Lab Sample Preparation Procedures · Lab Sample Preparation Procedures March 20, 2006 14:15:18 Page...

March 20, 2006 14:15:18Lab Sample Preparation Procedures

of 91

0800597 Ogden Railyard (US EPA Region 8)

Source Procedure ID Procedure Name Citation

1668

200.7

2216-90

3510C

7470A

7471A

8015B

8015B MOD

3010-A

3050-B

3510-B

3550-B

unknown

unknown

unknown

unknown

Unknown

Unknown

Unknown

Unknown

Acid Digestion of Aqueous Samples and Extracts forTotal Metals for Analysis fy FLAA or ICPSpectrometry

Acid Digestion of Sediments, Sludges, and Soils forMetals Analysis by FLAA/ICP or GFAA/ICPMS

Separatory Funnel Extraction, Liquid-Liquid

Ultrasonic Extr. of Nonvolatile/Semivolatile Organicsfrom Soils, Sludges, and Wastes (NoOrganophosphorus Compounds)

Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --








USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III




0800597

0800597

0800597

0800597

0800597

0800597

0800597

0800597

USEPA

USEPA

USEPA

USEPA


of 91

1119USBR Bureau of Reclamation


200.7-T Total Metals Preparation for EPA 200.2 USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III

USEPA


of 91

11DELMOD Delaware River Basin Commission


9230-C-2

200.2

Fecal Streptococcus and Enterococcus Group,Membrane Filter Sample Preparation

Preparation for Water, Soil, or Waste Samples

American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111

APHA

USEPA


of 91

11NPSWRD National Park Service


SEDSIEVELT2MM

SEDSIEVELT63UM

Sediment Sieved to <2mm

Sediment Sieved to <63 micrometers



11NPSWRD

11NPSWRD


of 91

21CAOCSD Orange County Sanitation District California


LPROC001 organics USEPA, 1982, Test Method for the Determination of PolychlorinatedBiphenyls in Transformer Fluid and Waste Oils, USEPA, EPA 600/4-81-045

21CAOCSD


of 91

21COL001 Colorado Dept. of Public Health & Environment


200.2 Preparation for Water, Soil, or Waste Samples USEPA, 1994, Methods for the Determination of Metals inEnvironmental Samples, Supplement I, USEPA, EPA 600-R-94-111

USEPA


of 91

21DCBAWQ District of Columbia Dept of Health, Water Quality Division


LSP-001

LSP-002

LSP-003

LSP-004

Filtration of water samples, 0.45

Preparation of biological samples for inorganicchemical analysis

Manual digestion with persulfate for polyphosphatesand phosphorus compounds

Filtration of water samples, particle retention =1.6um

USEPA, 1983, Methods for Chemical Analysis of Water and Wastes,USEPA, EPA 600/4-79-020




21DCBAWQ

21DCBAWQ

21DCBAWQ

21DCBAWQ


of 91

21FLACEP Alachua County Environmental Protection Department (Florida)


351.2

365.2/365.3

FIELD_FLTRD

FILTRATION

3005-A

351.2

Phosphorus- Total

Field Filtered

Filtration

Total Recoverable and Dissolved Prep for FLAA, ICP






21FLACEP

21FLACEP

21FLACEP

21FLACEP

USEPA


of 91

21FLAVON Avon Park Air Force Range - 18 ASOG DET 1 OL A/CEV


EPA 351.2 11

SM 10200 H 1

SM 4500-P B 5

Acid digestion by block digestor

Pigment extraction

Persulfate digestion




21FLAVON

21FLAVON

21FLAVON


of 91

21FLBFA FL Dept. of Environmental Protection


DIG-TKN-TP

DIG-TP-LOW

DIG-TKN-TP

Preparation method for TKN and TP

Preparation method for low-level phosphorus

Preparation method for TKN and Total Phosphorus




21FLBFA

21FLBFA

21FLCMP


of 91

21FLBREV Brevard County Stormwater Utility Department (Florida)


10200-H

160.2

351.2

365.4

SW846-3005A

Chlorophyll a

TSS

TKN

Total Phosphorus

Metals


USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008




21FLBREV

21FLBREV

21FLBREV

21FLBREV

21FLBREV


of 91

21FLBROW Broward Co Dept of Natural Resource Protection (Florida)


P001

P002

P003

P004

Bacti Prep

Chlorophyll Extraction

EPA 600

MIBK EXTRACTION




USEPA, 1996, Method 1637: Determination of Trace Elements inAmbient Waters by Chelation Preconcentration with GFAA., USEPA,EPA 821/R-96-004

21FLBROW

21FLBROW

21FLBROW

21FLBROW


of 91

21FLCEN Florida Department of Environmental Protection


10200-H

1631

200.2

Prep chlorophyll and pheophytin

Mercury


Lou, Ley, 2002, Volume Name, Department of Environmental ProtectionCentral District, v.1

USEPA, 1999, Method 1631, rev B: Mercury in Water by Oxication,Purge and Trap, and Cold Vapor Atomic Fluorescence Spectrometry.,USEPA, EPA 821/R-99-005


21FLCEN

21FLCEN

USEPA


of 91

21FLCMP FL Dept. of Environmental Protection


351.2

DIG-TKN-TP

351.2

365.4

LAB

TKN Sample Preparation Procedure


Preparation for Ammonia+Organic Nitrogen, Total(as N)

Preparation for Phosphorus, Total (as P)

Methodology for Chemical Analysis



FDEP Central Lab, 1999, FDEP SOP1, FDEP Central Lab, 1-1000



21FLCMP

21FLCMP

21FLFTM

21FLFTM

21FLPNS


of 91

21FLDADE Dade Environmental Resource Management (Florida)


