ID 33341e TC 67/SC · Web viewa The minimum forward flow rate of 1 m3/min (6 bbl/min) is only for...

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved. Cementing Float Equipment API SPECIFICATION 10F FOURTH EDITION, [MONTH][YEAR] MONOGRAM PROGRAM EFFECTIVE DATE: [MONTH][DAY][YEAR]

Transcript of ID 33341e TC 67/SC · Web viewa The minimum forward flow rate of 1 m3/min (6 bbl/min) is only for...

Page 1: ID 33341e TC 67/SC · Web viewa The minimum forward flow rate of 1 m3/min (6 bbl/min) is only for use on float equipment for casing sizes 139.7 mm (5 ½ in.) and smaller. Larger sized

This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

Cementing Float EquipmentAPI SPECIFICATION 10FFOURTH EDITION, [MONTH][YEAR]

MONOGRAM PROGRAM EFFECTIVE DATE: [MONTH][DAY][YEAR]

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

Special Notes

API publications necessarily address problems of a general nature. With respect to particular circumstances, local, state, and federal laws and regulations should be reviewed.

Neither API nor any of API's employees, subcontractors, consultants, committees, or other assignees make any warranty or representation, either express or implied, with respect to the accuracy, completeness, or usefulness of the information contained herein, or assume any liability or responsibility for any use, or the results of such use, of any information or process disclosed in this publication. Neither API nor any of API's employees, subcontractors, consultants, or other assignees represent that use of this publication would not infringe upon privately owned rights.

API publications may be used by anyone desiring to do so. Every effort has been made by the Institute to assure the accuracy and reliability of the data contained in them; however, the Institute makes no representation, warranty, or guarantee in connection with this publication and hereby expressly disclaims any liability or responsibility for loss or damage resulting from its use or for the violation of any authorities having jurisdiction with which this publication may conflict.

API publications are published to facilitate the broad availability of proven, sound engineering and operating practices. These publications are not intended to obviate the need for applying sound engineering judgment regarding when and where these publications should be utilized. The formulation and publication of API publications is not intended in any way to inhibit anyone from using any other practices.

Any manufacturer marking equipment or materials in conformance with the marking requirements of an API standard is solely responsible for complying with all the applicable requirements of that standard. API does not represent, warrant, or guarantee that such products do in fact conform to the applicable API standard.

Classified areas may vary depending on the location, conditions, equipment, and substances involved in any given situation. Users of this specification should consult with the appropriate authorities having jurisdiction.

Users of this specification should not rely exclusively on the information contained in this document. Sound business, scientific, engineering, and safety judgment should be used in employing the information contained herein.

All rights reserved. No part of this work may be reproduced, translated, stored in a retrieval system, or transmitted by any means, electronic, mechanical, photocopying, recording, or otherwise, without prior written permission from the

publisher. Contact the Publisher, API Publishing Services, 1220 L Street, NW, Washington, DC 20005.

Copyright © 2015 American Petroleum Institute

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

Foreword

Nothing contained in any API publication is to be construed as granting any right, by implication or otherwise, for the manufacture, sale, or use of any method, apparatus, or product covered by letters patent. Neither should anything contained in the publication be construed as insuring anyone against liability for infringement of letters patent.

The verbal forms used to express the provisions in this recommended practice are as follows:

the term “shall” denotes a minimum requirement in order to conform to the specification;

the term “should” denotes a recommendation or that which is advised but not required in order to conform to the specification;

the term “may” is used to express permission or a provision that is optional; and

the term “can” is used to express possibility or capability.

This document was produced under API standardization procedures that ensure appropriate notification and participation in the developmental process and is designated as an API standard. Questions concerning the interpretation of the content of this publication or comments and questions concerning the procedures under which this publication was developed should be directed in writing to the Director of Standards, American Petroleum Institute, 1220 L Street, NW, Washington, DC 20005. Requests for permission to reproduce or translate all or any part of the material published herein should also be addressed to the director.

Generally, API standards are reviewed and revised, reaffirmed, or withdrawn at least every five years. A one-time extension of up to two years may be added to this review cycle. Status of the publication can be ascertained from the API Standards Department, telephone (202) 682-8000. A catalog of API publications and materials is published annually by API, 1220 L Street, NW, Washington, DC 20005.

Suggested revisions are invited and should be submitted to the Standards Department, API, 1220 L Street, NW, Washington, DC 20005, [email protected].

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

ContentsThe Table of Contents will be developed by API with the final page proofs.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

Cementing Float Equipment

1 Scope

1.1 Coverage

This specification provides minimum performance requirements, test procedures, and marking requirements for cementing float equipment that are deemed adequate for use in well construction in the oil and natural gas industries.

2 Normative References

The following referenced documents are indispensable for the application of this document. For undated references, the latest edition of the referenced document applies (including any addenda/errata). For dated references, only the edition cited applies. However, not all documents listed may apply to your specific needs. The body of the standard should be referred to for how these documents are specifically applied.

API Recommended Practice 13B-1, Recommended Practice for Field Testing Water-Based Drilling FluidsAPI Specification 13A, Specification for Drilling Fluid MaterialsAPI Specification Q1, Specification for Quality Management System Requirements for Manufacturing Organizations

for the Petroleum and Natural Gas Industry

For a list of other documents associated with this standard, see the Bibliography.

