::: Excellence in Microwave Synthesis

Masterwave BTRMicrowave Synthesis in the Kilolab

Photos: Croce & Wir

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Specificationssubject to change

without notice.

Instruments for:Density & concentration measurement

Rheometry & viscometry

Sample preparation

Microwave synthesis

Colloid science

X-ray structure analysis

Refractometry

Polarimetry

High-precision temperature measurement

Anton Paar® GmbHAnton-Paar-Str. 20A-8054 GrazAustria - EuropeTel: +43 (0)316 257-0Fax: +43 (0)316 257-257E-mail: info@anton-paar.comWeb: www.anton-paar.com

Authentic workhorse

4 Rapid heating of any solvent on any scale4 Target temperatures smoothly achieved4 Software controller prevents target overshoots4 Efficient cooling by microwave-transparent

cooling liquid4 Improved purity due to suppressed by-product

formation

User-friendly interface

4 Intuitive software with touchscreen navigation4 Bright large icons for easy operation4 Customized parameter display4 One-click editing of reaction parameters4 Direct method transfer from other Anton Paar

devices4 Optional remote control (VNC open source)

Comprehensive data management

4 Customized reaction graphs showing all relevant parameters

4 Experiment review with zoom function for detailed plot

4 Method library for up to 1000 experiments4 Data export via USB storage device or Ethernet4 In-situ printing of GMP-style reaction reports in

PDF format

Serving Scale-up Requirements

Renowned service, support & expertise

4 Quick, hassle-free installation by trained service engineers

4 Comprehensive service contracts for periodic maintenance provided on request

4 Immediate support due to global Anton Paar network

4 Application expertise of renowned microwave chemists

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Based on a revolutionary new technique, the all-new Masterwave BTR benchtop reactor for the first time transfers microwave synthesis to the kilolab.

Productivity in your lab is considerably increased: Depending on your sample, you can process up to 1 kilo per day. The reactor’s magnetically driven overhead stirrer provides independent stirring regimes for individual content.

Due its rising-sensor temperature measurement technique, Masterwave BTR features the high temperature accuracy required for direct method transfer from any smaller microwave device.

Reliable processing of several kilograms per week

Throughout the last decade, efficient microwave synthesis was strictly limited to small-scale applications in R&D laboratories. Masterwave BTR is the first of a new class of instruments that close the gap between research and kilolab processing in microwave synthesis.

A new microwave generation technique (patent pending, US 2009/0194528) overcomes heating difficulties in scale-up and provides efficient heating of a 1L reactor.

The filling of a single vessel results in product amounts far beyond 100 g per run. Several kilograms per week are easily processed.

Safety first

As always, Anton Paar takes every precaution to ensure users’ safety. Dealing with large amounts of chemical reagents at elevated conditions requires additional care.

Due to Masterwave BTR’s comprehensive safety concept, large-scale microwave processing is as safe as using conventional reflux glassware.

In case of a venting action, the instrument is connected to any in-house expansion tank system via a standardized mechanical interface.

A Kilo a Day Microwave Goes Kilolab

Want more? Scale up!

Any method developed with Anton Paar’s R&D instrument Monowave 300 is easily transferred to Masterwave BTR. Thanks to identical software interfaces, all it takes is a simple switch of USB devices.

Total reaction volumes of up to 750 mL and the powerful stirrer’s capacity for agitating up to 200 g of solid material ensure significant product output in any single run. In addition, the system’s integrated cooling considerably decreases overall process times.

Subsequent processing of several reaction vessels yields kilogram amounts of your valuable compounds daily.

Your “walk on, walk off” solution

Despite its increased productivity, Masterwave BTR is still standard laboratory equipment.

Place it in the fume hood, connect it to the corresponding interfaces and and start your chemistry right away.

There are no specific safety measures to observe, no extraordinary pre-installation requirements – you are free to use your available lab space in the most efficient way.

If required, you can seamlessly process your experiments via an optional remote control from your PC.

Join the family

Monowave 300, Synthos 3000, Masterwave BTR – Anton Paar provides an across-the-board portfolio for microwave synthesis, including solutions for reaction screening of smallest amounts, parallel optimization and kilolab productivity.

Any chemistry, any scale, anyone, anywhere!

New Dimensions in Microwave Synthesis

Efficiency beyond the R&D scale

4 New microwave generation technique 4 Industry-validated performance and

productivity4 Designed in close cooperation with leading

pharmaceutical companies4 Compact footprint for operation in a standard

fume hood

Pushing technical frontiers

4 1700 W applicable microwave power4 Two installed magnetrons for utmost field

homogeneity4 Reaction conditions of up to 250 °C and

30 bar4 Rising PT100 temperature sensor4 Integrated hydraulic pressure sensor device4 Internal closed-cycle cooling system

Instant productivity

4 Unrivaled productivity > 1 kg/d4 Bayonet-locked 1L reaction vessel4 Chemically inert & resistant PTFE vessel material4 Easy-handling lip-type seal4 Integrated mechanical stirrer with software-guided

stirring regime4 Compressed air-driven vessel ejector

Vessel material PTFE

Reaction volume 250 - 750 mL

Max. temperature 250 °C

Operating pressure 30 bar (435 psi)

Stirring 0 - 600 rpm

Enhance your output in valuable synthesis:

4 Metal-catalyzed Reactions4 Cycloadditions4 Fluorine Chemistry4 Preparation of Nanomaterials4 Solid-phase Synthesis4 Polymer Synthesis4 Zeolithe Synthesis4 Ionic Liquid Chemistry

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