1310-A

1311

1311-HG

1311-MT

1311-V

1625P

200.2

200.2-M

200.7-T

200.8-CR

200.8-T

Extraction Procedure Toxicity Test Method andStructural Integrity Test

TCLP Preparation for Semivolatiles

TCLP Preparation for Mercury

TCLP Preparation for Metals

TCLP Preparation ZHE

BNA (isotopic dilution) Preparation


Total Recoverable Metals Digestion

Total Metals Preparation for EPA 200.2

Clean Room Preparation for EPA 200.8













USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA


of 91



3005-A

3010-A

3015

3015-M

3020-A

3040

3040-A

3050-A

3050-B

3051



Microwave Assisted Acid Digestion of AqueousSamples and Extracts

Aqueous Sample Prep for Total Metals (modified)Suspended Solids, ICP,GFAA,ICP-MS

Acid Digestion of Aqueous Samples and Extracts forTotal Metals for Analysis by GFAA Spectroscopy

Oily Waste Prep for Soluble Metals by AA and ICP

Dissolution Procedure for Oils, Greases, and Waxes

Acid Digestion of Sediments, Sludges, and Soils


Microwave Assisted Acid Digestion of Sediments,Sludges, Soils, and Oils











USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA


of 91



3510-B

3510-C

3520-B

3520-C

3540-B

3540-C

3550-A

3550-B

3580-A

3585

50.6


Separatory Funnel Liquid-Liquid Estraction

Continuous Liquid-Liquid Extraction for Organics

Continuous Liquid-Liquid Extraction for Organics

Soxhlet Extraction for Nonvolatile and SemivolatileOrganic Compounds from Solids, Solid SamplesOnly

Soxhlet Extraction for Nonvolatile and SemivolatileOrganics from Soils, Sludges, and Wastes

Ultrasonic Extraction of Nonvolatile and SemivolatileOrganic Compounds form Soils, Sludges, andWastes


Waste Dilution

Waste Dilution

Phase Separation and Aliquotting











USEPA, 19--, CLP SOW for Inorganics Analysis-IHC01_3, USEPA,IHC01_3

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA


of 91



5030-A

548.1-P

549.1-P

8150-P

P-010-1

SFSAS_FT_PREP

Sample Preparation and Extraction for VolatileOrganic Analysis by Purge-and Trap

Endothall Preparation

Diquat and Paraquat Preparation

Herbicide Preparation Portion of 8150

Preparation for Pesticides/PCB in Water/Soil

Fish Tissue Preparation Technique





USEPA, 1994, Field Methods Compendium., USEPA, FMC_METHODS

USEPA, 1980, Methods for the Sampling and Analysis of PriorityPollutants in Sediments and Fish Tissue, USEPA, EPA-600/4-81-055

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA


of 91

21FLEECO Lee County (Florida)


3030-E Nitric Acid Digestion of Metals American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

APHA


of 91

21FLFMRI Florida Fish & Wildlife C C / Marine Research Institute


PROC 1 Field Hydrolab Sample Procedures ORG-01 - U.S. Environmental Protection Agency, 2001, NationalCoastal Assessment Field Operations Manual, USEPA, Unknown

21FLFMRI


of 91

21FLFTM Florida Department of Environmental Protection


DIG-TKN-TP

245.1

351.2

365-1

365.4

DIG-TKN-TP-2

PK-SETTLE

SOP-AB02_1

SOP-AB04

SOP-AB05

SOP-AB10_1

SOP-AB11

SOP-BB01

SOP-BB02

SOP-TA08_01/08_

W-M-DIGEST

200.2

200.7-T


Mercury Analysis


Preparation for Total Phosphorus in Water



Pheophytin preparation analysis

Phytoplankton Identification - Diatom

Phytoplankton Identification - Wet Taxa

DEP Phytoplankton Preparation - Wet Taxa

DEP-SOP-0/001

Proceedure for Phytoplankton Sample Receipt andSample Handling for Taxonomic Analysis

Preparation for Bacterial Analysis

Preparation for Chlorophyll-A (Monochromatic) &Pheophytin-A (Monochromatic)

Preparation for Algal Growth Potential

ICP Metals Digestion





















21FLCMP

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

21FLFTM

USEPA

USEPA


of 91

21FLGFWF Florida Fish and Wildlife Conservation Commission


4500-P-B(1)

4500-P-B(5)

3030-B

3030-E

4500-NH3(B)

Preliminary filtration for orthophosphorus 0.45ummembrane filter

Persulfate digestion for total phosphorus

Preliminary Filtration of Metals Samples

Nitric Acid Digestion of Metals

Preliminary Distillation Step






21FLGFWF

21FLGFWF

APHA

APHA

APHA


of 91

21FLGW FL Dept. of Environmental Protection


351.2

365.4

SOP-BB02

351.2 SEDIMENT

365.1

365.4 SEDIMENT

MERCURY

ORGANIC EXT

SOP-AB02_1

SOP-AB11

SOP-BB02

SOP-TA08_01-04

TOTAL DIGESTION

200.2




Preparation of samples for total kjeldahl nitrogenanalysis

Preparation for Total Phosphorus in Water

Preparation of samples for total phoshorus analysis

Preparation of solid and liquid matrices for mercuryanalysis

Extraction of non-volatile and semi-volatile organiccompounds from soils, sludges, wastes

Preparation of Periphyton Diatoms

Proceedure for Phytoplankton Sample Receipt andSample Handling for Taxonomic Analysis

Proceedure for Phytoplankton Sample Filtering

Proceedure for Algal Growth Potential

TOTAL TOTAL DIGESTION





Laura Morse, 2000, Florida Ambient Monitoring Network QualityAssurance Plan, FDEP, vol 1











