ICP Test Report Certification Packet/media/electronics... · 2 . Table 1: List of Raw Materials...

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: 5x20 Cartridge Fuse Product #: 219XA Series Issue Date: March 13, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC/ 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

< Global EHS Engineer>

(1) Parts, sub-materials and unit parts This document covers the 5x20 Fuse Rohs-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 C910541 Cap 3-6 2 C909542/C909543 Body 7-11 3 11-0595 (082xxx-001) Element – 99% Sn Plated Cu 12-15 4 687xxx-001 Element - Sn Plated Ag Cu 16-20 5 YTW102 (692535-002) Solder Wire 21-25

6 934-077/C030208 Overcap (Cap base and plating) Overcap (Wire base and plating) 26-29

7 648901 Yarn 30-36 8 648115 Yarn 37-43 9 648150 Yarn 44-50 10 425900 Ink-Orange 51-61 11 425901 Ink-Red 62-72 12 425902 Ink-Black 73-83 13 425904 Ink-Blue 84-94 14 425906 Ink-Brown 95-105 15 425907 Ink-Green 106-116 16 425909 Ink-Grey 117-127

Customer: Suzhou FuHong Electronjc InduslrialCo., Lld.

Addres!: NO.89 WEIDU ROAD, WANGTINGTOWN, XIANGCHENG DlsTRlCT, SUZHOU, CHINA

Report on ths submitred s.mplesald to be

S.mple name: CoppeJ,shell

Mod€h/

Item/LoiNo.:/

Metar lal : / ,

Buyer: / ,

Suppli€r: /

Samplo recaivsd d.te: Ocl. 08. 2012

Testins period: Ffom oct os, 20!€ 1o'O4r'10, 2012 . . ,,' \ l '

E9S!.s-Ecs!ed9!f

NO.: 4002R12100802+1 R02

As specified by dient, to determine ihe Lead, cadmlun,

accordance with Dircctive 2002/95/EC {RoHS).

AOV"BPFS,U

LiTingting, Maggie

Chemic€l Test Direcror

TEST REPORTDare: ocr.10, 2012

Mercury & Hexavalent Chrcmium content in the submitled sample in

Ylan Qi, lrickey

Ec!!!s-ee$9!.:Testing ltem Measunng instrumeni I\4QL

Lead (Pb) IEC 62321: 2008, s€ction 9 ICP€ES 2-'nglkg

Cadmium (cd) |EC62321: 2008, seclion I ICP-OES 2 mg/kg

[4ercury (Hg) lEc 62321 2008, seclron 7 tcP-oEs 2 mg/kg

Chromum (Cr\rl) IEC 62321 2008 Annex B 0.02m9/k9'

Ieqr 0.02 mg/kg reE|s to the MQL ofsample extfaction liquid

SsElcge!:-when tesled as speci{i€d the submitted sample complied with the requirements of commission Decision ol 18 Aug 2005

amending Directjve 2002/95/Ec noiilied under document 2005/618/Ec

ILS, PLEASE REFER TOTHE FOLLOWNG PAGE(S)***

signed lor and on behalfof

Shenzhen AOV Tesling Technology Co., Ltd, Kunshan Brcncn

caeateaaer: /blfil **n*"oor, We-r k] n ooo,',*or44.

SI tEN2HEN AOV Tf S I ING T€CHNOI ,O6Y CO. , I "TO.KUNSNAN BRANCTI /// \ Noll ne, J a,t 7tt) 9€'t'o

AOV'*F#S,[

NO.: 4002R121008024-1 R02

TEST REPORTOate :Od.10,2012

Content i|retb.r sulit€le). \ .

Cooling the vess€|, nlter;washed and

Rlled 10 the mark with distill€d wat€r.

The sample is digested in the

microwave oven following a specific

decomposrlon program

Test the sample solution and lhe 0.02

ng/kg standard solltion by uv-vls.F;;1.-

SH€NZH€N AOV TESTITIG lCCINOLOGY CO.,LTD.KUNSIIAN BSANCH( :

H o t l r n e'tL)0 700 8600

1. To Determiney'.ead, C€dmium Contenli (Metal subslrate)

I*redby (y'a04*

Add ihe digestion solulioni the

vessel is heated unlil the sampleWeigh ihe sample into

Add HrOruntilthe sample is clear

To Dete

Weigh ihe sample

Cooling the vessel, tiltei washed and

filled lothe maiK wilh dislilled water.Tested by lcP-oES

Chromium Contenl (boiling- wat€F €xtlaclion): ([4etal Eubstrate)

Remove lhe sample, and cool

the beak€r to room temperature,

and do the color reaction

Take the (50i5) cm,

sample in the beaker.Heat 50 mL of Olwater in

the be6ker to boiling for 1o

nov'Bpf,F,il

NO.: 4002R121008024-1R02

5. To oetemine Hexavalenl Chromium Contonl in_ .. -i\

: va'hu't'

TEST REPORTDaie: Ocl.10, 2012

colorless and colored chromate coating on metats: iPtating)

5.2 Boiling-wateF enradion

lfthe lest result is positive,

the sample is considered to

have hexavalent chmmium

Place 1-5

and the 0.02 mg/kg

Boiling- water- extraotionprocedu€ shall be used to

lflhee is interference or it is hard to decide

whetherlhe sample have lhe hexavalent

Remove the sample, and coolthe beaker lo room temperalure,and do lhe color reaction

sample in the beaker.Heat 50 mlof Dlwaier in the

beaker to boiling for 10 min

Test tne sample solution and lhe 0.02mg/kg standad solulion by UV-VIS.

Sample Delcriptlon:

Code Sample Descndion

1-1 Substrate

Plating

Te3t R63ulb:

Unit RoHS Limit

Lead (Pb) msfts 1000 N.D. 1 0

Cadmium (Cd) mg/K9 100 N.D. N.O.Merorry (Hg) ms/Kg 1000 N.D, N.D.

Chromium {Crl,ll) m9/kg 1000 Negative Negative

s8€NZh€N AOV T€SrtNG TECHNOlOSY CO,,tTD,TUNSHAI!ARANCH H ot l in e.100 700 B6a0

,.r

nov'F"Ff"qn

No.: A002R1210o602:L1 R02

neoatve.,-"The te8t is bas€d on lhe followins d!!{mplifi:

maybe cannot stand lor the physical lrdh 6t s€r

TEST REPORT

Coppershell

-The new RoHS dircclive 2011/6tEU, on Jul. 21, 2011 come into forc€, on Jan. 03, 2013lhe formal implementation, Direclive

2002r'95/EC ahall be repealed simultaneously.

