ICP Test Report Certification Packet/media/electronics_technical/...2010/06/07 · + 886 (02)2299...

ICP Test Report Certification Packet

Company name : Littelfuse, Inc.

Product Series: ML_MLE NRX1 Series

Product #: ML_MLE NRX1 Series

Issue Date: June 7, 2010

It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive

2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for

packing/packaging materials, and for additives and the like in the manufacturing processes.

In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used

for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing

processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts

This document covers the ML_MLE NRX1 Series RoHS-Compliant series products

manufactured by Littelfuse, Inc.

＜ Raw Materials Used

Please see Table 1

(2) The ICP data on all measurable substances

Please see appropriate pages as identifed in Table 1

Remarks：

With exemption RoHS 5. Lead in glass of cathode ray tubes, electronic components and fluorescent tubes.

1Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part

Number Raw Material Description Page(s) 1 N/A Body – Zinc Oxide 3-9

2 N/A Glass Flux in Metal Oxide Layer 10-16

3 N/A Internal Electrode – Conductive Paste 17-22

4 N/A Internal Electrode – Conductive Paste

(Halogens) 23-26

5 N/A Additives 27-33

6 N/A End Termination Paste 34-46

7 N/A Nickel electrode 47-56

8 N/A Tin Electrode 57-62

9 N/A Overcoat Solder Resist 63-70

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SGS Taiwan Ltd.台灣檢驗科技股份有限公司 Chemical-Taipei 33 WuChyuan Road, Wuku Industrial Zone, Taipei County, Taiwan /台北縣五股工業區五權路33號 t + 886 (02)2299 3279 f + 886 (02)2299 3237 www.sgs.com

Member of the SGS Group (SGS SA)

Unless otherwise stated the results shown in this test report refer only to the sample(s) tested. This test report cannot be reproduced, except in full, without prior written permission of the Company.除非另有說明，此報告結果僅對測試之樣品負責。本報告未經本公司書面許可，不可部分複製。This Test Report is issued by the Company under its General Conditions of Service printed overleaf or available on request and accessible at http://www.sgs.com/terms_and_conditions.htm. Attention is drawn to the limitation of liability, indemnification and jurisdiction issues defined therein. Any holder of this Test Report is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law.

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1) yzXY~ÚÛÜ�ÝoÞ��ßàáâãäå��%&��æçè / These samples weredissolved totally by pre-conditioning method according to below flow chart. Cr6+ test method excluded

2) %&éêkëìí / Name of the person who made measurement: Climbgreat Yang3) %&îïékðñ / Name of the person in charge of measurement: Troy Chang

��òÙ / Sample Material óFôõö÷ / Digestion Acid

ø , ù, ú, ûü /Steel, copper, aluminum, solder

ýþ, �ô, �ô, �±ô, �Eþ /Aqua regia, HNO3, HCl, HF, H2O2

�� / Glass �ô,�±ô / HNO3/HF� , , , �� /Gold, platinum, palladium, ceramic

ýþ / Aqua regia

/ Silver �ô / HNO3

�� / Plastic �ô, �Eþ, �ô, �ô /H2SO4, H2O2, HNO3, HCl

�� / Others ��ô�àáâã /Any acid to total digestion

âõ / Solution

�� Cr6+� Pb�� Cd

¡¢7£¤¥¦§¨©ª« / ICP-AES

�z��~òÙ�X��~ô��ó

F(eY�{ ) / Acid digestion by suitableacid depended on different samplematerial (as below table)

!" / Filtration

#$ / Residue

1) %&'� /Alkali Fusion

2) �ôâã /HCl to dissolve

%&��() / Sample Measurement

*+�,Î�� / Cutting Preparation

�ô/�ô/�±ô~-.óF /Microwave digestion with

HNO3/HCl/HF

�/��01��óF23 / Heat toappropriatetemperature to extract

456!"�� /Cool, filter digestatethrough filter

��§»78» / Adddiphenyl-carbazide forcolor development

X9ç©-:s©©ª«Þ)%��âõ;540 nm ~<n1 /measure theabsorbance at 540 nmby UV-VIS

=��)óFõ / Addappropriate amount ofdigestion reagent

� Hg




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��ÃÂÚÛÜ / PBB/PBDE analytical FLOW CHART1) %&éêk>?@ / Name of the person who made measurement: Roman Wong2) %&îïékABC / Name of the person in charge of measurement: Shinjyh ChenDE%&ÛF / First testing process

GHIJ¬ÛF / Optional screen process

cdÛF / Confirmation process

Sample / ��

Issue Report KL'(

Sample extraction ��23/Soxhlet method MN23�

Analysis by GC/MS /×ØÁÂÙª«ÃÂ

Filter / 23õ!"

