ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO....
Transcript of ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO....
1
ICP Test Report Certification Packet
Company name : Littelfuse, Inc. Product Series: 3AB Axial Leads Product #: 325xxxP Series Issue Date: February 28, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the 3AB Axial Leads RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used
Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1
Remarks:
Form 585-047 Rev. A 2/21/06
2
Table 1: List of Raw Materials covered by this report
Total Parts Raw Material Part Number Raw Material Description Page(s) 1 910-005 Cap 3-6
2 C610
(909-532, 909-162, 909-165) Ceramic Body 7-35 3 11-0595 (082xxx-001) Element- CU99.9MSn 36-39 4 917-44xxxx Element - Cu(CA102) Cu110 Strip 40-43 5 RD series (899-401X-1) Resistor - RoHS 44-49 6 899-401X-1 Resistor - Halogens 50-53 7 912-228 Spring – Copper Berrylium rod 54-57 8 (YTW108) 692535-003 Solder 58-62 9 YTW102 (648102) Yarn 63-70 10 090187 Filler 71-77 11 090184 Filler 78-85 12 (3M 3779-PG) 087244 HMA - RoHS 86-89 13 (3M 3779-PG) 087244 HMA - RoHS 90-92 14 934-055 Overcap – Cap Base & Plating 93-96
nov^TEST REPORT
NO. 4002R12050740-1R02 Daie: May. 09, 2012
T€stino method:
I\l1QL
IEC 62321:2008, seclion I tcP-oEs 2mg/kg
cadmium (Cd) IEC 62321:2008, seclion 9 rcP-oEs 2 mg/kg
Mercury (Hs) IEC 62321 2008, s€ction 7 tcP-oEs 2 mSeS
chrcmium (Cr VI) IEC 62321i200E Ann€x B 0.02mg/kg'
Ieq
Cu8tomer: Suzhou FuHong Electrcnic IndustrialCo., Ltd.
AddT€€3: NO,69\ryEIDU ROAD, WANGTING TO\M{, XIANGCHENG OISTRICI SUZHOU. CHINA
R€pot on the submitt€d sample sald to b€
Sample nah€: Copp€r sh€ll
Supplier: /
Sample rocolv€d date: lvlay. 07, 2012
T6tf ng pedod: Frcm luay.07,29l2toMay.A9,2012
T€€tino R€ou€6tod
As specified by clienl, lo delermine the Lead, Cadmium, l\,telcury & Hexavalent Chrcmium mntent in the submitled sample in
.ccodance wilh Dircctive 200295/EC (RoHS).
r 0.02 mgl(g efers to the MQLofsampb enraction tiquid.
Concll|3ion:-When lested as specified lhe submitled sampl€ €omplied with the requircments of commission Decision of 18 Aug 2005
amending Direcnve 2002r95/Ec notified underdocument 2005/61E/Ec.
*'*FOR FURTHER DETAILS. PLEASE REFERTOTHE FOLLOWING PAGE{S).*'"
Sigmd ior and on behalfof
Shenzhen AOV Tesling Technology Co., Lld, Kunshan Branch
,.r.ou.o.,, /uI?'Li nngtng, lMaggie
Ch€mical Test Di€ctor
oro.'n,44.
S}I€I\IZIIEN AOV TESTING TECHNOLOGY CO.,ITD.(UI{SHAN ERANCH ol:9Jllis,.*""
nov'NO. A002R12050740-1R02
Cooling, filter;washed and fjll€d
lo lhe mark with Dl water.
-------------l --________' r€st€d by
l__rl nupo,r IInstumenl | | |
Add lhe digeslion €olution; lhe
vessel is heal€d unlil the sample
TEST REPORT
T6st€d by tCP-OEs
f*--* -j.-
d, C4lmium and Mercury Conbnt (Plating)
f*;;1.,-
Chromium Content (boiting- warer- ext€crion)r {Mstat subsrrare)
SHENZHEI\I AOV T€STII{O TECHI{OLOGY CO.,!TO.XUNSTIA BNA CH
Cooling lhe vessel, fiteri washed and
filled to the man( with dislilled water
Th8sample is digesred in the
micrcwave ov€n iollowing a specific
decomposition program
Test lhe sample solution and lhe 0.02
mg/kg standard solution by W-VIS.
Hotllne
Coolinglhe vessol, filtsr; wasi€d and
filled lo lhe markwilh distilled water.
Remove tne sample, snd cool
lhe beaker to rcom temp€€turc,
and do the color r€action
Heal 50 mL ofDlwalerin the
beaker to boiling for 'l 0 min
To Dsbmine
nov'To Detemine H€xavalent Ch.omium
",ffii'Q*a*
NO
5.
TEST REPORTDats: iray 09,2012
Contenl in colorless and colored chromate
Page3ot4
coaling on metals: (Plaling)
lf lh€ tast r€sult is positive,
lhe sample ls considered lo
hav€ hexavalenl chromium
and lhe 0.0? mg/kg
Boiling- waler- enraclion
proc€dure shall be used tolfthe l€st tesull
lfthe|e is interierence oritis hard lodecidewhether
the sample have lhe ho(avalent chromium
5.2 Boiling- waleF exlraclion
Take the (5015) cm'z
SHENZHEN AOV TISTII{G IECHNOfOGY CO.,!TO.XUNSIIAT INA CH Hotline36.512-55100000
Remov€ lhe sample, and cool
the b€akor lo room tsmp€ralute,
and do the color reaction
Heat s0 mlof orwaler in lhebeaker !o boiling for 10 min
Tesl the samplesolution and the 0.02
mg/kg slandarit solution by UV-VIS.
Pl€ring
Unil RoHS Limil
Lead (Pb) mg/xg 1000 N.D. N.D.cadmium (cd) mg/Kg 100 N.D. N.D.
Mercury (Hg) mg/xg 1000 N.D. N.D.
chromium (Cr\,I) mg/xg 1000 Negalive Negalive
nov-NO.: 4002R12050740-1R02
TEST REPORT
Photograph of Sample
-Tne n€w RoHS di€ctive 201 1/65/EU, on Jul. 21 , 201 1 com€ inlo iorce, on Jan 03, 201 3 the fomat imptemenlaton, Dircctrve2002/95/EC sh.ll be rcp€aled simultaneousty.
-Specimens, which requesred to detemine Lead, Cadmium and MercuryConrent, have boen dissotved compt€r€ty.
-N.D.=not detecGd(<rUaL)
]\,lQL=lvlethod Quantilation Limit-Negative=Absene or cr (VI):'Positive=Presence of Cr (VI)l
Uncedain= can nol v€dfy whether the sample hav€ Hexavalent Chromium by spot-test.(The lerled sample should be tunher veified by boiting,wal€r+xtraclion method if lhe spot test resutt is uncedain ol
single layer and each pa( is unifom The test resultsThe tesl is based on the followi.g assumplion: The sampte ptaring is a
maybe cannot srand ior lh€ physicalttuth ofsampte ptating.
SHINZIIENAOVTESIINGTFCHNOLOGYCO.,LTO-KUNSHA BRAI{CH
Ollo.tll.?,.""""
Signature plidForQueslionPlease Qltwith SGSwww.tw.sal-om
rtlt[tll][]|lt
Test Report No.: CE/20't3l/13191 Dale 2013101121 Page: 1 of 29
CERAMTEC GMBHGESCHAFTSBEREICH IJULTIFUNKTIONSKEMMIK,LUITPOLDSTRABE'I5. 91207 LAUF
The following sample(s) was/werc submitted and identified by/on behatf of the client as:
Sample DesoriptionStyle/ltem No.Sample Receiving DateTesting Period
CERAMICc6102013t1tl42013t1tl4 10 2013tO1n1
Test Re3ult(s)
Conclusion
: Please lefer to next page(s).
: Based on the pedomed test6 on 6ubmitted 6amples, the test results of Cadmium, Lead,I\rercury, Hexavalent Chromium Cr(Vl), PBBS and PBDES comply with tho limits as set byRoHS Dircctive 201'1/65/EU Annex ll; recasting 2002/95/EC.
