Material Testing Report MAT9855 VESTAKEEP 3300 G High Purity · Material Testing Report MAT9855...
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Material Testing Report MAT9855 VESTAKEEP 3300 G High Purity Prepared for: Evonik Resource Efficiency GmbH Baul-Baumann-Straße 1 Marl, 45768 Germany Prepared by: Beaumont Advanced Processing 6100 West Ridge Rd Erie, PA 16506 USA Prepared on: 28 May, 2020
Transcript of Material Testing Report MAT9855 VESTAKEEP 3300 G High Purity · Material Testing Report MAT9855...
Material Testing Report
MAT9855
VESTAKEEP 3300 G High Purity
Prepared for:
Evonik Resource Efficiency GmbH
Baul-Baumann-Straße 1
Marl, 45768
Germany
Prepared by:
Beaumont Advanced Processing
6100 West Ridge Rd
Erie, PA 16506
USA
Prepared on:
28 May, 2020
Report Created By:
David Schmidt
Materials Lab Engineer
28 May, 2020
© Beaumont Advanced Processing 2020. This report may not be reproduced.
Test results relate only to the item tested. Autodesk disclaims all warranties express or implied, including warranties of merchantability and fitness for a particular purpose. Beaumont Advanced Processing expressly disclaims all incidental and consequential damages that may arise from the use of this information.
Contents
Summary .............................................................................................................................. 4
Viscosity ............................................................................................................................. 10
Thermal conductivity ......................................................................................................... 16
Specific heat ....................................................................................................................... 18
Pressure-Volume-Temperature ......................................................................................... 20
Shrinkage ............................................................................................................................ 23
Mechanical ......................................................................................................................... 29
Elastic modulus and Poisson's ratio .............................................................................. 29
Shear modulus ............................................................................................................... 30
Nonlinear Mechanical Model ........................................................................................ 31
Coefficient of linear thermal expansion ........................................................................ 33
Mold verification ................................................................................................................ 34
Contact details ................................................................................................................... 37
mat9855 Summary
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Summary
Description
Family name KETONE-BASED RESINS (PEEK, PAEK, ...)
Trade name VESTAKEEP 3300 G High Purity
Manufacturer EVONIK Resource Efficiency GmbH
Family abbreviation PEEK
Material structure Crystalline
Data source Beaumont Advanced Processing : pvT-Measured : mech-Measured
Date last modified 28-MAY-20
Date tested 28-MAY-20
Data status Non-Confidential
Material ID 60855
Grade code mat9855
Supplier code EVONIKRE
Fibers/fillers Unfilled
Recommended Processing
Mold surface temperature 180.00 °C
Melt temperature 380.00 °C
Mold temperature range (recommended)
Minimum 160.00 °C
Maximum 200.00 °C
Melt temperature range (recommended)
Minimum 360.00 °C
Maximum 400.00 °C
Absolute maximum melt temperature 420.00 °C
Ejection temperature 261.00 °C
Maximum shear stress 0.50 MPa
Maximum shear rate 50000 1/s
Maximum shear stress and maximum shear rate values have been supplemented with generic estimates.
