734 Caryophyllene 0.172 a-Pinene 0.1412 Limonene 0.15 b-Pinene 0.09236 Humulene 0.08819 trans-Ocimene 0.07621 Linalool 0.05642* pseudo-Valence 0.04843* Selinadiene 0.027
ref# Name %41* b-Maaliene 0.02623 Fenchol 0.02333* Farnesene 0.01926 Terpineol 0.01215* Eucalyptol 0.0063* Camphene 0.00449 Bisabolol 0.003917 g-Terpinene 0.002218 Terpinolene 0.001910* a-Terpinene 0.0017
ref# Name %8* Carene 0.0013T Total 1.6
Most Volatile Least Volatile *Compounds identified using a spectral library.
These testing results are certified by scientific examination of a single sample provided by the Producer/Processor. Confidence Analytics and its agents did not observe or participate in the sampleselection process, and cannot confirm the authenticity of the sample or its representativeness of the associated lot/batch. The sample, as received, was homogenized before subsamples were drawn
for specific analyses. This report is supplemental to any other reports with the same analytic sample number.
Authenticity Verification:MPTPYMQDb6OpJZfOfnvbVk
2019-05-28 08:22:42
19
.041
.54
.046
.11
69%MONO
TERPENES
6%MONO
TERPENOIDS
23%SESQUI
TERPENES
0%SESQUI
TERPENOIDS
THCmax (a.k.a. Total THC) = THC + ( THC-A * 0.877 )CBDmax (a.k.a. Total CBD) = CBD + ( CBD-A * 0.877 )
Total Cannabinoid is a raw sum of all measured cannabinoidsIn Traceability, Total Cannabinoid is a sum of THCmax and CBDmax
Figures may differ slightly from traceability due to rounding
ND = Not DetectedNE = NotExamined
Unk = Unknown
Analytical Methods UsedCannabinoids: HPLC-UVMicrobial: Plate Counting
Terpenes: HS-GC-FIDSolvents: HS-GC-MS
Trace Residue: UHPLC-MSMSWater Activity: HYGROMER®
Page 2 of 4
Official Test Results for Laboratory Sample # 6051344Origination: The OK Cannabis Program UBI #: Inventory #: 20190516AJT0007
Strain: Soulshine Cannabis - Loopy Fruit License #: QA #: 20190516AJT0007Type: Flower Harvest Date: Unknown Result #: Unlisted
Address: 2310 E Union St, Seattle Date of Receipt: 2019-05-16 Approved By: N. Mosely, CEOSeattle, WA 98112 Date of Testing: 2019-05-20 S. Stevens, LDR
Quantitative Impurities Report
Concentrations of analytes used to determine pass/fail status of individual tests.
* Greater than lower limit of detection (>LLOD) and less than lower limit of quantification (<LLOQ) . Applies to instances when theanalyte has been detected and positively identified, but the concentration is lower than we can accurately quantify. Literally: signalto noise ratio greater than 3 and signal less than calibration. LLOD is ~0.001 ppm for most analytes, LLOQ is ~0.01 for mostanalytes. Number shown is lower end of calibration (LLOQ).
** Greater than upper limit of quantification (>ULOQ). Applies to instances when the analyte concentration in the sample is greaterthan we can accurately measure without additional testing. Number shown is upper end of calibration (ULOQ).
Findings
ALKANES NOT EXAMINED
ALCOHOLS NOT EXAMINED
SOLVENT IMPURITIES NOT EXAMINED
MYCOTOXINSAnalyte Concentration Action Level*Aflatoxin B1 < LLOQ 20 ppbAflatoxin B2 < LLOQ 20 ppbAflatoxin G1 < LLOQ 20 ppbAflatoxin G2 < LLOQ 20 ppbOchratoxin A < LLOQ 20 ppb*Action Level is Sum of Aflatoxins
MICROBIOLOGICALSOrganism CFU/g Action LevelBTGN Bacteria 0 10,000Yeast and Mold 0 N/AE. coli 0 1Salmonella 0 1
These testing results are certified by scientific examination of a single sample provided by the Producer/Processor. Confidence Analytics and its agents did not observe or participate in the sampleselection process, and cannot confirm the authenticity of the sample or its representativeness of the associated lot/batch. The sample, as received, was homogenized before subsamples were drawn
for specific analyses. This report is supplemental to any other reports with the same analytic sample number.