Sp€cimens, which r€Slested lo detemine Lead, Cadmium and Mercury Content, have been dissolved completely,-mg/kg=ppm ,-N.D.=not

i",, ,,,,( The iested sample result is uncertain or

SH€NZII AOVTIST|n|G TECHNOIOCV CO.,ITD.KUNSHAN AFANCH H ot l in e400 /00 8600

Test Report No. CANEC1207912202 Date:26 Jun 2012 Page 1 of 5

XIAMEN LICHUN ELECTRONIC ELEMENT CO.,LTD

42 2XINGLIN WEST RD.,361O22,JIMEI DISTRICT,XIA['EN,,FUJIAN,P.R.C

Test Results :

Conclusion :

The following s€mple(s) was^/vere submitted and identified on behalf of the clients as : BOSI GLASS TUBE

SGS Job No. : XM13901119EC-XM

Date of Sample Received : 18 Jun 2012

Testing Period : 18 Jun 2012 '26 Jun 2012

Test Requested : Selected test(s) as requested by client.

Test Method : Please fefer to next page(s)

Please refer to next page(s).

Based on the oeformed tests on submitted samples, the results of Lead,Mercury, Cadmium. Hexavalent chromium, Polybrominated biphenyls (PBB),

Polybrominated diphenyl ethers (PBDE) comply with the limits as s€t by RoHSDireclive 2011/65/EU Annex ll; recasting 2002/95/EC.

Signed for and on behalf ofscs-csrc Ltd.

Luc'y WuApproved Signatory

ii:trii";df#i*iil:i":#i'Tiiiqili'",'iq;l[i+ill$]*Ji":ia"#r.:ilr.'""?ir"'i1i':"'"#-

1g(drRods&$rdorgn Edu{t1drlUDtd(FlilkEoldogtu 510€63

+q.r'rijSt&^4t8fl*dfl6gls3€ i!fr:s10663r 66-201s2r56666 ' 136-20 e07t 13r is6xre,5s5s5 r €6-20)s2o75us e 3$sd1*e4tm

Momb€.ollhdscs GrouP {scs sA)

Test Report No. CANEC1207912202 oate:26 Jun 2012 Page 2 of5

Test Results :

Test Part Descriotion :

Spodmen No. SGS Sample lD O€6cfiption1 CAN12-079122.002 Transparent glass tube

Remarks :(1) 1 mg/kg = 1 PPm = 0 0001%

(2) MDL = Method Detection Limit

(3) ND = Not Detected ( < l\rDL )(4) "-" = Not Regulated

RoHS Dlr€div6 2()l 1/85/EU

Test Method : with reference to lEc 62321:2008(1) Detemination ofCadmium by ICP-OES.(2) Determination of Lead by ICP-OES(3) Determination of lrerdiry by ICP-OES.(4) Determination of Hexavalent Chromium by Colorimetdc Method using lJV_Vis'

(5) Determination of PBBS / PBDES content by GC-MS

Test ltem{s)C.dmium (Cd)Lead (Pb)

[,lercury (Hg)

Hexavalent Chromium (crvl)

Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiPhenylPentabromobiPhenylHexabromobiphenylHeptabromobiphenylOctabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobromodiphenyl ether

Limit Unit MDL

100 mS/kS 2

1.000 mg/kg 2

1,000 mg/kg 2

1,000 mg/kg 2

1,000 mg/kg- mdkg 5, mg/kg 5- mdkS 5- mg/kg 5- mg/kg 5- mo/kg 5- mg/kg 5- ms/kg 5- msiks 5- mg/lq 5

1,000 mg/kg- mdkg 5

'Sield&rrdrrituttbt@rln{qtc.@d0dotdsotu 510663

F!.Ttir'F8fii*&4fl+ffl**1$q 8r:5i0663

9uNDN DNDN DNDNDNDNDNDNDNDNDNDNDNDNDND

r i!5-08a56656 I l!6_20)32075113 Mc03{tl.n

l is-Oe156s6 1(!F20)3207s113 ' {sch*€is3s

Memb€rorlh€ scs Gmw {sossA}

illi:tr1y:lr:i;i:1":'"sf;:H:l'1i5$i{,ff;1ti!.'di$:::fiirtriii,i"s.ii:'#ii#;*,r#S{s.,#lU-"tii}HilffiiltliFtldlffi"{;;tu'i d-k-.;ehd6.,"h.

Test Report

Test ltem(sl

Dibrcmodiphenyl elhet

Tribromodiphenyl ether

Tetrabromodiphenyl ether

Pentabromodiphenyl ether

Hexabromodiphenyl ether

Heptabromodiphenyl ethe.

Octabromodiphenyl etherNonabromodiphenyl ethetDecabromodiphenyl ether

Notes :

No. CANEC1207912202 Date: 26 Jun 2012 Page 3 ol 5

:q ̂ nftd soFE Prrcdd! tow tqrotT t'0dloJgslm 51m6J

4@ .r ,l1 .&fitl^f&D 6e!i! e&l$e ar' )'r$63

0!2NDNDNDNDNDNDNDNDND

j lS6 rrel$666 | 136_&)3?0751i3r (86 20) s2r555s5 r lS6-2OlS2O7t'3 e s€s dB@'3ss M

Menbe 'or lho SGs GrouP (sGS SA)

t!d! ui!mgKgmg/Kgmg/Kgmg/KgmgKgmg/Kgmg/Kgmg/Kgmg/Kg

IVDL

555555555

(1) The maximum permissible limit is quoted ftom the directive 2011/65/EU, Annex ll

i

Test Report No. CANEC1207912202 Date: 26 Jun 2012 Page 4 of 5

ATTACHMENTSRoHS Testing FlowChart

'1 ) Name of the peEon who made testing: Bella Wang / Cutey Yu2) Name of the person in charge of testing: Adams Yu / Ryan Yang3lThese samolis were dissolved tcElly by pre-conditioning method according to below flow chart'(Cf*

and PBBS/PBDES test method excluded).

ifu i.,!;"#Isi.:11*fiifi ';2l':l-:i,:lil"'li"rX=r*fr jip;;rs.#*i*t$1g$]lt$#ffi*$;'#f$$ili'l$liryh]ii:ffit*rtr*:i::i;i"r"*:?ril?!?:li:ni3*:*"

,0qcdbdprolss''*rkddq0,.r'li0.dci*Eo* r(863,ffi;:;ffi I ffi:trl,i " JX$T:sE.r- i t l .E t ,GtreEsgt iF&* la3t 6t :51

Pbrcd/Hg PBB3/PBDE8

Positive

Acid digestion withmicrcwaveJ hotplate

1) Alkali Fusion /Dry Ashing

2) Acid todissolve

Adding 1,tdiphenylcarbazidefor colordevelopment

Adding 1,5-diphenylcarbazidefor colordevelopment

A red colorindicates thepresence of CF*.f necessary,confirm with

M6mberollho sGS GrouP (SGs sA)

