'IMRET ; 7 (Lausanne) : 2003.09.07-10' - GBV · 2008-07-15 · Scientific Programme LectureSession...

*&i«^" ^wmwm,

MM

^4,1

mmJ DECHEMA

'

j

Book of Abstracts

IMRET 7

7 International Conference on Microreaction Technology

September 7-10, 2003

Lausanne / Switzerland

r*JV>l_

Please vtelt mir arabsna mtpMSWWdaohsma ttodMaETT

V

Scientific Programme - Lecture Session

Sunday, 7 September 2003

15.00- 20.30 h Registration

18.15 h Opening

A. Renken, EPFL-SP-ISP, LGRC, Lausanne/CH

18.25 — 19.15 h Evening Lecture

Microreaction technology and the quest for innovative

sustainable developmentM. Matlosz, LSGC-ENSIC, Nancy/F

19.15 - 20.30 h Welcome Reception

Monday, 8 September 2003

08.25 h Welcome and Opening Address

A. Renken, EPFL-SB-ISP, Lausanne/CH

08.30 h Keynote Lecture

Highly selective reactions using microstructured reactors

J.-I. Yoshida, A. Nagaki, S. Suga, Kyoto University/J

Topic 3: Microstructured Devices as Tools in Chemical Research and Development

09.10 h New gas-liquid and gas-liquid-solid microreactors for the 3

investigation of catalysisC. de Bellefon, T. Lamouille, R. Abdallah, V. Meille, CNRS/ESCPE,

Lyon/F

09.30 h A microreactor-based system for the characterization of fast 7

exothermic reactions in liquid phaseM.-A. Schneider, F. Stoessel, EPFL, Lausanne/CH

09.50 h Electrochemical synthesis in micro reactors 10

P. Watts, University of Hull/UKjB_

__—-»"-«•-"»""——«

TECHNISCHE

INFORMATIONSQIBLIOTHEK

UNiVERSITATSBIBUOTHEKHANNOVER

10.10 h Coffee Break

10.40 h Poster Presentations

12.10 h Lunch

14.00 h Keynote Lecture13

Promising prospects for micro reaction technology

W. Ehrfeld, Ehrfeld Mikrotechnik AG, Wendelsheim/D

UB/TIB Hannover

125 334 540


Monday, 8 September 2003

Topic 2: Microstructured Devices for New Energy Systems

14.50 h MEMS-based components of a miniature fuel cell/fuel reformer 16

systemS. Tanaka. K.-B. Min, K.-S. Chang, D. Satoh, K. Yoshida,

M. Esashi, Tohoku University, Sendai/J

15.10 h Progress in developing a microchannel-based fuel processor 19

for automotive PEM fuel cell power systems

W.E. TeGrotenhuis, K.P. Brooks, J.M. Davis, CM. Fischer,

D.L. King, LR. Pederson, V.S. Stenkamp, R.S. Wegeng,

G.A. Whyatt, Pacific Northwest National Laboratory, Richland,

WA/USA

15.30 h Hydrogen production for fuel cell application in an autothermal 22

micro-channel reactor

P. Reuse, A. Renken, EPFL-LGRC, Lausanne/CH


14.50 h A novel high-throughput micro-reactor for screening of 25

catalyst coatings for highly exothermic reactions

M.J.M. Mies. E.V. Rebrov, M.H.J.M, de Croon, J.C. Schouten,

Eindhoven University of Technology/NL

15.10 h Microstructured reactors for heterogeneously catalysed gas 28

phase reaction: Influence of coating procedure on catalytic

acitivity and selectivityM. Bron, M. Lucas, S. Schimpf. P. Claus, TU Darmstadt/D

15.30 h Fast temperature cycling of CO oxidation in microstructure 30

devices

J.J. Brandner, K. Schubert, Karlsruhe Research Center/D; G. Emig,

M.A. Liauw, University of Erlangen/D


16.20 h Poster Presentations

19.00 h Poster Discussion (beer party)