Authenticity Verification:MPTPYMQDb6OpJZfOfnvbVk
2019-05-28 08:22:42
THCmax (a.k.a. Total THC) = THC + ( THC-A * 0.877 )CBDmax (a.k.a. Total CBD) = CBD + ( CBD-A * 0.877 )
Total Cannabinoid is a raw sum of all measured cannabinoidsIn Traceability, Total Cannabinoid is a sum of THCmax and CBDmax
Figures may differ slightly from traceability due to rounding
ND = Not DetectedNE = NotExamined
Unk = Unknown
Analytical Methods UsedCannabinoids: HPLC-UVMicrobial: Plate Counting
Terpenes: HS-GC-FIDSolvents: HS-GC-MS
Trace Residue: UHPLC-MSMSWater Activity: HYGROMER®
Page 3 of 4
Official Test Results for Laboratory Sample # 6051344Origination: The OK Cannabis Program UBI #: Inventory #: 20190516AJT0007
Strain: Soulshine Cannabis - Loopy Fruit License #: QA #: 20190516AJT0007Type: Flower Harvest Date: Unknown Result #: Unlisted
Address: 2310 E Union St, Seattle Date of Receipt: 2019-05-16 Approved By: N. Mosely, CEOSeattle, WA 98112 Date of Testing: 2019-05-20 S. Stevens, LDR
Chemical Residue Screen - Test Report
Cannabis samples were homogenized and extracted using a custom protocol. Instrumental analysis was performedwith UHPLC-MS/MS (tandem quadrupole). Target compounds were identified by matching to Certified ReferenceMaterials. Ion-selective detection (multiple reaction monitoring, or MRM) was used to ensure that precursor andproduct ions of the correct masses co-eluted and were observed in ratios matching those for the referencematerials.
Dozens of compounds representing many different classes of fungicides, herbicides, and plant growth regulatorswere screened for. This document lists all analytes detected in the Chemical Residue Screen.
Findings
Analyte Name CAS #Amount
In Sample PASS/FAILWA State
Action Level(sum) Spinosads NA NOT DETECTED PASS 0.20 ppm(sum) Permethrins NA NOT DETECTED PASS 0.20 ppmAbamectin B1a 71751-41-2 NOT DETECTED PASS 0.50 ppmAcephate 30560-19-1 NOT DETECTED PASS 0.40 ppmAcetamiprid 135410-20-7 NOT DETECTED PASS 0.20 ppmAldicarb 116-06-3 NOT DETECTED PASS 0.40 ppmAzoxystrobin 131860-33-8 NOT DETECTED PASS 0.20 ppmBifenazate 149877-41-8 NOT DETECTED PASS 0.20 ppmBifenthrin 82657-04-3 NOT DETECTED PASS 0.20 ppmBoscalid 188425-85-6 NOT DETECTED PASS 0.40 ppmCarbaryl 63-25-2 NOT DETECTED PASS 0.20 ppmCarbofuran 1563-66-2 NOT DETECTED PASS 0.20 ppmChlorantraniliprole 500008-45-7 NOT DETECTED PASS 0.20 ppmChlormequat 7003-89-6 NOT DETECTED PASS 0.10 ppmChlorpyrifos 2921-88-2 NOT DETECTED PASS 0.20 ppmcis-Permethrin 52645-53-1 NOT DETECTED PASS 0.20 ppmClofentezine 74115-24-5 NOT DETECTED PASS 0.20 ppmDaminozide 1596-84-5 NOT DETECTED PASS 1.00 ppm
Analyte Name CAS #Amount
In Sample PASS/FAILWA State