Efnrd fr. aod
Chqdcd frbot bry-Trlgd
tHl5";vtr^:,)n*$i"d h8 T.u:lM
I d!'€'' ledn'"Jg onr oi.-i"oiji.--," **o o n"c.ru rcele o1r{ o'd.r'"€.o*or
f';;il*-fl9#'i"15;; d;hd,"...bndd;cmsns. E-i '.r ' i ' 'r s.rd bndid roE. .1Yand{o1ouon! (
; -to;;'; ;;:' de. rdd a- i {d d s'***d $;i-.h'';l:*l;-*.":*:;;*|'!6;, .,1;TtydT PJ.;1ii:;;T*.iiift i;;5#;i"'":1'"p,;ilbe tme or E fleiEdm onry ad s
t";!i;y1;;*"*#:;;lim:r"r"*li:;.::ir*"'r;fff";ffij'i"""ffi'13il*:#ift'r-"-".ff'""1;",1#,;1""H{i;:i""'ri"rl,1;ii , : : : n r . l l i r i l l i
Test Report No. : CE/2013/13191 DaIe :2013101121 Page: 2ol 29
CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNfiIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF
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Test Result(s)
PART I{AME No.1 : CREAM CERAirlC
Test ltem(s) Unit Method MDLReault
LimitNo.t
Cadmium (Cd) mg/Kg with reference to lEc 62321: 2008 andperformed by ICP-AES.
2 n.d. '100
Lead (Pb) mdkg With reference to IEC 62321: 2008 andperformed by lCPiEs.
2 204 1000
Mercury (Hg) mg/Kg With reference to IEC 6232 1 : 2008 andperformed by ICP-AES.
2 n.d. 1000
Hexavalent Chromium cr(Vl) msyKg With reference to IEC 62321: 2008 andperfonned by UV-VIS.
2 n.d. 1000
BBP (Benzyl butyl phthalate) (CASNo. : 85-68-7)
With reference to EN 14372. Analysis,ras performed by GC/MS.
0.003 n.d.
DEHP (Di- (2-ethylhexyl)phthalate) (CAS No.: 117-81-7)
o/. With reference to EN 14372. Analysiswas perfomed by GC/MS.
0.003 n.d.
DIDP (Di-i6odecyl phthalate) (CASNo. : 26761 -4O0)
% With reference to EN 14372. Analysis,,,€s p€rformed by GC/|\4S.
0.01 n.d.
DINP (Di-isononyl phthalate) (CASNo.:28553-12-0)
o/o With reference to EN 14372. AnalysiswEs perfomed by GC/MS.
0.01 n.d.
DNOP (Di-n-octyl phthalate) (CASNo.: 117-84-0)
o/o With reference to EN 14372. Analysisw€s perfomed by Gc/Ms.
0.003 n.d.
DBP (Dibutyl phthalate) (CAS No.u-7+2\
% With feference to EN 14372. Analysiswas performed by GC/MS.
0.003 n.o.
Perf luotooctane sulf onates(PFOS-Acid, Metal Salt, Amide)
mg/kg With reference to US EPA 3550C;2007. Analysis was performed byLC/MS.
1 0 n_o.
PFOA (CAS No.; 33S7-1) mg/Kg With reference to Us EPA 355ocl2007. Analysi6 was pedomed byLC/MS.
1 0 n.d,
Polychlorinated Biphenyls (PCBS)(CAS No.r '133,S36-3)
mg/kg with referenc€ to us EPA 3540cmethod. Analysis was perfomed byGC/MS.
0.5 n.d.
Test Report No. I CE/2013/13191Oate | 2013101121Page :3o f29
CERAI,ITEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[/|IK,LUITPOLDSTMBE 15. 9'1207 LAUF
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Test ltem(s) Unit Method MDLR€6ult
LimitNo.'l
Polychlorinat€d Terphenyls(PCTs)
mS/kg With reference to US EPA 3540Cmethod. Analysis\ ras perfomed byGC/MS.
0.5 n . d .
Polychlorinat€d Naphthalene(PCNs)
mgKg Wth reference to US EPA 3540Cmethod. Analysis\ ras performed byGC/MS.
5 n.d.
Alkanes, C10-13, chloro (ShortChain Chlorinated Paraffins) (CASNo. : 85535-84-8)
mg/Kg With reference to US EPA 3540Cmethod. Analysis was performed byGC/l\rs.
'100 n.d.
PVC Analysis was performed by FTIR andFLAME Te6t.
Negative
Formaldehyde (CAS No.: 50{0-0) mg/Kg With reference to ISO 17226-1(2008).Analysis was performed by HPLC/DAD.
3 n.d.
Monomethyl dibromodiphenylmethane (DBBT)
mg/Kg With reference to uS EPA 8270Dmethod. Analysis was performed byGC/MS.
0.5 n.d.
Monomethyl dichlorodiphenylmethane (Ugilec121)
mg/Kg With refefence to US EPA 8270Dmethod. Analysis was performed byGC/MS.
0.5 n.d.
[4onomethyl tetrachlorodiphenylmethane (Ugilec141)
mg/kg With reference to US EPA 8270Dmethod. Analysis was performed byGC/rlts.
0.5 n.d.
HalogenHalogen-Fluodne (F) (CAs No.:14762444\
mg/Kg
Wilh €fe.ence to BS EN USA2:20O7.Analysis was p€rfomed by lC.
50 n.d.
Halogen-Chlorine (Cl) (CAS No.:22537-15-1)
mg/Kg 50 n . d .
Halogen-Bromine (Br) (CAS No.:1OO97-32-2)
mg/Kg 50 n.d.
Halogenlodine (l) (CAS No.:1436244-8)
mg/Kg 50 n.d.
Oryanic.tin compoundaTdbuvl Tin (TBT) mg/Kg With reference to DIN 38407-13.
Analysis was pertormed bY GC/FPD.0.03 n .d .
rriphenylTin (TphT) me/Kg 0.03 n.d.
TestReport No.:CE/201:r/13191 Date:2013t01t21 pase:4of2s
CERAI,TEC GI,BH |I]|||tt][tt rlGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF
Test ltem(s) Unit method MDLResult
LimitNo.l
AabestosActinolite (CAS No.: 77536-66-4)
Wilh reference to EPA 600/R-93'/1 I 6method. Analysis was performed byStereo l\Iicroscope (SM), DispersionStaining Polarized Light Microscope(DS-PLlr) and X-ray DiffractionSpectrometef (XFID).
NegativeAmosite (CAS No.: 12172-73-5) o/o NegativeAnthophyllite (CAS No.: 77536-67-5)
% Negative
Chrysotjle (CAS No.: 12001-29-5) NegativeCrocidolite (CAS No.: 12OU-2a4\ ok NegaliveTremolile (CAS No.: 7753e68$) % Negative,zo1): 4-AMINODIPHENYL (CAS No.:92-67-1)
mg/Kg With reference to LFGB 82.02-2.Analysis uras performed by cC/lVS.
3 n.d,
BENZIDINE (CAS No.: 92-87- mg/Kg With feference to LFGB 82.02-2.Analysis was performed by GC/IVIS.
3 n.d.
3): 4.cHLORO-O-TOLUIDINE(CAS No.: 9569-2)
mg/Kg With reference to LFGB 82.02-2.Analysis u/as performed by GC/MS.
3 n.d.
4)r 2-NAPHTHYLAMINE (cASNo.r91-59-8)
mg/Kg With reference to LFGB 82.02-2.Analysis w€s performed by GC/MS.
3 n.d.
5): O-AMINOAZOTOLUENE (CASNo.:97-56-3)
mg/kg With reference to LFGB 82.02-2.Analysis was performed by GC/tu|S.
3 n .d .
6): 2-AMlNO.4-NITROTOLUENE(CAS No.: 99-55-8)
mgikg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.
n.o.
7): P-CHLOROANILINE (CAS No.:10647-8)
mg/Kg With referenc€ to LFGB 82.02-2.Analysis wEs performed by GC/MS.
n.d.
8): 2,4-DIAMINOANISOLE (CASNo.:6'15-05-4)
m9Kg With reference to LFGB 82.02-2.Analysis was performed by GC/[,!S.
3 n.d.
9'):4,4-DIAMINODIPHENYLI\4ETHANE(CAS No.: 101-77-9)
mg/Kg With reference to LFGB 82.02-2.Analysis was performed by Gc/Ms.
3 n.d.
10): 3,3'-DICHLOROBENZIDINE(CAS No.: 91-9+1)
mg/Kg with reference to LFGB 82.02-2.Analysis was performed by GC/MS.
3 n.d.
1 1)r 3,3'-DIMETHOXYBENzIDINE(cAS No.r 11$9&)
mgftg With roference to LFGB 82.02-2.Analysis w€s perfomed by GC/MS.
