UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175 Project 12-0297 Aberdeen Groundwater- Reported by Jeffrey Hendel

4SESD-MTSB

MEMORANDUM

Apr i l 272012

SUBJECT FINAL Analytical Report

Project 12-0297 Aberdeen Groundwater

Superfijnd Remedial

FROM

THRU

Jeffrey Hendel

Quality Assurance Section Chemist

Marilyn Maycock Chief

Quality Assurance Section

TO Jon Bomholm

Attached are the final results for the analytical groups listed below These analyses were performed in accordance with the associated contract Statement Of Work (SOW) In general project data quality objectives have not been used to evaluate these data prior to release by the Quality Assurance Section For a listing of specific data qualifiers and explanations please refer to the Data Qualifier Definitions included in this report

Analyses Included in this report Method Used

Organochlorine Pesticides (OCP)

Organochlorine pesticides CLP Pesticides

Page 1 of 12 CI2I50I OCP FINAL 42712 816

^ UNITED STATES ENVIRONMENTAL PROTECTION AGENCY jS ^ Q B Region 4 Science and Ecosystem Support Division f l ^ ^ ^ I) 980 College Station Road Athens Georgia 30605-2700 ^S^JJ DART Id 12-0175

XpoundPROiS Project 12-0297 Aberdeen Groundwater-Reported by Jeffrey Hendel

Report Narrative for Work Order C121501 Project 12-0297 Site Name Aberdeen Groundwater Aberdeen NC CLPCaseNo 42313 ELEMENT Sample Nos C121307-01 through C121307-07

C121501-01 through C121501-08

Organic Analysis KAP Technologies Inc The Woodlands TX

The ESAT Work Team reviewed data for fourteen (14) water samples analyzed for Pesticide Compounds per CLP Statement of Work SOM012 The samples were collected between 031312 and 031512 and were received by the laboratory on 031512 and 031612 The final data package was received on 040912 by the USEPA Quality Assurance Section Region 4 SESDMTSB The analytical results were reported in one sample delivery group (SDG) by the laboratory In addition to the field samples the laboratory also analyzed one performance evaluation sample (PES) for evaluating the laboratorys perfbnnance with using the method

The laboratory satisfied all technical analysis and extraction holding time requirements A Stage 4 validation consisting of an electronicmanual review (S4VEM) was performed on the organic samples submitted for this case The data package presents acceptable technical performance with qualifications

The percent recovery for gamma-BHC was greater than the upper quality control limit in the matrix spikematrix spike duplicate (MSMSD) performed for sample G121501-01 The positive result for this compound was qualified J (QM-2) in the native sample only

Pesticide results were N CLP12 qualified whenever the percent difference between analytical column results exceeds 25 but is less than 70 Higher percent differences with the attached N qualifier may be indicative of a false positive result

Data qualification factors are explained by the Region 4 - specific qualifier definitions which are included elsewhere in this report Further details are provided in the complete data review report which is on file in the Region 4 SESD Records Center

cc Nardina Turner

Page 2 of 12 C12150I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported byJeffrey Hendel

SAMPLES INCLUDED IN THIS REPORT

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID

ACGMW 12

ACGMW 18

ACGMW25

GE1MW22D

GE1MW24D

GEIMW924D

GE1MW34D

USGS-02-02

Laboratory ID MD D Matrix

C12150I-0I

C121501-02

C121501-03

C12150I-04

C121501-05

C121501-06

C121501-07

C121501-08

6Q26

6Q27

6Q19

6Q22

6Q25

6Q28

6Q24

6Q23

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Date Collected

31412 09

31312 18

31312 16

31312 13

31312 14

31312 14

31312 12

31412 11

20

28

26

18

45

47

16

26

Page 3 of 12 C12I50I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater- Reported by Jeffrey Hendel

DATA QUALIFIER DEFINITIONS

U The analyte was not detected at or above the reporting limit

CLPO 1 Concentration reported is less than the lowest standard on calibration curve

CLPl 2 Difference between GC columns above method waming limit

J The identification of the analyte is acceptable the reported value is an estimate

ISlJ Presumptive evidence that analyte is present reported as a tentative identification wilh an estimated value

OM-2 Matrix Spike Recovery greater than method control limits

ACRONYMS AND ABBREVIATIONS

CAS Chemical Abstracts Service Note Anaiytes with no known CAS identifiers have been assigned codes beginning with E the EPA ID as assigned by the EPA Substance Registry System (wwwepagovsrs) or beginning with R4- a unique identifier assigned by the EPA Region 4 laboratory

MDL Method Detection Limit - The minimum concentration of a substance (an analyte) that can be measured and reported with a 99 confidence that the analyte concentration is greater than zero

MRL Minimum Reporting Limit - Analyte concentration that cortesponds to the lowest demonstrated level of acceptable quantitation The MRL is sample-specific and accounts for preparation weights and volumes dilutions and moisture content of soilsediments

TIC Tentatively Identified Compound - An analyte identified based on a match with the instrument softwares mass spectral library A calibration standard has not been analyzed to confirm the compounds identification or the estimated concentration reported

Page 4 of 12 C121501 OCP FINAL 42712 816

^ UNITED STATES ENVIRONMENTAL PROTECTION AGENCY jS ^ Q B Region 4 Science and Ecosystem Support Division f l ^ ^ ^ I) 980 College Station Road Athens Georgia 30605-2700 ^S^JJ DART Id 12-0175

XpoundPROiS Project 12-0297 Aberdeen Groundwater-Reported by Jeffrey Hendel

Report Narrative for Work Order C121501 Project 12-0297 Site Name Aberdeen Groundwater Aberdeen NC CLPCaseNo 42313 ELEMENT Sample Nos C121307-01 through C121307-07

C121501-01 through C121501-08

Organic Analysis KAP Technologies Inc The Woodlands TX

The ESAT Work Team reviewed data for fourteen (14) water samples analyzed for Pesticide Compounds per CLP Statement of Work SOM012 The samples were collected between 031312 and 031512 and were received by the laboratory on 031512 and 031612 The final data package was received on 040912 by the USEPA Quality Assurance Section Region 4 SESDMTSB The analytical results were reported in one sample delivery group (SDG) by the laboratory In addition to the field samples the laboratory also analyzed one performance evaluation sample (PES) for evaluating the laboratorys perfbnnance with using the method

The laboratory satisfied all technical analysis and extraction holding time requirements A Stage 4 validation consisting of an electronicmanual review (S4VEM) was performed on the organic samples submitted for this case The data package presents acceptable technical performance with qualifications

The percent recovery for gamma-BHC was greater than the upper quality control limit in the matrix spikematrix spike duplicate (MSMSD) performed for sample G121501-01 The positive result for this compound was qualified J (QM-2) in the native sample only

Pesticide results were N CLP12 qualified whenever the percent difference between analytical column results exceeds 25 but is less than 70 Higher percent differences with the attached N qualifier may be indicative of a false positive result