Sample pretreatment / ��OPQ

Screen analysis / DJÃÂ

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®¯ÃÂÚÛÜ Analytical flow chart of halogen content

/ /Sample pretreatment/separation

/Weighting and putting sample in cell

/Oxygen Bomb Combustion / Absorption

/Analysis was performed by IC

/Dilution to fixed volume

1) %&éêkAVW / Name of the person who made measurement: Alan Chen2) %&îïékðñ / Name of the person in charge of measurement: Troy Chang




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============================================================================================

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The following sample(s) was/were submitted and identified by/on behalf of the client as:

Sample Receiving Date

Testing Period

VALE INCO ELECTROLYTIC NICKEL R ROUNDSSample Description

200 Bay Street, Royal Bank Plaza, Suite 1600, South Tower, P.O. Box 70, Toronto, Ontario, M5J 2K2, Canada

No. : CE/2010/22806 Date : 2010/02/24 Page : 1 of 10Test Report��Vale Inco Limited

2010/2/10

2010/2/10 TO 2010/02/24

Please refer to next page(s).Test Result(s)

Conclusion Based upon the performed tests by submitted samples, the test results of Cadmium,Lead, Mercury, Hexavalent Chromium Cr(VI), PBBs and PBDEs comply with the limits ofRoHS Directive 2002/95/EC and its subsequent amendments.




Test Result(s)

Result

NO.1

mg/kg With reference to IEC 62321: 2008 andperformed by ICP-AES.

2 n.d. 100


2 n.d. 1000


2 n.d. 1000

** With reference to IEC 62321: 2008 andperformed by Spot test / boiling waterextraction (UV-VIS) Method. (See Note7)

0.02mg/kgwith 50 cm²

surfacearea

Negative #

** Analysis was performed by FTIR andFLAME Test.

- Negative -

mg/kg With reference to US EPA 3540C:1996 method for PFOS Content.Analysis was performed by LC/MS.

10 n.d. -

mg/kg With reference to US EPA 3540C:1996 method for PFOA Content.Analysis was performed by LC/MS.

10 n.d. -

mg/kg With reference to BS EN 14582:2007.Analysis was performed by IC.

50 n.d. -


50 n.d. -


50 n.d. -


50 n.d. -

Limit

Cadmium (Cd)

Lead (Pb)

Test Item (s):

Perfluorooctane sulfonates(PFOS)PFOS – AcidPFOS – Metal SaltPFOS – Amide

PFOA (CAS No.: 000335-67-1)

Halogen-Fluorine (F) (CAS No.:014762-94-8)

Halogen-Chlorine (Cl) (CAS No.:022537-15-1)

Halogen-Bromine (Br) (CAS No.:010097-32-2)

MDLMethodUnit

Halogen

SILVER COLORED METAL

Halogen-Iodine (I) (CAS No.:014362-44-8)


Test Report No. : CE/2010/22806 Date : 2010/02/24 Page : 2 of 10

Vale Inco Limited ��

PART NAME NO.1

Mercury (Hg)

Hexavalent Chromium Cr(VI) bySpot test / boiling water extraction

PVC




Result

NO.1

- n.d. 1000

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

- n.d. 1000

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

5 n.d. -

PFOS Reference Information : Directive 2006/122/EC(1) May not be placed on the market or used as a substance or constituent of preparations in a concentration equal to orhigher than 0.005 % by mass.(2) May not be placed on the market in semi-finished products or articles, or parts thereof, if the concentration of PFOSis equal to or higher than 0.1 % by mass calculated with reference to the mass of structurally or microstructurallydistinct parts that contain PFOS or, for textiles or other coated materials, if the amount of PFOS is equal to or higher

than 1µg/m2 of the coated material.

Heptabromobiphenyl

Octabromobiphenyl

Nonabromobiphenyl

Decabromobiphenyl

Sum of PBBs

Monobromobiphenyl

Dibromobiphenyl

Tribromobiphenyl

Tetrabromobiphenyl

Pentabromobiphenyl

Hexabromobiphenyl

Tribromodiphenyl ether

Nonabromodiphenyl ether

Decabromodiphenyl ether

Heptabromodiphenyl ether

Sum of PBDEs

Monobromodiphenyl ether

Dibromodiphenyl ether

Tetrabromodiphenyl ether

Pentabromodiphenyl ether

Hexabromodiphenyl ether

Test Report

Octabromodiphenyl ether

No. : CE/2010/22806 Date : 2010/02/24 Page : 3 of 10



Test Item (s): Unit Method MDL Limit

mg/kgWith reference to IEC 62321: 2008 andperformed by GC/MS.




1.

2.

3.

4.

5.

6.

7.

8.

Note

Boiling-water-extraction:

# = Positive indicates the presence of Cr(VI) on the tested areas and result be regarded as not comply with RoHS

requirement.

Negative indicates the absence of Cr(VI) on the tested areas and result be regarded as comply with RoHS

requirement.

Negative = Undetectable / Positive = Detectable

n.d. = Not Detected




mg/kg = ppm 0.1wt% = 1000ppm

Negative = Absence of Cr(VI) coating / surface layer; Positive = Presence of Cr(VI) coating / surface layer;(The tested sample should be further verified by boiling-water-extraction method if the spot test result cannot beconfirmed.)