Action LevelDiazinon 333-41-5 NOT DETECTED PASS 0.20 ppmDichlorvos 62-73-7 NOT DETECTED PASS 0.10 ppmDimethoate 60-51-5 NOT DETECTED PASS 0.20 ppmEthoprophos 13194-48-4 NOT DETECTED PASS 0.20 ppmEtofenprox 80844-07-1 NOT DETECTED PASS 0.40 ppmEtoxazole 153233-91-1 NOT DETECTED PASS 0.20 ppmFenoxycarb 72490-01-8 NOT DETECTED PASS 0.20 ppmFenpyroximate 134098-61-6 NOT DETECTED PASS 0.40 ppmFipronil 120068-37-3 NOT DETECTED PASS 0.40 ppmFlonicamid 158062-67-0 NOT DETECTED PASS 1.00 ppmFludioxonil 131341-86-1 NOT DETECTED PASS 0.40 ppmHexythiazox 78587-05-0 NOT DETECTED PASS 1.00 ppmImazalil 35554-44-0 NOT DETECTED PASS 0.20 ppmImidacloprid 138261-41-3 NOT DETECTED PASS 0.40 ppmKresoxim-methyl 143390-89-0 NOT DETECTED PASS 0.40 ppmMalathion 121-75-5 NOT DETECTED PASS 0.20 ppmMetalaxyl 57837-19-1 NOT DETECTED PASS 0.20 ppmMethiocarb 2032-65-7 NOT DETECTED PASS 0.20 ppm
* Greater than lower limit of detection (>LLOD) and less than lower limit of quantification (<LLOQ) . Applies to instances when the analyte has been detected and positively identified, but theconcentration is lower than we can accurately quantify. Specifically: signal to noise ratio greater than 3 and signal less than calibration. LLOD is ~0.001 ppm for most analytes, LLOQ is ~0.01 formost analytes. Number shown is lower end of calibration (LLOQ).
** Greater than upper limit of quantification (>ULOQ). Applies to instances when the analyte concentration in the sample is greater than we can accurately measure without additional testing.Number shown is upper end of calibration (ULOQ).
These testing results are certified by scientific examination of a single sample provided by the Producer/Processor. Confidence Analytics and its agents did not observe or participate in the sampleselection process, and cannot confirm the authenticity of the sample or its representativeness of the associated lot/batch. The sample, as received, was homogenized before subsamples were drawn
for specific analyses. This report is supplemental to any other reports with the same analytic sample number.
Authenticity Verification:MPTPYMQDb6OpJZfOfnvbVk
2019-05-28 08:22:42
THCmax (a.k.a. Total THC) = THC + ( THC-A * 0.877 )CBDmax (a.k.a. Total CBD) = CBD + ( CBD-A * 0.877 )
Total Cannabinoid is a raw sum of all measured cannabinoidsIn Traceability, Total Cannabinoid is a sum of THCmax and CBDmax
Figures may differ slightly from traceability due to rounding
ND = Not DetectedNE = NotExamined
Unk = Unknown
Analytical Methods UsedCannabinoids: HPLC-UVMicrobial: Plate Counting
Terpenes: HS-GC-FIDSolvents: HS-GC-MS
Trace Residue: UHPLC-MSMSWater Activity: HYGROMER®
Page 4 of 4
Official Test Results for Laboratory Sample # 6051344Origination: The OK Cannabis Program UBI #: Inventory #: 20190516AJT0007
Strain: Soulshine Cannabis - Loopy Fruit License #: QA #: 20190516AJT0007Type: Flower Harvest Date: Unknown Result #: Unlisted
Address: 2310 E Union St, Seattle Date of Receipt: 2019-05-16 Approved By: N. Mosely, CEOSeattle, WA 98112 Date of Testing: 2019-05-20 S. Stevens, LDR
Chemical Residue Screen - Test Report
Cannabis samples were homogenized and extracted using a custom protocol. Instrumental analysis was performedwith UHPLC-MS/MS (tandem quadrupole). Target compounds were identified by matching to Certified ReferenceMaterials. Ion-selective detection (multiple reaction monitoring, or MRM) was used to ensure that precursor andproduct ions of the correct masses co-eluted and were observed in ratios matching those for the referencematerials.