mat9855 Summary
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Rheological Properties
Cross WLF Viscosity Model
n 0.36027
Tau 4.43678e+005 Pa
D1 4.05976e+009 Pa-s
D2 403.15 K
D3 0 K/Pa
A1 18.244
A2 51.600 K
Juncture loss method coefficients
C1 0.00124 Pa^(1-c2)
C2 1.5
Transition temperature
Ttrans 281.00 °C
Moldflow Viscosity Index VI(380)394
mat9855 Summary
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Thermal Properties
Specific heat data
Temperature (T)
°C
Specific heat (Cp)
J/kg-°C
Heating/Cooling rate
°C/s
380.5 2677.4 -0.33
296.95 2525.9 -0.33
287.67 2511.8 -0.33
283.55 2628.1 -0.33
279.49 3398.2 -0.33
274.6 5808.5 -0.33
272.73 6238.0 -0.33
270.6 5920.9 -0.33
266.32 4397.3 -0.33
262.04 3446.5 -0.33
257.83 2945.6 -0.33
251.59 2590.7 -0.33
237.12 2433.3 -0.33
160.76 2062.1 -0.33
139.08 1847.2 -0.33
30.746 1330.2 -0.33
Thermal conductivity data
Temperature (T)
°C
Thermal conductivity
(k) W/m-°C
Heating/Cooling rate
°C/s
395.00 0.355 0.0
345.00 0.324 0.0
315.00 0.311 0.0
295.00 0.310 0.0
255.00 0.309 0.0
245.00 0.309 0.0
215.00 0.312 0.0
185.00 0.313 0.0
155.00 0.317 0.0
125.00 0.315 0.0
95.00 0.309 0.0
65.00 0.299 0.0
mat9855 Summary
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PVT Properties
Melt density 1.0732 g/cm3
Solid density 1.3164 g/cm3
2-domain Tait PVT model coefficients
b5 623.75 K
b6 7.105e-008 K/Pa
b1m 0.000917 m3/kg
b2m 5.156e-007 m3/kg-K
b3m 8.41033e+007 Pa
b4m 0.004773 1/K
b1s 0.000827 m3/kg
b2s 2.055e-007 m3/kg-K
b3s 1.60456e+008 Pa
b4s 0.003991 1/K
b7 0.00009 m3/kg
b8 0.02527 1/K
b9 6.095e-009 1/Pa
mat9855 Summary
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Mechanical Properties
Mechanical properties data Elastic modulus, 1st principal direction [E1] 3707.71 MPa
Elastic modulus, 2nd principal direction [E2] 3686.63 MPa
Poisson's ratio [v12] 0.3750
Poisson's ratio [v23] 0.3750
Shear modulus [G12] 1355.30 MPa
Transversely isotropic coefficient of thermal expansion [CTE] data Alpha1 4.510e-005 1/°C
Alpha2 4.940e-005 1/°C
Nonlinear Mechanical property data
Sigma Zero 91.9772 MPa
N 3.63485
Alpha 1
Beta 1
Eig 0
Matrix Modulus 2967.82 MPa
Matrix Poisson’s Ratio 0.375
Fiber Modulus 0 MPa
Fiber Poisson’s Ratio 0
Maximum Von Mises matrix stress at failure 96.6508 MPa
A1 0 1/ MPa2
A2 0 1/ MPa2
A4 0 1/ MPa2
Temperature 23.0 C
Relative Humidity 50.0 %
Strain rate 0.000833 1/s
The nonlinear mechanical data are derived from RO Library Version 2.
mat9855 Summary
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Shrinkage Properties
Corrected residual in-mold stress (CRIMS) model coefficients A1 1.073392
A2 0.100348
A3 0.001269
A4 1.242376
A5 0.048838
A6 0.00133
Residual strain model coefficients Parallel Perpendicular
A1 0.066563 0.13618
A2 -0.005343 -0.004712
A3 0.000895 -0.000022
A4 -9.4037e-008 -1.1497e-008
A5 0.013479 0.011645
The shrinkage models shown above are valid for Autodesk Moldflow Insight 2018 Revision 2 and later. Shrinkage models for previous software versions are included in the 21000.udb file.