3 n.o,
'1 2): 3,3'-DII,iIETHYLBENZIDINE(CAS No.: 119-93-7)
m9Kg With reference to LFGB 82.02-2.Analy6is was performed by GC/lltS.
3 n.d.
fi ' ' !,"l;*'"*.;*.-".:;". ' ' ' ,.""""...].,";..":"'.s"*"...*"-':.."'"."."-, i l ; , .n i ' jn . i , .n t tomaroi - . "* . -d€o6|er ,ardcotro|3|oLeiii, iil.-niiniiv-iiiiiinnn-in,ii^?,aitd;*uBdlin6dthe;;^i i i i i i i"i,i ir,i*o' -ry-"*ri tr. -'borc ctihqrudm' Ir'l -tcomdars ea s!oo!oi,.i"*.i- m * os no a i r.' q*
" o o'qa'o* -0.'- nino;r'doe-44 n s do' -d -moin. ?erc!L("d P e0
li;fiii rii;" r;;a; tao: b's;t "abi"r.d*
oJ rhe @;;;;;i;;;;;i $ n@*i' "
*h*tu sa otundds mai be prcsdcd b '
, " , . , , , . : i l i i ; i l . r , qno*' t r"aFt i r i . l i . { rrr * f : rr}L s d ..::i-:-1' 9P !.ll!!.r.1
Test Report No. : CE/2013/13191 Dale:2013101121 Paqe | 5 of 29
CERAI\4TEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[IIK,LUITPOLDSTMBE 15, 91207 LAUF
Il]mttfittltl
Test ltem(s) Unit lrethod MDLR€ult
LimitNo.l
1 3): 3,3!DIMETFIYL-4,4-DIAIJINODIPHENYLMETHANE(CAS No.: 838-88-0)
mg/Kg With reference to LFGB 82.m-2.Analysis was performed by GC/lrS.
3 n.ct.
14)r P-CRESIDINE (2-IUETHOXY-s-METHYLANILINE) (CAS No. I120-71-8)
msasWith reference to LFGB 82.02-2.Analysis was performed by GC/MS.
3 n.d.
'1 5): 4,4.-METI-IYLENE-BIS- (2-CHLOROANILINE) (CAS No.:101-144)
m!/(g With reference to LFGB 82.02-2.Analysis was performed by GC/MS_
3 n.d.
16): 4,4'-OXYDIANILINE (CASNo.r 101-80-4)
mg/Kg With reference to LFGB 82.02-2.Analysjs wEs p€rfomed by GC/MS-
3 n.d.
17): 4,4'-THIODIANILINE (CASNo.: 139€5-1)
mg/Kg With reference to LFGB 82.02-2.Analysis w€s perfomed by GC/MS.
3 n.d.
1E): O-TOLUIDINE (CAS No : 95-s34)
mg/Kg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.
3 n.d.
'1 9): 2,4-TOLUYLENEDIAMINE(CAS No.: 95-80-7)
mg/Kg With reference to LFGB 82.02-2.Analysis wa6 performed by GC/MS.
3 n . d .
20): 2,4,5-TRIMETHYLANILINE(CAS No.: 137-17-7)
mdkg With reference to LFGB 82.02-2.Analysis\ ras performed by co/l\rs.
3 n.d.
21): O-ANISIDINE (CAS No.:90-04-0)
mg/Kg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.
3 n.d.
22): P-AMINOAZOBENZENE(CAS No.r 6M9-3)
mg/Kg With reference to LFGB 82.02-2.Analysis was perfomed by GC/MS.
3 n.d.
23): 2,4-XYLIDINE (CAS No.r95-68-1)
mg/kg With reference to LFGB 82.02-2.Analysis was performed by GC/IVS.
3 n.d.
24): 2,6-XYLIDINE (CAS No.: 87-62-7)
mg/Kg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.
3 n.d.
CFC's (Chlorofl uorocarbons)Group IChlorofluorocabon-1 1 (CAS No.l75€9-4)
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
n .d .
Chlorof luorocarbon-1 2 (CAS No. :75-714]
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
n-d.
;ii; i;i;;; ; ,!,.i .d '; ri. c.-,;;' ',ti; b iL; &ne'ar condi om d;; ;;;;i i;; d;-tu:^a 3uh;ed b rem! ano co.o @ns h' rrqd. b;{.I d{w.{s.o- e.i ; ; d ; l a ' ' h " i j . ' i - * ' ; . d i $a fnn ' 3 . "dddh .F 'ha rme or i! 'meilerton onrv and -; ; ; ; - ; ; h : ; . ; n . d J , ' i . i ' . c ' o i d 0 a f ; i " ' d f u r 1 a " .
Nev tdiFi .ir r.iws / I -: .'. qi i ni {li3rrL
Test Report No. : CE/2013/13191 Date: 2013t01t21 Paoe : 6of 29
CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 15. 91207 LAUF
rlfll tlt! ttt]l
lest ltem(s) Unit Me{hod MDL R€6ultLimitNo.1
Chlorof luorocarbon-1 13 (CAS No.:76-13-1)
mg/Kg With reference to US EPA 502 1method. Analysis was performed byGC/t S.
1 n.d.
Chlorcfluorocarbon-1 14 (CAS No.l7efi-2)
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
1 n.o.
Chlorotluorocarbon-l 15 (CAS No.:76-15-3)
msasWith reference to US EPA 5021method. Analysis was performed byGC/MS,
1 n . d .
Group lllChlorof luoroca6on-1 3 (CAS No.:75-72-9)
mg/kg With reference to US EPA 502 1method. Analysis wEs perfomed byGC/MS.
1 n.d-
Chlorof luoroca6on-'1 1 1 (CAS No.:354-56-3)
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
1 n.d-
Chlorofluoroc€rbon-'112 (CAS No.:76-12-O)
mlyKg With reference to US EPA 5021method. Analysis was performed byGC/MS.
'I n . d .
Chlorof luorocarbon-2l 1 (CAS No.:422-78-8)
mgikg With reference to US EPA 5021method. Analysis was pertormed byGC/MS.
'I n.d.
Chlorof luorocarbon-21 2 (CAS No. :3182-%-1)
mg/Kg With refefence to US EPA 5021method. Analysis wEs performed byGC/MS.
1 n.d.
Chlorof luoocarbon-21 3 (CAS No.:2354{6-5)
mg/kg With reference to US EPA 5021method- Analysis was performed byGC/[rS.
1 n.d.
Chlorof luoroca6on-214 (CAS No.:29255-31-0)
mgKg With reference to US EPA 5021method. Analysis was performed byGC/MS.
n.d.
Chlorof luorocarbon-215 (CAS No.:425943-2)
mgi Kg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.
n .d .
. ! . .;
"'.i;-.. ; *d b' h6 cmou
,no b' e€dM c romar dnoments rd pd 6 hr3 and cot ions b' Lrecl;;;;tmh ;A;ii-6; md :.$-r,sr3ne . reo rE 'n r . ne f l ono -vdFowt i n ' h . 'mbo rca -s iF taon< 3 l ponqb f t v ' r o c iP "d t r sdo* *o , j " t ' o . i * - " " 0 a i r
" mo l imdmb- i 5doo - t ' a t b pno ' l de roo t l a o . i c
( omod i Mv r s ! o zao arasrca o's.ry o' r;sfr-ton ol I e d+n d
.-""'.,ii::lliiillr: r l Y"!:1t]:rt"pjrtrg:.11':11j'-
Test Report No.: CE/201313191 DaIe 2013101121 Paoe 7 of 29
CERAMTEC GMBHGESCHAFTSBEREICH MULIIFUNKTIONSKERA[TIK,LUITPOLDSTMBE 15, 91207 LAUF
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Test ltem(e) unit Method I'DLResult
LimitNo.l
Chlorof luoroc€6on-216 (CAS No.l661-97-2)
mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/tUS.
1 n.d.
Chlorof luoroca6on-217 (CAS No.:422-E&6)
mg/kg With referenc€ to US EPA 5021method. Analysis was performed byGC/t S.
1 n.d.
HCFCa(Hydrochlorofl uorocalbons)HCFC-21 (CAS No.: 75434) mg/Kg With reference to US EPA 5021
method. Analy6is was performed byGC/MS.
I n.o,
HCFC-22 (CAS No.: 75-45$) mg/Kg Wilh reference to US EPA 502'1method. Analysis was pertormed byGC/MS.
'I n.d.
