IPC Reg. POO21-02 - EPA · 2016. 9. 21. · Environmental Protection Agency Castlebar Regional...
Transcript of IPC Reg. POO21-02 - EPA · 2016. 9. 21. · Environmental Protection Agency Castlebar Regional...
Environmental Protection Agency Castlebar Regional Inspectorate Castlebar, CO, Mayo
IPC Reg. No. POO21-02
2 1 st July 201 6
Reference: Effluent Treatment Plant and Settling Pond Sludge Metal and Moisture Analysis 2016
Dear Sir/Madam,
In accordance with Schedule C.4 of POO21-02 please find enclosed metals and moisture results for sludge from the effluent treatment plant and settling pond 2018.
There are no licence limits for the annual metal analysis of the effluent treatment plant sludge and the settling pond sludge or for the annual moisture analysis.
Table I shows the trend 2014 to 2016 for Lead and Zinc which are the metals of significance for change. Both parameters are exceptionally low although showing variation from 2014 to 2018 is evident. There is a possible upward trend in the storm water pond sludge; however with only three years of data it is to early to be sure this is the case. This table will be maintained for future years to build up a longer time trend of data.
Organic matter and moisture content have not been trended in graph format as they are always stable year on year.
The full set of metal results for both sludges is included in Appendix A.
If you have any queries or if you require any additional information on any aspect of the enclosed, ptease do not hesitate to contact me.
Yours sincerely,
Brian Mallon Environmental Compliance Manager
Masonite Ireland Drumsna, Carrick on Shannon, Co. Leitrim, Republic of Ireland Phone: +353 77 9659500 9 Fax: +353 71 9659508
Registered in Ireland No. 229654 I V.A.T. No. lE8229654lJ Registered Office: 6 Fitzwilliarn Square, Dublin 2 Directors: J. Klngry (USA); C. Kearns (Irish)
www.masonife-europe.com
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POO21-02 Effluent Treatment Plant Sludge, Settling Pond Sludge Annual and Bi-Annual Analysis
in Accordance with Schedule C.4
Waste Sludge from Effluent Treatment Plant
Annual 2014 71.3 19,4
97.82 79,73
Parameter Waste Sludge from
Effluent Treatment Pla Annual 20 15
14.5 1.8
97.93 80,88
Zinc Lead Organic Matter Water Content
Waste Sludge from Settling Ponds Annual 2014
Waste Sludge from Settling Ponds Annual 201 5
Waste Sludge from Effluent Treatment Pla
Annual 201 6 76.4 15.5
97.78 79.85
Units -1 Parameter
Zinc Lead Organic Matter Water Content
Waste Sludge from Settling Ponds Annual 2016
96.82 99.53 91.44
111.3 10.3
48.35 95.6
Units
WWTP Sludge, Zinc & lead mg/kg 2014 - 2016 90 I 80 70 60
3 50 %
40 -Zinc
30 1 .1
k-7 -Lead
20
19 - -
0 I I 7
Annual 2014 Annual 2016 Annual 2015 Date
Settling Fond Sludge, Zinc I& Lead mg/kg 2014 - 2016
150
120 !