Filler Properties
Filler data Description Weight %
mat9855 Viscosity
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Viscosity
Method: AMPL Test Method
Instrument: Arburg Allrounder 270S Injection Molding Machine
Test Specifications: Sample Form: Pellets
Pre-Processing: Dried at 150°C for 3 hours in a hopper dryer
Moisture Level: 0.0103 %
Capillary A: Length: 31.9693 mm
L/D: 15.98465
Die Entry Angle: 90 degrees
Capillary B: Length: 7.9731 mm
L/D: 3.98655
Die Entry Angle: 90 degrees
Barrel Diameter: 30 mm
Plastication Time: 20 sec
Dwell Time: 20 sec
Corrections: Bagley, Rabinowitsch and shear heating
Date Received: 11-MAY-20
Date Tested: 12-MAY-20
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
mat9855 Viscosity
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Apparent Viscosity Data
Temperature
(°C)
Apparent Shear Rate
(sec-1)
Apparent Viscosity (Pa-s)
Die Diameter
(mm)
Die L/D (-)
367.7 201 766.12 2.00 15.99
367.7 320 684.80 2.00 15.99
368.8 771 491.94 2.00 15.99
369.7 1349 388.00 2.00 15.99
370.8 2601 281.94 2.00 15.99
372.8 3851 226.92 2.00 15.99
376.7 9014 155.02 2.00 15.99
377.8 200 732.39 2.00 15.99
377.8 319 609.27 2.00 15.99
378.1 15409 109.81 2.00 15.99
378.8 774 456.02 2.00 15.99
379.8 1349 368.29 2.00 15.99
380.8 2598 267.18 2.00 15.99
380.8 12798 119.16 2.00 15.99
383.8 6492 157.20 2.00 15.99
386.7 25636 72.27 2.00 15.99
387.8 196 648.93 2.00 15.99
387.8 321 547.50 2.00 15.99
388.7 778 418.77 2.00 15.99
389.3 12774 108.76 2.00 15.99
389.8 1354 343.09 2.00 15.99
390.7 2592 253.03 2.00 15.99
393.8 6491 148.91 2.00 15.99
395.8 38644 50.50 2.00 15.99
397.8 205 556.75 2.00 15.99
397.8 321 524.99 2.00 15.99
398.8 778 383.44 2.00 15.99
399.8 1352 314.15 2.00 15.99
400.3 12772 96.91 2.00 15.99
400.8 2593 236.91 2.00 15.99
403.8 6498 142.92 2.00 15.99
372.9 320 705.14 2.00 3.99
373.0 201 740.77 2.00 3.99
374.0 771 518.56 2.00 3.99
375.0 1349 412.88 2.00 3.99
380.0 2601 299.27 2.00 3.99
384.0 319 652.73 2.00 3.99
384.0 774 491.67 2.00 3.99
384.0 3851 241.38 2.00 3.99
385.0 200 768.96 2.00 3.99
386.0 1349 397.60 2.00 3.99
389.1 15409 101.39 2.00 3.99
389.5 12798 112.25 2.00 3.99
390.0 2598 287.69 2.00 3.99
mat9855 Viscosity
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Temperature
(°C)
Apparent Shear Rate
(sec-1)
Apparent Viscosity (Pa-s)
Die Diameter
(mm)
Die L/D (-)
394.0 321 586.98 2.00 3.99
395.0 196 664.60 2.00 3.99
395.0 778 454.15 2.00 3.99
396.0 1354 371.62 2.00 3.99
396.1 9014 144.79 2.00 3.99
398.5 12774 107.89 2.00 3.99
399.0 25636 80.41 2.00 3.99
400.0 2592 272.86 2.00 3.99
400.0 6492 170.64 2.00 3.99
406.0 321 571.61 2.00 3.99
406.0 778 414.78 2.00 3.99
407.0 205 574.14 2.00 3.99
407.0 1352 337.80 2.00 3.99
409.7 6491 162.93 2.00 3.99
410.2 38644 58.97 2.00 3.99
411.0 2593 253.77 2.00 3.99
413.4 12772 103.23 2.00 3.99
419.8 6498 155.55 2.00 3.99
mat9855 Viscosity
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Calculated Viscosity
Temperature
(°C)
Shear Rate (sec-1)
Calculated Viscosity
(Pa-s)
367.7 320 647.45
367.7 201 738.88
368.8 771 470.54
369.7 1349 369.29
370.8 2601 269.05
372.8 3851 217.82
372.9 320 622.07
373.0 201 707.85
374.0 771 454.40
375.0 1349 357.74
376.7 9014 134.53
377.8 200 682.54
377.8 319 600.43
378.1 15409 98.23
378.8 774 440.08
379.8 1349 347.76
380.0 2601 255.94
380.8 2598 255.03
380.8 12798 108.13
383.8 6492 156.21
384.0 319 573.85
384.0 774 425.76
384.0 3851 205.83
385.0 200 645.46
386.0 1349 335.51
386.7 25636 70.18
387.8 196 635.11
387.8 321 557.91
388.7 778 412.78
389.1 15409 93.80
389.3 12774 104.40
389.5 12798 104.19
389.8 1354 328.02
