Lab Scale Freeze Dryer (Lyophilizer)

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~ 1 ~ FD scale freeze dryer FD SERIES Freeze Dryer Lab Scale Freeze Dryer (Lyophilizer) Description: Vacuum freezing dryer is widely used in the medical, pharmaceutical, biological, chemical and food and other fields, FD series is suitable for laboratory use or low-volume production to meet the requirements of most laboratories conventional lyophilization. Features: Microprocessor controls Environment-friendly, conform to international standard (CE, ISO); Communication interface & LCD display include drying curve, vacuum, condenser temp., run time, ambient temperature; LCD touch display panel is optional With pre-freezing for samples, widely open condenser, without inner coil; Large refrigerating capacity and slight noise of DANFOSS(SECOP) compressor; The pre-cooling shelf can be used as draft tube to accelerate drying speed; Condenser and the operation panel are made of 304 stainless steel, which is corrosion-resistant and easy to clean; Transparent bell-cap drying kiln is safe and easy to observe; Stainless steel sample shelf, the space among common sample tray can be adjusted; Novel design, small size and simple operation; For water based samples, the -55°C condenser is the perfect choice with effective cost. For samples containing solvents or with low eutectic points, the -80 C dual cascade refrigeration condenser provides maximum performance. For labs that needs quick turn-around, electric heating defrost is optional. Nitrogen inflation valve is optional. It includes the following types: Normal type, Top-press type, multi-manifold T type and multi-manifold Top-press type to meet the various requirements.

Transcript of Lab Scale Freeze Dryer (Lyophilizer)

Page 1: Lab Scale Freeze Dryer (Lyophilizer)

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FD scale freeze dryer

FD SERIES Freeze Dryer

Lab Scale Freeze Dryer (Lyophilizer)

Description: Vacuum freezing dryer is widely used in the

medical, pharmaceutical, biological, chemical

and food and other fields, FD series is suitable

for laboratory use or low-volume production to

meet the requirements of most laboratories

conventional lyophilization.

Features: Microprocessor controls

Environment-friendly, conform to international

standard (CE, ISO);

Communication interface & LCD display

include drying curve, vacuum, condenser

temp., run time, ambient temperature; LCD

touch display panel is optional

With pre-freezing for samples, widely open

condenser, without inner coil;

Large refrigerating capacity and slight noise of

DANFOSS(SECOP) compressor;

The pre-cooling shelf can be used as draft tube

to accelerate drying speed;

Condenser and the operation panel are made

of 304 stainless steel, which is corrosion-resistant

and easy to clean;

Transparent bell-cap drying kiln is safe and

easy to observe;

Stainless steel sample shelf, the space among

common sample tray can be adjusted;

Novel design, small size and simple operation;

For water based samples, the -55°C condenser

is the perfect choice with effective cost. For

samples containing solvents or with low

eutectic points, the -80 C dual cascade

refrigeration condenser provides maximum

performance.

For labs that needs quick turn-around,

electric heating defrost is optional.

Nitrogen inflation valve is optional.

It includes the following types: Normal type,

Top-press type, multi-manifold T type and

multi-manifold Top-press type to meet the

various requirements.

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FD scale freeze dryer

FD SERIES Freeze Dryer

FD-10 Bench-top type Model FD-10-R FD-10-MR FD-10-TP FD-10-MTP FD-10-MT

Image

Total shelf area 0.12 m2 0.12 m2 0.07m2 0.07m2 /

Shelf size(mm) Φ200*4pcs Φ200*4pcs Φ180 * 3pcs Φ180 * 3pcs /

Max shelf qty 6 pcs 6 pcs 3 pcs 3 pcs /

Vials load

capacity

Φ12mm 920 Pcs 920 Pcs 560 Pcs 560 Pcs

24 ports Φ16mm 480 Pcs 480 Pcs 285 Pcs 285 Pcs

Φ22mm 260 Pcs 260 Pcs 165 Pcs 165 Pcs

Cold Trap Temp. <-55°C (-80°C oreven lower is optional)

Ultimate Vacuum <10 Pa

Ice capture capacity 3~4kg/24hours

Power 700W

Voltage 220v/50Hz or 110v/60Hz

Dimensions 460*625* (370+430)(mm)

Weight 100 kg 110kg 105kg 120kg 65kg

FD-12 FLOOR TYPE

Model FD-12-R FD-12-MR FD-12-TP FD-12-MTP FD-12-MT

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Total shelf area 0.12 m2 0.12 m2 0.1 m2 0.1 m2 /