22.00 h End


Tuesday, 9 September 2003

09.00 h Keynote Lecture 33

Micro reactors - Tools or toys for chemical and biochemical

processingS.J. Haswell, University of Hull/UK

Topic 1b: Microstructured Devices for Process Intensification - Unit Operations

09.40 h Construction, analysis and evaluation of a microfabricated 35

stripping column

S.H. Cypes, J.R. Engstrom, Cornell University, Ithaca, NY/USA

10.00 h Microextraction characteristics of the n-hexane/water/acetone- 38

systemD. Kirschneck, Microinnova, Graz/A; A. Wojik, R. Marr, TU Graz/A

10.20 h MicroChannel devices for the coalescence of dispersed 41

droplets produced for use in rapid extraction processes

Y. Okubo. M. Toma, H. Ueda, Sumitomo Chemical Co. Ltd.,

Osaka/J; T. Maki, K. Mae, Kyoto University/J


Topic 1a: Microstructured Devices for Process Intensification - Reactors

11.10 h Microreactor direct synthesis of hydrogen peroxide from hydro- 44

gen and oxygenT. Inoue, E.R. Murphy, M.A. Schmidt, K.F. Jensen, Massachusetts

Institute of Technology, Cambridge, MA/USA

11.30 h Microreaction engineering studies of the gas phase epoxidation 47

of propene by hydrogen peroxideE. Dietzsch, Th. Schwarz, D. H6nicke, TU Chemnitz/D; E. Klemm,

A. Lange de Oliveira, F. Becker, Degussa AG, Hanau/D

11.50 h DEMIS: Demonstrating the technical feasibility of heterogene- 49

ous gas phase catalysis in micro structured reactors on the

pilot scaleS. Schirrmeister, Uhde GmbH, Dortmund/D; G. Markowz, Degussa

AG, Hanau/D

12.10 h Novel microreactors for functional polymer beads 51

T. Nisisako, T. Torii, T. Higuchi, University of Tokyo/J

12.30 h Micro-structured string reactor for autothermal production of H2 54

C. Horny, L. Kiwi-Minsker, A. Renken, EPFL-LGRC, Lausanne/CH


Tuesday, 9 September 2003

12.50 h Lunch

14.20 h Keynote Lecture

Highthroughput experimentation in catalyst synthesis and

screeningW.H. Weinberg, Symyx Technologies, Santa Clara, CA/USA


15.10 h Digital reaction technology by micro segmented flow - compo- 57

nents, concepts and applicationsJ.M. Kohler, Th. Kirner, TU llmenau/D; Th. Henkel, Institute of Physi¬

cal High Technology, Jena/D; A. Grodrian, J. Metze, Institute for

Bioprocessing and Analytical Measurement Techniques, Heiligen-

stadt/D; M. Roth, K. Martin, Hans-Knoll-lnstitute, Jena/D

15.30 h A novel flow - microreactor for temperature-controlled protein 60

crystallizationM. Berg. M. Urban, M. Kielpinski, G. Mayer, Institute for Physical High

Technology, Jena/D; P. Miihlig, T. Klupsch, InstitutfurMolekulare

Biotechnologie e.V., Jena/D; R. Hilgenfeld, University of Liibeck/D

15.50 h Microchemical systems for colloidal materials synthesis and 62

separationS.A. Khan, K.F. Jensen, Massachusetts Institute of Technology,

Cambridge, MA/USA

Topic 5: Characterization and Simulation of Microstructured Devices and Systems

15.10 h Porous media simplified simulation of single and two phase flow 64

heat transfer in micro channel heat exchangersU. Imke, Karlsruhe Research Center/D

15.30 h Exploring the flow of two immiscible fluids in a square mini- 67

channel by direct numerical simulation

B.E. Ghidersa, M. Worner, D.G. Cacuci, Karlsruhe Research

Center/D

15.50 h Numbering-up of micro devices: A first liquid-flow splitting unit 71

R. Schenk, V. Hessel, C. Hofmann, J. Kiss, H. Lowe, F. Schonfeld,

Institut fur Mikrotechnik Mainz GmbH/D


*Abstract not received by the publication deadline


[Tuesday, 9 September 2003


16.40 h Design of an integrated microstructured reactor-heat exchanger: 74

A selective CO oxidation device for a portable fuel processor

E.R. Delsman, M.H.J.M. de Croon, J.C. Schouten, Eindhoven

University of Technology/NL; Ch. Hofmann, V. Cominos, Institut fur

Mikrotechnik Mainz GmbH/D; P.D. Cobden, Energy Research Centre

of the Netherlands, ECN, Petten/NL

17.00 h Catalytic performance of a CuO/ZnO/AI203 methanol steam 77

reforming catalyst coated on micro-channel surfaces

J. Bravo, A. Karim, A. Datye, University of New Mexico, Albuquerque,NM/USA

17.20 h A new proton-conducting porous silicon membrane for small 80

fuel cells

T. Pichonat, B. Gauthier-Manuel, D. Hauden, LPMO/CNRS,Besancon/F


16.40 h A model for predicting axial mixing during gas-liquid Taylor flow 83

in microreactors at low Peclet numbers

W. Salman, A. Gavriilidis, P. Angeli, University College London/UK

17.00 h Experimental approaches to a better understanding of mixing 86

efficiency of microfluidic devices

S. Panic, J. Antes, B. Richert, D. Boskovic, T. Tuercke, F. Schnuerer,E. Marioth, S. Loebbecke, Fraunhofer-lnstitute for Chemical Techno¬

logy, Pfinztal/D

17.20 h Numerical and experimental investigations on liquid mixing in 88

static micro mixers

M. Engler, N. Kockmann, P. Woias, Albert-Ludwigs-University of

Freiburg/D

17.40 h End of the Lecture Programme

20.00 h Conference Dinner at „Le Chalet Suisse"


