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Maplewood Farms

SITE PREPARATION PLAN

24 Ball Hill Road

Berlin, Massachusetts

August 8, 2011

Site Preparation Plan 24 Ball Hill Road Berlin, Massachusetts

Richard G. Stromberg, CPG, LSP, LEP Principal Geologist

Prepared for:

Maplewood Farms

Prepared by:

ARCADIS U.S., Inc.

194 Forbes Road

Braintree

Massachusetts 02184

Tel 781 356 7300

Fax 781 356 2211

Our Ref.:

BN030465.0000

Date:

August 8, 2011

This document is intended only for the use

of the individual or entity for which it was

prepared and may contain information that

is privileged, confidential and exempt from

disclosure under applicable law. Any

dissemination, distribution or copying of

this document is strictly prohibited.

BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc i

Table of Contents

1. General 1

1.1 Introduction 1

1.2 Site Environmental Background 5

1.3 Names and Addresses of Parties Involved 6

1.4 Overview of Screening and Testing Requirements for Soil Acceptance 7

2. Soil Testing Requirements 11

3. Laboratory Environmental Analyses 12

4. Soil Approval and Placement 14

4.1 Soil Approvals 14

4.2 Soil Placement and Tracking 14

5. Other Considerations 15

5.1 Site Access and Quantity Estimating 15

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Table of Contents

Figures

Figure 1 USGS Site Locus Map

Figure 2 SA Farms Soil Placement Layout and Current Grade Elevations and SA Farms Future Grade Elevations

Figure 3 Wetland Area and Buffer Zone Map

Figure 4 Zoning Map

Figure 5 MassDEP GIS Map

Tables

Table 1 Summary of Soil Data Results and Acceptance Criteria

Appendices

Appendix A Section of M.G.L. Chapter 40 Section 3A

Appendix B List of MCP Disposal Sites

Appendix C Background Sampling Analytical Data

Appendix D Soil Profile Package Information

Appendix E Private Well Completion Report and Testing

1

Site Preparation Plan

24 Ball Hill Road Berlin, Massachusetts

1. General

1.1 Introduction

The following is a “Site Preparation Plan”, Phase I Area prepared in support of the

planned use of a 4-acre portion of a parcel of land known as the Maplewood Farms

Site (“the Site”) for farming purposes located off of 24 Ball Hill Road in Berlin,

Massachusetts. The Phase I area is shown on Figure 1 and the area where soil will be

placed is shown on Figure 2. The portion of the property where soil will be placed in

Phase I is located on Lot A and B-1 just east of Ball Hill Road. The Owner is Tamara

and Archibald Johnston (individually) of 24 Ball Hill Road,the Operator is Lighthouse Environmental Management LLC. 184 Stone Street Clinton MA 01510 and the Operations Manager is Kevin Francis Gervais (617-699-5245).

The Phase I Site is currently a horse paddock and open vegetated land that has been

used for farming and agricultural purposes in the past and is proposed by the owner to

continue to be used for the same purposes (General Farming and Raising of

Livestock). A section of M.G.L. Chapter 40, Section 3A is provided in Appendix A that

apply to this property and these regulations. Although the clearing of land may be

greater than one acre, any amount of clearing for agricultural purposes is not

considered an industrial activity under the storm water regulations. Section 402(l)(1) of

the 1987 Water Quality Act exempts agricultural storm water discharges from NPDES

permitting requirements including storm water permitting. This exemption only applies,

however, if the clearing of land is solely for agricultural purposes.

The portion of this Phase I parcel that is planned for clearing, leveling, and construction

of a new horse paddock through import of soil is shown on Figure 2. This Phase I Area

is located outside of currently delineated wetland areas and buffer zones as shown on

Figure 3. This area will utilize the existing access road for placement of the soil from

an average elevation of 575’ to a planned elevation of Elev.610’ as shown on Figure 2.

A Stormwater Pollution and Protection Plan (SWPPP) filing for discharges from

construction activities (such as clearing, grading, excavating, and stockpiling) that

disturb one or more acres, are regulated under the National Pollutant Discharge

Elimination System (NPDES) stormwater program. Prior to discharging stormwater,

construction operators must obtain coverage under an NPDES permit, which is

administered by either the State (if it has been authorized to operate the NPDES

stormwater program) or EPA, depending on where the construction site is located.

According to the Operator, a SWPPP filing is not necessary due to agricultural

exemptions but dust and storm water will be controlled by the Operator.

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Certain management practices will be exercised by the Owner, Operator, and

Operations Manager (Mr. Kevin Gervais) to prevent changes in runoff patterns toward the wetland areas and buffer zones located to the south.

The period of time expected to import the necessary soils is 6-12 months. It is expected that about 360,000 cy of soil will be required in the placement area to achieve the continued use of the property for agricultural purposes by the owner.

This management plan provides information for the specific placement of soil at this portion of the Site that meet certain physical and chemical criteria. This plan provides

the status of applicable land use regulations, areas to be cleared to some degree and leveled, and a discussion of applicable MCP regulations.

The information utilized for this plan was obtained from the owner, information on file at the Berlin Town Offices, and other publicly available information as well as testing and surveys conducted on the Site.

Coordination was made by the Operator with Berlin local officials for the “Right to Farm” bylaw recognized by Berlin and no filings were required. A Notice of Intent (NOI)

filing with the Berlin Conservation Commission (BCC) or Nashoba Board of Health was deemed not required at this time because work won’t be conducted in wetlands or buffer zones. The access road will be maintained outside the buffer zones.

The area of the Site is residentially-zoned land and open space as shown on Figure 4. Figure 5 is a MassDEP Geographic Information System (GIS) map for the Site.

Figure5 also provides the Area Resource Map from the MassDEP and indicates that the Site is not located within an MassDEP designated Zone II drinking water resource area, Interim Wellhead Protection Area (IWPA), sole source aquifers, or Area of Critical

Environmental Concern (ACEC). There are no mapped vernal pools or habitats for rare wildlife/species on or near the Phase I Site.

The Site is currently served by two private wells. The house well at 24 Ball Hill Road as shown on Figure 2 was drilled to 425 feet in bedrock yielding 25 gpm. Information regarding this house well was provided by Mr. Bill Brookings of the Nashoba Board of

Health via a telefax request on July13, 2011. The Well Completion Report and testing of the well is provided in Appendix E. The well was tested in September and October 2010 for primary/secondary drinking water parameters and coliform, manganese, and

iron exceeded criteria. The well was chlorinated and were re-tested in November 2010 and July 2011 and passed.

3



The well is currently used for human consumption this well replaced the previously

drilled two prior house wells, which have since been decommissioned and abandoned.

A second private well on 24 Ball Hill Road is near the barn and provised potable water,

which is used both for animal and human consumption. Mr. Brookings indicated there

were no municipal wells located within ½ mile of the Site.

The Site is bounded to the west by Ball Hill Road and to the north, east, and south by

property owned by the Owners. There will be no buildings constructed on the Phase I

Site as it is planned for a horse paddock and raising of livestock. The unpaved road will

be used for access by machinery. The road condition will be maintained by the Owner

such that visible dust will be kept to a minimum. Soil from the Site will not be tracked

onto Ball Hill Road. There will be no other water supply wells drilled on the Site.

There will also be no athletic fields or areas of high intensive children activity in the

area to be filled under this plan. There are also no planned communal vegetable

gardens or generation of produce for sale on the Site.

A review of MassDEP’s list of MCP Disposal Sites in Appendix B indicated that there

were no release sites located in the vicinity of the Site.

The geological conditions on the Site consist of an overburden veneer of thin to absent

glacial till over bedrock as mapped on the MassDEP GIS Surficial Geology map for

Berlin (Dec. 2009). The bedrock consists of gray, medium-grained schist and gneiss.

It has been determined that soil of sufficient chemical and physical quality is necessary

to be imported for the project to bring certain areas to the required grade for farming.

Lighthouse Environmental Management,LLC. has entered into agreement with owner to manage soil import activities. Arcadis was retained by Lighthouse to prepare the soil

re-use management plan on behalf of the Owner and to review candidate soils for

compliance with this plan. Arcadis, Lighthouse and the Owner were responsible to

ascertain that appropriate local and state regulations were reviewed for the intended

use of the Site and permits were acquired as necessary to implement the continued

future use. Lighthouse and the Owner are responsible through their contractual

arrangements for ensuring that only soils approved under this plan are brought to the

Site.


4



The soil re-use activities and all other construction-related activities will be conducted

in accordance with this plan. It is the Owner’s and Lighthouse’s indication that the

filling will be conducted in the specified area as shown on Figure 2 which depict current

and planned grade. The owner and Lighthouse have indicated they have discussed

with the municipality, its boards and commissions the nature of the planned Site use

and necessary import of material to obtain elevations shown on Figures 2.

MassDEP’s Bureau of Waste Site Cleanup (BWSC) under the Massachusetts

Contingency Plan (MCP) does not provide approval for “<RCS-1” soil re-use at a site

like this one but requires that “anti-degradation” provisions at 310 CMR 40.0032 (3) be

followed for the soil to be chemically suitable. The physical suitability of the soil will be

determined by Lighthouse and the Owner. The Site is classified as “RCS-1” under the

MCP since the Site is located within 500 feet of a residence. The MCP groundwater

classification in the area is “GW-1, 2 and 3” for current or potential drinking water,

exposures to residential indoor air, and surface water bodies as defined in the MCP.

Re-use of soils on the Site from outside sources is necessary to create a level surface

for horse farming. The soil must also abide by certain physical acceptance

requirements and not significantly alter the drainage patterns in the area. It is

understood that certain fine grained silt/clay and some organic soils will be accepted as

long as hydrogen sulfide odors are not apparent and moisture is tolerated for mixing

with granular soils, but no dredge spoils or dredged organic silt or peat material will be

accepted unless specifically permitted for use in upland areas by the appropriate

agency and the LSP for this project.

The final goal of this plan is to formalize the soil management process and the soils

acceptance policy at the Site in order to meet re-use requirements and to give

generators a sufficient level of comfort that their material is being handled

appropriately.





The Owner and Lighthouse intend to conduct the soil management operations with

approved “clean” fill and natural soils from off-site locations that are considered to be

the following:

• Non-Massachusetts Contingency Plan (MCP) regulated soils (“<RCS-1”). Soils that

are recognized to contain fill materials (reworked natural soil or soil with some small

proportion of anthropogenic residual material) from non-MCP regulated sites, or

other soils brought from an MCP-regulated site that are < RCS-1 standards and not

considered part of a Disposal Site as defined in the MCP by the sending LSP. This

soil is also MCP restricted in that it must also meet MCP “anti-degradation provisions” at 40.0032. This requirement is addressed through the development of “Acceptance Criteria” in this plan.

• Naturally occurring, non-impacted soils that do not originate from within affected layers on an MCP site or a site with filling activities and are not otherwise regulated.

These soils generally will not require the amount of testing as soils noted above

and compliance with 40.0032 except as specifically requested by the Project LSP,

Lighthouse or the Owner based on certain site conditions or features (i.e. certain

clay that may contain certain metals and conductance). For natural soils to be

accepted without testing, a written Generator “Certification Statement” will be required outlining the basis for the statement subject to the approval of the Project LSP, Lighthouse, and the Owner.

Soils from on-going and proposed projects will be delivered to the appropriate section of the re-use area as specified by Lighthouse and the Owner and will be placed and tracked in accordance with procedures in this plan.

Approximately 360,000 cubic yards) of common soil fill is estimated for the project.

1.2 Site Environmental Background

The Site does not contain sensitive environmental receptors but groundwater is used

for drinking water and by residents and animals. The Owners live on parcels where soil will be imported. Surface water exists in a natural brook to the east of the Site.




There were a series of analytical tests conducted on naturally occurring surface soils in

the Site in June 2011 by ARCADIS and Lighthouse. A total of three composite

samples designated as “PH I SS-1 through 6” located throughout the Phase I re-use

area to be developed were collected by Lighthouse and ARCADIS. Analysis included:

SVOCs, VOCs, TPH, and Priority Pollutant 13 Metals, pesticides/herbicides, PCBs,

and specific conductance. The analytical data sheets are included in Appendix C.

The results were used to summarize average and maximum Site “background”

concentrations as shown on Table 1. For comparative purposes, Table 1 also depicted

the current MCP RCS-1 values promulgated by MassDEP.

The significance of this background environmental testing is described later in this plan

for development of soil “Acceptance Criteria”.

1.3 Names and Addresses of Parties Involved

The owner of the property is:

- Tamara and Archibald Johnston, 24 Ball Hill Road, Berlin, MA

The Operator of the Site is:

- Lighthouse Environmental Management,LLC 184 Stone Street, Clinton MA 01510

The operations Manager of the Site for soil placement operations is:

- Mr. Kevin Francis Gervais (617-699-5245)

The “Site LSP” reviewing candidate soil packages is:

- Mr. Richard Stromberg, ARCADIS-US, Inc., 194 Forbes Road, Braintree, MA02184. Cell Phone: (617) 908-7094, Tel: (781) 356-7300 x203.




1.4 Overview of Screening and Testing Requirements for Soil Acceptance

Soil to be placed at the Phase I part of the Site, other than some certified naturally-

occurring soils, will require field screening and analytical testing to conform with MCP

requirements and to demonstrate that the material is chemically suitable for the project.

The physical suitability will be reviewed and approved by Lighthouse and the Owner.

Soil Profile Package information for the approval candidate soils is provided in

Appendix D.

Screening Criteria

Lighthouse or a specified representative may conduct periodic screening of soils that

will be shipped to the Site to make sure soils are as represented. Candidate soil must

be evaluated by the generator for the following screening criteria and these results

must be addressed in the soil profiling package prepared by the generator. Candidate

soil being placed in the Site shall not exceed the following field screening/visual criteria:

• Field screening results of soil headspace from representative samples must not exhibit an average reading of Total Organic Vapors (TOV) in the jar headspace exceeding 2 parts per million (ppm) by volume due to volatile constituents. If screening has not been performed by the generator, it may be performed at the Site by Lighthouse or another designated party as appropriate to verify certain loads. If screening at the Site results in exceedances to the criteria above, the load(s) will be rejected.

• Visually, the soil must not exhibit any staining, odors, or other discolorations indicative of oil and hazardous material (OHM) releases as demonstrated by the representative of the soil to be imported.

• The urban fill soils must not contain any refuse, trash or solid waste. The soil may contain ancillary non-coated or non-painted bricks or non-coated/stained or non-impregnated concrete or cobbles less than 6 inches diameter if it is contained within certain fill soils in very small quantities. This material must be less than 5% of the fill material. If soils contain more than this amount, the above-listed excluded material must be physically separated and sent to a designated construction and demolition (C&D) or permitted Asphalt, Brick, Concrete (ABC) disposal facility by the generator. Loads received that contain more than the acceptable amount of solid waste will be rejected by Lighthouse and sent back to the site of origin at the generator’s cost.




• Soil may contain naturally deposited silt and clay and a certain portion of naturally occurring organic content and moisture since drainage of the soil can occur on the Site while it is being worked as represented by Lighthouse. No dredge spoils will be allowed unless permitted by MassDEP.

• Upon arrival of the trucks at the Site, soils will be visually inspected and field screened from representative loads by Lighthouse or another designated party and discrete soil samples may be collected from a representative number of loads to prepare a composite sample from the candidate property for confirmatory analysis by the owner or Lighthouse at their discretion.

Rationale for Development of Analytical Acceptance Criteria

In developing the Acceptance Criteria for the Site, the following step-wise rationale was developed as described below for soils other than certified, non-impacted, naturally occurring soils. Naturally occurring soil may be subject to certain chemical testing based on site-specific conditions as evaluated by the generators engineer, qualified environmental professional (QEP) or LSP.

The rationale considered current MCP RCS-1 soil standards, the environmental conditions at and in the immediate vicinity of the Site, and characteristics of certain constituents that may be included in the candidate soil (adsorption coefficient, toxicity, and frequency of occurrence in the environment). Site-specific soil sampling was also performed from surface and near surface soils in and around the Phase I fill area of the Site to use this information as the primary tool for calculating Acceptance Criteria.

A summary of the background sampling results for the Site is provided on Table 1. This table includes the maximum concentration observed on the Site, the average concentration, three times (3X) the average concentration for use in calculating PAH/SVOC and metal Acceptance Criteria, MassDEP published “natural soil” concentrations, and current and current MCP RCS-1 standards.

These categories have been applied at similar sites in the Commonwealth of Massachusetts by ARCADIS for preparing acceptance criteria with MassDEP acknowledgement at one site.




The average and maximum concentrations were utilized in developing Acceptance Criteria for Priority Pollutant -13 metals, PCBs, TPH, and SVOCs/SVOCs. With regard to “other metals”, the MassDEP published values for natural soils and RCS-1 standards (where available) should be consulted when site –specific data was generated. These “other metals” do not necessarily require testing for acceptance unless a given natural condition warranted testing for one of these metals by the generator, i.e. known natural accumulation of a certain element or elements in certain soils. Elevated concentrations of these metals at a candidate site not associated with natural conditions will not be accepted at this Site.

Once the Acceptance Criteria were selected, they were checked against current and proposed RCS-1 standards for compliance.

Summary of Acceptance Criteria

1. For VOCs all constituent concentrations must be below laboratory detectablelimits because no detectable levels were found in Site-specific sampling. A traceamount of a lone VOC may be accepted if it is clearly identified to be an outlier inthe data set and the soils are not part of a VOC release or if it is a laboratorycontaminant (acetone) or by product of the sampling preservative and soil. Thelaboratory detectable limits shall not be higher than MCP RCS-1 soil standardsfor a given VOC constituent. PCBs will not be accepted above a detection limit of0.1 ppm. A trace below 0.1 ppm in one sample may be accepted provided thegenerator certifies that there were no known releases of PCBs to the soils thatwould give rise to concentrations > 0.1 ppm and other samples are ND (minimumof two).