Data qualification factors are explained by the Region 4 - specific qualifier definitions which are included elsewhere in this report Further details are provided in the complete data review report which is on file in the Region 4 SESD Records Center

cc Nardina Turner

Page 2 of 12 C12150I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported byJeffrey Hendel

SAMPLES INCLUDED IN THIS REPORT

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID

ACGMW 12

ACGMW 18

ACGMW25

GE1MW22D

GE1MW24D

GEIMW924D

GE1MW34D

USGS-02-02

Laboratory ID MD D Matrix

C12150I-0I

C121501-02

C121501-03

C12150I-04

C121501-05

C121501-06

C121501-07

C121501-08

6Q26

6Q27

6Q19

6Q22

6Q25

6Q28

6Q24

6Q23

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Date Collected

31412 09

31312 18

31312 16

31312 13

31312 14

31312 14

31312 12

31412 11

20

28

26

18

45

47

16

26

Page 3 of 12 C12I50I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater- Reported by Jeffrey Hendel

DATA QUALIFIER DEFINITIONS

U The analyte was not detected at or above the reporting limit

CLPO 1 Concentration reported is less than the lowest standard on calibration curve

CLPl 2 Difference between GC columns above method waming limit

J The identification of the analyte is acceptable the reported value is an estimate

ISlJ Presumptive evidence that analyte is present reported as a tentative identification wilh an estimated value

OM-2 Matrix Spike Recovery greater than method control limits

ACRONYMS AND ABBREVIATIONS

CAS Chemical Abstracts Service Note Anaiytes with no known CAS identifiers have been assigned codes beginning with E the EPA ID as assigned by the EPA Substance Registry System (wwwepagovsrs) or beginning with R4- a unique identifier assigned by the EPA Region 4 laboratory

MDL Method Detection Limit - The minimum concentration of a substance (an analyte) that can be measured and reported with a 99 confidence that the analyte concentration is greater than zero

MRL Minimum Reporting Limit - Analyte concentration that cortesponds to the lowest demonstrated level of acceptable quantitation The MRL is sample-specific and accounts for preparation weights and volumes dilutions and moisture content of soilsediments

TIC Tentatively Identified Compound - An analyte identified based on a match with the instrument softwares mass spectral library A calibration standard has not been analyzed to confirm the compounds identification or the estimated concentration reported

Page 4 of 12 C121501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported byJeffrey Hendel

SAMPLES INCLUDED IN THIS REPORT

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID

ACGMW 12

ACGMW 18

ACGMW25

GE1MW22D

GE1MW24D

GEIMW924D

GE1MW34D

USGS-02-02

Laboratory ID MD D Matrix

C12150I-0I

C121501-02

C121501-03

C12150I-04

C121501-05

C121501-06

C121501-07

C121501-08

6Q26

6Q27

6Q19

6Q22

6Q25

6Q28

6Q24

6Q23

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Groundwater

Date Collected

31412 09

31312 18

31312 16

31312 13

31312 14

31312 14

31312 12

31412 11

20

28

26

18

45

47

16

26

Page 3 of 12 C12I50I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater- Reported by Jeffrey Hendel

DATA QUALIFIER DEFINITIONS

U The analyte was not detected at or above the reporting limit

CLPO 1 Concentration reported is less than the lowest standard on calibration curve

CLPl 2 Difference between GC columns above method waming limit

J The identification of the analyte is acceptable the reported value is an estimate

ISlJ Presumptive evidence that analyte is present reported as a tentative identification wilh an estimated value

OM-2 Matrix Spike Recovery greater than method control limits

ACRONYMS AND ABBREVIATIONS

CAS Chemical Abstracts Service Note Anaiytes with no known CAS identifiers have been assigned codes beginning with E the EPA ID as assigned by the EPA Substance Registry System (wwwepagovsrs) or beginning with R4- a unique identifier assigned by the EPA Region 4 laboratory

MDL Method Detection Limit - The minimum concentration of a substance (an analyte) that can be measured and reported with a 99 confidence that the analyte concentration is greater than zero

MRL Minimum Reporting Limit - Analyte concentration that cortesponds to the lowest demonstrated level of acceptable quantitation The MRL is sample-specific and accounts for preparation weights and volumes dilutions and moisture content of soilsediments

TIC Tentatively Identified Compound - An analyte identified based on a match with the instrument softwares mass spectral library A calibration standard has not been analyzed to confirm the compounds identification or the estimated concentration reported

Page 4 of 12 C121501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater- Reported by Jeffrey Hendel

DATA QUALIFIER DEFINITIONS

U The analyte was not detected at or above the reporting limit

CLPO 1 Concentration reported is less than the lowest standard on calibration curve

CLPl 2 Difference between GC columns above method waming limit

J The identification of the analyte is acceptable the reported value is an estimate

ISlJ Presumptive evidence that analyte is present reported as a tentative identification wilh an estimated value

OM-2 Matrix Spike Recovery greater than method control limits

ACRONYMS AND ABBREVIATIONS

CAS Chemical Abstracts Service Note Anaiytes with no known CAS identifiers have been assigned codes beginning with E the EPA ID as assigned by the EPA Substance Registry System (wwwepagovsrs) or beginning with R4- a unique identifier assigned by the EPA Region 4 laboratory

MDL Method Detection Limit - The minimum concentration of a substance (an analyte) that can be measured and reported with a 99 confidence that the analyte concentration is greater than zero

MRL Minimum Reporting Limit - Analyte concentration that cortesponds to the lowest demonstrated level of acceptable quantitation The MRL is sample-specific and accounts for preparation weights and volumes dilutions and moisture content of soilsediments

TIC Tentatively Identified Compound - An analyte identified based on a match with the instrument softwares mass spectral library A calibration standard has not been analyzed to confirm the compounds identification or the estimated concentration reported

Page 4 of 12 C121501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater- Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID ACGMW12

Station ID ACGMW12

Date Collected 31412 920

Lab ID C12150I-01

Matrix Groundwater

MDNo

D No 6Q26 KAP

f4v Ntstiiher i deg t

ns-72-55-9

50-29-3

309-00-2

319-84-6

5103-71-9

319-85-7

3 I 9-X(i-X

60-57-1

959-)X-X

33213-65-9

1031-07-X

72-20-8

7421-93-4

53494-70-5

58-89-9

5566-34-7

76-44-X

1024-57-3

72-43-gt

8001-35-2

i-DDD(pp-DDl

44-DDE (pp-DDE)

44-DDT(pp-DD^

ldrin

alpha-BHC

alpha-Chlordane

beta-BHC

delta-BHC

Dieldrin

I ndosullan I (alpha)

Endosulfan 11 (beta)

Endosulfan Sulfate

Endrin

I ndnn aldehdi

Endrin ketone

gamma-BHC (L indani

gamma-Chlordane

I Icptachlor

Heptachlor epoxide

Mclhow thiol

Toxaphene

Page 5 of 12 C121501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID A C G M W 1 8