21FLFTM

21FLFTM

21FLFTM

21FLGW

21FLGW

21FLGW

21FLGW

21FLGW

21FLGW

21FLGW

21FLGW

21FLGW

21FLGW

USEPA


of 91

21FLLCPC Lake County Water Resource Management (Florida)


GENPREP General Preparation LAKE COUNTY WATER RESOURCE LAB, 2001, LAKE COUNTYWATER RESOURCE MANAGEMENT QUALITY SYSTEMS MANUAL,LAKE COUNTY WATER RESOURCE MANAGEMENT, ALL PAGES

21FLLCPC


of 91

21FLLEON Leon County Public Works (Florida)


3510-C Separatory Funnel Liquid-Liquid Estraction USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III

USEPA


of 91

21FLLOX Loxahatchee River District (Florida)



USEPA


of 91

21FLMANA Manatee County Environmental Management Dept (Florida)


GENERIC General Listing of Field and Lab AnalyticalProcedures for Manatee County

Greg Blanchard, 2002, General Listing of Field and LaboratoryAnalytical Procedures for Manatee County, Manatee County, 1

21FLMANA


of 91

21FLMCGL McGlynn Laboratories, Inc


10200-H Chlorophyll a-b-c Determination American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

21FLMCGL


of 91

21FLNWFD Northwest Florida Water District



USEPA


of 91

21FLORAN Orange County Environmental Protection (Florida)


3020A

EPA100.1

EPA110.2

EPA120.1

EPA130.1

EPA150.1

EPA160.1

EPA160.2

EPA160.3

EPA160.4

EPA170.1

EPA180.1

EPA200.7

EPA210.2

Metals Prep

Depth, Secchi disk depth

True Color

Specific Conductance

Harness by titration

pH

Volatile Solids

Total Suspended Solids

Total Solids

Dissolved Solids

Temperature, water

Turbidity

ICAP Metals

Beryllium















21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN


of 91



EPA213.2

EPA239.2

EPA245.1

EPA270.2

EPA272.2

EPA279.2

EPA310.1

EPA325.3

EPA350.1

EPA351.2

EPA353.2

EPA360.2

EPA365.1

EPA375.4

Cadmium

Lead

Mercury

Selenium

Silver

Thallium

Alkalinity

Chloride

Ammonia, unionized

Nitrogen, Kjeldahl

Nitrogen Suite

Dissolved Oxygen

Phosphorus Suite

Sulfate















21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN


of 91



EPA405.1

EPA410.4

EPA500.1

EPD100.1

SM10200H

SM2120B

SM2310B

SM2320B

SM2340B

SM2340C

SM3113B

SM6010B

SM9222B

SM9222D

Biochemical Oxygen Demand

Chemical Oxygen Demand

Nitrogen, organic

Depth, secchi disk depth

Chlorophyll Suite

Color

Acidity as CaCO3

Alkalinity, Total

Hardness, Ca, Mg

Harness, Ca, Mg

Metals Prep

Metals Prep Procedure

Total Coliform

Total Fecal Coliform















21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN

21FLORAN


of 91



SM9230C Fecal Strep USEPA, 1999, EPA Methods and Guidance for the Analysis of Water,Version 2.0., USEPA, EPA 821/C-99-008

21FLORAN


of 91

21FLPDEM Pinellas County Dept. of Environmental Management (Florida)


3005A

GEN PREP

LSP 001

Metals

General Preparation

Filtration of water samples, 0.45 micron

Pinellas County Department of Environmental Management, 1998, 1998Comprehensive Quality Assurance Plan, Pinellas County Department ofEnvironmental Management, 1

DEP-QA-001/92, 1992, Florida Department of Environmental ProtectionQA-001/92, DEP, Page 1of 3


21FLPDEM

21FLPDEM

21FLPDEM


of 91

21FLPNS Florida Department of Environmental Protection


351.2

365.4

200.2

3050

351.2

BIO

DIG-TKN-TP

LAB

SOP-HG-020

3050-B

3540-B

3540-C

3550-B



Metals EPA Method 200.1

ICP Mass Spec for Metals in Sediment

351.2 (March 1983) TKN Prep

Methodology for Bacteria and Biological OxygenDemand

Preparation Method for TKN and TP

Methodology for Chemical Analysis

Mercury in Sediment







FDEP, UNK, USEPA - Modified, Central Lab, Unknown, unk

USEPA, 1990, Method 6020 CLP-M: Inductively Coupled Plasma-MassSpectrometry., USEPA, O1A0007861





FDEP, UNK, USEPA - Modified, Central Lab, Unknown, unk





21FLFTM

21FLFTM

21FLPNS

21FLPNS

21FLPNS

21FLPNS

21FLPNS

21FLPNS

21FLPNS

USEPA

USEPA

USEPA

USEPA


of 91

21FLPOLK Polk County Water Resources (Florida)


9230-C-2

LSP-01

3030-B

3030-D

3030-E

4500-NH3-B

9230-C-2

200.2

200.2-M

200.7-T

200.8-T

MT_PREP1

Enterococci (MF)

Nutrients


Preliminary Digestion for Metal Samples


Preliminary Distillation for Ammonia in Water

Fecal Streptococcus and Enterococcus Group,Membrane Filter Sample Preparation





Preparation of Metals Samples in Water

DEP Methods, 1992, DEP Standard Methods, DEP, ALL

DEP Methods, 1992, DEP Standard Methods, DEP, ALL










USEPA, 19--, CLP SOW for Inorganics Analysis-ILM03_0, USEPA,ILM03_0

21FLPOLK

21FLPOLK

APHA

APHA

APHA

APHA

APHA

USEPA

USEPA

USEPA

USEPA

USEPA


of 91

21FLSEM Seminole County (Florida)