390.0 2598 243.25
390.7 2592 242.65
393.8 6491 149.42
394.0 321 534.40
395.0 778 397.63
395.0 196 602.28
395.8 38644 52.99
396.0 1354 317.01
396.1 9014 123.59
mat9855 Viscosity
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Temperature
(°C)
Shear Rate (sec-1)
Calculated Viscosity
(Pa-s)
397.8 321 520.78
397.8 205 584.56
398.5 12774 100.56
398.8 778 388.89
399.0 25636 66.93
399.8 1352 310.88
400.0 2592 231.91
400.0 6492 145.44
400.3 12772 99.88
400.8 2593 231.04
403.8 6498 143.09
406.0 321 493.57
406.0 778 373.17
407.0 205 548.46
407.0 1352 299.46
409.7 6491 139.78
410.2 38644 50.34
411.0 2593 220.36
413.4 12772 95.06
419.8 6498 134.29
mat9855 Viscosity
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Rheological Data
Cross WLF Viscosity Model
n 0.36027
Tau 4.43678e+005 Pa
D1 4.05976e+009 Pa-s
D2 403.15 K
D3 0 K/Pa
A1 18.244
A2 51.600 K
Juncture loss method coefficients
C1 0.00124 Pa^(1-c2)
C2 1.5
1.0E+0
1.0E+1
1.0E+2
1.0E+3
1.0E+4
1.0E+1 1.0E+2 1.0E+3 1.0E+4 1.0E+5
Vis
cosi
ty (
Pa-
s)
Shear rate (1/s)
Viscosity vs shear rate
T = 360 °C T = 380 °C T = 400 °C
mat9855 Thermal conductivity
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Thermal conductivity
Method: ISO 22007-2, Plastics - Determination of thermal conductivity and thermal diffusivity - Part 2: Transient plane heat source (hot disc) method
Instrument: Hot Disk TPS 2500 S Thermal Constants Analyser
Test Specifications: Sample Form: 19 mm disks (2) machined from molded plaque
Pre-Processing: N/A
Moisture Level: DAM (Dry As Molded)
Sensor Specification Hot Disk 5465 3.189mm Kapton sensor
Measurement Time 20 sec
Heating Power 55 mW
Date Received: 11-MAY-20
Date Tested: 18-MAY-20
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
mat9855 Thermal conductivity
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Thermal conductivity data
Temperature (T) °C
Thermal conductivity (k) W/m-°C
Heating/Cooling rate °C/s
395.00 0.355 0.0
345.00 0.324 0.0
315.00 0.311 0.0
295.00 0.310 0.0
255.00 0.309 0.0
245.00 0.309 0.0
215.00 0.312 0.0
185.00 0.313 0.0
155.00 0.317 0.0
125.00 0.315 0.0
95.00 0.309 0.0
65.00 0.299 0.0
0.00
0.05
0.10
0.15
0.20
0.25
0.30
0.35
0.40
0.45
0.50
0 50 100 150 200 250 300 350 400 450
The
rmal
co
nd
uct
ivit
y, k
(W
/m-°
C)
Temperature (°C)
Thermal conductivity vs temperature
mat9855 Specific heat
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Specific heat
Method: ASTM E 1269, Standard Test Method for Determining Specific Heat Capacity by Differential Scanning Calorimetry ASTM D 3418, Standard Test Method for Transition Temperatures and Enthalpies of Fusion and Crystallization of Polymers by Differential Scanning Calorimetry
Instrument: TA Instruments Discovery Differential Scanning Calorimeter
Test Specifications: Sample Form: Pellets
Pre-Processing: Dried at 150°C for 3 hours in a hopper dryer
Moisture Level: 0.0103 %
Initial Temperature: 400°C
Final Temperature: 20°C
Cooling Rate: -20°C/min
Equilibrium Time: 3 min
Sample holder material: Aluminum
Sample holder volume: 40 µl
Sample holder mass: 53 mg (pan+lid)
Purge gas: 99.99% pure nitrogen
Purge gas flow rate: 50 ml/min
Date Received: 11-MAY-20
Date Tested: 12-MAY-20
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
mat9855 Specific heat
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Specific heat data
Temperature (T)
°C
Specific heat (Cp)
J/kg-°C
Heating/Cooling
rate °C/s
380.5 2677.4 -0.33
296.95 2525.9 -0.33
287.67 2511.8 -0.33
283.55 2628.1 -0.33
279.49 3398.2 -0.33
274.6 5808.5 -0.33
272.73 6238.0 -0.33
270.6 5920.9 -0.33
