LABORATORY NOTEBOOK (Pre-lab)
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Transcript of LABORATORY NOTEBOOK (Pre-lab)
LABORATORY NOTEBOOK(Pre-lab)
•TITLE AND DATE
• OBJECTIVES
•TABLE OF PHYSICAL DATA • Include the MW, bp, density, and hazard information for 2-bromoheptane, cis-2-heptene, trans-2-heptene, 1-heptene, methanol, and t-butanol. • Include the MW, mp, and hazard information for sodium methoxide and potassium t-butoxide.
•CHEMICAL EQUATION • Include the general chemical equation from page 99.
• PROCEDURE • Include a brief outline of the procedure for the experiment. Do NOT copy directly from the lab manual.• Include a reference to the lab manual including page numbers where the actual procedure can be found.
LABORATORY NOTEBOOK(In-lab)
OBSERVATIONS/CALCULATIONS Identity of base and solvent pair Initial weight of 2-bromoheptane Initial weight of base used Initial volume of alcohol used VR setting for reflux VR setting for distillation Theoretical yield calculation % yield calculation Physical state and color of product GC vial slot # Give an example of an adjusted area % calculation