Stat ion ID A C G M W I 8

Lab ID C12I501-02

Matr ix Groundwater

MD No

D No 6Q27 K A P

Date Collected 3 I3 I2 1828

r4 bulltip-- Number Jiiplnirve Results Qualifiers - Units

bull bullbullbull-A amp m bull bull bull euro ^

MRL Prepiirvd Uiah-zetd Method bull - - bull - bull bull bull - bull bullbull - - m i

72-54-8

72-55-9

j|Sff^DDD (pp-DpD)

44-DDE(pp-DDE)

sipPZP^^^MpSin iP -^Tfp^p-k

bull j i i i i - pound O IOU

OIOU ugL

010 bullbull 317i2 3 2 3 ^ ^ ^ g t P SOMO 12 P

OIO 31712 32312 CLP SOMOI2 P

bull 11 -f1 - HtfJM -j v - fr

bdquolaquoltiirn )KriirAbdquo rtffwir^f- gts-bdquo=j

rr-pip - 31712K-ij323l^j6LPSOM0i2PJ

309-00- Aldrin 0050 U 31712 32312 CLP SOMOI2 P

31712 -Pi- 32312l-ClJP SOM012 P

I7I2 32312 CLPSOMOI 2 P

31712 32312 CLPSO|M6I2 P

31712 32312 CLPSOMOI2 P

31712 bull 32312 CLplsOMOliz P

32312 CLP SOMOI2 P

37i2j-b 32312dji^Si3M))r^

Page 6 of 12 C12150I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID ACGMW25

Station ID ACGMW25

Lab ID CI2I501-03

Mat r ix Groundwater

MD No

D No 6Q19 K A P

Date Collected 31312 1626

-=-raquo -gtr- bull -s-mdash-J-- bull raquoiraquoft^^amp- -bull -bull-

CASA^ bull Ap-gt ^ Z m p ^ A-ttiihber^ -bull A Antilvte bull^C^t^p bull

i A - -i - bull --i-^ii -

AmAfpA0mp-gtA A A Af(A - C r Ar^S^ A p^i0ii-- bull ^ H ^ iz- A f i ^ ReyultipoundQiiiilifiert~y-A-i Units-

bullbullT-vi AAP i-A cipiA pAp bull MRI bull Preparedbull 1nalvredAMetlttid - ^j C^

72-54-8 bull-bull

72-55-9

5 0 - 2 9 ^ ^

44-DDD (pp DDD)

44-DDE(pp-DDE)

4j4-DpT (pp-DDTTsn

309-00-2

PTramp4^ bull-bullilSJif^ s t A i bull

5103-71-9

O IOU

010 Ll

_0J_0_

0050 U

ral^1taiBHC7^- ^^^pFr

010 31712

010 31712

010 31712

32312 bull-CLP SOM0I2 P - -

32312 CLP SOMOI 2 P

32312 =CLP S6M01 2 P A

bull^^ bull Ji^^0050Dfeaii-lI V^s

0050 3I7I2 32312 CLPSOMOI2 P

bullbull 0d50 3 17 12 bull i - i -3 23^^Cl ^M0f^^H

alpha-Chlordane 0050 U ugL

3 1 - 8 5 ^ | -

319-86-8

eojsfEf^ 1mdashjiiA^^-^-j^

959-98-8

bull ^ W ^ B ^ yen ^ mdash - ^ bull bull-bulll^^^t^^^

laquobaaBHC bull bull bull A m ^

delm-BHC

pieltJnn bull u^

^ v i ^ laquo ^ mdash mdash mdash

Endosulfan 1 (alpha)

bull omom fimiaiiii

bull-mam 0050 31712 32312 CLPSOMOI2 P

tf0050^W^J1712Sfct323l2SiCURSOM0iaRivi- S-- bull_ fj L -di i- a 31si i-- l_ iFsigt bullbull- bulli ix- bull WMA

WI

Endosiilfari 11 (beta) -bull^SMSSM

0050 U bull- -s-S^Vl~

0050 U

bullbull~3|roTo7j

UgL

Endosulfan Sulfate

Endnni^r-^ti bullgt bullgtamp

OIO u

5_3494-70-5

58-89-9

5566-34-7

76-44-8

1024^57^3 bullv^iJafrS^ia

010-ii

^ f - igt Vv^it^gtoioiJ--- VV bull Endrin aldehyde 010 U

Endrinl^elone A -r

gamma-BHC (Lindane) 0050 I

gamma-cihlordane - -- bull - =fe 0050 U

Heptachlor 0050 Ll

31712 32312 CLPSOMOI2 P

VI7I2 bull bull- 323^poundCllSOM0ll2jEj

3I7I2 32312 CLPSOMOI2 P

31712 323l2(CL5SOM01-2P

3I7I2 32312 CLPSOMOI2 P T-~niTgilaquoijlaquo -^fsr-mdash^----mdash^ - bull^ 3l-712|iP32312iCLPSOM012 P-

jfjaHeptachlor epoxide bull P050 U

32312 CLP SOMOI 2 P

A i O i i n CtPSOM012P

31712 32312 CLP SOMOI 2 P

31712 32312 CLPSOM012P

31712 32312 CLPSOMOI2 P bullbulljmm^w

0 bullir317i2lv323l2ampCL|SOMdlgtai^iii ---i^^- ii i mssM^fiampJjMi^Mk

72-43-5

800135^2t

Methoxychlor 0 50 11 ugL 050 31712 32312 CLPSOMOI2 P

iampD0J317iaai3237l2lfebRSOM01l2Prf- E^^ - bullbull bull|=gr^F^^K^r^^ferl^bull^^^bullafcrgt-A^^^bull^bullbullbull i -r^^^^i-^l ^ -bull

Page 7 of 12 CI2150I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater- Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID GEIMW22D

Station ID GEIMW22D

Date Collected 31312 1318

Lab ID C121S01-04

Matrix Groundwater

MDNo

D No 6Q22 KAP

Dttjhei Results tAuitiifieis (HK bullIf irepiired tmih-zed IferitDif

72-S4-8

72-55-9

50-29-3-

309-OII-2

319-84-6

5103-71-9

319-85-7

319-86-8

60-57-1

959-9X-X

33213-65-9

I (C1-07-8

72-20-8

7421-93-4

53494-70-5

58-X9-9

5566-34-7

76-44-X

1024-57-3

72-43-5

8001-35-2

44-DDU(pp-DDD)

4 4-DDL (pp-DDI )

44-DDT (pp-DrgtT)

Aldrin

alpha-BHC

alpha-Chlordane

beta-BHC

delta-BHC

Dicldrt

I ndosullan I (alpha)