SGSTest Report

Sample photo:

cAN12-079122.002

SGS authenticate the photo on onginal report only

'** End of Report *-

;H:S:,I"t'*i;H'"ltT:-l::.t:,':ffi:'.-.#i":._a.r-li!;i;1".j;:r*,T::Xt;:,ru1rw,*ir.!:iitii:i,-Si,'lit1{.i:iiT:iq',iT#ilii:i::iij"::'j,*'rfl'#rffliilrl-":ll;r,lrurii:**'"r

1106-,0)&155696 I {3H0)320751r3 Mm 59rM

I (st-!o)s?155556 l 1s6-2o)s20751ls' ssscrrna€F$M

No. CANEC1207912202 Datet 26 Jun 2012 Page 5 of 5

rlt{0r! R6l5edlP'l(slr{dnEdni&di@06!hFstod'{otgaroi! 510663

+!l' et&**AE*+r*i+$*re3S 4n:s1m63MeFborolrhe SGs6DuP (SGSSA)

Test Report Number： SHAH00361401

Authorized by： For intertek testing services Ltd., Shanghai

Jacob Lin General Manager

Page 1 Of 4 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

Applicant： LITTELFUSE,INC. Date： JAN 16, 2013 800 E. NORTHWEST HWY Attn： A.DIVIETRO/D.UNTIEDT

Sample Description： One (1) submitted sample said to be Grey Wire. Item Name ： Wire Tin Plated Cu. Part No. ： Element.

************************************************************************************************************************************************************ Tests Conducted：

As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************

To be continued


Tests Conducted





(Ⅰ) Test Result Summary： Testing Item Result (ppm)

(1) Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg With 50cm2) Negative (< 0.02)

Testing Item Result (ppm)

(2) Heavy Metal Cadmium (Cd) content / Plating ND Lead (Pb) content / Plating 60 Mercury (Hg) content / Plating ND Chromium VI (Cr6+) content (mg/kg With 50cm2) / Plating Negative (< 0.02)

Remarks： ppm = parts per million = mg/kg

ND = not detected @ = Due to the insufficient sample area, reduced total sample surface of 10 cm2 was used and the dilution factor

was adjusted accordingly. mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre

Tested components：

(1)Substrate. (2)Plating. Responsibility of Chemist: Dent Fang / Ken He

(Ⅱ) RoHS Requirement：

Restricted substances Limits Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)

The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.

(Ⅲ) Test Method：

Testing item Testing method Reporting limit

Cadmium (Cd) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in Annex B, by boiling water extraction and determined by UV-VIS Spectrophotometer.

0.02 mg/kg with 50cm2

Remark：Reporting limit = Quantitation limit of analyze in sample Date Sample Received：Jan.9, 2013 Testing Period：Jan.9, 2013 to Jan.14, 2013

************************************************************************************************************************************************************ To be continued


Tests Conducted





(Ⅳ) MEASUREMENT FLOWCHART: Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs contents Reference standard: IEC 62321 edition 1.0:2008 REMARKS： *1: LIST OF APPROPRIATE ACID：

MATERIAL ACID ADDED FOR DIGESTION Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4

*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED. ************************************************************************************************************************************************************

To be continued

Sampling/grinding or cutting

Weigh sample and for different material,

digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline

solution

Definite temp. Extraction

Make up with deionized water and add Diphenyl-

carbazide solution

Cr6+

Weigh sample andadd organic

solvent

Soxhlet extractionor

Solvent extraction

Concentrate the extract and make up with organic

solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples

Boiling water extraction

Metal Polymers / electronics

Negative*2

Confirm the tested samples are totally

dissolved

No

Cool and filter the extract

Yes


Tests Conducted





***********************************************************************************************************************************************************

End of report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.








Applicant： ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU Date： JAN 18, 2013 GMBH

GEWERBESTRASSE 87,D-98669 VEILSDORF, GERMANY

Sample Description： Two(2) pieces of submitted samples said to be ： (1) Mixed all kinds of metal substrates. (2) Mixed all kinds of plating layers. Item Name ： Silver Plated & Pure Silver Wires. Item No. ： (B-1) 101.014 -. ----

– silver plated copper wire – Cu, Ag--% (B-2) 101.0131.---- – pure silver wire – Ag 1000 (B-3) 101.0123.0--- – silver plated purest nickel wire – Ni99.98%, Ag1% (B-4) 101.0182.0--- – silver-copper alloy plated copper plated iron nickel alloy wire – ElconD, AgCu5% (B-5) 101.0120.0--- – silver plated constantan wire – CuNi44, Ag5% (B-6) 101.0151.0--- – silver plated copper - nickel 44 alloy wire – CuNi44, Ag10% (B-7) 1050--31.-------- – pure silver strips – Ag 1000 pure

Country Of Origin ： Germany. ************************************************************************************************************************************************************ Tests Conducted：


To Be Continued


Tests Conducted





(A) Test result of RoHS Directive： Result

Testing item (1)

Cadmium (Cd) content (mg/kg) ND

Lead (Pb) content (mg/kg) ND

Mercury (Hg) content (mg/kg) ND Chromium (VI)(Cr6+) result (by boiling water extraction on metal) (mg/kg with 50cm2) ND

Result

Testing item (2)

Cadmium (Cd) content (mg/kg) /Plating ND

Lead (Pb) content (mg/kg) /Plating ND

Mercury (Hg) content (mg/kg) /Plating ND

Chromium (VI)(Cr6+) result (by boiling water extraction on metal) (mg/kg with 50cm2) /Plating ND

Remark：mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter

ND = not detected (B) RoHS Requirement：

Restricted substances Limits Cadmium (Cd) 0.01% (100 mg/kg) Lead (Pb) 0.1% (1000 mg/kg) Mercury (Hg) 0.1% (1000 mg/kg) Chromium (VI) (Cr6+) 0.1% (1000 mg/kg)


(C) Test method： Testing item Testing method Reporting limit

Cadmium (Cd) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 mg/kg

Lead (Pb) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 mg/kg

Mercury (Hg) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 mg/kg

Chromium (VI) (Cr6+) content (for metal)

With reference to IEC 62321 Edition 1.0: 2008, by boiling water extraction and determined by UV-VIS Spectrophotometer.