GEN PREP Standard Preperation Methods Used by HarborBranch

Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --21FLSEM


of 91

21FLSFWM South Florida Water Management District


AZODIPH

BNA-SF

CARBALK

DIPHENYLHYDRA

ETHYL

GAMMA

GEC

GROSS

HAL1000

HAL1099

LP-1

MALE

METHYL

MFILT

SFWMD: Azobenzene/1-2-Diphenylhydrazine

LAB TEST: W-BNA-SF

SFWMD: Carbonate Alkalinity (CaCO3)

/1,2- Diphenylhydrazine

Ethyl

Gamma Count

Gross Error Count

Gross

SFWMD: Halowax 1000

SFWMD: Halowax 1099

LAB PREPARATION PROCEDURE

Male

Methyl

Membrane Filtrate

SFWMD, 2004, SFWMD SOP's For Water Quality Monitoring, SouthFlorida Water Management District, 1














21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM


of 91

21FLSFWM South Florida Water Management District


NET

NITRODIPHE

ORGCOMP

SOMATIC

T60D

TITRATION

TRIBEN

UNSPECIFIED

VOC-SF

XIL1

XYL2

200.2

MT_PREP1

Net

SFWMD: N-Nitrosodiphenylamine/Diphenylamin

SFWMD: In Organic Compounds

Somatic

SFWMD: Temperature = 60 Deg C

Alkalinity by Titration

SFWMD: Trifluralin/Benfluralin

Unspecified BHC

LAB TEST: W-VOC-SF

SFWMD: Xylene

SFWMD: Xylenes (Total)
















21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

21FLSFWM

USEPA

USEPA


of 91

21FLSJWM St. Johns Water Management District


ACID DIGES

ACID DIGEST

EPA 200.7

EPA 200.8

EPA 315.2

EPA 351.2

EPA 365.2

EPA 365.3

EPA 395.3

EPA 415.1

EPA METAL

EPA METALS

EPA3010

METHOD

NONE

SM 10200H

TP/TKN PRE

TP/TKN PREP

ACID DIGEST

Acid Digest

EPA 200.8

EPA 200.8

EPA 315.2

EPA 351.2

EPA 365.2

EPA 365.3

EPA 395.3

EPA 415.1

EPA METAL

EPA METALS

EPA3010

METHOD

NONE

SM 10200H

TP/TKN PREP

TP/TKN Prep

Unknown, 19--, SJRWMD standard preparation methods, none, Vol--


















21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM

21FLSJWM


of 91

21FLTBW Tampa Bay Water


CHLA Chlorophyll Preparation American Public Health Association, 1998, Standard Methods for theExamination of Water and Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

21FLTBW


of 91

21FLTPA Florida Department of Environmental Protection


SOP-2 Standard Methods Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --21FLTPA


of 91

21FLVEMD Volusa County Environmental Health Lab (Florida)


SOP-2

SOP-3

SOP-4

SOP-5

Determination of Ammonia Nitrogen by Semi-Automated Colorimetry

Determination of Total Kjeldahl Nitrogen by Semi-Automated Colorimetry

Determination of Nitrate-Nitrite Nitrogen byAutomated Colorimetry

Determination of Phosphorus by Semi-AutomatedColorimetry

USEPA, 1993, Methods for the Determination of Inorganic Substancesin Environmental Samples, USEPA, EPA 600/R-93-100




21FLVEMD

21FLVEMD

21FLVEMD

21FLVEMD


of 91

21FLWPB Florida Department of Environmental Protection


351.2

365.4

245.6

3050

351.2 MAR 83

3550B

365.4 (SED)

DEPSED SOP-003

DEPSED SOP-008

DEPSED SOP-012

DEPSED SOP-015

DEPSED SOP-019

DEPSED SOP-021

SOP-GC-002

SOP-HG-020

200.2



Fish Tissue Preparation Central Lab Tallahassee

Metals in Sediments

Preparation for Ammonia and TKN

Sediment

Preparation for Phosphorus, Total as P

Ammonia automated phenate method

chlorophyll determination

nitrate-nitrite determination

Preparation for Reactive Orthophosphate

total kjeldahl nitrogen

total phosphorus

Preparation for pesticides in water

Mercury in Sediments


















21FLFTM

21FLFTM

21FLWPB

21FLWPB

21FLWPB

21FLWPB

21FLWPB

21FLWPB

21FLWPB

21FLWPB

21FLWPB

21FLWPB

21FLWPB

21FLWPB

21FLWPB

USEPA


of 91

21FLWPB Florida Department of Environmental Protection


3510-B Separatory Funnel Extraction, Liquid-Liquid USEPA, 1998, Test Methods for Evaluating Solid Waste,Physical/Chemical Methods, 3rd Edition, Final Update III., USEPA, SW-846_III

USEPA


of 91

21FLWQA Florida Department of Environmental Protection


351.2

365.4

SOP-BB02

DEP-SOP-BB02

DEP-SOP-NU-048




Phytoplankton Sample Filtering for Chlorophyll aAnalysis

Preparation of Waters and Sediments for Nitrogenand Phosphorus Analysis; based on EPA methods351.2 and 365.4




