J8445-1 Std Tal L2 Final Report...The test results in this report relate only to sample(s) as...

ANALYTICAL REPORT

Job Number 200-8445-1

SDG Number WC02

Job Description LPRSA - Phase I Removal Action

ForARCADIS US Inc

2300 Eastlake Avenue EastSuite 140

Seattle WA 98102

Attention Ms Shannon Dunn

_____________________________________________

Approved for releaseKirk F YoungProject Manager I12222011 423 PM

Kirk F YoungProject Manager I

kirkyoungtestamericainccom12222011

cc Mr Joe HouserMr Don ReedMr Ryan Shatt

The test results in this report relate only to sample(s) as received by the laboratory These test results were derivedunder a quality system that adheres to the requirements of NELAC Pursuant to NELAC this report may not beproduced in full without written approval from the laboratory

TestAmerica Laboratories Inc

TestAmerica Burlington 30 Community Drive Suite 11 South Burlington VT 05403

Tel (802) 660-1990 Fax (802) 660-1919 wwwtestamericainccom

12222011 of 53

Table of ContentsCover Title Page 1

Report Narrative 3

Method Summary 4

Method Analyst Summary 5

Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 17

QC Results 19

Qc Association Summary 20

Surrogate Recovery Report 24

Qc Reports 32

Client Chain of Custody 51

Sample Receipt Checklist 52

12222011Page 2 of 53

CASE NARRATIVE

Client ARCADIS US Inc

Project LPRSA - Phase I Removal Action

Report Number WC02 (200- 8445-1) Enclosed is the data set for the referenced project work With the exceptions noted as flags or footnotes standard analytical protocols were followed in performing the analytical work and the applied control limits were met Calibration and calibration verification were assessed on an analyte specific basis Initial calibration and continuing calibration criteria may not have been met in all instances Calculations were performed before rounding to avoid round-off errors in calculated results All holding times were met and proper preservation noted for the methods of analysis Manual integration was employed in deriving certain of the analytical results Positive instrument responses in the analysis of samples and quality controls were evaluated to the established method detection limit (MDL) This is an abbreviated report A more formal report will be issued in a CLP-like format with supportive documentation and further narrative discussion

12222011Page 3 of 53

METHOD SUMMARY

Client ARCADIS US Inc Job Number 200-8445-1Sdg Number WC02

Preparation MethodMethodLab LocationDescription

Matrix Solid

LowMedium Volatiles TAL BUR SOM012 SOM012VOA

TCLP Extraction SW846 1311

Volatile Sample Preservation TCLP Leachate TAL BUR SOM012 SOM012VOA_PR

Semivolatiles TAL BUR SOM012 SOM012SV


Continuous Liquid-Liquid Extraction of Water Samples SOM012 SOM012SV_CLLE

Aroclors TAL BUR SOM012 SOM012PCB

Ultrasonic Extraction of SoilSediment Samples SOM012 SOM012PCB_SONC

Sulfuric AcidPermanganate Cleanup SOM012 SOM012SO4CU

Pesticides TAL BUR SOM012 SOM012Pest


Separatory Funnel Extraction of Water Samples SOM012 SOM012Pes_SFE

Florisil Cleanup SOM012 SOM012FLCU

ISM012 Mercury TAL BUR ISM012 ISM012HG


Preparation ISM012 Mercury (EPA 7470A) ISM012 ISM012HG

ISM012 Metals (ICP) TAL BUR ISM012 ISM012ICP


Preparation ISM012 Metals ICP (EPA 2007) ISM012 ISM012ICP

ISM012 Cyanide TAL BUR ISM012 ISM012CN

Preparation ISM012 Cyanide (MIDI-Distillation) ISM012 ISM012CN

Matrix Water


Volatile sample preservation Field Preserved Water TAL BUR SOM012 SOM012VOA_PR

Lab References

TAL BUR = TestAmerica Burlington

Method References

ISM012 = US Environmental Protection Agency

SOM012 = US Environmental Protection Agency

SW846 = Test Methods For Evaluating Solid Waste PhysicalChemical Methods Third Edition November 1986 And Its Updates

TestAmerica Burlington 12222011Page 4 of 53

METHOD ANALYST SUMMARY

Client ARCADIS US Inc Job Number 200-8445-1

Method Analyst Analyst ID

Sdg Number WC02

Phillips Mark T MTPSOM012 SOM012VOA

Edwin Joseph JESOM012 SOM012SV

Duncan Stacee L SLDSOM012 SOM012PCB

Hammond Ryan J RJHSOM012 SOM012Pest

Holzschuh Jessica A JAHISM012 ISM012HG

Lyons Benjamin BLISM012 ISM012ICP

Nelson Andrea J AJNISM012 ISM012CN

TestAmerica Burlington

12222011Page 5 of 53

SAMPLE SUMMARY


Client Sample IDLab Sample ID Client Matrix Sampled ReceivedDateTime DateTime

200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MSD PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-2STOBLK VHBLK01 Water 12072011 1430 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 53

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid

Date Sampled 12062011 1330

Date Received 12072011 1140

SOM012VOA LowMedium Volatiles-TCLP

Dilution

12152011 1722

12152011 1722

10

SOM012VOA

Final WeightVolume

Initial WeightVolume

Lab File ID

Instrument ID

nfea19d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Analysis Method

Prep Method

12132011 1145Leach Date

Analyte DryWt Corrected N Result (ugL) Qualifier RL

50 U 50Vinyl chloride50 U 5011-Dichloroethene35 B 102-Butanone52 50Chloroform50 U 50Carbon tetrachloride50 U 50Benzene50 U 5012-Dichloroethane22 50Trichloroethene0098 J 50Tetrachloroethene50 U 50Chlorobenzene50 U 5014-Dichlorobenzene

Surrogate Rec Acceptance LimitsQualifier

92 65 - 131Vinyl chloride-d3103 71 - 131Chloroethane-d580 55 - 10411-Dichloroethene-d2229 49 - 1552-Butanone-d5148 78 - 121Chloroform-d100 78 - 12912-Dichloroethane-d4105 77 - 124Benzene-d6101 79 - 12412-Dichloropropane-d6105 77 - 121Toluene-d8103 73 - 121trans-13-Dichloropropene-d4230 28 - 1352-Hexanone-d5109 50 - 15014-Dioxane-d80 73 - 1251122-Tetrachloroethane-d2107 80 - 13112-Dichlorobenzene-d4


Analytical Data


Client Sample ID

Lab Sample ID

VHBLK01

Client Matrix

200-8445-2STOBLK

Water



SOM012VOA LowMedium Volatiles

Dilution

12152011 1751

12152011 1751

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea20d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

200-30798

NA

Analysis Method

Prep Method

Analyte Result (ugL) Qualifier RL

50 U 50Vinyl chloride50 U 5011-Dichloroethene10 U 102-Butanone50 U 50Chloroform50 U 50Carbon tetrachloride50 U 50Benzene50 U 5012-Dichloroethane028 J B 50Trichloroethene50 U 50Tetrachloroethene50 U 50Chlorobenzene50 U 5014-Dichlorobenzene




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid



SOM012SV Semivolatiles-TCLP

Dilution

12132011 2213

12202011 0837

10

SOM012SV

Injection Volume

Final WeightVolume


Lab File ID

Instrument ID

rjqha06d

200 mL

1000 uL

2 uL

SOM012SV_CLLE

Ri

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Method

Prep Method

12122011 1717Leach Date


039 J 25Pyridine25 U 252-Methylphenol25 U 254-Methylphenol25 U 25Hexachloroethane25 U 25Nitrobenzene25 U 25Hexachlorobutadiene55 25246-Trichlorophenol120 25245-Trichlorophenol25 U 2524-Dinitrotoluene50 U 50Pentachlorophenol25 U 25Total Cresols