HCFC-31 (CAS No.: 593-70-4) mg/Kg With reference to US EPA 5021method. Analysis u/as performed byGC/MS.
'I n.d.
HCFC-121 (CAS No.: 354-14-3) mg/Kg With refefence to US EPA 5021method. Analysis was performed byGC/MS.
'I n.d.
HCFC-122 (CAS No.: 354-21-2) m!/Kg With reference to uS EPA 5021method. Analysi6 was pedormed byGC/MS.
1 n.d.
HCFC-123 {CAS No.: 306-83-2) mg/Kg With refere.ce to US EPA 502 1method. Analysis was performed byGC/rVlS.
1 n.d.
HCFC-124 (CAS No.: 2837-89-0) mg/Kg With reference to US EPA 5021method. Analysis rvas performed byGC/tVS.
n.d.
HCFC-13'1 (CAS No.r 359-28.4) mg/Kg With reference to US EPA 5021method. Analysis was pedormed byGC/tVS.
n.d.
HCFC-132b (CAS No.: 1649-08-7)mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
n.d.
-nn.'"iJ'""r
" **o
"iuie coma;";b,*
"iGa*eft codod'"s"1eor'sode' .s5i-ier-'-,nd rtro 5b
i J6 i i " oJ . i t i j a ' . i ' . n " , ' " ' , qa i 6 re - , ddod id ' b 'F3ad i , { do ' *La€ - . d t ?n &
rhermed b deiudio onl! d{sh F. aborc ens'n{rdo'' ' l;;;;" b; ;;-ii!i;,;. ilis i; ;'q;,r"";, iir" r*a;m;ry ay lmdb';d *sdon. ro@ery o, disddoi dr he 6n,ent o
Test Report No.: CE/2013/13191 Date:2013101121 Page: 8 of 29
CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF
rll |ltt][ttllll
Test liem(s) Unit Method MDLResult
LimitNo.'l
HCFC-133a (CAS No.: 75-88-7) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/t S.
n.cl.
HCFCI4lb (CAS No.: 1717-00€) mgKg With reference to US EPA 5021method. Anaiysis was performed byGC/MS.
I n.d.
HCFC-142b (CAS No.: 75-68-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
1 n-d.
HCFC-221 (CAS No.: 422-264) mg/kg With reference to US EPA 502 1method. Analysis was performed byGC/l\rs.
1 n.d.
HCFC-222 (CAS No.r 422-49-1) mg/Kg With reference to US EPA 5021melhod. Analysis was performed byGC/MS.
1 n.d-
HCFC-223 (cAs No.: 422-526) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
'I n.d.
HCFC-224 (CAS No.: 422-54-8) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
1 n.d.
HCFC-22sca (CAS No.: 422-56-0) mg/Kg With reference to US EPA 502'lmethod. Analysis u/as performed byGC/MS.
1 n.d.
HCFC-22scb (CAS No.i 507-55-1) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.
n.d.
HCFC-226 (CAS No.: 431-87-8) mg/Kg With reference to US EPA 502'1method. Analysis wes performed byGC/MS.
n.d.
HCFC-231 (CAS No.r 421-94-3) m9Kg With reference to tJS EPA 502'1method. Analysis was Performed bYGC/[iS.
't n.d.
HCFC-232 (CAS No.: 460-89-9) mg/Kg With reference to US EPA 502 1method. Analysis was Performed bYGC/MS.
1 n.d.
ow. m h's 3s B@. FF ul b ne 3
.;;.";;-", is ,rd b, h c-ps y sD.eq,o 6 Gr6rcdoj:i.,.*,pffii;F"1;f;*&,;:,#"r,,!;ri:\t,itr,:xi{.y;%1"iffT"1_i;j ?;:jli:i:",Sblecl lo rems and @ndhons ftr.,m. o. ar .* dstrnra,o, nd.inedd 'nu*"- "t:lll.lj;;1.;:t*"*;,f;:::*i;;fjl,,". if;ti* ilf,;'"-;le:'i:";i;; -?":ig:";',?lli0,:"ii
* * " " "a - , * ' - " - , - . J i i - a ; l ,mom.EF .do - -a ' 6 fdc r e . , & y l 1 a n 1 o n z e d " s d d , . - ' # i ; ; ; ; : ; ; i ; ; * : l i " ^ r ' r o b r o - d i b ' r e * d b r r l l e ' " ' { r o L h e b n
r\eift peicivft rs/:r";iii i ) i il i i 4firb
Test Report No- : CE/201313191 Date:2013101121 Paoe i gof 29
CERAMTEC GMBHGESCHAFTSBEREICH
rllllllat][ ttltMULTIFUNKTIONSKERAMIK,LUITPOLDSTRAEE 15. 91207 LAUF
Te6t ltem(a) Unit method MDL Re€ultLimit
No.1HCFC-233 (CAS No.: 7125-84-0) mg/Kg With reference to US EPA 5021
method. Analysis wa6 performed byGC/MS.
'I n.d.
HCFC-234 (CAS No.: 425-94-5) mg/Kg With reference to US EPA 5021method. Analysis was perlormed byGC/MS.
1 n.d.
HCFC-235 (CAS No.: 450-92-4) rnglkg With reference to US EPA 5021method. Analysis wEs perfomed byGC/MS.
1 n . d .
HCFC-241 (CAS No.: 666-27-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
1 n . d .
HCFC-242 (CAS No.r 46063-9) mgag With reference to US EPA 5021method. Analysi6 was performed byGC/MS.
1 n .d .
HCFC-243 (CAS No.: 460$9-5) mgKg With reference to US EPA 502 1melhod. Analysis was perfomed byGC/MS.
1 n.d-
HCFC-244 mg/Kg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.
1 n .d .
HCFC-251 (CAS No.: 421-41-0) mg/Kg With reference to US EPA 502 1method. Analysis was pertormed byGC/MS.
1 n.d.
HCFC-252 {CAS No.: 819-00-1) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
'I n.d.
HCFC-253 (CAS No.: 460-35-5) mdkg With reference to US EPA 5021method. Analysis was performed byGC/MS.
n.d.
HCFC-261 (CAS No.: 420-97-3) mg/Kg With reference to US EPA 5021method. Analysis w€s perfomed byGC/MS.
n.d.
HCFC-262 (CAS No.: 421-m-03) mdkg With reference to IJS EPA 5021method. Analysis was performed byGC/MS.
n.d.
I i B . I I l !anv5ub ] . db tGE la | cond lonso ' sed@prn iedowdca i ' ava iab |eon r€
qedb ams sr co-o m\!o' ehdd rinsdidon 'sEs ddd rhere n 6y io &r of b s eumd ; adv 3ad Lh be company s {indino! ar
Test Report No. : CE/201313191 Dale 2013t01t21 paoe | 10 of 29
CERAIVTEC G[/lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15. 91207 LAUF
rtrr lrt][ttt||l
Tegt ltem(s) unit Method MDL ResultLimitNo.1
HCFC-271 (CAS No.r 430-55-7) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.
1 n .d .
HalonsHalon-1211 (CAS No.: 353-59-3) mg/Kg With reference to US EPA 5021
method. Analysis wEs performed byGC/MS.
1 n.d.Halon-1301 (CAS No.: 75-63-8) mg/Kg 1 n.d.Halon-2402 (CAS No.: 124-73-2) mg/Kg 1 n.d.CHCs (Chlorinate hydrocarbon)1, 1, 1,2-Tetrachloroelhane (CASNo.:630-206)
mg/Kg With reference to US EPA 5021melhod. Analysi6 w€s performed byGC/MS.
1 n.d.
'1 , 1 ,'1 -Trichloroethane (CAS No. :71-55€)
mdkg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.
1 n . d .
'1, 1,2,2-Tetrachloroethane (CASNo.:79-34-5)
mgKg With reference to US EPA 5021method. Analysis wa6 perforned byGC/MS.
1 n . d .
1,1,2-Trichloroethane (CAS No.:79-00-s)
mg/Kg With reference to US EPA 5021method. Analysis $/as performed byGC/t\rs.
I n.d.
1,1-Dichloroethane (CAS No.: 7$34-3)
mgKg With reference to US EPA 5021method. Analysis was performed byGC/MS,
,| n .d .
't ,1-Dichloroethene (CAS No.: 75-354)
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
1 n.d.
1,1-Dichloropropene (CAS No.:5695&6)
mg/Kg With reference to US EPA 5021method- Analysis was performed byGC/tVS.
n.d.
