Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME...
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![Page 1: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/1.jpg)
Infrared Beamline (EMIRA) at SESAMECurrent Status and New Updates
Ibraheem YOUSEFSESAME Synchrotron
Electro-Magnetic Infrared RAdiation
![Page 2: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/2.jpg)
Outlines Simulation and Design of the Infrared Beamline
at SESAME
a) The Infrared Source Characteristics for SESAMEb) Optical Design Simulationc) Beamline Designd) Experimental Station
The Progress in the IR beamline since the last SAC
![Page 3: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/3.jpg)
IR beamline will be one of the three Day-1 beamline at SESAME
IR beamline will be the first one fully designed at SESAME
Parameter
Description Value
E Electron energy 2.5 GeV
B Magnetic field 1.4554 T
R Bending radius 5.726 m
I Electron current 400 mA
L Straight section length 4.4 m
SESAME Storage Ring Parameters
![Page 4: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/4.jpg)
Collection and Design Details Infrared light will be collected from (ER +BM
sources)
Vertical collection angle = 15 mrad Horizontal collection angle = 39
mrad Collection geometry optimized using
SRW and Rays Tracing
![Page 5: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/5.jpg)
10 microns(Mid-IR )
100 microns(Far-IR)
Initial Wavefront ProfileCenter of aperture (optical axis)
Straight section axis
11 mrad
15 m
rad
15 m
rad
39 mrad
![Page 6: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/6.jpg)
Note: SOLEIL (black) 78mrad (H) x 20mrad (V); 500mA, DIAMOND (blue) and Australian Synchrotron (green).
Comparison with SOLEIL and other Synchrotrons
![Page 7: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/7.jpg)
Simulation and Design of the Infrared Beamline at SESAME
a) The Infrared Source Characteristics for SESAMEb) Optical Design Simulationc) Beamline Designd) Experimental Station
The Progress in the IR beamline since the last SAC
![Page 8: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/8.jpg)
Space and optimized distances
Tunnel wall
Bending M
agnet
TOP VIEWSide VIEW
![Page 9: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/9.jpg)
Source
M1 FlatM2 Toroid
M3 Flat
M4 Flat
Cylindrical mirrors (HFM)
Cylindrical mirror (VFM)
M7 A Flat
M7 B FlatM8 A Parabolic
M8 B Paraboli
c
Spectrometer 1
Spectrometer 2
Branch 1
Branch 2
Diamond window
Tunnel wall
Optical Layout
Schematic layout of optical path from the source inside the tunnel wall until the instruments
![Page 10: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/10.jpg)
Wavefront simulation using SRW and SpotX: 10
µm
![Page 11: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/11.jpg)
M4 Flat
Cylindrical mirrors (HFM)
Cylindrical mirror (VFM)
M7 A Flat
M7 B FlatM8 A Parabolic
M8 B Parabolic
Spectrometer 1
Spectrometer 2
Branch 1
Branch 2
Diamond window
Optical Layout after the first focus
![Page 12: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/12.jpg)
Branch 1 Branch 2
Profile at 8.7 m Profile at 8.7 m
Profile at 11.7 mProfile at 11.7 m
Beam Profile simulation
(20x30)mm²
(20x30)mm²
![Page 13: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/13.jpg)
Extraction mirror: the most critical aspect in
IR beamline
![Page 14: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/14.jpg)
Initial wavefront distribution of the 10 mm wavelength on first
mirror
Calculated power density on the same mirror
30
25
20
15
10
5
W/m
m2
-30mm -20 -10 0 10 20 30Horizontal Position
30
25
20
15
10
5
0
W/m
m2
-10mm 0 10Vertical Position
Heat load at first mirror: solution= slotted M1
![Page 15: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/15.jpg)
@ 2.05 meter from source
Heat load on first mirror (zoom)
![Page 16: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/16.jpg)
Proposed solution: A slot of 4 mm total (1.95 mrad)
Flux At slotted M1 in Photons/s./0.1% bw 6.93607e+13 Ph/s/0.1%bw
Flux Initial in Photons/s./0.1% bw 8.32854e+13 Ph/s/0.1%bw
17 % of the 10 µm wavelength removed
![Page 17: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/17.jpg)
M1 Holder Design
![Page 18: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/18.jpg)
Facing Deformation Due to Local Heat Load
Performed by J.P. Daguerre ( SOLEIL)
![Page 19: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/19.jpg)
Modified M1 holder Design
![Page 20: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/20.jpg)
M1 (Extraction Mirror) Manipulator1
2
4
5
3
(1) Step motor for mirror motion control, (2) Thermocouple feedthrough, (3) Motion swifts, (4) Translation mechanism, (5) Water cooled feedthrough.