0.02mg/kg with 50cm2

(in testing solution)

Date sample received： Jan.14, 2013 Testing period： Jan.14, 2013 To Jan.17, 2013

************************************************************************************************************************************************************ To Be Continued


Tests Conducted





(D) Measurement flowchart：

Test for Cd/Pb/Hg/Cr (VI)/PBBs/PBDEs contents Reference standard: IEC 62321 Edition 1.0: 2008

Remarks： *1: list of appropriate acid：

Material Acid added for digestion Polymers HNO3,HCL,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

************************************************************************************************************************************************************ To Be Continued


Weigh sample and for different material, digest

the sample with appropriate acid*1


Cd/Pb/Hg

Analyzed by ICP-OES


solution


Make up with deionized waterand add diphenyl-carbazide

solution

Cr6+

Weigh sample and add organic

solvent


Solvent extraction


solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples



Positive*2


dissolved

No


Yes


Tests Conducted





************************************************************************************************************************************************************

To Be Continued


Tests Conducted





************************************************************************************************************************************************************

End Of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Test Report No. SHAECl216714748 Date: 25 Sep 20 1 2 Page 1 of 5

ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO'' LTD

XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE' CHINA

The follorving sample(s) wasl/verc submitted and identified on behalf of the clienb as : LEAD'FREE SOLOER

WIRE

sGS Job No. :

Part No. (P/N) :

Composition :

Date ol Sample Received :

Testing Period :

Test Reqlested :

Test Method :

Test Resulb :

Condusion :

sP12-028285 - SH

YTW1o8 (692535-001' 692535-003 )

Sn3.0CuRE21 gep 2012

21 Sep 2012 - 25 seq 20 12

Seleded test(s) as requested by client.

Please refer to next page(s).

Ple€se refer to next Page(s)Based on the perfrcrmed tests on submitted samples, the results of Lead'

Mercury, cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB)' -Polybrominatecl diphenylethe6 (PBDE) comply with the limits as set by RoHS

Direciive 2011/6tEu Annex lli recasting 200295/EC.

Signed for and on behalf ofsc$csrc Ltd.

,zQv"-Fan Jingjie, JJApproved Signatory

rhb@drb &.d tt tu cqryry aDld b b-

r4rg,.giffi:iii; ftH,#'ffiffiffiffffififfii';:i;c*;ivi ;f -d.urb-r-brbcld-n

tltrridtarblnlud.'i.groh 2@+t.rt.lE6lufte+eet al:4

iElE6-?1Fa€m9 wd{rm*.oeagms . *!|h.e4(!ii

108{S.?r)61{!!anL(d-21nl4@a

ri.rnb.lol0|. Sos oollP (8oS S )

Teet Report

Test Resufts :

No. SHAEC1216714748 Date; 25 Sep 2012 Page 2 of 5

Test Part Desc.iption :

SpodmqrNo. SGSSandolD D*qiptlon1 SHA'12167147.041 Silvery wire

Rema*€ :(1 ) I mg /kg= 1 PPm=00001%(2) MDL = Method Detedion Limit

(3) ND = Not Detected ( < NIDL )(4)

"" = Not Regulated

RoHS Diradv€ 201 1/65/EU

Test Method : with reference to lEc 62321i2008(1) Determination of Cadmium by ICP-OES.(2) Oetemination of Lead by ICP-oES(3) Determination of Merdiry bv ICP'OES(4) Determination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis

(5) Determination of PBBS / PBDES by GC-MS'

Test ltem(s)

Cadmium (Cd)

Lead (Pb)

Mercury (Hs)

Hexavalent Chromium (Cr(Vl))

Sum ol PBBSMonobrcmobiphenylDibrcmobiphenylTribromobiphenylTetrabromobiPhenylPentabromobiphenYlHexabromobtphenylHeptabromobiPhenylOctabromobiphenylNonabromobiphonylDecabromobiPhenylSum of PBDESMonobromodiphenyl ether

Limit ud! M0!100 mg/kS 2

1000 mSftS 2

1000 mS/kg 2o

1000 mgkg- mSikS 5- mdkS 5- mS/kS 5- ms/ks 5- mdkS 5- mg/kg 5- mg/kg 5- mgftS 5

mdkg 5- mS/kg 5

1000 mS/kg- mdkg 5

@1ND55ND

NegativeNDNDNDNDNDNDNDNDNDNDNONDND

;i;a' ir*&{.d n dnl.,.d/bb 6rr.{.tt.d '

tlrr'ttafi$bDd|rddna.{rofr !93{l -I*.*trBlt!l8aea3+l aI: 2@

rE E6+r)B1a@ IEE€GA)6|€Sdrgnj{c-2rtauozg $i6GA)4|d063

M.n&r ot fi. Soa or.r0 (8Gs sA)

sGqTest Report

Test ltem{s)

Dibromodiphenyl etherTribromodiphenyl etherTelrabromodiphenyl elherPentabrcmodiphenyl etherHexabromodiphenyl etherHeptabromodiphenyl elherOctabromodiphenyl elherNonabromodiphenyl ethetDecabromodiphenyl ether

Notes :(1) The maximum permissible limit is quoted ffom direclive 2011/65/EU' Annex ll(2) ospoltest:

Negative = Absence of Cr(Vl) coating, Positive = Presence of Cr(Vl) coating;

Ohe tested sample should be further vedfied by boiling-wateFexlraction method if the spot test result

is Negative or cannot be confimed-)oBoiling-wateFextraction:Negative = Absence of Cr(Vl) coatingpositive = Presence of Cr(Vl) coating; the detected concentration in boiling-wateFextraction solution is

equal or greater than O.O2 mg/kg with 50 crn" sample surface areaForcorosionprotectioncoatingsonmeta|s:|nformationonstorageconditionsandproducliondateofthe tested sample is unavailable and thus results of Cr(Vl) represent status of the sample at the time

of testing.

No. SHAEC1216714748 Date: 25 Sep 2012

ud! Mot @1mg/kS 5 NDmS/kS 5 NDmdks 5 NDmSikS 5 NDmg/kS 5 NDmSftS 5 NDmdkS 5 NDmS/kS 5 NDmdkS 5 ND

Page 3 of 5

tird!

iiiiir-r'ud-poa-t.ovbrk.md(.rrrd'

ttlEttlFYErto d!| |lqsrflddctrr 2@ rE E64r)6la{!54rii('-zl5r4&t4

ra€6+1F*n19f{! (6-er)6,La6t+l -ll.*tr6lurlftaer+gttl l|: 2a@

€mD.r ot !h. sGE GrcuP (8GS SA)

Test R€port No. SHAECl216714748 Date: 25 Sep 2012 Pag€ 4 of 5

ATTACHMENTS

RoHS Testing Flow Chart

1) Name of the person who made testing: Jan Shi/Yoyo Wangr'Allen XiaolGaryXu2) Name of the person in charge of testing: Jeff Zhanglceorge Xu/ Linda Li3) These sampleswere dissolved lotally by pre-conditioning method according to betow flow chart. (Cf'

and PBB!,/PBDES test method excluded)