1,2,3-Tichloropropane (CAS No.:96-184)
mdks With reference to US EPA 5021method. Analysis was pedormed byGC/tVlS.
n.d.
'1,2-Dichloroethane (CAS No.:107-06-2)
mgftg With reference to US EPA 5021method. Analysis was performed byGC/l\,!S.
n.d.
LN4r : i F (V r r iw in rn 1 . 1 ' n i l r i i f r : t { J
Test Report No. : CE/201 3/1 3 1 91 Dale : 2013t01t21 page : .l .1 of 29
CERAMTEC GMBHGESCTIAFTSBEREICH MULTIFUNKTIONSKERAI\4IK,LUITPOLDSTMBE .l 5, 91 207 LAUF
lfl tl|[ tllttl
Test lt€m(s) Unit Method i,DLRegult
LimitNo.l
1,2-Dichloroprcpane (CAS No.:78-87-5)
mg/kg With reference to US EPA 5021method. Analysis wEs perfomed byGC/MS.
1 n.d.
'l,}Dichloropropane (CAS No. :142-2&9)-
mg/Kg With referenc€ to US EPA 5021method. Analysis was performed byGC/MS.
1 n.o.
z,2-Dichloropropane (CAS No.:53+20-7',)
mg/Kg with reference to us EPA 5021method. Analysis wa6 performed byGC/MS.
I n.d.
Carbon tetrachloride (CAS No.i56-23-5)
mgikg Wath reference to US EPA 5021method. Analysis was pertormed byGC/MS.
1 n . d .
Chloroethane (CAS No.: 7$00-3) mg/Kg With reference to US EPA 502 1method. Analysis was porformed byGC/MS.
1 n.d.
Chlorofom {CAS No.: 67-66-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/[rS.
1 n.o.
Chloromethane (CAS No.: 74-87-3)
mg/Kg With reference to US EPA 5021method. Analysis wEs performed byGC/MS.
1 n.d.
cis-1,2-Dichloroethene (CAS No.:15G59-2)
mdkg With reference to uS EPA 5021method. Analysis\ ras pertormed byGC/MS.
1 n . d .
ci6-l,3-Dichloropropene (CAS No.l10061-01-5)
mg/Kg with reference to us EPA 502 1method. Analysis was performed byGC/MS,
1 n.d.
Hexachlorobutadiene (CAS No.i8768-3)
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
'I n-d.
Methylene Chloride (CAS No.: 75-09-2)
mg/kg With referenc€ to US EPA 5021method. Analysis was performed byGC/MS.
n.d.
Tetrachloroethene (CAS No.: 127-184)
mgI(g With reference to uS EPA 5021method. Analysis was performed byGC/MS,
n.d.
s r lEk t repo ld - r t bs ' s
i ;T f t :k" ' ' ' , . " " " "* - , " . " . " " . " - ; - . " ' " " ' " : . . i " , ' i ' . "s . . *p**"" . i .a 'a-uu"" ' l .osdo!esbA-"e!o 'o 'i * i i " i
" an ' i n t ma r ; i e r c i . r i d . db -em, ' bco r ' . " r ' ' edonLOo@f t1Rd"ms { ' , o -
a1 eas , dco ,d tuo s r8Tseooai ; ; ; ; j b ; i i ; # ; i i " ; ; i ; ; . i " " " ; . ^ d ' * h . * , e ' ' d o . t r | ' 0 r ' a ' ' a d . gh " | - . d k FE ; \ ed on odv and w ,h i d he im so c rems nsMros ' L r v i b i s r r . l a d lF tum"d6;;;(-;;;;;;-;;;;6;i;;oi:a ;; ;;J;, . ;. :ie r,..obidd-.-d -n, oo@r1 d "o 0- re o! @o "oo;#ffi;:p;;;;,-,i;;;:d i;i,;: i;a;t ;iai,n-i;";i h" -"bd
"; r . : r i r ! r ' i ' i t - l r .
Test Report No.:CE/2013/13191 Dale 201310121 Paoe:12 ot 29
CERAMTEC GMBHGESCI-I,AFTSBEREICH
tl| |l lrtl]lIVULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF
T€6r ltem(s) Unii method MDLResult
LimitNo.1
trans-1,2-Dichloroethene (CASNo. : 1 56-60-5)
mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.
'I n.d.
trans-1,3-Dichloropropene (CASNo.: 10061-02€)
mg/Kg With reference to US EPA 502'method. Analysis was performed byGC/MS.
1 n.d.
Trichloroethylene (CAS No.: 7$.01€)
mg/Kg With refefence to US EPA 5021method. Analysis was performed byGC/US.
'I n.o,
Sum of PBBS mg/Kg
With reference to lEc 62321: 2008 andoertormed bv GC/I\IS.
n.d. 1000lMonobromobiphenyl mg,iKg 5 n.d.Dibromobiphenyl mdkg 5 n .d .Tribromobiphenyl mg/kg 5 n.d.Tetrabromobiphenyl mg/Kg n.o,Pentabromobiphenyl mg/Kg n.d.Hexabromobiphenyl mg/Kg 5 n.d.
Heptabromobiphenyl mgKg 5 n .d .Octabromobiphenyl mg/kg 5 n.d.Nonabomobiphenyl mg/Kg n.d.Decabromobiphenyl mg/Kg 5 n . d .
Sum of PBOE5 mg/Kg n.d. 1000Monobromodiphenyl ether mg/Kg 5 n.d.
Dibromodiphenyl ether mgikg 5 n.d.
Tribromodiphenyl ether mg/Kg 5 n.d.Tetrabromodiphenyl ether mg/Kg 5 n.d.
Pentabromodiphenyl ether mg/Kg 5 n.d.
Hexabromodiphenyl ether mg/kg 5 n.d.
Heptabromodiphenyl ether mg/Kg 5 n.d.
Octabromodiphenyl ether mgKg 5 n.d.
Nonabromodiphenyl ether mg/Kg 5 n.o.
oecabromodiphenyl ether mg/Kg 5 n.d.
i . , ; j i t r : l e t . r \ i
Test Report No. I CE/2013/13191Dale | 2013101121Page : 13 ot 29
CERAMTEC GMBHGESCI-I,AFTSBEREICH iNULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 15, 9.1207 LAUF
lm[llt rt]I
Not. :'1. mg/kg = ppm | 0.1wt% = loooppm2. n.d. = Not Detecled3. MDL = Method Detection Limit4. "-"= Not Regulated5. - = Qualitative analysis (No Unit)6. N€gative = Undet€ctable / Positive = DetectableT Testing range of asbestos qualitative analysis is from less than 0.1% to 1OO%. The judgment crjterion: asbestos fibers
being found is shown as "Positive'; asbeslos fibers not being found is shown as,'Negative..
PFOS Refe.ence Intormetion : POPS - (EU) 757m10Outlawing PFOS as substances or preparations in concentrations above O.OOl% (lOppm), in s€mi-finished products ofarticle6 or parts at a level above 0.1%(1000ppm), in textiles or other coated materials above 1pg/m,.
3liffJ*:"iT,:'?jil\"ri+iTi:?i,iii)i:;::ii:?i"T::i:rl'!{i'iili:r!':ti,li;'rflf'l"1-'e@rcd@d eed rtur Mhdrp
ii":l"H*;:;rls,:iixs'.9"r;i"'t*;:ffagfi"u;::"^'J:rffis#j:r,x*ir5'Lri!tr:"i3;xlf;,i:;-x'#;%1:"#il";: rd,rll,l'Ti"'4ri,:"-..r-o'in|;n,*..neo,-d .<-'.*"a,doids";, ti;o; tr: dMm{ F;dre 'edsI e (omLnr\ihdin$''iiiiilni.l *'r"i'*ro" on" a"o *ti".m rns or ce.' +.*"i ';q Fe.d",p".v"d"."po"'blv ' 'o r! LrPl' . t r ' ood ̂ " diliil;a; i."- d*o.ri+e
"e;fi;;l!;;;'.;-*o;;&;1.;i;;: 6;s;t ;iaianai,* .r h. -dei, (
Test Report No.:CEl2013l13191 DaIe:2013101121 Page: 14 of 29
CERA['TEC GI,lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE'15, 9'1207 LAUF
1 ) These samples were dissolved toblly by pretonditioning method according to belolt/ flow chart.( Cf' te€t method excluded )
Name of the person who made measurement Climbgleat YangName of the person in charge of measurement: Troy Chang
2)3)
SamDle Mderial DioestionAcid
S'teel, copper, aluminum, solder Aqua reqia, HNOr, HCl, HE HzO:
Glass HNOy'HF
Gold, platinum, palladium, ce€mic Aqua regia
Silver HN03
Plastic H,SO., H,O,, HNO3, HCI
Others Added appropriate reagent to totaldiOe6tion
Note- : (1) For non{netallic material, add alkaline digestion reagent and heat to 90'95f(2) For metallic material, add pure water and heat to bdling.