2. For TPH, levels of TPH were detected at 120-170 mg/kg. The levels wereattributed to some bits of asphalt in the loam and surface soil observed. Theaverage TPH concentration was 140 mg/kg and three times average was 420mg/kg which is below the current RCS-1 standard of 1,000 ppm. An AcceptanceCriteria of 300 ppm was developed to address both natural soils and soils thatcontained asphalt that may contain some TPH. Some averaging will be allowedfor certain cases. Since a certain proportion of fill already exists at the Site, avalue of 300 (asphalt or binder material source) was considered not tosignificantly exceed background and still be protective for future use since roadsand machinery traffic will be placed or occur on the development. TPH at thislimit must be from asphalt and not from a fuel oil release in the subject soils andwill not be accepted.




3. The SVOC results indicated that a few target SVOCs were detectable, however,all of the detections were below the RCS-1 reportable concentrations. SomeSVOC compounds are considered by MassDEP to be ubiquitous in theenvironment (including some from forest fires) and are generally not consideredto be mobile in subsurface aqueous systems. Since certain SVOCs have beendocumented by MassDEP to be present in naturally occurring soils (especiallyforest mat with burnt wood remnants) as shown in Table 1, an AcceptanceCriteria of 3 times the one-half detection limit and the detected concentrationswere utilized. The concept of three times one-half DL or average concentrationwas acknowledged by MassDEP for SVOCs on a similar site. The AcceptanceCriteria ranged from 0.6 to 4.8 ppm.

4. With regard to the metals analyzed during the background sampling program,the results were fairly uniform with no significant deviations. In certain cases,levels of arsenic, chromium, and barium can be found in naturally depositedBoston Basin marine clays/silts like that excavated from the Central ArteryTunnel (CAT) project. Arithmetic mean arsenic concentrations from some ofthese soils as reported by MassDEP was 8 to 44 mg/kg for arsenic,(Memorandum from Paul Locke to Steve Lipman of MassDEP, July 2002). TheMADEP 90th percentile published background value for arsenic is 20 mg/kg.Arsenic is also known to be naturally occurring in Worcester County at levels of20-40 ppm (O’Neill,1995). The arsenic Acceptance Criteria was identified as< 20ppm based on an average concentration of 15 ppm with the RCS-1 of 20 ppm.Some slightly higher concentrations may be acceptad on a case by case basis.Other non-exempt fill soils containing arsenic must be below 20 ppm which is theRCS-1. This criteria is consistent with documented natural soil arsenicconcentrations in Worcester County.

With regard to lead, the average Site concentration was 26 ppm. Since most fill soils and some natural soils contain some levels of lead < 100 mg/kg, and the MassDEP Rural Soil concentration is 100 mg/kg, an Acceptance Criteria of 79 ppm was established which is consistent with the 3X concept and is not significantly above the Site maximum.

With regard to other metals Acceptance Criteria were chosen at 3X background which included detects and ½ detection limits where not detected.




5. No pesticides/herbicides were detected at the Site. Since this is farmland, a traceof some pesticides/herbicides well below RCS-1 can be accepted on a case bycase basis as long as the predominance of samples are ND and concentrationscan be demonstrated to have resulted from properly applied materials.

6. The pH range should be 5-9 pH units and specific conductance should be lessthan 1,000 umhos/cm2 for granular soils as long as the metals are compliant. Inthe case of naturally deposited, non-impacted Boston Basin marine clay/silt, aconductance of 1,000-2,000 umhos/cm can be accepted in consideration ofmetal concentrations. This is well below MassDEP’s criteria of 4,000 umhos/cmfor unlined landfills. The acceptance of natural silty clay with higher conductancewill depend on the quantity and the available location for placement on the Site,i.e. not in close proximity to wetlands/streams.

The candidate soil must not originate from nor be contiguous with an MCP-regulated release area or “disposal site”, unless in certain circumstances, the soil can be taken from an MCP disposal site as long as the soil strata in question are not impacted above Acceptable Criteria as demonstrated by the Engineer/LSP. For example: a non-impacted fill zone or layer < RCS-1 that also meets Acceptance Criteria or a non-impacted natural soil layer below or above an impacted layer that also meets Acceptance Criteria. This must be documented and signed by the candidate site LSP/QEP or Engineer.

Laboratory results must meet these criteria. In certain instances, averaging within a given profile may be utilized. The averaging should be discussed with the Site LSP before the generator prepares the soil profile package.

2. Soil Testing Requirements

The majority of the soil that is scheduled to be placed in the Site is contemplated to originate from large construction projects where the soils have either been pre-

characterized during the engineering phase of the development or characterized from stockpiled soil. All soils to be placed in the Site will be pre-characterized by the generator, except in some cases non-impacted, naturally occurring soils where a

Generator’s Certification Statement is received and approved. Some testing of these soils may still be required.

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Prior to placement of material in the Site, the Site LSP will review the pre-

characterization data packages of all potential candidate soils prior to acceptance of

the materials. This will be done to demonstrate that the soils from the generator’s

property are in compliance with Acceptance Criteria and other provisions of this plan.

The Site LSP, Owner or Lighthouse may also request to review any environmental

investigative reports regarding potential OHM release(s) and soil quality at the

originating property.

For acceptance of soils, the generator shall provide a soil profile package including

laboratory analytical data for the parameters listed in Section 3.0. The sampling

frequency shall be a minimum of one composite soil sample per every 500 cubic yards

of soil to be delivered, or at a frequency considered suitable and sufficient by the

Engineer/LSP/QEP for the soil in question (i.e. 1,000 cy for undisturbed, non-impacted

natural soil in proximity to regulated soil) as described in various MassDEP’s policies

for due diligence assessments. If sufficient analytical data is not available from the

generator, the owner, Lighthouse or the Site LSP, will require that the generator of the

soils collect additional samples. This will ensure that, at a minimum, the material is less

than the Acceptance Criteria set forth in this plan and the equivalent frequency of

testing requirements that is typically employed for MassDEP permitted Massachusetts

Landfills have been met. This will enable Lighthouse to provide the necessary

background information to verify that material deposited in the Site is acceptable.

In some cases, crushed bedrock may also be accepted and physical/chemical analysis

of the rock will be determined on a case-by-case basis for its intended use.

3. Laboratory Environmental Analyses

Samples requiring environmental analysis shall be submitted to a laboratory certified

by MassDEP for the chemical analyses required.

Environmental samples shall be collected, labeled, and preserved in accordance with

established protocols for the respective analysis, and submitted to the analytical

laboratory under chain-of-custody procedures.





Laboratory environmental analyses for the following parameters shall be in accordance

with the latest version of the specified test method:

Parameter EPA Test Method

Total Petroleum Hydrocarbons (GC-FID)(TPH)

ASTM D 3328

Volatile Organic Compounds (VOCs) 8260

Semi-Volatile Organic Compounds (SVOCs)

8270

Polychlorinated Biphenyls (PCBs), 8082

Priority Pollutant 13 or RCRA 8 Metals (and other Metals as Appropriate)

6010/7000

Pesticides/herbicides 8081B

Specific Conductance will be run. Reactive sulfide/cyanide, and pH will also be run if

there is reason to suspect that these hazardous waste characteristics need to be

evaluated. Sampling and QA/QC procedures acceptable to MassDEP will be adhered

to and QA/QC results will be considered by the generating facility in determining if the

soil profiling is acceptable.

Laboratory analytical data sheets, chain-of-custody’s, and laboratory QA/QC reports

will be provided with the soil profiling packages along with pertinent maps/sketches and

field testing results for review by Lighthouse and the LSP.

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4. Soil Approval and Placement

4.1 Soil Approvals

Once the generator’s Engineer, QEP or LSP representative has approved the

analytical results as described in this plan, a generator representative should forward

the results of the soil profile package or pre-characterization study in letter format with

attachments to Lighthouse who will provide initial feedback on the potential

acceptance of a given soil. Appendix D contains information on requirements for the

Soil Profile Package submittals. After initial approval is gained, the package will be

sent to the Site LSP for review. Characterization results from each candidate property

will be reviewed to confirm that the soil meets the requirements set forth in this plan.

The Site LSP will then prepare an acknowledgement and approval letter to the owner/

Lighthouse confirming the acceptance of the soil for confirmatory signature by

Lighthouse. The letter will specify the approved quantity, the quantity to be shipped,

dates, restrictions (if any), and other pertinent items. The letter will be forwarded by

Lighthouse to the generator.

4.2 Soil Placement and Tracking

Once the analytical data from the proposed generator’s property has been reviewed

and approved by the owner, Lighthouse, and the Site LSP, the soils will be designated

to a specific area which will be logged into the facility’s database, with the estimated

quantity. All soils being placed in the applicable area will require a MassDEP Material

Shipping Record (MSR) or Bill-of-Lading (BOL) to accompany each truckload. The

designated area will be placed on all MSRs or BOLs. The Site LSP will periodically

inspect the Site and records on file at the Site for conformance with this plan.

The trucks may be weighed at the Site or another location as specified by Lighthouse.

Scaling will be at Berlin Stone Co, 322 Sawyer Hill Road,Berlin MA. Once the truck

has been weighed on a certified scale it will be directed to place the material into a

specific area. The appropriate paperwork will be left on site at a designated location or

handed directly to on-site personnel. The Soil piles will be placed within the

designated area to be filled and will be spread out by the Site earth-works contractor

until the desired grade is met. Then the area will be noted and coded in the files.


15



If the on-site personnel deem the material to be suspect after dumping the truck will be

rejected and sent back to the generator for additional testing, or returned at the

generator’s expense. If loads are received that contain large pieces of solid waste, the

pieces will be segregated and stockpiled for re-loading and transport back to the site of

origin at the generator’s expense.

5. Other Considerations

5.1 Site Access and Quantity Estimating

The Site is located about 40 miles west of Boston in Berlin.. From 495,Take 62W exit towards Berlin and after 0.5 mile you will see Sawyer Hill Road on your right, go down to 322 Sawyer Hill Road at Berlin Stone Co to do the scaling and then get back on 62W, follow 62W and then take left at the blinking yellow light on to Barnes Hill Road, take left on Linden Ave and then right on Ball Hill Road to reach Maplewood Farms 24 ball hill road. While leaving Maplewood exit right on Ball Hill Road to Linden Ave, take right on Linden Ave to 62E.Please note while coming in you have to go through Barnes Hill Road and not Linden Ave as there is a low weight bridge on Linden Ave."

Prior to shipment, trucks will be weighed at a certified scale. Access will be through the

access road into the Site and to the given phase area as directed by Lighthouse.

Roadways will be maintained for truck access. Hours of operation are 7:00 am to 3:30

pm from Monday to Friday and some Saturdays.

The owner maintains the appropriate equipment year-round to spread, dry, and

compact the soils.


FIGURES

MassDEP - Bureau of Waste Site Cleanup MCP Numerical Ranking System Map: 500 feet & 0.5 Mile Radii Site Name:

24 Ball Hill Road Berlin, MA RTN: NAD83 MA Coordinates:

0mE, 0mN July 12, 2011

The information shown on this map is the best available at the date of printing. For more information please refer to www.mass.gov/mgis/massgis.htm

Page 1 of 1Map Output

7/12/2011http://maps.massgis.state.ma.us/servlet/com.esri.esrimap.Esrimap?ServiceName=matowns...

5

TABLES

DRAFT Table 1Summary of Soil Results and Acceptance CriteriaMaplewood Farms, 24 Ball Hill Road, Berlin, MA

OIL or HAZARDOUS MATERIAL

Berlin Site Max Concentration

Berlin Site Background Avg

3X Site Background AvgConcentration in

"Natural" Soil (MADEP, Spring 2002) RCS1 Berlin Acceptance Criteria PH 1 SS-1 PH 1 SS-2 PH 1 SS-3 MAX Avg 3X average

GC/MS SEMI VOC/PAHs BY 8270D mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

1,2,4-Trichlorobenzene 0.4 0.4 1.1 NA 2 1.1 0.37 0.37 0.375 ND 0.4 1.12

1,2-Dichlorobenzene 0.4 0.4 1.1 NA 9 1.1 0.37 0.37 0.375 ND 0.4 1.12

1,3-Dichlorobenzene 0.4 0.4 1.1 NA 1 0.9 0.37 0.37 0.375 ND 0.4 1.12

1,4-Dichlorobenzene 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12

2,2'-oxybis[1-chloropropane] 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12

2,4,5-Trichlorophenol 0.4 0.4 1.1 NA 4 1.1 0.37 0.37 0.375 ND 0.4 1.12

2,4,6-Trichlorophenol 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12

2,4-Dichlorophenol 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12

2,4-Dimethylphenol 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12

2,4-Dinitrophenol 0.4 0.4 1.1 NA 3 1.1 0.37 0.37 0.375 ND 0.4 1.12

2,4-Dinitrotoluene 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12

2,6-Dinitrotoluene 0.4 0.4 1.1 NA 100 1.1 0.37 0.37 0.375 ND 0.4 1.12

2-Chloronaphthalene 0.4 0.4 1.1 NA 1000 1.1 0.37 0.37 0.375 ND 0.4 1.12

2-Chlorophenol 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12

2-Methylnaphthalene 0.2 0.2 0.6 0.7 0.7 0.6 0.185 0.185 0.19 ND 0.2 0.56

2-Methylphenol 0.4 0.4 1.1 NA 500 1.1 0.37 0.37 0.375 ND 0.4 1.12

2-Nitrophenol 0.4 0.4 1.1 NA 100 1.1 0.37 0.37 0.375 ND 0.4 1.12

3 & 4 Methylphenol 0.4 0.4 1.1 NA 500 1.1 0.37 0.37 0.375 ND 0.4 1.12

3,3'-Dichlorobenzidine 0.8 0.8 2.3 NA 1 0.9 0.75 0.75 0.75 ND 0.8 2.25

4-Bromophenyl phenyl ether 0.4 0.4 1.1 NA 100 1.1 0.37 0.37 0.375 ND 0.4 1.12

4-Chloroaniline 0.8 0.8 2.3 NA 1 0.9 0.75 0.75 0.75 ND 0.8 2.25

4-Nitrophenol 1.9 1.9 5.6 NA 100 5 1.85 1.85 1.9 ND 1.9 5.60

Acenaphthene 0.2 0.2 0.6 0.5 4 0.6 0.185 0.185 0.19 ND 0.2 0.56

Acenaphthylene 0.2 0.2 0.6 0.5 1 0.6 0.185 0.185 0.19 ND 0.2 0.56

Acetophenone 0.4 0.4 1.1 NA 1000 1.1 0.37 0.37 0.375 ND 0.4 1.12

Aniline 1.9 1.9 5.6 NA 1000 5 1.85 1.85 1.9 ND 1.9 5.60

Anthracene 0.2 0.2 0.6 1.0 1000 0.6 0.185 0.185 0.19 ND 0.2 0.56

Azobenzene 0.4 0.4 1.1 NA NA 1.1 0.37 0.37 0.375 ND 0.4 1.12

Benzo[a]anthracene 0.8 0.6 1.7 7 7 1.7 0.38 0.8 0.5 0.8 0.6 1.68

Benzo[a]pyrene 0.9 0.7 2.0 2 2 1.9 0.47 0.93 0.64 0.93 0.7 2.04

Benzo[b]fluoranthene 1.5 1.0 3.1 7 7 3.1 0.68 1.5 0.94 1.5 1.0 3.12

Benzo[g,h,i]perylene 0.6 0.4 1.2 1,000 1000 1.2 0.185 0.64 0.41 0.64 0.4 1.24

Benzo[k]fluoranthene 0.5 0.4 1.2 1,000 70 1.2 0.195 0.52 0.44 0.52 0.4 1.16

Bis(2-chloroethoxy)methane 0.4 0.4 1.1 NA 500 1.1 0.37 0.37 0.375 ND 0.4 1.12

Bis(2-chloroethyl)ether 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12

Bis(2-ethylhexyl) phthalate 3.1 1.3 3.8 200 200 3.8 3.1 0.37 0.375 3.1 1.3 3.85

Butyl benzyl phthalate 0.7 0.5 1.5 NA 100 1.5 0.74 0.37 0.375 0.74 0.5 1.49

Chrysene 1.1 0.8 2.3 70 70 2.3 0.53 1.1 0.68 1.1 0.8 2.31

Dibenz(a,h)anthracene 0.2 0.2 0.6 0.7 0.7 0.6 0.185 0.185 0.19 ND 0.2 0.56

Dibenzofuran 0.4 0.4 1.1 NA 100 1.1 0.37 0.37 0.375 ND 0.4 1.12

Diethyl phthalate 0.4 0.4 1.1 NA 10 1.1 0.37 0.37 0.375 ND 0.4 1.12

Dimethyl phthalate 0.4 0.4 1.1 NA 30 1.1 0.37 0.37 0.375 ND 0.4 1.12

Di-n-butyl phthalate 0.4 0.4 1.1 NA 50 1.1 0.37 0.37 0.375 ND 0.4 1.12

Di-n-octyl phthalate 0.4 0.4 1.1 NA 1000 1.1 0.37 0.37 0.375 ND 0.4 1.12

Fluoranthene 2.6 1.6 4.8 1,000 1000 4.8 0.86 2.6 1.3 2.6 1.6 4.76

Fluorene 0.2 0.2 0.6 1,000 1000 0.6 0.185 0.185 0.19 ND 0.2 0.56

Hexachlorobenzene 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12

Hexachlorobutadiene 0.4 0.4 1.1 NA 6 1.1 0.37 0.37 0.375 ND 0.4 1.12

Hexachloroethane 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12

Indeno[1,2,3-cd]pyrene 0.4 0.4 1.1 7 7 1.1 0.37 0.37 0.375 ND 0.4 1.12

Isophorone 0.4 0.4 1.1 NA 100 1.1 0.37 0.37 0.375 ND 0.4 1.12

Naphthalene 0.2 0.2 0.6 4 4 0.6 0.185 0.185 0.19 ND 0.2 0.56

Nitrobenzene 0.4 0.4 1.1 NA 500 1.1 0.37 0.37 0.375 ND 0.4 1.12

Pentachlorophenol 1.9 1.9 5.6 NA 3 2.9 1.85 1.85 1.9 ND 1.9 5.60

Phenanthrene 1.5 0.9 2.6 10 10 2.6 0.43 1.5 0.7 1.5 0.9 2.63

Phenol 0.4 0.4 1.1 NA 1 1.1 0.37 0.37 0.375 ND 0.4 1.12Pyrene 1.9 1.3 3.8 1,000 1000 3.8 0.76 1.9 1.1 1.9 1.3 3.76