Sample PrepaEtion

1) Alkali Fusion /DryAshing

2) Acid to dissolve

Heating to 90-957for extraction

Adding 1,5-diphenylcalbaAde

for colordevelopment

Adding 1,5-diphenylcarbaade

for colordevelopment

A rcd colorindicatesthe

presence of cr8t.necessary,

Pb/CdHg PBBs/PBDES

t6&tttY|laf{dpdtrd,st{iatr @'Fr.-*.ltrEtdttidotsr+l lr:2@3

r ErE F2!) 8r@53rll Fzl6lil&5aa

I€EF{|FMDrij F€i)i6063

lLint r ot th.sos Gro{p (8GS s,l)

Teet Report

Sample photo:

No. SHAEC1216714748 Oate: 25 Sep 2012 Page 5 of 5

sHA12-167147.041

SGS authenticate the photo on odginal report only

". End of Report '_

tu&.{drbdnrtbtu d..{d I bd rr h orFry ndd b rr oodr c.ddr o, sdi- rtu orr..r. hrlbd .rrh i!ra..!...* t'd @r'oqtuqd n rmr d c.du| @ Edmr o.eid d tlndrsso&E sEs4!ll4.r-ril_kr.rllnddb end r. dn-d b.k*r'd!. dnfu i.d| dr6 i. ct'e6r'.bffimidror. h.&,dr.dr4ffiFLb.tur&ldFcu&..rdLl&lr rd.&k, .bglfuoi.lb..oo&qan6pihtun,riMt st'ff..'|erEdctuc.ir4d|n-tu|i-.hAnrdrrrd

't6.h.nril*dnN..rnhidrtb6 |hpr.Gl6H.

fbtlnsll||lto dftnrada.cfirr ?w rEl.Fa)flroe5a r€.EFtl6&9 w.o.!.ch-tl'*,EEldJlsaol€tl i*@ u!9Fa)6l.aa!Da t{jF46ea .{.d*reg.@

[.tn!.rolfr. scaGr.{, {8GSA )

Cuslomer: Suzhou FuHong Electronic IndustriatCo., 16.

Addr6s: NO.89 \/ElDU ROAD, WANGTING TOVIN, XTANGCHENG DISTR|CI SUZHOU. CHINARepod on the submltted samrl€ said to be

sample name: Lead wife coppershell

Modol:/

Itefi/Lot Io.: /Matonal:/Buyen/ :S u p p l i e r : / ,

l i lanufacturE:/- . _ - i

- fSample recelved date: Gq _08, 2012 :t*,tn o"n.o, t.. o".;;,,013

"."r.-,.,,613, 1 ,]

&glirs-Bgsccsgq i

As specifed by dienl, to determine the L€ad, Cadrium, l,tercury & tiexayabntChrcmium conle in the 6ubmitted sampte inaccodance with Directive 2OO2I95/EC {RoHS). j

l\OV'BF.F.q,A

TEST REPORTNO.: 4002R121008024-2R02 Oate: Oct.1 0, 2012

Testing ltem Measufing instrument ,MQL

Lead (Pb) IEC 62321:2008. section I rcP-oEs a!gagcadmium (Cd) IEC 62321:2008, s€ction 9 tcP-oEs 2 mg/kg

[,lercury (Hg) IEC 62321r2008, s€ction 7 rcP-oEs 2 mg/kg

Chromium (CrM) IEC 62321: 2008, Annex B 0.02mg/kg*

Testino method:

lsqj 0.02 mg/tg rcturs to the MQL olsample exlraction liquid.

Conclu3ion:-\ryhen tested as specified lhe submilied sample compried with th€ requircments of commission D€cision of 18 Aug 2005

amending Dircctive 2002/95/EC notilied under docum€nt 2005/618/EC.

LiTingting, Maggie

Chemical Test Direclor

Yuan Qi, l,lickey

LabManager

Sign€d ior and on behallol

Shenzhen AOV Testing Technology Co., Ltd, Kunshan 8ran6h

ea"arc"a"r, A?1 W a l b n OrO."*0r44

."*FOR FURTHER DETAILS, PLEASE REFERTOT

Technical Di€clor

STIENZIIEN AOVTE$Tl'{G I€CHI!OLOGY CO,.I.TD,KUNSHAN BRANCI]

(,10",'ll,,u*

l\ov"BF,?sn

NO.: A0O2R12100802+2R02

T63l Flow:

Cooling the vessel, fiitei washed and

fllled lo the mafK with distilled waler.

Add the digestion solulionj thevess€l is heated until the sample

TEST REPORTDate Oci .10,2012

L To Detemine/lead, Cldmium Content (Metal substrale)lestedbY

L7.^otq,

-*".irl,"*J "r,to,"t|,

Add lhe digestion soluUon, closelhe microwave vessel.

f---- -].-

(Plating)

The sample is digested in the

micrcwave oven tollowing a specinc

deoomposilion progrcm.

Test the sample solulion and ihe 0.02

mg/kg slandard solution by uv-vls.

' H o t l r n e40a 700 8600

Cooling the vessel, frller;washed and

filled to the maft wilh dislilled waler.

Remove lhe sample, and cool

the beak€r lo room temperature,

and do the color reaclion

______-l "*rn nrte,.washedand l_____*p;-r, f;;-1

I rilled lo$e mark with Dlwaler I

ShENZH€N AOV I6STII {G T 'C NOIOGY CO.. ITD.XUNSHAN OEANCH

/\OV"BF#,HN

NO.i A002R121008024-2R02

Sample Doscripilon:

TEST REPORTOate :Oc l10 2012

5. To Deiermine Hexavalent Chromium Content in colorless and colorcd chromate coaling on metals: (Plating)

r e s t e d b v : l ) ^ ,' L/A^U,4.

5.1 Spotlesl (

f l;"')l;**SN€$ZHEN AOVI :STING T€C NOIOGY CO' ' ITD.XUNSI lAN BBANCI I

lf the lest result is posiiive,

ihe sample is considered lo

have hexavalenl chromium

Place 1-5

and the 0.02 mg/kg

Boiling- water- extracton

procedurc shall be us€d tolf the test reslrlt

lltherc is intederence or it is had to decide

whetherlhe sample have the hexavalent

5.2 Boilin9- water- enractronRemove the sample, and cool

the beaker to rcom temperalu€,

and do the color rcaolion

Take the (50i5)cm2

sample in the beaker.Heat 50 ml ol Dl waler in the

beak€r to boiling lof 10 min

Code Sample Desc{iplion Code

copper shell subslfate

Lead wire Plating 24 Copper shell Platng

Unit RoHS Limit Result

2-3

Lead {Pb) mg/l(g 1000 N.D. N.D. N.D. N.O

Cadmium (Cd) mg/k9 100 N.D. N.D. N.D, N.D.