266.32 4397.3 -0.33
262.04 3446.5 -0.33
257.83 2945.6 -0.33
251.59 2590.7 -0.33
237.12 2433.3 -0.33
160.76 2062.1 -0.33
139.08 1847.2 -0.33
30.746 1330.2 -0.33
Ttrans 281.00 °C
Ejection temperature 261.00 °C
0
1000
2000
3000
4000
5000
6000
7000
0 50 100 150 200 250 300 350 400
Spec
ific
hea
t, C
p (
J/kg
-°C
)
Temperature (°C)
Specific heat vs temperature
mat9855 Pressure-Volume-Temperature
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Pressure-Volume-Temperature
Method: High Pressure Indirect Dilatometry Instrument: Gnomix pvT Apparatus Test Specifications:
Sample Form: Molded Plaque
Pre-Processing: Not required
Scan type: Isothermal Cooling
Date Received: 11-MAY-20
Date Tested: 14-MAY-20
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
mat9855 Pressure-Volume-Temperature
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pvT Experimental Data
Temperature (°C)
Pressure (MPa)
0MPa 50MPa 100MPa 150MPa 200MPa
43.29 0.7654 0.7588 0.7530 0.7478 0.7427
48.70 0.7661 0.7594 0.7537 0.7484 0.7431
56.96 0.7674 0.7606 0.7550 0.7496 0.7445
69.90 0.7692 0.7626 0.7568 0.7515 0.7462
83.30 0.7717 0.7645 0.7586 0.7531 0.7477
96.91 0.7736 0.7664 0.7605 0.7548 0.7493
110.90 0.7758 0.7683 0.7622 0.7565 0.7510
125.10 0.7781 0.7702 0.7639 0.7581 0.7525
139.80 0.7806 0.7720 0.7657 0.7597 0.7539
154.90 0.7842 0.7738 0.7671 0.7609 0.7551
170.10 0.7887 0.7765 0.7684 0.7620 0.7560
185.70 0.7938 0.7803 0.7711 0.7631 0.7565
201.20 0.7996 0.7847 0.7744 0.7654 0.7576
219.70 0.8060 0.7892 0.7782 0.7685 0.7596
236.00 0.8120 0.7940 0.7822 0.7720 0.7625
251.90 0.8186 0.7991 0.7863 0.7756 0.7659
268.10 0.8263 0.8046 0.7910 0.7795 0.7690
284.10 0.8345 0.8103 0.7953 0.7828 0.7720
300.10 0.8445 0.8167 0.7998 0.7865 0.7750
315.80 0.8576 0.8245 0.8051 0.7905 0.7784
331.90 0.8770 0.8363 0.8129 0.7959 0.7825
348.10 0.9112 0.8658 0.8328 0.8051 0.7884
360.70 0.9223 0.8789 0.8532 0.8342 0.8123
371.40 0.9280 0.8827 0.8562 0.8368 0.8210
381.90 0.9330 0.8866 0.8593 0.8392 0.8233
391.80 0.9383 0.8907 0.8627 0.8421 0.8259
mat9855 Pressure-Volume-Temperature
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Melt density 1.0732 g/cm3
Solid density 1.3164 g/cm3
2-domain Tait PVT model coefficients
b5 623.75 K
b6 7.105e-008 K/Pa
b1m 0.000917 m3/kg
b2m 5.156e-007 m3/kg-K
b3m 8.41033e+007 Pa
b4m 0.004773 1/K
b1s 0.000827 m3/kg
b2s 2.055e-007 m3/kg-K
b3s 1.60456e+008 Pa
b4s 0.003991 1/K
b7 0.00009 m3/kg
b8 0.02527 1/K
b9 6.095e-009 1/Pa
0.70
0.75
0.80
0.85
0.90
0.95
1.00
20 70 120 170 220 270 320 370
Spe
cifi
c vo
lum
e (
cm^
3/g
)
Temperature (°C)
Specific volume vs temperature
0 MPa 50 MPa 100 MPa 150 MPa 200 MPa
mat9855 Shrinkage
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Shrinkage
Method: AMPL Shrinkage Test Method (QOP-17-M)
Instrument: Krauss Maffei KM160-750CX Injection molding machine Test mold inscribed with a fine grid pattern Temperature and Humidity Controlled Room OGP Smartscope Flash 400 metrology system
Test Specifications: Sample Form: Pellets
Pre-Processing: Dried at 150°C for 3 hours in a hopper dryer
Moisture Level: 0.0103 %
Date Molded: 12-MAY-20
Post-Processing: Conditioned at 23°C / 50% relative humidity for 7 days
Date Measured: 19-MAY-20
Shrinkage Data Correlated With: Moldflow Insight 2018 Revision 2
Default Shrinkage Model: Residual Stress (CRIMS)
Date Received: 11-MAY-20
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing. Shrinkage measurements have been corrected to account for mold thermal expansion. Data for some process conditions may have been removed in the determination of the favored model.