Shelf size (mm) Φ200*4pcs Φ200 * 4pcs Φ180 * 3pcs Φ180 * 3pcs /

Vials load

quantity

Φ12mm 920 Pcs 920 Pcs 560 Pcs 560 Pcs

24 ports Φ16mm 480 Pcs 480 Pcs 285 Pcs 285 Pcs

Φ22mm 260 Pcs 260 Pcs 165 Pcs 165 Pcs

CondenserTemp. <-55°C (-80°C or even lower is optional)

Vacuum Degree <10 Pa

Condenser capability 4 Kg/24h

Power 750W

Voltage 220v/50Hz or 110v/60Hz

Dimensions 460×556×(720+465)(mm)

Weight 120 kg 135kg 130kg 140kg 76 kg

FD-18 FLOOR TYPE

Model FD-18-R FD-18-MR FD-18-TP FD-18-MTP FD-18-T

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FD scale freeze dryer

FD SERIES Freeze Dryer

Image

Total shelf area 0.18~0.27 m2 0.18~0.27 m2 0.1 m2 0.1 m2 /

Shelfsize (mm) Φ240 * 4pcs Φ200 * 3pcs Φ200 * 3pcs /

Vials load

capacity

Φ12mm 1320 Pcs 1320 Pcs 990 Pcs 990 Pcs

12 ports Φ16mm 740 Pcs 740 Pcs 555 Pcs 555 Pcs

Φ22mm 360 Pcs 360 Pcs 270 Pcs 270 Pcs

Condenser Temp. <-55°C (-80°C or even lower is optional)

Vacuum Degree <10 Pa

Ice capture capability 6 Kg/24h

Power 1400W

Voltage 220v/50Hz or 110v/60Hz

Dimensions 540×610×(963+445)(mm)

Weight 170 kg 185kg 185kg 195kg 105 kg

FD-18S type (Shelves heating & program control)

Model FD-18S-R FD-18S-MR FD-18S-TP FD-18S-MTP FD-18S-RA FD-18S-TPA

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Shelves area 0.18m2 0.18m2 0.09m2 0.09m2 0.18m2 0.12 m2

Shelves size Φ240mm *4 pcs Φ240mm *4 pcs Φ200mm * 3 Φ200mm * 3 Φ240mm *4 pcs Φ200mm * 3

Quantity can be customized

Vials load

capacity

ф12mm 1320pcs 1320pcs 990pcs 990pcs 1320pcs 990pcs

ф16mm 480pcs 480pcs 285pcs 285pcs 480pcs 285pcs

ф22mm 360pcs 360pcs 270pcs 270pcs 360pcs 270pcs

Condenser temp. <-60°C (-80°C or even lower is optional)

Shelves temp. -55~60°C

Ultimate vacuum <10 Pa

Condenser capability 6 Kg/24h

Power 1530 W

Voltage 220v/50Hz or 110v/60Hz

Standard Configuration Stainless steel condenser with opening, stainless steel operation tops, seamless welding with round cornerwhich is

anti-corrosion and easy to clean

Stainless steel shelf & rack, 4 or 6 pcs shelves optional, shelf removable and spacing height adjustable

Stainless steel pre-cooling rack with metal cover

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FD scale freeze dryer

FD SERIES Freeze Dryer

Integrally molded glass dried barrel adopted special plastic will not break

Used SECOP (DANFOSS) quality compressor, high performance condenser fan, LCD touch display, history data can be

stored, searched and exported to computer.