Meroury (Hg) mg/kg 1000 N.D. N.D. N.D, N D .

Chromum (Crl'I) mg/K9 1000 Negalive Negalrve Negaliv€ Negative

TEST REPORToare: oct.10,2012

-:fh€ new RoHS di€ctive 2011/65/EU, on Jul. 21,2011 come inlo force, on Jan. 03, 2013 ths formal implementation, Direcliv€

200295/EC ahall be repeal€d simultaneously-

Sp€cimens, which ggqeted to d€temine Lead, Cadmium and Mercury conient have been dissolved completelv.

NO.: A0O2R12100802+2R02

-mg/Kg=ppm

--The iest is bas€d on the following

ce of C_rl\,I)lif"veiry/y6hetp ttef.limere sr{.q!.be/rurTr v ii'iffyiT-''

*'q:*lhe spot test result is uncertain or

each pad is unifom. The tesl rcsult

maybe cannot stand for the physical truth-Photo is included

Lead wir€ copper shell

"'End of Repod""

sHEI\tZH:ir AOVrlsrr'tc IECNl'lO!OeY CO.,ITD KUNSHAN SRANCIi

r.r i35.1J:55i0eo0o Fd.3F1t?55roEr$ hrr ,w.d{.di' Fodrdo 1r.r00/ , Hot l rne

I , 400 700 8600









Sample Description： One(1) submitted sample said to be White Yarn. Item Name ： Glass Yarn. Part No. ： 648901.

************************************************************************************************************************************************************ Tests Conducted：


To Be Continued


Tests Conducted





1 (Ⅰ) Test Result Summary： Testing Item Result (ppm)

Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Remarks：ppm = parts per million = mg/kg

ND = not detected

Responsibility of Chemist: Dent Fang / Leaf Liu

(Ⅱ) RoHS Requirement： Restricted substances Limits Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)


************************************************************************************************************************************************************ To Be Continued


Tests Conducted





(Ⅲ) Test Method： Testing item Testing method Reporting limit


2 ppm


2 ppm


2 ppm

Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-VIS Spectrophotometer. 1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm

Remark：Reporting limit = Quantitation limit of analyze in sample

************************************************************************************************************************************************************ To Be Continued


Tests Conducted








To Be Continued





Cd/Pb/Hg

Analyzed by ICP-OES


solution



carbazide solution

Cr6+


solvent


Solvent extraction


solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples



Negative*2


dissolved

No


Yes


Tests Conducted





2 Halogen content

(Ⅰ) Test result summary： Testing item Result (ppm) Fluorine (F) 350 Chlorine (Cl) 150 Bromine (Br) ND Iodine (I) ND


ND = Not detected

Responsibility of chemist：Grave Wang

(Ⅱ) Test method：


Halogen content With reference to EN 14582：2007 by combustion flask with oxygen and determined by ion chromatography 50 ppm

Remark：Reporting limit = quantitation limit of analyte in sample Date sample received：Jan.8, 2013 Testing period：Jan.8, 2013 To Jan.14, 2013

************************************************************************************************************************************************************ To Be Continued


Tests Conducted





(Ⅲ) MEASUREMENT FLOWCHART：

Test for halogen content REFERENCE STANDARD：EN 14582

************************************************************************************************************************************************************

To Be Continued

Add absorbent in a combustion flask & place weighed sample in equipment

Fill the combustion flask with oxygen

Ignite then leave the flask at room temperature

Transfer the absorbent into a volumetric flask



Analyzed by ion chromatography


Tests Conducted





************************************************************************************************************************************************************










Sample Description： One(1) submitted sample said to be White Yarn. Item Name ： Yarn. Part No. ： 648115.

************************************************************************************************************************************************************ Tests Conducted：


To Be Continued


Tests Conducted






Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND


ND = not detected

Responsibility of Chemist: Dent Fang / Leaf Liu (Ⅱ) RoHS Requirement：



************************************************************************************************************************************************************ To Be Continued


Tests Conducted







2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


************************************************************************************************************************************************************ To Be Continued


Tests Conducted








To Be Continued





Cd/Pb/Hg

Analyzed by ICP-OES


solution



carbazide solution

Cr6+


solvent


Solvent extraction


solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples



Negative*2


dissolved

No


Yes


Tests Conducted





2 Halogen content

(Ⅰ) Test result summary： Testing item Result (ppm) Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND


ND = Not detected





Remark：Reporting limit = quantitation limit of analyte in sample Date sample received：Jan.8, 2013 Testing period：Jan.8, 2013 To Jan.15, 2013

************************************************************************************************************************************************************ To Be Continued


Tests Conducted







************************************************************************************************************************************************************

To Be Continued









Tests Conducted





************************************************************************************************************************************************************










Sample Description： One(1) submitted sample said to be ：White Yarn. Item Name ： Glass Yarn. Part No. ： 648150.

************************************************************************************************************************************************************ Tests Conducted：


To be continued


Tests Conducted






Heavy Metal Cadmium (Cd) content ND Lead (Pb) content 27 Mercury (Hg) content ND Chromium VI (Cr6+) content ND Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Remarks： ppm = parts per million = mg/kg

ND = not detected Responsibility of Chemist: Dent Fang / Leaf Liu

(Ⅱ) RoHS Requirement：



************************************************************************************************************************************************************ To be continued


Tests Conducted







2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


************************************************************************************************************************************************************ To be continued


Tests Conducted








To be continued





Cd/Pb/Hg

Analyzed by ICP-OES


solution



carbazide solution

Cr6+

Weigh sample and add organic

solvent


Solvent extraction


solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples



Negative*2


dissolved

No


Yes


Tests Conducted





2 Halogen content

(Ⅰ) Test result summary：

Testing item Result (ppm)

Fluorine (F) 850 Chlorine (Cl) 300 Bromine (Br) ND Iodine (I) ND


ND = Not detected





Remark：Reporting limit = quantitation limit of analyte in sample Date sample received：Jan.8, 2013 Testing period：Jan.8, 2013 to Jan.14, 2013

************************************************************************************************************************************************************ To be continued


Tests Conducted







************************************************************************************************************************************************************

To be continued









Tests Conducted





*****************************************************************************************************************************************************

End of report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

TEST REPORT NUMBER: SHAH00345629

AUTHORIZED BY： FOR INTERTEK TESTING SERVICES LTD., SHANGHAI

JACOB LIN GENERAL MANAGER

PAGE 1 OF 11 Intertek Testing Services Ltd., Shanghai




APPLICANT: LITTELFUSE,INC. DATE: OCT 29, 2012 800 E. NORTHWEST HWY ATTN: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE ORANGE INK. PART DESCRIPTION : INK-ORANGE. PART NUMBER : 425900. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012.

