JACOBSVILLE NEIGHBORHOOD SOIL ... - … (FSP) dated "November 2004" and the Quality Assurance...

EPA Region 5 Records Ctr.

253851

JACOBSVILLE NEIGHBORHOODSOIL CONTAMINATION SITE

EVANSVILLE, INDIANA

TECHNICAL MEMORANDUM #6PRELIMINARY SITE CHARACTERIZATION SUMMARY FOR

SAMPLING EVENTDATES: OCTOBER 17-27, 2005

January 23, 2006Revision: 0

Prepared by:

Jena Sleboda BraunU.S. Environmental Protection Agency

Region 577 West Jackson Boulevard

Chicago, Illinois 60604

Jacobsville Neighborhood Soil ContaminationTechnical Memorandum #6Revision: 0Date: January 23, 2006Page: i

TAB:LE OF CONTENTS

Section Title Page

1.0 INTRODUCTION 1

2.0 SITE DESCRIPTION 1

3.0 SITE CHARACTERIZATION 23.1 Investigation Activities 23.2 Results 2

4.0 CONCLUSIONS 3

5.0 REFERENCES 4

Jacobsvillc Neighborhood Soil ContaminationTechnical Memorandum #6Revision: 0Dale: January 23, 2006Page: i i

FIGURES

Figure Title

1 Unadjusted Soil Concentrations for Sampling Event #3

2 Adjusted Soil Concentrations for Sampling Event #3

3 Adjusted Soil Concentrations for Sampling Events #1, #2, and #3

Jacobsville Neighborhood Soil ContaminationTechnical Memorandum #6Revision: 0Date: January 23, 2006Page: i i i

APPENDICES

Appendix Title

A Statistical Cs Iculations and Laboratory-XRF Value Correlation

B Laboratory Results for Sampling Event #3

C XRF Results (Undadjusted) for Sampling Event #3

D Tables of Adjusted Lead Concentration Values (Using Correlation) forSampling Event #3

in

Jacobsvillc Neighborhood Soil ContaminationTechnical Memorandum #6Revision: 0

Date: January 23, 2006Page: 1 of4

1.0 INTRODUCTION

This report presents the results of soil contamination sampling for the Jacobsville Neighborhood

Soil Contamination Site (Site) in Evansville, Indiana. The sampling took place October 17-27,

2005 and was conducted by the U.S. Environmental Protection Agency (U.S. EPA) Region 5.

The sampling was conducted in accordance with the procedures outlined in the Field Sampling

Plan (FSP) dated "November 2004" and the Quality Assurance Project Plan Addendum B dated

"September 20, 2005." The objective of this investigation was to evaluate soils in and around

previous sampling event sample locations that had adjusted lead concentrations of greater than

400 ppm, so as to locate hotspots within the delineated contamination plume.

The investigation included taking surficial soil samples from residential and public properties

within the Jacobsville Neighborhood Soil Contamination contaminant plume, which was

delineated from prior sampling events, so as to better describe the contamination within the

previously delineated boundaries. Information regarding the sampling event can be found in the

Technical Memorandum #5: Field Summary Report dated December 28, 2005.

2.0 SITE DESCRIPTION

The Site is described by the Indiana Department of Environmental Management's (IDEM)

Integrated Assessment Report as follows:

The site is located Evansville [sic], Vanderburgh County, Indiana. The site can befound on the U.S.G.S. Evansville South Quadrangle Topographic Maps. The sitelies in the southeast corner of 19 and southwest corner of section 20 Township 6South, Range 10 West. The site is bounded to the west by Edgar St., to the southby Lloyd Expressway, to the east by Heidelbach, and to the north by Iowa Street.

The site as described by IDEM is commonly known as the "Jacobsville Neighborhood" in

Evansville, Indiana. Although IDEM's site boundaries were cited in the National Priorities List

(NPL) package, samples were taken well outside IDEM's site boundaries to ensure the areal

extent of contamination was captured. The Jacobsville Neighborhood is an urban residential area

and the city of Evansville is a long established city on the Ohio River with many industrial areas.

The suspected sources of lead contamination are four now-defunct factories in the Jacobsville

Neighborhood that operated before and at the beginning of the 20th century. Additional

Jacobsville Neighborhood Soil ContaminationTechnical Memorandum #6Revision: 0


information on the Site background can be found in IDEM's Integrated Assessment Report and

the Jacobsville Neighborhood Soil Contamination Site Quality Assurance Project Plan (QAPP)

dated December 7, 2004.

3.0 SITE CHARACTERIZATION

3.1 Investigation Activities

182 locations were sampled consistent with the procedures described in the QAPP, QAPP

Addendum B, and FSP. The fivs-point composite samples were analyzed with a field

portable X-Ray Fluorescence (XRF) unit at the sampling location, and twenty percent of

the samples were also sent to U.S. EPA's Central Regional Laboratory (CRL) for ICP

metals analysis. The XRF concentrations had a low bias when compared to the

laboratory concentrations, but there was a very strong correlation (R2 = 0.958) between

the XRF values and the laboratory values. The statistical calculations and conclusions for

the data correlation can be found in Appendix A.

3.2 Results

This sampling verified that previous samples that had high lead concentrations were

unquestionably in areas with high lead contamination. Samples were also taken along the

boundaries delineated in Sampling Event #2, and lead concentrations greater than 400

ppm were not found outside of the boundaries. All samples that had adjusted

concentrations of greater than 400 ppm were within the Evansville city limits.

The soil screening value being used in the initial investigative sampling is 400 ppm, a

generic screening value often used by the U.S. EPA. In January and February 2006 , risk

sampling will be done to determine a site specific clean up goal (CUG) that is based on

exposure and risk specific to the; environment in Evansville.

A visual representation of the raw field (XRF) concentrations is presented as Figure 1. A

visual representation of the concentrations after adjusting for the low bias of the XRF

concentrations is presented as Figure 2. A visual representation of the combined

adjusted XRF values from U.S. EPA Sampling Events 1,2, and 3 is presented as Figure 3.



The laboratory results for Sampling Event #3 can be found in Appendix B. The original

XRF data tables for Sampling Event #3 can be found in Appendix C. Tabular data that

represents the adjusted XRF concentrations for Sampling Event #3 can be found in

Appendix D. The data indicates that there are concentrations of concern (greater than

400 parts per million (ppm) outside of the Jacobsville Neighborhood.

4.0 CONCLUSIONS

From this sampling event, it can be seen that there are several pockets within the contamination

boundaries that have very high lead concentrations. Some of these areas are outside the

Jacobsville Neighborhood. It appears that all adjusted lead concentrations greater than 400 ppm

are within a two mile radius of the Jacobsville Neighborhood. Enough surficial soil data has

been gathered to determine the boundaries of the lead contamination that is greater than 400

ppm. After the January-February Risk Assessment Sampling Event, there the site-specific clean

CUG will be determine and the boundaries of the area that needs to be remediated will be

adjusted as necessary if the CUG is a value different than 400 ppm.

It was also noted from the sampling results that many areas of Evansville have been re-graded or

filled with new soils since the contamination occurred. These residences have been found

directly adjacent to properties that had lead soil concentrations of greater than 400 ppm.

Therefore, it is expected that many residences within the final delineated contamination plume

will not have lead concentrations greater than the site CUG and will not need remedial action.



5.0 REFERENCES

NITON Corporation. 1998. 300 series and 700 series User's Guide Version 5.2.

U.S. EPA. 1992. Specification and Guidance for Obtaining Contaminant-Free SampleContainers. EPA 540/R-93/051. 1992.

U.S. EPA, Region I. 1996. Standard Operating Procedure for Elemental Analysis Usingthe X-Met 920 Field X-Ray Fluorescence Analyzer.

U.S. EPA. 1998a. Environmental Technology Verification Report: Field Portable X-rayFluorescence Analyzer - Niton XL Spectrum Analyzer. EPA/600/R-97/150. March 1998.

U.S. EPA. 1998b. Test Methods for Evaluating Solid Waste, Physical/Chemical Methods(SW-846), Draft Update IVA. Method 6200 (pp. 6200-1 - 6200-31).

U.S. EPA. 2000. Short Sheet: TRW Recommendations for Sampling and Analysis of Soilat Lead (Pb) Sites. OSWER 928.7-38. April 2000.

U.S. EPA. 2003. Superfund Lead-Contaminated Residential Sites Handbook. OSWER9285.7-50, August2003.

U.S. EPA, 2004. Jacobsville Neighborhood Soil Contamination Site, Evansville, Indiana,

Field Sampling Plan. November 2004.

Figures

Figure 1. UnadjustedXRF Concentrationsfor the JacobsvilleNeighborhood SoilContamination SiteSampling Event #3

Legend

O Sampling Event #1 Locations


Unadjusted Values (ppm)

RESULTS

O 0-100

@ 101-200

• 201-1250

0.5

I Miles

Prepared by:Jena Sleboda Braun

Figure 2. AdjustedXRF Concentrationsfor the JacobsvilleNeighborhood SoilContamination SiteSampling Event #3

Legend



Lab Results (ppm)Results

© 74 - 300

© 301 - 400

• 401 - 2500

Adjusted Values (ppm)Results

O 0-300

O 301 - 400

• 401 - 2500

0.53 Miles


Figure 3. AdjustedXRF Concentrationsfor the JacobsvilleNeighborhood SoilContamination SiteSampling Events#1, #2, and #3

N

Legend

Sampling #1 Results

Adjusted Values (ppm)

D 0-300

D 301 - 400

• 401 - 2500

Sampling #2 Results

Adjusted Values (ppm)A 0-300

A 301 - 400

A 401 - 2500

Sampling #3 Results

Adjusted Values (ppm)O 0-300

O 301 - 400

• 401 - 2500


Appendix A:

Statistical Calculations andLaboratory-XRF Value Correlation

(Analysis by: L. Walston)

JACOBSVILLE NEIGHBORHOOD ANALYSES

EVANSVILLE, IN

DATA COLLECTED OCTOBER 2005(ANALYZED 18 JANUARY 2006)

1. RELATIONSHIP BETWEEN XRF SOIL SAMPLES AND LABORATORYRESULTS FOR LEAD (Pb) CONCENTRATIONS

2. TEST OF PARALELLISM BETWEEN TWO XRF DEVICES

3. TEST OF PARALLELISM BETWEEN ENVIRONMENTAL CONDITIONS

DESCRIPTIVE STATISTICS - TOTAL XRF SAMPLES

Osing £

I3uaiBiiiSaxAvg

3tdStdaVaeVatsSJ»H

Kurt

eld : RESULTS

*7T718.35.0293.356,587*14966

16. ZBSStSB'lZ16. B'JSOSQES675 ,7396545tQ? .027939S,OZ 1Q26I671.3fi4334€94S4

MEAN PB CONCENTRATION (XRF):256.59 PPM

PBJ*DDUP_OCT_05

XRF_PPM

• <200• 200-400« 400-300• >800

LABORATORY ANALYTIC SAMPLES

f *e ^ *6 u*ra py s»x TBJP ^̂ ggr

.

*u^j

3-..• v

*r»if» "OflM «

CTH-7MK1

Of the 147 XRF samples collected, 28 were preserved for laboratory analysis.Each XRF sample was collected using one of two XRF devices (XL-700 or XLP-712).

Environmental information was also recorded for each sampling day (i.e., temperature, weather).

Spatial distribution of XRF samples preserved for laboratory analytics is shown on the next slide.

LEAD (Pb) SOIL CONTAMINATIONF'VANSVILIE IN OCTOBER M05 SAMPLING

- . . . . - -*uw* ̂ -.TMrru^-T^uat*?**;:*fc*»lf* UulLltt M SOOMft *c*

LEAD CONCENTRATION OCT 2009xOF ; .*B RATIO

• jRF • L*6 -o

« KSF > LAB /^

Relationship between XRF and Laboratory values of Pb Concentration

To determine the validity of XRF lead values, correlation/regression analyses were performed between XRF andLaboratory values of Pb concentration.

A) Pearson / Spearman correlationsB) Simple linear regression

I. Data Posting - Scatter PlotXRFvs Laboratory Lead Concentrations

TIM

MM

MM

'

£Ml

1*0*

0

ft

II IHtO !ON XW

Relationship between XRF and

II. Descriptive Statistics For Both Varia

XRF Pb Concentration

.

Lab Pb Concentration

Laboratory values of Pb Concentration

blCS I n = 28 for both variables)

Onlng field : XRF_PB

Selection exists, using layer; LEAP CCWCENTRATICN - OCT 2QO3

N -28Sum - 9702.6Kin - 49.5tiax - 3000.0

Sectian- 211.353td - 549.1<26S^75IStda - 559.525042869V«r - 301887. 263B27Vacs - J13068. 2735963fc«* - 4-^1030777276Kurt • 17.26817336

Using Held : LAB PB

Selection exists, uaiaa layer: LEAK CCHCEMTRATION - CXTT 2005

« - 28Sum - 16987.0din - 39.0Rax - 6300.0Avg - 506. 678571429Hedi«n- 295.03cd - 11S1.2B9678S13cds - U82. 59952376Vac - 1348593.71811Vmftt " 1)99541.6336Skew - 1.39593674992


III. Are the variables correlated? (Pearson & Spearman Correlations)

LABJ'BXRF_PB

N Mean

28 606.67857

The CORR Procedure

2 Uariables: I AS _PB XRf PB

Simple Statistics

Std De«.- Median flinimi

1183 295.00000 39.00000000

(lax inun Label

6300 Laboratory ppm3000 XRF ppm

LftB_PHLaboratory ppm

LAB_PB

I.00000

XHF_PB

0.98985

Spearman Correlation Coefficients. NProb > !r! under HO: Rho=0

LAB_PHLaboratory |

XRF_PHXRF ppm

LAB.PB

I.00000

0.35071<.0001

.XHF PB

0.95071


IV. THE REGRESSION MODEL (Proc Reg) Assumptions (5):1. Linear relationship2. Equality of Error Variances3 Normal distribution of residuals4 Independence of residuals5. Homoscedasticity

model lab pb = xr£ pb /id xrf pb;

u95=up 195=down;

p r elm :.nf luence dw; utpui table 'oclober_out'

p = Predicted values for the dependent variable. These may also be created in a new output table ("october_out")r= residuals -amount of error of the observed values from the predicted values (This option uses 'studentizedresiduals' -

residuals that are divided by their standard errors; student residuals also follow the (-distribution).dm = Calculates 95 % confidence limits around the predicted values. In the new output table, these values may be further

described as " u95' and "I95" as the upper 95% limit and lower 95% limit, respectively. Thisoption will also ca culate the standard error around the predicted values.

influence = Calculates influence statistics, which are often used to detect outliers. This option measures the impact of eachobservation on the model prediction (i.e., how much of an /nfluenceeach observation has).Specific metrics irclude studentized residuals, Hat Diagonals (H), Covariance Ratio, Dffits, andDfbetas - all metrics may be viewed in the output table. Additionally, fie output table may bespecified to produce the CooKs D (coofcd)statistic (another diagnostic statistic).