mat9855 Shrinkage
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Shrinkage Experimental Data
Process Condition
Melt Temperature
(°C)
Mold Temperature
(°C)
Flow Rate (cc/sec)
Part Thickness (mm)
Packing Pressure
(MPa)
Packing Time (sec)
Cooling Time (sec)
1 362.7 176.0 38.4 3 25.4 20 10
2 361.6 177.0 37.0 3 54.9 20 10
3 360.8 168.4 37.7 3 84.7 20 10
4 357.9 172.1 18.7 3 54.8 20 10
5 362.5 174.3 54.9 3 55.0 20 10
6 379.5 176.6 37.7 3 45.2 25 10
7 379.2 176.9 37.7 3 65.0 25 10
8 379.0 176.9 38.4 3 84.8 25 10
9 379.6 176.2 19.2 3 64.8 25 10
10 379.2 177.2 58.2 3 65.0 25 10
11 361.6 176.3 50.6 5 25.4 28 10
12 362.2 177.5 46.2 5 45.1 28 10
13 361.4 178.0 46.2 5 64.5 28 10
14 361.0 177.7 23.8 5 44.8 28 10
15 361.3 178.1 77.7 5 45.1 28 10
16 380.0 177.8 47.6 5 25.4 33 10
17 379.4 177.7 49.0 5 45.1 33 10
18 379.7 178.2 49.0 5 64.9 33 10
19 379.3 177.8 23.1 5 44.9 33 10
20 379.0 178.2 70.8 5 45.2 33 10
mat9855 Shrinkage
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Part Shrinkage
Process Condition Average Measured Parallel
Average Measured Perpendicular
Average Predicted Volumetric
1 1.632% 2.033% 7.260%
2 1.501% 1.848% 5.841%
3 1.164% 1.395% 4.510%
4 1.397% 1.720% 5.844%
5 1.505% 1.795% 5.805%
6 1.466% 1.796% 6.251%
7 1.342% 1.639% 5.352%
8 1.215% 1.467% 4.526%
9 1.310% 1.636% 5.372%
10 1.347% 1.627% 5.347%
11 1.885% 2.368% 9.034%
12 1.782% 2.207% 8.068%
13 1.746% 2.162% 7.163%
14 1.765% 2.219% 8.001%
15 1.855% 2.266% 8.068%
16 1.867% 2.319% 9.114%
17 1.764% 2.166% 8.134%
18 1.653% 2.075% 7.248%
19 1.749% 2.202% 8.061%
20 1.776% 2.188% 8.140%
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Residual Stress Coefficients
Corrected residual in-mold stress (CRIMS) model coefficients
A1 1.073392
A2 0.100348
A3 0.001269
A4 1.242376
A5 0.048838
A6 0.00133
Residual Strain Coefficients
Parallel
Coefficient Lower Limit Upper Limit Centroid
1 0.066563 0.043943 0.091308 0.068569
2 -0.005343 0.060231 0.85836 0.27919
3 0.000895 0.46137 3.9677 1.6498
4 -9.4037e-008 8895.10 43616.00 23044.00
5 0.013479 0 0 0
Perpendicular
Coefficient Lower Limit Upper Limit Centroid
1 0.13618 0.044182 0.091308 0.069201
2 -0.004712 0.060231 0.8537 0.26434
3 -0.000022 0.46137 3.9677 1.5945
4 -1.1497e-008 4296.90 20718.00 8366.30
5 0.011645 0 0 0
The shrinkage models shown above are valid for Autodesk Moldflow Insight 2018 Revision 2 and later. Shrinkage models for previous software versions are included in the 21000.udb file.