Florida DEP Central Laboratory, 19-, FDEP, Unknown, Unkown

Florida DEP Central Laboratory, 19-, FDEP, Unknown, Unkown

21FLFTM

21FLFTM

21FLFTM

21FLWQA

21FLWQA


of 91

21GUAM Guam Environmental Protection Agency


GUAM-S01 Guam EPA Legacy Sample Preparation Procedures Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol --21GUAM


of 91

21IOWA Iowa Dept. of Natural Resources


3510-B

8150-P


Herbicide Preparation Portion of 8150



USEPA

USEPA


of 91

21NEB001 Nebraska Dept. of Environmental Quality


CHLOROPHYLL A

3030-G

1311

1311-HG

1311-MT

1311-V

200.2

200.2-M

200.7-T

200.8-T

3005-A

Chlorophyll A preparation for analysis. Filtering

Nitric and Sulfuric Acid Digestion

TCLP Preparation for Semivolatiles

TCLP Preparation for Mercury

TCLP Preparation for Metals

TCLP Preparation ZHE

















21NEB001

APHA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA


of 91



3015

3040

3051

3510-B

3510-C

3540-B

3540-C

3550-A

3550-B

3580-A

Microwave Assisted Acid Digestion of AqueousSamples and Extracts

Oily Waste Prep for Soluble Metals by AA and ICP



Separatory Funnel Liquid-Liquid Estraction





Waste Dilution











USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA


of 91



3585

50.6

5030-A

MT_PREP1

MT_PREP2

MT_PREP3

P-010-1

PAH-010

PCB-007

R-003-1

SFSAS_S_PREP

Waste Dilution


Sample Preparation and Extraction for VolatileOrganic Analysis by Purge-and Trap


Preparation of Metals Samples in Soils

Sample Preparation Using Microwave Digestion


Preparation of Samples for PAH Analysis

Preparation of Samples for PCB Analysis

Preparation of Soil for Radiological Analysis

Sediment Preparation Technique












USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA

USEPA


of 91

21NJDEP1 NJ Department of Environmental Protection


350.2

351.3

365.2

4500-N

4500-CN(B)

4500-F-B

200.2-M

Ammonia (as N) Distillation

Kjeldahl Nitrogen (as N) Digestion and Distillation

Phoshporus (as P) Persulrate Digestion

Persulfate Method (proposed)

Preliminary Treatment of Cyanide Samples

Preliminary Distillation for Water Samples ContainingFluoride





American Public Health Association, 199X, Stardard Methods for theExamination of Water and Wastewater, American Public HealthAssociation, 19th Edition




21NJDEP1

21NJDEP1

21NJDEP1

21NJDEP1

APHA

APHA

USEPA


of 91

21NYDECA NYS Dept. of EnCon, Division of Water


RIBS-BSED

RIBS-WCOL

RIBS-WCOL-FLT

RIBS Bottom Sediment Sample Collection

RIBS Water Column Sample Collection

RIBS Filtered Water Column Sample Collection

J.A.Myers, etal., 2000, Program Plan for Statewide Waters MonitoringProgram, NYSDEC, 47 pgs (plus append)



21NYDECA

21NYDECA

21NYDECA


of 91

21SC60WQ SC Dept. of Health & Environmental Control


D3976 Std. Practice for Prep. of Sediment Samples forChemical Analysis

American Society for Testing of Materials, 1994, ASTM Standards.Water and Environmental Technology (II), American Society for Testingand Materials, Vol 11.02

ASTM


of 91

21SCSANT Santee Cooper - South Carolina Public Service Authority


BACTERIA

CHPYL A

METAL

NUTRIENTS

SOLIDS

Bacteria Analysis Procedure

Chlorophyll a analysis

Metals Analysis Procedures

Nutrients Analysis Procedures

Total Dissolved Solids / Total Dissolved Solids






21SCSANT

21SCSANT

21SCSANT

21SCSANT

21SCSANT


of 91

21SDAK01 SD Dept of Environmental & Natural Resources


515TDS

CATION-ANION %

SAR

TDS

VISUAL

WRAP

Total Dissolved Solids

Cation-Anion Balance

SAR

TDS

VISUAL

Water Resources Assistance Program Procedure

USEPA, 1979, Methods for Analysis of Water., USEPA, EPA 600/4-79-020






21SDAK01

21SDAK01

21SDAK01

21SDAK01

21SDAK01

21SDAK01


of 91

21VASWCB Virginia Department of Environmental Quality (VADEQ)


D3987

3020-A

Shake Extraction of Solid Waste and Water




ASTM

USEPA


of 91

21WIS Wisconsin Dept. of Natural Resources


99436 PCB Congerners in surface water American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

21WIS


of 91

22LAGWTR Louisiana Dept of Environmental Quality


BMP-FLD

HG-106

METAL-1

METAL-2

NUTRNT-1

PEST/PCB

PEST/PCB-2

SVOC-1

SVOC-2

VOC-1

VOC-2

WQ-1

Field Measurements

Merecury in Water (106)

Total Metals in Water

Total Metals in Water (106)

Nutrients in Water

Pesticides/PCB's in Water (8270C)

Pesticides/PCB's in Water (106)

SVOC's in Water (8270C)

SVOC's in Water (106)

VOC's in Water (8260B)

VOC's in Water (106)

Water Quality Parameters Prep

Baseline Monitoring Project, 1999, Baseline Monitoring Project, QualityAssurance Project Plan, LDEQ, 198pp






USEPA, 1984, Guidelines Establishing Test Procedures for the Analysisof Pollutants Under the Clean Water Act, USEPA, 40CFR136






22LAGWTR

22LAGWTR

22LAGWTR

22LAGWTR

22LAGWTR

22LAGWTR

22LAGWTR

22LAGWTR

22LAGWTR

22LAGWTR

22LAGWTR

22LAGWTR


of 91

31DELRBC Delaware River Basin Commission


MT_PREP1

P-010-1

PAH-010

PCB-007









USEPA

USEPA

USEPA

USEPA


of 91

31ORWUNT Ohio River Sanitation Commission


200.2

245.1

3500CR D

9213D

9222D

Digestion, ICP, ICPMS

Mercury Digestion

Chromium Hexavalent

E. Coli

Fecal Coliform






31ORWUNT

31ORWUNT

31ORWUNT

31ORWUNT

31ORWUNT


of 91

COE/ISU Des Moines River - Corp of Engineers (IOWA)