GC/MS VOA BY 8260C mg/kg mg/kg mg/kg mg/kg mg/kg

1,1,1,2-Tetrachloroethane 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,1,1-Trichloroethane 0.0 0.0 0.0 ND 30 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,1,2,2-Tetrachloroethane 0.0 0.0 0.0 ND 0.005 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,1,2-Trichloroethane 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,1-Dichloroethane 0.0 0.0 0.0 ND 0.4 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,1-Dichloroethene 0.0 0.0 0.0 ND 3 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,1-Dichloropropene 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,2,3-Trichlorobenzene 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,2,3-Trichloropropane 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,2,4-Trichlorobenzene 0.0 0.0 0.0 ND 2 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,2,4-Trimethylbenzene 0.0 0.0 0.0 ND 1000 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,2-Dibromo-3-Chloropropane 0.0 0.0 0.1 ND 10 ND 0.0215 0.014 0.0155 ND 0.0 0.05

1,2-Dichlorobenzene 0.0 0.0 0.0 ND 9 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,2-Dichloroethane 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,2-Dichloropropane 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,3,5-Trimethylbenzene 0.0 0.0 0.0 ND 10 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,3-Dichlorobenzene 0.0 0.0 0.0 ND 1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,3-Dichloropropane 0.0 0.0 0.0 ND 500 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,4-Dichlorobenzene 0.0 0.0 0.0 ND 0.7 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

1,4-Dioxane 0.2 0.2 0.5 ND 0.2 ND 0.215 0.14 0.155 ND 0.2 0.51

2,2-Dichloropropane 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01

2-Butanone (MEK) 0.0 0.0 0.1 ND 4 ND 0.0215 0.014 0.0155 ND 0.0 0.05

2-Chlorotoluene 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

2-Hexanone 0.0 0.0 0.1 ND 100 ND 0.0215 0.014 0.0155 ND 0.0 0.05

4-Chlorotoluene 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01

4-Isopropyltoluene 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

4-Methyl-2-pentanone (MIBK) 0.0 0.0 0.1 ND 0.4 ND 0.0215 0.014 0.0155 ND 0.0 0.05

Acetone 0.2 0.2 0.5 ND 6 ND 0.215 0.14 0.155 ND 0.2 0.51

Benzene 0.0 0.0 0.0 ND 2 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Bromobenzene 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Bromoform 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Bromomethane 0.0 0.0 0.0 ND 0.5 ND 0.00425 0.0028 0.00315 ND 0.0 0.01

Carbon disulfide 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Carbon tetrachloride 0.0 0.0 0.0 ND 5 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Chlorobenzene 0.0 0.0 0.0 ND 1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Chlorobromomethane 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Chlorodibromomethane 0.0 0.0 0.0 ND 0.005 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Chloroethane 0.0 0.0 0.0 ND 100 ND 0.00425 0.0028 0.00315 ND 0.0 0.01

Chloroform 0.0 0.0 0.0 ND 0.3 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Chloromethane 0.0 0.0 0.0 ND 100 ND 0.00425 0.0028 0.00315 ND 0.0 0.01

cis-1,2-Dichloroethene 0.0 0.0 0.0 ND 0.3 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

cis-1,3-Dichloropropene 0.0 0.0 0.0 ND 0.01 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Dibromomethane 0.0 0.0 0.0 ND 500 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Dichlorobromomethane 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Dichlorodifluoromethane 0.0 0.0 0.0 ND 1000 ND 0.00425 0.0028 0.00315 ND 0.0 0.01

Ethyl ether 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Ethylbenzene 0.0 0.0 0.0 ND 40 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Ethylene Dibromide 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Hexachlorobutadiene 0.0 0.0 0.0 ND 6 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Isopropyl ether 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Isopropylbenzene 0.0 0.0 0.0 ND 1000 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Methyl tert-butyl ether 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Methylene Chloride 0.0 0.0 0.0 ND 0.1 ND 0.0085 0.0055 0.0065 ND 0.0 0.02

m-Xylene & p-Xylene 0.0 0.0 0.0 ND 300 ND 0.00425 0.0028 0.00315 ND 0.0 0.01

Naphthalene 0.0 0.0 0.1 ND 4 ND 0.0215 0.014 0.0155 ND 0.0 0.05

n-Butylbenzene 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01

N-Propylbenzene 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

o-Xylene 0.0 0.0 0.0 ND 300 ND 0.00215 0.0014 0.00155 ND 0.0 0.01








sec-Butylbenzene 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Styrene 0.0 0.0 0.0 ND 3 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Tert-amyl methyl ether 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Tert-butyl ethyl ether 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01

tert-Butylbenzene 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Tetrachloroethene 0.0 0.0 0.0 ND 1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Tetrahydrofuran 0.0 0.0 0.1 ND 500 ND 0.0215 0.014 0.0155 ND 0.0 0.05

Toluene 0.0 0.0 0.0 ND 30 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

trans-1,2-Dichloroethene 0.0 0.0 0.0 ND 1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

trans-1,3-Dichloropropene 0.0 0.0 0.0 ND 0.01 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Trichloroethene 0.0 0.0 0.0 ND 0.3 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

Trichlorofluoromethane 0.0 0.0 0.0 ND 1000 ND 0.00425 0.0028 0.00315 ND 0.0 0.01Vinyl chloride 0.0 0.0 0.0 ND 0.6 ND 0.00215 0.0014 0.00155 ND 0.0 0.01

GC SEMI VOA BY 8015B

Total Petroleum Hydrocarbons (C9-C36) 170.0 140.0 420.0 ND 1000 300 120 170 130 170 140.0 420.00

Pesticides BY 8081B mg/kg mg/kg mg/kg mg/kg mg/kg

4,4'-DDD 0.0 0.0 0.0 NA 4 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

4,4'-DDE 0.0 0.0 0.0 NA 3 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

4,4'-DDT 0.0 0.0 0.0 NA 3 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

Aldrin 0.0 0.0 0.0 NA 0.04 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

alpha-BHC 0.0 0.0 0.0 NA 50 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

beta-BHC 0.0 0.0 0.0 NA 10 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

Chlordane (technical) 0.3 0.3 0.8 NA 0.7 ND (<0.15) 0.275 0.28 0.28 ND 0.3 0.84

delta-BHC 0.0 0.0 0.0 NA 10 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

Dieldrin 0.0 0.0 0.0 NA 0.05 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

Endosulfan I 0.0 0.0 0.0 NA 0.5 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

Endosulfan II 0.0 0.0 0.0 NA 0.5 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

Endosulfan sulfate 0.0 0.0 0.0 NA NA ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

Endrin 0.0 0.0 0.0 NA 8 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

Endrin ketone 0.0 0.0 0.0 NA NA ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

gamma-BHC (Lindane) 0.0 0.0 0.0 NA 0.003 ND (<0.15) 0.00165 0.0017 0.0017 ND 0.0 0.01

Heptachlor 0.0 0.0 0.0 NA 0.2 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

Heptachlor epoxide 0.0 0.0 0.0 NA 0.09 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

Hexachlorobenzene 0.0 0.0 0.0 NA 0.7 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02Methoxychlor 0.0 0.0 0.0 NA 200 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02

PCBs BY 8082A mg/kg mg/kg mg/kg mg/kg mg/kg

PCB-1016 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17

PCB-1221 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17

PCB-1232 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17

PCB-1242 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17

PCB-1248 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17

PCB-1254 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17

PCB-1260 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17

PCB-1262 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17PCB-1268 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17

Herbicides BY 8151A mg/kg mg/kg mg/kg mg/kg mg/kg

2,4,5-T 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03

2,4-D 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03

2,4-DB 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03

Dalapon 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03

Dicamba 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03

Dichlorprop 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03

Dinoseb 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03

MCPA 1.0 1.0 2.9 NA NA ND (<0.03) 0.95 0.95 0.95 ND 1.0 2.85

Mecoprop 1.0 1.0 2.9 NA NA ND (<0.03) 0.95 0.95 0.95 ND 1.0 2.85Silvex (2,4,5-TP) 0.0 0.0 0.0 NA 100 ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03








METALS BY 6010B mg/kg mg/kg mg/kg mg/kg mg/kg

Antimony 0.3 0.3 0.9 1 20 0.9 0.325 0.32 0.295 ND 0.3 0.94

Arsenic 16.0 15.0 45.0 20 20 20 16 16 13 16 15.0 45.00

Beryllium 0.4 0.4 1.1 0.4 100 1.1 0.31 0.36 0.4 0.4 0.4 1.07

Cadmium 0.1 0.1 0.4 2 2 0.4 0.13 0.13 0.12 ND 0.1 0.38

Chromium 17.0 16.3 49.0 30 30 49 15 17 17 17 16.3 49.00

Copper 31.0 20.7 62.0 40 1000 62 20 31 11 31 20.7 62.00

Lead 31.0 26.3 79.0 300 300 79 31 27 21 31 26.3 79.00

Nickel 16.0 13.0 39.0 20 20 39 12 16 11 16 13.0 39.00

Selenium 0.3 0.3 0.9 0.5 400 0.9 0.325 0.32 0.295 ND 0.3 0.94

Silver 0.7 0.6 1.9 0.6 100 1.9 0.65 0.65 0.6 ND 0.6 1.90

Thallium 0.7 0.6 1.9 0.6 8 1.9 0.65 0.65 0.6 ND 0.6 1.90Zinc 37.0 35.3 106.0 100 2500 106 35 37 34 37 35.3 106.00

METALS BY 7471A mg/kg mg/kg mg/kg mg/kg mg/kg

Mercury 0.0 0.0 0.1 0.3 20 0.1 0.0385 0.0385 0.039 ND 0.0 0.12

GENERAL CHEMISTRY BY MOISTURE % % % % % 0

Percent Moisture 12.0 11.0 33.0 NA NA No Free Water 10 11 12 12 11.0 33.00Percent Solids 90.0 89.0 267.0 NA NA 90 89 88 90 89.0 267.00

GENERAL CHEMISTRY BY SM 2510B umhos/cm umhos/cm umhos/cm umhos/cm umhos/cm

Specific Conductance 500.0 370.0 1110.0 NA NA <1,000 290 500 320 500 370.0 1110.00

General Notes:

NA= Not Applicable, NS= Not Sampled

One-half the laboratory detection limit (DL) is shown in yellow and was utilized to estimate the average concentration shown.

PAHs:3 times site ave. including 1/2 Detection Limits for non-detect samples were used to calc. Acceptance Criteria.

Arsenic: Levels are somewhat elevated in Worcester County as Doc. By DEP (30 ppm or so). Value of 20 was selected but may range to 30 in natural non-impacted soils.

Otherwise soils > 20 ppm Arsenic without exempt status cannot be accepted.

Chromium: 30 is Hex Chromium Std. Chromium can be accepted to 49 ppm with demonstration hex chromium is <30 ppm.

PCBs: No PCBs < 0.10 can be accepted.

Pest/Herbs: Trace levels of pesticides/herbicides can be accepted on case-bycase basis..

Lead and TPH: These are typical constituents in fill soils. Lead value of 79 ppm used as 3X. 300 ppm TPH acceptable from asphalt and not from a fuel oil release.

Conductance: <1,000 umhos/cm can be accepted provided conc's of other metals are low enough.

Trace levels of VOCs may be accepted on case-by-case basis.

Nickel:Nickel 3X ave. was 39 and levels can be accepted up to 39 ppm from natural non-impacted, non-MCP reportable soils.

Otherwise soils > 20 ppm Nickel without exempt status cannot be accepted.

Appendix A

Section of M.G.L. Chapter 40 Section

3A

Appendix B

List of MCP Disposal Sites

Appendix C

Background Sampling Analytical Data

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica WestfieldWestfield Executive Park53 Southampton RoadWestfield, MA 01085Tel: (413)572-4000

TestAmerica Job ID: 360-34572-1Client Project/Site: 28 Ball Hill RoadRevision: 1

For:ARCADIS U.S., Inc194 Forbes RoadBraintree, Massachusetts 02184

Attn: Mr. Rick Stromberg

Authorized for release by:07/01/2011 02:58:20 PMJoe ChimiReport Production [email protected]

Designee for

Becky MasonProject Manager [email protected]

Results relate only to the items tested and the sample(s) as received by the laboratory.The test results in this report meet all 2003 NELAC requirements for accredited parameters,exceptions are noted in this report. Pursuant to NELAC, this report may not be reproducedexcept in full, and with written approval from the laboratory. For questions please contactthe Project Manager at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signatureis intended to be the legally binding equivalent of a traditionally handwritten signature.

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Table of Contents

Client: ARCADIS U.S., IncProject/Site: 28 Ball Hill Road

TestAmerica Job ID: 360-34572-1

Page 2 of 65TestAmerica Westfield

07/01/2011

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65

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Case NarrativeClient: ARCADIS U.S., Inc TestAmerica Job ID: 360-34572-1

Project/Site: 28 Ball Hill Road

Job ID: 360-34572-1

Laboratory: TestAmerica Westfield

Narrative

Revision 1: Report was revised on 07/01/2011 to report method 8270D at a lower dilution. This final report replaces the final report

generated on 06/30/2011.

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no

problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control

limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of

the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,

the reporting limits are adjusted relative to the dilution required.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the

individual sections below.

RECEIPT

The samples were received on 06/17/2011; the samples arrived in good condition, properly preserved and on ice. The temperature of the

coolers at receipt was 0.8 C.

Note: All samples which require thermal preservation are considered acceptable if the arrival temperature is within 2 C of the required

temperature or method specified range. For samples with a specified temperature of 4 C, samples with a temperature ranging from just

above freezing temperature of water to 6 C shall be acceptable. Samples that are hand delivered immediately following collection may not

meet these criteria, however they will be deemed acceptable according to NELAC and State standards, if there is evidence that the chilling

process has begun, such as arrival on ice, etc.

TestAmerica’s Reporting Limits (RLs) for this report may not always meet WSC-CAM-III method reporting limits due to various reasons

such as methodology, dilutions or moisture content (soils). TestAmerica’s MA pivot table EDD documents which compound(s) exceed

certain regulatory standards. If not included with your deliverables, please contact your Project Manager about the availability of this EDD

for your report.

VOLATILE ORGANIC COMPOUNDS (GC-MS)

Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for volatile organic

compounds (GC-MS) in accordance with SW846 8260C. The samples were prepared on 06/26/2011 and analyzed on 06/27/2011.

1,4-Dioxane exceeded the rpd limit for LCSD 360-75985/2-A. Refer to the QC report for details.

1,1,2,2-Tetrachloroethane, 2-Hexanone, 4-Methyl-2-pentanone (MIBK) and Tetrahydrofuran failed the continuing calibration verification

(CCV) criteria low; Dichlorodifluoromethane failed the criteria high.

No other difficulties were encountered during the VOC analyses.

All other quality control parameters were within the acceptance limits.

SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS)

Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for semivolatile organic

compounds (GC-MS) in accordance with SW846 8270D. The samples were prepared on 06/21/2011 and analyzed on 06/24/2011 and

06/25/2011.

Aniline failed the recovery criteria low for LCS 360-75634/2-A and LCSD 360-75634/3-A. Refer to the QC report for details.

The calibration curve used quadratic regression for 1,2,4-Trichlorobenzene, 2,4-Dimethylphenol, 2-Nitrophenol, Hexachlorobutadiene,

Isophorone and Naphthalene.

Samples PH 1 SS-1 (360-34572-1)[2X], PH 1 SS-2 (360-34572-2)[2X] and PH 1 SS-3 (360-34572-3)[2X] required dilution prior to analysis

due to black color. The reporting limits have been adjusted accordingly.

TestAmerica Westfield

Page 3 of 65 07/01/2011

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Job ID: 360-34572-1 (Continued)

Laboratory: TestAmerica Westfield (Continued)

No other difficulties were encountered during the SVOC analyses.


CHLORINATED PESTICIDES

Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for chlorinated pesticides in

accordance with EPA SW-846 Method 8081A. The samples were prepared and analyzed on 06/21/2011.

4,4'-DDD and Endrin failed the recovery criteria high for LCS 360-75557/9-A. 4,4'-DDD, 4,4'-DDE, Endrin and Heptachlor failed the

recovery criteria high for LCSD 360-75557/10-A. These analytes were not detected in the associated samples. Results would be biased

high. Refer to the QC report for details.

For the opening continuing calibration verification (CCV), 4,4’-DDT failed the criteria low (primary column only). 4,4’-DDD failed the criteria

high (primary column only) and 4,4’-DDE, Dieldrin, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin and Heptachlor failed the

criteria high (secondary column only). For the closing CCV, 4,4’-DDT and Methoxychlor failed the criteria low (primary and secondary

columns). The associated samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were re-analyzed

with similar results. The original results are reported. 4,4’-DDD and 4,4’-DDE failed the criteria high (primary column only) and Endrin

failed the criteria high (secondary column only).

No other difficulties were encountered during the pesticides analyses.


POLYCHLORINATED BIPHENYLS (PCBS)

Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for polychlorinated biphenyls

(PCBs) in accordance with SW846 8082A. The samples were prepared and analyzed on 06/21/2011.

No difficulties were encountered during the PCBs analyses.

All quality control parameters were within the acceptance limits.