Observed Shrinkage
Observed nominal shrinkage
Parallel 1.586%
Perpendicular 1.956%
Observed shrinkage
Minimum Parallel 1.164%
Maximum Parallel 1.885%
Minimum Perpendicular 1.395%
Maximum Perpendicular 2.368%
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Residual Stress Plots
0.00%
0.50%
1.00%
1.50%
2.00%
2.50%
0 2 4 6 8 10 12 14 16 18 20
Shri
nka
ge (
%)
Process conditions
Parallel shrinkage
Experimental value Predicted (with CRIMS) Predicted (without CRIMS)
0.00%
0.50%
1.00%
1.50%
2.00%
2.50%
3.00%
0 2 4 6 8 10 12 14 16 18 20
Shri
nka
ge (
%)
Process conditions
Perpendicular shrinkage
Experimental value Predicted (with CRIMS) Predicted (without CRIMS)
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Residual Strain Plots
0.00%
0.50%
1.00%
1.50%
2.00%
2.50%
0 10 20 30 40 50 60 70 80
Shri
nka
ge (
%)
Process conditions
Parallel shrinkage
Experimental Prediction
0.00%
0.50%
1.00%
1.50%
2.00%
2.50%
3.00%
0 10 20 30 40 50 60 70 80
Shri
nka
ge (
%)
Process conditions
Perpendicular shrinkage
Experimental Prediction
mat9855 Mechanical
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Mechanical
Elastic modulus and Poisson's ratio
Method: ASTM D 638, Standard Test Method for Tensile Properties of Plastics ASTM E 132, Standard Test Method for Poisson's Ratio at Room Temperature
Instrument: MTS Sintech 5/G Universal Testing Machine
Test Specifications: Specimens Tested: 8 (per direction)
Pre-Processing: 23°C +/-2°C at 50% +/-5% relative humidity for a minimum of 40 hours
Sample Form: Machined from molded plaques
Test Speed: 5 mm/min
Date Received: 11-MAY-20
Date Tested: 19-MAY-20
Operator’s Notes: Testing was performed per standard testing procedures. V23 tested below v12. To eliminate errors in the .udb, v23 was made equal to v12.
Elastic modulus
Elastic modulus, 1st principal direction [E1] 3707.71 MPa
Elastic modulus, 2nd principal direction [E2] 3686.63 MPa
Poisson's ratio
Poisson's ratio [v12] 0.3750
Poisson's ratio [v23] 0.3750
mat9855 Mechanical
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Shear modulus
Method: ASTM D 638, Standard Test Method for Tensile Properties of Plastics
Instrument: MTS Sintech 5/G Universal Testing Machine
Test Specifications: Specimens Tested: 8
Pre-Processing: 23°C +/-2°C at 50% +/-5% relative humidity for a minimum of 40 hours
Sample Form: Machined from molded plaques
Test Speed: 5 mm/min
Date Received: 11-MAY-20
Date Tested: 19-MAY-20
Operator’s Notes: Shear modulus is calculated using orthotropic elasticity from the tensile modulus measured on a sample cut at an angle of 45° with the flow direction. Testing was performed per standard testing procedures. No anomalies were noted during testing.
Shear modulus
Shear modulus [G12] 1355.30 MPa
mat9855 Mechanical
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Nonlinear Mechanical Model
Method: ASTM D 638, Standard Test Method for Tensile Properties of Plastics
Instrument: MTS Sintech 5/G Universal Testing Machine
Test Specifications: Specimens Tested: 8 (per direction)
Pre-Processing: 23°C +/-2°C at 50% +/-5% relative humidity for a minimum of 40 hours
Sample Form: Machined from molded plaques
Test Speed: 5 mm/min
Date Received: 11-MAY-20
Date Tested: 19-MAY-20
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
Ramberg Osgood Parameter (Tension)
Sigma Zero 91.9772 MPa
n 3.63485
Alpha 1
Beta 1
Eig 0
Matrix Modulus 2967.82 MPa
Matrix Poisson’s Ratio 0.375
Fiber Modulus 0 MPa
Fiber Poisson’s Ratio 0
Maximum Von Mises matrix Stress at failure 96.6508 MPa
A1 0 1/MPa2
A2 0 1/MPa2
A4 0 1/MPa2
Temperature 23.0 C
Relative Humidity 50.0 %
Strain Rate 0.000833 1/s
The nonlinear mechanical data are derived from RO Library Version 2.