Wednesday, 10 September 2003

Topic 6: Development, Manufacturing and Modularization of Microstructured Devices

and Systems

09.00 h Novel multifunctional microreaction unit for chemical 91

engineeringR. Keoschkerjan, M. Richter, Fraunhofer-lnstitute for Reliabilty and

Microinte-gration, Munich/D; D. Boscovic, F. Schnuerer,S. Loebbecke, Fraunhofer-lnstitute for Chemical Technology,Pfinztal/D

09.20 h A micro plasma reactor for fluorinated waste gas treatment 93

P. Sichler, L. Baars-Hibbe, C. Schrader, S. Buttgenbach,K.-H. Gericke, TU Braunschweig/D

09.40 h CYTOS® Continuous chemistry - a coherent chemical synthesis 96

technology from research through to productionT. Schwalbe, G. Wille, CPC-Cellular Process Chemistry Systems

GmbH, Frankfurt am Main/D


09.00 h Advantage on mixing in microreactors compared to mechanical 97

turbulent mixingH. Okamoto, Sumitomo Chemical Co., Ltd, Osaka/J and NagoyaInstitute of Technology/J; T. Ushiiima, Nagoya Institute of

Technology/J

09.20 h A coaxial multi-layered MicroTube device for micro-chemical 99

processingT. Hirano, H. Inukai, K. Hanaki, M.Ohshima, Kyoto University/J

09.40 h Static micro mixers for modular chip reactor arrangements in 101

two-step reactions and photochemical activated processes

T. Kirner, M. Gunther, K. Reinhackel, TU llmenau/D; J.M. Kohler, TU

llmenau and Institute for Physical High Technology, Jena/D; J. Albert,

G. Mayer, Institute for Physical High Technology, Jena/D




and Systems

10.30 h Enhanced mass transfer using a novel polymer/carrier 106

microreactor

H. Schonfeld, K. Hunger, U. Kunz, TU Clausthal-Zellerfeld/D;

R. Cecilia, University of Malaga/E

10.50 h Microfluidic lab-on-a-chip systems based on polymers - 109

Fabrication and applicationA.E. Guber, M. Heckele, D. Herrmann, A. Muslija, V. Saile,

L. Eichhorn, T. Gietzelt, W. Hoffmann, Karlsruhe Research Center/D;

P.C. Hauser, T. Tanyanyiwa, University of Basel/CH; A. Gerlach,

N. Gottschlich, G. Knebel, Greiner Bio-One, Frickenhausen/D

11.10 h Chip modules for generation and manipulation of fluid segments 112

for micro serial flow processes

T. Henkel, T. Bermig, M. Kieipinski, Institute for Physical High Tech¬

nology, Jena/D; A. Grodrian, J. Metze, Institute for Bioprocessing and

Analytical Measurement Techniques, Heilbad Heiligenstadt/D;J.M. Kohler, Institute for Physical High Technology, Jena and TU

llmenau/D


10.30 h New methods for increasing productivity by using microreactors 115

- planar pumping and alternating pumping typesH. Okamoto, T. Ushijima, Nagoya Institute of Technology/J

10.50 h g/l-Dispersion in interdigital micromixers with different mixing 117

chamber geometriesP. Lob, H. Pennemann, V. Hessel, Institut fur Mikrotechnik Mainz

GmbH/D

11.10 h Development of micromixer for rapid production of soap free 120

emulsion

K. Mae, T. Maki, I. Hasegawa, U. Eto, Y. Mizutani, Kyoto

University/J; N. Honda, Yamatake Corporation, Fujisawa/J

11.35 h Poster Awards - Closing remarks

12.00 h End of the Conference Programme

Scientific Programme - Poster Session

Topic 1a: Microstructured Devices for Process Intensification - Reactors -

1a.1 A gas microreactor: Application of electrostatic micromanipula- 123

tion techniqueT. Ito, T. Nisisako, T. Torii, T Higuchi, University of Tokyo/J

1a.2 One-step conversion of benzene to phenol using micro plasma 126

reactor

H. Sekiguchi, M. Ando, C. Kuroda, Tokyo Institute of Technology/J

1a.3 Development of multi-functional microstructured device for 127

inorganic fine particle crystallizationH. Nagasawa, Kyoto Laboratory/J; K. Mae, Kyoto University/J