2.1 Use of SI and US Customary Units

This document contains SI and US customary oil field units. For the purposes of this document, the conversion between the systems is not exact and has been intentionally rounded to allow for ease of use in calibration and measurement.

3 Terms and Definitions

For the purposes of this document the following terms and definitions apply.

3.1autofill (auto-fill)A feature or design of float equipment check containing one or more valves that allow the flow check system to be temporarily disengaged so fluid may pass in either direction, for the primary purpose of automatic filling of the casing.

NOTE This action may reduce surge pressures in the well that may otherwise be present if float valves remained closed during running of the casing.

3.2float equipmentfloat equipment assemblyCasing accessories containing one or more check valves and become part of the lower section of a casing string for the purpose of preventing the reverse flow of cement once placed in a well bore annulus.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

3.3forward flow Process of flowing fluid in the direction the valve is designed to open.

3.4manufacturerThe firm, company, or corporation responsible for the manufacturing and marking of the product to warrant that the product conforms to the specification.

3.5reverse flowProcess of flowing fluid in the direction the float equipment valve is designed to close.

3.6U-tubingWhen a fluid in the annulus (area between the pipe and hole) at the end of displacement exerts a greater hydrostatic pressure due to its higher density than that of a fluid inside the pipe the heavier fluid flows from the annulus into the pipe until the hydrostatic pressures equalize. NOTE: U-tubing may occur in either direction during casing running and cementing due to hydrostatic imbalances.

4 Symbols and Abbreviations

AF Auto Fill

ASTM American Society for Testing and Materials

D Cumulative forward flow duration hours (table 1)

EN European Standard

HT High Temperature

HP High Pressure

ISO International Organization for Standardization

LP Low Pressure

NIST National Institute of Standards and Technology

P Pressure category for high pressure static test (table 5)

R Forward flow rate for flow durability testing (table 3)

T Temperature category for high temperature static test (table 4)

5 General Information

5.1 Functions of Cementing Float Equipment

The term “cementing float equipment” (float equipment) refers to one or more check valves incorporated into a well casing string that prevent fluid flow up the casing while allowing fluid flow down the casing. The primary purpose of

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

cementing float equipment is to prevent cement that has been placed in the casing/wellbore annulus from flowing up the casing (U-tubing). The float equipment itself will not prevent fluid flowing from the casing to the annulus.

Float equipment may be used for lessening the load on the drilling rig. Since float equipment blocks fluid flow up the casing, the buoyant force acting on casing reduces the load the rig is required to carry. This can be achieved through managing the hydrostatic pressure inside the casing relative to the hydrostatic pressure outside the casing, either through managing fluid height or fluid density.

Float equipment is also sometimes used as a device to assist in pressure testing of casing. This is normally done by landing a solid (top) cementing plug on the float equipment assembly which seals the casing at that point so that the pressure integrity of the casing can be tested. The plugs seal the casing at the float equipment point so that the pressure integrity of the casing above the floats may be tested. Pressure testing may be performed either before or after cement curing, at the discretion of the user.

Casing fill-up, also called “auto-fill”, float equipment is a special type of float equipment that allows the casing to fill from the bottom as the casing is run. This is desirable, in some cases, to help reduce pressure surges as the casing is lowered. Fill-up type float equipment may help ensure that the collapse pressure of the casing is not exceeded. Once the casing is run, the check valve mechanism of fill-up or auto-fill type float equipment is activated and the float equipment is converted to “standard” equipment. The conversion is normally executed by either pumping a surface-released ball through the equipment or by circulating above a predetermined rate.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

5.2 Performance of Cementing Float Equipment

There are a number of performance criteria that may be used to evaluate the suitability of a particular piece of float equipment for a given well. Float equipment should function after a fluid containing solids has been circulated through the equipment for a period of time. Flow period, flow rate, fluid temperature and fluid properties can impact the durability of the equipment. Float equipment should be capable of withstanding a differential pressure with the higher pressure being exerted from below the check valve, and capable of functioning at the temperature to which it is exposed. While this specification does not address pressure from above, the float equipment assembly should be capable of withstanding differential pressure being exerted from above the check valve.

The testing procedures consist of two parts: (1) flow durability and (2) static pressure and temperature testing. The flow durability tests entail installing the float equipment in a flow loop, and pumping a specified test fluid for a set amount of time. This is followed by applying a low backpressure to determine if the valve holds pressure. If casing fill up equipment is being evaluated, the equipment is subjected to reverse flow of fluids for a specified time and then converted prior to testing forward flow. Following the flow durability tests, the float equipment is mounted in an apparatus that allows the equipment to be heated to elevated temperature and backpressure applied to determine if the valve leaks. This standard does not address flow or testing with fluids in a gaseous state.

6 Calibration

6.1 General

This clause defines the requirements for calibration and verification of measurements by instruments and acquisition systems used in testing cementing float equipment. The term calibration is used to mean either calibration or verification according to the requirements of this specification. Prior to running a test, calibrations shall have been performed using instruments and devices certified and traceable to a national/international body such as NIST, DIN, ISO, or equivalent within the previous 12 months. Equipment calibrated to the requirements of this specification is considered to be accurate if calibration is within the specified limits. Calibration dates for instruments used in the tests of cementing float equipment shall be recorded on the test report.