IV. THE REGRESSION MODEL (cont'd)

Overall model is significant:F, „ = 1260.73; P< 0.0001

Intercept is significant:t=-3.09;/> = 0.005

XRF is significant predictor of Lab Value:1=35.5;/><O.OOOI

4«u n * *••!

1/1 wit i* ttijia • • *m«N Oft? Mi ft-Q« • kit*


EV. REGRESSION DIAGNOSTICS| a. View The Output Table ('october_out'|

•b. Create a plot of Predicted vs. Observed Values With 95 % CLMc. Outlier Detection / Residual Observations

d. Influence Statistics

Table 1. Output table with diagnostic variables

318.? 8M4B9 -39. 38832264 6? f . 50581 24 1 101 .MlfSSI239,6 680571 -113.3121008 598. £65/1221 30.32319428

tOt . 38801 79 -2S8 . 1 6351 77 460 . 9395535 38 SI t 982 1 0

1 .8033S3fSM -358.2K30S79 361 .86976541 108 136646?

IB? 05934689 -197. 2234376 S21 .34218636 2/.9406f.310

B 4? . aOBB03G93 -3 1 7 . 0345038 402 652 1 1 1 1 8 57 .1911 9630

0.602537932 0.0071616211 0. 180G001 IS 0.000668098

0.23035B06E3 0.001181014

0.530307368S 0 00680344S

0 . 64650B06I 5 0 . 0099B5873

0 . 1 665577539 0 . OOOS9388 1

0 , 34 1 5037208 0 . 002 70348 7

0.0379549110.033354737

0.042615229

O.M44S8222

0 046tSI2t

0 045603407

0 .04IOS7500

-0. 114433208-0 . 1 56430596

0. 1181836810.0358666872

O.M770562M3

,0460511785

.052372^228

. 1 1500701GB

.1 39704531 1-0. I52B72S48

0.0338127093

0 .0443080567 0.0722664S33


IV. REGRESSION DIAGNOSTICSa. View The Output Table 'october_out'

|b. Plot o f Predicted vs. Observed Vdues With 95 % CLM

c. Outlier Detection / Residual Observationsd. Influence Statistics

•fXW

•_ 'QUO

z

-KHK>

ACTUAtLABOOTiCC

XXKI


IV. REGRESSION DIAGNOSTICSa. View The Output Table roctober_out'tb. Plot of Predicted vs. Observed Values With 95 % CLM

e. Outlier Detection / Residual Observations

d. Influence Statistics

Studentized residuals follow the t-distribution; values from thisdistribution greater than 2.5 are rare.Therefore, Studentized residuals i. 2.5are useful n identifying large residuals

potential outliers. Studentizedresiduals may be viewed in the outputtable ( 'october_out'(, and theirmagnitude may be better viewed byplotting them against predictedlaboratory Pb values.

From this data. 1 value stands out thatexceeds the 2.5 threshold forStudentized residuals; two otherresiduals are near 2.5 and may also beconsidered outliers.

studentr

-0. BO 7314856-0.8112167420.2672997376-0.413680617-0.383047862-0.364859123

0.6025379320. 18)600116

-0.0971449371 .0434806297-3.7937021380.69232340742.28647665380.2303580663-0.2711169670.21750019310.41529293220.279'33334860.530:30736852.2871777791-1 .3012697530.011 15174940. 646110806 15-0.481106391-0.23:1140148O.I66M77539-0 .01HSI703I0.34111032208

Studei

0

-4• I

tized Residuals vs Predicted Values

|© O

3L *

AOil 0 IftOO lOfK) Ujttf mW <OOU K000 'iMKt

O < -2.5 or > 2.5

r\ 12\_) Potential outliers (near 2. 5)

6

Relationship between XRF and Laboratory values of Pb ConcentrationIV. REGRESSION DIAGNOSTICS

a. View The Output Table ('october_out')

b. Plot of Predicted vs. Observed Values With 95 % CLMc. Outlier Detection / Residual Observations

I d. Influence Statistics

The presence of outliers tends to pull the regression response towards them, sometimes making their studentized residuals more obscure. To overcomethis, influence statistics measure the influence of each observation on the regression model Those with a stronger influence (more likely to be outliers)will have a greater influence statistic.The influence statistics of concern are RSTUDENT, OFF/IS , DFBETAS, and Cook's D. Also see the -2 -1012 plot!

The -2-1012 plot is another schematic of thedevialionofstudentized residuals from zero (0).

RSTUDENT is another version of studentizedresiduals, using the standard error from Ihe influencestatistics. A more sensitive residual statistic than the

the RSTUDENT should also follow ihe t-distriburion;however, three points deviate from zero greater than2.5 (these are the same 3 points identified in theresidual plot-previous slide).

DFF1TS measure the difference between thepredicted value for that observation and the equationestimated by all other observations except thatobservation.

COOK'S D is similar to DFFITS. but scaled to makemore extreme values stand out (outliers are moreobvious).

-4.illI.ZW' * I

Ml

.-•)Ill

t tnz*.«4TI Ml

-*.Mat ItT

-4 ttUi* HZ

EXTREME COOK'S D


V. REMOVE OUTLIERS / RE-RUN MODEL. • REXCVl C DTL 1.175 : RX-Pt

LI »t »ilr»'.i • IT tkftft II* p*> • , i' -1 .2 tlUW Xft pt » . :

-».» cb«» tif,.F* • • r• -7.* tiM l«_pb - . ;

' pfc ^ » t CiJ»

Siudtmired Rruduh i \ Prcdirtcd Vatara

O Ao

•.

Sas code (left) removes outliers in a new dataset Cnojjullier').Outliers determined by studenii7ed residuals and cook'sd.

•—

NEW REGRESSION MODEL!

14

XRF \ s Laboralon Lead Concentrations XRF \ s Labooion Lead Concent rations

All Data (n=28)

OVERALL MODEL: F = 1260; P < 0.0001

Adj R:: 0.970

Intercept: t = -3.09; P =0.005XRF: 1 = 35.51; P< 0.0001

I .ih Ph ( 2 0 W ) * X R I lid 1«

I .11 H' "'I'-.. I t|<

Outliers Removed (n=25)

OVERALL MODEL: F = 549.12; P < 0.0001

Adj R:: 0.958

Intercept: t = -2.87; P = 0.009XRF: t-23.43; P< 0.0001

Lab.Pb I I9 I5 I *XRI ; 726415

NEW SHAPEFILE FOR 'ADJUSTED' Pb CONCENTRATIONS

ID | X | ¥ | XIFJV | LAB_PB [ ADJUST

JN3-SXN-45

JN3-SXS-55

JN3-SXN-55

JN3-SLN-06

JN3-SXN-1 03

JN3-SXN-07

JN3-SXN-18

JN3-SXS-65

JN3-SXS-22

JN3-SXS-63

JN3-SXS-39

JN3-SXS-14

JN3-SXS-44

JN3-SXN-1 1 7

JN3-SXS-OS

JN3-SXS-S2

JN3-SXS-02

JN3-SXS-40

JN3-SXS-51

JN3-SXN-1 1 6

JN3-SXS-35

JN3-SXS-41

JN3-SXS-07

JN3-SXS-26

JN3-SXS-33

JN3-SXS-27

AA) LABORAT

FOR

B) THE RESU

448766 261290 4204565.80941

450914297857 420143268553

449024 177717 4204939.834150

449693 368995 4203823 667570

448437 4661 62 4205427 .57S22

451 226 498422 4203S85 388

451 040 321 955 4204422.69591

450672 996756 4201 999.976930

451 156.321 44 4201 756.088500

45021 5.14905 4201972165060

451333 335635 4199990.375510

452023 039485 4201 1 82.87098

449588 184472 4201043.677970

451062 976349 4205697.39362

451271 216999 4200716.160900

452711 9726SS 4201003.15436

452837 1 99359 42001 25 .51 4690

450894 497665 4200473.85893

4521 42 81 5274 4200957 86782

451687 6234S7 420551 S. 37205

451 1 77 256505 4202285.21 1 93

451371 647129 4200442080200

451 744 248672 4200738 923465

452234 566294 4201734.382820

208.85 420 420.00

366 7 430 43000

599 9 480 480 00

358.3 530 530.00

292.85 670 670.00

3734 710 710.00

274 2 840 840 00

523.2 960 960.00

1050 2000 2000.00

1 0 1.00

12 0 12.00

1 0 1 00

40 3 0 4.53

451 0 1373

4635 0 16.12

5005 0 2321

55.1 0 32.88

55.6 0 33.83

57 0 36.52

57.3 03709

58.7 0 39.77

61 .2 0 44.56

62 7 0 ;47.43

63.7 0 49.35

450772385912 4202173.105090 66.8 0 5528

4525C8328160 4201752740950 74 0 69.07

DJUSTED VALUE EQUALS:}RY VALUE FOR THOSE 28 SAMPLES ANALYZED IN THE LABORATORY

_T OF THE MODIFIED REGRESSION EQUATION:ADJUSTED VALUE - XRF*l.9l5- 72.64

16

8

OCT05_ADJU5T_PB

ADJUST

. < 200 PPM

. 200 - 400 PPM

400 - 800 PPM

. > 800 PPM

XRF VALUEUsing field : SRF_PB

Selection exist,

Sum • 37718.35Kin -1.0Sax - 1203.8JLvg = 256.58741496fcdian- 192.8Sea - 216.22855883

- 216.96780392- 46754.789654- 47075.037939- 2.0291026167« 4.8643346945

StdsVar

SkewKurt

ADJUSTED VALUEUsing field : ADJUST

N - 147Sum = 61863.91Mm = l.DMax - 2232.64

Hedian= 294.27

StdsVarVarsSkewKurt

411.559929184168237.494181169389.8057852.132114538135.2807909639

17

TEST OF PARALELLISM BETWEEN 2 XRF DEVICESMETHOD I: DUMMY VARIABLE AND INTERACT TEST

O U T L I E R S REMOVED ( n 2 5 )

nm-mm tarmv^nan

r. ' -• thin <hnr>tj

-If I»»MI I 51f-I -fa l»l«i o 4n»

-» » • ?»v*r i> . «rti

-0 M • (HIt. 01 «.*5M

18

9

TEST OF PARALELLISM BETWEEN 2 XRF DEVICESMETHOD 2: DUMMY VARIABLE (NO INTERACT TEST)

12 atvlc««"l'..i • i " tMx I-*;

rPf -M- «*ri«fl.j

I* rt • iff ,J* I IS*** It .' Mt

IttoJtB * -w-

ltl*X toy xsr ;Jtaui-« :iueS ' M

OUTLIERS REMOVED ( n - 2 5 )

at Mrew*tf<m> vtUi NiMlnq U*Kwi

**«-• r *»IUM F* > r

femcUrt fatal

IK* I MlHSMIS

131W43

JJ.IUI*

(I **.>6«

VWM*I« L^Mi or c«fc»Miilnurc^» inuruvt I -If l*l«

""" *~ ' -tt iSS*

t u*iu« Pr -• Ul fw. I :

TEST OF PARALELLISM BETWEEN 2 XRF DEVICESMETHOD 3: PROC GLM

01 ILIhRS REMOVED (n - ^5)- -. - , .. . . . . . . .' '«— w*« ; VEW %• • Czca JUtn 1-lH* * T7«

EamBkwTb^ iwrnwE*v«.i w e-^ «rprar M* d*tv*n^ • i* lit •

Ml t*^'. «*_tt «*Y>« «f_^**v.« /!»fc«i .r* i* - OH! »p> 3

clt^l O^s-w 1 llt'rarf iTL'-'c-.rM.:«uit

Mi «3.

• -I

* TTP. I

The Gl.I1 Procedure

dependent Variable: LAB _PB Labor a to

Source DF

Model 9

Error 21

Corrected Total 24

R -Square C

0.972164

Source DF

XRF PB 1DEVICE 1XRF_PB*DEVICE 1

Source DF

XRF PB 1DEVICE 1XRF PB*DEVICE 1

ry pom

Sum ofSquares

3821230.088

109415.352

3930645.440

Mean Square F Value Pr > F

1273743.363 244.47 < .0001

5210.255

oeff Var Root PISE LAB..F8 Mean

19.26500 72.

Type 1 1 SS

3561372.0131005.437

21375.669

Type 1 1 1 SS

1392324.2851005.437

21375.669

18210 374.6800

Mean Square F Value Pr > F

3561372.01 3 683.53 < .00011005.437 0.19 O.GG49

21375. EG9 4. 10 0.0557

Dean Square F Value Pr > F

1392324.285 267.23 <.00011005.437 0.19 0.6649

21375.669 4.10 0.0557

20

10

PARALLELISM SCATTER PLOT WITH REGRESSION LINES( i r i l . lKKS Rl \I()\ K l ) ( n = 25 )

\RF\s Laboralon. Lead ConcentrationsIT TM pcvrcc

XRF in*"*CCV1CI *•• XLM — 'I

NOl'fc. N(l SK.N1I !t \NI l.in-.c I l.lh 1)1 VIC |- ON 1 \B !>B C()N{ 0 - O.(l5)Mil Kl H IK I Kl (.KI'.^SION ! • ( _ ) ( ' \ | IONS ] ' ( )R INDIVIDU.M. DEVICES 91

(NOTK i -I !> l\ :>l ! i ! < M I N l N f ; -\DJHSTF-t) PH V V

TEST OF PARALLELISM BETWEEN DEVICES(NO OUTLIERS REMOVED - ALL DATA |n = 28||

PROCGLM (TYPE iuss)

OVERALL MODEL:Fu, = 949.60: P< 0.001

PARAMETERS:XRF: F- 191.27: P< 0.001DEVICE: F = 3.25; f = 0.084XRF 'DEVIO- F :4?9. P- D . U C I I

X R F \ s Laboralon Lead ( onccntralions

PROCREG (METHODS)

OVERALL MODEL:F,,7- 949.60; P< 0.001

PARAMETERS:XRF: t-4.51 : />< 0.001INTERCEPT: t= 1.36: P- 0.188DEVICE(Z): t « - l . 8 0 ; P = 0.084/R l -S I : ] I t 4%. /' (l()»!

. I ff

22

11

EFFECT OF SOIL MOISTURE - WEEK 1 ONLY(18-21 OCTOBER2005)

SOIL MOISTURE: 'DRV vs 'WET'

XRF \t I \Bt >RAT( >RY 1BAD a iNCENTRATK WS

18OCT-- 'DRY'19OCT = 'DRY'20OCT- 'WET'21OCT= 'WET'

I"

MJ.,,.,,1

PROCREG (METHOD .1)

OVERALL MODEL:F,.,, = 283.22; P< 0.001

PARAMETERS:XRF: 1 = 28.04; P<O.OOIINTERCEPT: t = - l .77; /> = 0.099DEVICE (Z): t = 0.30; P= 0.766/ R t - S I I I 1 044 /' 0 !