1a.4 Micro reaction engineering studies of the hydroxylation of 130

benzene with nitrous oxide

U. Hiemer, T. Selvan, F. Scheffler, W. Schwieger, G. Emig,University of Erlangen/D; E. Klemm, University of Erlangen, TU

Chemnitz and Degussa AG, Hanau/D

1 a.5 Sol-gel Pt/Al203 catalyst film for microchannel reactors 132

H. Chen, X. Ouyang, W.C. Shin, S.M. Park, L. Bednarova,

R.S. Besser, W.Y. Lee, Stevens Institute of Technology, Hoboken,

NJ/USA

1a.6 Radical polymerization in a micro tube reactor 135

T. Iwasaki, Micro Chemical Process Technology Research Associati¬

on (MCPT), Kyoto/J; J.-l. Yoshida, Kyoto University/J

1a.7 Electrochemical microflow reactors for organic synthesis 138

S. Suga, M. Okajima, J.-l. Yoshida, Kyoto University/J

1a.8 Fabrication of palladium thin film for micro membrane chemical 141

reactor

S.H. Lee, R. Maeda, AIST Tsukuba/J; F. Mizukami, T. Hanaoka,

AIST Tohoku/J

1 a.9 A new microreactor for gas phase epoxidation of propene with 146

hydrogen peroxideT.M. Kruppa, F. Schuth, Max-Planck-lnstitut fur Kohlenforschung,Mulheim/D

1a. 10 Effect of downscaling on chemical reactions in microplasma 148

reactor

S. Mori, S. Akaji, M. Suzuki, Tokyo Institute of Technology/J

1 a. 11 Microsegmented electrodes for process intensification in 151

organic synthesisS. Rode, S. Altmeyer, M. Matlosz. CNRS-ENSIC, Nancy/F



1 b. 1 Normal and reduced gravity testing of microchannel phase 153

separators and condensers

W.E. TeGrotenhuis, V.S. Stenkamp, Pacific Northwest National

Laboratory, Richland, WA/USA

1 b.2 Design of microchannels for use in distillation devices 156

K.-l. Sotowa, K. Kusakabe, Kyushu University, Fukuoka/J

1b.3 New methods for increasing productivity by using microreac- 158

tors - development and fluidics of alternating pumping systemT. Ushijima, O. Kitoh, T. Fujiwara, Nagoya Institute of Technology/J;H. Okamoto, Sumitomo Chemical Co. Ltd., Osaka/J and NagoyaInstitute of Technoiogy/J


2.1 Hydrogen production in the reverse-flow autothermal catalytic 160

microreactor

T. Kikas, I. Bardenshteyn, C. Williamson, C. Ejimofor, A.G. Fedorov,

Woodruff School of Mechanical Engineering, Georgia Tech, Atlanta,

GA/USA; P. Puri, Air Products & Chemicals Inc., Allentown, PA/USA

2.2 Fuel processing microreactors for hydrogen production in mi- 163

cro fuel cell applicationsA.V. Pattekar, M.V. Kothare, Lehigh University, Bethlehem, PA/USA

2.3 Micro-structured-reactor-system for the steam reforming of 167

methanol

C. Cremers, Technical University Munchen/D; J. Dehlsen,

Bayrisches Zentrum fur Angewandte Energieforschung e.V.,

Garching/D; U. Stimming, TU Munchen/D und Bayrisches Zentrum

fur Angewandte Energieforschung e.V., Garching/D; P. Reuse,

A. Renken, LGRC-ISP-SB, Lausanne/CH; K. Haas-Santo, O. Gorke,

K. Schubert, Karlsruhe Research Center/D

2.4 Influence of CO2 and steam on high-flux H2 selective Pd 170

membranes manufactured with microsystem technologyF.C. Gielens, Eindhoven University of Technology/NL; H.D. Tong,

University of Twente, Enschede/NL; M.A.G. Vorstman,J.T.F. Keurentjes, Eindhoven University of Technoiogy/NL

2.5 The water gas shift reaction for automotive applications: 173

Preparation and testing of microstructured catalystsG. Germani, A.S. Quiney, A. van Veen, Y. Schuurman, C. Mirodatos,