6.2 Timers

Timers shall be accurate within ±5 seconds per hour and shall be verified over a period of no less than 12 minutes. Calibration may use the time signal from the NIST or similar web sites and radio stations. If not within required accuracy, the units shall be adjusted or replaced.

6.3 Flow Meter Systems

The flow meter system shall be capable of measuring the flow rate of the circulating test fluid being pumped through the float equipment in 15 L/min (0.1 bbl/min) or smaller increments and be accurate within ±15 L/min (±0.1 bbl/min) for the flow rate of the test being performed. Turbine type flow meters do not meet the requirements of this specification and are not acceptable for use when testing for the purpose of this specification.

6.4 Pressure Measuring Systems

Pressure measuring systems shall be readable to ±0.5 % of the test pressure range or better and cover the range to be measured. The system shall be able to maintain ±2 % accuracy of the test pressure range. Calibration shall be done at 25 %, 50 %, 75 %, and 100 % of test pressure, using a certified deadweight tester or master gauge to ±1 % of full range or minimum gauge increment, whichever is greater.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

6.5 Temperature Measuring Systems

Temperature measuring systems shall be accurate to within ±1 °C (±2 °F).

6.6 Data Acquisition System

Data acquisition may be by chart recorder or by electronic recording, such as computer data acquisition, or both. Data shall be collected at least every 60 seconds for the duration of the test.

6.7 Volumetric Glassware and Liquid Receivers

Calibration of pipettes, graduated cylinders and similar equipment is generally performed by the glassware supplier and can be part of the purchase specification. Users should obtain documented evidence of glassware calibration from the supplier. Calibration can be checked gravimetrically. Periodic re-calibration is not required.

6.8 Balances

Balances shall be accurate to±0.1 % of reading for measurements made at 10 g or greater up to the full scale of the balance. Balances shall be accurate to±1 % of reading for measurement made less than 10 g. Balances shall have two (2) decimal place precision at a minimum. Each range of a dual range balance shall be calibrated.

7 Flow Durability Time Categories

7.1 Categories

Four categories for flow durability testing are noted. The categories are shown in Table 1.

Table 1 — Categories of Flow Durability Tests for Float Equipment

CategoryCumulativea Forward Flow

Durationhours (-0/+15 min)

D8 8

D12 12

D24 24

D36 36

a Cumulative forward flow duration does not require continuous flow through the test equipment. For example, a 36-hour test may be conducted over several days.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

7.2 Auto-fill Equipment – Reverse Flow Test

For auto-fill equipment, prior to the conversion of the valve system, Table 2 lists the required reverse flow periods. The reverse flow rate shall be not less than 0.5 m3/min (3 bbl/min). The actual flow rate used for the reverse flow test shall be noted on the report form. This test shall be performed prior to the flow durability test. Following the reverse flow duration test, conversion of the valve per manufacturer’s recommendations shall be performed. See 9.2.2.

Table 2 — Reverse Flow Duration for Casing Fill-up EquipmentCategory Cumulativea Reverse Flow Duration

hours (-0/+15 min)AF 4 4AF 8 8

AF 12 12a Cumulative reverse flow duration does not require continuous flow through the test equipment. For example, a 12-hour test may be conducted over several days.

8 Flow Durability Rate Categories

Three categories for forward flow rate testing are noted. The categories are shown in Table 3.

Table 3 — Forward Flow Rates for Flow Durability TestingCategory Flow Ratea

m3/min (-0/+0.08) Flow Ratea

bbl/min (-0/+0.5)R6 1.0 6

R10 1.6 10R20 3.2 20

a The minimum forward flow rate of 1 m3/min (6 bbl/min) is only for use on float equipment for casing sizes 139.7 mm (5 ½ in.) and smaller. Larger sized equipment may be tested using either 1.6 m3/min or 3.2 m3/min (10 bbl/min or 20 bbl/min) for the duration of the flow test.

9 Apparatus and Materials

9.1 Flow Loop

9.1.1 General

The flow durability test system shall be capable of pumping the circulating test fluid through the float equipment at the circulation rate specified for the float equipment casing size range being tested within a tolerance of -0/+0.08 m3/min (-0/+0.5 bbl/min). Instrumentation shall be provided to measure and record the circulating test fluid flow rate and temperature over the duration of the test.

Figures 1 through 3 are example diagrams for flow loop for durability testing, indicate fluid flow directions and are illustrative only and not to scale. Other configurations are possible. The major components of the loop are the mud tank, piping network, pump, and instrumentation. These components are discussed in the following paragraphs.