89 39 - 106Phenol-d578 40 - 105Bis(2-chloroethyl)ether-d884 41 - 1062-Chlorophenol-d4115 25 - 1114-Methylphenol-d893 43 - 108Nitrobenzene-d595 40 - 1082-Nitrophenol-d4100 37 - 10524-Dichlorophenol-d381 1 - 1454-Chloroaniline-d494 47 - 114Dimethylphthalate-d691 41 - 107Acenaphthylene-d863 33 - 1164-Nitrophenol-d489 42 - 111Fluorene-d1082 22 - 10446-Dinitro-2-methylphenol-d295 44 - 110Anthracene-d1090 52 - 119Pyrene-d1099 32 - 121Benzo(a)pyrene-d12


Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix Moisture 405

200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date

Analysis Batch 200-30597

200-30424Prep Batch

Analysis Method

Prep Method

Analyte DryWt Corrected Y Result (ugKg) Qualifier RL

5500 U 5500Aroclor-10165500 U 5500Aroclor-12215500 U 5500Aroclor-12325500 U 5500Aroclor-12425500 U 5500Aroclor-12485500 U 5500Aroclor-12545500 U 5500Aroclor-12605500 U 5500Aroclor-12625500 U 5500Aroclor-1268


0 30 - 150DTetrachloro-m-xylene0 30 - 150DDecachlorobiphenyl


Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type SECONDARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid



SOM012Pest Pesticides-TCLP

Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


0018 J P 0047gamma-BHC (Lindane)00049 J P B 0047Heptachlor0013 J P 0047Heptachlor epoxide0011 J P 0094Endrin00031 J P 047Methoxychlor47 U 47Toxaphene047 U 047Chlordane (technical)


111 30 - 150Decachlorobiphenyl105 30 - 150Tetrachloro-m-xylene


Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid



ISM012HG ISM012 Mercury-TCLP

ISM012HG Instrument ID

Lab File ID 121911BBPRN

Dilution 10 Initial WeightVolume 50 mL

12192011 1124 Final WeightVolume 50 mL

12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date

Analyte DryWt Corrected N Result (ugL) Qualifier MDLE RL

020 U 0200084Mercury

ISM012ICP ISM012 Metals (ICP)-TCLP

ISM012ICP Instrument ID

Lab File ID 121511-04ttx



12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date

Analyte DryWt Corrected N Result (ugL) Qualifier MDL RL

95 J 10032Arsenic369 20035Barium50 U 50037Cadmium269 10010Chromium139 10025Lead87 J 35039Selenium100 U N 100081Silver


Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



Analyte Result Qual Units MDL RL Dil Method

Cyanide 031 J mgKg 014 080 10 ISM012CNDryWt Corrected YAnalysis Date 12152011 1414Analysis Batch 200-30744

Prep Batch 200-30715 Prep Date 12152011 0930


DATA REPORTING QUALIFIERS


Lab Section Qualifier Description

Sdg Number WC02

GCMS VOA

Analyzed for but not detectedU

Indicates an estimated valueJ

Surrogate exceeds the control limit

The analyte was found in an associated blank as well as in the sample

B

GCMS Semi VOA


Compound concentration exceeds the upper level of the calibration range of the instrument for that specific analysis

E



GC Semi VOA



E


Sample was analyzed at a higher dilution factorD

The Difference between columns is greater than 25P


B

Metals

Indicates analyzed for but not detectedU

Sample result is greater than the MDL but below the CRDLJ

Spiked sample recovery is not within control limitsN


12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53

QUALITY CONTROL RESULTS


12222011Page 19 of 53

Quality Control Results


QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Sdg Number WC02

ReportBasis

GCMS VOA

Prep Batch 200-30568Method Blank Solid 1311MB 200-305681-A P

SolidPRR1WC-CS03 1311200-8445-1 PMatrix Spike Solid 1311200-8445-1MS PMatrix Spike Duplicate Solid 1311200-8445-1MSD P

Analysis Batch200-30798Method Blank Solid SOM012VOAMB 200-305681-A PMethod Blank Water SOM012VOAMB 200-307984 T

SolidPRR1WC-CS03 SOM012VOA200-8445-1 PMatrix Spike Solid SOM012VOA200-8445-1MS PMatrix Spike Duplicate Solid SOM012VOA200-8445-1MSD P

WaterVHBLK01 SOM012VOA200-8445-2STOBLK T

Report Basis

P = TCLP

T = Total

GCMS Semi VOA

Prep Batch 200-30524SolidPRR1WC-CS03 1311200-8445-1 P

Matrix Spike Solid 1311200-8445-1MS PMatrix Spike Duplicate Solid 1311200-8445-1MSD P

Prep Batch 200-30614Method Blank Water SOM012SV_CLLMB 200-306141-A T

Solid 200-30524PRR1WC-CS03 SOM012SV_CLL200-8445-1 PMatrix Spike Solid 200-30524SOM012SV_CLL200-8445-1MS PMatrix Spike Duplicate Solid 200-30524SOM012SV_CLL200-8445-1MSD P

Analysis Batch200-31040Method Blank Water 200-30614SOM012SVMB 200-306141-A T

Solid 200-30614PRR1WC-CS03 SOM012SV200-8445-1 PMatrix Spike Solid 200-30614SOM012SV200-8445-1MS PMatrix Spike Duplicate Solid 200-30614SOM012SV200-8445-1MSD P

Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA

Prep Batch 200-30424Lab Control Sample Solid SOM012PCB_SLCS 200-304242-C TMethod Blank Solid SOM012PCB_SMB 200-304241-C T

SolidPRR1WC-CS03 SOM012PCB_S200-8445-1 TMatrix Spike Solid SOM012PCB_S200-8445-1MS TMatrix Spike Duplicate Solid SOM012PCB_S200-8445-1MSD T



Analysis Batch200-30597Lab Control Sample Solid 200-30424SOM012PCBLCS 200-304242-C TMethod Blank Solid 200-30424SOM012PCBMB 200-304241-C T

Solid 200-30424PRR1WC-CS03 SOM012PCB200-8445-1 TMatrix Spike Solid 200-30424SOM012PCB200-8445-1MS TMatrix Spike Duplicate Solid 200-30424SOM012PCB200-8445-1MSD T

Prep Batch 200-30607Lab Control Sample Water SOM012Pes_SFLCS 200-306072-C TMethod Blank Water SOM012Pes_SFMB 200-306071-C T

Solid 200-30524PRR1WC-CS03 SOM012Pes_SF200-8445-1 PMatrix Spike Solid 200-30524SOM012Pes_SF200-8445-1MS PMatrix Spike Duplicate Solid 200-30524SOM012Pes_SF200-8445-1MSD P

Analysis Batch200-30815Lab Control Sample Water 200-30607SOM012PestLCS 200-306072-C TMethod Blank Water 200-30607SOM012PestMB 200-306071-C T

Solid 200-30607PRR1WC-CS03 SOM012Pest200-8445-1 PMatrix Spike Solid 200-30607SOM012Pest200-8445-1MS PMatrix Spike Duplicate Solid 200-30607SOM012Pest200-8445-1MSD P

Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals

Prep Batch 200-30524TCLP SPLPE Leachate Blank Solid 1311LB 200-305241-B PTCLP SPLPE Leachate Blank Solid 1311LB 200-305241-C P

SolidPRR1WC-CS03 1311200-8445-1 PDuplicate Solid 1311200-8445-1DU PMatrix Spike Solid 1311200-8445-1MS PMatrix Spike Solid 1311200-8445-1MSDL P