CHLORINATED HERBICIDES

Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for chlorinated herbicides in

accordance with EPA SW-846 Method 8151A. The samples were prepared on 06/24/2011 and analyzed on 06/26/2011.

This analysis was performed at TestAmerica Edison, 777 New Durham Road, Edison, NJ 08817.

The following required QA/QC procedures, which may affect Presumptive Certainty, were not met: This method was performed using

laboratory in-house control limits rather than MCP program control limits.

2,4-Dichlorophenylacetic acid failed the surrogate recovery criteria high for PH 1 SS-1 (360-34572-1). No target analytes were detected in

this sample. Results would be biased high. Refer to the QC report for details.

Dinoseb failed the recovery criteria low for LCSD 460-77865/3-A. Dalapon and Dinoseb exceeded the rpd limit. Percent recoveries for the

LCS were within control limits. Refer to the QC report for details.

No other difficulties were encountered during the herbicides analyses.


TOTAL METALS (ICP)

Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for total metals (ICP) in

accordance with EPA SW-846 Method 6010B. The samples were prepared and analyzed on 06/20/2011.

At the request of the client, a modified MCP analyte list (EPA PP13 vs. WSC CAM III-A) was reported for this job.


Page 4 of 65 07/01/2011

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Job ID: 360-34572-1 (Continued)

Laboratory: TestAmerica Westfield (Continued)

No difficulties were encountered during the metals analyses.


TOTAL MERCURY

Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for total mercury in

accordance with EPA SW-846 Method 7471A. The samples were prepared and analyzed on 06/20/2011.

No difficulties were encountered during the mercury analyses.


DIESEL RANGE ORGANICS

Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for diesel range organics in

accordance with EPA SW-846 Method 8015B - DRO. The samples were prepared on 06/21/2011 and analyzed on 06/23/2011.

Samples PH 1 SS-1 (360-34572-1)[10X], PH 1 SS-2 (360-34572-2)[10X] and PH 1 SS-3 (360-34572-3)[10X] required dilution prior to

analysis due dark, black color. The reporting limits have been adjusted accordingly.

No difficulties were encountered during the DRO analyses.


PERCENT SOLIDS

Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for percent solids in

accordance with EPA Moisture. The samples were analyzed on 06/20/2011.

No difficulties were encountered during the % solids analyses.


SPECIFIC CONDUCTIVITY

Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for specific conductivity in

accordance with SM20 2510B. The samples were leached on 06/23/2011 and analyzed on 06/23/2011.

No difficulties were encountered during the conductivity analyses.



Page 5 of 65 07/01/2011

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Project #:

RTN:

Matrices: Groundwater/Surface Water Soil/Sediment Drinking Water Air

7470/7471 Hg Mass DEP VPH 8081 Pesticides 7196 Hex CrCAM III B CAM IV A CAM V B CAM VI B7010 Metals Mass DEP EPH 8151 Herbicides 8330 ExplosivesCAM III C CAM IV B CAM V C CAM VIII A

6020 Metals 8082 PCB9014 Total Cyanide/PAC 332.0 Perchlorate

CAM III D CAM V A CAM VI A CAM VIII B

A Yes No

B Yes No

C Yes No

D Yes No

Yes No

Yes No

F Yes No

G Yes No1

H Yes No

I Yes No

Signature: Position:

Printed Name: Date:

This form has been electronically signed and approved


CAM IX A

This form provides certifications for the following data set: list Laboratory Sample ID Number(s):

Project Location:

Were all QC performance standards specified in the CAM protocol(s) achieved?

1 All negative responses must be addressed in an attached laboratory narrative.

Responses to Questions G, H and I below are required for "Presumptive Certainty" status

Laboratory Name: 360-34572-1

Laboratory Director

CAM III A

CAM II B

6010 Metals

Does the laboratory report comply with all the reporting requirements specified in CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"?

b. APH and TO-15 Methods only: Was the complete analyte list reported for each method?E

Were all required corrective actions and analytical response actions specified in the selected CAM protocol(s) implemented for all identified performance standard non-conformances?

a. VPH, EPH and APH Methods only: Was each method conducted without significant modification(s)? (Refer to the individual method(s) for a list of significant modifications).

Were all applicable CAM protocol QC and performance standard non-conformances identified and evaluated in a laboratory narrative (including all "No" responses to Questions A through E)?

Steven C. Hartmann 6/28/11 15:08

MassDEP Analytical Protocol Certification Form

I, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief,

Data User Note: Data that achieve "Presumptive Certainty" status may not necessarily meet the data usability and representativeness requirements described in 310 CMR 40. 1056 (2)(k) and WCS-07-350

CAM IX B

Other:

Berlin MA

is accurate and complete.

Were the reporting limits at or below all CAM reporting limits specified in the selected CAM protocol(s)?

Were results reported for the complete analyte list specified in the selected CAM protocol(s) ?

Were the analytical method(s) and all associated QC requirements specified in the selected CAM protocol(s) followed?

TO-15 VOC

CAM Protocols (check all that apply below):

360-34572-(1-3)

Were all samples received in a condition consistent with those described on the Chain-of-Custody, properly preserved (including temperature) in the field or laboratory, and prepared/analyzed within method holding time.

8270 SVOC

8260 VOCCAM II A

Mass DEP APH

Affirmative Responses to Questions A through F are required for "Presumptive Certainty" status

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

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Project #:

RTN:

Matrices: Groundwater/Surface Water Soil/Sediment Drinking Water Air

7470/7471 Hg Mass DEP VPH 8081 Pesticides 7196 Hex Cr

CAM III B CAM IV A CAM V B CAM VI B7010 Metals Mass DEP EPH 8151 Herbicides 8330 Explosives

CAM III C CAM IV B CAM V C CAM VIII A

6020 Metals 8082 PCB9014 Total Cyanide/PAC 332.0 Perchlorate

CAM III D CAM V A CAM VI A CAM VIII B

A Yes No

B Yes No

C Yes No

D Yes No

Yes No

Yes No

F Yes No

G Yes No1

H Yes No

I Yes No

Signature: Position:

Printed Name: Date:

MassDEP Analytical Protocol Certification Form

I, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief,

Data User Note: Data that achieve "Presumptive Certainty" status may not necessarily meet the data usability and representativeness requirements described in 310 CMR 40. 1056 (2)(k) and WCS-07-350

CAM IX B

Other:

a. VPH, EPH and APH Methods only: Was each method conducted without significant modification(s)? (Refer to the individual method(s) for a list of significant modifications). E

TestAmerica Edison

CAM II B

6010 Metals

Does the laboratory report comply with all the reporting requirements specified in CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"?

Were all required corrective actions and analytical response actions specified in the selected CAM protocol(s) implemented for all identified performance standard non-conformances?

Affirmative Responses to Questions A through F are required for "Presumptive Certainty" status

Were all samples received in a condition consistent with those described on the Chain-of-Custody, properly preserved (including temperature) in the field or laboratory, and prepared/analyzed within method holding time.

Were the analytical method(s) and all associated QC requirements specified in the selected CAM protocol(s) followed?

Catalina Dalangin

GC SemiVolatiles Manager II

is accurate and complete.

CAM III A

b. APH and TO-15 Methods only: Was the complete analyte list reported for each method?

Were all applicable CAM protocol QC and performance standard non-conformances identified and evaluated in a laboratory narrative (including all "No" responses to Questions A through E)?

CAM IX ATO-15 VOC

CAM Protocols (check all that apply below):

6/29/11 0:00

Were all QC performance standards specified in the CAM protocol(s) achieved?

1 All negative responses must be addressed in an attached laboratory narrative.

Responses to Questions G, H and I below are required for "Presumptive Certainty" status

Were the reporting limits at or below all CAM reporting limits specified in the selected CAM protocol(s)?

Were results reported for the complete analyte list specified in the selected CAM protocol(s) ?

360-34572-1, 360-34572-2 and 360-34572-3

Laboratory Name:

8270 SVOC

8260 VOC

CAM II A

This form provides certifications for the following data set: list Laboratory Sample ID Number(s):

Project Location:

360-34572-1

28 Ball Hill Road

Mass DEP APH

X

X

X

X

X

X

X

X

X

X

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Detection SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


Client Sample ID: PH 1 SS-1 Lab Sample ID: 360-34572-1

Analyte Result Qualifier Unit Method Prep TypeD

☼

Dil Fac

Benzo[a]anthracene 380

RL

370 ug/Kg 8270D Total/NA2

MDL

☼Benzo[a]pyrene 8270D Total/NA470 370 ug/Kg 2

☼Benzo[b]fluoranthene 8270D Total/NA680 370 ug/Kg 2

☼Bis(2-ethylhexyl) phthalate 8270D Total/NA3100 740 ug/Kg 2

☼Chrysene 8270D Total/NA530 370 ug/Kg 2

☼Fluoranthene 8270D Total/NA860 370 ug/Kg 2

☼Phenanthrene 8270D Total/NA430 370 ug/Kg 2

☼Pyrene 8270D Total/NA760 370 ug/Kg 2

☼Arsenic 6010B Total/NA16 1.3 mg/Kg 1

☼Beryllium 6010B Total/NA0.31 0.26 mg/Kg 1

☼Chromium 6010B Total/NA15 0.65 mg/Kg 1

☼Copper 6010B Total/NA20 2.6 mg/Kg 1

☼Nickel 6010B Total/NA12 2.6 mg/Kg 1

☼Lead 6010B Total/NA31 0.65 mg/Kg 1

☼Zinc 6010B Total/NA35 3.3 mg/Kg 1


☼

Dil Fac

Total Petroleum Hydrocarbons

(C9-C36)

120

RL

36 mg/Kg 8015B Total/NA10

RL

Specific Conductance SM 2510B Soluble290 3.9 umhos/cm 1



☼

Dil Fac


RL


MDL



☼Benzo[g,h,i]perylene 8270D Total/NA640 370 ug/Kg 2

☼Benzo[k]fluoranthene 8270D Total/NA520 390 ug/Kg 2


☼Fluoranthene 8270D Total/NA2600 370 ug/Kg 2










☼Mercury 7471A Total/NA0.077 0.071 mg/Kg 1


☼

Dil Fac


(C9-C36)

170

RL


RL




☼

Dil Fac


RL


MDL



☼Benzo[g,h,i]perylene 8270D Total/NA410 380 ug/Kg 2

☼Benzo[k]fluoranthene 8270D Total/NA440 400 ug/Kg 2



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Detection SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


Client Sample ID: PH 1 SS-3 (Continued) Lab Sample ID: 360-34572-3


☼

Dil Fac

Fluoranthene 1300

RL


MDL











☼

Dil Fac


(C9-C36)

130

RL


RL



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Method SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


Method Method Description LaboratoryProtocol

MA DEP8260C Volatile Organic Compounds (GC/MS) TAL WFD

MA DEP8270D Semivolatile Organic Compounds (GC/MS) TAL WFD

SW8468015B 8100M (Modified) Total Extractable Petroleum Hydrocarbons TAL WFD

MA DEP8081B Organochlorine Pesticides (GC/ECD) TAL WFD

MA DEP8082A Polychlorinated Biphenyls (GC/ECD) TAL WFD

SW8468151A Herbicides (GC) TAL EDI

SW8466010B Metals (ICP) TAL WFD

SW8467471A Mercury (CVAA) TAL WFD

EPAMoisture Percent Moisture TAL WFD

SMSM 2510B Conductivity, Specific Conductance TAL WFD

Protocol References:

EPA = US Environmental Protection Agency

MA DEP = Massachusetts Department Of Environmental Protection

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL EDI = TestAmerica Edison, 777 New Durham Road, Edison, NJ 08817, TEL (732)549-3900

TAL WFD = TestAmerica Westfield, Westfield Executive Park, 53 Southampton Road, Westfield, MA 01085, TEL (413)572-4000


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Sample SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

360-34572-1 PH 1 SS-1 Solid 06/16/11 14:00 06/17/11 16:55

360-34572-2 PH 1 SS-2 Solid 06/16/11 14:00 06/17/11 16:55

360-34572-3 PH 1 SS-3 Solid 06/16/11 14:00 06/17/11 16:55


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Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


Method: 8260C - Volatile Organic Compounds (GC/MS)

Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1

Matrix: SolidDate Collected: 06/16/11 14:00

Percent Solids: 89.9Date Received: 06/17/11 16:55

Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac

1,1,1,2-Tetrachloroethane ND 4.3 ug/Kg ☼ 06/26/11 10:49 06/27/11 07:50 1

Analyte

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1,1-Trichloroethane ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1,2,2-Tetrachloroethane ND


4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1-Dichloroethane ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1-Dichloroethene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1-Dichloropropene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2,3-Trichlorobenzene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2,3-Trichloropropane ND


4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2,4-Trimethylbenzene ND

43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2-Dibromo-3-Chloropropane ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2-Dichlorobenzene ND


4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2-Dichloropropane ND





430 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,4-Dioxane ND *


43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼2-Butanone (MEK) ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼2-Chlorotoluene ND

43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼2-Hexanone ND


4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼4-Isopropyltoluene ND

43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼4-Methyl-2-pentanone (MIBK) ND

430 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Acetone ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Benzene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Bromobenzene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Bromoform ND

8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Bromomethane ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Carbon disulfide ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Carbon tetrachloride ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chlorobenzene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chlorobromomethane ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chlorodibromomethane ND

8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chloroethane ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chloroform ND

8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chloromethane ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼cis-1,2-Dichloroethene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼cis-1,3-Dichloropropene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Dibromomethane ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Dichlorobromomethane ND

8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Dichlorodifluoromethane ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Ethyl ether ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Ethylbenzene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Ethylene Dibromide ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Hexachlorobutadiene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Isopropyl ether ND


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Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)





Isopropylbenzene ND 4.3 ug/Kg ☼ 06/26/11 10:49 06/27/11 07:50 1

Analyte

8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼m-Xylene & p-Xylene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Methyl tert-butyl ether ND

17 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Methylene Chloride ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼n-Butylbenzene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼N-Propylbenzene ND

43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Naphthalene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼o-Xylene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼sec-Butylbenzene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Styrene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Tert-amyl methyl ether ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Tert-butyl ethyl ether ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼tert-Butylbenzene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Tetrachloroethene ND

43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Tetrahydrofuran ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Toluene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼trans-1,2-Dichloroethene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼trans-1,3-Dichloropropene ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Trichloroethene ND

8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Trichlorofluoromethane ND

4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Vinyl chloride ND

Qualifier Prepared Analyzed Dil Fac % Recovery Limits

4-Bromofluorobenzene 108 70 - 130 06/26/11 10:49 06/27/11 07:50 1

Surrogate

Dibromofluoromethane 108 06/26/11 10:49 06/27/11 07:50 170 - 130

Toluene-d8 (Surr) 103 06/26/11 10:49 06/27/11 07:50 170 - 130






Analyte



















280 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,4-Dioxane ND *


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2,2-Dichloropropane ND 2.8 ug/Kg ☼ 06/26/11 10:49 06/27/11 08:14 1

Analyte



28 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼2-Hexanone ND




280 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Acetone ND

2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Benzene ND












2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼cis-1,2-Dichloroethene ND










2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Isopropylbenzene ND







2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼o-Xylene ND


2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Styrene ND






2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Toluene ND






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Vinyl chloride ND 2.8 ug/Kg ☼ 06/26/11 10:49 06/27/11 08:14 1

Analyte



Surrogate


Toluene-d8 (Surr) 102 06/26/11 10:49 06/27/11 08:14 170 - 130






Analyte



















310 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,4-Dioxane ND *




31 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼2-Hexanone ND




310 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Acetone ND

3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Benzene ND













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cis-1,2-Dichloroethene ND 3.1 ug/Kg ☼ 06/26/11 10:49 06/27/11 08:39 1

Analyte










3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Isopropylbenzene ND







3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼o-Xylene ND


3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Styrene ND






3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Toluene ND





3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Vinyl chloride ND



Surrogate


Toluene-d8 (Surr) 105 06/26/11 10:49 06/27/11 08:39 170 - 130


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Method: 8270D - Semivolatile Organic Compounds (GC/MS)





1,2,4-Trichlorobenzene ND 740 ug/Kg ☼ 06/21/11 11:45 06/30/11 16:56 2

Analyte

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼1,2-Dichlorobenzene ND



740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,2'-oxybis[1-chloropropane] ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4,5-Trichlorophenol ND


740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4-Dichlorophenol ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4-Dimethylphenol ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4-Dinitrophenol ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4-Dinitrotoluene ND


740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2-Chloronaphthalene ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2-Chlorophenol ND

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2-Methylnaphthalene ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2-Methylphenol ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2-Nitrophenol ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼3 & 4 Methylphenol ND

1500 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼3,3'-Dichlorobenzidine ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼4-Bromophenyl phenyl ether ND

1500 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼4-Chloroaniline ND


370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Acenaphthene ND

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Acenaphthylene ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Acetophenone ND

3700 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Aniline ND *

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Anthracene ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Azobenzene ND

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Benzo[a]anthracene 380

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Benzo[a]pyrene 470

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Benzo[b]fluoranthene 680

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Benzo[g,h,i]perylene ND

390 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Benzo[k]fluoranthene ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Bis(2-chloroethoxy)methane ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Bis(2-chloroethyl)ether ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Bis(2-ethylhexyl) phthalate 3100

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Butyl benzyl phthalate ND

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Chrysene 530

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Di-n-butyl phthalate ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Di-n-octyl phthalate ND

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Dibenz(a,h)anthracene ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Dibenzofuran ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Diethyl phthalate ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Dimethyl phthalate ND

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Fluoranthene 860

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Fluorene ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Hexachlorobenzene ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Hexachlorobutadiene ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Hexachloroethane ND

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Indeno[1,2,3-cd]pyrene ND


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Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)