Dozens of compounds representing many different classes of fungicides, herbicides, and plant growth regulatorswere screened for. This document lists all analytes detected in the Chemical Residue Screen.
Findings
Analyte Name CAS #Amount
In Sample PASS/FAILWA State
Action LevelMethomyl 16752-77-5 NOT DETECTED PASS 0.40 ppmMyclobutanil 88671-89-0 NOT DETECTED PASS 0.20 ppmNaled 300-76-5 NOT DETECTED PASS 0.50 ppmOxamyl 23135-22-0 NOT DETECTED PASS 1.00 ppmPaclobutrazol 76738-62-0 NOT DETECTED PASS 0.40 ppmPhosemet (Imidan) 732-11-6 NOT DETECTED PASS 0.20 ppmPiperonyl Butoxide 51-03-6 NOT DETECTED NA NAPrallethrin 23031-36-9 NOT DETECTED PASS 0.20 ppmPropiconazole 60207-90-1 NOT DETECTED PASS 0.40 ppmPropoxur 114-26-1 NOT DETECTED PASS 0.20 ppmPyrethrin I 8003-34-7 NOT DETECTED NA NAPyridaben 96489-71-3 NOT DETECTED PASS 0.20 ppmSpinosad A 168316-95-8 NOT DETECTED PASS 0.20 ppmSpinosad D 168316-95-9 NOT DETECTED PASS 0.20 ppmSpiromesifen 283594-90-1 NOT DETECTED PASS 0.20 ppmSpirotetramat 203313-25-1 NOT DETECTED PASS 0.20 ppmSpiroxamine 118134-30-8 NOT DETECTED PASS 0.40 ppmTebuconazole 80443-41-0 NOT DETECTED PASS 0.40 ppm
Analyte Name CAS #Amount
In Sample PASS/FAILWA State
Action LevelThiacloprid 111988-49-9 NOT DETECTED PASS 0.20 ppmThiamethoxam 153719-23-4 NOT DETECTED PASS 0.20 ppmtrans-Permethrin 52645-53-2 NOT DETECTED PASS 0.20 ppmTrifloxystrobin 141517-21-7 NOT DETECTED PASS 0.20 ppmUniconazole 83657-22-1 NOT DETECTED PASS 0.10 ppm
* Greater than lower limit of detection (>LLOD) and less than lower limit of quantification (<LLOQ) . Applies to instances when the analyte has been detected and positively identified, but theconcentration is lower than we can accurately quantify. Specifically: signal to noise ratio greater than 3 and signal less than calibration. LLOD is ~0.001 ppm for most analytes, LLOQ is ~0.01 formost analytes. Number shown is lower end of calibration (LLOQ).
** Greater than upper limit of quantification (>ULOQ). Applies to instances when the analyte concentration in the sample is greater than we can accurately measure without additional testing.Number shown is upper end of calibration (ULOQ).
These testing results are certified by scientific examination of a single sample provided by the Producer/Processor. Confidence Analytics and its agents did not observe or participate in the sampleselection process, and cannot confirm the authenticity of the sample or its representativeness of the associated lot/batch. The sample, as received, was homogenized before subsamples were drawn
for specific analyses. This report is supplemental to any other reports with the same analytic sample number.
Authenticity Verification:MPTPYMQDb6OpJZfOfnvbVk
2019-05-28 08:22:42