CNRS, Villeurbanne/F; G. Kolb, Institut fur Mikrotechnik Mainz

GmbH/D



2.6 Hybrid micro membrane micro reactor for in situ pure hydrogen 176

productionS. Mukherjee, M.K. Hatalis, M.V. Kothare, Lehigh University, Bethle¬

hem, PA/USA

2.7 Design methodology for microreactor for preferential oxidation 179

ofCO

R.S. Besser, W.Y. Lee, P. Ho, X. Quyang, H. Chen, L. Bednarova,

Stevens Institute of Technology, Hoboken, NJ/USA

2.8 CO selective oxidation in microchannel reactor for PEM fuel cell 182

automotive applicationG. Chen, Q. Yuan, S. Li, Chinese Academy of Sciences, Dalian/PRC

2.9 Development of a new catalytic microreactor assembled with 185

noble carbon membrane catalyst and reactor elements for

methanol decompositionT. Maki, T. Ueyama, K. Mae, Kyoto University/J

2.10 Fuel processing using microstructured devices for hydrogen 188

productionP.M. Irving, T.M. Moeller, Q. Ming, InnovaTek Inc., Richland,

WA/USA

2.11 Methanol steam reforming in a microreactor using Cu/Ce02/y- 191

Al203 catalysts of different compositionY. Men, H. Gnaser, C. Ziegler, University of Kaiserslautern/D;R. Zapf, V. Hessel, Institut fur Mikrotechnik Mainz GmbH/D

2.12 Catalytic conversion of propane to hydrogen in microstructured 194

reactors

I. Aartun, A. Holmen, Norwegian University of Science and Techno¬

logy, Trondheim/N; T. Gjervan, H. Venvik, M. Fathi, SINTEF-Applied

Chemistry, Trondheim/N; O. Gorke, P. Pfeifer, K. Schubert,Karlsruhe Research Center/D

2.13 The thermodynamics of microsystem process networks 197

R.S. Wegeng, K.P. Brooks, W.E. TeGrotenhuis, G.A. Whyatt, Pacific

Northwest National Laboratory, Richland, WA/USA

2.14 Development of microchannel methanol steam reformer 199

G.-G. Park, D.J. Seo, S.-H. Park, Y.-G. Yoon, C.-S. Kim, W.L. Yoon,

Fuel Cell Research Center, Daejon/ROK

2.15 Micro-structured reactors for coupled steam-reforming and 202

catalytic combustion of methane

C. Cremers, M. Stummer, U. Stimming, J. Find, J.A. Lercher, TU

Munchen/D; O. Kurtz, K. Cramer, Atotech Deutschland GmbH,

Berlin/D; K. Haas-Santo, O. Gorke, K. Schubert, Karlsruhe Research

Center/D



3.1 The implementation of clinical diagnostic immunoassays using 205

micro reactors

P.A. Greenwood, V. Skelton, S. Haswell, Micro Chemical Systems

Ltd., Hull/UK; G. Greenway, University of Hull/UK

3.2 Remarkable micromixing effects in (4+2) cycloaddition using 208

N-acyliminium ion poolS. Suga, A. Nagaki, Y. Tsutsui, J.-l. Yoshida, Kyoto University/J

3.3 y-Ray-initiated dispersion polymerization of vinyl acetate in 211

microreactor

Z. Chang, G. Liu, Y. Tian, Z. Zhang, University of Science and

Technology of China, Hefei/PRC

3.4 Micron-size process systems for a production of recombinant 214

endonucleases of microquantitiesK. Ohtaguchi, K. Asami, Tokyo Institute of Technology/J

3.5 Direct monitoring of biochemical processes using 216

microstructured heat power detectors

J. Lerchner, A. Wolf, R. Huttl, G. Wolf, TU Bergakademie Freiberg/D

3.6 Synthesis of pigments in a three stage microreactor pilot plant - 219

an experimental reportCh. Wille, Th. Haller, H.-P. Gabski, H. Kim, L. Unverdorben,R. Winter, Clariant GmbH, Frankfurt am Main/D

3.7 Mesh multiphasic microreactor with integrated solid catalyst 221

N. Walker, P. Wenn, J. Shaw, V. Bains, Central Research Laborato¬

ries Limited, Hayes/UK

3.8 Process optimisation of a micro mixer based high-throughput 228

screening apparatus with respect to gas/liquid reactions

H. Pennemann, V. Hessel, Institut fur Mikrotechnik Mainz GmbH/D;

C. de Bellefon, CNRS/ESCPE Lyon, Villeurbanne/F

3.9 Feasibility study on concentration of slurry and classification of 231

contained particles by microchannel

S. Ookawara, R. Higashi, K. Ogawa; Tokyo Institute of Technology/J;D. Street, Fluent AP, Tokyo/J

3.10 Grignard exchange reactions using a micromixer 234

H. Wakami, Microchemical Process Technology Research Associa¬

tion, Kyoto/J; A. Naguki, S. Suga, J.-l. Yoshida, University of Kyoto/J;H. Mitsui, Nippon Shokubai Co. Ltd., Osaka/J