23

EFFECT OF WEATHER ON XRF-LAB RELATIONSHIPTEST OF PARALLELISM BICTWEEN WEATHER CATEGORIES (SUNNY vs OVERCAST)

TTST (Jt PUMLLCLJ5I — HT «1TB

- true OUI - «.» John JWM tfj. Ill «;;p«t«Ll»Un (or* »LBP«* •TUHll fac UM t«e

nj [<::' f if»ll«Uj. XBT dwtcM. Da* Trp* III r-« at 5<r«r<« 35

- * xtt pfa IKATM*

xrr .-j i •*...-. .'SY BitTHEF ' . H L ' i f i f f Jt»»i<Ul' . '

I (1.-MH.: U* n L*ur.10ry „.

BA

9 iririn.tw

M HI.? *;t

11Mtt41 . M9

t .H3MI « 041/1

ifeoi «se i*.ji« »-»

R.ttUi in.Hot

?i;s431 55 • >W1

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F WhM FV

24

12

XRF vs. Laboratory Lead ConcentrationsBY WEATHER CATOEWY

— <wo

•i 50

XKFljjpui)25

13

Appendix B:

Laboratory Results for Sampling Event #3

Soils—ICP Metals Analysis

SAMPDATA So/I ICP Metals

CLIENTSuperfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,

US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region SUS EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5

PROJECTJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsville

LABNAMEAlton - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlton - ESAT ContractAlion - ESAT Contract

SAMPLENAMEJN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS61-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS25-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SLS65-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SXS46-01

LABSAMPIDE5 10002-01E51 0002-01E51 0002-01E510002-01E51 0002-01E51 0002-01E51 0002-01E51 0002-01E510002-01E51 0002-01E510002-01E510002-01E51 0002-01E51 0002-01E51 0002-01E51 0002-01E51 0002-01E510002-01E51 0002-02E5 10002-02E51 0002-02E5 10002-02E51 0002-02E5 10002-02E510002-02E51 0002-02E5 10002-02E5 10002-02E51 0002-02E5 10002-02E51 0002-02E51 0002-02E51 0002-02E51 0002-02E51 0002-02E51 0002-02E51 0002-03E51 0002-03E5 10002-03E51 0002-03E5 10002-03E51 0002-03E5 10002-03E51 0002-03E51 0002-03E51 0002-03E51 0002-03E5 10002-03E510002-03E5 10002-03E51 0002-03E5 10002-03E51 0002-03E51 0002-03E51 0002-04E51 0002-04E51 0002-04E51 0002-04E51 0002-04E51 0002-04E5 10002-04E51 0002-04E51 0002-04E51 0002-04E51 0002-04E5 10002-04E51 0002-04E5 10002-04E51 0002-04

MATRIX SAMPDATE PREPDATE ANADATE BATCH METHODCODESoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoil

10/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/2005

11/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/2005

11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)

METHODNAME PREPNAMEEPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200. 7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7

Hot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block Digestion

ANALYTEAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilver

CASNUMBER7429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-4

SURROGATE RESULT DL RL UNITSFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSE

7900860.61

U20009.9111320000391500

66014830U16156976001100.64

1.12600148.245480002701500

50020880U341737080002500.71

1.22600156.644230009601700

41015840U30213205800670.46

0.75

59009.59.026220001401700

490211100U

5.9 20 mg/kg0.24 0.79 mg/kg0.040 0.099 mg/kg0.47 1 .6 mg/kg6.7 20 mg/kg1.4 4.9 mg/kg1.2 4.0 mg/kg0.30 0.99 mg/kg3.6 12 mg/kg16 49 mg/kg5.9 1 8 mg/kg0.16 0.49 mg/kg1.6 6.9 mg/kg20 63 mg/kg0.40 1 .2 mg/kg5.9 20 mg/kg1.4 4.9 mg/kg1.4 4.9 mg/kg5.9 20 mg/kg0.23 0.78 mg/kg0.039 0.098 mg/kg0.47 1.6 mg/kg6.6 20 mg/kg1.4 4.9 mg/kg1.2 3.9 mg/kg0.29 0.98 mg/kg3.5 12 mg/kg16 49 mg/kg5.9 18 mg/kg0.16 0.49 mg/kg1 .6 6.8 mg/kg20 63 mg/kg0.39 1.2 mg/kg5.9 20 mg/kg1.4 4.9 mg/kg1.4 4.9 mg/kg5.9 20 mg/kg0.24 0.78 mg/kg0.039 0.098 mg/kg0.47 1.6 mg/kg6.7 20 mg/kg1.4 4.9 mg/kg1 .2 3.9 mg/kg0.29 0.98 mg/kg3.5 12 mg/kg16 49 mg/kg5.9 18 mg/kg0.16 0.49 mg/kg1.6 6.9 mg/kg20 63 mg/kg0.39 1 .2 mg/kg5.9 20 mg/kg1 .4 4.9 mg/kg1 .4 4.9 mg/kg5.8 19 mg/kg0.23 0.77 mg/kg0.038 0.096 mg/kg0.46 1 .5 mg/kg6.5 19 mg/kg1 .4 4.8 mg/kg1 .2 3.8 mg/kg0.29 0.96 mg/kg3.5 12 mg/kg15 48 mg/kg5.8 17 mg/kg0.15 0.48 mg/kg1.5 6.7 mg/kg19 61 mg/kg0.38 1.2 mg/kg

BASIS DILUTION ANALYST ANOTEDRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1

SCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSC

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Page 1

SAMPDATA Soil ICP Metals


US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5


LABNAMEAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT Contract

SAMPLENAMEJN3-SXS46-01JN3-SXS46-01JN3-SXS46-01JN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS20-DZJN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS12-01JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-02JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01

LABSAMPIDE51 0002-04E5 10002-04E5 10002-04E51 0002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-05E5 10002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-05E51 0002-06E51 0002-06E51 0002-06E51 0002-06E51 0002-06E51 0002-06E51 0002-06E51 0002-06E51 0002-06E51 0002-06E51 0002-06E5 10002-06E5 10002-06E51 0002-06E51 0002-06E51 0002-06E5 10002-06E5 10002-06E5 10002-07E51 0002-07E51 0002-07E5 10002-07E5 10002-07E5 10002-07E51 0002-07E51 0002-07E51 0002-07E5 10002-07E5 10002-07E51 0002-07E51 0002-07E51 0002-07E5 10002-07E51 0002-07E51 0002-07E51 0002-07E51 0002-08E5 10002-08E51 0002-08E51 0002-08E51 0002-08E51 0002-08E5 10002-08E510002-08E51 0002-08E51 0002-08E51 0002-08E51 0002-08

MATRIX SAMPDATE PREPDATE ANADATE BATCH METHODCODE METHODNAME PREPNAMESoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoil

10/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/2005

11/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/2005

11/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.7


ANALYTESodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganese

CASNUMBER7440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-5

SURROGATEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSE

RESULT191222084008400.73

3.92400258.7442300063001400

59017780U28201000

6900660.53

0.56

11009.85.122190003401200

30012680U151611076001300.60

0.90

5100107.719180001901300

67015950U321414075001300.64

0.98

55009.97.321210002501300

690

DL RL5.8 191.3 4.81.3 4.86.0 200.24 0.80

0.040 0.100.48 1.66.8 201.4 5.01.2 4.00.30 1.03.6 1216 506.0 180.16 0.50

1.6 7.020 640.40 1.26.0 201.4 5.01.4 5.05.8 190.23 0.77

0.038 0.0960.46 1.56.5 191.4 4.81.2 3.80.29 0.96

3.5 1215 485.8 170.15 0.48

1.5 6.719 620.38 1.25.8 191.3 4.81.3 4.85.9 200.24 0.79

0.039 0.0990.47 1.66.7 201.4 4.91.2 3.90.30 0.99

3.6 1216 495.9 180.16 0.49

1.6 6.920 630.39 1.25.9 201.4 4.91.4 4.95.9 200.24 0.79

0.040 0.0990.48 1.66.7 201.4 4.91.2 4.00.30 0.993.6 1216 495.9 180.16 0.49

UNITS BASISmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRY

DILUTION ANALYST ANO111111111111111111111111111111111111111111111111111111111111111111111

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Page 2






SAMPLENAMEJN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS59-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS79-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS55-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS47-01JN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS 16-01JN3-SLS16-01JN3-SLS16-01

LABSAMPIDE51 0002-08E51 0002-08E51 0002-08E51 0002-08E51 0002-08E5 10002-08E51 0002-09E51 0002-09E51 0002-09E51 0002-09E5 10002-09E51 0002-09E51 0002-09E51 0002-09E51 0002-09E5 10002-09E51 0002-09E51 0002-09E5 10002-09E51 0002-09E51 0002-09E51 0002-09E51 0002-09E51 0002-09E5 10002-10E5 10002-10E51 0002-10E510002-10E51 0002-10E51 0002-10E51 0002-10E5 10002-10E51 0002-10E51 0002-10E5 10002-10E5 10002-10E51 0002-10E51 0002-10E5 10002-10E51 0002-10E51 0002-10E510002-10E5 10002-11E51 0002-11E51 0002-11E5 10002-11E51 0002-11E51 0002-11E51 0002-11E5 10002-11E51 0002-11E51 0002-11E51 0002-11E51 0002-11E51 0002-11E5 10002- 11E51 0002-11E51 0002-11E51 0002-11E51 0002-11E510002-12E51 0002-1 2E51 0002-1 2E51 0002-1 2E510002-12E510002-12E51 0002-1 2E51 0002-1 2E51 0002-1 2


10/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/2005

11/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/20051 1/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/2005

11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)

METHODNAME PREPNAMEEPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7


ANALYTENickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron

CASNUMBER7440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-6

SURROGATE RESULT DL RLFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSE

16930U44141607000800.59

U20009.77.523190002201200

52014750U241511078001400.63

0.732100

157.819190004301400

56015720U23172005800700.53

0.46

2100

9.17.320180001301300

31014790U31111308600680.60U2400129.12125000

1.6 6.920 630.40 1.25.9 201.4 4.91.4 4.95.7 190.23 0.77

0.038 0.0960.46 1.56.5 191.4 4.81.1 3.80.29 0.963.4 1115 485.7 170.15 0.48

1.5 6.719 610.38 1.15.7 191.3 4.81.3 4.85.6 190.22 0.75

0.037 0.0930.45 1.56.3 191.3 4.71.1 3.70.28 0.933.4 1115 475.6 170.15 0.47

1.5 6.519 600.37 1.15.6 191.3 4.71.3 4.75.7 190.23 0.76

0.038 0.0950.46 1.56.5 191.4 4.81.1 3.80.29 0.95

3.4 1115 485.7 170.15 0.48

1.5 6.719 610.38 1.15.7 191.3 4.81.3 4.86.0 200.24 0.80

0.040 0.100.48 1.66.8 201.4 5.01.2 4.00.30 1.03.6 12

UNITSmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kg

BASIS DILUTION ANALYST ANOTEDRY 1DRY 1DRY 1DRY 1DRYDRYDRYDRYDRYDRYDRYDRYDRYDRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1


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Page3





LABNAMEAlton - ESAT ContractAlton - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlton - ESAT ContractAlion - ESAT ContractAlton - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT Contract

SAMPLENAMEJN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS16-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS28-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLS22-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN6-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01

LABSAMPIDE51 0002-1 2E510002-12E510002-12E510002-12E510002-12E510002-12E5 10002- 12E51 0002-1 2E510002-12E51 0002-1 3E51 0002-1 3E51 0002-1 3E51 0002-1 3E51 0002-1 3E510002-13E51 0002-1 3E51 0002-1 3E51 0002-1 3E5 10002-1 3E510002-13E51 0002-1 3E51 0002-1 3E510002-13E51 0002-1 3E51 0002-1 3E5 10002-1 3E510002-13E510002-14E510002-14E5 10002-1 4E510002-14E510002-14E510002-14E5 10002-1 4E510002-14E510002-14E5 10002-1 4E51 0002-14E510002-14E510002-14E510002-14E5 10002-1 4E510002-14E510002-14E510002-14E5 10002-1 5E51 0002-1 5E51 0002-1 5E51 0002-1 5E51 0002-1 5E51 0002-1 5E51 0002-1 5E510002-15E510002-15E51 0002-1 5E51 0002-1 5E510002-15E510002-15E510002-15E51 0002-1 5E51 0002-1 5E510002-15E510002-15E510002-16E510002-16E510002-16E510002-16E510002-16E51 0002-1 6


10/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/2005

11/1/200511/1/200511/1/200511/1/200511/1/200511/1/20051 1/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/2005

11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ531 02 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53 102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)11/8/2005 EJ53102 Metals SF ICP (S)1 1/8/2005 EJ53102 Metals SF ICP (S)



ANALYTELeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromium

CASNUMBER7439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-3


1102100

43020990U291511083001100.77

1.22700178.325250001701700

530171100

0.65

352017077002900.68

0.58

3500196.6382100020001400

69020630U90162007100

3000.692.911000206.6562100053023005402613000.48881753088003501.02.52100020

16 506.0 180.16 0.50

1.6 7.020 640.40 1.26.0 201.4 5.01.4 5.06.0 200.24 0.80

0.040 0.100.48 1.66.8 201.4 5.01.2 4.00.30 1.03.6 1216 506.0 180.16 0.50

1.6 7.020 640.40 1.26.0 201.4 5.01.4 5.05.9 200.24 0.79

0.040 0.0990.48 1.66.7 201.4 5.01.2 4.00.30 0.99

3.6 1216 505.9 180.16 0.50

1.6 6.920 630.40 1.25.9 201.4 5.01.4 5.06.0 200.24 0.80

0.040 0.100.48 1 .66.8 201.4 5.01.2 4.00.30 1.03.6 1216 506.0 180.16 0.50

1.6 7.020 640.40 1 .26.0 201.4 5.01.4 5.05.8 190.23 0.77

0.039 0.0960.46 1.56.6 191.4 4.8

UNITS BASIS DILUTION ANALYST ANOTEmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRY

111111111111111111111111111111111111111111111111111111111111111111111


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SAMPLENAMEJN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLN07-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLS50-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN55-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN51-01JN3-SLN103-01JN3-SLN 103-01JN3-SLN 103-01