Prep Batch 200-30648Lab Control Sample Water ISM012ICPLCS 200-306482-A TMethod Blank Water ISM012ICPMB 200-306481-A TTCLP SPLPE Leachate Blank Solid 200-30524ISM012ICPLB 200-305241-B P

Solid 200-30524PRR1WC-CS03 ISM012ICP200-8445-1 PDuplicate Solid 200-30524ISM012ICP200-8445-1DU PMatrix Spike Solid 200-30524ISM012ICP200-8445-1MS PMatrix Spike Solid 200-30524ISM012ICP200-8445-1MSDL P

Prep Batch 200-30804Method Blank Water ISM012HGMB 200-3080411-A TTCLP SPLPE Leachate Blank Solid 200-30524ISM012HGLB 200-305241-C P

Solid 200-30524PRR1WC-CS03 ISM012HG200-8445-1 PDuplicate Solid 200-30524ISM012HG200-8445-1DU PMatrix Spike Solid 200-30524ISM012HG200-8445-1MS P

Analysis Batch200-30845TCLP SPLPE Leachate Blank Solid 200-30648ISM012ICPLB 200-305241-B PLab Control Sample Water 200-30648ISM012ICPLCS 200-306482-A TMethod Blank Water 200-30648ISM012ICPMB 200-306481-A T


Analysis Batch200-30941TCLP SPLPE Leachate Blank Solid 200-30804ISM012HGLB 200-305241-C PMethod Blank Water 200-30804ISM012HGMB 200-3080411-A T


Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry

Prep Batch 200-30715Method Blank Solid ISM012CNMB 200-3071511-A T

SolidPRR1WC-CS03 ISM012CN200-8445-1 TDuplicate Solid ISM012CN200-8445-1DU TMatrix Spike Solid ISM012CN200-8445-1MS T

Analysis Batch200-30744Method Blank Solid 200-30715ISM012CNMB 200-3071511-A T

Solid 200-30715PRR1WC-CS03 ISM012CN200-8445-1 TDuplicate Solid 200-30715ISM012CN200-8445-1DU TMatrix Spike Solid 200-30715ISM012CN200-8445-1MS T

Report Basis

T = Total


12222011Page 23 of 53


Job Number 200-8445-1Sdg Number WC02


Surrogate Recovery Report


Client Matrix Solid TCLP

Lab Sample ID Rec

VCL CLA DCE BUT CLF DCA BEN DPA

Client Sample ID Rec Rec Rec Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104

Surrogate Acceptance Limits

VCL = Vinyl chloride-d3 65-131CLA = Chloroethane-d5 71-131DCE = 11-Dichloroethene-d2 55-104BUT = 2-Butanone-d5 49-155CLF = Chloroform-d 78-121DCA = 12-Dichloroethane-d4 78-129BEN = Benzene-d6 77-124DPA = 12-Dichloropropane-d6 79-124


12222011Page 24 of 53







Lab Sample ID Client Sample ID

TOL TDP HEX DXE TCA DCZ

Rec Rec Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104


TOL = Toluene-d8 77-121TDP = trans-13-Dichloropropene-d4 73-121HEX = 2-Hexanone-d5 28-135DXE = 14-Dioxane-d8 50-150TCA = 1122-Tetrachloroethane-d2 73-125DCZ = 12-Dichlorobenzene-d4 80-131


12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53





SOM012SV Semivolatiles


Lab Sample ID Rec

PHL BCE 2CP 4MP NBZ 2NP DCP 4CA


200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46


PHL = Phenol-d5 39-106BCE = Bis(2-chloroethyl)ether-d8 40-1052CP = 2-Chlorophenol-d4 41-1064MP = 4-Methylphenol-d8 25-111NBZ = Nitrobenzene-d5 43-1082NP = 2-Nitrophenol-d4 40-108DCP = 24-Dichlorophenol-d3 37-1054CA = 4-Chloroaniline-d4 1-145


12222011Page 28 of 53







Lab Sample ID Rec

DMP ACY 4NP FLR NMP ANC PYR BAP


200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90


DMP = Dimethylphthalate-d6 47-114ACY = Acenaphthylene-d8 41-1074NP = 4-Nitrophenol-d4 33-116FLR = Fluorene-d10 42-111NMP = 46-Dinitro-2-methylphenol-d2 22-104ANC = Anthracene-d10 44-110PYR = Pyrene-d10 52-119BAP = Benzo(a)pyrene-d12 32-121


12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97

200-8445-1 MS PRR1WC-CS03 MS 0D 0D 0D 0D

200-8445-1 MSD PRR1WC-CS03 MSD 0D 0D 0D 0D


TCX = Tetrachloro-m-xylene 30-150DCB = Decachlorobiphenyl 30-150


12222011Page 30 of 53





SOM012Pest Pesticides



DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103


DCB = Decachlorobiphenyl 30-150TCX = Tetrachloro-m-xylene 30-150


12222011Page 31 of 53


Job Number 200-8445-1Client ARCADIS US IncSdg Number WC02

WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943

Method Blank - Batch 200-30798

Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL

Method SOM012VOAPreparation SOM012VOA_PR

NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA

Analyte Result Qual RL

50 U 50Vinyl chloride50 U 5011-Dichloroethene10 U 102-Butanone50 U 50Chloroform50 U 50Carbon tetrachloride50 U 50Benzene50 U 5012-Dichloroethane017 J 50Trichloroethene0044 J 50Tetrachloroethene50 U 50Chlorobenzene50 U 5014-Dichlorobenzene

Surrogate Rec Acceptance Limits

Vinyl chloride-d3 89 65 - 131Chloroethane-d5 99 71 - 13111-Dichloroethene-d2 78 55 - 1042-Butanone-d5 110 49 - 155Chloroform-d 100 78 - 12112-Dichloroethane-d4 98 78 - 129Benzene-d6 105 77 - 12412-Dichloropropane-d6 98 79 - 124Toluene-d8 104 77 - 121trans-13-Dichloropropene-d4 104 73 - 1212-Hexanone-d5 108 28 - 13514-Dioxane-d8 125 50 - 1501122-Tetrachloroethane-d2 103 73 - 12512-Dichlorobenzene-d4 103 80 - 131




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL

Method SOM012VOAPreparation SOM012VOA_PRTCLP

NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date


50 U 50Vinyl chloride50 U 5011-Dichloroethene33 102-Butanone50 U 50Chloroform50 U 50Carbon tetrachloride50 U 50Benzene50 U 5012-Dichloroethane50 U 50Trichloroethene50 U 50Tetrachloroethene50 U 50Chlorobenzene50 U 5014-Dichlorobenzene






Dilution

Dilution

12152011 1449

12152011 1517

Solid

Matrix SpikeMatrix Spike Duplicate Recovery Report - Batch 200-30798

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA

Analyte RPD LimitRPDLimit

Rec

MS MSD MS Qual MSD Qual

113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform

105 102 75 - 125 3 15Carbon tetrachloride

108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane

181 181 71 - 120 0 14Trichloroethene

104 103 75 - 125 1 15Tetrachloroethene

107 107 75 - 130 0 13Chlorobenzene

98 98 75 - 125 1 1514-Dichlorobenzene

Surrogate Acceptance LimitsMS Rec MSD Rec

Vinyl chloride-d3 95 97 65 - 131Chloroethane-d5 97 99 71 - 13111-Dichloroethene-d2 109 112 55 - 104 2-Butanone-d5 238 242 49 - 155 Chloroform-d 8 7 78 - 121 12-Dichloroethane-d4 107 106 78 - 129Benzene-d6 109 107 77 - 12412-Dichloropropane-d6 107 104 79 - 124Toluene-d8 108 106 77 - 121trans-13-Dichloropropene-d4 108 104 73 - 1212-Hexanone-d5 283 279 28 - 135 14-Dioxane-d8 116 107 50 - 1501122-Tetrachloroethane-d2 0 0 73 - 125 12-Dichlorobenzene-d4 106 104 80 - 131




WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL

Method SOM012SVPreparation SOM012SV_CLLE

RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA

Prep Date Injection Volume12132011 2213 2 uL

Leach Date NA


25 U 25Pyridine25 U 252-Methylphenol25 U 254-Methylphenol25 U 25Hexachloroethane25 U 25Nitrobenzene25 U 25Hexachlorobutadiene25 U 25246-Trichlorophenol25 U 25245-Trichlorophenol25 U 2524-Dinitrotoluene50 U 50Pentachlorophenol25 U 25Total Cresols


Phenol-d5 77 39 - 106Bis(2-chloroethyl)ether-d8 72 40 - 1052-Chlorophenol-d4 73 41 - 1064-Methylphenol-d8 95 25 - 111Nitrobenzene-d5 85 43 - 1082-Nitrophenol-d4 86 40 - 10824-Dichlorophenol-d3 80 37 - 1054-Chloroaniline-d4 86 1 - 145Dimethylphthalate-d6 98 47 - 114Acenaphthylene-d8 84 41 - 1074-Nitrophenol-d4 106 33 - 116Fluorene-d10 89 42 - 11146-Dinitro-2-methylphenol-d2 65 22 - 104Anthracene-d10 88 44 - 110Pyrene-d10 86 52 - 119Benzo(a)pyrene-d12 90 32 - 121




Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL

Method SOM012SVPreparation SOM012SV_CLLETCLP

Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol

76 42 30 - 120 57 40Hexachloroethane

95 91 30 - 120 5 40Nitrobenzene

77 40 30 - 120 63 40Hexachlorobutadiene

92 90 30 - 120 2 40246-Trichlorophenol


98 96 24 - 96 2 3824-Dinitrotoluene

80 79 9 - 103 2 50Pentachlorophenol


Phenol-d5 90 86 39 - 106Bis(2-chloroethyl)ether-d8 77 73 40 - 1052-Chlorophenol-d4 80 77 41 - 1064-Methylphenol-d8 114 103 25 - 111Nitrobenzene-d5 91 87 43 - 1082-Nitrophenol-d4 91 88 40 - 10824-Dichlorophenol-d3 93 87 37 - 1054-Chloroaniline-d4 65 46 1 - 145Dimethylphthalate-d6 84 83 47 - 114Acenaphthylene-d8 89 82 41 - 1074-Nitrophenol-d4 59 62 33 - 116Fluorene-d10 82 78 42 - 11146-Dinitro-2-methylphenol-d2 81 82 22 - 104Anthracene-d10 87 86 44 - 110Pyrene-d10 92 96 52 - 119Benzo(a)pyrene-d12 92 90 32 - 121




SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg

Method SOM012PCBPreparation SOM012PCB_SONC

5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Column ID PRIMARYLeach Date NA




Tetrachloro-m-xylene 97 30 - 150Decachlorobiphenyl 103 30 - 150






Solid

10

Lab Control Sample - Batch 200-30424

Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C

Analysis Date 12132011 0800

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

Prep Date Injection Volume 1 uL

Leach Date

12092011 1708

Column ID PRIMARYNA

Analyte QualLimit RecResultSpike Amount

333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260


Tetrachloro-m-xylene 95 30 - 150

Decachlorobiphenyl 97 30 - 150

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID SECONDARYNA


333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260


Tetrachloro-m-xylene 0 0 30 - 150D DDecachlorobiphenyl 0 0 30 - 150D D

Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL

Method SOM012PestPreparation SOM012Pes_SFE

5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA




0050 U 0050gamma-BHC (Lindane)000066 J P 0050Heptachlor0050 U 0050Heptachlor epoxide010 U 010Endrin050 U 050Methoxychlor50 U 50Toxaphene050 U 050Chlordane (technical)


Decachlorobiphenyl 115 30 - 150Tetrachloro-m-xylene 97 30 - 150






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA


00500 0051 101 50 - 120gamma-BHC (Lindane)

00500 0056 113 50 - 150Heptachlor epoxide

0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY

Method SOM012PestPreparation SOM012Pes_SFETCLP

5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


99 95 56 - 123 5 15gamma-BHC (Lindane)

101 97 40 - 131 4 20 P B P BHeptachlor

82 79 40 - 130 3 20Heptachlor epoxide

115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor


Decachlorobiphenyl 112 110 30 - 150Tetrachloro-m-xylene 103 101 30 - 150




Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



36 32 40 - 131 12 20 E P B B PHeptachlor


33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene

94 93 40 - 130 1 30 P PChlordane (technical)




Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene



Decachlorobiphenyl 104 104 30 - 150Decachlorobiphenyl 104 108 30 - 150Decachlorobiphenyl 106 104 30 - 150Decachlorobiphenyl 106 108 30 - 150Tetrachloro-m-xylene 101 101 30 - 150Tetrachloro-m-xylene 101 103 30 - 150Tetrachloro-m-xylene 99 101 30 - 150Tetrachloro-m-xylene 99 103 30 - 150




WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL

Method ISM012HGPreparation ISM012HG

MEPCV3 IIMB 200-3080411-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA

Analyte Result Qual MDLE RL


SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120

TCLP SPLPE Leachate Blank - Batch 200-30804

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL

Method ISM012HGPreparation ISM012HGTCLP

MEPCV3 IILB 200-305241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10

Matrix Spike - Batch 200-30804

Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717

Analyte QualLimit RecResultSpike AmountSample ResultQual

020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10

Duplicate - Batch 200-30804

Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717

Analyte QualLimitRPDResultSample ResultQual

020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL

Method ISM012ICPPreparation ISM012ICP

METICP7MB 200-306481-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA

Analyte Result Qual MDL RL

100 U 10032Arsenic200 U 20035Barium50 U 50037Cadmium100 U 10010Chromium100 U 10025Lead350 U 35039Selenium100 U 100081Silver

SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL

Method ISM012ICPPreparation ISM012ICPTCLP

METICP7LB 200-305241-B

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7LCS 200-306482-A


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date Run Type DL

Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


8895 J 7 100 JArsenic

348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead

7787 J 12 350 JSelenium

100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg

Method ISM012CNPreparation ISM012CN

WCLachatMB 200-3071511-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA


050 U 0500087Cyanide

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53

Login Sample Receipt Checklist


SDG Number WC02

Login Number 8445

Question Answer Comment

Creator Holt Jamie

List Source TestAmerica Burlington

List Number 2

NARadioactivity either was not measured or if measured is at or below background

Lab does not accept radioactive samples

TrueThe coolers custody seal if present is intact No numbers

TrueThe cooler or samples do not appear to have been compromised or tampered with

TrueSamples were received on ice

TrueCooler Temperature is acceptable

TrueCooler Temperature is recorded 04 ordmC IR gun ID 96 CF= 0

TrueCOC is present

TrueCOC is filled out in ink and legible

TrueCOC is filled out with all pertinent information

FalseIs the Field Samplers name present on COC Refer to Job Narrative for details

TrueThere are no discrepancies between the sample IDs on the containers and the COC