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(1) Hopper (10) Agitator(2) High Volume Pump (11) Flow Meter(3) LP Safety Valve (12) Reverse / Bypass Flow Line(4) Pressure Transducers (13) Temperature Transducer(5) HP Large Line Valves (14) LP Sample Valve(6) HP Pump (15) HP Sample Valve(7) Test Piece (16) Bypass Valve(8) HP Safety Valve (17) Reverse Flow Valve(9) Tank

Figure 1 – Forward Flow

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

(1) Hopper (10) Agitator(2) High Volume Pump (11) Flow Meter(3) LP Safety Valve (12) Reverse / Bypass Flow Line(4) Pressure Transducers (13) Temperature Transducer(5) HP Large Line Valves (14) LP Sample Valve(6) HP Pump (15) HP Sample Valve(7) Test Piece (16) Bypass Valve(8) HP Safety Valve (17) Reverse Flow Valve(9) Tank

Figure 2 – Reverse Flow

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

(1) Hopper (10) Agitator(2) High Volume Pump (11) Flow Meter(3) LP Safety Valve (12) Reverse / Bypass Flow Line(4) Pressure Transducers (13) Temperature Transducer(5) HP Large Line Valves (14) LP Sample Valve(6) HP Pump (15) HP Sample Valve(7) Test Piece (16) Bypass Valve(8) HP Safety Valve (17) Reverse Flow Valve(9) Tank

Figure 3 – Backflow Pressure Testing

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

9.1.2 Piping Network

The piping network provides a conduit for the circulating test fluid to flow from the mud tank to the pump, through the float equipment, and back to mud tank. The inside diameter of the piping ahead of the float equipment shall be at least as large as the float valve inlet diameter for a distance of at least 3x the float valve inlet diameter. The inside diameter of the piping behind the float equipment shall be at least as large as the float valve outlet diameter for a distance of at least 2x the float valve outlet diameter.

Means shall be provided within the piping system to apply pressure for back pressure testing to at least 700 kPa ±170 kPa (100 psi ±25 psi) and to release pressure and to measure flow back or leakage across the float equipment. It should also provide a means of taking circulating test fluid samples.

Piping and valves shall be configured and verified such that the measured flow through the flow meter is measuring the flow through to the float equipment.

9.1.3 Pump System

A pump or combination of pumps shall be capable of pumping the circulating test fluid through the float equipment at the rates required for the category of the equipment being tested. An additional pump or pumps may be provided to apply the pressure required for backpressure testing and/or auto-fill float equipment conversion.

9.1.4 Instrumentation

The instrumentation for the flow loop shall include a flow meter, a temperature probe and pressure transducers. A data acquisition system shall be provided for recording the outputs from these devices during testing. Minimum data recording rates should be sufficient to provide an accurate record of each segment of the test.

NOTE Measurement of the back flow volume shall be via graduated cylinder or balance.

9.2 Circulating Test Fluid

9.2.1 The circulating test fluid shall be a water-based drilling fluid that has the following properties.

a) density: 1440 kg/m3 to 1500 kg/m3 (12.0 lb/gal to 12.5 lb/gal)

b) sand content: 2 % to 4 % volume fraction

The weighting material used in the test fluid shall be barite that meets the specifications of API 13A. The fluid properties shall be measured and calculated in accordance with API 13B-1. The sand used in the test fluid should be 212/75 micrometers (70/200 US mesh) silica sand.

9.2.2 The circulating fluid shall have the following properties at 50°C +/- 3 °C (120°F +/- 5 °F).

a) plastic viscosity: 10 mPas to 50 mPas (10 cP to 50 cP)

b) yield point: 2.4 Pa to 12.0 Pa (5 lbf/100 ft2 to 25 lbf/100 ft2)

c) 10 s gel strength:  1.9 Pa (> 4 lbf/100 ft2)

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10 Durability Test

10.1 Test Set-up10.1.1 Test Fluid

The test fluid shall be prepared in accordance with 8.2. The prepared fluid shall be circulated through the test loop (bypassing the float equipment) until the fluid properties have stabilized to within the requirements in 8.2 at 50 °C ±3 °C (120 °F ±5 °F). The fluid is considered stabilized when the rheological properties of two samples taken a minimum of 30 minutes apart have properties as described in 8.2.

NOTE There is no temperature requirement for the fluid in the test loop, only for the rheological testing of the sample of the fluid.

10.1.2 Equipment Orientation

The float equipment to be tested shall be mounted in the test section of a flow loop as described in 8.1. The orientation of the float equipment shall be within 10 degrees of horizontal. The equipment shall remain in the flow loop for the duration of the flow durability test.

For testing of flapper-type float equipment, the hinge of the flapper (or one of the flappers on double valve equipment) shall be within 45 degrees of the bottom (low side) so that closure is not assisted by gravity. Following the flow durability test, the hinge and spring should be inspected and the condition noted on the report form; with color photos taken before and after the test included in the report.

10.2 Procedure

10.2.1 Conventional (non-auto-fill) Float Equipment

10.2.1.1 Fluid Temperature

Fluid circulating temperature shall be recorded during the test.

10.2.1.2 Test Procedure

The following procedure shall be followed for testing conventional cementing float equipment.

a) Verify calibration documentation of instrumentation and measurement equipment in accordance with Section 5.

b) Prepare and/or validate the circulation test fluid in accordance with 8.2 and 9.1.1.

c) Install float equipment in flow loop oriented in accordance with 9.1.2.

d) Verify data collection in accordance with 5.6.

e) Begin circulation of test fluid at the desired rate to initiate the test.

f) The density and sand content of the circulation fluid shall be tested every 2 hrs (±15 min) and adjusted if necessary before continuing the test.

g) Circulate the test fluid through the float equipment for 4 hours (-0/+15 min).

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h) Stop circulation and perform a backflow test.