r ! { e * h p e . 4 f t t $ / i i : l i i i r d r i r : l i i 4 3 \ 1
Cutting / Preparation
Sample Measurement
Add appropriate amountof digestion reagent
Acid dige6tion by suitable aciddeoended on different samolematedal (as below table)
Microv/ave digestion withHN03/HCI/HF
Heat to appropriatetemperatuae to erdr€ct
1) Alkal iFusion2) HClto dissolve
Add d iphenyltarbazidefor color development
measute the absotbanceat 540 nm by UV-VIS
Test Report No. ICE/2013i/13191Dele :2013101121Page : 15 of 29
CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE 1 5. 91 207 LAUF
]tI|tt][tttutl
PFOA/PFOS analytical flow chart of Ultrasonic extraction (LC/MS) procedure
r Name of the person who made me€surement: Roman WongI Name ofthe person in chaqe of measurement Troy Chang
ffi um*m,1*ffit*'r,*ffi*#iHl*gl+rsirti*ffikNdrripd.tvlriw:i/li: ' n ] ': Iiriti33li
r+elo2)r4rD ||e6Orlr??1 ?1
Test Report No. : CE2013l'13'191 Date 201?,10121 Paoe: 16of 29
CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE 15, 91207 LAUF
lm[tr|| ||tt]t
Data
PCTS analytical flow chert
t Name ofthe petson who made measurement Barry T6engr Name ofthe per6on in charge of measurement: Troy Chang
. i r i { r i c f n r \ i
Test Report No. : CE/2013/13191 Dale : 2013101121 Page : 17 of 29
CEMMTEC GMBHGESCFI,AFTSBEREICH MULTIFUNKTIONSKERA[/lIK,LUITPOLDSTMBE 1 5, 91 207 LAUF
ll] ttJflllafll
PBB/PBDE analytical FLOW CHART
I Name ofthe person who made measurement Roman Wongr Name of the person in charge of measurement Troy Chang
First testing process -----'
Optional screen proce6s ....
Confirmation procegs -.>
[J-"'d;---l--------r-------[s-"-lrj--jr"t""t.-tl-T-
Screen analysis
Sample e)draction/Soxhlet method
Concentrate./DiluteExtEcted solution
Filter
Analysis by GC/lvlS
lssue Report
" " " " " " ' f " " " " " "
a;; . : : ' ' . <we p" 'ed owtd ars dbir oll, :T i ;e1d; : - . ;F ; l ;u . ; " ;o€ ; '6hr 'mdcordb4u i ;n rc : .oo . - . ' l dMa ' jdq |
" ' , , . . - ' * * . . " ' , , " , , " ;r i , i j t i i o is ; ; l *m, - rv - " - ' . ,n " . ,uo |cs '+n ' .d ;n i; a ; i i i i ' . i # a j g . * , g , ' r - ' g t : T o o ] g ! j l o B J n d e l ' 9 ? n % d f ' @ o - 4 k T i 3 d o (
u ' { i;:;; ;;;;r;;: : 'oeft | s 5d|" oo'arc"a -dib'
l i i i ,: r !l I {lii:rri
Test Report No. : CE/2013/13191 Dale:20131O1n1Page : 18 of 29
CERAI,TTEC GI,/lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15. 91207 LAUF
PCBe analytical flow chart
r Name ofthe person who made measurement Bafiy Tsengr Nameoftheperson incharge of measurcment: Troy Chang
Data
lll |ltt][ttlllt
M ti rhlsresr €Don rerer ont ro be tpdorMtbpembsondrE
rhsiftinmr'a €sid b! lh€ cmoanv eubEci ro 'ls Gne'arcndiions orseruie or ed o6'ldat a$ abeonie ms .M,@iditons lrhand ror € adrof, c romd dntum.nb e 6 e d 6 re' ms and C.d ton s lo' Ered msad.Cond( ons/rerm* Dotuft
d u'is. dion isues derned bere i tuv s Ihe companvs nnd'nqs ari heheo ib i n l e iwn1ono i vandw id i n l he ] im$o l c i e i 1sns1 rc i ons f ; nyTheco Inpas$ |e Iespon3b |ftnsdon rrom err"vnq ri h., adFioftJml' hEoodm"lrConprnJ diy iaLtdzeo arleu on
Test Report No. : CE/2013i13191Dale:2013101121Page : 19 of 29
CERAMTEC GMBHGESCHAFTSBEREICH [/|ULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 1 5, 91 207 LAUF
Chlorinated Paraffins analytical flow chart
r Name oflhe person who made measurement: Bary Tsengr Nam€ of the person in charge of measuremenl Troy Chang
Data
tl][ || t|:ll]I
a m o € ' : e e e d I i ' 6 r ? o o ' € o' , t . - I . t i ,
i i i i i . i . * . " * . * o " o e c o . o a ; ' ' o d b ' i c s t . | L d d ' o ' ' d . o l , o ' 3 e e * o A d e 3 s 9 J - l;; ;i; ;.;;; ;;;' ;r;. ;;;B &;ed b rems rm cdiGmb 0 Eranrcn( ooom.{ . ar "B {- "o_ .innn;iiri,h ,omnta;.; d :1d'do sr! d,,rd h.r,he ru or r 'n,ei!en, on oi v dnd dbinher+aorcrcn \'ran01"; ; ; ; ; ; ; ; ' ; " ^ n ; ; i ; ; i o i " * o o t a " . ' ' c . * . u " ' * . ' o , ' o o J m ' 6 i I o o J - e { o ' '( dmoa., hr ,rd bo zen ,n4no'
N€r tdFi.[r ri iwri / i i-: ' !: ]. ' i : . r {iLli! l i
Test Report No. : CE/2013/13191D?[e:2013101121Page:20 ol 29
CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAIV]IK,LUITPOLDSTMBE 1 5. 91 207 LAUF
Analysis flow cha.t for determination of Asbe6tos
I Name ofthe person who made measuremenl: Victor KaoI Name of the person in charge of measurementt Wendy Wei
( Reie.ence method: EPA 600/R-93/l 16l
Sampling
Contai ning AsbestovPositive Not conhining Asbesto6/ N€gative
!]l[ttt ltt]l
" i t , 1rh6 do.irm.m E Lsusd s rha com"nd b . l . {on . r .mar o@merb . . ' iF - d re- 'dndco ld ro 's ro Fsa vdm(odor - " -3€Dor_ena
ndemnrca( on and 'LlNd d6 6su6rheriftdl6 d.iwi{on otrlv a qsi r;nrTh?com0anyssercspoi5br'ry'' 'o Lsc'en and'hsdocum.ndt r sdo hma . G ro a r i t e nConpaiy ay unauhdzad a lsrdion
k { 4 r t P ( r y r . e d / i . l : i . i 1 1 i t * j : t j r
Continue when probl€rnsarc encournefed withDS-PLM and/or for quality assurance pufposes
Asbestos identifc€lion by dispetsion stainingpola zed light micrcscope (DS-PLM)
Asbe€tos idenlifcation by X-faydiff raclion speclrometer (XRD)
Test Report No. : CEl2013i/13191 Date : 2013101121 Paae : 21 of 29
CERAI,iITEC GMBHGESCHAFTSBEREICH
!