TrueSamples are received within Holding Time

TrueSample containers have legible labels

TrueContainers are not broken or leaking

TrueSample collection datetimes are provided

TrueAppropriate sample containers are used

TrueSample bottles are completely filled

NASample Preservation Verified

TrueThere is sufficient vol for all requested analyses incl any requested MSMSDs

TrueVOA sample vials do not have headspace or bubble is lt6mm (14) in diameter

TrueMultiphasic samples are not present

TrueSamples do not require splitting or compositing

NAResidual Chlorine Checked Check done at department level if required


ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE



Report Number WC02 (200-8445-2) Enclosed is the data set for the referenced project work With the exceptions noted as flags or footnotes standard analytical protocols were followed in performing the analytical work and the applied control limits were met Calibration and calibration verification were assessed on an analyte specific basis Initial calibration and continuing calibration criteria may not have been met in all instances Calculations were performed before rounding to avoid round-off errors in calculated results Manual integration was employed in deriving certain of the analytical results For the Method 8151A analysis positive instrument responses in the analysis of samples and quality controls were evaluated to the established method detection limit (MDL) This is an abbreviated report A more formal report will be issued in a CLP-like format with supportive documentation and further narrative discussion

12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid

Herbicides (GC) TAL BUR SW846 8151A


Extraction (Herbicides) SW846 8151A

pH TAL BUR SW846 9045D

Paint Filter TAL BUR SW846 9095B

Ignitability Solids TAL EDI SW846 1030

Sulfide Acid Soluble and Insoluble (Titrimetric) TAL EDI SW846 9034

Sulfide Distillation (Acid Soluble and Insoluble) SW846 9030B

Lab References


TAL EDI = TestAmerica Edison

Method References






Sdg Number WC02

Hammond Ryan J RJHSW846 8151A

Cabanganan Maria MBSW846 1030

Vu Huan HVSW846 9034

Nelson Andrea J AJNSW846 9045D

Tam Michelle N MNTSW846 9095B


12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid



8151A Herbicides (GC)-TCLP

Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)


122 60 - 130p24-Dichlorophenylacetic acid


Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


492 60 - 130X24-Dichlorophenylacetic acid


Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)


155 60 - 130p D X24-Dichlorophenylacetic acid546 60 - 130D X24-Dichlorophenylacetic acid


Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid




Sulfide 146 U mgKg 54 146 10 9034DryWt Corrected YAnalysis Date 12132011 1700Analysis Batch 460-96374


Analyte Result Qual Units Dil Method

pH 120 HF SU 10 9045DDryWt Corrected NAnalysis Date 12082011 1635Analysis Batch 200-30350

Free Liquid Absent mL100g 10 9095BDryWt Corrected NAnalysis Date 12082011 1930Analysis Batch 200-30372

Analyte Result Qual Units RL RL Dil Method

Burn Rate 220 U mmsec 220 220 10 1030DryWt Corrected NAnalysis Date 12192011 1130Analysis Batch 460-96407





Sdg Number WC02

GC Semi VOA

Compound was found in the blank and sampleB

Indicates the analyte was analyzed for but not detectedU

MS MSD The analyte present in the original sample is 4 times greater than the matrix spike concentration therefore control limits are not applicable

4

Result exceeded calibration rangeE

Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value

J

Sample results are obtained from a dilution the surrogate or matrix spike recoveries reported are calculated from diluted samples

D

Surrogate is outside control limitsX

The RPD between the primary and confirmation columndetector is gt40 The lower value has been reported

p

General Chemistry

Field parameter with a holding time of 15 minutesHF


MSMSD Recovery or RPD exceeds the control limitsF


12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA

Prep Batch 200-30524SolidPRR1WC-CS03 1311200-8445-1 PSolidPRR1WC-CS03 1311200-8445-1DL P


Prep Batch 200-30670Lab Control Sample Water 8151ALCS 200-306705-A TMethod Blank Water 8151AMB 200-306701-A T

Solid 200-30524PRR1WC-CS03 8151A200-8445-1 PSolid 200-30524PRR1WC-CS03 8151A200-8445-1DL P

Matrix Spike Solid 200-305248151A200-8445-1MS PMatrix Spike Duplicate Solid 200-305248151A200-8445-1MSD P

Analysis Batch200-31004Lab Control Sample Water 200-306708151ALCS 200-306705-A TMethod Blank Water 200-306708151AMB 200-306701-A T



Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry

Analysis Batch200-30350SolidPRR1WC-CS03 9045D200-8445-1 T

Duplicate Solid 9045D200-8445-1DU T

Analysis Batch200-30372SolidPRR1WC-CS03 9095B200-8445-1 T

Duplicate Solid 9095B200-8445-1DU T

Prep Batch 460-96372Lab Control Sample Solid 9030BLCS 460-963723-A TMethod Blank Solid 9030BMB 460-963721-A T

SolidPRR1WC-CS03 9030B200-8445-1 TMatrix Spike Solid 9030B200-8445-1MS TMatrix Spike Duplicate Solid 9030B200-8445-1MSD T

Analysis Batch460-96374Lab Control Sample Solid 460-963729034LCS 460-963723-A TMethod Blank Solid 460-963729034MB 460-963721-A T

Solid 460-96372PRR1WC-CS03 9034200-8445-1 TMatrix Spike Solid 460-963729034200-8445-1MS TMatrix Spike Duplicate Solid 460-963729034200-8445-1MSD T

Analysis Batch460-96407SolidPRR1WC-CS03 1030200-8445-1 T

Duplicate Solid 1030200-8445-1DU T

Report Basis

T = Total


12222011Page 15 of 28





8151A Herbicides (GC)



DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X

200-8445-1 MSD PRR1WC-CS03 MSD 119p 449X


DCPA = 24-Dichlorophenylacetic acid 60-130


12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL

Method 8151APreparation 8151A

0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)


24-Dichlorophenylacetic acid 94 60 - 130



Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY

Method 8151APreparation 8151ATCLP

0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)


24-Dichlorophenylacetic acid 120 119 60 - 130p p


24-Dichlorophenylacetic acid 401 449 60 - 130X X




mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume 10 mL

Method 1030Preparation NA

No Equipment 200-8445-1

Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA


220220 U NC 10 UBurn Rate




SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg

Method 9034Preparation 9030B

No Equipment MB 460-963721-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg


No Equipment LCS 460-963723-A


Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL

Method 9045DPreparation NA

WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume 10000 g

Method 9095BPreparation NA


Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA


AbsentAbsent NCFree Liquid


12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary

List Source TestAmerica Edison

List Creation 120811 1226 PMList Number 1


TrueThe coolers custody seal if present is intact 419142




TrueCooler Temperature is recorded 50 deg C IR 50

TrueCOC is present



TrueIs the Field Samplers name present on COC








TrueSample Preservation Verified





TrueResidual Chlorine Checked




SDG Number WC02

Login Number 8445


Creator Meyers Gary



TrueRadioactivity either was not measured or if measured is at or below background

TrueThe coolers custody seal if present is intact




TrueCooler Temperature is recorded

TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present


















J8445-1 Std_Tal_L2 Final Report

Cover Title Page

Table of Contents

Report Narrative

Method Summary

Method Analyst Summary

Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results

Qc Association Summary


Qc Reports

Client Chain of Custody

Sample Receipt Checklist


Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 17

QC Results 19



Qc Reports 32



12222011 of 53

CASE NARRATIVE




12222011Page 3 of 53

METHOD SUMMARY



Matrix Solid






















Matrix Water



Lab References


Method References








Sdg Number WC02









12222011Page 5 of 53

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140



SAMPLE RESULTS


12222011Page 7 of 53

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12152011 1722

12152011 1722

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea19d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Analysis Method

Prep Method

12132011 1145Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

VHBLK01

Client Matrix

200-8445-2STOBLK

Water




Dilution

12152011 1751

12152011 1751

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea20d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

200-30798

NA

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12132011 2213

12202011 0837

10

SOM012SV

Injection Volume

Final WeightVolume


Lab File ID

Instrument ID

rjqha06d

200 mL

1000 uL

2 uL

SOM012SV_CLLE

Ri

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Method

Prep Method

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



CASE NARRATIVE




12222011 of 53

METHOD SUMMARY



Matrix Solid






















Matrix Water



Lab References


Method References








Sdg Number WC02









12222011Page 5 of 53

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140



SAMPLE RESULTS


12222011Page 7 of 53

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12152011 1722

12152011 1722

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea19d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Analysis Method