Spot-test:

MDL = Method Detection Limit

" - " = Not Regulated

** = Qualitative analysis (No Unit)

Negative = Absence of Cr(VI) coating / surface layer; Positive = Presence of Cr(VI) coating / surface layer;The detected concentration in boiling-water-extraction solution is equal or greater than 0.02 mg/kg with 50 cm²sample surface area.




No. : CE/2010/22806 Date : 2010/02/24 Page : 5 of 10

��


Test ReportVale Inco Limited

1) These samples were dissolved totally by pre-conditioning method according to below flow chart.

Cr6+ test method excluded

2) Name of the person who made measurement: Climbgreat Yang

3) Name of the person in charge of measurement: Troy Chang

Cr6

Sample Material Digestion Acid

Steel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2

Glass HNO3/HF

Gold, platinum, palladium, ceramic Aqua regia

Silver HNO3

Plastic H2SO4, H2O2, HNO3, HCl

Others Any acid to total digestion

Pb Cd

Solution

ICP-AES

Acid digestion by suitable aciddepended on different samplematerial (as below table)

Filtration

Residue

1) Alkali Fusion2) HCl to dissolve

Sample Measurement

Cutting / Preparation

Microwave digestion with

HNO3/HCl/HF

Heat to appropriate

temperature to extract

Cool, filter digestate

through filter

Add diphenyl-carbazide for

color development

measure the absorbance

at 540 nm by UV-VIS

Add appropriate amount of

digestion reagent

Hg







Analysis flow chart for determination of PVC in material

Sample pre-treatment

Flame test

Sample analyzed by FTIR

Check wave-number of C-Cl bonding

Data

1) Name of the person who made measurement: Eva Chao

2) Name of the person in charge of measurement: Shinjyh Chen







Analytical flow chart of Soxhlet extraction (LC/MS) procedure

�Test Items: PFOS/PFOA�Benzotriazole

1) Name of the person who made measurement: Lydia Fu


Sample pretreatment/separation

Sample extraction by soxhlet method

Concentrate/Dilute Extracted solution

Analysis was performed by LC/MS

Data







Analytical flow chart of halogen content

Sample pretreatment / Separation

Weighting and putting sample in cell

Oxygen Bomb Combustion / Absorption

Analysis was performed by IC

Dilution to fixed volume

1) Name of the person who made measurement: Rita Chen

2) Name of the person in charge of measurement: Troy Chang







PBB/PBDE analytical FLOW CHART

First testing process

Optional screen process

Confirmation process

Sample

Screen analysis

Issue Report

Sample pretreatment

Sample extraction/Soxhlet method

Concentrate/DiluteExtracted solution

Analysis by GC/MS

Filter

1) Name of the person who made measurement: Roman Wong





** End of Report **




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€ {..& + r*4t rt tf &}f,,i] . / sithre fe rence to lnc 62321: 2008 andper fo rned 6y ICP- , !S ,

1 0 0

JE / L€ad (Pb) 44 lEE 6232r, 2oost-A. rraA,t*?.t{,-i+&#*,*f,t*,Fl. / si thi e f€ rencc to lF I : .62321t 2OOa anaper fo rned by ICP AES.

2 t 0 0 0

*. / Nercury (Hs) +4rFE 6232r, 2oosr;!, ,(6,tgjA€f&+*41*,*A*jr1. / withre fe rence to IEC 62321: 2008 andperfo.ned by ICP-AIS.

1 0 0 0

xf i l& / Hexavalent chroniun cr(v t ) byalkal ine €xt ract i on

ns/kg 4-+rF/c 6232r. 2008tii, ,)(w-vrs*i l j . / { i l h re fe r€nce to tEc 62321:2008 a .d per fo rmed by UV-VIS.

2 1 0 0 0

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4{fr/t*r/qfreai&&'619Micf owave digestjon with

HNO3/HCI/HF

6r"itljFtL* /Addapprcpiate amount ofdigeslion reagent

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Gmperature to extract

ftlse* /

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t , a, h.. ka tGold, platinum, pa sdium, ceramic

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*-r".*h*ilt+&*en tAnalysia flow chart for delemination of pVC in material

]J ,lA-,(..f : {tiift /Nameofthe person wfio made me€surement Eva Cheo2) ,lllAEt/.: t*#? / Name ofthe person in charge of measurement: StrinJyrr Cnen

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chad of halogen contentmade measuremenlt AIan Chencnarge of measuremenl: Troy Chang

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t &$*t t *#*e+fi.)natr / PBB/PBDE anatyticat FLOWGHART1) ,Xli{,,,l.A : tiqd / Name oflhe person who made measurement: Roftan Wong2) ,4dtA*l:&Sf / Name of the person in charge of meesurement Stri4yn C'trenvt)K)a'lA4ZE / First testing process _____,'5#,l4SAt:F / Optjonat screen process __...--,,Eiti:.$ / Q6n1116696n process -._>

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