3030-E Nitric Acid Digestion of Metals American Public Health Association, 1992, Standard Methods for theExamination of Water and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

APHA


of 91

DANTEST Dan's DUMMY test organizarion


9215-D-3

3050-A

3050-B

3051

Heterotrophic Plate Count, Membrane Filter MethodSample Preparation








APHA

USEPA

USEPA

USEPA


of 91

DEMOTEST The Commission for a Good Clean Chesapeake Bay


3030-C

4500-S2(B)

D3326-A

D3326-B

D3326-D

D3326-G

D4638

LSP-001

LSP-002

OC010R

3020-A

Treatment for Acid-Extractable Metals

Separation of Soluble and Insoluble Sulfides

Std. Practice for Prep. of Samples for Id. ofWaterborne Oils of Large Samples

Std. Practice for Prep. of Samples for Id. ofWaterborne Oils in Limited Sample Volumes ofHeavy Oils

Std. Practice for Prep. of Samples for Id. ofWaterborne Oils Composed of Mixed Petroleum-based & Animal/Vegetable Oils

Std. Practice for Prep. of Samples for Identification ofWaterborne Oils in Oil-Soaked Samples

Preparation of Biological Samples for InorganicChemical Analysis

Acid Digestion of Sediments for Organics Analysis

Filtration of Water Samples, 0.45 micron

Preparation of VOC Samples ContainingHydrocarbons








American Society for Testing of Materials, 1994, ASTM Standards.Water and Environmental Technology (I), American Society for Testingand Materials, Vol 11.01

CGCCB_SOPS - Commission for a Good Clean Chesapeake Bay,1991, Standard Procedures for Sampling the Chesapeake Bay, VirginiaBeach Press, 290 pp

SAMPLE_CB - Dr. Lee Manning, 1987, Sampling the Chesapeake Bayfor Fun and Profit, University of Virginia Press, 589 pp

USDOE, 1995, Methods for Evaluating Environmental and WasteManagement Samples, April 1995, USDOE, DOE


APHA

APHA

ASTM

ASTM

ASTM

ASTM

ASTM

DEMOTEST

DEMOTEST

USDOE/ASD

USEPA


of 91

DEMOTEST The Commission for a Good Clean Chesapeake Bay


3050-B

3510-B

50.6

MT_PREP3

P-010-1

SFSAS_FT_PREP




Sample Preparation Using Microwave Digestion









USEPA

USEPA

USEPA

USEPA

USEPA

USEPA


of 91

EMAP-CS Environmental Monitoring and Assessment Program


90%ACEX

ASE

ASTM1993

CHLA-NCA

EMAP-E

EPA 160.2

EPA245.5

EPA3051

EPA3052

EPA3052/3050B

Chlorophyll a filter suspended in 10ml of 90 %acetone until frozen

Accelerated Solvent Extraction

Standard guide for conducting 10-day static sedimenttoxicity tests w/marine organisms

Pigment extraction from filter with 90% acetone

Methods in EMAP 1995 Laboratory Methods Manual

Water sample filtered for TSS

Mercury in sediment (cold vapor with permanganatedigestion)

Strong acid microwave method

Microwave assisted acid digestion of siliceous andorganically based matrices

Microwave/hot plate assisted acid digestion ofsiliceous and organically based matrices

Tom Heitmuller, USGS, 2001, Quality Assurance Project Plan; EMAP-West-Coastal Monitoring, USEPA: EMAP, Gulf Breeze Laboratory, 152p

U.S. Environmental Protection Agency, 2001, EMAP-National CoastalAssessment Quality Assurance Project Plan 2001-2004, USEPA,NHEERL Gulf Ecology Division, Gulf Breeze, FL, 202 p

ASTM, 1993, Standard guide for conducting 10-day static sedimenttoxicity tests with marine and estuarine amphipods. E1367-92. In:Annual Book of ASTM Standards. Vol. 11.04. Philadelphia, PA, ASTM,pp. 1138-1163

J. Kiddon, H. Buffum, 2002, EMAP-NCA Northeast 2000 NutrientCollections/Chemistry Metadata, U.S. Environmental Protection Agency,10 p

U.S. EPA, 1995, EMAP: Laboratory Methods Manual-Estuaries, Volume1: Biological and Physical Analyses, Environmental Protection Agency,Office of Research and Development, Narragansett, RI, 128 p






EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS


of 91



HF/HNO3

HG-NCA

HNO3/HCL

HSGAS

MASE

MET-NCA

MGNO3

NA

NOTREC

NR

NUT-NCA

Total digestion using HF/HNO3 in an open beaker ona hot plate

Cold vapor AA for Hg (persulfate acid digestion)

Microwave digestion using HNO3/HCl in a closedteflon-lined pressure vessel

React sediment w/ hydrochloric acid; trap theevolved hydrogen sulfide gas

Microwave assisted solvent extraction

Sediment dried and completely digested innitric/hydrofluoric acids

Magnesium Nitrate addition w/ hydrochloric aciddigestion

Not analyzed

Procedure not recorded

Not relevant

Filtration operation using a 0.7 micron glass-fiberfilter

C. Strobel, 1996, EMAP-Estuaries 1993 Virginian Province SedimentChemistry Metadata, U.S. Environmental Protection Agency, 15 p

J. Kiddon, H. Buffum, 2002, EMAP-NCA Northeast 2000 SedimentChemistry Metadata, U.S. Environmental Protection Agency, 16 p




J. Kiddon, H. Buffum, 2002, EMAP-NCA Northeast 2000 SedimentChemistry Metadata, U.S. Environmental Protection Agency, 16 p