Endosulfan II (beta)

r ndosullan Sultate

Endnn

Endrin aldehyde

Endrin ketone

janinia-l| K (I indane)

gamma-Chlordane

lloplachlor

Heptachlor epoxide

Mithochlor

Toxaphene

0031 NJ CLPOI

CLP 12

ugL

010

0 10

010

0050

0050

01150

0 050

0050

0 10

00^0

OfO

010

OfO

OH)

010

0 050

0 050

0 050

0 050

050

50

31712

-vl712

31712

bull - 2

3111 n

5 r 12

31712

31712

317I2

5 17 12

31712

r 12

31712

- r 12

31712

31712

31712

-- 17 12

31712

31712

31712

32312

-2312

32312

- 2-- 12

32312

-- 2- 12

-32312

32312

32312

--2-12

32312

-bullbull2-12

32312

-v23 12

-32312

-bull2M2

32312

V2V12

32312

3 2 3 1 2

32312

C l P S O M 0 L 2 P

Cl PSOMdl 2 P

CLPSOMOI 2 P

( I PSOMdl 2 P

CLP SOMO 12 P

CIPSOMdl 2 P

CLP SOMO 12 P

CLP SOMOI2 P

CLP SOMOI 2 P

( 1 PSOMdl 2 P

CLP SOMO 12 P

CLPSOMOI 2 P

CLP SOV101-2 P

Cl PSOMdl 2 P

CLP SOMO 12 P

(1 PSOMdl2 P

CLP SOMO 12 P

Cl PSOMdl 2 P

CLPSOM012P

Cl PSOMdl 2 P

C L P S O M 0 I 2 P

Page 8 of 12 C121501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175 Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID GEIMW24D

Station ID GEIMW24D

Date Collected 31312 1445

Lab ID C121501-05

Matrix Groundwater

MDNo D No 6Q25 KAP

i t f i l iv t i Results Qualifiers Units MHI Preptiral Imilr-ed Slelhud

bull72-54-8

72-35-9

50-29-3

309-OO-2

319-84-6

5103-71-9

319-85-7

314-X6-X

60-57-1

959-98-8

S213-65-9

1031-07-8

72-20-8

7421-93-4

53494-70-5

58-X9-4

5566-34-7

76-44-X

1024-57-3

72-43-5

SM^35-2

44-DDD (pp-D0D)

44-DDF(pp-DDH)

44-DDT (pp-DD

Aldrin

alpha-BHC

alpha-Chlordane

beta-BHC

delta-BHC

Dteli

[ ndosulfan I (alpha

Endosulfan II (betaj

Endosulfan Sulfate

Endrin

lndrin aldehyde

Endrin ketoi

gamma-BHC (Lindane

gamma-Chlordane

Heptachlor

Heptachlor epoxide

Methoxychlor

Toxaphene

32412 CLPSOMOI2 P

12 I I PSOMdl 2 P

324l2 CLPSOMOI 2 P

CLPSOMOI 2 P

32412 CLPSOMOI2 P

5 24 12 (1 PSOMOl 2 P

32412 C L P S O M 0 I 2 P

CLPSOMOI 2 P

CLPSOMOI2 P

CLPSOMOI 2 P

CLPSOMOI 2 P

CLPSOMOI 2 P

CLP SOMOI 2 P

Cl PSOMOl 2 P

CLP SOMOI 2 P

CLPSOMOI 2 P

PSOM012P

CLPSOMOI 2 P

CLP SOM012 P

Cl PSOMOl 2 P

CLP SOMOI 2 P

Page 9 of 12 Ct2150I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID G E I M W 9 2 4 D

Stat ion I D G E I M W 2 4 D

Lab ID C121S01-06

M a t r i x Groundwater

M D N o

D No 6 0 2 8 K A P

Date Collected 31312 1447

laquo laquo amp f Imllte Results (htaiifiers Units MKI- Pi-epilrcd Analyzed Melhtnl

72-54-8 --Ai bullvV a^^ A-

-44-DDD (pp-DDD)

44-DDf (pp-UDI )

44-DDT (pp-DD

ldrin

alpha-BHC

alpha-C hlordanc

beta-BHC

dellJ-BHC

Dieldntt

Liidosultan I (alpha)

Endosulfan II (beta)ii

Endosulfan Sulfate

Endrin

lindrin aldehyde

Endrin ketone

gamma-BHC 11indane

gamma-Chlordane

Heptachlor

Heptachlor epoxide

Methowehlor

Toxaphene

CLP SOMO 12 P

Cl PSOMOl 2 P

CLPSOM0L2P

Cl P SOMOI 2 P

CLPSOMOI2P

Cl PSOMOl 2 P

CLP SOMO 12

CLPSOMOI 2 P

CLP SOM012 P

ClPSOMdl

CLPSOMOI

Cl PSOMOl

CLPSOMOI

ClPSOMdl

CLP SOMOI

CLPSOMOI

2 P

2 P

2P

2P

2 P

32312 CLPSOM012P

- 21 12 Cl PSOMdl 2 P

32312 CLPSOM012li

CLPSOMOI 2 P

31712 32312 ClPSOM0i2P

Page 10 of 12 CI2I501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID ACGMW25

Station ID ACGMW25

Lab ID CI2I501-03

Mat r ix Groundwater

MD No

D No 6Q19 K A P

Date Collected 31312 1626

-=-raquo -gtr- bull -s-mdash-J-- bull raquoiraquoft^^amp- -bull -bull-

CASA^ bull Ap-gt ^ Z m p ^ A-ttiihber^ -bull A Antilvte bull^C^t^p bull

i A - -i - bull --i-^ii -

AmAfpA0mp-gtA A A Af(A - C r Ar^S^ A p^i0ii-- bull ^ H ^ iz- A f i ^ ReyultipoundQiiiilifiert~y-A-i Units-

bullbullT-vi AAP i-A cipiA pAp bull MRI bull Preparedbull 1nalvredAMetlttid - ^j C^

72-54-8 bull-bull

72-55-9

5 0 - 2 9 ^ ^

44-DDD (pp DDD)

44-DDE(pp-DDE)

4j4-DpT (pp-DDTTsn

309-00-2

PTramp4^ bull-bullilSJif^ s t A i bull

5103-71-9

O IOU

010 Ll

_0J_0_

0050 U

ral^1taiBHC7^- ^^^pFr

010 31712

010 31712

010 31712

32312 bull-CLP SOM0I2 P - -

32312 CLP SOMOI 2 P

32312 =CLP S6M01 2 P A

bull^^ bull Ji^^0050Dfeaii-lI V^s

0050 3I7I2 32312 CLPSOMOI2 P

bullbull 0d50 3 17 12 bull i - i -3 23^^Cl ^M0f^^H

alpha-Chlordane 0050 U ugL

3 1 - 8 5 ^ | -

319-86-8

eojsfEf^ 1mdashjiiA^^-^-j^

959-98-8

bull ^ W ^ B ^ yen ^ mdash - ^ bull bull-bulll^^^t^^^

laquobaaBHC bull bull bull A m ^

delm-BHC

pieltJnn bull u^

^ v i ^ laquo ^ mdash mdash mdash

Endosulfan 1 (alpha)

bull omom fimiaiiii

bull-mam 0050 31712 32312 CLPSOMOI2 P

tf0050^W^J1712Sfct323l2SiCURSOM0iaRivi- S-- bull_ fj L -di i- a 31si i-- l_ iFsigt bullbull- bulli ix- bull WMA