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0
20
40
60
80
100
120
0 0.01 0.02 0.03 0.04 0.05 0.06 0.07 0.08
Stre
ss (
MP
a)
Strain (-)
Nonlinear Mechanical Stress vs Strain
0° Measured 0° Fitted
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Coefficient of linear thermal expansion
Method: QOP-11, Coefficient of Linear Thermal Expansion of Plastics
Instrument: Quartz tube dilatometer per ASTM
Test Specifications: Specimens Tested: 2 (per direction): test repeated 2 times per specimen
Pre-Processing: 23°C +/-2°C at 50% +/-5% relative humidity for a minimum of 40 hours
Sample Form: Machined from molded plaques
Specimen Geometry: Rectangular, 8mm x 50mm, full thickness
Temperature Range: 0°C to 60°C
Date Received: 11-MAY-20
Date Tested: 19-MAY-20
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
Transversely isotropic coefficient of thermal expansion [CTE] data
Alpha 1 4.510e-005 1/°C
Alpha 2 4.940e-005 1/°C
mat9855 Mold verification
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Mold verification
Method: AMPL Mold Verification Test Method (QOP-16-M)
Instrument: Krauss Maffei KM160-750CX Injection molding machine
Test Specifications: Sample Form: Pellets
Pre-Processing: Dried at 150°C for 3 hours in a hopper dryer
Moisture Level: 0.0103 %
Date Received: 11-MAY-20
Date Tested: 12-MAY-20
Operator’s Notes: Testing was performed per standard testing procedures. No anomalies were noted during testing.
mat9855 Mold verification
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3mm tag die
Experiment Number
Flow Rate (cc/sec)
Melt Temperature
Mold Temperature
Cyc0041 13.1 378.4 176.2
Cyc0053 64.1 380.4 179.1
0
5
10
15
20
25
30
35
40
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5
Pre
ssu
re (
MP
a)
Time (s)
Cavity Pressure vs Time
Experimental data AMI2018R2 simulation
Part thickness : 3.0 mmFlow rate : 13.1 cc/secMelt temperature : 378.4 °CMold temperature : 176.2 °C
0
5
10
15
20
25
30
35
40
45
50
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7
Pre
ssu
re (
MP
a)
Time (s)
Cavity Pressure vs Time
Experimental data AMI2018R2 simulation
Part thickness : 3.0 mmFlow rate : 64.1 cc/secMelt temperature : 380.4 °CMold temperature : 179.1 °C
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5mm tag die
Experiment Number
Flow Rate (cc/sec)
Melt Temperature
Mold Temperature
Cyc0104 16.2 378.1 177.4
Cyc0116 83.9 379.7 180
0
1
2
3
4
5
6
7
8
9
10
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5
Pre
ssu
re (
MP
a)
Time (s)
Cavity Pressure vs Time
Experimental data AMI2018R2 simulation
Part thickness : 5.0 mmFlow rate : 16.2 cc/secMelt temperature : 378.1 °CMold temperature : 177.4 °C
0
2
4
6
8
10
12
14
16
18
20
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7
Pre
ssu
re (
MP
a)
Time (s)
Cavity Pressure vs Time
Experimental data AMI2018R2 simulation
Part thickness : 5.0 mmFlow rate : 83.9 cc/secMelt temperature : 379.7 °CMold temperature : 180.0 °C
Contact details
Beaumont Advanced Processing Page 37 of 37
Contact details
Beaumont Advanced Processing
6100 West Ridge Rd
Erie, PA 16506
USA
Phone: +1-814-899-6390
Fax: +1-814-899 7117
Email: [email protected]
Testing enquiries: [email protected]
Beaumont Advanced Processing website: www.bapmolding.com