State of California, 1986, Procedures for analysis of selenium andarsenic in fish and wildlife tissues with emphasis on quality control, Stateof California, Department of Fish and Game, Lab. Rpt 86-3





EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS


of 91



ORG-NCA

PSEP86

SE

SE(VP)

SM2540D

SM4500NH3

SM4500NO3

SM4500P

SOXHLET

TAAII

National Status and Trends Organic Methods

PSEP86: Sediment grain size

Solvent extraction

Soxhlet extraction and extract drying, concentrationand clean-up

SM2540D: EMAP-West CA 1999-2000 for TSS

SM4500NH3: EMAP-West CA 1999-2000 for NH4-Nand NO3-N

SM4500NO3: EMAP-West CA 1999-2000 for NO2

SM4500P: EMAP-West CA 1999-2000 for PO4

Soxhlet solvent extraction

Lab sample prep procedures for using a TechniconAutoAnalyzer II

Lauenstein, G. G. and A. Y. Cantillo (eds.), 1993, Sampling andanalytical methods of the National Status and Trends Program NationalBenthic Surveillance and Mussel Watch Projects 1984-1992:Comprehensive descriptions of trace organic analytical methods,Volume IV NOAA Technical Memorandum NOS ORCA 71, SilverSpring, MD., NOAA, Silver Spring, MD, 182 p










EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS

EMAP-CS


of 91



TOX-NCA

TSS-NCA

V-EPA245.5

3010-A

3020-A

Sediment toxicity test laboratory set-up

Water sample filtered

Method variation of EPA245.5 developed by VarianAnalytical Instruments



U.S. EPA, 1995, EMAP: Laboratory Methods Manual-Estuaries, Volume1: Biological and Physical Analyses, Environmental Protection Agency,Office of Research and Development, Narragansett, RI, 128 p





EMAP-CS

EMAP-CS

EMAP-CS

USEPA

USEPA


of 91

HI301H City and county of Honolulu


3030-B

3030-E

NITRIC-PEROXIDE

PERSULF DIG

SPE

SPE-SGT

200.2-M



nitric acid and peroxide digestion for As and Se

Persulfate Digestion for Total Nitrogen

Solid Phase Extraction

solid phase extraction followed by fog removal by sgtcolumn









APHA

APHA

HI301H

HI301H

HI301H

HI301H

USEPA


of 91

IL_EPA Illinois EPA


FIELD

LAB

ANALYZED IN FIELD

ANALYZED IN LAB

IEPA FIELD - Illinois EPA, 1994, Illinois EPA field methods manual,Illinois EPA, Sections B and H

IEPA LAB - Illinois EPA, 1993, IEPA Lab Methods Manual, Illinois EPA, Volumes 1 and 2

IL_EPA

IL_EPA


of 91

LAKELAND City of Lakeland (Florida)


2120 C

2540 C

2540 D

3111 B

3111 D

3113 B

4500-NH3-G

9222-B

9222-D

CHLA 4.3.1

EPA 310.1

Color in Water by Specrophotometry

FilterableTDS residues

Nonfilterable TSS Residues

CA/MG/FE/CD/ZN

ALUMINUM

Cr/aS/Pb/Se/Ag/Cu

AMMONIA IN WATER USING AUTOMATEDPHENOTE METHOD

Total Coliform analysis

Fecal Coliform Analysis

CHLOROPHYL A ANALYSIS

Alkalinity by Titration












LAKELAND

LAKELAND

LAKELAND

LAKELAND

LAKELAND

LAKELAND

LAKELAND

LAKELAND

LAKELAND

LAKELAND

LAKELAND


of 91

LAKELAND City of Lakeland (Florida)


EPA 350.1

EPA 353.2

EPA 365.1

EPA 365.4

EPA6.4

NITROGEN

AMMONIA NITROGEN BY COLORIMETRY

NITRATE NITRITE NITROGEN BY COLORIMETRY

PHOSPHORUS BY COLORIMETRY

TOTAL PHOSPHORUS AFTER DIGESTION BLOCK

EPA Macroinvert Field & Lab methods for evaluatingBiological integrity of Surface Waters

TOTAL NITROGEN



USEPA, 2000, Methods for the Determination of Organic and InorganicCompounds in Drinking Water, vol 1., USEPA, 815/R-00-014


USEPA, Donald J. Klemm, Philip A. Lewis, Florence Fulk, and James M.Lazorchak, 1990, Macroinvertebrate Field and Laboratory Methods forEvaluating the Biological Integrity of Surface Waters, USEPA,Environmental Monitoring Systems Laboratory- Cincinnati, Office ofResearch and Development, 600/4-90/030

City of Lakeland, 1999, Total Nitrogen, City of Lakeland, 1

LAKELAND

LAKELAND

LAKELAND

LAKELAND

LAKELAND

LAKELAND


of 91

MDEDAT01 Maryland Dept. of the Environment Dredging Ambient Data


CBL001 Sample preparation of biotic tissue used byChesapeake Biological Laboratory - yr01

Jay C. Means, October 1982, "Data on Trace Organic Contaminants inWater, Sediments and the Biota". Assessment of the EnvironmentalImpacts of Construction and Operation of the Hart and Miller IslandsContainment Facility, 1981 - 1982, Chesapeake Research Consortium,VII, pp. 210-272

MDEDAT01


of 91

MDEDAT09 Maryland Dept. of the Environment Risk Assessment Data


200.7-T

P-010-1

PAH-010

PCB-007

SFSAS_FT_PREP











USEPA

USEPA

USEPA

USEPA

USEPA


of 91

MNPCA1 Minnesota Pollution Control Agency


FLT CHL A Filtration of sample prior to lab delivery forchlorophyll analysis

Minnesota Pollution Control Agency Quality Assurance Program, 2000,www.pca.state.mn.us/programs/qa_p.html, Minnesota Pollution ControlAgency, all pages