WI

Endosiilfari 11 (beta) -bull^SMSSM

0050 U bull- -s-S^Vl~

0050 U

bullbull~3|roTo7j

UgL

Endosulfan Sulfate

Endnni^r-^ti bullgt bullgtamp

OIO u

5_3494-70-5

58-89-9

5566-34-7

76-44-8

1024^57^3 bullv^iJafrS^ia

010-ii

^ f - igt Vv^it^gtoioiJ--- VV bull Endrin aldehyde 010 U

Endrinl^elone A -r

gamma-BHC (Lindane) 0050 I

gamma-cihlordane - -- bull - =fe 0050 U

Heptachlor 0050 Ll

31712 32312 CLPSOMOI2 P

VI7I2 bull bull- 323^poundCllSOM0ll2jEj

3I7I2 32312 CLPSOMOI2 P

31712 323l2(CL5SOM01-2P

3I7I2 32312 CLPSOMOI2 P T-~niTgilaquoijlaquo -^fsr-mdash^----mdash^ - bull^ 3l-712|iP32312iCLPSOM012 P-

jfjaHeptachlor epoxide bull P050 U

32312 CLP SOMOI 2 P

A i O i i n CtPSOM012P

31712 32312 CLP SOMOI 2 P

31712 32312 CLPSOM012P

31712 32312 CLPSOMOI2 P bullbulljmm^w

0 bullir317i2lv323l2ampCL|SOMdlgtai^iii ---i^^- ii i mssM^fiampJjMi^Mk

72-43-5

800135^2t

Methoxychlor 0 50 11 ugL 050 31712 32312 CLPSOMOI2 P

iampD0J317iaai3237l2lfebRSOM01l2Prf- E^^ - bullbull bull|=gr^F^^K^r^^ferl^bull^^^bullafcrgt-A^^^bull^bullbullbull i -r^^^^i-^l ^ -bull

Page 7 of 12 CI2150I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater- Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID GEIMW22D

Station ID GEIMW22D

Date Collected 31312 1318

Lab ID C121S01-04

Matrix Groundwater

MDNo

D No 6Q22 KAP

Dttjhei Results tAuitiifieis (HK bullIf irepiired tmih-zed IferitDif

72-S4-8

72-55-9

50-29-3-

309-OII-2

319-84-6

5103-71-9

319-85-7

319-86-8

60-57-1

959-9X-X

33213-65-9

I (C1-07-8

72-20-8

7421-93-4

53494-70-5

58-X9-9

5566-34-7

76-44-X

1024-57-3

72-43-5

8001-35-2

44-DDU(pp-DDD)

4 4-DDL (pp-DDI )

44-DDT (pp-DrgtT)

Aldrin

alpha-BHC

alpha-Chlordane

beta-BHC

delta-BHC

Dicldrt

I ndosullan I (alpha)

Endosulfan II (beta)

r ndosullan Sultate

Endnn

Endrin aldehyde

Endrin ketone

janinia-l| K (I indane)

gamma-Chlordane

lloplachlor

Heptachlor epoxide

Mithochlor

Toxaphene

0031 NJ CLPOI

CLP 12

ugL

010

0 10

010

0050

0050

01150

0 050

0050

0 10

00^0

OfO

010

OfO

OH)

010

0 050

0 050

0 050

0 050

050

50

31712

-vl712

31712

bull - 2

3111 n

5 r 12

31712

31712

317I2

5 17 12

31712

r 12

31712

- r 12

31712

31712

31712

-- 17 12

31712

31712

31712

32312

-2312

32312

- 2-- 12

32312

-- 2- 12

-32312

32312

32312

--2-12

32312

-bullbull2-12

32312

-v23 12

-32312

-bull2M2

32312

V2V12

32312

3 2 3 1 2

32312

C l P S O M 0 L 2 P

Cl PSOMdl 2 P

CLPSOMOI 2 P

( I PSOMdl 2 P

CLP SOMO 12 P

CIPSOMdl 2 P

CLP SOMO 12 P

CLP SOMOI2 P

CLP SOMOI 2 P

( 1 PSOMdl 2 P

CLP SOMO 12 P

CLPSOMOI 2 P

CLP SOV101-2 P

Cl PSOMdl 2 P

CLP SOMO 12 P

(1 PSOMdl2 P

CLP SOMO 12 P

Cl PSOMdl 2 P

CLPSOM012P

Cl PSOMdl 2 P

C L P S O M 0 I 2 P

Page 8 of 12 C121501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175 Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID GEIMW24D

Station ID GEIMW24D

Date Collected 31312 1445

Lab ID C121501-05

Matrix Groundwater

MDNo D No 6Q25 KAP

i t f i l iv t i Results Qualifiers Units MHI Preptiral Imilr-ed Slelhud

bull72-54-8

72-35-9

50-29-3

309-OO-2

319-84-6

5103-71-9

319-85-7

314-X6-X

60-57-1

959-98-8

S213-65-9

1031-07-8

72-20-8

7421-93-4

53494-70-5

58-X9-4

5566-34-7

76-44-X

1024-57-3

72-43-5

SM^35-2

44-DDD (pp-D0D)

44-DDF(pp-DDH)

44-DDT (pp-DD

Aldrin

alpha-BHC

alpha-Chlordane

beta-BHC

delta-BHC

Dteli

[ ndosulfan I (alpha

Endosulfan II (betaj

Endosulfan Sulfate

Endrin

lndrin aldehyde

Endrin ketoi

gamma-BHC (Lindane

gamma-Chlordane

Heptachlor

Heptachlor epoxide

Methoxychlor

Toxaphene

32412 CLPSOMOI2 P

12 I I PSOMdl 2 P

324l2 CLPSOMOI 2 P

CLPSOMOI 2 P

32412 CLPSOMOI2 P

5 24 12 (1 PSOMOl 2 P

32412 C L P S O M 0 I 2 P

CLPSOMOI 2 P

CLPSOMOI2 P

CLPSOMOI 2 P

CLPSOMOI 2 P

CLPSOMOI 2 P

CLP SOMOI 2 P

Cl PSOMOl 2 P

CLP SOMOI 2 P

CLPSOMOI 2 P

PSOM012P

CLPSOMOI 2 P

CLP SOM012 P

Cl PSOMOl 2 P

CLP SOMOI 2 P

Page 9 of 12 Ct2150I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID G E I M W 9 2 4 D