LABSAMPIDE51 0002-1 6E510002-16E51 0002-1 6E51 0002-1 6E51 0002-1 6E51 0002-1 6E51 0002-1 6E51 0002-1 6E51 0002-1 6E51 0002-1 6E51 0002-1 6E51 0002-1 6E51 0002-1 7E51 0002-1 7E51 0002-1 7E51 0002-1 7E51 0002-1 7E51 0002-1 7E51 0002-1 7E51 0002-1 7E5 10002-1 7E51 0002-1 7E51 0002-1 7E510002-17E5 10002-1 7E51 0002-1 7E51 0002-1 7E5 10002-1 7E51 0002-1 7E51 0002-1 7E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E510002-18E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 8E51 0002-1 9E51 0002-1 9E510002-19E51 0002-1 9E51 0002-1 9E51 0002-1 9E510002-19E51 0002-1 9E51 0002-1 9E51 0002-1 9E51 0002-1 9E510002-19E51 0002-1 9E51 0002-1 9E51 0002-1 9E510002-19E51 0002-1 9E51 0002-1 9E51 0002-20E51 0002-20E51 0002-20

MATRIX SAMPDATE PREPDATE ANADATE BATCHSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoil

10/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/20/200510/20/200510/20/2005

11/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/2005

11/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ53102

METHODCODEMetals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)



ANALYTECobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBeryllium

CASNUMBER7440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-7

SURROGATEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSE

RESULT DL RL7.360380007102000430261800

0.74

310315307700770.56

U1600118.114210001001500

38015650U321510079001600.80

1.28400181431240004803800910311300

U861433073001100.73

0.72

2800115.723180002601300

42014780U371714073001800.62

1.2 3.90.29 0.963.5 1215 485.8 170.15 0.48

1.5 6.819 620.39 1.25.8 191.4 4.81.4 4.85.8 190.23 0.77

0.038 0.0960.46 1.56.5 191.4 4.81.2 3.80.29 0.963.5 1215 485.8 170.15 0.48

1.5 6.719 610.38 1.25.8 191.3 4.81.3 4.86.0 200.24 0.800.040 0.100.48 1.66.8 201 .4 5.01.2 4.00.30 1.03.6 1216 506.0 180.16 0.50

1.6 7.020 640.40 1.26.0 201.4 5.01.4 5.05.8 190.23 0.77

0.039 0.0970.46 1.56.6 191.4 4.81.2 3.90.29 0.97

3.5 1215 485.8 170.15 0.48

1.5 6.819 620.39 1.25.8 191.4 4.81.4 4.85.7 190.23 0.77

0.038 0.096

UNITS BASISmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYrng/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRYmg/kg DRY

DILUTION ANALYST ANOTE111111111111111111111111111111111111111111111111111111111111111111111


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SAMPLENAMEJN3-SLN103-01JN3-SLN103-01JN3-SLN103-01JN3-SLN103-01JN3-SLN103-01JN3-SLN103-01JN3-SLN1 03-01JN3-SLN103-01JN3-SLN103-01JN3-SLN 103-01JN3-SLN103-01JN3-SLN103-01JN3-SLN103-01JN3-SLN103-01JN3-SLN103-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SXN1 14-01JN3-SLN106-01JN3-SLN106-01JN3-SLN106-01JN3-SLN1 06-01JN3-SLN 106-01JN3-SLN 106-01JN3-SLN106-01JN3-SLN106-01JN3-SLN106-01JN3-SLN 106-01JN3-SLN106-01JN3-SLN106-01JN3-SLN106-01JN3-SLN1 06-01JN3-SLN106-01JN3-SLN 106-01JN3-SLN106-01JN3-SLN106-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01JN3-SLS38-01

LABSAMPIDE51 0002-20E51 0002-20E51 0002-20E51 0002-20E5 10002-20E51 0002-20E5 10002-20E51 0002-20E51 0002-20E51 0002-20E51 0002-20E51 0002-20E5 10002-20E5 10002-20E5 10002-20E510002-21E51 0002-21E510002-21E510002-21E5 10002-21E510002-21E51 0002-21E51 0002-21E5 10002-21E510002-21E510002-21E510002-21E5 10002-21E510002-21E510002-21E51 0002-21E510002-21E5 10002-21E51 0002-22E51 0002-22E5 10002-22E5 10002-22E51 0002-22E51 0002-22E51 0002-22E5 10002-22E5 10002-22E51 0002-22E51 0002-22E51 0002-22E51 0002-22E5 10002-22£510002-22E51 0002-22E51 0002-22E51 0002-22E5 10002-23E51 0002-23E51 0002-23E51 0002-23E5 10002-23E5 10002-23E51 0002-23E51 0002-23E51 0002-23E51 0002-23E5 10002-23E5 10002-23E5 10002-23E51 0002-23E51 0002-23E510002-23E51 0002-23E5 10002-23

MATRIX SAMPDATE PREPDATE ANADATE BATCHSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoil

10/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/200510/25/2005

11/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/2005

11/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ53102

METHODCODEMetals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)



ANALYTECadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZinc

CASNUMBER7440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-6

SURROGATE RESULT DLFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSE

1.839000189.4482400067038007102912000.94

96183808800850.59

0.81

2800148.02424000741900

58020960U34181508100

1700.84

1.5560016124325000360200069019960U71252608300990.80

0.54

24000149.03326000190220065019970U5324160

0.46

6.51.41.10.29

3.4155.70.15

1.5190.38

5.71.31.36.00.24

0.0400.48

6.81.41.20.30

3.6166.00.16

1.6200.406.01.41.45.70.23

0.0380.46

6.51.41.10.293.4155.70.15

1.5190.38

5.71.31.35.90.24

0.0400.48

6.71.41.20.30

3.6165.90.16

1.6200.40

5.91.41.4

RL UNITS1.5 mg/kg19 mg/kg4.8 mg/kg3.8 mg/kg0.96 mg/kg1 1 mg/kg48 mg/kg1 7 mg/kg0.48 mg/kg6.7 mg/kg61 mg/kg1.1 mg/kg19 mg/kg4.8 mg/kg4.8 mg/kg20 mg/kg0.80 mg/kg0.10 mg/kg1.6 mg/kg20 mg/kg5.0 mg/kg4.0 mg/kg1.0 mg/kg12 mg/kg50 mg/kg18 mg/kg0.50 mg/kg7.0 mg/kg64 mg/kg1 .2 mg/kg20 mg/kg5.0 mg/kg5.0 mg/kg19 mg/kg0.76 mg/kg0.096 mg/kg1.5 mg/kg19 mg/kg4.8 mg/kg3.8 mg/kg0.96 mg/kg1 1 mg/kg48 mg/kg17 mg/kg0.48 mg/kg6.7 mg/kg61 mg/kg1.1 mg/kg19 mg/kg4.8 mg/kg4.8 mg/kg20 mg/kg0.79 mg/kg0.099 mg/kg1.6 mg/kg20 mg/kg5.0 mg/kg4.0 mg/kg0.99 mg/kg12 mg/kg50 mg/kg18 mg/kg0.50 mg/kg6.9 mg/kg63 mg/kg1 .2 mg/kg20 mg/kg5.0 mg/kg5.0 mg/kg



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SAMPLENAMEJN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SXS355-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN 16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN16-01JN3-SLN 18-01JN3-SLN18-01JN3-SLN18-01JN3-SLN18-01JN3-SLN18-01JN3-SLN18-01JN3-SLN18-01JN3-SLN18-01JN3-SLN18-01JN3-SLN 18-01JN3-SLN18-01JN3-SLN 18-01JN3-SLN18-01JN3-SLN18-01JN3-SLN 18-01JN3-SLN18-01JN3-SLN18-01JN3-SLN18-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN39-01

LABSAMPIDE5 10002-24E51 0002-24E5 10002-24E51 0002-24E51 0002-24E51 0002-24E51 0002-24E5 10002-24E51 0002-24E51 0002-24E51 0002-24E510002-24E51 0002-24E5 10002-24E51 0002-24E5 10002-24E51 0002-24E51 0002-24E5 10002-25E51 0002-25E5 10002-25E51 0002-25E5 10002-25E51 0002-25E51 0002-25E5 10002-25E51 0002-25E51 0002-25E51 0002-25E51 0002-25E5 10002-25E51 0002-25E51 0002-25E51 0002-25E51 0002-25E5 10002-25E5 10002-26E5 10002-26E51 0002-26E5 10002-26E51 0002-26E51 0002-26E5 10002-26E51 0002-26E5 10002-26E51 0002-26E510002-26E51 0002-26E510002-26E51 0002-26E51 0002-26E51 0002-26E51 0002-26E5 10002-26E510002-27E51 0002-27E51 0002-27E51 0002-27E51 0002-27E51 0002-27E5 10002-27E5 10002-27E5 10002-27E51 0002-27E51 0002-27E51 0002-27E5 10002-27E51 0002-27E5 10002-27

MATRIX SAMPDATE PREPDATE ANADATE BATCH METHODCODE METHODNAME PREPNAMESoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoil

10/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/26/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/2005

11/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/20051 1/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/20051 1/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/2005

11/8/2005 EJ53102 Metals SF ICP (S) EPA200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.71 1/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA 200.711/8/2005 EJ531 02 Metals SF ICP (S) EPA 200.711/8/2005 EJ53 102 Metals SF ICP (S) EPA200.711/8/2005 EJ53102 Metals SF ICP (S) EPA 200.7


ANALYTEAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilver

CASNUMBER7429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-4


6400840.63

U27009.15.51316000741200

82014680U19177072001600.66

0.814600138.123190003601800

540171000

0.88

341525066001600.82

1.43600146.629240008401300

50016920U362430059001100.69

1,04900114.925140003201400

28015900U

5.6 190.22 0.75

0.037 0.0940.45 1.56.4 191.3 4.71.1 3.70.28 0.94

3.4 1115 475.6 170.15 0.47

1.5 6.619 600.37 1.15.6 191.3 4.71.3 4.76.0 200.24 0.800.040 0.100.48 1.66.8 201.4 5.01.2 4.00.30 1.03.6 1216 506.0 180.16 0.50

1.6 7.020 640.40 1.26.0 201.4 5.01.4 5.05.9 200.24 0.79

0.040 0.0990.47 1.66.7 201.4 4.91.2 4.00.30 0.99

3.6 1216 495.9 180.16 0.491.6 6.920 630.40 1.25.9 201.4 4.91.4 4.96.0 200.24 0.80

0.040 0.100.48 1.66.8 201.4 5.01.2 4.00.30 1.03.6 1216 506.0 180.16 0.50

1.6 7.020 640.40 1.2

UNITSmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kg



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CLIENTSuperfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,

US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5

PROJECTJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsville

LABNAMEAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT ContractAlion - ESAT Contract

SAMPLENAMEJN3-SLN39-01JN3-SLN39-01JN3-SLN39-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN45-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01JN3-SLN22-01

LABSAMPIDE51 0002-27E51 0002-27E51 0002-27E51 0002-28E51 0002-28E51 0002-28E5 10002-28E51 0002-28E51 0002-28E51 0002-28E51 0002-28E5 10002-28E51 0002-28E5 10002-28E51 0002-28E51 0002-28E51 0002-28E5 10002-28E510002-28E5 10002-28E51 0002-28E5 10002-29E51 0002-29E51 0002-29E5 10002-29E51 0002-29E51 0002-29E5 10002-29E51 0002-29E51 0002-29E51 0002-29E5 10002-29E51 0002-29E51 0002-29E51 0002-29E51 0002-29E5 10002-29E51 0002-29E51 0002-29

MATRIX SAMPDATE PREPDATE ANADATE BATCHSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoil

10/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/200510/19/2005

11/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/20051 1/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/2005

11/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ5310211/8/2005 EJ53102

METHODCODEMetals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)Metals SF ICP (S)

METHODNAME PREPNAMEEPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7

Hot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block Digestion

ANALYTESodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZincAluminumBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSilverSodiumVanadiumZinc

CASNUMBER7440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-67429-90-57440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57440-02-27440-09-77440-22-47440-23-57440-62-27440-66-6

SURROGATE RESULT DL RLFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSE

301717086001601.51.24000171073300004202000520261300

U280261700

70001100.77

0.93

4300126.924220002701500

45017750U3027170

6.0 201.4 5.01.4 5.05.7 190.23 0.77

0.038 0.0960.46 1.56.5 191.4 4.81.1 3.80.29 0.96

3.4 1115 485.7 170.15 0.48

1.5 6.719 610.38 1.15.7 191.3 4.81.3 4.86.0 200.24 0.80

0.040 0.100.48 1.66.8 201.4 5.01.2 4.00.30 1.03.6 1216 506.0 180.16 0.50

1.6 7.020 640.40 1.26.0 201.4 5.01.4 5.0

UNITSmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kg

BASIS DILUTION ANALYST ANOTEDRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1DRY 1

SCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSCSC

KL

*

J

J

L

L

•*

J

J

LKL

Page 8

LNOTE Soil ICP Metals

QUALIFIEI DESCRIPTION# Spike audit not valid. The sample concentration exceeds twice the concentration of the spike added. No qualification made for this QC audit.* The duplicate analysis precision is not within control limits. The reported value is estimated.