3.11 Microflow synthesis of alkynes by Sonogashira coupling 236

reaction

T. Fukuyama, S. Nishitani, R. Yamaura, M. Sato, I. Ryu, Osaka

Prefecture University/J

Scientific Programme -Poster Session


3.12 Flow-through electrochemistry in micro channels for standard 239

students experimentsM. Gunther, J.M. Kohler, TU llmenau/D

3.13 Separation of recombinant DNAse I under micron-size aqueous 242

polymer two-phase systemsK. Asami, K. Ohtaguchi, Tokyo Institute of Technology/J

3.14 Parallel and ultra-low-volume droplets operation for 244

chemical/biochemical screeningsM. Yamada, N.Y. Lee, M. Seki, University of Tokyo/J

3.15 Flow regime sensing in microchemical systems 247

T Kraus, A. Guenther, N. de Mas, M.A. Schmidt, K.F. Jensen,Massachusetts Institute of Technology, Cambridge, MA/USA

3.16 Integrated BioModules composed of microfluidics and digitally 250

controlled microelectrodes for processing biomoleculesP.F. Wagler, U. Tangen, T. Maeke, H.P. Mathis, J.S. McCaskill,Fraunhofer-Gesellschaft fur Biomolekulare Informationsverarbeitung,Sankt Augustin/D

3.17 Spatially resolved detection in miniaturized reaction diffusion 253

experiments in chip reactors for education

T. Kirner, P. Jaschinsky, J.M. Kohler, TU llmenau/D

3.18 Microfluidic system for a gene diagnosis 256

K. Yamashita, M. Miyazaki, H. Nakamura, Y. Yamaguchi, H. Maeda,

National Institute of Advanced Industrial Science and Technology,

Saga/J

3.19 Microfabricated flow-through reactor for DNA amplification - 258

towards in situ gene analysisT. Fukuba, T. Fujii, University of Tokyo/J; T. Naganuma, Hiroshima

University/J

3.20 Miniaturised chemistry platforms for drug discovery 261

E. Garcia-Egido, M. Femandez-Suarez, GSK Cambridge TechnologyCentre/UK; V. Spikmans, S.Y.F. Wong, B.H. Warrington,GlaxoSmithKline Pharmaceuticals, Harlow/UK


Topic 4: Nanomaterials and Microstructured Devices

4.1 Preparation of functionalised nanostructures on microchannel 263

surface and their usage for enzyme microreactors

M. Miyazaki, H. Shimizu, H. Maeda, Micro-space Chemistry Labora¬

tory, Saga/J; J. Kaneno, R. Kohama, K. Kanno, M. Fujii, Kinki

University, Fukuoka/J; M. Uehara, Kyushu University, Fukuoka/J

4.2 A new micro device assembled with same axle dual pipe for the 266

production of various fine particlesM. Takagi, T. Maki, M. Miyahara, K. Mae, Kyoto University/J

4.3 A simple modification method of inner wall of micro-reactor with 269

a self assembly of nano-particles and its application for a

photocatalytic reaction

H. Nakamura, S. Lee, H.Wang, M. Uehara, M. Miyazaki, H. Maeda,

AIST Saga/J

4.4 Generation of metal, micro- and nanoparticles in a micro flow 272

reactor

J. Wagner, T. Kirner, TU llmenau/D; G. Mayer, J. Albert, Institute for

Physical High Technology, Jena/D; J.M. Kohler, TU llmenau /D and

Institute for Physical High Technology, Jena/D

4.5 Porous alumina-supported catalyst coatings in steel 276

microchannels

R. Zapf, V. Hessel, G. Kolb, A. Ziogas, Institut fur Mikrotechnik Mainz

GmbH/D; K. Berresheim, H. Gnaser, Universitat Kaiserslautem/D

4.6 Investigations of microreaction technology for the production of 279

semicon ductor nanocrystalsJ. Kroon, C.-H. Chang, F. Nwachukwu, B.K. Paul, Oregon State

University, Corvallis, OR/USA


5.1 Reaction monitoring within micro reactors using an inverted 280

Raman microscopic spectrometerP.D. Fletcher, S.J. Haswell, X. Zhang, University of Hull/UK