Model R TP MR MTP MT

Image

Description Normal type Stoppering 8 port manifold Stoppering + 8 ports

manifold

Multi-ports manifold

Freeze Dryer ● ● ● ● ●

Transparent dry

chamber

● ● ● ●

Vacuum pump ● ● ● ● ●

Stoppering device ● ●

Manifold Ports 8 ports (28/ 32mm) 8 ports (28/ 32mm) 12 or 24 ports

Freezing rack ● ● ● ● ●

Drying rack ● ● ● ●

Tray 4 pcs 3 pcs 4 pcs 3 pcs

Optional items

Item No. Item Name Item No. Item Name

FD1001 -80°C Condenser FD1009250 250ml flask

FD1002 RS232 & Software FD1009500 500ml flask

FD1003 Defrost device FD10091000 1000ml flask

FD1004 Refrigerant R404a, R502, R23 and etc FD1010 Leybold vacuum pump

FD1005 Oil mist filter FD1011 Touch LCD display

FD1006 Shelves heating & Program segment control

Can stored 16 programs, each program can be set up

36segments, correct program data in computing, memorize

the drying curve

FD1012 Anti-back oil device

FD1007 Additional trays (6pcs) FD1013 Eutectic point test device

FD1008 Removable lid for drying drum FD1014 Vacuum regular device

FD1009100 100ml flask

Vacuum Pump

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FD scale freeze dryer

FD SERIES Freeze Dryer

Adapter Quick-release pipe Small-bore pipe Oil mist collector

Specifications of vacuum pump

Pilot scale automaticfreeze dryer Features: Rectangular freezing-dryingin one chamber,

inside round corner, easy to clean. PLC control with LCD touch graphic display, can

be operated in auto, semi-auto and manual mode.

Electric or silicone oil shelf heating can be choose.

Shelf temperature adjustable, controllable, explore suitable for pilot and production processes.

32 programs, each program can be set as 36 segments, curve can be stored, processingparameters can be modified in real time.

Integrity or separately condenser and chamber can be choose.

Fitted with inflation valve , rechargeable dry inert gas.

Main characteristics:

Model 2XZ-0.5 2XZ-1 2XZ-2C 2XZ-4C 2XZ-6C 2XZ-8C 2XZ-15C

Pumping Speed: L/S 0.5 1 2 4 6 8 15

Ult.

Vacuum

Pa

Without gas ballast ≤6×10-2

With gas ballast ≤6.5 ≤1.33

Speed: r/min(50HZ) 1400

Power Required: Kw 0.18 0.25 0.37 0.55 0.75 1.1 1.5

Diameter of inlet port: mm 16 16 25 25 40 40 40

Temp. rise of pump oil: °C ≯40 ≯45 ≯45 ≯65 ≯70

Oil capacity: L 0.60 0.70 0.10 1.2 2.0 3.0 4.0

Overall Dimensions: mm

447

168

260

469

168

260

514

168

282

514

168

282

565

200

342

650

240

430

770

240

430

Weight: kg 16 17 20 22 40 60 75

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FD scale freeze dryer

FD SERIES Freeze Dryer

Drying chamber made by SS 304 or SS316L, adopted high strength, high transmittance plexiglassdoor, easy to observe.

Drum-type cold trap,with high transmittance plexiglasswindow. Dual-stage cooling, famous hermetic compressor which is low noise, capillary throttling

technology, air-cooled or water-cooled is available. Two-stage rotary vane vacuum pump, vacuum degree is automatic adjust and can be

set.Brazed plate heat exchanger, GUNDFOS shielded circulating pump and PID control electric heating component; circulation liquid used Low-temperature low- viscosity silicone oil

FD-10F Series

FD-10F Series

Model FD-10F-R (Silicon oil heating) FD-10-RE (Electric heating)

FD-10F-TP (Silicon oil heating) FD-10F-TPE (Electric heating)

Specification Normal With stoppering

Picture

Drying chamber

Shelf area 0.2 m2 0.1 m2 Shelf quantity 2 pcs 1pc

Shelf temp. range -70°C ~ +65°C -50°C ~ 65°C

Shelf spacing 70mm Shelf dimension 265*400*25mm Φ22mmvials(piece) 440 220 Φ16mm vials (piece) 868 434 Φ12mmvials (piece) 1554 777

Condenser Maxtemp.

≤-80°C ≤-55°C

Ice capture capacity 3~5 Kg/24hs Electric defrost Optional

Basic parameters

Vacuum degree ≤10 Pa Style of cooling Air-cooled Dimension(L*W*H) 605*610*1200mm 605*610*1330mm

FD-30F Series

FD-30F Series Model

FD-30F-R (Silicon oil) FD-30F-ER (electric)

FD-30F-TP

Type Normal With stoppering

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FD scale freeze dryer

FD SERIES Freeze Dryer

Picture

Drying chamber

Freeze-drying area 0.4 m2 0.3 m2 Shelf quantity 4+1 pcs 3+1 pcs Shelf temp. range -50~70°C -50~70°C Temp. Difference +/-1°C (balance) +/-1°C (balance) Shelf dimension 300*320*15mm 300*340*15mm Shelf spacing 50mm 70mm

Vial load capacity φ22 vials (piece) 728 546 φ16 vials (piece) 1440 1080 φ12vials (piece) 2600 1950