< 5X One or both concentration values for the duplicate analysis audit were less than 5 times the MDL value AND the difference between the two values was less than the MDL value. The duplicate audit is acceptable. No qualification made for this QC audit.J The identification of the analyte is acceptable; the reported value is an estimate.K The identification of the analyte is acceptable; the reported value may be biased high. The actual value is expected to be less than the reported value.L The identification of the analyte is acceptable; the reported value may be biased low. The actual value is expected to be greater than the reported value.X U

Page 1

Soils-Arsenic (As) Analysis

SAMPDATA Soil As

CLIENT PROJECT LABNAME SAMPLENAMESuperfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS61-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS25-01Superfund. US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS65-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SXS46-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS20-DZSuperfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS12-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS59-02Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS59-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS79-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS55-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS47-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS16-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS28-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS22-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN6-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN07-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS50-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN55-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN51-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN103-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SXN1 14-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN106-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS38-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SXS355-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN16-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN18-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN39-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN45-01Superfund, US EPA Region 5 Jacofasville Alion - ESAT Contract JN3-SLN22-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS40-RB

LABSAMPIDE510002-01E51 0002-02E51 0002-03E510002-04E51 0002-05E51 0002-06E5 10002-07E6 10002-08E510002-09E510002-10E51 0002-11E510002-12E510002-13E51 0002-14E510002-15E51 0002-1 6E5 10002- 17

E5 10002-1 8E510002-19E5 10002-20E51 0002-21E510002-22E510002-23E510002-24E51 0002-25E510002-26E5 10002-27E510002-28E510002-29E510002-30

MATRIX

SoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilWater

SAMPDATE PREPDATE10/18/200510/19/200510/19/200510/20/200510/20/200510/20/200510/21/200510/21/200510/24/200510/24/200510/25/200510/25/200510/25/200510/25/200510/18/200510/24/200510/26/200510/20/200510/19/200510/20/200510/24/200510/21/200510/25/200510/26/200510/19/200510/24/200510/19/200510/19/200510/19/200510/20/2005

11/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/200511/1/2005

10/31/2005

ANADATE BATCH11/2/2005 EJ5310211/2/2005 EJ5310211/2/2005 EJ5310211/2/2005 EJ5310211/3/2005 EJ5310211/2/2005 EJ5310211/2/2005 EJ5310211/2/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/2/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/2/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/3/2005 EJ5310211/2/2005 EJ53103

METHODCODE METHODNAMEGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 AsGFAA 800 As

METALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAAMETALS GFAA

PREPNAME

Hot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block Digestion

ANALYTE CASNUMBER

ArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenicArsenic

7440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-27440-38-2

SURROGATE RESULT DL RL UNITS BASIS DILUTION ANALYST ANOTEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSE

8.99

12.816.312.728.6

11.710.512.4

11.811.7

8.7516.713.015.6

12.815.8

10.611.511.220.814.7

16.322.7

10.811.619.59.7718.116.6

U

0.20 0.79 mg/kg DRY0.39 1.56 mg/kg DRY0.39 1.57 mg/kg DRY0.38 1.53 mg/kg DRY1.00 3.99 mg/kg DRY0.38 1.54 mg/kg DRY0.39 1.58 mg/kg DRY0.40 1.58 mg/kg DRY0.48 1.91 mg/kg DRY0.47 1.86 mg/kg DRY0.19 0.76 mg/kg DRY0.50 2.00 mg/kg DRY0.50 2.00 mg/kg DRY0.50 1.98 mg/kg DRY0.50 2.00 mg/kg DRY0.48 1.93 mg/kg DRY0.48 1.92 mg/kg DRY0.50 1.99 mg/kg DRY0.48 1.93 mg/kg DRY0.48 1.91 mg/kg DRY0.50 2.00 mg/kg DRY0.48 1.91 mg/kg DRY0.99 3.97 mg/kg DRY0.47 1.87 mg/kg DRY0.50 1.99 mg/kg DRY0.49 1.98 mg/kg DRY0.50 2.00 mg/kg DRY0.48 1.92 mg/kg DRY0.50 1.99 mg/kg DRY0.5 2.0 ug/L NA

244

41044

455

2555

55555

5551055

555

51

SCscSC

scscscscscscscscscscscscscscscscscscscscscscscscscscsc

Page 1

LNOTE Soil As

QUALIFIER DESCRIPTION< 5X One or both concentration values for the duplicate analysis audit were less than 5 times the MDL value AND the difference between the two values was less than the MDL value. The duplicate audit is acceptable. No qualification made for this Q(L The identification of the analyte is acceptable; the reported value may be biased low. The actual value is expected to be greater than the reported value.

Page 1

Soils—pH Analysis

SAMPDATA Soil pH

CLIENT PROJECT LABNAME SAMPLENAMESuperfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS61-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS25-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS65-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SXS46-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS20-DZSuperfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS12-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS59-02Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS59-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS79-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS55-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS47-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS16-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS28-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS22-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN6-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN07-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS50-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN5S-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN51-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN103-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SXN1 14-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN106-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLS38-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SXS355-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN16-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN18-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN39-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN45-01Superfund, US EPA Region 5 Jacobsville Alion - ESAT Contract JN3-SLN22-01

LABSAMPIDE51 0002-01E51 0002-02E51 0002-03E51 0002-04E5 10002-05E51 0002-06E51 0002-07E51 0002-08E51 0002-09E51 0002-10E51 0002-11E51 0002-1 2E51 0002-1 3E510002-14E510002-15E51 0002-1 6E51 0002-1 7E51 0002-1 8E51 0002-1 9E51 0002-20E51 0002-21E51 0002-22E51 0002-23E51 0002-24E51 0002-25E51 0002-26E51 0002-27E51 0002-28E51 0002-29

MATRIX SAMPDATE PREPDATE ANADATE BATCH

SoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoilSoil

10/18/200510/19/200510/19/200510/20/200510/20/200510/20/200510/21/200510/21/200510/24/200510/24/200510/25/200510/25/200510/25/200510/25/200510/18/200510/24/200510/26/200510/20/200510/19/200510/20/200510/24/200510/21/200510/25/200510/26/200510/19/200510/24/200510/19/200510/19/200510/19/2005

10/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/28/2005 10/28/2005 EK5020110/31/2005 10/31/2005 EK5080110/31/2005 10/31/2005 EK5080110/31/2005 10/31/2005 EK5080110/31/2005 10/31/2005 EK5080110/31/2005 10/31/2005 EK5080110/31/2005 10/31/2005 EK5080110/31/2005 10/31/2005 EK5080110/31/2005 10/31/2005 EK5080110/31/2005 10/31/2005 EK5080110/31/2005 10/31/2005 EK5080110/31/2005 10/31/2005 EK50801

METHODCODEpH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespM Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespM Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespM Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastespH Soils and wastes

METHODNAME

SW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045CSW-846 9045C

PREPNAMEGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral PreparationGeneral Preparation

ANALYTE CASNUMBER SURROGATE RESULT UNITS BASIS DILUTION ANALYST ANOTEpH

pHpH

pHpHPHpHpH

pH

pH

pHpHpH

pH

PHpHpH

PHpHpHpH

pH

pHpH

pHpHpH

pHpH

NANA

NANANA

NANANANA

NANA

NANA

NANANANA

NANANA

NANANANA

NANANANANA

FALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSE

6.25.96.1

7.36.55.66.7

7.06.2

6.0

5.96.15.7

6.67.47.2

5.86.76.4

7.96.7

6.97.86.4

7.16.4

6.96.06.6

pH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units WetpH Units Wet

10

1010101010

101010

1010102010

101010101010

1010101010101010

10

LMLMLM

LMLMLMLMLMLM

LMLMLMLM

LMLM

LMLMLMLM

LMLMLMLMLM

LMLMLMLMLM

JJ

J

JJ

JJ

J

JJ

J

JJ

J

JJ

J

JJ

JJ

J

JJ

JJ

JJ

J

Page 1

LNOTE Soil pH

QUALIFIEI DESCRIPTIONJ The identification of the analyte is acceptable; the reported value is an estimate.

Page 1

Field Rinse BlankSample Number JN3-SLS40-RB

SAMPDATA Rinse Blank

CLIENTSuperfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,Superfund,

US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5US EPA Region 5

PROJECTJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsvilleJacobsville

LABNAMEAlionAlionAlionAlionAlionAlionAlionAlionAlionAlionAlionAlionAlionAlionAlionAlionAlionAlion

- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract- ESAT Contract

SAMPLENAMEJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RBJN3-SLS40-RB

LABSAMPIDE51 0002-30E51 0002-30E51 0002-30E51 0002-30E51 0002-30E51 0002-30E51 0002-30E51 0002-30E51 0002-30E51 0002-30E51 0002-30E51 0002-30E51 0002-30E51 0002-30E510002-30E51 0002-30E51 0002-30E51 0002-30

MATRIXWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWater

SAMPDATE PREPDATE10/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/2005

10/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/200510/31/2005

ANADATE11/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/200511/2/2005

11/15/2005

BATCHEJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103EJ53103

METHODCODECd 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 (CP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Metals SF 4300 ICP (W)Pb 4300 ICP (W)Na ICP (W)

METHODNAMEEPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200.7EPA 200. 7EPA 200.7EPA 200.7EPA 200.7

PREPNAMEHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block DigestionHot Block Digestion

ANALYTECadmiumAluminumBariumBerylliumCalciumChromiumCobaltCopperIronMagnesiumManganeseNickelPotassiumSilverVanadiumZincLeadSodium

CASNUMBER7440-43-97429-90-57440-39-37440-41-77440-70-27440-47-37440-48-47440-50-87439-89-67439-95-47439-96-57440-02-27440-09-77440-22-47440-62-27440-66-67439-92-17440-23-5

SURROGATEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSEFALSE

RESULTU20313.6

U782UUU30489.2

8.3UUUU15.8

9.11060

DL RL0.4 2.028.0 1000.5 2.00.2 0.535.0 1002.0 6.00.3 1.01.8 6.04.0 20.07.0 30.00.2 1.00.6 2.0660 20001.0 4.01.2 10.010.0 30.03.0 20.056.0 400

UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

BASISNANANANANANANANANANANANANANANANANANA

DILUTION111111111111111111

ANALYSTMMMMMMMMMMMMMMMMMMMMMMMMMMMMMMMMMMMM

ANOTE

*

*

*

JJ, KK, *

Page 1

LNOTE Rinse Blank

QUALIFIER DESCRIPTION* The duplicate analysis precision is not within control limits. The reported value is estimated.< 5X One or both concentration values for the duplicate analysis audit were less than 5 times the MDL value AND the difference between the two values was less than the MDL. value. The duplicate audit is acceptable. No qualification made for this Q(J The identification of the analyte is acceptable; the reported value is an estimate.K The identification of the analyte is acceptable; the reported value may be biased high. The actual value is expected to be less than the reported value.

Page 1

Appendix C:

XRF Results (Unadjusted)For Sampling Event #3

X Y449986.578495 4203265.684900449056.214833 4203603.155130449334.625284 4203668.504530450326.695439 4203599.434530451606.115926 4202978.948020449103.186001 4204060.447250449251.322168 4204039.041790449615.162498 4204072.824810449615.799332 4204072.844920449164.942391 4204338.860270449693.368995 4203823.667570449429.559920 4203831.806340449169.937438 4203805.325540451274.745963 4200959.156640451698.800668 4201015.477450451026.260273 4201232.131960451198.756443 4201535.031700451482.827212 4201726.537970451218.484619 4200989.311350447507.041538 4204269.516800447102.595548 4204098.953640451386.080734 4202028.499880451685.294431 4202159.018960451685.637605 4202159.118650451797.563397 4202255.310500451430.133428 4202417.697820451062.976349 4205697.393620451967.476368 4202909.295080451856.618194 4202726.278530451032.301078 4202934.652130450988.603705 4205289.758840451687.628457 4205515.372050451238.474526 4201755.907290451288.865247 4201521.118950450743.562421 4202874.558980451069.042398 4202447.984770451177.256505 4202285.211930451156.321440 4201756.088500

PB_CONC292.3252.3578.9601.9233.0

1060.1395.4287.8261.6924.0358.3399.8395.2135.877.0

129.1374.2136.6135.2184.676.5

110.074.5BDL

153.1249.045.1

138.8134.0139.1159.257.3

307.0155.2482.0125.258.7

1020.0

PB_ERR UNITS48.7 ppm45.6 ppm55.4 ppm55.4 ppm42.3 ppm71.4 ppm48.8 ppm43.3 ppm43.5 ppm64.6 ppm50.1 ppm48.3 ppm46.0 ppm40.4 ppm38.3 ppm39.5 ppm51.3 ppm39.7 ppm37.0 ppm40.3 ppm36.0 ppm38.5 ppm35.9 ppmBDL ppm39.8 ppm44.5 ppm29.0 ppm34.2 ppm34.0 ppm33.4 ppm35.0 ppm28.6 ppm41.3 ppm36.0 ppm45.9 ppm34.5 ppm30.2 ppm65.6 ppm

DATE_ TIME DEV_MODEL10/18/2005 112150 XLp-70010/18/2005 115228 XLp-70010/18/2005 240939 XLp-70010/18/2005 243005 XLp-70010/18/2005 095636 XL-70010/18/2005 162807 XLp-70010/18/2005 164537 XLp-70010/18/2005 170753 XLp-70010/18/2005 171408 XLp-70010/18/2005 173624 XLp-70010/18/2005 144234 XLp-70010/18/2005 150115 XLp-70010/18/2005 151255 XLp-70010/26/2005 103316 XLp-70010/26/2005 105036 XLp-70010/26/2005 111355 XLp-70010/26/2005 113201 XLp-70010/26/2005 115121 XLp-70010/26/2005 095026 XLp-70010/26/2005 150243 XLp-70010/26/2005 152131 XLp-70010/26/2005 132737 XLp-70010/26/2005 134236 XLp-70010/26/2005 134429 XLp-70010/26/2005 140737 XLp-70010/26/2005 143032 XLp-70010/25/2005 104238 XL-70010/25/2005 110958 XL-70010/25/2005 112945 XL-70010/25/2005 115157 XL-70010/25/2005 094857 XL-70010/25/2005 100413 XL-70010/25/2005 165217 XL-70010/25/2005 171249 XL-70010/25/2005 142414 XL-70010/25/2005 144524 XL-70010/25/2005 151340 XL-70010/25/2005 153708 XL-700

LOC_DESCJN3-SXN-01JN3-SXN-30JN3-SXN-31JN3-SXN-33JN3-SXS-83JN3-SXN-37JN3-SXN-38JN3-SLN-39JN3-SLN-39JN3-SXN-11JN3-SLN-06JN3-SXN-05JN3-SXN-04JN3-SXS-495JN3-SXS-50JN3-SXS-115JN3-SXS-555JN3-SXS-23JN3-SXS-49JN3-SXW-100JN3-SXW-101JN3-SXS-675JN3-SXS-355JN3-SXS-355JN3-SXS-356JN3-SXS-785JN3-SXN-117JN3-SXS-84JN3-SXS-38JN3-SXS-82JN3-SXN-115JN3-SXN-116JN3-SXS-225JN3-SXN-56JN3-SXS-81JN3-SXS-78JN3-SXS-35JN3-SXS-22

LOC_ZONEEEEEEEEEDUPLICATEEEEEEEEEEEEEEEE-DUPLICATEEEEEEEEEEEEEEE

Page 1 of 5

X451156.321440451407.541013451085.391342450636.085703449833.287494451228.498422451228.498422451098.247435451518.930179451588.294937452082.255246452081.390950451317.218898450300.550620451040.321955448980.586095449124.790895450424.847744449117.679807448893.448149448760.856639449024.177717449343.605981449599.249147449199.630543448916.431997448429.219704448783.807970448369.310406448230.622029448437.466162448437.439822448559.403037448800.162335448801.775590450806.360938451302.556495450692.821612

Y PB_CONC PB_ERR4201756.0885004203803.2512804204087.0288504203972.4163404203795.1166404203885.3880004203885.3880004204567.8971404203912.3227004204229.5202704204168.5222904204166.8999904204377.8780704204082.9375004204422.6959104205243.9377704205546.6097204205001.1916804205841.2763304205833.6123704205834.3780404204939.8341504204991.5460404204945.2053304204822.0402804204809.9966504204797.4351704205043.1830504204600.6063804204761.7805204205427.5752204205428.0395604205578.6210704205556.2951904205557.5500004204069.6739404204083.0805504204335.364200

