LCMS Report - AbMole · LCMS Report Injection Date : Fri, 28. Feb. 2020 Inj. Vol. : 5ul Acq...
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L C M S Report Injection Date : Fri, 28. Feb. 2020 Inj. Vol. : 5ul Acq Operator : lcms-5 Location : Vial 32 Acq. Method : D:\data-lcms-5\2020\02-20\28\1\P-05-95.M Method Info. : column:ZORBAX C18 5um 4.6*50mm ;mobile phase:B(ACN) ! A(0.02%NH4Ac); gradient(B%) as Acq.Method above min 0 2 4 6 mAU 0 200 400 600 800 1000 1200 1400 4.732 3.333 3.148 4.412 4.125 min 0 2 4 6 mAU 0 100 200 300 3.333 3.149 4.124 min 0 2 4 6 0 200000 400000 600000 800000 1000000 3.171 3.353 4.149 ========================================================================== Integration Results ========================================================================== Signal 1: DAD1 A, Sig=214,8 Ref=off # R.T. Type Height Height% Width Area Area % ----------------------------------------------------------------- 1 3.148 MF 4.584 0.286 0.050 13.640 0.197 2 3.333 MF 5.231 0.327 0.050 15.564 0.225 3 4.125 MF 1578.874 98.656 0.072 6852.601 98.925 Instrument 1 Fri, 28. Feb. 2020 07:27:31 pm Page 1 of 2 Sample Name : Opaganib (ABC294640) -02 Data File : D:\DATA-LCMS-5\20 20\02-20\28\1\ Opaganib (ABC294640) -02 .D DAD1 A, Sig=214,8 Ref=off (2020\02-20\28\1\Opaganib (ABC294640)-02.D) DAD1 B, Sig=254,8 Ref=off (2020\02-20\28\1\Opaganib (ABC294640)-02.D) MSD1 TIC, MS File (D:\DATA-LCMS-5\2020\02-20\28\1\Opaganib (ABC294640)-02.D) ES-API, Pos, Scan, Frag: 80
Transcript of LCMS Report - AbMole · LCMS Report Injection Date : Fri, 28. Feb. 2020 Inj. Vol. : 5ul Acq...
L C M S Report
Injection Date : Fri, 28. Feb. 2020 Inj. Vol. : 5ulAcq Operator : lcms-5 Location : Vial 32Acq. Method : D:\data-lcms-5\2020\02-20\28\1\P-05-95.MMethod Info. : column:ZORBAX C18 5um 4.6*50mm ;mobile phase:B(ACN)
!A(0.02%NH4Ac); gradient(B%) as Acq.Method above
min0 2 4 6
mAU
0200400600800
100012001400
4.7
32
3.3
33 3
.148
4.4
12
4.1
25
min0 2 4 6
mAU
0
100
200
300
3.3
33 3
.149
4.1
24
min0 2 4 60
200000
400000
600000
800000
1000000
3.1
71 3.3
53
4.1
49
==========================================================================Integration Results
==========================================================================
Signal 1: DAD1 A, Sig=214,8 Ref=off
# R.T. Type Height Height% Width Area Area % ----------------------------------------------------------------- 1 3.148 MF 4.584 0.286 0.050 13.640 0.197 2 3.333 MF 5.231 0.327 0.050 15.564 0.225 3 4.125 MF 1578.874 98.656 0.072 6852.601 98.925
Instrument 1 Fri, 28. Feb. 2020 07:27:31 pm Page 1 of 2
Sample Name : Opaganib (ABC294640)-02Data File : D:\DATA-LCMS-5\2020\02-20\28\1\Opaganib (ABC294640)-02.D
DAD1 A, Sig=214,8 Ref=off (2020\02-20\28\1\Opaganib (ABC294640)-02.D)
DAD1 B, Sig=254,8 Ref=off (2020\02-20\28\1\Opaganib (ABC294640)-02.D)
MSD1 TIC, MS File (D:\DATA-LCMS-5\2020\02-20\28\1\Opaganib (ABC294640)-02.D) ES-API, Pos, Scan, Frag: 80
# R.T. Type Height Height% Width Area Area % ----------------------------------------------------------------- 4 4.412 FM 4.007 0.250 0.067 16.026 0.231 5 4.732 FM 7.689 0.480 0.063 29.202 0.422-----------------------------------------------------------------
Signal 2: DAD1 B, Sig=254,8 Ref=off
# R.T. Type Height Height% Width Area Area % ----------------------------------------------------------------- 1 3.149 BB 2.761 0.620 0.048 8.471 0.509 2 3.333 MF 2.642 0.593 0.050 7.915 0.476 3 4.124 VB 439.934 98.787 0.060 1647.349 99.015-----------------------------------------------------------------
Signal 3: MSD1 TIC, MS File
# R.T. Type Height Height% Width Area Area % ----------------------------------------------------------------- 1 3.171 MM 57007.227 4.226 0.069 237690.500 2.224 2 3.353 MM 226998.031 16.826 0.072 973854.875 9.112 3 4.149 MM 1.065e+006 78.948 0.148 9.476e+006 88.664-----------------------------------------------------------------
m/z200 400 600 8000
20
40
60
80
441
.3
495
.3
623
.2
339
.0
141
.1
302
.2
175
.1
247
.5
323
.1 3
01.1
174
.1
m/z200 400 600 8000
20
40
60
80
272
.2 2
71.2
m/z200 400 600 8000
20
40
60
80
384
.2 3
81.2
========================================================================== *** End of Report ***
Instrument 1 Fri, 28. Feb. 2020 07:27:31 pm Page 2 of 2
*MSD1 SPC, time=3.175 of D:\DATA-LCMS-5\2020\02-20\28\1\Opaganib (ABC294640)-02.D ES-API, Pos, Scan, Frag: 80
*MSD1 SPC, time=4.158 of D:\DATA-LCMS-5\2020\02-20\28\1\Opaganib (ABC294640)-02.D ES-API, Pos, Scan, Frag: 80
*MSD1 SPC, time=3.350 of D:\DATA-LCMS-5\2020\02-20\28\1\Opaganib (ABC294640)-02.D ES-API, Pos, Scan, Frag: 80