Prep Method

12132011 1145Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

VHBLK01

Client Matrix

200-8445-2STOBLK

Water




Dilution

12152011 1751

12152011 1751

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea20d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

200-30798

NA

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12132011 2213

12202011 0837

10

SOM012SV

Injection Volume

Final WeightVolume


Lab File ID

Instrument ID

rjqha06d

200 mL

1000 uL

2 uL

SOM012SV_CLLE

Ri

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Method

Prep Method

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



METHOD SUMMARY



Matrix Solid






















Matrix Water



Lab References


Method References




TestAmerica Burlington 12222011 of 53




Sdg Number WC02









12222011Page 5 of 53

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140



SAMPLE RESULTS


12222011Page 7 of 53

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12152011 1722

12152011 1722

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea19d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Analysis Method

Prep Method

12132011 1145Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

VHBLK01

Client Matrix

200-8445-2STOBLK

Water




Dilution

12152011 1751

12152011 1751

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea20d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

200-30798

NA

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12132011 2213

12202011 0837

10

SOM012SV

Injection Volume

Final WeightVolume


Lab File ID

Instrument ID

rjqha06d

200 mL

1000 uL

2 uL

SOM012SV_CLLE

Ri

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Method

Prep Method

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports






Sdg Number WC02









12222011 of 53

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140



SAMPLE RESULTS


12222011Page 7 of 53

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12152011 1722

12152011 1722

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea19d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Analysis Method

Prep Method

12132011 1145Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

VHBLK01

Client Matrix

200-8445-2STOBLK

Water




Dilution

12152011 1751

12152011 1751

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea20d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

200-30798

NA

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12132011 2213

12202011 0837

10

SOM012SV

Injection Volume

Final WeightVolume


Lab File ID

Instrument ID

rjqha06d

200 mL

1000 uL

2 uL

SOM012SV_CLLE

Ri

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Method

Prep Method

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140



SAMPLE RESULTS


12222011Page 7 of 53

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12152011 1722

12152011 1722

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea19d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Analysis Method

Prep Method

12132011 1145Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

VHBLK01

Client Matrix

200-8445-2STOBLK

Water




Dilution

12152011 1751

12152011 1751

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea20d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

200-30798

NA

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12132011 2213

12202011 0837

10

SOM012SV

Injection Volume

Final WeightVolume


Lab File ID

Instrument ID

rjqha06d

200 mL

1000 uL

2 uL

SOM012SV_CLLE

Ri

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Method

Prep Method

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



SAMPLE RESULTS


12222011 of 53

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12152011 1722

12152011 1722

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea19d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Analysis Method

Prep Method

12132011 1145Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

VHBLK01

Client Matrix

200-8445-2STOBLK

Water




Dilution

12152011 1751

12152011 1751

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea20d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

200-30798

NA

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12132011 2213

12202011 0837

10

SOM012SV

Injection Volume

Final WeightVolume


Lab File ID

Instrument ID

rjqha06d

200 mL

1000 uL

2 uL

SOM012SV_CLLE

Ri

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Method

Prep Method

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12152011 1722

12152011 1722

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea19d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Analysis Method

Prep Method

12132011 1145Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

VHBLK01

Client Matrix

200-8445-2STOBLK

Water




Dilution

12152011 1751

12152011 1751

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea20d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

200-30798

NA

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12132011 2213

12202011 0837

10

SOM012SV

Injection Volume

Final WeightVolume


Lab File ID

Instrument ID

rjqha06d

200 mL

1000 uL

2 uL

SOM012SV_CLLE

Ri

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Method

Prep Method

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

VHBLK01

Client Matrix

200-8445-2STOBLK

Water




Dilution

12152011 1751

12152011 1751

10

SOM012VOA

Final WeightVolume


Lab File ID

Instrument ID

nfea20d

5 mL

5 mL

SOM012VOA_PR

Ni

Analysis Date

Prep Date

Analysis Batch

Prep Batch

200-30798

NA

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12132011 2213

12202011 0837

10

SOM012SV

Injection Volume

Final WeightVolume


Lab File ID

Instrument ID

rjqha06d

200 mL

1000 uL

2 uL

SOM012SV_CLLE

Ri

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Method

Prep Method

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

12132011 2213

12202011 0837

10

SOM012SV

Injection Volume

Final WeightVolume


Lab File ID

Instrument ID

rjqha06d

200 mL

1000 uL

2 uL

SOM012SV_CLLE

Ri

Analysis Date

Prep Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Method

Prep Method

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid



SOM012PCB Aroclors

Dilution

SOM012PCB

SOM012PCB_SONC

100

12132011 0824

12092011 1708

Instrument ID


Final WeightVolume

Injection Volume


3038 g

10000 uL

1 uL

5253i

Analysis Date

Prep Date


200-30424Prep Batch

Analysis Method

Prep Method




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date






Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

SOM012Pest

SOM012Pes_SFE

10

12152011 0038

12132011 1942

Instrument ID


Final WeightVolume

Injection Volume


1060 mL

10000 uL

1 uL

5005i

Analysis Date

Prep Date


200-30524

200-30607Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid








12142011 1215

ISM012HG

MEPCV3 II

Analysis Date

Prep Date


200-30804

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date








12142011 1131

ISM012ICP

METICP7

Analysis Date

Prep Date


200-30648

200-30524

Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid










Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011Page 17 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports






Sdg Number WC02

GCMS VOA





B

GCMS Semi VOA



E



GC Semi VOA



E





B

Metals





12222011 of 53




Sdg Number WC02

General Chemistry




12222011Page 18 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports






Sdg Number WC02

General Chemistry




12222011 of 53



12222011Page 19 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





12222011 of 53





Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011Page 20 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports







Sdg Number WC02

ReportBasis

GCMS VOA






Report Basis

P = TCLP

T = Total

GCMS Semi VOA







Report Basis

P = TCLP

T = Total


12222011 of 53





Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011Page 21 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports







Sdg Number WC02

ReportBasis

GC Semi VOA











Report Basis

P = TCLP

T = Total


12222011 of 53





Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011Page 22 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports







Sdg Number WC02

ReportBasis

Metals











Report Basis

P = TCLP

T = Total


12222011 of 53





Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011Page 23 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports







Sdg Number WC02

ReportBasis

General Chemistry





Report Basis

T = Total


12222011 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011Page 24 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports









Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 92 103 80 229 148 100 105 101

MB 200-307984 89 99 78 110 100 98 105 98

MB 200-305681-A 91 102 80 121 104 102 106 102

200-8445-1 MS PRR1WC-CS03 MS 95 97 109 238 8 107 109 107

200-8445-1 MSD PRR1WC-CS03 MSD 97 99 112 242 7 106 107 104




12222011 of 53










200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011Page 25 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports












200-8445-1 PRR1WC-CS03 105 103 230 109 0 107

MB 200-307984 104 104 108 125 103 103

MB 200-305681-A 106 105 148 156 113 106

200-8445-1 MS PRR1WC-CS03 MS 108 108 283 116 0 106

200-8445-1 MSD PRR1WC-CS03 MSD 106 104 279 107 0 104




12222011 of 53






Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011Page 26 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports








Client Matrix Water

Lab Sample ID Rec



200-8445-2 VHBLK01 82 92 72 97 91 89 96 90




12222011 of 53






Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011Page 27 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports








Client Matrix Water




200-8445-2 VHBLK01 95 97 103 99 97 94




12222011 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011Page 28 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports









Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 89 78 84 115 93 95 100 81

MB 200-306141-A 77 72 73 95 85 86 80 86

200-8445-1 MS PRR1WC-CS03 MS 90 77 80 114 91 91 93 65

200-8445-1 MSD PRR1WC-CS03 MSD 86 73 77 103 87 88 87 46




12222011 of 53







Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011Page 29 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports









Lab Sample ID Rec



200-8445-1 PRR1WC-CS03 94 91 63 89 82 95 90 99

MB 200-306141-A 98 84 106 89 65 88 86 90

200-8445-1 MS PRR1WC-CS03 MS 84 89 59 82 81 87 92 92

200-8445-1 MSD PRR1WC-CS03 MSD 83 82 62 78 82 86 96 90




12222011 of 53





SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011Page 30 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports







SOM012PCB Aroclors

Client Matrix Solid


TCX1 TCX2 DCB1 DCB2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 0D 0D 0D 0D

MB 200-304241-C 97 100 108 103

LCS 200-304242-C 95 95 105 97






12222011 of 53








DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011Page 31 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports










DCB1 DCB2 TCX1 TCX2

Rec Rec Rec Rec

200-8445-1 PRR1WC-CS03 111 114 106 105

MB 200-306071-C 115 116 97 99

LCS 200-306072-C 124 127 110 111

200-8445-1 MS PRR1WC-CS03 MS 115 112 103 103

200-8445-1 MS PRR1WC-CS03 MS 104 106 99 101

200-8445-1 MSD PRR1WC-CS03 MSD 110 111 102 101

200-8445-1 MSD PRR1WC-CS03 MSD 104 108 101 103




12222011 of 53



WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





WaterClient Matrix

10Dilution

Lab Sample ID

12152011 0943


Instrument ID

Lab File ID


Final WeightVolume

nfea04d

5 mL

5 mLUnits ugL


NiMB 200-307984

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

NA

NA

Prep Date 12152011 0943

Leach Date NA








SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1421


Instrument ID

Lab File ID


Final WeightVolume

nfea13d

5 mL

5 mLUnits ugL


NiMB 200-305681-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

Prep Date 12152011 1421

12132011 1145Leach Date








Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





Dilution

Dilution

12152011 1449

12152011 1517

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12152011 1449

12152011 1517

12132011 1145

12132011 1145

nfea14d

5 mL

5 mL

5 mL

nfea15d

5 mL

5 mL

5 mL


Ni

Ni

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

Analysis Batch

Prep Batch

Leach Batch

200-30798

200-30568

NA

NA


Rec


113 120 75 - 125 6 15Vinyl chloride

117 123 61 - 145 4 1411-Dichloroethene

122 122 75 - 125 0 15 B B2-Butanone

104 103 75 - 125 1 15Chloroform


108 108 76 - 127 1 11Benzene

107 107 75 - 125 0 1512-Dichloroethane



107 107 75 - 130 0 13Chlorobenzene







WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





WaterClient Matrix

10Dilution

Lab Sample ID

12202011 1025


Instrument ID

Lab File ID


Final WeightVolume

rjqha09d

200 mL

1000 uLUnits ugL


RiMB 200-306141-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

NA


Leach Date NA








Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





Dilution

Dilution

12202011 0913

12202011 0949

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Client Matrix Solid

12132011 2213

12132011 2213

12122011 1717

12122011 1717

rjqha07d

200 mL

1000 uL

2 uL

rjqha08d

200 mL

1000 uL

2 uL


Ri

Ri

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31040

200-30614

200-30524


Rec


78 76 30 - 120 2 40Pyridine

92 83 30 - 120 10 402-Methylphenol


95 91 30 - 120 5 40Nitrobenzene











SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





SolidClient Matrix

10Dilution

Lab Sample ID

12132011 0736


Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r071d

3000 g

10000 uLUnits ugKg


5253iMB 200-304241-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA












Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708

Column ID PRIMARYNA


333 37 110 50 - 150Aroclor-1016

333 32 96 J50 - 150Aroclor-1260




Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

12dec112108-r081d

3000 g

10000 uLUnits ugKg


5253iLCS 200-304242-C


Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA


Leach Date

12092011 1708



333 37 110 50 - 150Aroclor-1016

333 35 106 50 - 150Aroclor-1260







Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

PRIMARY

12dec112108-r101d

3015 g

10000 uL

1 uL

PRIMARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260



Dilution

Dilution

12132011 0912

12132011 0848

Solid


100

100

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12092011 1708

12092011 1708

12dec112108-r111d

3031 g

10000 uL

1 uL

SECONDARY

12dec112108-r101d

3015 g

10000 uL

1 uL

SECONDARY


5253i

5253i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

Analysis Batch

Prep Batch

Leach Batch

200-30597

200-30424

NA

NA


Rec


0 0 29 - 135 15 U UAroclor-1016

0 0 29 - 135 20 U UAroclor-1260






WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





WaterClient Matrix

10Dilution

Lab Sample ID

12142011 2346


Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r011d

1000 mL

10000 uLUnits ugL


5005iMB 200-306071-C

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA












Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942

Column ID PRIMARYNA




0100 011 111 50 - 120Endrin




Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

14dec111359-r021d

1000 mL

10000 uLUnits ugL


5005iLCS 200-306072-C


Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

NA


Leach Date

12132011 1942





0100 012 117 50 - 120Endrin







Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

PRIMARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec



101 97 40 - 131 4 20 P B P BHeptachlor


115 111 56 - 121 4 21Endrin

117 114 40 - 130 3 20Methoxychlor






Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





Dilution

Dilution

12152011 0129

12152011 0104

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r051d

1050 mL

10000 uL

1 uL

SECONDARY

14dec111359-r041d

1055 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec





33 31 56 - 121 6 21Endrin

117 115 40 - 130 2 20Methoxychlor



Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

PRIMARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

PRIMARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


87 84 40 - 130 4 30 P PToxaphene





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





Dilution

Dilution

12152011 0221

12152011 0155

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12132011 1942

12132011 1942

12122011 1717

12122011 1717

14dec111359-r071d

1055 mL

10000 uL

1 uL

SECONDARY

14dec111359-r061d

1050 mL

10000 uL

1 uL

SECONDARY


5005i

5005i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-30815

200-30607

200-30524


Rec


113 110 40 - 130 3 30 P PToxaphene







WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1118


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

NA

Prep Date 12142011 1215

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12192011 1120


Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date 12142011 1215

12122011 1717Leach Date



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mLUnits ugL


MEPCV3 II200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020 U 100 90 90 75 - 125Mercury




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121911BBPRN

50 mL

50 mL


MEPCV3 II200-8445-1

Analysis Date

Analysis Batch

12192011 1126

Prep Batch

Leach Batch

200-30941

200-30804

200-30524

Prep Date

Leach Date

12142011 1215

12122011 1717


020020 U UMercury




WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





WaterClient Matrix

10Dilution

Lab Sample ID

12162011 0212


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date 12142011 1131

Leach Date NA



SolidClient Matrix

10Dilution

Lab Sample ID

12162011 0226


Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date 12142011 1131

12122011 1717Leach Date






Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL




Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

NA

Prep Date

Leach Date

12142011 1131

NA


200 227 113 70 - 130Arsenic

400 414 104 70 - 130Barium

100 105 105 70 - 130Cadmium

200 210 105 70 - 130Chromium

200 181 90 70 - 130Lead

700 746 107 70 - 130Selenium

200 210 105 70 - 130Silver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717