1080.0301.6223.6626.0

99.2332.4414.4

91.0271.8237.6

67.331.7

142.7170.7274.2162.2256.4398.8223.3105.0250.4589.9303.6277.0351.0

1203.8192.8386.3136.7299.4282.1303.6142.1BDL92.6

187.8220.2400.4

66.839.136.451.530.443.247.530.840.036.929.928.432.935.337.442.345.152.141.738.742.755.845.646.548.970.844.650.641.446.944.744.841.1BDL38.141.345.750.9

UNITSppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppmppm

DATE_10/25/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/24/200510/21/200510/21/200510/21/200510/21/200510/21/200510/21/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/20/200510/19/200510/19/200510/19/2005

TIME154550103712111205114647094043100753101337145153151546153818155902160514143356132445141227105429111503115456095659100922102816114727240134242222100757102517104001110215145202150843153727153942160704162058162324090553092253094318

DEV_MODEL LOC_DESCXL-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700

JN3-SXS-22JN3-SXN-08JN3-SXN-42JN3-SXN-40JN3-SXN-109JN3-SXN-07JN3-SXN-07JN3-SXN-111JN3-SXN-112JN3-SXN-113JN3-SXN-114JN3-SXN-114JN3-SXN-19JN3-SXN-110JN3-SXN-18JN3-SXN-107JN3-SXN-108JN3-SXN-60JN3-SXN-104JN3-SXN-105JN3-SXN-106JN3-SXN-55JN3-SXN-56JN3-SXN-57JN3-SXN-21JN3-SXN-100JN3-SXN-20JN3-SXN-54JN3-SXN-101JN3-SXN-102JN3-SXN-103JN3-SXN-103JN3-SXN-62JN3-SXN-63JN3-SXN-63JN3-SXN-41JN3-SXN-43JN3-SXN-17

LOC_ZONEDUPEEEEEDUPEEEEDUPEEEEEEEEEEEEEEEEEEEDUPLICATEEEDUPLICATEEEE

Page 2 of 5

X Y450409.714147 4204318.360060450195.166791 4204343.287150449392.700861 4204365.648810448699.061608 4204404.842610448547.010164 4204571.021560448786.261290 4204565.809410448785.972521 4204566.206960449416.644622 4204766.532320450804.478823 4204605.266030450429.586144 4204849.079320449969.833026 4204809.566960449417.202358 4204765.840930449780.826734 4204566.900860450061.777717 4204548.267890450315.423758 4204542.753680450574.967448 4204611.162810449320.179096 4204613.636810449065.150541 4204596.113240450215.149050 4201972.165060450579.373287 4201011.794040450794.523947 4201012.568770451014.374313 4200788.223610451012.195934 4200788.303220452142.815274 4200957.867820452211.755156 4201314.927240452519.736130 4201231.389250450485.990979 4201278.713620450832.177985 4201192.828090452593.658529 4201589.136650452158.719937 4202455.959650451906.485057 4201991.110720451598.945629 4202022.932620452508.328160 4201752.740950452507.709866 4201752.665020452762.511513 4201725.605270452036.761496 4200543.972820450772.385912 4202173.105090451641.647889 4202495.207190

PB^CONC259.8624.1388.6153.6187.0231.6186.1217.8211.8178.7371.2212.0348.0279.4213.8348.8276.4826.4

BDL120.080.3

170.0169.857.0

163.757.4

177.7538.1255.699.9

238.81017.5

78.769.3

156.5161.466.8

160.8

PB_ERR UNITS44.9 ppm56.9 ppm50.0 ppm41.2 ppm43.2 ppm43.7 ppm40.7 ppm44.8 ppm43.8 ppm38.7 ppm50.8 ppm42.8 ppm48.1 ppm42.6 ppm42.3 ppm46.2 ppm44.9 ppm65.0 ppmBDL ppm41.7 ppm34.7 ppm42.5 ppm41.9 ppm36.2 ppm41.1 ppm35.5 ppm42.7 ppm53.5 ppm47.1 ppm39.7 ppm45.5 ppm65.8 ppm33.6 ppm35.5 ppm43.6 ppm40.2 ppm37.2 ppm36.3 ppm

DATE_ TIME DEV_MODEL10/19/2005 100554 XLp-70010/19/2005 102320 XLp-70010/19/2005 104705 XLp-70010/19/2005 111352 XLp-70010/19/2005 113234 XLp-70010/19/2005 115118 XLp-70010/19/2005 115253 XLp-70010/19/2005 165235 XLp-70010/19/2005 153845 XLp-70010/19/2005 155820 XLp-70010/19/2005 161702 XLp-70010/19/2005 163950 XLp-70010/19/2005 141627 XLp-70010/19/2005 143614 XLp-70010/19/2005 145154 XLp-70010/19/2005 150441 XLp-70010/19/2005 135201 XLp-70010/19/2005 133510 XLp-70010/25/2005 094208 XLp-70010/25/2005 100433 XLp-70010/25/2005 102336 XLp-70010/25/2005 104315 XLp-70010/25/2005 104457 XLp-70010/25/2005 110847 XLp-70010/25/2005 112628 XLp-70010/25/2005 114807 XLp-70010/25/2005 170515 XLp-70010/25/2005 173048 XLp-70010/25/2005 162654 XLp-70010/25/2005 141010 XLp-70010/25/2005 142600 XLp-70010/25/2005 144416 XLp-70010/25/2005 152305 XLp-70010/25/2005 152506 XLp-70010/25/2005 154046 XLp-70010/24/2005 171024 XLp-70010/24/2005 100527 XLp-70010/24/2005 102431 XLp-700

LOC_DESCJN3-SXN-16JN3-SXN-15JN3-SXN-12JN3-SXN-09JN3-SXN-44JN3-SXN-45JN3-SXN-45JN3-SXN-22JN3-SXN-53JN3-SXN-26JN3-SXN-24JN3-SXN-22JN3-SXN-49JN3-SXN-50JN3-SLN-51JN3-SXN-52JN3-SXN-47JN3-SXN-46JN3-SXS-63JN3-SXS-47JN3-SXS-48JN3-SXS-04JN3-SXS-04JN3-SXS-51JN3-SXS-15JN3-SXS-16JN3-SXS-10JN3-SXS-1 1JN3-SXS-100JN3-SXS-80JN3-SXS-69JN3-SXS-68JN3-SXS-27JN3-SXS-27JN3-SXS-28JN3-SXS-42JN3-SXS-33JN3-SXS-79

LOG ZONEEEEEEEE-DUPDUPLICATEEEEEEEEEEEEEEEFDEEEEEEEEEEFDEEEE

Page 3 of 5

X Y451647.828091 4202648.878880451647.780361 4202648.977180450914.297857 4201432.685530450626.615367 4201476.940490450857.770894 4201765.234540451333.335635 4199990.375510450724.247232 4200751.578010452186.607038 4201496.215880451884.453686 4201505.121590451614.796989 4201518.378800450231.435526 4201752.199490450520.152465 4201717.002280450376.142933 4201067.529470450269.923312 4201241.577370449588.184472 4201043.677970451371.647129 4200442.080200450894.497665 4200473.858930451271.216999 4200716.160900451268.696814 4200715.892970451245.110822 4201214.488620450898.512216 4202391.314670450898.512216 4202391.314670451133.788017 4201971.915330450922.043994 4202006.148060450672.996758 4201999.976930450384.599233 4201954.712200449889.682863 4201948.410110450147.649610 4201483.225120451035.905147 4202193.389440450472.138326 4202175.810590450229.591574 4202162.904480449984.732226 4202238.846260449767.366523 4202268.917850452022.028278 4201761.782520451747.515076 4201758.470430452234.566294 4201734.382820450011.240122 4201724.439760451744.248672 4200738.923465

PB_CONC361.0356.1366.7276.4385.7

12.087.8

128.4255.4131.9275.0561.2105.081.540.361.255.645.647.1

163.5113.992.7

370.0397.8523.2415.2385.4191.6805.2261.2478.0199.3145.7171.1326.263.7

243.262.7

PB_ERR UNITS45.2 ppm45.6 ppm47.3 ppm44.7 ppm49.6 ppm27.9 ppm29.4 ppm29.7 ppm36.8 ppm30.4 ppm41.3 ppm50.2 ppm31.5 ppm35.7 ppm29.7 ppm30.4 ppm30.5 ppm30.1 ppm30.0 ppm32.8 ppm35.1 ppm33.6 ppm41.8 ppm44.4 ppm47.5 ppm45.0 ppm45.4 ppm36.2 ppm61.2 ppm39.8 ppm48.9 ppm39.1 ppm33.1 ppm35.6 ppm42.0 ppm32.0 ppm39.2 ppm29.5 ppm

DATE_ TIME DEV_MODEL10/24/2005 104419 XLp-70010/24/2005 104557 XLp-70010/24/2005 142049 XLp-70010/24/2005 144540 XLp-70010/24/2005 132832 XLp-70010/21/2005 111751 XL-70010/21/2005 115329 XL-70010/21/2005 100323 XL-70010/21/2005 102707 XL-70010/21/2005 104830 XL-70010/20/2005 102049 XL-70010/20/2005 104541 XL-70010/20/2005 112102 XL-70010/20/2005 115553 XL-70010/20/2005 242216 XL-70010/20/2005 160351 XL-70010/20/2005 162811 XL-70010/20/2005 153032 XL-70010/20/2005 153618 XL-70010/20/2005 150524 XL-70010/19/2005 111951 XL-70010/19/2005 171026 XL-70010/19/2005 100201 XL-70010/19/2005 105750 XL-70010/19/2005 134256 XL-70010/19/2005 143112 XL-70010/19/2005 161048 XL-70010/19/2005 164918 XL-70010/19/2005 102618 XL-70010/19/2005 140645 XL-70010/19/2005 144959 XL-70010/19/2005 150735 XL-70010/19/2005 152612 XL-70010/19/2005 092050 XL-70010/19/2005 094047 XL-70010/19/2005 085314 XL-70010/19/2005 163150 XL-70010/18/2005 171024 XL-700

LOC_DESCJN3-SXS-37JN3-SXS-37JN3-SXS-55JN3-SXS-54JN3-SXS-21JN3-SXS-39JN3-SXS-03JN3-SXS-59JN3-SXS-58JN3-SXS-57JN3-SXS-19JN3-SXS-20JN3-SXS-46JN3-SXS-09JN3-SXS-44JN3-SXS-41JN3-SXS-40JN3-SXS-05JN3-SXS-05JN3-SXS-12JN3-SXS-77JN3-SXS-77JN3-SXS-67JN3-SXS-66JN3-SXS-65JN3-SXS-64JN3-SXS-62JN3-SXS-53JN3-SXS-34JN3-SXS-32JN3-SXS-31JN3-SXS-30JN3-SXS-29JN3-SXS-25JN3-SXS-24JN3-SXS-26JN3-SXS-18JN3-SXS-07

LOC_ZONEEFDEEEEEEEEEEEEEEEEDUPEEDUPEEEEEEEEEEEEEEEE

Page 4 of 5

X451754.217833452023.039485452831.365343452711.972655452712.875208452440.334902452837.199359452113.232585452525.629971452401.725954

Y PB_CONC PB_ERR4201238.757220 97.2 33.74201182.870980 BDL N/A4201471.0665004201003.1543804201001.7344704201045.0999204200125.5146904201964.2706904202095.7009004201505.735520

53.844.955.2

124.755.1

109.4101.4115.7

31.30,31.35,32.33,32,32.

2,6.3,2.7,1,9.9

UNITSppmppmppmppmppmppmppmppmppmppm

DATE_10/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/200510/18/2005

TIME165240171141141338144814145423152117155122111508114140240853

DEV_MODEL LOC_DESCXL-700 JN3-SXS-13XL-700 JN3-SXS-14XL-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700

JN3-SXS-61JN3-SXS-52JN3-SXS-52JN3-SXS-06JN3-SXS-02JN3-SXS-70JN3-SXS-71JN3-SXS-60

LOC_ZONEEEEEDUPEEEEE

*BDL: Below Detection Limits

Page 5 of 5

Appendix D:

Tables of Adjusted Lead Concentration Values(Using Derived Correlation) for

Sampling Event #3

OCT05_ADJUST_PB

IDJN3-SXS-61JN3-SXN-114JN3-SXS-355JN3-SXS-50JN3-SXS-16JN3-SXS-47JN3-SXS-46JN3-SXS-28JN3-SXS-38JN3-SXS-59JN3-SXS-79JN3-SLN-51JN3-SXN-22JN3-SXS-25JN3-SLN-39JN3-SXS-12JN3-SXN-106JN3-SXN-16JN3-SXN-45JN3-SXS-55JN3-SXN-55JN3-SLN-06JN3-SXN-103JN3-SXN-07JN3-SXN-18JN3-SXS-65JN3-SXS-22JN3-SXS-63JN3-SXS-39JN3-SXS-14JN3-SXS-44JN3-SXN-117JN3-SXS-05JN3-SXS-52JN3-SXS-02JN3-SXS-40JN3-SXS-51JN3-SXN-116JN3-SXS-35JN3-SXS-41JN3-SXS-07JN3-SXS-26JN3-SXS-33JN3-SXS-27JN3-SXW-101JN3-SXS-48JN3-SXS-09JN3-SXS-03JN3-SXN-111JN3-SXN-63JN3-SXS-13JN3-SXN-109JN3-SXS-80JN3-SXS-71JN3-SXS-77JN3-SXN-105JN3-SXS-70JN3-SXS-675JN3-SXS-60JN3-SXS-06JN3-SXS-78JN3-SXS-115

452831.36534299800452082.25524600000451685.29443100000451698.80066800000452519.73612999800450579.37328699900450376.14293300000452762.51151300000451856.61819399800452186.60703800000451641.64788900000450315.42375800000449417.20235799800452022.02827800000449615.16249800000451245.11082200000448760.85663900000450409.71414699900448786.26128999900450914.29785700000449024.17771700000449693.36899500000448437.46616200000451228.49842199800451040.32195499900450672.99675799900451156.32144000000450215.14905000000451333.33563500000452023.03948500000449588.18447199900451062.97634900000451271.21699900000452711.97265499900452837.19935900000450894.49766499800452142.81527399900451687.62845700000451177.25650500000451371.64712899900451744.24867200000452234.56629400000450772.38591200000452508.32815999800447102.59554800000450794.52394699800450269.92331200000450724.24723199900451098.24743500000448800.16233500000451754.21783300000449833.28749399900452158.71993700000452525.62997100000450898.51221600000448893.44814900000452113.23258499900451386.08073400000452401.72595400000452440.33490199800451069.04239800000451026.26027299900