Isophorone ND 740 ug/Kg ☼ 06/21/11 11:45 06/30/11 16:56 2

Analyte


740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Nitrobenzene ND

3700 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Pentachlorophenol ND

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Phenanthrene 430

740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Phenol ND

370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Pyrene 760


2,4,6-Tribromophenol 38 30 - 130 06/21/11 11:45 06/30/11 16:56 2

Surrogate

2-Fluorophenol 41 06/21/11 11:45 06/30/11 16:56 230 - 130

Nitrobenzene-d5 41 06/21/11 11:45 06/30/11 16:56 230 - 130

Phenol-d5 37 06/21/11 11:45 06/30/11 16:56 230 - 130

Terphenyl-d14 40 06/21/11 11:45 06/30/11 16:56 230 - 130

2-Fluorobiphenyl 41 06/21/11 11:45 06/30/11 16:56 230 - 130






Analyte












740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2-Chloronaphthalene ND













3700 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Aniline ND *







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Benzo[g,h,i]perylene 640 370 ug/Kg ☼ 06/21/11 11:45 06/30/11 17:30 2

Analyte

390 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Benzo[k]fluoranthene 520



740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Bis(2-ethylhexyl) phthalate ND


370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Chrysene 1100








370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Fluorene ND





740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Isophorone ND





740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Phenol ND

370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Pyrene 1900


2,4,6-Tribromophenol 45 30 - 130 06/21/11 11:45 06/30/11 17:30 2

Surrogate

2-Fluorophenol 48 06/21/11 11:45 06/30/11 17:30 230 - 130

Nitrobenzene-d5 45 06/21/11 11:45 06/30/11 17:30 230 - 130

Phenol-d5 44 06/21/11 11:45 06/30/11 17:30 230 - 130

Terphenyl-d14 49 06/21/11 11:45 06/30/11 17:30 230 - 130

2-Fluorobiphenyl 46 06/21/11 11:45 06/30/11 17:30 230 - 130






Analyte













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2-Chloronaphthalene ND 750 ug/Kg ☼ 06/21/11 11:45 06/30/11 18:05 2

Analyte













3800 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Aniline ND *






380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Benzo[g,h,i]perylene 410

400 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Benzo[k]fluoranthene 440



750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Bis(2-ethylhexyl) phthalate ND


380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Chrysene 680








380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Fluorene ND





750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Isophorone ND





750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Phenol ND

380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Pyrene 1100


2,4,6-Tribromophenol 41 30 - 130 06/21/11 11:45 06/30/11 18:05 2

Surrogate

2-Fluorophenol 44 06/21/11 11:45 06/30/11 18:05 230 - 130

Nitrobenzene-d5 41 06/21/11 11:45 06/30/11 18:05 230 - 130

Phenol-d5 42 06/21/11 11:45 06/30/11 18:05 230 - 130


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Terphenyl-d14 46 30 - 130 06/21/11 11:45 06/30/11 18:05 2

Surrogate

2-Fluorobiphenyl 43 06/21/11 11:45 06/30/11 18:05 230 - 130


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Method: 8015B - 8100M (Modified) Total Extractable Petroleum Hydrocarbons




Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac


(C9-C36)

120 36 mg/Kg ☼ 06/21/11 10:12 06/23/11 13:12 10

Analyte


o-Terphenyl 73 40 - 140 06/21/11 10:12 06/23/11 13:12 10

Surrogate






(C9-C36)

170 36 mg/Kg ☼ 06/21/11 10:12 06/23/11 13:43 10

Analyte


o-Terphenyl 63 40 - 140 06/21/11 10:12 06/23/11 13:43 10

Surrogate






(C9-C36)

130 37 mg/Kg ☼ 06/21/11 10:12 06/23/11 14:15 10

Analyte


o-Terphenyl 99 40 - 140 06/21/11 10:12 06/23/11 14:15 10

Surrogate


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Method: 8081B - Organochlorine Pesticides (GC/ECD)





4,4'-DDD ND * 11 ug/Kg ☼ 06/21/11 09:51 06/21/11 17:19 1

Analyte

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼4,4'-DDE ND *

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼4,4'-DDT ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Aldrin ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼alpha-BHC ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼beta-BHC ND

3.3 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼gamma-BHC (Lindane) ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼delta-BHC ND

550 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Chlordane (technical) ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Dieldrin ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Endosulfan I ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Endosulfan II ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Endosulfan sulfate ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Endrin ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Endrin ketone ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Heptachlor ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Heptachlor epoxide ND


11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Methoxychlor ND


Tetrachloro-m-xylene 86 30 - 150 06/21/11 09:51 06/21/11 17:19 1

Surrogate

Tetrachloro-m-xylene 78 06/21/11 09:51 06/21/11 17:19 130 - 150

DCB Decachlorobiphenyl 97 06/21/11 09:51 06/21/11 17:19 130 - 150






4,4'-DDD ND * 11 ug/Kg ☼ 06/21/11 09:51 06/21/11 17:40 1

Analyte

11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼4,4'-DDE ND *

11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼4,4'-DDT ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Aldrin ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼alpha-BHC ND

11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼beta-BHC ND


11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼delta-BHC ND


11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Dieldrin ND




11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Endrin ND







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Method: 8081B - Organochlorine Pesticides (GC/ECD) (Continued)



Surrogate








4,4'-DDD ND * 11 ug/Kg ☼ 06/21/11 09:51 06/21/11 18:02 1

Analyte

11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼4,4'-DDE ND *

11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼4,4'-DDT ND

11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Aldrin ND

11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼alpha-BHC ND

11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼beta-BHC ND


11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼delta-BHC ND


11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Dieldrin ND




11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Endrin ND








Surrogate





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Method: 8082A - Polychlorinated Biphenyls (GC/ECD)





PCB-1016 ND 110 ug/Kg ☼ 06/21/11 09:51 06/21/11 17:12 1

Analyte

110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1221 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1232 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1242 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1248 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1254 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1260 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1262 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1268 ND



Surrogate








PCB-1016 ND 110 ug/Kg ☼ 06/21/11 09:51 06/21/11 17:34 1

Analyte

110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1221 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1232 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1242 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1248 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1254 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1260 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1262 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1268 ND



Surrogate








PCB-1016 ND 110 ug/Kg ☼ 06/21/11 09:51 06/21/11 17:56 1

Analyte

110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1221 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1232 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1242 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1248 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1254 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1260 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1262 ND

110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1268 ND



Surrogate


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Method: 8082A - Polychlorinated Biphenyls (GC/ECD) (Continued)






Surrogate




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Method: 8151A - Herbicides (GC)





Dalapon ND * 19 ug/Kg ☼ 06/24/11 10:56 06/26/11 20:50 1

Analyte

19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼Dicamba ND

19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼Dichlorprop ND

19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼2,4-D ND

19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼2,4-DB ND

19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼Silvex (2,4,5-TP) ND

19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼2,4,5-T ND

19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼Dinoseb ND *

1900 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼MCPA ND

1900 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼Mecoprop ND


2,4-Dichlorophenylacetic acid 137 101 - 150 06/24/11 10:56 06/26/11 20:50 1

Surrogate

2,4-Dichlorophenylacetic acid 173 X 06/24/11 10:56 06/26/11 20:50 1101 - 150





Dalapon ND * 19 ug/Kg ☼ 06/24/11 10:56 06/26/11 21:21 1

Analyte

19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼Dicamba ND


19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼2,4-D ND

19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼2,4-DB ND

19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼Silvex (2,4,5-TP) ND

19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼2,4,5-T ND

19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼Dinoseb ND *

1900 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼MCPA ND

1900 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼Mecoprop ND



Surrogate

2,4-Dichlorophenylacetic acid 149 06/24/11 10:56 06/26/11 21:21 1101 - 150





Dalapon ND * 19 ug/Kg ☼ 06/24/11 10:56 06/26/11 21:51 1

Analyte

19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼Dicamba ND


19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼2,4-D ND

19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼2,4-DB ND

19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼Silvex (2,4,5-TP) ND

19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼2,4,5-T ND

19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼Dinoseb ND *

1900 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼MCPA ND

1900 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼Mecoprop ND



Surrogate

2,4-Dichlorophenylacetic acid 146 06/24/11 10:56 06/26/11 21:51 1101 - 150


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Method: 6010B - Metals (ICP)





Silver ND 1.3 mg/Kg ☼ 06/20/11 07:33 06/20/11 16:09 1

Analyte

1.3 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Arsenic 16

0.26 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Beryllium 0.31

0.26 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Cadmium ND

0.65 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Chromium 15

2.6 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Copper 20

2.6 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Nickel 12

0.65 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Lead 31

0.65 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Selenium ND

1.3 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Thallium ND

3.3 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Zinc 35

0.65 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Antimony ND





Silver ND 1.3 mg/Kg ☼ 06/20/11 07:33 06/20/11 16:12 1

Analyte

1.3 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Arsenic 16

0.26 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Beryllium 0.36

0.26 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Cadmium ND

0.64 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Chromium 17

2.6 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Copper 31

2.6 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Nickel 16

0.64 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Lead 27

0.64 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Selenium ND

1.3 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Thallium ND

3.2 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Zinc 37

0.64 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Antimony ND





Silver ND 1.2 mg/Kg ☼ 06/20/11 07:33 06/20/11 16:15 1

Analyte

1.2 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Arsenic 13

0.24 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Beryllium 0.40

0.24 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Cadmium ND

0.59 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Chromium 17

2.4 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Copper 11

2.4 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Nickel 11

0.59 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Lead 21

0.59 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Selenium ND

1.2 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Thallium ND

3.0 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Zinc 34

0.59 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Antimony ND


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Method: 7471A - Mercury (CVAA)





Mercury ND 0.077 mg/Kg ☼ 06/20/11 10:07 06/20/11 15:08 1

Analyte





Mercury 0.077 0.071 mg/Kg ☼ 06/20/11 10:07 06/20/11 15:10 1

Analyte





Mercury ND 0.078 mg/Kg ☼ 06/20/11 10:07 06/20/11 15:12 1

Analyte


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General Chemistry



Date Received: 06/17/11 16:55


Percent Moisture 10 1.0 % 06/20/11 11:46 1

Analyte

1.0 % 06/20/11 11:46 1Percent Solids 90






Analyte

1.0 % 06/20/11 11:46 1Percent Solids 89






Analyte

1.0 % 06/20/11 11:46 1Percent Solids 88


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General Chemistry - Soluble





Specific Conductance 290 3.9 umhos/cm 06/23/11 14:00 1

Analyte






Analyte






Analyte


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Definitions/GlossaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


Qualifiers

GC/MS VOA

Qualifier Description

* RPD of the LCS and LCSD exceeds the control limits

Qualifier

GC/MS Semi VOA


* LCS or LCSD exceeds the control limits

Qualifier

GC Semi VOA


* LCS or LCSD exceeds the control limits

Qualifier

* RPD of the LCS and LCSD exceeds the control limits

E Result exceeded calibration range.

X Surrogate is outside control limits

Glossary

These commonly used abbreviations may or may not be present in this report.

☼ Listed under the "D" column to designate that the result is reported on a dry weight basis.

Abbreviation

EPA United States Environmental Protection Agency

ND Not Detected above the reporting level.

MDL Method Detection Limit

RL Reporting Limit

RE, RE1 (etc.) Indicates a Re-extraction or Reanalysis of the sample.

%R Percent Recovery

RPD Relative Percent Difference, a measure of the relative difference between two points.


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QC Association SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


GC/MS VOA

Prep Batch: 75985

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Total/NA Solid 5035LCS 360-75985/1-A Lab Control Sample

Total/NA Solid 5035LCSD 360-75985/2-A Lab Control Sample Dup

Total/NA Solid 5035MB 360-75985/3-A Method Blank

Total/NA Solid 5035360-34572-1 PH 1 SS-1



Analysis Batch: 75986


Total/NA Solid 8260C 75985LCS 360-75985/1-A Lab Control Sample

Total/NA Solid 8260C 75985LCSD 360-75985/2-A Lab Control Sample Dup

Total/NA Solid 8260C 75985MB 360-75985/3-A Method Blank

Total/NA Solid 8260C 75985360-34572-1 PH 1 SS-1



GC/MS Semi VOA

Prep Batch: 75634










Total/NA Solid 8270D 75634MB 360-75634/1-A Method Blank

Total/NA Solid 8270D 75634LCS 360-75634/2-A Lab Control Sample

Total/NA Solid 8270D 75634LCSD 360-75634/3-A Lab Control Sample Dup



Total/NA Solid 8270D 75634360-34572-1 PH 1 SS-1



GC Semi VOA



Total/NA Solid 8082A 75557MB 360-75557/1-A Method Blank

Total/NA Solid 8082A 75557LCS 360-75557/2-A Lab Control Sample

Total/NA Solid 8082A 75557LCSD 360-75557/3-A Lab Control Sample Dup

Prep Batch: 75555






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GC Semi VOA (Continued)

Prep Batch: 75555 (Continued)





Prep Batch: 75557
















Total/NA Solid 8015B 75555MB 360-75555/1-A Method Blank

Total/NA Solid 8015B 75555LCS 360-75555/2-A Lab Control Sample

Total/NA Solid 8015B 75555LCSD 360-75555/3-A Lab Control Sample Dup



Total/NA Solid 8082A 75557360-34572-1 PH 1 SS-1






Total/NA Solid 8081B 75557LCS 360-75557/9-A Lab Control Sample

Total/NA Solid 8081B 75557LCSD 360-75557/10-A Lab Control Sample Dup

Total/NA Solid 8081B 75557360-34572-1 PH 1 SS-1








Prep Batch: 77865


Total/NA Solid 8151AMB 460-77865/1-A Method Blank

Total/NA Solid 8151ALCS 460-77865/2-A Lab Control Sample

Total/NA Solid 8151ALCSD 460-77865/3-A Lab Control Sample Dup

Total/NA Solid 8151A360-34572-1 PH 1 SS-1


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GC Semi VOA (Continued)

Prep Batch: 77865 (Continued)









Total/NA Solid 8151A 77865LCS 460-77865/2-A Lab Control Sample

Total/NA Solid 8151A 77865LCSD 460-77865/3-A Lab Control Sample Dup


Metals

Prep Batch: 75498


Total/NA Solid 3050BMB 360-75498/1-A Method Blank

Total/NA Solid 3050BLCSSRM 360-75498/2-A Lab Control Sample

Total/NA Solid 3050BLCDSRM 360-75498/3-A LCDSRMLab Control Sample Dup

Total/NA Solid 3050B360-34572-1 PH 1 SS-1



Prep Batch: 75533


Total/NA Solid 7471AMB 360-75533/1-A Method Blank

Total/NA Solid 7471ALCSSRM 360-75533/2-A Lab Control Sample

Total/NA Solid 7471ALCDSRM 360-75533/3-A LCDSRMLab Control Sample Dup







Total/NA Solid 7471A 75533LCSSRM 360-75533/2-A Lab Control Sample

Total/NA Solid 7471A 75533LCDSRM 360-75533/3-A LCDSRMLab Control Sample Dup







Total/NA Solid 6010B 75498LCSSRM 360-75498/2-A Lab Control Sample

Total/NA Solid 6010B 75498LCDSRM 360-75498/3-A LCDSRMLab Control Sample Dup





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General Chemistry



Total/NA Solid Moisture360-34572-1 PH 1 SS-1



Leach Batch: 75814


Soluble Solid DI LeachMB 360-75814/1-A Method Blank

Soluble Solid DI LeachLCS 360-75814/2-A Lab Control Sample

Soluble Solid DI Leach360-34572-1 PH 1 SS-1





Soluble Solid SM 2510BMB 360-75814/1-A Method Blank

Soluble Solid SM 2510BLCS 360-75814/2-A Lab Control Sample

Soluble Solid SM 2510B360-34572-1 PH 1 SS-1




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Surrogate SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


Method: 8260C - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (70-130) (70-130) (70-130)

BFB DBFM TOL

108 108 103360-34572-1

Percent Surrogate Recovery (Acceptance Limits)

PH 1 SS-1

105 107 102360-34572-2 PH 1 SS-2

108 107 105360-34572-3 PH 1 SS-3

114 105 109LCS 360-75985/1-A Lab Control Sample

112 105 107LCSD 360-75985/2-A Lab Control Sample Dup

118 109 106MB 360-75985/3-A Method Blank

Surrogate Legend

BFB = 4-Bromofluorobenzene

DBFM = Dibromofluoromethane

TOL = Toluene-d8 (Surr)

Method: 8270D - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (30-130) (30-130) (30-130) (30-130) (30-130) (30-130)

TBP 2FP NBZ PHL TPH FBP

38 41 41 37 40 41360-34572-1


PH 1 SS-1

45 48 45 4944 46360-34572-2 PH 1 SS-2

41 44 41 4642 43360-34572-3 PH 1 SS-3

63 61 59 6562 62LCS 360-75634/2-A Lab Control Sample

63 62 61 6562 63LCSD 360-75634/3-A Lab Control Sample Dup

61 65 63 6564 61MB 360-75634/1-A Method Blank

Surrogate Legend

TBP = 2,4,6-Tribromophenol

2FP = 2-Fluorophenol

NBZ = Nitrobenzene-d5

PHL = Phenol-d5

TPH = Terphenyl-d14

FBP = 2-Fluorobiphenyl

Method: 8015B - 8100M (Modified) Total Extractable Petroleum HydrocarbonsPrep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (40-140)

OTPH1

73360-34572-1


PH 1 SS-1

63360-34572-2 PH 1 SS-2

99360-34572-3 PH 1 SS-3

80LCS 360-75555/2-A Lab Control Sample

86LCSD 360-75555/3-A Lab Control Sample Dup

83MB 360-75555/1-A Method Blank

Surrogate Legend

OTPH = o-Terphenyl


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Surrogate SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


Method: 8081B - Organochlorine Pesticides (GC/ECD)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (30-150) (30-150) (30-150) (30-150)