1) Apply 700 kPa ±170 kPa (100 psi ±25 psi) to the high pressure portion of the flow loop and attempt to backflow through the valve.

2) Release pressure upstream of the float equipment by opening a valve upstream of the float equipment, sufficiently large enough to bleed the upstream pressure to atmospheric pressure in no more than 15 sec, while maintaining the 700 kPa ±170 kPa (100 psi ±25 psi) for the duration of the test.

i) Measure backflow through valve.

During the test period, any flow through the float equipment is to be measured through the use of a graduated cylinder or alternately the fluid may be weighed and the weight converted to a volume.

i) Weight shall be measured to within ±0.5 g. Fluid relative density may be determined using a hydrometer, in accordance to API 13J.

1) If needed, a stabilization time of no more than 2 minutes is allowed prior to the start of the 3 minute test period.

2) The maximum allowable flow is 50 ml through the float equipment over the 3 minute test period.

3) If no stabilization period is required, the back pressure test requires a total of 3 minutes and the test shall be completed within 5 minutes.

j) In the event of failure of the valve to close.

1) If the valve will not close, attempt to achieve valve closure by flowing in a reverse direction against the valve for a maximum of 19 liters (5 gallons).

2) During this process, the pressure shall not exceed 870 kPa (125 psi).

3) After closure maintain 700 kPa ±170 kPa (100 psi ±25 psi) for the duration of the test.

4) Float equipment that does not pass this step after one attempt constitutes a failure of this test.

k) Restart circulation of the test fluid at the desired rate.

l) Repeat steps ‘f’ through ‘k’ for the total cumulative flow period of 8-, 12-, 24-, or 36-hrs, depending on the test category as shown in Table 1.

Following the final back pressure test, back pressures exceeding 700 kPa (100 psi) may be applied.

Equipment qualified for longer flow periods and a particular rate is considered qualified for the shorter time periods and equal or lower flow rates as well.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

At the end of the cumulative circulation period, remove the float equipment from the flow loop and visually inspect the equipment for any signs of abrasion or wear. Note any abnormalities. Photograph the top and bottom of the valve assembly and include photos in the testing report.

Proceed with the high-temperature/high-pressure test as outlined in Section 11 using the same piece of float equipment tested in the flow durability test.

10.2.2 Casing Fill-up Equipment (auto-fill equipment)

10.2.2.1 Conversion Testing

10.2.2.1.1 Circulation Rate

Following the requirements of 9.2.1.1 and 9.2.1.2 paragraphs a) - f), circulate in the reverse direction through the float equipment at not less than 0.5 m3/min (3 bbl/min) for reverse flow as shown in Table 2. Circulating temperature shall be as in 9.1.1.

10.2.2.1.2 Equipment Conversion

Convert the float equipment valve in accordance with the manufacturer’s recommendation. Record the pressure and/or rate required to activate the check valve.

Following completion of the equipment conversion, perform the durability test for regular float equipment as indicated in 9.2.1.

11 Static High-temperature/High-pressure Category Rating

Four categories for static high-temperature/high-pressure testing are noted. The categories for static high-temperature/high-pressure testing are shown in Tables 4 and 5.

Table 4 — Temperature Categories of Static High-temperature Tests

Category Temperaturea

°C (°F)

T200 93 (200)

T300 150 (300)

T350 177 (350)

T400 205 (400)

a Duration at temperature is no less than 8 continuous hours prior to testing to be held within ±5 % for the duration of the test.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

Table 5 –Pressure Categories of High-pressure Tests

Category Test Pressurea

kPa (psi)

P1.5 10,300 (1500)

P3 20,700 (3000)

P5 34,500 (5000)

P7.5 51,700 (7500)

a Control of pressure for this test shall be

-0/+ 2100 kPa (300 psi).

The pressure test category only evaluates the capability of the float equipment to withstand the noted differential pressure with a silicone-based oil (as per 11.1) during the test for specification purposes. The test does not investigate prevention of gas flow.

12 High-temperature/High-pressure Test Cell

12.1 Apparatus

A special test apparatus is recommended for applying temperature and pressure to float equipment as described in later clauses of this document. The apparatus shall be rated for safe operation at the temperatures and pressures required for the test category. Figure 4 is a schematic diagram of a typical apparatus for applying temperature and pressure to float equipment. Other apparatus and methods for applying temperature and pressure to float equipment are acceptable.

The test apparatus illustrated in Figure 4 consists of a chamber body with attached end caps to which the float equipment is attached. For pressure-testing float equipment, it may be more desirable to build several chambers rather than one large chamber. The chamber body, end caps, and support equipment shall be manufactured and assembled to withstand the anticipated pressures and stresses.

During pressure-temperature tests, the entire chamber (including the internal portion of the float equipment) shall be filled with a silicone-based oil (with a flash point above the test temperature) such that, to the extent practicable, air is removed from the chamber. The silicone-based oil shall not contain viscosity enhancers or added solids.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

Figure 4 — Typical Controlled Pressure-Temperature Test Cell

12.2 Test Cell Procedure

The following procedure shall be followed for the test cell.

a) Perform a flow durability test in accordance with Section 9.

b) Photograph the valve assembly (top and bottom) prior to the test.

1) Install the float equipment in the high-temperature/high-pressure test apparatus.