***************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED





1 (Ⅰ) Test Result Summary : Testing Item Result (ppm)

Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

(Ⅲ) Test Method:

Testing Item Testing Method Reporting Limit


2 ppm


2 ppm


2 ppm

Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 1 ppm


With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm



5 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





(Ⅳ) Measurement Flowchart:

Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008

REMARKS: *1: List of appropriate acid：

Material Acid added for digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected. *****************************************************************************************************************************************************

TO BE CONTINUED

sampling/grinding or cutting

weigh sample and for different

material, digest the sample with

make up with deionized water

Cd/Pb/Hg

analyzed by ICP-OES

weigh sample and add alkaline solution

definite temp.

make up with deionized water and add diphenyl-

carbazide solution

Cr6+

weigh sample and add organic

soxhlet extraction or

solvent extraction

concentrate the extract and make up with organic

PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples

boiling water extraction

metalpolymers / electronics

negative*2

confirm the tested samples are totally

dissolved No

cool and filter the extract


TESTS CONDUCTED





2 ( ) Ⅰ Test Result Summary :

Testing Item Result (ppm)

Halogen Content Fluorine (F) ND Chlorine (Cl) 14500 Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million = mg/kg ND = Not detected

Responsibility Of Chemist : LEAF LIU

(Ⅲ) Test Method:


Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography 50 ppm


***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






Test For Halogen Content Reference Standard： EN 14582

*****************************************************************************************************************************************************

TO BE CONTINUED

add absorbent in a combustion flask & place weighed sample in equipment

fill the combustion flask with oxygen

ignite then leave the flask at room temperature

transfer the absorbent into a volumetric flask



analyzed by ion chromatography


TESTS CONDUCTED





3 (A) TEST RESULT SUMMARY: TESTING ITEM RESULT(ppm)

HBCD (HEXABROMOCYCLODODECANE) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED

(B) TEST METHOD :

TESTING ITEM TESTING METHOD REPORTING LIMIT

HBCD (HEXABROMOCYCLODODECANE) WITH REFERENCE TO USEPA 3540C, BY SOLVENT EXTRACTION AND DETERMINED BY GC/MS 10 ppm

***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART

TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT *****************************************************************************************************************************************************

TO BE CONTINUED

WEIGH SAMPLE AND PLACE INTO A THIMBLE

SOXHLET EXTRACTION WITH ORGANIC SOLVENT

CONCENTRATE THE EXTRACT

ANALYZE BY GC-MSD

MAKE UP WITH ORGANIC SOLVENT

TRANSFER THE EXTRACT INTO A VOLUMETRIC FLASK


TESTS CONDUCTED





4 PHTHALATE CONTENT TEST

WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.

LIMIT(%,W/W) TESTED COMPOUND RESULT (%,W/W) (MAX.)

DIBUTYL PHTHALATE (DBP) ND --- DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND --- BENZYL BUTYL PHTHALATE (BBP) ND --- SUM OF THREE PHTHALATES ND 0.1

REMARK： THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII

ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.

DETECTION LIMIT = 0.01%(W/W) ND = NOT DETECTED


WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.

LIMIT(%,W/W) TESTED COMPOUND RESULT (%,W/W)

(MAX.) DI-BUTYL PHTHALATE (DBP) ND 0.1 DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND 0.1 BENZYL BUTYL PHTHALATE (BBP) ND 0.1

REMARK： THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER

PRODUCT SAFETY IMPROVEMENT ACT 2008 & AMENDMENT H.R.2715 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES. DETECTION LIMIT = 0.01%(W/W) ND = NOT DETECTED

DATE SAMPLE RECEIVED：OCT.15, 2012 TESTING PERIOD：OCT.15, 2012 TO OCT.18, 2012

***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART:

TEST FOR PHTHALATES CONTENTS (EN14372) *****************************************************************************************************************************************************

TO BE CONTINUED

WEIGH SAMPLE AND PLACE IN A THIMBLE

EXTRACTED BY SOXHLET EXTRACTION WITH ORGANIC SOLVENT


ANALYZE BY GC-MSD


Transfer the extract into a volumetric flask


TESTS CONDUCTED






TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3) *****************************************************************************************************************************************************

TO BE CONTINUED

Weigh sample and place in a tube

Extracted with organic solvent by ultrasonic water bath

Analyze by GC-MSD


TESTS CONDUCTED





*****************************************************************************************************************************************************

END OF REPORT This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.








APPLICANT: LITTELFUSE,INC. DATE: OCT 29, 2012 800 E. NORTHWEST HWY ATTN: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE RED INK. PART DESCRIPTION : INK-RED. PART NUMBER : 425901. DATE SAMPLE RECEIVED : OCTOBER.19, 2012. DATE TEST STARTED : OCTOBER.19, 2012.

***************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED





1 (Ⅰ) Test Result Summary :

Testing Item Result (ppm) Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND



(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







REMARKS:

*1: List of appropriate acid： Material Acid added for digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4


************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED






Testing Item Result (ppm) Halogen Content

Fluorine (F) ND Chlorine (Cl) 1000 Bromine (Br) ND Iodine (I) ND


Responsibility Of Chemist : Leaf Liu

(Ⅲ) Test Method:




************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







**************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED





3 (A) TEST RESULT SUMMARY:

TESTING ITEM RESULT(ppm) HBCD (HEXABROMOCYCLODODECANE) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED (B) TEST METHOD :

TESTING ITEM TESTING METHOD REPORTING LIMIT

HBCD (HEXABROMOCYCLODODECANE) WITH REFERENCE TO USEPA 3540C, BY SOLVENT EXTRACTION AND DETERMINED BY GC/MS

10 ppm

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT

************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED









REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH

REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.






REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY

IMPROVEMENT ACT 2008 & AMENDMENT H.R.2715 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.


DATE SAMPLE RECEIVED : OCT.19, 2012 TESTING PERIOD : OCT.19, 2012 TO OCT.23, 2012

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (EN14372)

************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)

************************************************************************************************************************************************** TO BE CONTINUED


EXTRACTED WITH ORGANIC SOLVENT BY ULTRASONIC WATER BATH

ANALYZE BY GC-MSD


TESTS CONDUCTED





**************************************************************************************************************************************************


TEST REPORT NUMBER: SH AH00345635







APPLICANT: LITTELFUSE,INC. DATE: OCT 29, 2012 800 E. NORTHWEST HWY ATT N: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE BLACK INK. PART DESCRIPTION : INK-BLACK. PART NUMBER : 425902. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012.