I
Analytical flow chan of Organic-Tin content
Name ofthe person who made measurement: Ginny ChenName ofthe person in charge of measuremenl Troy Chang
It] tttI[ltr tMULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF
ui4s dheNs sbcd hs e$ 6 s,o!.n ,n h'' '6d rcpoi erer o'u.bri€ 3aT?fFr,!".i:i .iii:iif...;r':pd
**d b
"K1 i l ; "1 . , . " ; , , " . * . *# ; " , " . * ' " " ; ' * , . J , * * . '9 {ep ' ' coo ' " l "a ] ' .€ ,bPo1 'a;;.rii;etu .-d oie.- ',oFc6 krsmd hthE,o L] . i i i ' i " ' i n * l "nd6mnid lo ,a t '1 r$oo '9ae ' *nare6 ' : , i , i i "nnn.s i io ; { ' , i .Nsddd'r. t-n:
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3'Ji;::i:,m^'tf:3.'illli'i*:?fJliP','€*":ii#l;iik"," '""doneid-" *vbfi;;;;ih;i6.1eiii"brih" ""
Test Report No.:CE201?'13191 Date:2013101121 Page: 22 of 29
CEMMTEC GIVBHGESCHAFTSBEREICH
rtl ltrt ttlllllMULTIFUNKTIONSKERAI/|IK,LUITPOLDSTRABE 15, 91207 LAUF
PCNS analytical flow chart
r Name ofthe person who made measurement: BarryTsengI Name of the person in charge of measurement; Troy Chang
Data
Test Report No.: CE/201313191 DaIe 2013101121 Paqe: 23 of 29
CERAMTEC GMBHGESCHAFTSBEREICH IVULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE 15. 91207 LAUF
tn[lnl|l l|l]t]
Analytical flow chad of phthalate content
I Name of the person who made measufementr Roman Wongr Name of the pe6on in charge of measurement: Troy Chang
Data
' ' r i n l ! r i r r f t i3 r l ' i
Concentrate./Dilute Extracted solution
An€lysis was perfomed by GC/MS
Test Report No. : CE/2013/13191 Dale : 2013101121
CERAMTEC GMBHGESCIIAFTSBEREICH
Page:24 ol 29
91207 LAUFll| |l!] |lttl
I,IULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 1 5,
I
I
Formaldehyde analytical flow chart
Name of the pe6on who made measurement: Scott KuN€me of the person in charge of measurement: Troy Chang
I Test Method : US EPA 83154 ' ISO 17226-1 ]
Dala
Derived by DNPH ConcentrateJDilute Extractedsolution
Test Report No. :CE/2013 /13191Dale'.2013101121Page : 25 of 29
Analyais flow chart for determination of PVC In material
CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAI,!IK.LUITPOLDSTMBE 1 5. 9'1 207 LAUF
||]tIltt][t [Il
I
I
Name ofthe person who made measurement: Ginny ChenName of the person in charge of measurement: Troy Chang
Sample analyzed by FTIR
Check wave-number of c-cl bonding
Test Report No. CE2013,/13191 Dale:2O1AO1121 Page : 26 of 29
CERAMTEC GMBHGESCHAFTSBEREICH
|ln[ t][tll]rMULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF
II
DBBT analytical flow chart
Name ofthe pe6on who made me€surement Roman WongName ofthe person in charge of measurement: Troy Chang
Dala
. i : r , i l r 1 i l i t - l j
Sample pretreatmenvseparation
Sample extraction by 6oxhlet method
Test Report No.:CEl2013/13191Dale: 2o13lo1nl Page 27 ot 29
CERAI.TTEC GI,/IBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAI/|IK,LUITPOLDSTRABE'1 5, 9'1 207 LAUF
Analytical flow chart of halogen content'1) Name of the oerson vt/t|o made measurement: Rita Chen2) Name of the person in charge of measurement: Troy Chang
||l ||tt]tI|tttll
9fj] iH*"", ';:* ' ' ,*.- '"], ' ' , ;;"...""*.l"i"".-".n.*,." ' '-"*"'.n-.*'."1' ; ; t i ; d f u .bmddmmmE' *oFdhh rsmdcodbn 'b ; ; i . nn . cDo6m{ | J# { , od 'ri,:"luri6'in
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r i in i i , " j r . * lo i rua i r " monoodm. . ' i ' doo .ne1rcomoanv try unau,tu'z& abad.,-q.ry * I'kh*- drb-tu;it;iFt€ne or th sdturud smawtu
i. ., + i _ri;\l
lFli33!1
Sample pretreatment / separation
Wdghting and putting sample in cell
Oxygen Bomb Cornbustion / Absorption
Dilution to fixed volume
Analysis was performed by lC
Test Report No. : CE/20'13/13191Dai'e : 2O13101n1 Page : 28 of 29
CERAMTEC GMBHGESCHAFTSBEREICH l/TULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 1 5, 91207 LAUF
Analytical flow chart ofvolatile organic compounds (VOCS)
I Name ofthe oe6on who made measurement : Chun WuI Name of the person in charge of measurernent : Shinjyh Chen
(Reference method : US EPA 5021)
lfl||tt][ttl||ll
Sample pretreatment
Take sample and put it intoheadspace glassware.
Analy6is was per{ormed by GCYlrs
Test Report No. : CE2013/13191D e: 2013101121Page : 29 of 29
cERAlilTEC GIVBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[/|IK,LUITPOLDSTRABE 15, 91207 LAUF
'The tested sample/ part is ma*ed by an arrow if ifs shown on lhe photo.'
'* End of Repod "
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kNewr i t s i . i vL {$ i , : - : ' . ! r , d r i i i l i l f n r \ i
Test Report Number: SHAH00361401
Authorized by: For intertek testing services Ltd., Shanghai
Jacob Lin General Manager
Page 1 Of 4 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
Applicant: LITTELFUSE,INC. Date: JAN 16, 2013 800 E. NORTHWEST HWY Attn: A.DIVIETRO/D.UNTIEDT
Sample Description: One (1) submitted sample said to be Grey Wire. Item Name : Wire Tin Plated Cu. Part No. : Element.
************************************************************************************************************************************************************ Tests Conducted:
As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************
To be continued
Test Report Number: SHAH00361401
Tests Conducted
Page 2 Of 4 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅰ) Test Result Summary: Testing Item Result (ppm)
(1) Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg With 50cm2) Negative (< 0.02)
Testing Item Result (ppm)
(2) Heavy Metal Cadmium (Cd) content / Plating ND Lead (Pb) content / Plating 60 Mercury (Hg) content / Plating ND Chromium VI (Cr6+) content (mg/kg With 50cm2) / Plating Negative (< 0.02)
Remarks: ppm = parts per million = mg/kg
ND = not detected @ = Due to the insufficient sample area, reduced total sample surface of 10 cm2 was used and the dilution factor
was adjusted accordingly. mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Tested components:
(1)Substrate. (2)Plating. Responsibility of Chemist: Dent Fang / Ken He
(Ⅱ) RoHS Requirement:
Restricted substances Limits Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)
The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.
(Ⅲ) Test Method:
Testing item Testing method Reporting limit
Cadmium (Cd) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in Annex B, by boiling water extraction and determined by UV-VIS Spectrophotometer.
0.02 mg/kg with 50cm2
Remark:Reporting limit = Quantitation limit of analyze in sample Date Sample Received:Jan.9, 2013 Testing Period:Jan.9, 2013 to Jan.14, 2013
************************************************************************************************************************************************************ To be continued
Test Report Number: SHAH00361401
Tests Conducted
Page 3 Of 4 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅳ) MEASUREMENT FLOWCHART: Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs contents Reference standard: IEC 62321 edition 1.0:2008 REMARKS: *1: LIST OF APPROPRIATE ACID:
MATERIAL ACID ADDED FOR DIGESTION Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4
*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED. ************************************************************************************************************************************************************
To be continued
Sampling/grinding or cutting
Weigh sample and for different material,
digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized water and add Diphenyl-
carbazide solution
Cr6+
Weigh sample andadd organic
solvent
Soxhlet extractionor
Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
Spot test
Get 50cm2 samples
Boiling water extraction
Metal Polymers / electronics
Negative*2
Confirm the tested samples are totally
dissolved
No
Cool and filter the extract
Yes
Test Report Number: SHAH00361401
Tests Conducted
Page 4 Of 4 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
***********************************************************************************************************************************************************
End of report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
SGqT€st Report
Testing Period :
Test Requested :
T€st Method :
Test Result6 :
Conclusion :
No. SHAECl215842621 Date: 13 Sep 2012 Page 1 of4
CHINALO LUOYANG COPPER CO., LTD.
NO,50.JIANSHE ROAD,LUOYANG.HENAN PROVINCE
The following sample(s) was6^/ere submitted and identfred on behalf of the clienb as : C10100(Tul)
SGS Job No. : sP12-027024 - SH
Date of Samole Received : 1 0 SeD 201 2
10 Seo 2012 - 13 SeD 2012
Selected tast(s) as requested by client.
Please refer to next page(s).
Plea66 refer to next page(s).
Bas€d on the performed tesb on 6ubmitted samples, the resulb of Lead,I\rercury, Cadmium, Hexavalent chromium comply wth the limits as set by RoHSDiredive 2011/65/EU Annex ll; recasting 200295/EC.