5.2 Application of hot wire anemometry for flow characterization in 284

microstructured devices

P. Pfeifer, A. Wenka, K. Schubert, Karlsruhe Research Center/D;

M.A. Liauw, G. Emig, University of Erlangen/D

5.3 Improvement of surface compatibility of Si/glass chip thermo- 287

cyclers for application towards miniaturized flow-through PCR

J. Felbei, I. Bieber, Institute for Physical High Technology, Jena/D;

J.M. Kohler, TU llmenau/D



5.4 Three-dimensional visualization and simulation of laminar flow 290

behavior in a curved microchannel

H. Maeda, National Institute of Advanced Industrial Science and

Technology and Kyushu University/J; Y. Yamaguchi, K. Yamashita,H. Shimizu, National Institute of Advanced Industrial Science and

Technology, Kyushu/J; F. Takagi, Kinki University, Kyushu/J

5.5 Membrane microreactors: Modeling, design and operability 293

K.A. Alfadhel, M.V. Kothare, Lehigh University, Bethlehem, PA/USA

5.6 Numerical simulation of temperature distribution inside micro- 296

fabricated free flow electrophoresis module

H. Matsumoto, N. Komatsubara, C. Kuroda, Tokyo Institute of Tech¬

nology/J; N. Tajima, E. Shinohara, H. Suzuki, Olympus Optical Co.

Ltd., Tokyo/J

5.7 Characterisation of electrically powered micro heat exchangers 299

T. Henning, J.J. Brandner, K. Schubert, Karlsruhe Research

Center/D

5.8 Mixing and enzyme reactions in a microchannel packed with 302

glass beads

K. Kusakabe, K.-l. Sotowa, R. Miyoshi, Kyushu University, Fukuoka/J

5.9 Internal flow in a droplet formed in a microchannel contactor for 304

solvent extraction

K.-l. Sotowa, K. Kusakabe, H. Katsuragi, Kyushu University,

Fukuoka/J

5.10 Mixing in microreactors: Influence on yield for multiple 306

reactions

N. Aoki, K. Mae, S. Hasebe, Kyoto University/J

5.11 A mimaturised membrane reactor for highly exothermic 309

reactions

A. Schuster, R. Lakshmanan, J.W. Ponton, K. Sefiane, University of

Edinburgh/UK

5.12 Quantification of the heat transfer in boiling flow in microstruc- 310

tures by image analysisC. Ferret, L. Falk, CNRS-LSGC-ENSIC, Nancy/F; U. d'Ortona,

LMSNM-L3M-IMT La Jetee, Marseille/F

5.13 Modeling of electric-field driven transport processes in 312

microdevices for DNA analysis and immunoassaysM. Pribyl, P. Hasal, J. Kosek, D. Snita, M. Marek, Institute of

Chemical Technology, Prague/CZ



5.14 Characterization of residence time and residence time distribu- 315

tion in chip reactors with modular arrangements by integrated

optical micro devices

M. Gunther, J.M. Kohler, TU llmenau/D; T. Henkel, M. Kielpinski,

Institute for Physical High Technology, Jena/D

5.15 Application of the lattice Boltzmann methods to gaseous micro- 318

flows

A. Yamamoto, The Research Association of Micro Chemical Process

Technology (MCPT), Tokyo/J; M. Suzuki, Tokyo Institute of Techno¬

logy/J

5.16 Flow distribution in different microreactor scale-out geometries 321

and the effect of manufacturing tolerances and channel

blockingC. Amador, A. Gavriilidis, P. Angeli, University College London/UK

5.17 Gas-liquid flow and mass transfer in microchemical systems 324

A. Guenther, M. Jhunjhunwala, T. Kraus, N. de Mas, M.A. Schmidt,

K.F. Jensen, Massachusetts Institute of Technology, Cambridge,

MA/USA

5.18 Gas-phase mass-transfer measurements in a falling-film micro- 327

reactor

J.-M. Commenge, T. Pbein, X. Framboisier, S. Rode, M. Matlosz,

CNRS INPL, Groupe ENSIC, Nancy/F; V. Schanen, P. Pitiot, Rhodia,

Research Center of Lyon,Saint-Fons/F

5.19 Optimization of interdigital micromixers via analytical modeling 330

- exemplified with the SuperFocus mixer

K.S. Drese, Institut fur Mikrotechnik Mainz GmbH/D

5.20 CFD-based optimal design of manifold in plate-fin microdevices 334

O. Tonomura, S. Tanaka, M. Noda, M. Kano, S. Hasebe, I. Hashimo¬

to, Kyoto University/J

521 Microbubbie beam (MBB), a potential dispersion mechanism for337

multiphase gas-liquid microreactor systemsG.N. Doku, W.W. Verboom, D.N. Reinhoudt, A. van den Berg,