************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





1 ( Ⅰ) Test Result Summary :





(Ⅲ) Test Method:

Testing Item T esting Method R eporting Limit


2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







REMARKS:


Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO 3,HCl,HF Electronics H NO3,HCl,H2O2,HBF4


************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED










(Ⅲ) Test Method:




************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







**************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED






TESTING ITEM R ESULT(ppm) HBCD (HEXABROMOCYCLODODECANE) ND


(B) TEST METHOD :

TESTING ITEM TE STING METHOD REPORTING LIMIT


10 ppm

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED





4 PHT HALATE CONTENT TEST


LIMIT(%,W/W) TESTED COMPOUND R ESULT (%,W/W) (MAX.)


REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.




LIMIT(%,W/W) TESTED COMPOUND R ESULT (%,W/W)





DATE SAMPLE RECEIVED: OCT.15, 2012 TESTING PERIOD : OCT.15, 2012 TO OCT.18, 2012

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED



Analyze by GC-MSD


TESTS CONDUCTED





**************************************************************************************************************************************************









APPLICANT: LITTELFUSE,INC. DATE: OCT 26, 2012 800 E. NORTHWEST HWY AT TN: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE BLUE INK. PART DESCRIPTION : INK-BLUE. PART NUMBER : 425904. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012. ******************************************************************************************************************************************************

TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

****************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED










(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample ******************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED







REMARKS:



*2: If the result of spot test is positive, Chromium VI would be determined as detected. ************************************************************************************************************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED








Remarks: ppm = Parts per million = mg/kg N D = Not detected


(Ⅲ) Test Method:




************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED







************************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED





3 (A) TEST RESULT SUMMARY: TESTING ITEM R ESULT(ppm)



(B) TEST METHOD :

TESTING ITEM T ESTING METHOD REPORTING LIMIT


************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT ************************************************************************************************************************************************************

TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED

















IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.


************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (EN14372) ************************************************************************************************************************************************************

TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3) ************************************************************************************************************************************************************

TO BE CONTINUED

WEIGH SAMPLE AND PLACE IN A TUBE

EXTRACTED WITH ORGANIC SOLVENT BY ULTRASONIC WATER

BATH

ANALYZE BY GC-MSD


TESTS CONDUCTED





************************************************************************************************************************************************************

END OF REPORT

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.









SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE BROWN INK. PART DESCRIPTION : INK-BROWN. PART NUMBER : 425906. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012.

***************************************************************************************************************************************************** TESTS CONDUCTED:

AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED





1 ( Ⅰ) Test Result Summary : Testing Item Result (ppm)

Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND



(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







REMARKS: *1: List of appropriate acid：

Material Acid added for digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO 3,HCl,HF Electronics H NO3,HCl,H2O2,HBF4


***************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED






Result (ppm) Testing Item

Halogen Content


Remarks: ppm = Parts per million = mg/kg N D = Not detected


(Ⅲ) Test Method:




***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







*****************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED






TESTING ITEM R ESULT(ppm)



(B) TEST METHOD :



10 ppm

***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT *****************************************************************************************************************************************************

TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED








DIBUTYL PHTHALATE (DBP) ND --- DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND --- BENZYL BUTYL PHTHALATE (BBP) ND ---

SUM OF THREE PHTHALATES ND 0.1

REMARK： THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 (FORMERLY KNOWN AS DIRECTIVE 2005/84/EC) FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.






REMARK： THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY

IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES. DETECTION LIMIT = 0.01%(W/W) ND = NOT DETECTED

DATE SAMPLE RECEIVED：OCT.15, 2012 TESTING PERIOD：OCT.15, 2012 TO OCT.23, 2012

***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






*****************************************************************************************************************************************************

TO BE CONTINUED

Weigh sample and place in a thimble

Extracted by Soxhlet extraction with organic solvent

Concentrate the extract

Analyze by GC-MSD

Make up with organic solvent



TESTS CONDUCTED






*****************************************************************************************************************************************************

TO BE CONTINUED



Analyze by GC-MSD


TESTS CONDUCTED





*****************************************************************************************************************************************************

END OF REPORT









APPLICANT: LITTELFUSE,INC. DATE: OCT 29, 2012 800 E. NORTHWEST HWY ATT N: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE GREEN INK. PART DESCRIPTION : INK-GREEN. PART NUMBER : 425907. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012.

************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED










(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







REMARKS:




************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED





2 ( ) Test Result Summary :Ⅰ


Fluorine (F) 200 Chlorine (Cl) 650 Bromine (Br) ND Iodine (I) ND



(Ⅲ) Test Method:




************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







**************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED






TESTING ITEM R ESULT(ppm) HBCD (HEXABROMOCYCLODODECANE) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED (B) TEST METHOD :

TESTING ITEM TE STING METHOD REPORTING LIMIT


10 ppm

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







************************************************************************************************************************************************** TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED







LIMIT(%,W/W) TESTED COMPOUND R ESULT (%,W/W) (MAX.)







LIMIT(%,W/W) TESTED COMPOUND R ESULT (%,W/W)





DATE SAMPLE RECEIVED : OCT.15, 2012 TESTING PERIOD : OCT.15, 2012 TO OCT.18, 2012

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED


EXTRACTED BY SOXHLETEXTRACTION WITH ORGANIC SOLVENT


ANALYZE BY GC-MSD

MAKE UP WITH ORGANICSOLVENT



TESTS CONDUCTED






************************************************************************************************************************************************** TO BE CONTINUED



Analyze by GC-MSD


TESTS CONDUCTED





**************************************************************************************************************************************************










SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE:GREY INK. PART DESCRIPTION : INK-GREY. PART NUMBER : 425909. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012. ******************************************************************************************************************************************************

TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

****************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED










(Ⅲ) Test Method:



2 ppm


2 ppm


2 ppm




5 ppm



5 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample ******************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED







REMARKS:



*2: If the result of spot test is positive, Chromium VI would be determined as detected. ************************************************************************************************************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples



negative*2


dissolved No



TESTS CONDUCTED







Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg N D = Not detected

Responsibility Of Chemist : Ken He

(Ⅲ) Test Method:




************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED







************************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED





3 (A) TEST RESULT SUMMARY: TESTING ITEM R ESULT(ppm)



(B) TEST METHOD :



************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT ************************************************************************************************************************************************************

TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED

















IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.


************************************************************************************************************************************************************ TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (EN14372) ************************************************************************************************************************************************************

TO BE CONTINUED




ANALYZE BY GC-MSD




TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3) ************************************************************************************************************************************************************

TO BE CONTINUED

WEIGH SAMPLE AND PLACE IN A TUBE

EXTRACTED WITH ORGANIC SOLVENT BY ULTRASONIC WATER

BATH

ANALYZE BY GC-MSD


TESTS CONDUCTED





************************************************************************************************************************************************************

END OF REPORT


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