TCX1 TCX2 DCB1 DCB2

86 78 97 110360-34572-1


PH 1 SS-1

90 80 115 118360-34572-2 PH 1 SS-2

86 77 110 110360-34572-3 PH 1 SS-3

87 88 86 102LCS 360-75557/9-A Lab Control Sample

95 94 89 110LCSD 360-75557/10-A Lab Control Sample Dup

87 90 83 97MB 360-75557/1-A Method Blank

Surrogate Legend

TCX = Tetrachloro-m-xylene

DCB = DCB Decachlorobiphenyl

Method: 8082A - Polychlorinated Biphenyls (GC/ECD)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (30-150) (30-150) (30-150) (30-150)

TCX1 TCX2 DCB1 DCB2

82 91 83 89360-34572-1


PH 1 SS-1

86 95 82 84360-34572-2 PH 1 SS-2

78 93 81 84360-34572-3 PH 1 SS-3

93 82 101 94LCS 360-75557/2-A Lab Control Sample

98 86 101 98LCSD 360-75557/3-A Lab Control Sample Dup

91 85 99 93MB 360-75557/1-A Method Blank

Surrogate Legend

TCX = Tetrachloro-m-xylene

DCB = DCB Decachlorobiphenyl

Method: 8151A - Herbicides (GC)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (101-150) (101-150)

DCPA1 DCPA2

137 173 X360-34572-1


PH 1 SS-1

136 149360-34572-2 PH 1 SS-2

142 146360-34572-3 PH 1 SS-3

118 135LCS 460-77865/2-A Lab Control Sample

109 118LCSD 460-77865/3-A Lab Control Sample Dup

142 121MB 460-77865/1-A Method Blank

Surrogate Legend

DCPA = 2,4-Dichlorophenylacetic acid


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QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


Method: 8260C - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 360-75985/3-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 75986 Prep Batch: 75985

Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL

1,1,1,2-Tetrachloroethane ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1

MB MB

Analyte

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1,1-Trichloroethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1,2,2-Tetrachloroethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1,2-Trichloroethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1-Dichloroethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1-Dichloroethene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1-Dichloropropene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2,3-Trichlorobenzene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2,3-Trichloropropane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2,4-Trichlorobenzene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2,4-Trimethylbenzene

ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2-Dibromo-3-Chloropropane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2-Dichlorobenzene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2-Dichloroethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2-Dichloropropane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,3,5-Trimethylbenzene




ND 250 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,4-Dioxane


ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 12-Butanone (MEK)

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 12-Chlorotoluene

ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 12-Hexanone

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 14-Chlorotoluene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 14-Isopropyltoluene

ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 14-Methyl-2-pentanone (MIBK)

ND 250 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Acetone

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Benzene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Bromobenzene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Bromoform

ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Bromomethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Carbon disulfide

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Carbon tetrachloride

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chlorobenzene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chlorobromomethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chlorodibromomethane

ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chloroethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chloroform

ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chloromethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1cis-1,2-Dichloroethene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1cis-1,3-Dichloropropene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Dibromomethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Dichlorobromomethane

ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Dichlorodifluoromethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Ethyl ether

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Ethylbenzene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Ethylene Dibromide

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Hexachlorobutadiene


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Isopropyl ether ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1

MB MB

Analyte

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Isopropylbenzene

ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1m-Xylene & p-Xylene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Methyl tert-butyl ether

ND 10 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Methylene Chloride

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1n-Butylbenzene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1N-Propylbenzene

ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Naphthalene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1o-Xylene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1sec-Butylbenzene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Styrene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Tert-amyl methyl ether

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Tert-butyl ethyl ether

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1tert-Butylbenzene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Tetrachloroethene

ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Tetrahydrofuran

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Toluene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1trans-1,2-Dichloroethene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1trans-1,3-Dichloropropene

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Trichloroethene

ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Trichlorofluoromethane

ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Vinyl chloride

% Recovery Qualifier Prepared Analyzed Dil FacLimits

4-Bromofluorobenzene 118 70 - 130 06/27/11 04:14 1

MB MB

Surrogate

06/26/11 10:49

109 06/26/11 10:49 06/27/11 04:14 1Dibromofluoromethane 70 - 130

106 06/26/11 10:49 06/27/11 04:14 1Toluene-d8 (Surr) 70 - 130

Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75985/1-A



Spike

Added Result Qualifier Unit % Rec

% Rec.

Limits

1,1,1,2-Tetrachloroethane 100 101 ug/Kg 101 70 - 130

DAnalyte

LCS LCS

1,1,1-Trichloroethane 100 104 ug/Kg 104 70 - 130

1,1,2,2-Tetrachloroethane 100 74.0 ug/Kg 74 70 - 130

1,1,2-Trichloroethane 100 96.0 ug/Kg 96 70 - 130

1,1-Dichloroethane 100 104 ug/Kg 104 70 - 130

1,1-Dichloroethene 100 97.0 ug/Kg 97 70 - 130

1,1-Dichloropropene 100 93.5 ug/Kg 94 70 - 130

1,2,3-Trichlorobenzene 100 106 ug/Kg 106 70 - 130

1,2,3-Trichloropropane 100 101 ug/Kg 101 70 - 130


1,2,4-Trimethylbenzene 100 102 ug/Kg 102 70 - 130

1,2-Dibromo-3-Chloropropane 100 109 ug/Kg 109 70 - 130

1,2-Dichlorobenzene 100 94.5 ug/Kg 95 70 - 130

1,2-Dichloroethane 100 97.0 ug/Kg 97 70 - 130

1,2-Dichloropropane 100 87.5 ug/Kg 88 70 - 130

1,3,5-Trimethylbenzene 100 96.0 ug/Kg 96 70 - 130


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Spike


% Rec.

Limits


DAnalyte

LCS LCS



1,4-Dioxane 1000 931 ug/Kg 93 70 - 130


2-Butanone (MEK) 1000 805 ug/Kg 81 70 - 130

2-Chlorotoluene 100 94.0 ug/Kg 94 70 - 130

2-Hexanone 1000 766 ug/Kg 77 70 - 130

4-Chlorotoluene 100 97.0 ug/Kg 97 70 - 130

4-Isopropyltoluene 100 103 ug/Kg 103 70 - 130

4-Methyl-2-pentanone (MIBK) 1000 738 ug/Kg 74 70 - 130

Acetone 1000 899 ug/Kg 90 70 - 130

Benzene 100 94.0 ug/Kg 94 70 - 130

Bromobenzene 100 85.5 ug/Kg 86 70 - 130

Bromoform 100 94.0 ug/Kg 94 70 - 130

Bromomethane 100 84.5 ug/Kg 85 70 - 130

Carbon disulfide 100 119 ug/Kg 119 70 - 130

Carbon tetrachloride 100 94.5 ug/Kg 95 70 - 130

Chlorobenzene 100 89.5 ug/Kg 90 70 - 130

Chlorobromomethane 100 102 ug/Kg 102 70 - 130

Chlorodibromomethane 100 104 ug/Kg 104 70 - 130

Chloroethane 100 87.0 ug/Kg 87 70 - 130

Chloroform 100 99.5 ug/Kg 100 70 - 130

Chloromethane 100 102 ug/Kg 102 70 - 130

cis-1,2-Dichloroethene 100 100 ug/Kg 100 70 - 130

cis-1,3-Dichloropropene 100 93.0 ug/Kg 93 70 - 130

Dibromomethane 100 102 ug/Kg 102 70 - 130

Dichlorobromomethane 100 96.5 ug/Kg 97 70 - 130

Dichlorodifluoromethane 100 92.0 ug/Kg 92 70 - 130

Ethyl ether 100 104 ug/Kg 104 70 - 130

Ethylbenzene 100 87.0 ug/Kg 87 70 - 130

Ethylene Dibromide 100 108 ug/Kg 108 70 - 130

Hexachlorobutadiene 100 99.5 ug/Kg 100 70 - 130

Isopropyl ether 100 95.0 ug/Kg 95 70 - 130

Isopropylbenzene 100 98.0 ug/Kg 98 70 - 130

m-Xylene & p-Xylene 200 174 ug/Kg 87 70 - 130

Methyl tert-butyl ether 100 101 ug/Kg 101 70 - 130

Methylene Chloride 100 92.0 ug/Kg 92 70 - 130

n-Butylbenzene 100 87.5 ug/Kg 88 70 - 130

N-Propylbenzene 100 88.5 ug/Kg 89 70 - 130

Naphthalene 100 99.0 ug/Kg 99 70 - 130

o-Xylene 100 96.5 ug/Kg 97 70 - 130

sec-Butylbenzene 100 97.5 ug/Kg 98 70 - 130

Styrene 100 102 ug/Kg 102 70 - 130

Tert-amyl methyl ether 100 98.0 ug/Kg 98 70 - 130

Tert-butyl ethyl ether 100 101 ug/Kg 101 70 - 130

tert-Butylbenzene 100 102 ug/Kg 102 70 - 130

Tetrachloroethene 100 96.5 ug/Kg 97 70 - 130

Tetrahydrofuran 1000 879 ug/Kg 88 70 - 130

Toluene 100 99.0 ug/Kg 99 70 - 130


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Spike


% Rec.

Limits

trans-1,2-Dichloroethene 100 98.5 ug/Kg 99 70 - 130

DAnalyte

LCS LCS

trans-1,3-Dichloropropene 100 87.0 ug/Kg 87 70 - 130

Trichloroethene 100 98.5 ug/Kg 99 70 - 130

Trichlorofluoromethane 100 80.5 ug/Kg 81 70 - 130

Vinyl chloride 100 94.5 ug/Kg 95 70 - 130

Qualifier % Recovery Limits

4-Bromofluorobenzene 70 - 130

Surrogate

114

LCS LCS

105Dibromofluoromethane 70 - 130

109Toluene-d8 (Surr) 70 - 130

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 360-75985/2-A



Spike


% Rec.

Limits RPD Limit

1,1,1,2-Tetrachloroethane 100 103 ug/Kg 103 70 - 130 2 20

DAnalyte

RPDLCSD LCSD

1,1,1-Trichloroethane 100 102 ug/Kg 102 70 - 130 2 20

1,1,2,2-Tetrachloroethane 100 74.5 ug/Kg 75 70 - 130 1 20

1,1,2-Trichloroethane 100 95.5 ug/Kg 96 70 - 130 1 20

1,1-Dichloroethane 100 105 ug/Kg 105 70 - 130 1 20

1,1-Dichloroethene 100 98.0 ug/Kg 98 70 - 130 1 20

1,1-Dichloropropene 100 94.0 ug/Kg 94 70 - 130 1 20

1,2,3-Trichlorobenzene 100 110 ug/Kg 110 70 - 130 4 20

1,2,3-Trichloropropane 100 102 ug/Kg 102 70 - 130 1 20


1,2,4-Trimethylbenzene 100 104 ug/Kg 104 70 - 130 2 20

1,2-Dibromo-3-Chloropropane 100 110 ug/Kg 110 70 - 130 1 20

1,2-Dichlorobenzene 100 96.0 ug/Kg 96 70 - 130 2 20

1,2-Dichloroethane 100 96.5 ug/Kg 97 70 - 130 1 20

1,2-Dichloropropane 100 87.0 ug/Kg 87 70 - 130 1 20

1,3,5-Trimethylbenzene 100 98.0 ug/Kg 98 70 - 130 2 20

1,3-Dichlorobenzene 100 101 ug/Kg 101 70 - 130 3 20


1,4-Dichlorobenzene 100 90.5 ug/Kg 91 70 - 130 2 20

1,4-Dioxane 1000 1170 * ug/Kg 117 70 - 130 22 20


2-Butanone (MEK) 1000 842 ug/Kg 84 70 - 130 4 20

2-Chlorotoluene 100 95.0 ug/Kg 95 70 - 130 1 20

2-Hexanone 1000 787 ug/Kg 79 70 - 130 3 20

4-Chlorotoluene 100 100 ug/Kg 100 70 - 130 3 20

4-Isopropyltoluene 100 104 ug/Kg 104 70 - 130 1 20

4-Methyl-2-pentanone (MIBK) 1000 754 ug/Kg 75 70 - 130 2 20

Acetone 1000 945 ug/Kg 94 70 - 130 5 20

Benzene 100 95.0 ug/Kg 95 70 - 130 1 20

Bromobenzene 100 85.5 ug/Kg 86 70 - 130 0 20

Bromoform 100 95.5 ug/Kg 96 70 - 130 2 20

Bromomethane 100 86.5 ug/Kg 87 70 - 130 2 20

Carbon disulfide 100 121 ug/Kg 121 70 - 130 2 20


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Spike


% Rec.

Limits RPD Limit

Carbon tetrachloride 100 95.0 ug/Kg 95 70 - 130 1 20

DAnalyte

RPDLCSD LCSD

Chlorobenzene 100 92.0 ug/Kg 92 70 - 130 3 20

Chlorobromomethane 100 102 ug/Kg 102 70 - 130 0 20

Chlorodibromomethane 100 103 ug/Kg 103 70 - 130 1 20

Chloroethane 100 87.5 ug/Kg 88 70 - 130 1 20

Chloroform 100 101 ug/Kg 101 70 - 130 1 20

Chloromethane 100 104 ug/Kg 104 70 - 130 2 20

cis-1,2-Dichloroethene 100 101 ug/Kg 101 70 - 130 1 20

cis-1,3-Dichloropropene 100 93.5 ug/Kg 94 70 - 130 1 20

Dibromomethane 100 101 ug/Kg 101 70 - 130 1 20

Dichlorobromomethane 100 96.0 ug/Kg 96 70 - 130 1 20

Dichlorodifluoromethane 100 91.0 ug/Kg 91 70 - 130 1 20

Ethyl ether 100 106 ug/Kg 106 70 - 130 2 20

Ethylbenzene 100 89.0 ug/Kg 89 70 - 130 2 20

Ethylene Dibromide 100 108 ug/Kg 108 70 - 130 0 20

Hexachlorobutadiene 100 103 ug/Kg 103 70 - 130 3 20

Isopropyl ether 100 95.5 ug/Kg 96 70 - 130 1 20

Isopropylbenzene 100 100 ug/Kg 100 70 - 130 2 20

m-Xylene & p-Xylene 200 179 ug/Kg 89 70 - 130 3 20

Methyl tert-butyl ether 100 100 ug/Kg 100 70 - 130 1 20

Methylene Chloride 100 92.5 ug/Kg 93 70 - 130 1 20

n-Butylbenzene 100 89.5 ug/Kg 90 70 - 130 2 20

N-Propylbenzene 100 90.5 ug/Kg 91 70 - 130 2 20

Naphthalene 100 102 ug/Kg 102 70 - 130 2 20

o-Xylene 100 101 ug/Kg 101 70 - 130 4 20

sec-Butylbenzene 100 97.0 ug/Kg 97 70 - 130 1 20

Styrene 100 104 ug/Kg 104 70 - 130 2 20

Tert-amyl methyl ether 100 97.5 ug/Kg 98 70 - 130 1 20

Tert-butyl ethyl ether 100 100 ug/Kg 100 70 - 130 0 20

tert-Butylbenzene 100 101 ug/Kg 101 70 - 130 0 20

Tetrachloroethene 100 97.5 ug/Kg 98 70 - 130 1 20

Tetrahydrofuran 1000 889 ug/Kg 89 70 - 130 1 20

Toluene 100 100 ug/Kg 100 70 - 130 1 20

trans-1,2-Dichloroethene 100 100 ug/Kg 100 70 - 130 2 20

trans-1,3-Dichloropropene 100 87.0 ug/Kg 87 70 - 130 0 20

Trichloroethene 100 99.5 ug/Kg 100 70 - 130 1 20

Trichlorofluoromethane 100 80.0 ug/Kg 80 70 - 130 1 20

Vinyl chloride 100 95.5 ug/Kg 96 70 - 130 1 20


4-Bromofluorobenzene 70 - 130

Surrogate

112

LCSD LCSD

105Dibromofluoromethane 70 - 130

107Toluene-d8 (Surr) 70 - 130


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Method: 8270D - Semivolatile Organic Compounds (GC/MS)





1,2,4-Trichlorobenzene ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1

MB MB

Analyte

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 11,2-Dichlorobenzene



ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,2'-oxybis[1-chloropropane]

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4,5-Trichlorophenol

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4,6-Trichlorophenol

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4-Dichlorophenol

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4-Dimethylphenol

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4-Dinitrophenol

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4-Dinitrotoluene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,6-Dinitrotoluene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12-Chloronaphthalene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12-Chlorophenol

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 12-Methylnaphthalene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12-Methylphenol

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12-Nitrophenol

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 13 & 4 Methylphenol

ND 670 ug/Kg 06/21/11 11:45 06/24/11 21:43 13,3'-Dichlorobenzidine

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 14-Bromophenyl phenyl ether

ND 670 ug/Kg 06/21/11 11:45 06/24/11 21:43 14-Chloroaniline

ND 1700 ug/Kg 06/21/11 11:45 06/24/11 21:43 14-Nitrophenol

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Acenaphthene

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Acenaphthylene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Acetophenone

ND 1700 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Aniline

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Anthracene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Azobenzene

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Benzo[a]anthracene

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Benzo[a]pyrene

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Benzo[b]fluoranthene

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Benzo[g,h,i]perylene

ND 180 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Benzo[k]fluoranthene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Bis(2-chloroethoxy)methane

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Bis(2-chloroethyl)ether

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Bis(2-ethylhexyl) phthalate

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Butyl benzyl phthalate

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Chrysene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Di-n-butyl phthalate

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Di-n-octyl phthalate

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Dibenz(a,h)anthracene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Dibenzofuran

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Diethyl phthalate

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Dimethyl phthalate

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Fluoranthene

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Fluorene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Hexachlorobenzene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Hexachlorobutadiene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Hexachloroethane


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Indeno[1,2,3-cd]pyrene ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1

MB MB

Analyte

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Isophorone

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Naphthalene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Nitrobenzene

ND 1700 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Pentachlorophenol

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Phenanthrene

ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Phenol

ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Pyrene


2,4,6-Tribromophenol 61 30 - 130 06/24/11 21:43 1

MB MB

Surrogate

06/21/11 11:45

65 06/21/11 11:45 06/24/11 21:43 12-Fluorophenol 30 - 130

63 06/21/11 11:45 06/24/11 21:43 1Nitrobenzene-d5 30 - 130

64 06/21/11 11:45 06/24/11 21:43 1Phenol-d5 30 - 130

65 06/21/11 11:45 06/24/11 21:43 1Terphenyl-d14 30 - 130

61 06/21/11 11:45 06/24/11 21:43 12-Fluorobiphenyl 30 - 130




Spike


% Rec.