2) Differential pressure may be applied to the float equipment as needed during the 8-hr soak period.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

c) Depending on the test category, stabilize the temperature to 93°C (200 °F), 150 °C (300 °F), 177 °C (350 °F) or 205 °C (400 °F) according to Table 4, and maintain the test temperature within ±5 % for a period of no less than 8 hours.

d) Following the 8-hr soak period, increase differential pressure to the pressure of the test category within 30 minutes and maintain the pressure shown in Table 5. In the event of a mechanical or power failure, test may be resumed when interruption is remedied. If the interruption exceeds 1 hour, the test must be redone.

NOTE Stopping the pressure up test to investigate flow at lower pressures per step (e) is allowable. Following each successful test step, the time to increase the pressure to the next category as shown in Table 5 shall not exceed 5 minutes per 1,000 psi.

e) Monitor the flow through the float equipment.

1) If needed, a stabilization period of no more than 15 minutes is allowed prior to the test.

i) If no stabilization period is needed, the back pressure test requires a total of 15 minutes.

ii) The test shall be completed within 30 minutes.

2) The maximum allowable flow is 750 ml over the next 15 min test period.

3) During the test period, any flow through the float equipment is to be measured.

i) Weight shall be measured to within ±0.5 g.

ii) Flow through the equipment may be continuously weighed and recorded, and volume corrected to the fluid relative density at 20 °C (70 °F). Fluid relative density may be determined using a hydrometer, in accordance to API 13J.

Following the test, remove the float equipment from the test chamber and photograph the top and bottom of the

valve assembly and include photos in the testing report. Equipment qualified for a specific temperature and pressure category is considered qualified for lower categories.

13 Scaling of test results

The test results of one model number or part number of float equipment may be applied to other models or part numbers of float equipment with the following restrictions:

a) Physical tests are required to rate equipment smaller than or equal to 13-3/8”b) The allowable variation in size shall be within ± 5 % of the nominal body ID of the tested design, orc) For float equipment larger than 13-3/8”, the supplier/manufacturer shall determine the stresses and mode of stress in the components of both the tested product and the scaled product. The stresses in the scaled product components stated as a percentage of material yield, shall not exceed those of the tested model at the maximum rated loads for the product.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

d) The test results of one grade of float equipment may be applied only to other grades with equal or larger minimum yield stress.

14 Review Frequency

A Design and Development Review, Verification, and Validation according to API Specification Q1 shall be conducted at least once every five years.

15 Reporting of Results

A suggested form for reporting the results of the performance testing described in this specification is shown in Annex B.

While not part of this specification, it is recommended that manufacturers report the material properties of the body of the float equipment.

16 Evaluation of Elastomers in Non-aqueous Fluids

The manufacturers of float equipment shall develop the design, procurement, and quality control procedures for assuring the elastomers used in the manufacture of the float equipment are appropriate for use in non-aqueous fluids. The manufacturer shall be able to show elastomers chosen for use in float equipment have been chosen to be resistant to deterioration by non-aqueous fluids. Information on the resistance of the selected elastomer should be maintained by the manufacturer and available for review if requested.

Annex C contains information on qualification of elastomers for use in non-aqueous fluids.

17 Marking

These marking requirements apply to API Monogram Licensees wishing to mark their products with the API Monogram.

The following marking requirements shall be made in sequential order on the casing float equipment:

a) name or mark of the manufacturer;

b) “API Spec 10F”;

c) size in inches, followed by durability time (D) in hrs, flow rate (R) in bbl/min, temperature (T) in °F, pressure (P) in psi/1000; and reverse flow period (AF) in hours (where applicable to auto-fill equipment).

U.S. Customary Units shall be used, but metric SI may be used in addition.

The required markings shall be die-stamped, located at appropriate external location to view, and appropriately sized for legibility.

Other markings or information may also be used as agreed between the purchaser and manufacturer.

Example Marking

An example of marking for 7 in. float equipment that has been tested for a flow durability time of 24 hours at 10 bpm and subsequently tested at 300 °F to a pressure of 5000 psi:

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

[name or mark] API Spec 10F: 7 inch – D24 R10 T300 P5

As above, an example marking for float equipment that has auto-fill capabilities and was reverse flow tested for 12 hours per table 2 would read:

[name or mark] API Spec 10F: 7 inch – D24 R10 T300 P5 AF12

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

Annex A(informative)

API Monogram ProgramUse of the API Monogram by Licensees

A.1 Scope

A.1.1 Applicability

This annex is normative (mandatory) for products supplied bearing the API Monogram and manufactured at a facility licensed by API; for all other instances it is not applicable.

A.1.2 General

The API Monogram® is a registered certification mark owned by the American Petroleum Institute (API) and authorized for licensing by the API Board of Directors. Through the API Monogram Program, API licenses product manufacturers to apply the API Monogram to products which comply with product specifications and have been manufactured under a quality management system that meets the requirements of API Q1. API maintains a complete, searchable list of all Monogram licensees on the API Composite List website (www.api.org/compositelist).