Stat ion I D G E I M W 2 4 D

Lab ID C121S01-06

M a t r i x Groundwater

M D N o

D No 6 0 2 8 K A P

Date Collected 31312 1447

laquo laquo amp f Imllte Results (htaiifiers Units MKI- Pi-epilrcd Analyzed Melhtnl

72-54-8 --Ai bullvV a^^ A-

-44-DDD (pp-DDD)

44-DDf (pp-UDI )

44-DDT (pp-DD

ldrin

alpha-BHC

alpha-C hlordanc

beta-BHC

dellJ-BHC

Dieldntt

Liidosultan I (alpha)

Endosulfan II (beta)ii

Endosulfan Sulfate

Endrin

lindrin aldehyde

Endrin ketone

gamma-BHC 11indane

gamma-Chlordane

Heptachlor

Heptachlor epoxide

Methowehlor

Toxaphene

CLP SOMO 12 P

Cl PSOMOl 2 P

CLPSOM0L2P

Cl P SOMOI 2 P

CLPSOMOI2P

Cl PSOMOl 2 P

CLP SOMO 12

CLPSOMOI 2 P

CLP SOM012 P

ClPSOMdl

CLPSOMOI

Cl PSOMOl

CLPSOMOI

ClPSOMdl

CLP SOMOI

CLPSOMOI

2 P

2 P

2P

2P

2 P

32312 CLPSOM012P

- 21 12 Cl PSOMdl 2 P

32312 CLPSOM012li

CLPSOMOI 2 P

31712 32312 ClPSOM0i2P

Page 10 of 12 CI2I501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater- Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID GEIMW22D

Station ID GEIMW22D

Date Collected 31312 1318

Lab ID C121S01-04

Matrix Groundwater

MDNo

D No 6Q22 KAP

Dttjhei Results tAuitiifieis (HK bullIf irepiired tmih-zed IferitDif

72-S4-8

72-55-9

50-29-3-

309-OII-2

319-84-6

5103-71-9

319-85-7

319-86-8

60-57-1

959-9X-X

33213-65-9

I (C1-07-8

72-20-8

7421-93-4

53494-70-5

58-X9-9

5566-34-7

76-44-X

1024-57-3

72-43-5

8001-35-2

44-DDU(pp-DDD)

4 4-DDL (pp-DDI )

44-DDT (pp-DrgtT)

Aldrin

alpha-BHC

alpha-Chlordane

beta-BHC

delta-BHC

Dicldrt

I ndosullan I (alpha)

Endosulfan II (beta)

r ndosullan Sultate

Endnn

Endrin aldehyde

Endrin ketone

janinia-l| K (I indane)

gamma-Chlordane

lloplachlor

Heptachlor epoxide

Mithochlor

Toxaphene

0031 NJ CLPOI

CLP 12

ugL

010

0 10

010

0050

0050

01150

0 050

0050

0 10

00^0

OfO

010

OfO

OH)

010

0 050

0 050

0 050

0 050

050

50

31712

-vl712

31712

bull - 2

3111 n

5 r 12

31712

31712

317I2

5 17 12

31712

r 12

31712

- r 12

31712

31712

31712

-- 17 12

31712

31712

31712

32312

-2312

32312

- 2-- 12

32312

-- 2- 12

-32312

32312

32312

--2-12

32312

-bullbull2-12

32312

-v23 12

-32312

-bull2M2

32312

V2V12

32312

3 2 3 1 2

32312

C l P S O M 0 L 2 P

Cl PSOMdl 2 P

CLPSOMOI 2 P

( I PSOMdl 2 P

CLP SOMO 12 P

CIPSOMdl 2 P

CLP SOMO 12 P

CLP SOMOI2 P

CLP SOMOI 2 P

( 1 PSOMdl 2 P

CLP SOMO 12 P

CLPSOMOI 2 P

CLP SOV101-2 P

Cl PSOMdl 2 P

CLP SOMO 12 P

(1 PSOMdl2 P

CLP SOMO 12 P

Cl PSOMdl 2 P

CLPSOM012P

Cl PSOMdl 2 P

C L P S O M 0 I 2 P

Page 8 of 12 C121501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175 Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID GEIMW24D

Station ID GEIMW24D

Date Collected 31312 1445

Lab ID C121501-05

Matrix Groundwater

MDNo D No 6Q25 KAP

i t f i l iv t i Results Qualifiers Units MHI Preptiral Imilr-ed Slelhud

bull72-54-8

72-35-9

50-29-3

309-OO-2

319-84-6

5103-71-9

319-85-7

314-X6-X

60-57-1

959-98-8

S213-65-9

1031-07-8

72-20-8

7421-93-4

53494-70-5

58-X9-4

5566-34-7

76-44-X

1024-57-3

72-43-5

SM^35-2

44-DDD (pp-D0D)

44-DDF(pp-DDH)

44-DDT (pp-DD

Aldrin

alpha-BHC

alpha-Chlordane

beta-BHC

delta-BHC

Dteli

[ ndosulfan I (alpha

Endosulfan II (betaj

Endosulfan Sulfate

Endrin

lndrin aldehyde

Endrin ketoi

gamma-BHC (Lindane

gamma-Chlordane

Heptachlor

Heptachlor epoxide

Methoxychlor

Toxaphene

32412 CLPSOMOI2 P

12 I I PSOMdl 2 P

324l2 CLPSOMOI 2 P

CLPSOMOI 2 P

32412 CLPSOMOI2 P

5 24 12 (1 PSOMOl 2 P

32412 C L P S O M 0 I 2 P

CLPSOMOI 2 P

CLPSOMOI2 P

CLPSOMOI 2 P

CLPSOMOI 2 P

CLPSOMOI 2 P

CLP SOMOI 2 P

Cl PSOMOl 2 P

CLP SOMOI 2 P

CLPSOMOI 2 P

PSOM012P

CLPSOMOI 2 P

CLP SOM012 P

Cl PSOMOl 2 P

CLP SOMOI 2 P

Page 9 of 12 Ct2150I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID G E I M W 9 2 4 D

Stat ion I D G E I M W 2 4 D

Lab ID C121S01-06

M a t r i x Groundwater

M D N o

D No 6 0 2 8 K A P

Date Collected 31312 1447

laquo laquo amp f Imllte Results (htaiifiers Units MKI- Pi-epilrcd Analyzed Melhtnl

72-54-8 --Ai bullvV a^^ A-

-44-DDD (pp-DDD)

44-DDf (pp-UDI )

44-DDT (pp-DD

ldrin

alpha-BHC

alpha-C hlordanc

beta-BHC

dellJ-BHC

Dieldntt

Liidosultan I (alpha)