University of Twente, Enschede/NL



and Systems

6.1 Modular micro process engineering and applications 339

G. Rinke. M. Kraut, Karlsruhe Research Center/D; A. Muller, B. Horn,Institut fur Mikrotechnik Mainz GmbH/D; K. Jahnisch, lnstitut fur

Angewandte Chemie Berlin-Adlershof e.V./D; V. Grolier, V. Hillmann,

Fraunhofer-lnstitut fur Zuverlassigkeit und Mikrointegration, Berlin/D;

A. Bazzanella, DECHEMA e.V., Frankfurt am Main/D

62 Microfluidic device for portable oxygen generators 342

D.R. Graham, P.S. Puri, Air Products and Chemicals, Inc., Allentown,PA/USA

6.3 Thin, strong and defect free microfabricated palladium 343

composite membranes for H2 separationH.D. Tong, J.G.E. Gardeniers, H.V. Jansen, W. Nijdam,M.C. Elwenspoek, University of Twente, Enschede/NL; F.C. Gielens,

Eindhoven University of Technology/NL; C.J.M. van Rijn, AquamarijnMicro Filtration B.V., Hengelo/NL

6.4 Multi-phase oxidation reaction and ozonolysis in the limit of 346

explosion with multi-channel microreactors

M.A. Schmidt, K.F. Jensen, Massachusetts Institute of Technology,

Cambridge, MA/USA, Y. Wade, Massachusetts Institute of Techno¬

logy, Cambridge, MA/USA and Mitsubishi Chemical Corporation,Yokohama/J

6.5 Microstructuring of polymeric materials by excimer laser 349

ablation techniqueZ. Yu, C. Tao, Y. Bohua, Z. Tiechuan, Beijing Polytechnic

University/PRC

6.6 Development of a modular, software-supported microreaction 351

systemJ. Antes, H. Polifke, T. Tuercke, F. Schnuerer, S. Loebbecke, Fraun¬

hofer-lnstitute for Chemical Technology ICT, Pfinztal/D;

R. Lenk, T. Moritz, J. Adler, Fraunhofer Institute for Ceramic Techno¬

logies and Sintered Materials IKTS, Dresden/D; E. Bremus-

Koebberlin, P. Jacobs, A. Gillner, Fraunhofer Institute for Laser

Technology ILT, Aachen/D; A. von Klitzing, S. Lange, Fraunhofer

Institute for Production Technology IPT, Aachen/D; R. Keoschkerjan,

M. Richter, F. Wenninger, Fraunhofer Institute for Reliability and

Microintegration IZM-M, Munchen/D; G. Deerberg, J. Danzig,

J. Graen-Heedfeld, Fraunhofer Institute for Environmental, Safety

and Energy Technology UMSICHT, Oberhausen/D



and Systems

6.7 Development of an automated microreaction system with inte- 353

grated sensorics for process screening and productionJ. Antes, W. Ferstl, H. Krause, S. Loebbecke, Fraunhofer Institute for

Chemical Technology, Pfinztal/D; M. Grund, M. Haeberl,H. Muntermann, D. Schmalz, Merck KGaA, Darmstadt/D; J. Hassel,

A. Lohf, A. Steckenborn, Siemens AG, Nurnberg/D; T. Bayer,M. Kinzl, I. Leipprand, Siemens Axiva GmbH & Co KG, Frankfurt am

Main/D

6.8 Component development for a microchannel in situ propellant 355

production systemK.P. Brooks, S.D. Rassat, R.S. Wegeng, V.S. Stenkamp,W.E. TeGrotenhuis, Pacific Northwest National Laboratory, Richland,WA/USA

6.9 Modular microreaction system for organic syntheses 358

T. Bieber, W. Ehrfeld, F. Herbstritt, S. Kammermeier, O. Koch,

M. Kroschel, C. Raffa, G. Rimmel, A. Salmon, F. Schael,

K.-P. Schelhaas, Ehrfeld Mikrotechnik AG, Wendelsheim/D

6.10 Microproducts Breakthrough Institute established 360

D.L Brenchley, L.D. Kannberg, Pacific Northwest National Laborato¬

ry, Richland, WA/USA; K. Drost, Oregon State University, Corvallis,

OR/USA

'IMRET ; 7 (Lausanne) : 2003.09.07-10' - GBV · 2008-07-15 · Scientific Programme LectureSession...

Documents

Transcript of 'IMRET ; 7 (Lausanne) : 2003.09.07-10' - GBV · 2008-07-15 · Scientific Programme LectureSession...