369 2000 2180 90 75 - 125Barium

50 U 500 467 93 75 - 125Cadmium

100 U 500 151 30 75 - 125 NSilver

Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mLUnits ugL


METICP7200-8445-1DL


Analysis Batch

Prep Batch

Leach Batch

200-30845

200-30648

200-30524


Leach Date

12142011 1131

12122011 1717


95 J 1000 999 99 75 - 125Arsenic

269 200 453 92 75 - 125Chromium

139 500 494 96 75 - 125Lead

87 J 2000 1980 98 75 - 125Selenium




ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





ugLUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

121511-04ttx

100 mL

100 mL


METICP7200-8445-1

Analysis Date

Analysis Batch

12162011 0256

Prep Batch

Leach Batch

200-30845

200-30648

200-30524

Prep Date

Leach Date

12142011 1131

12122011 1717



348369 6 200Barium

5050 U UCadmium

269269 0Chromium

134139 3 100Lead


100100 U USilver




SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





SolidClient Matrix

10Dilution

Lab Sample ID

12152011 1413


Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

100 g

50 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date 12152011 0930

Leach Date NA



Solid

10


Lab Sample ID

Client Matrix

Dilution

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

102 g

50 mLUnits mgKg


WCLachat200-8445-1


Analysis Batch

Prep Batch

Leach Batch

200-30744

200-30715

NA

Prep Date

Leach Date

12152011 0930

NA


031 J 824 86 101 75 - 125Cyanide

mgKgUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

OM_12-15-11_02-01-0

103 g

50 mL


WCLachat200-8445-1

Analysis Date

Analysis Batch

12152011 1415

Prep Batch

Leach Batch NA

200-30744

200-30715

Prep Date

Leach Date

12152011 0930

NA


029031 J 6 080 JCyanide


12222011Page 51 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



12222011 of 53

12222011Page 52 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



12222011 of 53



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present


















ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



ANALYTICAL REPORT


SDG Number WC02


ForARCADIS US Inc


Seattle WA 98102


_____________________________________________









12222011Page 1 of 28


Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Report Narrative 3

Method Summary 4


Sample Summary 6

Sample Results 7

Sample Datasheets 8

Data Qualifiers 12

QC Results 13



Qc Reports 17



12222011Page 2 of 28

CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



CASE NARRATIVE




12222011Page 3 of 28

METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



METHOD SUMMARY



Matrix Solid









Lab References



Method References






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports






Sdg Number WC02







12222011Page 5 of 28

SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



SAMPLE SUMMARY



200-8445-1 PRR1WC-CS03 Solid 12062011 1330 12072011 1140

200-8445-1MS PRR1WC-CS03 Solid 12062011 1330 12072011 1140


200-8445-1DU PRR1WC-CS03 Solid 12062011 1330 12072011 1140


SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



SAMPLE RESULTS


12222011Page 7 of 28

Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume

Result Type PRIMARY

950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 E B 10002724-D0079 J p 04000012Silvex (245-TP)




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1512

12142011 1242

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date




Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


Client Sample ID

Lab Sample ID

PRR1WC-CS03

Client Matrix

200-8445-1

Solid




Dilution

8151A

8151A

20

12192011 1445

12142011 1242

Run Type DL

Instrument ID


Final WeightVolume

Injection Volume


950 mL

10000 uL

1 uL

0911i

Analysis Date

Prep Date


200-30524

200-30670Prep Batch

Analysis Method

Prep Method

Leach Batch

12122011 1717Leach Date


150 B D 1002724-D011 J p D 400012Silvex (245-TP)




Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



Analytical Data


General Chemistry

Client Sample ID

Lab Sample ID

PRR1WC-CS03


200-8445-1

Solid















Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports






Sdg Number WC02

GC Semi VOA




4



J


D



p

General Chemistry





12222011Page 12 of 28



12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





12222011Page 13 of 28





Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports







Sdg Number WC02

ReportBasis

GC Semi VOA









Report Basis

P = TCLP

T = Total


12222011Page 14 of 28





Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports







Sdg Number WC02

ReportBasis

General Chemistry











Report Basis

T = Total


12222011Page 15 of 28








DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports










DCPA1 DCPA2

Rec Rec

200-8445-1 DL PRR1WC-CS03 DL 155p D X

546D X

200-8445-1 PRR1WC-CS03 122p 492X

MB 200-306701-A 94 91

LCS 200-306705-A 106 101

200-8445-1 MS PRR1WC-CS03 MS 120p 401X





12222011Page 16 of 28



WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





WaterClient Matrix

10Dilution

Lab Sample ID

12192011 1350


Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r051d

1060 mL

10000 uLUnits ugL


0911iMB 200-306701-A

Analysis Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA




00220 J p 045001224-D018 U 018000053Silvex (245-TP)





Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

19dec111133-r061d

1000 mL

10000 uLUnits ugL


0911iLCS 200-306705-A


Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

NA


Leach Date

12142011 1242

Column ID PRIMARYNA


800 829 104 70 - 13524-D

0800 0794 99 65 - 145Silvex (245-TP)








Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





Dilution

Dilution

12192011 1540

12192011 1608

Solid


20

20

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Instrument ID

Lab File ID


Final WeightVolume

Injection Volume

Column ID

Client Matrix Solid

12142011 1242

12142011 1242

12122011 1717

12122011 1717

19dec111133-r091d

945 mL

10000 uL

1 uL

PRIMARY

19dec111133-r101d

950 mL

10000 uL

1 uL

PRIMARY


0911i

0911i

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524

Analysis Batch

Prep Batch

Leach Batch

200-31004

200-30670

200-30524


Rec


-3 -183 70 - 135 11 30 E 4 E 424-D

110 102 65 - 145 7 30Silvex (245-TP)








mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





mmsecUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12192011 1130

Prep Batch

Leach Batch

NANA

NA

460-96407

Prep Date

Leach Date

NA

NA






SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





SolidClient Matrix

10Dilution

Lab Sample ID

12132011 1700


Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg



Analysis Date

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date 12132011 1037

Leach Date NA


87 U 8732Sulfide

Solid

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

25 g

100 mLUnits mgKg




Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372 NA

NA

Prep Date

Leach Date

12132011 1037

NA


952 6680 70 70 - 130Sulfide

Dilution

Dilution

12132011 1700

12132011 1700

Solid


10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Solid

12132011 1037

12132011 1037

25 g

100 mL

25 g

100 mL


NA

NA

No Equipment

No Equipment

200-8445-1

200-8445-1

MS Lab Sample ID

MSD Lab Sample ID

Analysis Date

Prep Date

Leach Date NA

Analysis Date

Prep Date

Leach Date NA

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

Analysis Batch

Prep Batch

Leach Batch

460-96374

460-96372

NA

NA


Rec


26 24 90 - 110 9 14 F FSulfide




SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





SUUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

40 mL

40 mL


WCpHmeter200-8445-1

Analysis Date

Analysis Batch

12082011 1635

Prep Batch

Leach Batch

NANA

NA

200-30350

Prep Date

Leach Date

NA

NA


1197120 008 5 HFpH




mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





mL100gUnits

Solid

Dilution 10


Lab Sample ID

Client Matrix

Instrument ID

Lab File ID





Analysis Date

Analysis Batch

12082011 1930

Prep Batch

Leach Batch

NANA

NA

200-30372

Prep Date

Leach Date

NA

NA




12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



12222011Page 23 of 28

12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



12222011Page 24 of 28



SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





SDG Number WC02

Login Number 8445


Creator Holt Jamie


List Number 2








TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present




















SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports





SDG Number WC02

Login Number 8445


Creator Meyers Gary









TrueCOC is present



















Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports




Cover Title Page

Table of Contents

Report Narrative

Method Summary


Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results



Qc Reports



J8445-1 Std Tal L2 Final Report...The test results in this report relate only to sample(s) as...

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Transcript of J8445-1 Std Tal L2 Final Report...The test results in this report relate only to sample(s) as...