Endosulfan II (beta)ii

Endosulfan Sulfate

Endrin

lindrin aldehyde

Endrin ketone

gamma-BHC 11indane

gamma-Chlordane

Heptachlor

Heptachlor epoxide

Methowehlor

Toxaphene

CLP SOMO 12 P

Cl PSOMOl 2 P

CLPSOM0L2P

Cl P SOMOI 2 P

CLPSOMOI2P

Cl PSOMOl 2 P

CLP SOMO 12

CLPSOMOI 2 P

CLP SOM012 P

ClPSOMdl

CLPSOMOI

Cl PSOMOl

CLPSOMOI

ClPSOMdl

CLP SOMOI

CLPSOMOI

2 P

2 P

2P

2P

2 P

32312 CLPSOM012P

- 21 12 Cl PSOMdl 2 P

32312 CLPSOM012li

CLPSOMOI 2 P

31712 32312 ClPSOM0i2P

Page 10 of 12 CI2I501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175 Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID GEIMW24D

Station ID GEIMW24D

Date Collected 31312 1445

Lab ID C121501-05

Matrix Groundwater

MDNo D No 6Q25 KAP

i t f i l iv t i Results Qualifiers Units MHI Preptiral Imilr-ed Slelhud

bull72-54-8

72-35-9

50-29-3

309-OO-2

319-84-6

5103-71-9

319-85-7

314-X6-X

60-57-1

959-98-8

S213-65-9

1031-07-8

72-20-8

7421-93-4

53494-70-5

58-X9-4

5566-34-7

76-44-X

1024-57-3

72-43-5

SM^35-2

44-DDD (pp-D0D)

44-DDF(pp-DDH)

44-DDT (pp-DD

Aldrin

alpha-BHC

alpha-Chlordane

beta-BHC

delta-BHC

Dteli

[ ndosulfan I (alpha

Endosulfan II (betaj

Endosulfan Sulfate

Endrin

lndrin aldehyde

Endrin ketoi

gamma-BHC (Lindane

gamma-Chlordane

Heptachlor

Heptachlor epoxide

Methoxychlor

Toxaphene

32412 CLPSOMOI2 P

12 I I PSOMdl 2 P

324l2 CLPSOMOI 2 P

CLPSOMOI 2 P

32412 CLPSOMOI2 P

5 24 12 (1 PSOMOl 2 P

32412 C L P S O M 0 I 2 P

CLPSOMOI 2 P

CLPSOMOI2 P

CLPSOMOI 2 P

CLPSOMOI 2 P

CLPSOMOI 2 P

CLP SOMOI 2 P

Cl PSOMOl 2 P

CLP SOMOI 2 P

CLPSOMOI 2 P

PSOM012P

CLPSOMOI 2 P

CLP SOM012 P

Cl PSOMOl 2 P

CLP SOMOI 2 P

Page 9 of 12 Ct2150I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID G E I M W 9 2 4 D

Stat ion I D G E I M W 2 4 D

Lab ID C121S01-06

M a t r i x Groundwater

M D N o

D No 6 0 2 8 K A P

Date Collected 31312 1447

laquo laquo amp f Imllte Results (htaiifiers Units MKI- Pi-epilrcd Analyzed Melhtnl

72-54-8 --Ai bullvV a^^ A-

-44-DDD (pp-DDD)

44-DDf (pp-UDI )

44-DDT (pp-DD

ldrin

alpha-BHC

alpha-C hlordanc

beta-BHC

dellJ-BHC

Dieldntt

Liidosultan I (alpha)

Endosulfan II (beta)ii

Endosulfan Sulfate

Endrin

lindrin aldehyde

Endrin ketone

gamma-BHC 11indane

gamma-Chlordane

Heptachlor

Heptachlor epoxide

Methowehlor

Toxaphene

CLP SOMO 12 P

Cl PSOMOl 2 P

CLPSOM0L2P

Cl P SOMOI 2 P

CLPSOMOI2P

Cl PSOMOl 2 P

CLP SOMO 12

CLPSOMOI 2 P

CLP SOM012 P

ClPSOMdl

CLPSOMOI

Cl PSOMOl

CLPSOMOI

ClPSOMdl

CLP SOMOI

CLPSOMOI

2 P

2 P

2P

2P

2 P

32312 CLPSOM012P

- 21 12 Cl PSOMdl 2 P

32312 CLPSOM012li

CLPSOMOI 2 P

31712 32312 ClPSOM0i2P

Page 10 of 12 CI2I501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID G E I M W 9 2 4 D

Stat ion I D G E I M W 2 4 D

Lab ID C121S01-06

M a t r i x Groundwater

M D N o

D No 6 0 2 8 K A P

Date Collected 31312 1447

laquo laquo amp f Imllte Results (htaiifiers Units MKI- Pi-epilrcd Analyzed Melhtnl

72-54-8 --Ai bullvV a^^ A-

-44-DDD (pp-DDD)

44-DDf (pp-UDI )

44-DDT (pp-DD

ldrin

alpha-BHC

alpha-C hlordanc

beta-BHC

dellJ-BHC

Dieldntt

Liidosultan I (alpha)

Endosulfan II (beta)ii

Endosulfan Sulfate

Endrin

lindrin aldehyde

Endrin ketone

gamma-BHC 11indane

gamma-Chlordane

Heptachlor

Heptachlor epoxide

Methowehlor

Toxaphene

CLP SOMO 12 P

Cl PSOMOl 2 P

CLPSOM0L2P

Cl P SOMOI 2 P

CLPSOMOI2P

Cl PSOMOl 2 P

CLP SOMO 12

CLPSOMOI 2 P

CLP SOM012 P

ClPSOMdl

CLPSOMOI

Cl PSOMOl

CLPSOMOI

ClPSOMdl

CLP SOMOI

CLPSOMOI

2 P

2 P

2P

2P

2 P

32312 CLPSOM012P

- 21 12 Cl PSOMdl 2 P

32312 CLPSOM012li

CLPSOMOI 2 P

31712 32312 ClPSOM0i2P

Page 10 of 12 CI2I501 OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID G E I M W 3 4 D

Stat ion ID G E I M W 3 4 D

Lab ID CI2IS01-07

Matr ix Groundwater

M D N o

D No 6Q24 KAP

Date Collected 31312 1216

C4V K ^ bull bull - - 5 -If v IT ^ = --

Nuniber bull-f^kf Analyte Resulls^Qiitiliflcrs - Unityi MRL Prepared

X- bullbull bullbullbull- 1 vlaquo-iK^yen bull - bull r -v-lt4f gtiift-laquogtrf Meiliod bull S J

72-54-8 bull^PP^P 44DDDrpp-DDD)

72-55-9 44-DDE(pp-DDE)

5 0 - 2 ^ Z A 4 4 - D D T (ppVpDT)

010ll-

010 u

309-00- Aldrin

oioVr 0050 U

ug^L

ugL

ugL

319-8456^2 -^-alpha-BHC 0050 XJ^yAA^l^i -bdquo-7^r^^n--w^

gtugKr

OIO 31712

0 10 31712

OIO 31712

0050 31712

0050 bull bull 3177l2

5103-71-9 alpha-Chlordane

i w- w i vyijs r -rmdash - j ^ 1 31985|7^--Sbeta-BHeraquo bully-A -i-~--i- lt m- iSmMi-tMiAir f- Viini Asajiijipoundi^ix^