/ P- -Lead
30
0 -I I t
Annual 2014 Annual 2015 Annual 2016 Date
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Unit 35,
Monitoring and Testing Services
A copy of this certificate is available on w.fitrsd.le
Customer Brian Mallon Masonite Ireland Drumsna Catrtck -on- Shannon CO Leitrim Ireland
Custom er PO
Customer Ref
Ref 2 Ref 3
WWTP Sludge I w6/2016
Boyne Business Park. Drugheda, Co. Louth Iceland
Tal: +35341 8845440 Fa% t-353 41 58846171 Web w. f i tzsc i . ie email [email protected]
Lab Report Ref. No. 48301290103
Date ofRecelpt 1610612018
Sampled On 4 5/0612016
Date testing Commenced 1610612015
Recelved or Collected Condiflon on Recelpt Accepfable Date of Repart 11~0732016
Courier: An Post
Sample Type Other
Test Parameter % Dry Matter 70 Rldsture Content % Organic Matter Acetone (Solid) Acefonitrlle (Solid1 Aluminium SaIld(OES) Antimony Solid (OES) Arsenic S o l i (OES] Barlum %[id (OES) Bery[liurn Soltd (OES) Boron Solid (065) Cadmium Solid (DES) Chromium Solid (OES) Cobalt Solid (OES) ,, Copper SolFd (OES) Ethanol (Solid) Iron Solid (QES) Isopropyl Acetate (Soltd) Lead Solld (OES). Manganese Solid (OES) Mercury (Solid) Nickel Sdrd (OW) Satenium Solid (OES) Semi W C (Solid)
CERTlFlCATE OF ANALYSlS SOP 302 235 333 328 328 224 224 214 224 224
224 224 224 224 224
224 328
328 224 224 178 177 224 321
AnalyticaI Technique Drying Q 104 C Drying Q 104 C Furnace 500°C GC-FID GC-FID ICP-OES ICP-OES ICP-OES ICP-OES ICP-OES ICP-DES ICP-OES ICP-OES ICP-OES ICP-OES GC-FtD ICP-DES GC-FID ICP-OES ICP-OES ICPMS ICP-OES ICP-DES GCMS
Result 20.T5 79.85 97.78
' 4 0 <IO
2085266 4448.37 767.84 36059.1
< I O
19837.8 64.55 f726 66.89
5598.42 < I O
522577 4 0
15505. I n 7889
S I
1055.1 285. I 4 3.6352
Signed : A \ - = - Aoife Harmon - Technical Supervisor
Date : I I/U7/2O16
ACC. :Accredited Parameters by 150 17025:2005 PVL - Parametric Value Llmit as per EU (Drlnking water) Regulations (SI 122 2014) For bacterial analysis a reeult of p means none detected in volume examined All orgenic results are analysed a6 received and all results are corrected for dry weight at 104 G Results shall not be reproduced, mxcepi in full, without the approval of Fitz ScientifE Results contained in this repod relate only to the samples tesbd
** : The test result for this parameter' may be invaild as I t has exceeded the recommended holding time (RS EN IS0 566732012)
2802 (PI : Presumptive Results
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Unit 35,
Monitoring and Testing Servtces
A copy of this cerlificate is available on www.fitisci.ie
Boyne Business Park, Drogheda, Co. Louth Ireland
Tel: +353 41 9845440 Fax: +35341 9846171 Web: www.fitzsci.ie email infoafitzscik
Custom er Brian Mallon Masanite Ireland
Drumsna Carrick -on- Shannon
Lab Report Ref. No. 4830/290/03
Date of Receipt 16/06/2016
Sampled On 15/06/2016
Date Testing Commenced 16/06/2016
CO Leitrim Ireland
Customer PO Ctistoomer Ref WWTP Sludge
Ref 2 -l5/06/2016 Ref 3
Test Parameter Silver Solid (OES)
Tin Solid (OES) Total Heavy Metals (Solid) (OES) Vinyl Chloride (Solid) VOC (Solid) Zinc Solid (OES)
Received or Collected
Condition on Receipt Acceptable
Date ofReport f 1/07/2016
Sample Type Other
Courier: An Post
CERTIFlCA E OF ANAL. YSlS SOP Analytical Technique 224 ICP-OES 224 ICP-OES 0 Calculation
203 GCMS 203 GCMS 224 ICP-OES
Result < I O
4459.53 2991789
<1.00 2040.314 76375.8
Signed: Date : 11/07/2016 Aoife H a r t h ? % ? ~ v i s o r Acc : Accredited Parameters by IS0 17025:2005 PVL -Parametric Value Limit as per EU (Drinking water) Regulations (SI 122 2014) For bacterial analysis a result of 0 means none detected in volume examined All organic results are analysed as received and all results are corrected for dry weight at 104 C Results shall not be reproduced, except in full, without the approval of Fitz Scientific Results contained in this report relate only to the samples tested
2802 (P) : Presumptive Results