Limits


DAnalyte

LCS LCS

1,2-Dichlorobenzene 1330 810 ug/Kg 61 40 - 140



2,2'-oxybis[1-chloropropane] 1330 897 ug/Kg 67 40 - 140

2,4,5-Trichlorophenol 1330 953 ug/Kg 72 30 - 130

2,4,6-Trichlorophenol 1330 930 ug/Kg 70 30 - 130

2,4-Dichlorophenol 1330 940 ug/Kg 71 30 - 130

2,4-Dimethylphenol 1330 923 ug/Kg 69 30 - 130

2,4-Dinitrophenol 1330 610 ug/Kg 46 30 - 130

2,4-Dinitrotoluene 1330 1060 ug/Kg 79 40 - 140

2,6-Dinitrotoluene 1330 973 ug/Kg 73 40 - 140

2-Chloronaphthalene 1330 900 ug/Kg 68 40 - 140

2-Chlorophenol 1330 890 ug/Kg 67 30 - 130

2-Methylnaphthalene 1330 907 ug/Kg 68 40 - 140

2-Methylphenol 1330 927 ug/Kg 70 30 - 130

2-Nitrophenol 1330 827 ug/Kg 62 30 - 130

3 & 4 Methylphenol 1330 970 ug/Kg 73 30 - 130

3,3'-Dichlorobenzidine 1330 1040 ug/Kg 78 40 - 140

4-Bromophenyl phenyl ether 1330 947 ug/Kg 71 40 - 140

4-Chloroaniline 1330 767 ug/Kg 58 40 - 140

4-Nitrophenol 1330 ND ug/Kg 72 30 - 130

Acenaphthene 1330 1110 ug/Kg 83 40 - 140

Acenaphthylene 1330 947 ug/Kg 71 40 - 140

Acetophenone 1330 867 ug/Kg 65 40 - 140

Aniline 1330 ND * ug/Kg 34 40 - 140

Anthracene 1330 1090 ug/Kg 82 40 - 140


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Spike


% Rec.

Limits

Azobenzene 1330 830 ug/Kg 62 40 - 140

DAnalyte

LCS LCS

Benzo[a]anthracene 1330 1180 ug/Kg 88 40 - 140

Benzo[a]pyrene 1330 1210 ug/Kg 91 40 - 140

Benzo[b]fluoranthene 1330 1100 ug/Kg 82 40 - 140

Benzo[g,h,i]perylene 1330 1180 ug/Kg 89 40 - 140

Benzo[k]fluoranthene 1330 1230 ug/Kg 92 40 - 140

Bis(2-chloroethoxy)methane 1330 887 ug/Kg 67 40 - 140

Bis(2-chloroethyl)ether 1330 827 ug/Kg 62 40 - 140

Bis(2-ethylhexyl) phthalate 1330 1040 ug/Kg 78 40 - 140

Butyl benzyl phthalate 1330 1010 ug/Kg 76 40 - 140

Chrysene 1330 1200 ug/Kg 90 40 - 140

Di-n-butyl phthalate 1330 1060 ug/Kg 79 40 - 140

Di-n-octyl phthalate 1330 1060 ug/Kg 79 40 - 140

Dibenz(a,h)anthracene 1330 1220 ug/Kg 92 40 - 140

Dibenzofuran 1330 950 ug/Kg 71 40 - 140

Diethyl phthalate 1330 990 ug/Kg 74 40 - 140

Dimethyl phthalate 1330 977 ug/Kg 73 40 - 140

Fluoranthene 1330 1030 ug/Kg 77 40 - 140

Fluorene 1330 1130 ug/Kg 85 40 - 140

Hexachlorobenzene 1330 930 ug/Kg 70 40 - 140

Hexachlorobutadiene 1330 760 ug/Kg 57 40 - 140

Hexachloroethane 1330 803 ug/Kg 60 40 - 140

Indeno[1,2,3-cd]pyrene 1330 1210 ug/Kg 91 40 - 140

Isophorone 1330 723 ug/Kg 54 40 - 140

Naphthalene 1330 860 ug/Kg 65 40 - 140

Nitrobenzene 1330 833 ug/Kg 63 40 - 140

Pentachlorophenol 1330 ND ug/Kg 68 30 - 130

Phenanthrene 1330 1100 ug/Kg 83 40 - 140

Phenol 1330 947 ug/Kg 71 30 - 130

Pyrene 1330 1150 ug/Kg 87 40 - 140


2,4,6-Tribromophenol 30 - 130

Surrogate

63

LCS LCS

612-Fluorophenol 30 - 130

59Nitrobenzene-d5 30 - 130

62Phenol-d5 30 - 130

65Terphenyl-d14 30 - 130

622-Fluorobiphenyl 30 - 130




Spike


% Rec.

Limits RPD Limit


DAnalyte

RPDLCSD LCSD




2,2'-oxybis[1-chloropropane] 1330 927 ug/Kg 70 40 - 140 3 30


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Spike


% Rec.

Limits RPD Limit

2,4,5-Trichlorophenol 1330 973 ug/Kg 73 30 - 130 2 30

DAnalyte

RPDLCSD LCSD

2,4,6-Trichlorophenol 1330 953 ug/Kg 72 30 - 130 2 30

2,4-Dichlorophenol 1330 983 ug/Kg 74 30 - 130 5 30

2,4-Dimethylphenol 1330 943 ug/Kg 71 30 - 130 2 30

2,4-Dinitrophenol 1330 617 ug/Kg 46 30 - 130 1 30

2,4-Dinitrotoluene 1330 1070 ug/Kg 80 40 - 140 1 30

2,6-Dinitrotoluene 1330 957 ug/Kg 72 40 - 140 2 30

2-Chloronaphthalene 1330 920 ug/Kg 69 40 - 140 2 30

2-Chlorophenol 1330 923 ug/Kg 69 30 - 130 4 30

2-Methylnaphthalene 1330 970 ug/Kg 73 40 - 140 7 30

2-Methylphenol 1330 973 ug/Kg 73 30 - 130 5 30

2-Nitrophenol 1330 870 ug/Kg 65 30 - 130 5 30

3 & 4 Methylphenol 1330 980 ug/Kg 74 30 - 130 1 30

3,3'-Dichlorobenzidine 1330 1100 ug/Kg 83 40 - 140 6 30

4-Bromophenyl phenyl ether 1330 990 ug/Kg 74 40 - 140 4 30

4-Chloroaniline 1330 787 ug/Kg 59 40 - 140 3 30

4-Nitrophenol 1330 ND ug/Kg 69 30 - 130 4 30

Acenaphthene 1330 1160 ug/Kg 87 40 - 140 5 30

Acenaphthylene 1330 973 ug/Kg 73 40 - 140 3 30

Acetophenone 1330 910 ug/Kg 68 40 - 140 5 30

Aniline 1330 ND * ug/Kg 34 40 - 140 1 30

Anthracene 1330 1160 ug/Kg 87 40 - 140 6 30

Azobenzene 1330 883 ug/Kg 66 40 - 140 6 30

Benzo[a]anthracene 1330 1210 ug/Kg 91 40 - 140 3 30

Benzo[a]pyrene 1330 1220 ug/Kg 92 40 - 140 1 30

Benzo[b]fluoranthene 1330 1110 ug/Kg 84 40 - 140 2 30

Benzo[g,h,i]perylene 1330 1190 ug/Kg 89 40 - 140 1 30

Benzo[k]fluoranthene 1330 1250 ug/Kg 94 40 - 140 2 30

Bis(2-chloroethoxy)methane 1330 930 ug/Kg 70 40 - 140 5 30

Bis(2-chloroethyl)ether 1330 877 ug/Kg 66 40 - 140 6 30

Bis(2-ethylhexyl) phthalate 1330 1050 ug/Kg 79 40 - 140 1 30

Butyl benzyl phthalate 1330 1020 ug/Kg 77 40 - 140 1 30

Chrysene 1330 1210 ug/Kg 91 40 - 140 1 30

Di-n-butyl phthalate 1330 1070 ug/Kg 80 40 - 140 1 30

Di-n-octyl phthalate 1330 1080 ug/Kg 81 40 - 140 2 30

Dibenz(a,h)anthracene 1330 1230 ug/Kg 92 40 - 140 1 30

Dibenzofuran 1330 967 ug/Kg 73 40 - 140 2 30

Diethyl phthalate 1330 1030 ug/Kg 77 40 - 140 4 30

Dimethyl phthalate 1330 977 ug/Kg 73 40 - 140 0 30

Fluoranthene 1330 1060 ug/Kg 80 40 - 140 3 30

Fluorene 1330 1160 ug/Kg 87 40 - 140 2 30

Hexachlorobenzene 1330 977 ug/Kg 73 40 - 140 5 30

Hexachlorobutadiene 1330 790 ug/Kg 59 40 - 140 4 30

Hexachloroethane 1330 820 ug/Kg 62 40 - 140 2 30

Indeno[1,2,3-cd]pyrene 1330 1200 ug/Kg 90 40 - 140 0 30

Isophorone 1330 767 ug/Kg 58 40 - 140 6 30

Naphthalene 1330 933 ug/Kg 70 40 - 140 8 30

Nitrobenzene 1330 897 ug/Kg 67 40 - 140 7 30

Pentachlorophenol 1330 ND ug/Kg 69 30 - 130 2 30

Phenanthrene 1330 1130 ug/Kg 85 40 - 140 3 30


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Spike


% Rec.

Limits RPD Limit

Phenol 1330 973 ug/Kg 73 30 - 130 3 30

DAnalyte

RPDLCSD LCSD

Pyrene 1330 1160 ug/Kg 87 40 - 140 1 30


2,4,6-Tribromophenol 30 - 130

Surrogate

63

LCSD LCSD

622-Fluorophenol 30 - 130

61Nitrobenzene-d5 30 - 130

62Phenol-d5 30 - 130

65Terphenyl-d14 30 - 130

632-Fluorobiphenyl 30 - 130

Method: 8015B - 8100M (Modified) Total Extractable Petroleum Hydrocarbons




Result Qualifier Unit D Prepared Analyzed Dil FacRL RL


(C9-C36)

ND 3.3 mg/Kg 06/20/11 12:36 06/21/11 09:47 1

MB MB

Analyte


o-Terphenyl 83 40 - 140 06/21/11 09:47 1

MB MB

Surrogate

06/20/11 12:36




Spike


% Rec.

Limits


(C9-C36)

167 117 mg/Kg 70 60 - 140

DAnalyte

LCS LCS


o-Terphenyl 40 - 140

Surrogate

80

LCS LCS




Spike


% Rec.

Limits RPD Limit


(C9-C36)

167 125 mg/Kg 75 60 - 140 7 50

DAnalyte

RPDLCSD LCSD


o-Terphenyl 40 - 140

Surrogate

86

LCSD LCSD


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Method: 8081B - Organochlorine Pesticides (GC/ECD)





4,4'-DDD ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1

MB MB

Analyte

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 14,4'-DDE

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 14,4'-DDT

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Aldrin

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1alpha-BHC

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1beta-BHC

ND 3.0 ug/Kg 06/20/11 12:38 06/21/11 16:14 1gamma-BHC (Lindane)

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1delta-BHC

ND 500 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Chlordane (technical)

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Dieldrin

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Endosulfan I

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Endosulfan II

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Endosulfan sulfate

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Endrin

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Endrin ketone

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Heptachlor

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Heptachlor epoxide

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Hexachlorobenzene

ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Methoxychlor


Tetrachloro-m-xylene 87 30 - 150 06/21/11 16:14 1

MB MB

Surrogate

06/20/11 12:38

90 06/20/11 12:38 06/21/11 16:14 1Tetrachloro-m-xylene 30 - 150

83 06/20/11 12:38 06/21/11 16:14 1DCB Decachlorobiphenyl 30 - 150





Spike


% Rec.

Limits

4,4'-DDD 60.0 87.0 * ug/Kg 145 40 - 140

DAnalyte

LCS LCS

4,4'-DDE 60.0 83.1 ug/Kg 139 40 - 140

4,4'-DDT 60.0 78.5 ug/Kg 131 40 - 140

Aldrin 60.0 74.6 ug/Kg 124 40 - 140

alpha-BHC 60.0 66.9 ug/Kg 112 40 - 140

beta-BHC 60.0 73.2 ug/Kg 122 40 - 140

gamma-BHC (Lindane) 60.0 67.2 ug/Kg 112 40 - 140

delta-BHC 60.0 58.9 ug/Kg 98 40 - 140

Dieldrin 60.0 76.3 ug/Kg 127 40 - 140

Endosulfan I 60.0 75.9 ug/Kg 127 40 - 140

Endosulfan II 60.0 76.9 ug/Kg 128 40 - 140

Endosulfan sulfate 60.0 76.0 ug/Kg 127 40 - 140

Endrin 60.0 93.1 * ug/Kg 155 40 - 140

Endrin ketone 60.0 74.7 ug/Kg 125 40 - 140

Heptachlor 60.0 78.7 ug/Kg 131 40 - 140

Heptachlor epoxide 60.0 69.5 ug/Kg 116 40 - 140

Hexachlorobenzene 60.0 61.0 ug/Kg 102 40 - 140

Methoxychlor 60.0 76.5 ug/Kg 128 40 - 140


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Method: 8081B - Organochlorine Pesticides (GC/ECD) (Continued)





Tetrachloro-m-xylene 30 - 150

Surrogate

87

LCS LCS

88Tetrachloro-m-xylene 30 - 150

86DCB Decachlorobiphenyl 30 - 150





Spike


% Rec.

Limits RPD Limit

4,4'-DDD 60.0 96.2 * ug/Kg 160 40 - 140 10 30

DAnalyte

RPDLCSD LCSD

4,4'-DDE 60.0 90.4 * ug/Kg 151 40 - 140 8 30

4,4'-DDT 60.0 82.3 ug/Kg 137 40 - 140 5 30

Aldrin 60.0 80.9 ug/Kg 135 40 - 140 8 30

alpha-BHC 60.0 74.4 ug/Kg 124 40 - 140 11 30

beta-BHC 60.0 79.1 ug/Kg 132 40 - 140 8 30

gamma-BHC (Lindane) 60.0 71.3 ug/Kg 119 40 - 140 6 30

delta-BHC 60.0 62.4 ug/Kg 104 40 - 140 6 30

Dieldrin 60.0 82.7 ug/Kg 138 40 - 140 8 30

Endosulfan I 60.0 81.6 ug/Kg 136 40 - 140 7 30

Endosulfan II 60.0 81.8 ug/Kg 136 40 - 140 6 30

Endosulfan sulfate 60.0 81.6 ug/Kg 136 40 - 140 7 30

Endrin 60.0 105 E * ug/Kg 175 40 - 140 12 30

Endrin ketone 60.0 80.6 ug/Kg 134 40 - 140 8 30

Heptachlor 60.0 85.7 * ug/Kg 143 40 - 140 9 30

Heptachlor epoxide 60.0 74.9 ug/Kg 125 40 - 140 7 30

Hexachlorobenzene 60.0 65.9 ug/Kg 110 40 - 140 8 30

Methoxychlor 60.0 80.8 ug/Kg 135 40 - 140 5 30



Surrogate

95

LCSD LCSD




Method: 8082A - Polychlorinated Biphenyls (GC/ECD)





PCB-1016 ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1

MB MB

Analyte

ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1221

ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1232

ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1242

ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1248

ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1254

ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1260


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Method: 8082A - Polychlorinated Biphenyls (GC/ECD) (Continued)





PCB-1262 ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1

MB MB

Analyte

ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1268


Tetrachloro-m-xylene 91 30 - 150 06/20/11 17:00 1

MB MB

Surrogate

06/20/11 12:38

85 06/20/11 12:38 06/20/11 17:00 1Tetrachloro-m-xylene 30 - 150






Spike


% Rec.

Limits

PCB-1016 500 507 ug/Kg 101 40 - 140

DAnalyte

LCS LCS

PCB-1260 500 547 ug/Kg 109 40 - 140



Surrogate

93

LCS LCS







Spike


% Rec.

Limits RPD Limit

PCB-1016 500 550 ug/Kg 110 40 - 140 8 30

DAnalyte

RPDLCSD LCSD

PCB-1260 500 560 ug/Kg 112 40 - 140 2 30



Surrogate

98

LCSD LCSD




Method: 8151A - Herbicides (GC)





Dalapon ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 1

MB MB

Analyte

ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 1Dicamba

ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 1Dichlorprop

ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 12,4-D

ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 12,4-DB


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Method: 8151A - Herbicides (GC) (Continued)





Silvex (2,4,5-TP) ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 1

MB MB

Analyte

ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 12,4,5-T

ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 1Dinoseb

ND 1700 ug/Kg 06/24/11 10:56 06/26/11 23:23 1MCPA

ND 1700 ug/Kg 06/24/11 10:56 06/26/11 23:23 1Mecoprop


2,4-Dichlorophenylacetic acid 142 101 - 150 06/26/11 23:23 1

MB MB

Surrogate

06/24/11 10:56

121 06/24/11 10:56 06/26/11 23:23 12,4-Dichlorophenylacetic acid 101 - 150




Spike


% Rec.