0050 U ugL 0050 3I7I2

32312

32312

32312

32312

32312

32312

32312-

CLP^pM012Pflt^

CLPSOMOI 2 P

CLPSOMOI 2P5y

CLP SOMO 12 P

CIPS0M()L2PS l^nSbdquofnrfi r ^^i i - ^ ^ J ^

CLP SOMO 12 P

V L P SOMO A - ^ ^ t A Akuiif- bull i r i ^ i U -

319-86-8 delta-BHC 0050 U ugL 0050

60 S7MraquoSgtSfe-Dieldrin^- bull A -amp- 2MMmM^^^M^ZMZimzm 959-98-8 Endosulfan 1 (alpha)

Endosulfan U(beta)

0050 U ugL 0050

Endosulfan Sulfate

---bullbullbull i W^ |a i^ - - - -Endnn bulllifi-kfi-U -m AlMiSiMi Endrin aldehyde

pm Endrin ketone

i^-^pASM 010 U

- bull i

- iftMB-iiiHii bull OIOU ugL

oio 010

- bull ^ - bull ^ ^

oio OIO

010

vi31712

f-31712laquos

3I7I2 - ^ ^ - r s - 3i712|S

58-89-9 gamma-BHC (Lindane) 0050 U ugL 0050 3I7I2

76-44-8

i ^ mdash T - ^ - - - - - C shyLi gaiiiihsffinlbrdane ^ ^

Heptachlor - I f

t0050 U 0050 31-712

--^^^^|g^-V-IJg^ 1024-^5731 Heptachlor epoxide ^-gf

0050 U

i |7H4oo5b u^

ugL

tbdquo-ugrt^^ r-Rmnfltbdquogt^^ihMrf

0 050

^^^0050 V- 31712 =-bull

72-43-5 Methox-ychlor 050 U ugL 050 V17I2 bull I iVf l^ l i j ^ bullJL^^wa--

50 U -A frsrjsrr lti^UgL bullbull-bullbull bullAXVX-H

bullAAXMP-bullgt^=^-T S^31712L

32312

32312J

32312

32312

32312

32312

32312

32312

32312

32312

32312

323i2

32312

32312

CLPSOMOI 2 P

iiCLPSOMOlaitj^K

CLP SOMO 12 P

CLPSOMOLIK^JV-^

CLP SOMO 12 P l l bull bull - bull ^ ^ bull bull bull w - K - J V -pCLP SOMO -gtgtbullbullbull l i i bull 3mdashiiSli^iS

CLP SOMO 12 P

bull |GDRsoMpr2gf|^i -assi i laquoSi

CLP SOMO 12 P

bullCL-fSOMoi2iraquo^

CLPSOMOI 2 P

(2LRSOM012PBS -gt-tJ bdquobull-bull-j^bdquo -ffl i)ife-i

CLP SOMO 12 P T--mdashmdashir-^mdash^bulltfjrj y -CLPSOM0i2gtHtlaquo bull - = =^-ti - V -

Page II of 12 C12I50 I OCP FINAL 42712 816

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division

980 College Station Road Athens Georgia 30605-2700

DART Id 12-0175

Project 12-0297 Aberdeen Groundwater - Reported by Jeffrey Hendel

Organochlorine Pesticides

Project 12-0297 Aberdeen Groundwater Contract Lab Case 42313

Sample ID USGS-02-02

Station ID USGS-02-02

Lab ID C12I501-08

Matr ix Groundwater

M D No

D No 6Q23 K P

Date Collected 31412 1126

C4V -

Number AnuMA^

-i-w^-f^^^-r - bullbullAA0Ap-A-^A A-i x RpfuitpQuittifters

h bull bull bull

U n i t t

-=bull--bull ~A bullbull S - f -aiP - -i bull - bull- bull bull Air A

MRL Prepared Aiialvzcd Method ^ J t

72-54-8 44-DDb (pp-DDD)

72-55-9 44-DDE(pp-DDE)

50-29-3 44-DpT (pp-DDT)

309-00-2 Aldrin

319-84-6 - aiphi^BMc

bull A A A i ^ bull

-

OIOU

OIO IJ

OIO U

---ugL-

ugL

0 1 0 - -31712

0 1 0 31712

0050 ll

AppA- ^A010gt3i712

0 0 5 0 31712 ugL

U g L - J ^ M bull 005Pi~-317l2

32312 CLP SOMOI2 P

32312 CLPSOMOI 2 P

32312 CLP SOMOI2 P

32312 CLP SOMOI 2 P

32312-- CLPSOM0l 2P r J

5103-71-9 a lpha-Chlordane 0050 II ugL 0050 32312 CLP SOMOI2 P

319-857-gtgt^gtbeta-BHei - - bull - - ^ A lt j i M i P^^^^^ioPp bull liSlimrygtT( r- mdash-mdash- rrmdashbullvsri-Jjiiiy iCLPSOM012Plt-f- an- Ti- fc--ar(iauiat

319-86-8 de l t a -BHC 0050 U ugL 0050 31712

bull32312-

32312 CLPSOMOI 2 P

6p57jlVpiCj^pieldrin -bull bull A^)AAApK- bull-^iflPiPM^A _j_i i i i a i i i s^atrade_

959-98-8 Endosulfan 1 (alpha)

33213^5^JV^ Endosulfkn 11 (beta)

1031-07-1

^2^20^8^

7421-93-4

S3494r7C

58-89-9

TmZ 76-44-8

Endosulfan Sulfate

_Endrin bull

Endrin a ldehyde

Endrin ke tone

g a m m a - B H C (Lindane)

Heptachlor

0050 Ll

010 U

ugL 0 0 5 0 31712

CLPSOM0L2 P- -

0050 U

i SlSi^ iMiSBK 0050 U CLPSOMOI

1024T5 7-3-i- -f v- Heptachlor eplt5xidei-j tajn-si-raquo-i-- s -ifaai^a^i

7- gssMJ - - - bull - -^ i i

fejetvt^0050iP-ffal^^r^ifi-j^iraquo^^iaiiii

5^--l^r ^ gtcuiglS^^igtSt)050| Sl7l2gt - ~ibdquobdquofivieraquo^abdquojjiSlaquo^ -^a

-32312 CLPSOM01-2PgtTr --J- -raquo^jVfi-i

72-43-5 Methoxychlor

800K352bull^bull bull - Toxaphenealaquoa||Kjr--^

050 U ugL 050 31712 32312

copyampbullbull bullbull5Ql|J3-^ ugL 50 bull 31712 bull bullbull32312 bull

CLPSOMOI 2 P

C L P S O M 0 1 2 P ^ ^

Page 12 of 12 CI2I50I OCP FINAL 42712 816