** : The test result for this parameter may be invalid as it has exceeded the recommended holding time (BS EN I S 0 5667-3:2012)
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Unit 35, Boyne Business Park, Dragheda, Co. Louth Ireland Tel: +353 41 9845440 Fax: +353 41 9846171 Web: w . f l l r sc i . i e ernail [email protected]
Monlforlng unci Testing Services
A copy of this certificaie is available on w. f i ksc i . ie
Lab Report Ref. No. 4830/290/04 Customer Brian Mallon Masonite Ireland Dale of Receipt q6/06/2016
Drumsna Sampled On 15/06120'I6
Carrick -on- Shannon Date Testing Commenced 16/06/2016
CO Leitrim Received or Collected Courier: An Post Ireland Condifton on Recelpf Acceptable
Date of Report 1 1 /07/2015 Customer PO
Customer R e f Stormpond Sludge Sample Type Other Ref2 l5/06/2016
I Ref3
Test Param eter % Dry Matter 96 Moisture Content % organic Matter Acetone (Solid) Acetonitrile (Solid) Aluminium Solid(OE5) Antimony Solid (OES) Arsenic Solid (OES) Barium Solid (OES) Beryllium Solid (OES) Boron Solid (OES) Cadmium Solid (OES) Chromium Solid (OES) Cobalt Solid (OES) Copper Solid (OES)
Iron Solid (OES) Isopropyl Acetate (Solid) Lead Solid (OESf Manganese Solid (OES) Mercury (Solid) Nickel Solid (OES) Selenium Solid (OES) Semi VOC (Solld)
' Ethanol (Sdid)
CERTfFlCAT€ OF ANALYSIS SOP 302 235 333 328 328 224 224 224 224 224 224 224 224 224 224 328 224 328 224 224 178 177 224 321
AnaIytical Technique Drying Q 104 C Drying @ 104 C Furnace 500'C GC-FID GC-RD ICP-OES ICP-OES ICP-OES ICP-OES ICP-OES ICP-OES ICP-OES ICP-OES [CP-OES ICP-OES G C F l O 1CP-OES GC-FID ICP-OES ICP-OES . ICPMS ,.
ICP-OES '
ICP-OES _,
GGMS
Signed: Aoife Harmon - Technical Supervisor
ResuIt 4.38
95.62 98 35
<I 0 < I O
242929 4899.54 790.71 6461.52
<I 0 135aa.2
Cl0 2007.68
4 0
5822.73 <10
537930 e10
10278 13452.7
<I t001.65 282.56 0.9314
Date : WQ7/2016
ACC. . Accredited Pararneiers by IS0 g7025:2005 PVL - Parametric Value Limit as per EU (Drinking water) Regulations (SI 122 2014) For bacterial analysis a result of 0 means none detected in volume examined All organic results are analysed a5 received and all results are corrected fur dry weight at 104 C Results shall not be reprodiiced, except In full, withaut the approval of Fitz Scientific Results contained in this report relate only to the samples tested
** : The test result for this parameter may be invalid as it has excaeded the recommended holding t h e (BS EN IS0 5667-3:2012)
(P) . Presumptive Results
U K A S
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t if ic
Monitoring and Tesffng Services
A copy af this certificate is available on w.f i tzsci . ie
Brian Mallon Lab Report Ref. No. 48301290104
Masonite Ireland Date of Recelpt 16/066016
Drumsna Sampled On 15/OUZOI 8
Carrick -on- Shannon Uafe Testing Commenced 16106/2016
CO Leitrim Received or Collected Courier: An Post Ireland Condiiion on Receipt Acceptable
Customer
Date of Report i1/07r2016
Sample Type Other
Custumer PO
Unit 35, Boyne Business Park, Drogheda, Co. Louth treland
Tel: +35341 9845440 Fax +35341 9846171 Web: ww.fitzsci.ie email [email protected]
Customer Ref Stormpond Sludge
Ref 2 15106/2016 Ref 3
CERTIFICATE OF ANALYSlS Test Parameter SOP Analytical Technique Silver Solid (OES) 224 ICP-OES Tin Solid (OES) 224 ICP-OES Total Heay Metals (Solid) (OES) 0 Calculation Vinyl Chloride (Solid) 203 GCMS VOC (Soltd) 203 GCMS Zinc Solid (OES) 224 ICP-OES
Result <I 0
1705.55 952046.8
<1.00 11.39
11’1297
I
t ”
I
Signed: AN-- Aoife Harmon - Technical Supervisor
Date : 7 1/O7/2016
Acc. : Accredited Paramebrs by IS0 17025;M05 PVL - Parametric Value Limit a6 per EU (Drinking water) Regulations (SI 122 2014) For bacterial analysis a result of 0 means n m e detected in volume examined All organic results are analysed as received and all results are carrecled for dry weight at 104 C
Results contained in this report relate only to the samples tested
** ; The test result for this parameter may be invalid as it has exceeded the recommended holding time (BS EN IS0 5687-3:2012)
Results shall not be reproduced. except in full, without the approval of Fitz Scientific 2802 (P) . Presumptive Results
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