The application of the API Monogram and license number on products constitutes a representation and warranty by the licensee to API and to purchasers of the products that, as of the date indicated, the products were manufactured under a quality management system conforming to the requirements of API Q1 and that the product conforms in every detail with the applicable standard(s) or product specification(s). API Monogram program licenses are issued only after an on-site audit has verified that an organization has implemented and continually maintained a quality management system that meets the requirements of API Q1 and that the resulting products satisfy the requirements of the applicable API product specification(s) and/or standard(s). Although any manufacturer may claim that its products meet API product requirements without monogramming them, only manufacturers with a license from API can apply the API Monogram to their products.

Together with the requirements of the API Monogram license agreement, this annex establishes the requirements for those organizations who wish to voluntarily obtain an API license to provide API monogrammed products that satisfy the requirements of the applicable API product specification(s) and/or standard(s) and API Monogram Program requirements.

For information on becoming an API Monogram Licensee, please contact API, Certification Programs, 1220 L Street, N. W., Washington, DC 20005 or call 202-682-8145 or by email at [email protected].

A.2 Normative References

In addition to the referenced standards listed earlier in this document, this annex references the following standard:

API Specification Q1, Specification for Quality Management System Requirements for Manufacturing Organizations for the Petroleum and Natural Gas Industry

For Licensees under the Monogram Program, the latest version of this document shall be used. The requirements identified therein are mandatory.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

A.3 API Monogram Program: Licensee Responsibilities

A.3.1 Monogram Program Requirements

For all organizations desiring to acquire and maintain a license to use the API Monogram, conformance with the following shall be required at all times:

a) the quality management system requirements of API Q1;

b) the API Monogram Program requirements of API Q1, Annex A;

c) the requirements contained in the API product specification(s) to which the organization is licensed; and

d) the requirements contained in the API Monogram Program License Agreement.

A.3.2 Control of the Application and Removal of the API Monogram

Each licensee shall control the application and removal of the API Monogram in accordance with the following:

a) products that do not conform to API specified requirements shall not bear the API Monogram;

b) each licensee shall develop and maintain an API Monogram marking procedure that documents the marking/monogramming requirements specified by this annex and any applicable API product specification(s) and/or standard(s). The marking procedure shall:

1) define the authority responsible for application and removal of the API Monogram and license number;

2) define the method(s) used to apply the Monogram and license number;

3) identify the location on the product where the API Monogram and license number are to be applied;

4) require the application of the date of manufacture of the product in conjunction with the use of the API Monogram and license number;

5) require that the date of manufacture, at a minimum, be two digits representing the month and two digits representing the year (e.g. 05-12 for May 2012) unless otherwise stipulated in the applicable API product specification(s) or standard(s); and

6) define the application of all other required API product specification(s) and/or standard(s) marking requirements.

c) only an API licensee shall apply the API Monogram and its designated license number to API monogrammable products;

d) the API Monogram and license number, when issued, are site-specific and subsequently the API Monogram shall only be applied at that site specific licensed facility location; and

e) the API Monogram may be applied at any time appropriate during the production process but shall be removed in accordance with the licensee’s API Monogram marking procedure if the product is subsequently found to be out of conformance with any of the requirements of the applicable API product specification(s) and/or standard(s) and API Monogram Program.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

For certain manufacturing processes or types of products, alternative API Monogram marking procedures may be acceptable. Requirements for alternative API Monogram marking are detailed in the, API Monogram Program Alternative Marking of Products License Agreement, available on the API Monogram Program website at http://www.api.org/alternative-marking.

A.3.3 Design and Design Documentation

Each licensee and/or applicant for licensing shall maintain current design documentation as identified in API Q1 for all of the applicable products that fall under the scope of each Monogram license. The design document information shall provide objective evidence that the product design meets the requirements of the applicable and most current API product specification(s) and/or standard(s). The design documentation shall be made available during API audits of the facility.

In specific instances, the exclusion of design activities is allowed under the Monogram Program, as detailed in Advisory # 6, available on API Monogram Program website at http://www.api.org/advisories.

A.3.4 Manufacturing Capability

The API Monogram Program is designed to identify facilities that have demonstrated the ability to manufacture equipment that conforms to API specifications and/or standards. API may refuse initial licensing or suspend current licensing based on a facility’s level of manufacturing capability. If API determines that an additional review is warranted, API may perform additional audits (at the organization’s expense) of any subcontractors to ensure their conformance with the requirements of the applicable API product specification(s) and/or standard(s).

A.3.5 Use of the API Monogram in Advertising

An API Monogram licensee shall not use the API Monogram and/or license number on letterheads, buildings or other structures, websites or in any advertising without an express statement of fact describing the scope of Licensee’s authorization (license number and product specification). The Licensee should contact API for guidance on the use of the API Monogram other than on products.

A.4 Product Marking Requirements

A.4.1 General

These marking requirements shall apply only to those API Licensees wishing to mark applicable products in conjunction with the requirements of the API Monogram Program.

A.4.2 Product Specification Identification

Manufacturers shall mark products as specified by the applicable API specifications or standards. Marking shall include reference to the applicable API specification and/or standard. Unless otherwise specified, reference to the API specifications and/or standards shall be, as a minimum, “API [Document Number]” (e.g., API 6A, or API 600). Unless otherwise specified, when space allows, the marking may include use of “Spec” or “Std”, as applicable (e.g., API Spec 6A or API Std 600).