Limits

Dalapon 167 220 ug/Kg 132 63 - 150

DAnalyte

LCS LCS

Dalapon 167 205 ug/Kg 123 63 - 150

Dicamba 167 196 ug/Kg 118 51 - 145

Dicamba 167 203 ug/Kg 122 51 - 145

Dichlorprop 167 133 ug/Kg 80 37 - 150

Dichlorprop 167 176 ug/Kg 106 37 - 150

2,4-D 167 171 ug/Kg 103 52 - 150

2,4-D 167 213 ug/Kg 128 52 - 150

2,4-DB 167 246 ug/Kg 148 10 - 150

2,4-DB 167 177 ug/Kg 106 10 - 150

Silvex (2,4,5-TP) 167 199 ug/Kg 120 73 - 148

Silvex (2,4,5-TP) 167 204 ug/Kg 122 73 - 148

2,4,5-T 167 178 ug/Kg 107 69 - 150

2,4,5-T 167 175 ug/Kg 105 69 - 150

Dinoseb 167 139 ug/Kg 83 42 - 140

Dinoseb 167 150 ug/Kg 90 42 - 140

MCPA 16700 16200 ug/Kg 97 70 - 130

MCPA 16700 18600 ug/Kg 112 70 - 130

Mecoprop 16700 19800 ug/Kg 119 70 - 130

Mecoprop 16700 21400 ug/Kg 128 70 - 130


2,4-Dichlorophenylacetic acid 101 - 150

Surrogate

118

LCS LCS





Spike


% Rec.

Limits RPD Limit

Dalapon 167 153 * ug/Kg 92 63 - 150 36 30

DAnalyte

RPDLCSD LCSD

Dalapon 167 150 * ug/Kg 90 63 - 150 31 30

Dicamba 167 169 ug/Kg 101 51 - 145 18 30

Dicamba 167 167 ug/Kg 100 51 - 145 16 30


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Method: 8151A - Herbicides (GC) (Continued)




Spike


% Rec.

Limits RPD Limit

Dichlorprop 167 114 ug/Kg 68 37 - 150 15 30

DAnalyte

RPDLCSD LCSD

Dichlorprop 167 152 ug/Kg 91 37 - 150 14 30

2,4-D 167 249 ug/Kg 150 52 - 150 16 30

2,4-D 167 199 ug/Kg 119 52 - 150 15 30

2,4-DB 167 243 ug/Kg 146 10 - 150 1 30

2,4-DB 167 205 ug/Kg 123 10 - 150 15 30

Silvex (2,4,5-TP) 167 172 ug/Kg 103 73 - 148 15 30

Silvex (2,4,5-TP) 167 174 ug/Kg 104 73 - 148 16 30

2,4,5-T 167 162 ug/Kg 97 69 - 150 9 30

2,4,5-T 167 157 ug/Kg 94 69 - 150 11 30

Dinoseb 167 55.5 * ug/Kg 33 42 - 140 86 30

Dinoseb 167 61.0 * ug/Kg 37 42 - 140 84 30

MCPA 16700 14500 ug/Kg 87 70 - 130 11 30

MCPA 16700 18100 ug/Kg 109 70 - 130 3 30

Mecoprop 16700 18300 ug/Kg 110 70 - 130 16 30

Mecoprop 16700 17900 ug/Kg 107 70 - 130 10 30



Surrogate

109

LCSD LCSD


Method: 6010B - Metals (ICP)





Silver ND 1.0 mg/Kg 06/20/11 07:33 06/20/11 15:04 1

MB MB

Analyte

ND 1.0 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Arsenic

ND 0.20 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Beryllium

ND 0.20 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Cadmium

ND 0.50 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Chromium

ND 2.0 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Copper

ND 2.0 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Nickel

ND 0.50 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Lead

ND 0.50 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Selenium

ND 1.0 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Thallium

ND 2.5 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Zinc

ND 0.50 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Antimony

Client Sample ID: Lab Control Sample DupLab Sample ID: LCDSRM 360-75498/3-A

LCDSRM



Spike


% Rec.

Limits RPD Limit

Silver 67.5 54.8 mg/Kg 81 56.9 - 113 3 30

DAnalyte

RPDLCDSRM LCDSRM

Arsenic 90.0 77.4 mg/Kg 86 61 - 117 2 30


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Method: 6010B - Metals (ICP) (Continued)


LCDSRM



Spike


% Rec.

Limits RPD Limit

Beryllium 83.0 67.8 mg/Kg 82 65.8 - 112 4 30

DAnalyte

RPDLCDSRM LCDSRM

Cadmium 106 85.3 mg/Kg 80 65.6 - 113 2 30

Chromium 272 240 mg/Kg 88 68.0 - 124 5 30

Copper 157 138 mg/Kg 88 70.7 - 117 5 30

Nickel 179 150 mg/Kg 84 67.6 - 117 3 30

Lead 267 203 mg/Kg 76 64.8 - 110 4 30

Selenium 154 115 mg/Kg 75 53.1 - 110 1 30

Thallium 286 223 mg/Kg 78 61.9 - 116 1 30

Zinc 655 517 mg/Kg 79 67.5 - 116 3 30

Antimony 152 30.2 mg/Kg 20 10.0 - 110 7 30

Client Sample ID: Lab Control SampleLab Sample ID: LCSSRM 360-75498/2-A



Spike


% Rec.

Limits

Silver 67.5 56.6 mg/Kg 84 56.9 - 113

DAnalyte

LCSSRM LCSSRM

Arsenic 90.0 78.6 mg/Kg 87 61 - 117

Beryllium 83.0 70.5 mg/Kg 85 65.8 - 112

Cadmium 106 86.9 mg/Kg 82 65.6 - 113

Chromium 272 251 mg/Kg 92 68.0 - 124

Copper 157 146 mg/Kg 93 70.7 - 117

Nickel 179 155 mg/Kg 86 67.6 - 117

Lead 267 210 mg/Kg 79 64.8 - 110

Selenium 154 116 mg/Kg 76 53.1 - 110

Thallium 286 226 mg/Kg 79 61.9 - 116

Zinc 655 532 mg/Kg 81 67.5 - 116

Antimony 152 32.4 mg/Kg 21 10.0 - 110

Method: 7471A - Mercury (CVAA)





Mercury ND 0.10 mg/Kg 06/20/11 10:07 06/20/11 14:42 1

MB MB

Analyte


LCDSRM



Spike


% Rec.

Limits RPD Limit

Mercury 9.36 8.41 mg/Kg 90 46.5 - 135 2 30

DAnalyte

RPDLCDSRM LCDSRM


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Method: 7471A - Mercury (CVAA) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCSSRM 360-75533/2-A



Spike


% Rec.

Limits

Mercury 10.3 8.60 mg/Kg 83 46.5 - 135

DAnalyte

LCSSRM LCSSRM

Method: SM 2510B - Conductivity, Specific Conductance


Matrix: Solid Prep Type: Soluble


Result Qualifier Unit D Prepared Analyzed Dil FacRL RL

Specific Conductance ND 4.0 umhos/cm 06/23/11 14:00 1

MB MB

Analyte


Matrix: Solid Prep Type: Soluble


Spike


% Rec.

Limits

Specific Conductance 5640 5600 umhos/cm 99 85 - 115

DAnalyte

LCS LCS


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Pesticide PEM Data

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Lab ChronicleClient: ARCADIS U.S., Inc TestAmerica Job ID: 360-34572-1


Client Sample ID: PH 1 SS-1 Lab Sample ID: 360-34572-1Matrix: SolidDate Collected: 06/16/11 14:00


Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared

Or Analyzed Analyst LabPrep Type

Total/NA Prep 5035 06/26/11 10:49 SS75985 TAL WFD

Total/NA Analysis 8260C 1 75986 06/27/11 07:50 SS TAL WFD

Total/NA Prep 3546 75634 06/21/11 11:45 OG TAL WFD

Total/NA Analysis 8270D 2 76250 06/30/11 16:56 CMR TAL WFD


Total/NA Analysis 8082A 1 75643 06/21/11 17:12 BRB TAL WFD

Total/NA Analysis 8081B 1 75661 06/21/11 17:19 BRB TAL WFD



Total/NA Prep 8151A 77865 06/24/11 10:56 ME TAL EDI

Total/NA Analysis 8151A 1 78058 06/26/11 20:50 SK TAL EDI

Total/NA Prep 7471A 75533 06/20/11 10:07 EMN TAL WFD

Total/NA Analysis 7471A 1 75577 06/20/11 15:08 EMN TAL WFD

Total/NA Prep 3050B 75498 06/20/11 07:33 EMN TAL WFD

Total/NA Analysis 6010B 1 75614 06/20/11 16:09 TJS TAL WFD

Total/NA Analysis Moisture 1 75547 06/20/11 11:46 EMN TAL WFD

Soluble Leach DI Leach 75814 06/23/11 09:50 AMS TAL WFD

Soluble Analysis SM 2510B 1 75858 06/23/11 14:00 AMS TAL WFD



Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared





















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Lab ChronicleClient: ARCADIS U.S., Inc TestAmerica Job ID: 360-34572-1




Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared




















Laboratory References:

TAL EDI = TestAmerica Edison, 777 New Durham Road, Edison, NJ 08817, TEL (732)549-3900

TAL WFD = TestAmerica Westfield, Westfield Executive Park, 53 Southampton Road, Westfield, MA 01085, TEL (413)572-4000


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Certification SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc


Laboratory Program Certification IDAuthority EPA Region

TestAmerica Westfield PH-0494State ProgramConnecticut 1

TestAmerica Westfield MA00014State ProgramMaine 1

TestAmerica Westfield M-MA014State ProgramMassachusetts 1

TestAmerica Westfield 2539NELACNew Hampshire 1

TestAmerica Westfield 10843NELACNew York 2

TestAmerica Westfield 647North Carolina DENRNorth Carolina 4

TestAmerica Westfield LAO00057State ProgramRhode Island 1

TestAmerica Westfield VT-10843State ProgramVermont 1

TestAmerica Edison PH-0200State ProgramConnecticut 1

TestAmerica Edison N/ADelaware DNRECDelaware 3

TestAmerica Edison 12028NELACNew Jersey 2

TestAmerica Edison 11452NELACNew York 2

TestAmerica Edison 68-00522NELACPennsylvania 3

TestAmerica Edison LAO00132State ProgramRhode Island 1

TestAmerica Edison NJCA-003-08USDAUSDA

Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s current list

of certified methods and analytes.


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State Accreditation Matrix

New Hampshire

(NELAC) prim. Mass ConnFlorida

(NELAC)North

Carolina

821-R-02-012 Toxicity, Acute (48-Hour)(list upon request) NP NP

SM 4500 Cl F Chlorine, Residual NP

SM 9215E Heterotrophic Plate Count (SimPlate) P

SM 9222D Coliforms, Fecal (Membrane Filter) P/NP

SM 9223 Coliforms, Total, and E.Coli (Colilert-P/A) P

SM 9224 Coliforms, Total, and E.Coli (Enumeration) P

1103.1 E.coli

Enterolert Enterococcus

200.8 Rev 5.4 Metals (ICP/MS) (list upon request) NP/P NP/P NP/P

200.7 Rev 4.4 Metals (ICP)(list upon request) NP/P NP/P NP/P

6010B Metals (ICP)(list upon request) NP/SW NP/SW

245.1 Mercury (CVAA) NP/P NP NP/P

7470A Mercury (CVAA) NP NP

7471A Mercury (CVAA) SW SW

SM 2340B Total Hardness (as CaCO3) by calculation NP/P NP NP/P

3005A Preparation, Total Recoverable or Dissolved Metals NP/P NP/P

3010A Preparation, Total Metals NP/P NP/P

3020A Preparation, Total Metals NP/P/SW NP/P/SW

3050B Preparation, Metals SW SW

504.1 EDB, DBCP and 1,2,3-TCP (GC) P P P

608 Organochlorine Pest/PCBs (list upon request) NP NP NP

625 Semivolatile Org Comp (GC/MS)(list upon request) NP NP

3546 Microwave Extraction SW

3510C Liquid-Liquid Extraction (Separatory Funnel) NP NP

3540C Soxhlet Extraction SW

3550B Ultrasonic Extraction SW SW

600/4-81-045 Polychlorinated Biphenyls (PCBs) (GC) NP NP

8081A Organochlorine Pesticides (GC)(list upon request) NP/SW NP/SW

8082 PCBs by Gas Chromatography(list upon request) NP/SW NP/SW

8270C Semivolatile Comp.(GC/MS)(list upon request) NP/SW NP/SW

CT ETPH Conn - Ext. Total petroleum Hydrocarbons (GC) NP/SW

MA-EPH Mass - Extractable Petroleum Hydrocarbons (GC) NP/SW NP/SW

524.2 Volatile Org Comp (GC/MS)(list upon request) P P P

524.2 Trihalomethane compounds P P P

624 Volatile Org Comp (GC/MS)(list upon request) NP NP NP

5035 Closed System Purge and Trap SW SW

5030B Purge and Trap NP NP

8260B Volatile Org Comp. (GC/MS)(list upon request) NP/SW NP/SW

MAVPH Mass - Volatile Petroleum Hydrocarbons (GC) NP/SW NP/SW

180.1 Turbidity, Nephelometric P P P

300 Anions, Ion Chromatography NP/P NP/P NP/P

410.4 COD NP NP NP

1010 Ignitability, Pensky-Martens Closed-Cup Method SW SW

10-107-06-2 Nitrogen, Total Kjeldahl NP NP NP

7196A Chromium, Hexavalent NP/SW NP/SW

9012A Cyanide, Total and/or Amenable NP/SW NP/SW

9030B Sulfide, Distillation (Acid Soluble and Insoluble) NP NP

9040B pH NP NP

9045C pH SW SW

L107041C Nitrogen, Nitrate NP P NP/P

L107-06-1B Nitrogen Ammonia NP NP NP/P

L204001A CN Cyanide, Total P NP/P NP/P

L210-001A Phenolics, Total Recoverable NP NP NP

SM 2320B Alkalinity NP/P NP/P NP/P

SM 2510B Conductivity, Specific Conductance NP/P NP/P NP/P

SM 2540C Solids, Total Dissolved (TDS) NP/P NP/P NP/P

SM 2540D Solids, Total Suspended (TSS) NP NP NP

SM 3500 CR D Chromium, Hexavalent NP NP

SM 4500 H+ B pH NP/P NP/P NP/P

SM 4500 NO2 B Nitrogen, Nitrite NP P NP/P

SM 4500 P E Phosphorus, Orthophosphate NP/P NP NP/P

SM 4500 P E Phosphorus, Total NP NP NP

SM 4500 S2 D Sulfide, Total NP NP

SM 5210B BOD, 5-Day NP NP NP

SM 5310B Organic Carbon, Total (TOC) NP/P NP NP/P

Not all organic compounds are accreditied under NELACFor methods with multiple compounds all compounds may not meet NELAC criteria, listing should be obtained from the laboratory

The lab carries additional accreditations with several states. This is the laboratories typcial listing but is subject to change based on the laboratories current certification standing.

State where Primary Accreditation is Carried

Method Name Description

ambient/ source

NP=Non Potable P= Potable SW=Solid Waste WI-QA-040r5 last updated 3/2/2011

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Login Sample Receipt Checklist

Client: ARCADIS U.S., Inc Job Number: 360-34572-1

Login Number: 34572

Question Answer Comment

Creator: Beaumier, Janine E

List Source: TestAmerica Westfield

List Number: 1

N/ARadioactivity either was not measured or, if measured, is at or below

background

N/AThe cooler's custody seal, if present, is intact.

TrueThe cooler or samples do not appear to have been compromised or

tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the sample IDs on the containers and

the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in

diameter.

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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Login Sample Receipt Checklist

Client: ARCADIS U.S., Inc Job Number: 360-34572-1

Login Number: 34572

Question Answer Comment

Creator: Retana, Camille

List Source: TestAmerica Edison

List Creation: 06/21/11 03:38 PMList Number: 1

N/ARadioactivity either was not measured or, if measured, is at or below

background

TrueThe cooler's custody seal, if present, is intact.

TrueThe cooler or samples do not appear to have been compromised or

tampered with.

TrueSamples were received on ice.

FalseCooler Temperature is acceptable.

TrueCooler Temperature is recorded. 8.4°C IR # 50

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the sample IDs on the containers and

the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in

diameter.

N/AMultiphasic samples are not present.

N/ASamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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Appendix D

Soil Profile Package Information

Appendix D - Soil Profile Package Requirements Maplewood Farms Site Preparation Plan

Berlin, Massachusetts

A Soil Profile Package shall be prepared by the candidate site owner/generator and Engineering Consultant/LSP, signed and dated for review by the owner/Lighthouse and the Site LSP.

The following information is required in the Soil Profile Package to obtain approval for the reuse of soil at the above referenced location: 1. Name of property owner (generator), and Engineering Consultant/LSP.

2. Project Name and Location, MCP Release Tracking Number (if applicable), and MCP historyrelative to candidate soils.

3. The quantity of soil planned for reuse, and the amount of soil samples collected (minimum 1sample/500 cy of soil).

4. A site sketch or map of the soils depicting sampling locations and field screening results.

5. The analytical data sheets and a summary of the analytical results in comparison toAcceptance Criteria in the Riverview Industrial Park Soil Re-use Management Plan,demonstrating that results meet the criteria and a discussion on the basis for averaging, ifutilized.

6. Discussion of shipment schedule, transporter (if known), and other pertinent coordinationitems.

A summary of the Acceptance Criteria is attached as Table 1. This information should be provided with the Soil Profile Package for completion.

Two copies of the Soil Profiling Package must be sent to Lighthouse which will be reviewed, and; if acceptable, forwarded to the Site LSP. The Site LSP will review the package and will issue a letter of acknowledgement and acceptance to Lighthouse or the generator for countersignature. The package will then be forwarded to the generator.

If the candidate soil is non-impacted natural soil, a generator/LSP certification letter will be required for review by Lighthouse and the Site LSP.

Appendix E

Private Well Completion Report and

Testing

Maplewood Farms Re-use Management... · 2018-05-12 · Maplewood Farms Prepared by: ARCADIS U.S.,...

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