4201471.066499990004204168.522289990004202159.018960000004201015.477450000004201231.389250000004201011.794040000004201067.529470000004201725.605270000004202726.278529990004201496.215880000004202495.207190000004204542.753680000004204765.840929980004201761.782519980004204072.824810000004201214.488620000004205834.378039980004204318.360059980004204565.809410000004201432.685530000004204939.834149990004203823.667569990004205427.575220000004203885.388000000004204422.695910000004201999.976929980004201756.088499990004201972.165059990004199990.375509990004201182.870980000004201043.677969990004205697.393620000004200716.160899990004201003.154380000004200125.514689990004200473.858930000004200957.867820000004205515.372050000004202285.211930000004200442.080199990004200738.923465000004201734.382819980004202173.105089990004201752.740949990004204098.953640000004201012.568769980004201241.577370000004200751.578010000004204567.897140000004205556.295190000004201238.757220000004203795.116639990004202455.959649990004202095.700899990004202391.314670000004205833.612370000004201964.270689990004202028.499880000004201505.735519990004201045.099919980004202447.984770000004201232.13195998000

XRF_PB LAB_PB ADJUST COUNT53.8049.5074.5077.0057.40

120.00105.00156.50134.00128.40160.80213.80214.90171.10274.70163.50250.40259.80208.85366.70589.90358.30292.85373.40274.20523.20

1050.001.00

12.001.00

40.3045.1046.3550.0555.1055.6057.0057.3058.7061.2062.7063.7066.8074.0076.5080.3081.5087.8091.0092.6097.2099.2099.90

101.40103.30105.00109.40110.00115.70124.70125.20129.10

39.0074.0074.00

100.00110.00130.00140.00170.00190.00220.00220.00260.00270.00270.00320.00340.00360.00360.00420.00430.00480.00530.00670.00710.00840.00960.00

2000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.00

39.0074.0074.00

100.00110.00130.00140.00170.00190.00220.00220.00260.00270.00270.00320.00340.00360.00360.00420.00430.00480.00530.00670.00710.00840.00960.00

2000.001.00

12.001.00

40.3045.1046.3550.0555.1055.6057.0057.3058.7061.2062.7063.7066.8074.0076.5081.1383.4395.50

101.63104.69113.50117.33118.67121.54125.18128.44136.86138.01148.93166.16167,12174.59

1.02.02.01.01.01.01.01.01.01.01.01.02.01.02.01.01.01.02.01.01.01.02.02.01.01.02.01.01.01.01.01.02.02.01.01.01.01.01.01.01.01.01.02.01.01.01.01.01.02.01.01.01.01.02.01.01.01.01.01.01.01.0

PB_ERR UNITS DEVICE31.20000000000 ppm29.90000000000 ppm35.90000000000 ppm38.30000000000 ppm35.50000000000 ppm41.70000000000 ppm31.50000000000 ppm43.60000000000 ppm34.00000000000 ppm29.70000000000 ppm36.30000000000 ppm42.30000000000 ppm44.80000000000 ppm35.60000000000 ppm43.30000000000 ppm32.80000000000 ppm42.70000000000 ppm44.90000000000 ppm43.70000000000 ppm47.30000000000 ppm55.80000000000 ppm50.10000000000 ppm44.70000000000 ppm43.20000000000 ppm37.40000000000 ppm47.50000000000 ppm65.60000000000 ppm

-11 11. 10000000000 ppm27.90000000000 ppm

0.00000000000 ppm29.70000000000 ppm29.00000000000 ppm30.10000000000 ppm30.60000000000 ppm32.70000000000 ppm30.50000000000 ppm36.20000000000 ppm28.60000000000 ppm30.20000000000 ppm30.40000000000 ppm29.50000000000 ppm32.00000000000 ppm37.20000000000 ppm33.60000000000 ppm36.00000000000 ppm34.70000000000 ppm35.70000000000 ppm29.40000000000 ppm30.80000000000 ppm

-1111.10000000000 ppm33.70000000000 ppm30.40000000000 ppm39.70000000000 ppm32.90000000000 ppm35.10000000000 ppm38.70000000000 ppm33.10000000000 ppm38.50000000000 ppm32.90000000000 ppm35.20000000000 ppm34.50000000000 ppm39.50000000000 ppm

XRF XL-700XRF XL-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XL-700XRF XLp-700XRF XL-700XRF XL-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XL-700XRF XLp-700XRF XL-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XL-700XRF XL-700XRF XL-700XRF XL-700XRF XLp-700XRF XL-700XRF XL-700XRF XL-700XRF XL-700XRF XL-700XRF XL-700XRF XL-700XRF XL-700XRF XLp-700XRF XL-700XRF XL-700XRF XL-700XRF XL-700XRF XL-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XL-700XRF XL-700XRF XL-700XRF XLp-700XRF XL-700XRF XL-700XRF XLp-700XRF XL-700XRF XL-700XRF XLp-700XRF XL-700XRF XLp-700XRF XL-700XRF XL-700XRF XL-700XRF XLp-700

DEC_DEG_X-87.53695386670-87.54563770000-87.55004158330-87.54980451670-87.54049105000-87.56253205000-87.56486873330-87.53774603330-87.54812816670-87.54427193330-87.55055956670-87.56578693330-87.57605075000-87.54618381670-87.57374040000-87.55498308330-87.58359273330-87.56470245000-87.58320841670-87.55876483330-87.58054595000-87.57294066670-87.58717710000-87.55534123330-87.55753688330-87.56155345000-87.55604001670-87.56675250000-87.55387893330-87.54613103330-87.57383811670-87.55739763330-87.55464705000-87.53827575000-87.53679418330-87.55892528330-87.54476665000-87.55023968330-87.55585936670-87.55349178330-87.54927400000-87.54375913330-87.56043396670-87.54063445000-87.60234398330-87.56009488330-87.56585395000-87.56091641670-87.55699253330-87.58312791670-87.54919468330-87.57123736670-87.54466371670-87.54049956670-87.55901328330-87.58209198330-87.54515936670-87.55342551670-87.54184195000-87.54137175000-87.55707586670-87.55742856670

DEC_DEG_Y DATE_ TIME37.95961713330 10/18/2005 14133837.98390123330 10/24/2005 15590237.96576561670 10/26/2005 13423637.95545616670 10/26/2005 10503637.9574342833010/25/2005 11480737.95534293330 10/25/2005 10043337.9558576333010/20/2005 11210237.96191555000 10/25/2005 15404637.9708858500010/25/2005 11294537.95981471670 10/21/2005 10032337.96877348330 10/24/2005 10243137.98717263330 10/19/2005 14515437.98913450000 10/19/2005 16523537.96220010000 10/19/2005 09205037.98290010000 10/18/2005 17075337.95723146670 10/20/2005 15052437.99873278330 10/21/2005 10281637.98515288330 10/19/2005 10055437.9872926333010/19/2005 11511837.95916910000 10/24/2005 14204937.99067426670 10/20/2005 11472737.98062640000 10/18/2005 14423437.99504048330 10/20/2005 15372737.98130631670 10/24/2005 10075337.98612930000 10/24/2005 14122737.96427533330 10/19/2005 13425637.96209983330 10/25/2005 15370837.96401423330 10/25/2005 09420837.9461241833010/21/2005 11175137.9569833167010/18/2005 17114137.95559601670 10/20/2005 24221637.99725378330 10/25/2005 10423837.95274738330 10/20/2005 15303237.95539795000 10/18/2005 14481437.9474911833010/18/2005 15512237.9505438833010/20/2005 16281137.9549548500010/25/2005 11084737.99601218330 10/25/2005 10041337.96690996670 10/25/2005 15134037.95026741670 10/20/2005 16035137.95296800000 10/18/2005 17102437.96196373330 10/19/2005 08531437.96584220000 10/24/2005 10052737.96214670000 10/25/2005 15230537.98299761670 10/26/2005 15213137.95537165000 10/25/2005 10233637.9573960833010/20/2005 11555337.9530633000010/21/2005 11532937.98736385000 10/24/2005 14515337.99624355000 10/20/2005 16205837.95747188330 10/18/2005 16524037.98040038330 10/24/2005 09404337.96846545000 10/25/2005 14101037.96522736670 10/18/2005 11414037.9678129000010/19/2005 11195137.99873550000 10/21/2005 10092237.9640334333010/18/2005 11150837.96456678330 10/26/2005 13273737.95991271670 10/18/2005 24085337.9557596000010/18/2005 15211737.96833368330 10/25/2005 14452437.9573911333010/26/2005 111355

PDOP GPS_ELEV GPS_DEVICE DEV_MAN DEV_MODEL LOC_ZONE2.10000000000 121.93000000000 NMEA 843.90000000000 122.82000000000 NMEA 842.40000000000 122.02000000000 NMEA 842.50000000000 118.42000000000 NMEA 842.60000000000 120.21000000000 NMEA 843.70000000000 118.24000000000 NMEA 842.80000000000 119.46000000000 NMEA 843.30000000000 118.86000000000 NMEA 841.80000000000 122.03000000000 NMEA 845.80000000000 117.98000000000 NMEA 842.20000000000 121.39000000000 NMEA 842.30000000000 121.55000000000 NMEA 845.50000000000 121.09000000000 NMEA 842.60000000000 119.60000000000 NMEA 841.90000000000 124.99000000000 NMEA 843.70000000000 118.24000000000 NMEA 842.30000000000 119.37000000000 NMEA 841.70000000000 122.72000000000 NMEA 841 .80000000000 1 21 .72000000000 NMEA 842.30000000000 119.84000000000 NMEA 841.80000000000 124.46000000000 NMEA 843.60000000000 120.65000000000 NMEA 842.00000000000 121.96000000000 NMEA 842.90000000000 121.07000000000 NMEA 842.40000000000 124.84000000000 NMEA 842.70000000000 119.94000000000 NMEA 848.30000000000 125.23000000000 NMEA 845.90000000000 117.73000000000 NMEA 843.40000000000 117.61000000000 NMEA 843.40000000000 120.91000000000 NMEA 843.10000000000 120.82000000000 NMEA 842.40000000000 121.09000000000 NMEA 846.70000000000 124.36000000000 NMEA 842.10000000000 117.96000000000 NMEA 842.20000000000 119.73000000000 NMEA 844.20000000000 119.20000000000 NMEA 843.10000000000 117.48000000000 NMEA 842.00000000000 121.89000000000 NMEA 842.00000000000 120.74000000000 NMEA 841 .70000000000 1 17.70000000000 NMEA 843.60000000000 184.41000000000 NMEA 842.30000000000 119.72000000000 NMEA 842.90000000000 119.72000000000 NMEA 842.10000000000 119.26000000000 NMEA 841 .70000000000 1 21 .48000000000 NMEA 842.20000000000 118.96000000000 NMEA 842.30000000000 118.58000000000 NMEA 842.00000000000 117.54000000000 NMEA 84

29.00000000000 121.67000000000 NMEA 842.90000000000 118.25000000000 NMEA 844.30000000000 122.56000000000 NMEA 846.90000000000 123.67000000000 NMEA 842.30000000000 119.47000000000 NMEA 842.40000000000 120.91000000000 NMEA 842.40000000000 120.49000000000 NMEA 842.00000000000 120.45000000000 NMEA 842.40000000000 120.14000000000 NMEA 842.90000000000 120.35000000000 NMEA 843.90000000000 119.79000000000 NMEA 844.10000000000 117.50000000000 NMEA 841.50000000000 118.33000000000 NMEA 841.90000000000 135.65000000000 NMEA 84

NitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNiton

XL-700XL-700XLp-700XLp-700XLp-700XLp-700XL-700XLp-700XL-700XL-700XLp-700XLp-700XLp-700XL-700XLp-700XL-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XL-700XL-700XL-700XL-700XLp-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700XL-700XLp-700XL-700XL-700XL-700XL-700XL-700XLp-700XLp-700XLp-700XLp-700XL-700XL-700XL-700XLp-700XL-700XL-700XLp-700XL-700XL-700XLp-700XL-700XLp-700XL-700XL-700XL-700XLp-700

EEEEEEEEEEEEDUPLICATEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEEE

Page 1 of 3

OCT05_ADJUST_PB

IDJN3-SXS-57JN3-SXS-49JN3-SXS^95JN3-SXS-23JN3-SXN-101JN3-SXS-84JN3-SXS-82JN3-SXN-62JN3-SXN-19JN3-SXS-29JN3-SXS-356JN3-SXN-09JN3-SXN-56JN3-SXN-115JN3-SXS-42JN3-SXN-107JN3-SXS-15JN3-SXS-04JN3-SXN-110JN3-SXS-10JN3-SXN-26JN3-SXW-100JN3-SXN-44JN3-SXN-41JN3-SXS-53JN3-SXN-20JN3-SXS-30JN3-SXN-53JN3-SXN-43JN3-SXN-104JN3-SXN-42JN3-SXS-83JN3-SXN-113JN3-SXS-69JN3-SXS-18JN3-SXS-785JN3-SXN-30JN3-SXS-58JN3-SXS-100JN3-SXN-108JN3-SXS-32JN3-SXN-112JN3-SXS-19JN3-SXN-47JN3-SXS-54JN3-SXN-57JN3-SXN-50JN3-SXN-01JN3-SXN-102JN3-SXN-08JN3-SXN-56JN3-SXS-225JN3-SXS-24JN3-SXN-49JN3-SXN-52JN3-SXN-21JN3-SXS-37JN3-SXS-67JN3-SXN-24JN3-SXS-555JN3-SXS-62JN3-SXS-21

X451614.79698899900451218.48461900000451274.74596299900451482.82721199800448369.31040600000451967.47636799800451032.30107799900448559.40303699800451317.21889800000449767.36652300000451797.56339700000448699.06160800000451288.86524700000450988.60370500000452036.76149624900448980.58609499800452211.75515600000451014.37431300000450300.55061999900450485.99097899900450429.58614400000447507.04153799900448547.01016399800450806.36093800000450147.64961000000448429.21970399900449984.73222599900450804.47882299800451302.55649500000449117.67980699800451085.39134199900451606.11592600000451588.29493700000451906.48505700000450011.24012199900451430.13342799800449056.21483299800451884.45368600000452593.65852900000449124.79089499800450472.13832600000451518.93017900000450231.43552599900449320.17909599800450626.61536699900449599.24914700000450061.77771699900449986.57849500000448230.62202900000451407.54101300000449343.60598100000451238.47452599800451747.51507600000449780.82673400000450574.96744799800449199.63054300000451647.82809099800451133.78801700000449969.83302600000451198.75644299900449889.68286300000450857.77089400000

4201518.378800000004200989.311350000004200959.156639990004201726.537969980004204600.606379980004202909.295079990004202934.652130000004205578.621070000004204377.878069990004202268.917849980004202255.310499990004204404.842609990004201521.118950000004205289.758840000004200543.972819980004205243.937769990004201314.927240000004200788.223609990004204082.937500000004201278.713619990004204849.079319990004204269.516800000004204571.021560000004204069.673940000004201483.225119990004204797.435170000004202238.846260000004204605.266029990004204083.080550000004205841.276329980004204087.028850000004202978.948020000004204229.520270000004201991.110720000004201724.439760000004202417.697820000004203603.155129980004201505.121589990004201589.136649990004205546.609720000004202175.810589980004203912.322700000004201752.199489990004204613.636810000004201476.940489980004204945.205330000004204548.267889980004203265.684899990004204761.780519990004203803.251280000004204991.546040000004201755.907289990004201758.470429990004204566.900860000004204611.162809990004204822.040280000004202648.878879990004201971.915330000004204809.566960000004201535.031700000004201948.410109990004201765.23453999000