A.4.3 Units

Products shall be marked with units as specified in the API specification and/or standard. If not specified, equipment shall be marked with U.S. Customary (USC) units. Use of dual units [USC units and metric (SI) units] may be acceptable, if such units are allowed by the applicable product specification and/or standard.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

A.4.4 Nameplates

Nameplates, when applicable, shall be made of a corrosion-resistant material unless otherwise specified by the API specification and/or standard. Nameplate shall be located as specified by the API specification and/or standard. If the location is not specified, then the licensee shall develop and maintain a procedure detailing the location to which the nameplate shall be applied. Nameplates may be attached at any time during the manufacturing process.

The API Monogram and license number shall be marked on the nameplate, in addition to the other product marking requirements specified by the applicable product specification and/or standard.

A.4.5 License Number

The API Monogram license number shall not be used unless it is marked in conjunction with the API Monogram. The license number shall be used in close proximity to the API Monogram.

A.5 API Monogram Program: Nonconformance Reporting

API solicits information on products that are found to be nonconforming with API specified requirements, as well as field failures (or malfunctions), which are judged to be caused by either specification and/or standard deficiencies or nonconformities against API specified requirements. Customers are requested to report to API all problems with API monogrammed products. A nonconformance may be reported using the API Nonconformance Reporting System available at http://compositelist.api.org/ncr.asp x .

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

Annex B(informative)

Results of Performance Tests on Cementing Float Equipment

I. General Information

Manufacturer__________________________________________________________________________________Type of float equipment tested____________________________________________________________________Size of float equipment tested ____________________________________________________________________Model number of float equipment tested ____________________________________________________________Location of plant where float equipment manufactured _________________________________________________Location of testing facility________________________________________________________________________Date of float equipment manufacture _______________________________________________________________Valve description ______________________________________________________________________________Valve material _________________________________________________________________________________Description of float equipment body________________________________________________________________

Calibration Dates:

Timer(s)_________________________________ Flow Meter System________________________________

Pressure Measurement System______________ Temperature Measurement_________________________

Data Acquisition Check_____________________ Balances________________________________________

II. Flow Durability Testing

Dates of testing _______________________________________________________________________________

Reverse flow duration (bbl/min) 4_______________ 8 ______________ 12 _____________ (auto-fill only)

Flow durability rate (bbl/min): 6_______________ 10 _____________ 20 _____________

Flow durability time (hrs): 8_______________ 12 _____________ 24 _____________ 36 _____________

Type of pump used for circulation _________________________________________________________________

Average sand concentration during test _____________________________________________________________

If pass, maximum backflow volume for closure _______________________________________________________

If pass, maximum rate for closure _________________________________________________________________

If pass, maximum test pressure used _______________________________________________________________

If fail, total duration until failure ____________________________________________________________________

If casing fill-up equipment, reverse-flow pressure drop across valve _______________________________________

If casing fill-up equipment, pressure and/or rate to activate ______________________________________________

Description of valve after test _____________________________________________________________________

____________________________________________________________________________________________

Attach photos of equipment before and after testing.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

III. High-Temperature/High-Pressure Testing

Dates of testing _______________________________________________________________________________

HT/HP test Pressure (psi) 1500________3000____________5000 ___________7500__________

HT/HP Test Temperature (°F) 200______ 300 ____________ 350____________ 400 __________

Type of pressure application: Internal only ________________ Internal and External ________________

If pass, maximum test pressure used _______________________________________________________________

If fail, maximum test pressure achieved _____________________________________________________________

Description of valve after test _____________________________________________________________________

Attach photos of equipment before and after testing.

Final API Test Category:

AF _________________

D___________________

R___________________

T___________________

P___________________

Signature __________________________ Title __________________________________

Name ____________________________ Contact Information ______________________

Date Signed _______________________

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

Annex C(informative)

Evaluation of Elastomers in Non-aqueous Fluids

Float equipment may be exposed to water based or non-aqueous based fluids during normal use in oil and gas wells. This specification evaluates durability through testing with a water based fluid which is chosen for safety, low environmental impact, and to represent a fluid with high abrasive characteristics. High pressure static testing utilizes a silicone oil as the heating media which is chosen for safety and heat transfer capabilities.

Qualification of elastomers should include exposure of the elastomer at elevated temperature and pressure to selected test fluids. The fluids used for elastomer testing are not necessarily intended to mimic non-aqueous fluids used in well operations, but may represent standard fluids for use in specification testing.

Example methods for testing elastomers are found in ASTM D471.

Information on the resistance of the selected elastomer should be maintained by the manufacturer and available for review if requested.

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This document is not an API Standard; it is under consideration within an API technical committee but has not received all approvals required to become an API Standard. It shall not be reproduced or circulated or quoted, in whole or in part, outside of API committee activities except with the approval of the Chairman of the committee having jurisdiction and staff of the API Standards Dept. Copyright API. All rights reserved.

Bibliography

[1] API Recommended Practice 10B-2, Recommended Practice for Testing Well Cements

[2] API Recommended Practice 13B-1, Recommended Practice for Field Testing Water-Based Drilling Fluids

[3] API Recommended Practice 13B-2, Standard Procedure for Field Testing Oil-based Drilling Fluids

[4] API Recommended Practice 13J, Testing of Heavy Brines

[5] ASTM D471, Standard Test Method for Rubber Property—Effect of Liquids