Cold trap Cold trap temperature

≤-70°C ≤-55°C

≤-70°C

Condenser capability 6 Kg/24h 6 Kg/24h Defrost Nature Electric or hot gas

Basic parameters

Style of top-press - Hydraulic pressure Ultimate vacuum ≤10Pa ≤10Pa Dimension 880*735*1310 mm 1280*900*1630 mm Weight 300 kg 400 kg Voltage Freeze dryer 380V±10%50Hz 380V±10%50Hz Power 4KW 4.2KW

FD-50F Series

FD-50F Series Model

FD-50F-R FD-50F-RE

FD-50F-TP

Type Normal With stoppering

Picture

Drying chamber Freeze-drying area 0.7 m2 0.5 m2

Shelf quantity 4+1 pcs 3+1 pcs Shelf temp. range -50~70°C -50~70°C Temp. Difference +/-1°C (balance) +/-1°C (balance) Shelf dimension 300*320*15mm 300*340*15mm Shelf spacing 50mm 100mm Material SS304 SS304

Vial load capacity φ22 vials (piece) 1408 1056

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FD scale freeze dryer

FD SERIES Freeze Dryer

φ16 vials (piece) 2728 2046 φ12vials (piece) 4920 3690

Cold trap Cold trap temperature

≤-70°C ≤-55°C

≤-70°C

Condenser capability 10 Kg/24h 10 Kg/24h Electric defrost Nature Electric or hot gas

Basic parameters Style of top-press - Hydraulic pressure Ultimate vacuum ≤10Pa ≤10Pa Dimension 960*785*1450 mm 1165*1310*1950 mm Weight 890 kg 950 kg Voltage Freeze dryer 380V±10%50Hz 380V±10%50Hz Power 6.5 kw 7 kw

FD-100F Series

FD-100F Series Model FD-100F-R FD-100F-TP Specification Normal With stoppering

Picture

Drying chamber

Drying area 1.0 m2 1.0 m2 Shelf quantity 6+1 layer 4+1 layer Shelf Temp range -50~70°C -50~70°C Shelf temp. difference

±1°C (balance) ±1°C (balance)

Shelves size 480*360*15mm 600*480*20mm Height space 70mm 100mm Φ22 vials (PCS) 2112 2428 Φ16 vials(PCS) 4092 4706 Φ12vials (PCS) 7920 8400

Cold trap

Condenser temp. ≤-70°C ≤-70°C Condenser capability

15 Kg/24h 15 Kg/24h

Defrost Electric or hot gas Electric or hot gas

Basic parameters

Vacuum degree ≤10 Pa ≤10 Pa Style of top-press - Hydraulic pressure Cooling type Water or Air Water or Air Dimension 1030*750*1700 mm 1300*1200*2200 mm Voltage 3p-380~400V/50Hz 3p-380~400V/50Hz

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FD scale freeze dryer

FD SERIES Freeze Dryer

FD-200F Series

Specifications:

FD-200F

Series

Model FD-200F-R FD-200F-TP

Specification Normal type With Stopper

Drying

chamber

Freeze-drying area 2.25 m2 1.98 m2

Shelves 5+1pcs 4+1pcs

Shelf Temperature -50~70°C -50~70°C

Shelf Temp.

Accuracy ± 1°C ± 1°C

Shelf spacing 110mm

(70 ~ 180mm customizable)

110mm

(70 ~ 180mm customizable)

Size of shelves 500*900*20 mm 610*810*20 mm

Material SS304 or SS316

Vials load

capacity

φ22 vials (PCS) 4100 3600

φ16 vials (PCS) 7800 6800

φ12 vials (PCS) 14400 12600

Condenser

Max temperature ≤-70°C

Water-capture

capability 40 Kg/24h 40 Kg/24h

Material Capacity 22L 20L

Defrost spray + soaking spray + soaking

Material SS304 or SS316

Basic

parameters

Vacuum degree ≤10 Pa ≤10 Pa (Range:1~300Pa)

Dimension 1200*2100*1700 mm 1300*3300*2500 (mm)

Max Power 13.5kw 15kw

Weight 2300 kg 2600 kg

Data Process RS232 Interface with software

Refrigeration Compressor Bitzer or TECUMSEH, 2 set

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FD scale freeze dryer

FD SERIES Freeze Dryer

unit Power 7 Kw

Refrigerant R507 & R23

Cooling type Air cooled or water cooled

Pressure controller DANFOSS

Expansion valve DANFOSS