XRF_PB LAB^PB ADJUST COUNT PB.131.90135.20135.80136.60136.70138.80139.10142.10142.70145.70153.10153.60155.20159.20161.40162.20163.70169.90170.70177.70178.70184.60187.00187.80191.60192.80199.30211.80220.20223.30223.60233.00237.60238.80243.20249.00252.30255.40255.60256.40261.20271.80275.00276.40276.40277.00279.40292.30299.40301 .60303.60307.00326.20348.00348.80351 .00358.55370.00371.20374.20385.40385.70

0.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.00

179.95186.27187.42188.95189.14193.16193.74199.48200.63206.38220.55221.50224.57232.23236.44237.97240.85252.72254.25267.66269.57280.87285.47287.00294.27296.57309.02332.96349.04354.98355.55373.56382.36384.66393.09404.20410.51416.45416.83418.37427.56447.86453.99456.67456.67457.82462.41487.11500.71504.92508.75515.27552.03593.78595.31599.53613.98635.91638.21643.95665,40665.98

1.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.02.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.02.01.01.01.01.01.0

_ERR UNITS30.40000000000 ppm37.00000000000 ppm40.40000000000 ppm39.70000000000 ppm41.40000000000 ppm34.20000000000 ppm33.40000000000 ppm41.10000000000 ppm32.90000000000 ppm33.10000000000 ppm39.80000000000 ppm41.20000000000 ppm36.00000000000 ppm35.00000000000 ppm40.20000000000 ppm42.30000000000 ppm41.10000000000 ppm42.50000000000 ppm35.30000000000 ppm42.70000000000 ppm38.70000000000 ppm40.30000000000 ppm43.20000000000 ppm41.30000000000 ppm36.20000000000 ppm44.60000000000 ppm39.10000000000 ppm43.80000000000 ppm45.70000000000 ppm41.70000000000 ppm36.40000000000 ppm42.30000000000 ppm36.90000000000 ppm45.50000000000 ppm39.20000000000 ppm44.50000000000 ppm45.60000000000 ppm36.80000000000 ppm47.10000000000 ppm45.10000000000 ppm39.80000000000 ppm40.00000000000 ppm41.30000000000 ppm44.90000000000 ppm44.70000000000 ppm46.50000000000 ppm42.60000000000 ppm48.70000000000 ppm46.90000000000 ppm39.10000000000 ppm45.60000000000 ppm41.30000000000 ppm42.00000000000 ppm48.10000000000 ppm46.20000000000 ppm48.90000000000 ppm45.20000000000 ppm41.80000000000 ppm50.80000000000 ppm51.30000000000 ppm45.40000000000 ppm49.60000000000 ppm

DEVICEXRF XL-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XL-700XRF XL-700XRF XLp-700XRF XL-700XRF XL-700XRF XLp-700XRF XLp-700XRF XL-700XRF XL-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XL-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XL-700XRF XLp-700XRF XL-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XL-700XRF XL-700XRF XL-700XRF XLp-700XRF XL-700XRF XLp-700XRF XLp-700XRF XL-700XRF XLp-700XRF XLp-700XRF XL-700XRF XL-700XRF XL-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XL-700XRF XLp-700XRF XL-700XRF XL-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XLp-700XRF XL-700XRF XLp-700XRF XLp-700XRF XL-700XRF XLp-700

DEC_DEG_X-87.55080783330-87.55527930000-87.55463400000-87.55231180000-87.58796241670-87.54688098330-87.55742361670-87.58586425000-87.55438615000-87.57188255000-87.54875746670-87.58421016670-87.55451900000-87.55822581670-87.62010000000-87.58105775000-87.54398720000-87.55758065000-87.56593838330-87.56361713330-87.56450168330-87.59775781670-87.58596386670-87.56018410000-87.56749815000-87.58728753330-87.56940386670-87.56023991670-87.55452985000-87.57955256670-87.55697231670-87.55100470000-87.55125303330-87.54750606670-87.56906855000-87.55296080000-87.58006981670-87.54773593330-87.53967406670-87.57942868330-87.56385250000-87.55204095000-87.56656138330-87.57713163330-87.56203588330-87.57398980000-87.56868843330-87.56946205000-87.58948996670-87.55331245000-87.57689256670-87.55509890000-87.54930498330-87.57186185000-87.56285336670-87.57851905000-87.55051061670-87.55630600000-87.56973890000-87.55551825000-87.57046703330-87.55945475000

DEC_DEG_Y37.9599942333037.9552049167037.9549253833037.9618552833037.9875783000037.9725537500037.9725997833037.9964274667037.9857108167037.9666490833037.9666281500037.9858694500037.9599833000037.9939322333041.8788000000037.9934075167037.9581795000037.9533650000037.9830240667037.9577953167037.9899450667037.9845508500037.9872954667037.9829283333037.9595891333037,9893660167037.9663911000037.9877610000037.9830601833037.9987929333037.9830917167037.9731427500037.9843608667037.9642538000037.9617553000037.9680752167037.9786313833037.9598892500037.9606714000037.9961398333037.9658514333037.9815292333037.9620229167037.9877387167037.9595702500037.9907610500037.9871987167037.9756726333037.9890630667037.9805663833037.9911664000037.9621058000037.9621558833037.9873579000037.9878142333037.9896181833037.9701784500037.9640472167037.9895648667037.9601114500037.9637674167037.96215658330

DATE_10/21/200510/26/200510/26/200510/26/200510/20/200510/25/200510/25/200510/20/200510/24/200510/19/200510/26/200510/19/200510/25/200510/25/200510/24/200510/21/200510/25/200510/25/200510/24/200510/25/200510/19/200510/26/200510/19/200510/19/200510/19/200510/20/200510/19/200510/19/200510/19/200510/21/200510/24/200510/18/200510/24/200510/25/200510/19/200510/26/200510/18/200510/21/200510/25/200510/21/200510/19/200510/24/200510/20/200510/19/200510/24/200510/20/200510/19/200510/18/200510/20/200510/24/200510/20/200510/25/200510/19/200510/19/200510/19/200510/20/200510/24/200510/19/200510/19/200510/26/200510/19/200510/24/2005

TIME PDOP GPS ELEV104830095026103316115121145202110958115157160704143356152612140737111352171249094857171024105429112628104315132445170515155820150243113234090553164918104001150735153845092253095659111205095636153818142600163150143032115228102707162654111503140645151546102049135201144540242222143614112150150843103712240134165217094047141627150441100757104419100201161702113201161048132832

2.300000000001 .900000000004.300000000002.800000000002.500000000002.100000000000.000000000002.100000000003.600000000005.100000000003.600000000002.400000000002.700000000005.000000000003.600000000002.400000000002.400000000002.400000000002.400000000002.500000000001.600000000001 .900000000003.900000000002.200000000004.300000000002.400000000004.500000000002.100000000001.800000000007.500000000001 .900000000007.800000000002.400000000003.300000000002.500000000003.700000000002.400000000002.000000000004.200000000002.300000000002.800000000002.200000000004.900000000002.400000000002.800000000003.100000000000.000000000002.300000000008.900000000002.300000000002.500000000003.100000000002.600000000002.200000000003.500000000003.200000000004.200000000006.700000000002.100000000002.600000000002.100000000002.60000000000

119.33000000000119.05000000000118.47000000000120.10000000000120.52000000000120.95000000000121.22000000000120.33000000000122.52000000000119.97000000000119.35000000000122.17000000000119.49000000000123.56000000000184.41000000000120.38000000000120.95000000000117.74000000000123.12000000000123.82000000000125.32000000000120.70000000000119.95000000000122.52000000000120.34000000000121.19000000000120.31000000000122.58000000000120.71000000000121.06000000000122.93000000000118.48000000000131.23000000000119.94000000000122.67000000000122.38000000000123.63000000000119.56000000000120.93000000000121.02000000000119.81000000000121.08000000000121.38000000000124.11000000000121.01000000000124.69000000000121.10000000000122.85000000000115.65000000000121.37000000000122.20000000000121.55000000000119.05000000000121.06000000000122.43000000000122.16000000000119.49000000000121.95000000000125.24000000000120.35000000000123.18000000000121.69000000000

GPS.DEVICE DEV_MAN DEV_MODEL LOC_ZONENMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 64NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84

NitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNiton

XL-700XLp-700XLp-700XLp-700XLp-700XL-700XL-700XLp-700XL-700XL-700XLp-700XLp-700XL-700XL-700XLp-700XLp-700XLp-700XLp-700XL-700XLp-700XLp-700XLp-700XLp-700XLp-700XL-700XLp-700XL-700XLp-700XLp-700XLp-700XL-700XL-700XL-700XLp-700XL-700XLp-700XLp-700XL-700XLp-700XLp-700XL-700XL-700XL-700XLp-700XLp-700XLp-700XLp-700XLp-700XLp-700XL-700XLp-700XL-700XL-700XLp-700XLp-700XLp-700XLp-700XL-700XLp-700XLp-700XL-700XLp-700

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OCT05_ADJUST_PB

IDJN3-SXN-54JN3-SXN-12JN3-SXN-04JN3-SXN-38JN3-SXS-66JN3-SXN-60JN3-SXN-05JN3-SXN-17JN3-SXS-64JN3-SXS-31JN3-SXS-81JN3-SXS-11JN3-SXS-20JN3-SXN-31JN3-SXN-33JN3-SXN-15JN3-SXN-40JN3-SXS-34JN3-SXN-46JN3-SXN-11JN3-SXS-68JN3-SXN-37JN3-SXN-100

448783.80797000000449392.70086099900449169.93743799900449251.32216799800450922.04399400000450424.84774400000449429.55992000000450692.82161200000450384.59923300000450229.59157400000450743.56242099800450832.17798500000450520.15246499900449334.62528400000450326.69543899800450195.16679100000450636.08570300000451035.90514699800449065.15054100000449164.94239099900451598.94562900000449103.18600099900448916.43199700000

4205043.183050000004204365.648810000004203805.325539990004204039.041790000004202006.148059990004205001.191680000004203831.806339990004204335.364199990004201954.712200000004202162.904480000004202874.558980000004201192.828090000004201717.002279990004203668.504529990004203599.434530000004204343.287150000004203972.416340000004202193.389440000004204596.113239980004204338.860270000004202022.932620000004204060.447250000004204809.99665000000

XRF_PB LAB_PB ADJUST COUNT PB_ERR UNITS DEVICE DEC_DEG_X DEC_DEG_Y DATE_ TIME PDOP386.30388.60395.20395.40397.80398.80399.80400.40415.20478.00482.00538.10561.20578.90601.90624.10626.00805.20826.40924.00

1017.501060.101203.80

0.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.000.00

667.12671.53684.17684.55689.15691 .06692.98694.13722.47842.73850.39957.82

1002.061035.951080.001122.511126.151469.321509.921696.821875.871957.452232.64

1.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.01.0

50.60000000000 ppm50.00000000000 ppm46.00000000000 ppm48.80000000000 ppm44.40000000000 ppm52.10000000000 ppm48.30000000000 ppm50.90000000000 ppm45.00000000000 ppm48.90000000000 ppm45.90000000000 ppm53.50000000000 ppm50.20000000000 ppm55.40000000000 ppm55.40000000000 ppm56.90000000000 ppm51.50000000000 ppm61.20000000000 ppm65.00000000000 ppm64.60000000000 ppm65.80000000000 ppm71.40000000000 ppm70.80000000000 ppm

XRFXLp-700 -87.58330716670 37.9915947500010/20/2005 110215XRFXLp-700 -87.57630875000 37.9855580667010/19/2005 104705XRFXLp-700 -87.57879103330 37.9804626167010/18/2005 151255XRFXLp-700 -87.57790385000 37.9825876667010/18/2005 164537XRFXL-700 -87.55871836670 37.9643443000010/19/2005 105750XRFXLp-700 -87.56464163330 37.9912926500010/21/2005 115456XRFXLp-700 -87.57581086670 37.9807213000010/18/2005 150115XRFXLp-700 -87.56151651670 37.9853307000010/19/2005 094318XRFXL-700 -87.56483396670 37.9638514500010/19/2005 143112XRFXL-700 -87.56661276670 37.9657194167010/19/2005 144959XRFXL-700 -87.56080208330 37.9721127500010/25/2005 142414XRFXLp-700 -87.55967495000 37.9570159333010/25/2005 173048XRFXL-700 -87.56327748330 37.9617124500010/20/2005 104541XRFXLp-700 -87.57691251670 37.9792482667010/18/2005 240939XRFXLp-700 -87.56560341670 37.9786821500010/18/2005 243005XRFXLp-700 -87.56715683330 37.9853774500010/19/2005 102320XRFXL-700 -87.56211936670 37.9820300333010/24/2005 114647XRFXL-700 -87.55743545000 37.9660378500010/19/2005 102618XRFXLp-700 -87.58002848330 37.9875811833010/19/2005 133510XRFXLp-700 -87.57888758330 37.9852650667010/18/2005 173624XRFXLp-700 -87.55099543330 37.9645553667010/25/2005 144416XRFXLp-700 -87.57955031670 37.9827590833010/18/2005 162807XRFXLp-700 -87.58178273330 37.9895163167010/20/2005 102517

2.700000000002.400000000002.500000000001 .800000000000.000000000001.900000000001 .900000000006.800000000002.200000000002.000000000002.100000000002.300000000002.500000000001 .700000000003.100000000001 .900000000003.100000000002.900000000002.900000000002.300000000005.600000000001 .800000000003.00000000000

GPS_ELEV121.31000000000122.39000000000120.60000000000126.04000000000120.99000000000126.72000000000123.08000000000117.39000000000121.81000000000120.32000000000120.04000000000121.65000000000122.48000000000125.20000000000125.04000000000122.85000000000123.72000000000120.80000000000121.30000000000124.14000000000112.06000000000124.93000000000123.38000000000

GPS_DEVICE DEV_MAN DEV_MODEL L(NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84NMEA 84

NitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNitonNiton

XLp-700XLp-700XLp-700XLp-700XL-700XLp-700XLp-700XLp-700XL-700XL-700XL-700XLp-700XL-700XLp-700XLp-700XLp-700XL-700XL-700XLp-700XLp-700XLp-700XLp-700XLp-700

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JACOBSVILLE NEIGHBORHOOD SOIL ... - … (FSP) dated "November 2004" and the Quality Assurance...

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