![Page 21: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/21.jpg)
Simulation and Design of the Infrared Beamline at SESAME
a) The Infrared Source Characteristics for SESAMEb) Optical Design Simulationc) Beamline Designd) Experimental Station
The Progress in the IR beamline since the last SAC
![Page 22: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/22.jpg)
IR Beamline Front-end (M1 Chamber)
Modified dipole chamber
Gate valve between M1 and M2
Bending Magnet
M1 chamber
Absorber
![Page 23: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/23.jpg)
M2-M3 Chamber
Diamond window
Gate valve
M2-M3 chamber
M3
M2
Tunnel
tube
M3
M2
![Page 24: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/24.jpg)
CVD Diamond Window
Two gate-valves isolating the section upstream and downstream
Upstream gate valve
Downstream gate valve
CVD Diamond window welded on a double sided CF40 flange
Small ion pump
![Page 25: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/25.jpg)
Cylindrical mirrors chamber
Branch 2
Branch 1
Splitting mirror
Matching box
Ion pump
(M7-M8) B Chamber
(M7-M8) A Chamber
Coupling to the Spectrometer
![Page 26: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/26.jpg)
Simulation and Design of the Infrared Beamline at SESAME
a) The Infrared Source Characteristics for SESAMEb) Optical Design Simulationc) Beamline Designd) Experimental Station
The Progress in the IR beamline since the last SAC
![Page 27: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/27.jpg)
Experimental Station for the IR Beamline
Future
IR exp
erimenta
l
room
Exp
erim
enta
l
room
Sample prepara
tion
and stora
ge
Table and chairs
Computer controlled Microscope
![Page 28: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/28.jpg)
Simulation and Design of the Infrared Beamline at SESAME
a) The Infrared Source Characteristics for SESAMEb) Optical Design Simulationc) Beamline Designd) Experimental Station
The Progress in the IR beamline since the last SAC
![Page 29: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/29.jpg)
Performing FT-IR spectroscopy at SESAME….
FT-IR Microscope will be available for users between March and April 2013.
Thermo Scientific Nicolet FT-IR Microscope
Call for tender for the Infrared Microscope has been already submitted in 22 February 2012. (Expected date of delivery March 2013)
![Page 30: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/30.jpg)
Infrared Laboratory..
IR beamline
IR Lab
IR Lab
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Scientific opportunities
![Page 32: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/32.jpg)
News of the beamline on the website of SESAME
A description of the infrared beamline and its characteristics has been posted on the website of SESAME, the call for proposals will be announced on the website soon, depending on the expected date of having the microscope.
![Page 33: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/33.jpg)
TDR will be issued, and completed by June 2013
Technical design review
Following the Conceptual Design Report, a Technical Design Review (TDR) is in preparation and will be produced to provide comprehensive details of the beamline design and the management of the complete project around June 2013.
In preparation…
![Page 34: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/34.jpg)
Presentation and invited talks
Simulation and Design of an Infrared Beamline for SESAME: Applications in Microspectroscopy and Imaging. Synchrotron SOLEIL, France, 12 december 2011. (Thesis defence)
Synchrotron Infrared Microspectroscopy: Applications in Biomedical and environmental science, Faculty of Pharmacy, the university of Jordan, 15 April 2012 (Oral presentation)
The construction and Design of an Infrared Beamline at SESAME: Applications in infrared Microspectroscopy. Jordanian National Committee of SESAME JNCS, the university of Jordan, 3 May 2012 (Oral presentation)
Biomedical applications using Synchrotron Infrared Microspectroscopy, Cancer center, the university of Jordan, 15 June 2012 (Oral presentation)
![Page 35: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/35.jpg)
Paper published
![Page 36: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/36.jpg)
IAEA Fellowship at BESSY II
IRIS Beamline
The Mid-IR and far-IR spectra (2-5000 cm-1) of hydrate Nafion membranes of various Cation forms.
Contribute at the beamline activities, mainly a Local Contact
THz Microspectroscopy with coherent synchrotron radiation, micro-cell ellipsometry and imaging, the infrared beamline IRIS of the Helmholtz-Zentrum Berlin in Germany, Fellowship, Sep-Dec 2012
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Synchrotron Infrared Microscopy at SESAME
IR workshop -10th SESAME users meeting
8th November 2012
Electro-Mgnetic Infrared RAdiation
![Page 38: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/38.jpg)
IR workshop Program
![Page 39: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/39.jpg)
Round table Discussion..
1. How IR can benefit your studies?2. Need of training…3. Beside a microscope, what accessories you think
is needed (microtome, objectives etc..)?
4. Access to the microscope (help with writing proposals) two pages proposal local contact for advices external reviewers for proposal feasibility
5. Offer of Beamtime from the CLS
![Page 40: Infrared Beamline (EMIRA) at SESAME Current Status and New Updates Ibraheem YOUSEF SESAME Synchrotron ibraheem.yousef@sesame.org.jo Electro-Magnetic Infrared.](https://reader030.fdocuments.us/reader030/viewer/2022032516/56649c7b5503460f9492f896/html5/thumbnails/40.jpg)
Users recommendations…
1. Samples preparation room at SESAME equipped with:
- Vibratome - Microtome
2. Training workshop using the off-line microscope:
- Record infrared spectra - Data analysis
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Plan 2013
Announce on the website of SESAME the call of proposals beginning of January 2013
Jan 21st - Feb 21st : Training program at the infrared beamline UVSOR (Japanese facility)
March 1st - April 1st : Installation, testing and commissioning of the
IR Set-up April 2ndn - end of May: Exploitation and using the Set-up (Expert
European users) June 1st - Dec 1st : Submission the first draft of the TDR and welcome
users at the IR lab.
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AcknowledgmentsAcknowledgments
Paul Dumas (SMIS-SOLEIL)
Stéphane Lefrançois (SMIS –SOLEIL)
Thierry Moreno (Optics Group – SOLEIL)
Jean Pierre Daguerre (SOLEIL)
Hafeez Hoorani (SESAME)
Amor Nadji (SOLEIL)
Firas Makahleh (SESAME)
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Thank you for your attention