MNPCA1


of 91

MONT-DEQ Montana Department of Environmental Quality


TPN-4500-N-C

3050-A

Persulfate Nitrogen Method




MONT-DEQ

USEPA


of 91

MT-DEQ Montana DEQ


4500-N-C

4500-P-B

TPN-4500-N-C

200.2

200.2-M

3051

3550-A

Persulfate Digestion

Sulfuric Acid and Persulfate Digestion SamplePreparation

Persulfate Nitrogen Method












MT-DEQ

MT-DEQ

MT-DEQ

USEPA

USEPA

USEPA

USEPA


of 91

MTWTRSHD Montana Watershed Data



USEPA


of 91

MWRDSTOR Metropolitan Water Reclamation District of Greater Chicago



USEPA


of 91

R2-LAB New York


D4638 Preparation of Biological Samples for InorganicChemical Analysis

American Society for Testing of Materials, 1994, ASTM Standards.Water and Environmental Technology (I), American Society for Testingand Materials, Vol 11.01

ASTM


of 91

SDWRAP SD Dept of Environmental & Natural Resources


SECCHI DISK SECCHI DISK TRANSPARENCY SDWRAP SOP - Watershed Assessment Team, June 2003, StandardOperating Procedure for Field Samplers Volume 1, State of SouthDakota, Voume 1

SDWRAP


of 91

SRMTAKNY St. Regis Mohawk Tribe (New York)


PCB-007

SFSAS_FT_PREP

SFSAS_S_PREP



Sediment Preparation Technique




USEPA

USEPA

USEPA


of 91

TDECDOE Tennessee Department of Environment and Conservation


3030-C

3030-D

% SOLIDS

A.12

A.18.1

A.18.2

A.18.4

A.18.8

A.18.8.1

A.18.9.1

A.19.1



Percent Solids

Total Hardness - State of Tennessee EnvironmentalLaboratories

Ammonia - State of Tennessee EnvironmentalLaboratories

Ammonia, sediment

NO3 & NO2 - State of Tennessee EnvironmentalLaboratories

Total Kjeldahl Nitrogen - State of TennesseeEnvironmental Laboratories

Total Kjeldahl Nitrogen, sediment

Total Phosphate - State of Tennessee EnvironmentalLaboratories

Oil and grease, sediment



Tennessee Department of Health Laboratory Services, 1999, StandardOperating Procedures, Tennessee Department of Health LaboratoryServices, Vol. __









APHA

APHA

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE


of 91



A.19.2

A.2

A.23.1

A.24.2

A.24.3

A.3

A.6

A.9

EPA 200.7

EPA 200.9

EPA 202.1

TPH Total Petroleum Hydrocarbons - sediment

BOD, 5-day - State of Tennessee EnvironmentalLaboratories

Total Phenols, sediment

Suspended Residue - State of TennesseeEnvironmental Laboratories

Dissolved Residue - State of TennesseeEnvironmental Laboratories

Boron, sediment

Low COD - State of Tennessee EnvironmentalLaboratories

Cyanide - State of Tennessee EnvironmentalLaboratories

Lithium

Metals - EPA

Aluminum by FLAA












TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE


of 91



EPA 206.2

EPA 208.1

EPA 213.1

EPA 215.1

EPA 218.1

EPA 219.1

EPA 220.1

EPA 236.1

EPA 236.2

EPA 239.1

EPA 242.1

Arsenic sediment

Barium, sediment

Cadmium, sediment

Calcium, sediment

Chromium, sediment

Cobalt, sediment

Copper, sediment

Iron

Iron sediment

Lead, sediment

Magnesium, sediment


USEPA, 1991, Methods for the Determination of Metals inEnvironmental Samples, USEPA, EPA 600/4-91-010










TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE


of 91



EPA 243.1

EPA 243.2

EPA 245.1

EPA 245.5

EPA 249.1

EPA 249.2

EPA 258.1

EPA 270.3

EPA 272.1

EPA 273.1

EPA 289.1

Manganese

Manganese sediment

Mercury - EPA

Mercury, sediment

Nickel, sediment

Nickel by GFAA

Potassium

Selenium

Silver

Sodium, sediment

Zinc












TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE


of 91



EPA 289.2

EPA 375.4

MS

MS+ECD

PARTSIZE

R.1.3

R.6

SM 9000

SM 9222-D

SM 9230-B

Zinc sediment

Sulfate by Turbidimetric Determination

Mass spec for extractable organics

Mass spec & electron capture for extractableorganics

Particle Size Distribution of Sediment

Gross Alpha & Beta, State of TennesseeEnvironmental Laboratory Services

Gamma Radionuclides, State of TennesseeEnvironmental Laboratories

E. Coli, Enterococcus - Standard Methods 9000

Fecal Coliform - Membrane filter procedure

Fecal Strep











TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE

TDECDOE


of 91



TOC

200.2

200.2-M

200.7-T

200.8-T

EPA 9060 Total Organic Carbon (TOC)










TDECDOE

USEPA

USEPA

USEPA

USEPA


of 91

TDECWPC Tennessee Department of Environment and Conservation


3030-C

3030-D

4500-NH3-B

200.2

200.2-M

200.7-T



Preliminary Distillation for Ammonia in Water










APHA

APHA

APHA

USEPA

USEPA

USEPA


of 91

USVIST Government US Virgin Islands


9230-C-2 Fecal Streptococcus and Enterococcus Group,Membrane Filter Sample Preparation


APHA

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