Signed for and on behalf ofscs-csrc Ltd.
,zQr"-Fan Jingjie, JJApproved Signatory
ryr{xrbrro-n'cFddd.ors{ "d *dn'bh rrbdsrh {r'@'f!qqrird-:miEr-
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t'in!|n,olt iod)qrlffii4li.Ciror! 20@3{t.til.ltraldll$e+391 lr:2M3
IEIE{6-g1)0L660 lE{E(6-il)610536D ffi 6.!..d
NrlE-21)614@4 HL(F21)t$qS3 .llidtEe.S@
Menb6. oi rh€ scs grouD lSGs s.{)
T€6t Report No. SHAEC1215842621 Date: 13 Sep 2012 Page2d4
Test R€sults :
Test Part Descaiption :
Sp€dmonNo. SGSS€mPlolD D6qiDdon1 SHA'12-158426 015 Copper metalsheet
Rema*s :(1) 1 mg/kg= 1 PPm=00001%(2) MDL = Method Detec{ion Limit
(3) ND = Not o€teded ( < MoL )(4) "'' = Not Regulated
Rolls Oil€ ive 201 1r85/EU
Test Method: With reference to IEC 6232'1:2008(1) Determination of Cadmium by ICP-OES(2) Determination of Lead bv ICP-OES'(3) Determination of Mercury by ICP-OES'(4) Determination of Hexavaler{ Chromium by Spot t€€t / Colodmetric lvelhod using Uv-vis
Te6t ltem{s)
Cadmium (Cd)
Lead (Pb)
Merdry (Hg)
Hexavalent Chrornium (Cr(Vl))
Notes :(1) The maximum permissible limit is quoted from direciive 2011/65/EU Annex ll
(2) osPot-test:N;gative = Absence of Cr(Vl) coating, Positive = Presenc€ of Cr(Vl) coating;.
Oh-e tested sample should be fufte; verified by boiling-wateFertrac'tion method if the spot test resuft
is Negative or cannot be confmed )o goiling-water-extraction:Negative = Absence of Cr(Vl) coatingpositive = presence of Cr(vt) coating; the detected conc€ntration in boiling-water-extraction solution is
equal or greater than O.O2 mg/kg with 50 cm" sample surface area
For conilon proteclion coating; on metals: Information on storage @nditions and prcducton date of
the tested sample is unavailable and thus results of Cr(Vl) rspres€nt status of the sample at the time
of testing-
t!nj! Ud! MpL pE
10O mSikS 2 ND1OOO msftg 2 ND1O0O mS/kS 2 ND
Negative
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r ElE {*-er)etoanrr j (i-a!1614s04
Test Report No. SHAEC121584262'1 Date: 13 Sep 2012 Page 3 of 4
ATTACHMENTS
RoHs Testing Flow chart
1) Name of the p€rson who made testing: Jan Shi^/oyo Wangy'Allen xiao2t Name oI the person in charge of testing: Jeff Zhang/George Xusiil;;;;;;;;; tisioiilo totarrv o'v pr*conditionrng methoo accordrng ro oero/ now chart (cf*
test method excluded)
Sample Preparation
Heating to g0-95cfor extraction
1) Alkali Fusion /DryAshing
2) Acid to dissolve
Adding'1,5-diphenylcarbazide
for colordevelopment
A red color indicatesthe presence of cf'lf nec€ssary, confirm
PbrcdrHg
Positive
Negative
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Test Report
Sample photo:
No. SHAEo1215842621 Date: 13 Sep 2012 Page 4 of 4
SGS adhenticate the photo on odginal repod only
"' End of Report *'
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Test Report No. SHAECl216714748 Date: 25 Sep 20 1 2 Page 1 of 5
ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO'' LTD
XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE' CHINA
The follorving sample(s) wasl/verc submitted and identified on behalf of the clienb as : LEAD'FREE SOLOER
WIRE
sGS Job No. :
Part No. (P/N) :
Composition :
Date ol Sample Received :
Testing Period :
Test Reqlested :
Test Method :
Test Resulb :
Condusion :
sP12-028285 - SH
YTW1o8 (692535-001' 692535-003 )
Sn3.0CuRE21 gep 2012
21 Sep 2012 - 25 seq 20 12
Seleded test(s) as requested by client.
Please refer to next page(s).
Ple€se refer to next Page(s)Based on the perfrcrmed tests on submitted samples, the results of Lead'
Mercury, cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB)' -Polybrominatecl diphenylethe6 (PBDE) comply with the limits as set by RoHS
Direciive 2011/6tEu Annex lli recasting 200295/EC.
Signed for and on behalf ofsc$csrc Ltd.
,zQv"-Fan Jingjie, JJApproved Signatory
rhb@drb &.d tt tu cqryry aDld b b-
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108{S.?r)61{!!anL(d-21nl4@a
ri.rnb.lol0|. Sos oollP (8oS S )
Teet Report
Test Resufts :
No. SHAEC1216714748 Date; 25 Sep 2012 Page 2 of 5
Test Part Desc.iption :
SpodmqrNo. SGSSandolD D*qiptlon1 SHA'12167147.041 Silvery wire
Rema*€ :(1 ) I mg /kg= 1 PPm=00001%(2) MDL = Method Detedion Limit
(3) ND = Not Detected ( < NIDL )(4)
"" = Not Regulated
RoHS Diradv€ 201 1/65/EU
Test Method : with reference to lEc 62321i2008(1) Determination of Cadmium by ICP-OES.(2) Oetemination of Lead by ICP-oES(3) Determination of Merdiry bv ICP'OES(4) Determination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis
(5) Determination of PBBS / PBDES by GC-MS'
Test ltem(s)
Cadmium (Cd)
Lead (Pb)
Mercury (Hs)
Hexavalent Chromium (Cr(Vl))
Sum ol PBBSMonobrcmobiphenylDibrcmobiphenylTribromobiphenylTetrabromobiPhenylPentabromobiphenYlHexabromobtphenylHeptabromobiPhenylOctabromobiphenylNonabromobiphonylDecabromobiPhenylSum of PBDESMonobromodiphenyl ether
Limit ud! M0!100 mg/kS 2
1000 mSftS 2
1000 mS/kg 2o
1000 mgkg- mSikS 5- mdkS 5- mS/kS 5- ms/ks 5- mdkS 5- mg/kg 5- mg/kg 5- mgftS 5
mdkg 5- mS/kg 5
1000 mS/kg- mdkg 5
@1ND55ND
NegativeNDNDNDNDNDNDNDNDNDNDNONDND
;i;a' ir*&{.d n dnl.,.d/bb 6rr.{.tt.d '
tlrr'ttafi$bDd|rddna.{rofr !93{l -I*.*trBlt!l8aea3+l aI: 2@
rE E6+r)B1a@ IEE€GA)6|€Sdrgnj{c-2rtauozg $i6GA)4|d063
M.n&r ot fi. Soa or.r0 (8Gs sA)
sGqTest Report
Test ltem{s)
Dibromodiphenyl etherTribromodiphenyl etherTelrabromodiphenyl elherPentabrcmodiphenyl etherHexabromodiphenyl etherHeptabromodiphenyl elherOctabromodiphenyl elherNonabromodiphenyl ethetDecabromodiphenyl ether
Notes :(1) The maximum permissible limit is quoted ffom direclive 2011/65/EU' Annex ll(2) ospoltest:
Negative = Absence of Cr(Vl) coating, Positive = Presence of Cr(Vl) coating;
Ohe tested sample should be further vedfied by boiling-wateFexlraction method if the spot test result
is Negative or cannot be confimed-)oBoiling-wateFextraction:Negative = Absence of Cr(Vl) coatingpositive = Presence of Cr(Vl) coating; the detected concentration in boiling-wateFextraction solution is
equal or greater than O.O2 mg/kg with 50 crn" sample surface areaForcorosionprotectioncoatingsonmeta|s:|nformationonstorageconditionsandproducliondateofthe tested sample is unavailable and thus results of Cr(Vl) represent status of the sample at the time
of testing.
No. SHAEC1216714748 Date: 25 Sep 2012
ud! Mot @1mg/kS 5 NDmS/kS 5 NDmdks 5 NDmSikS 5 NDmg/kS 5 NDmSftS 5 NDmdkS 5 NDmS/kS 5 NDmdkS 5 ND
Page 3 of 5
tird!
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€mD.r ot !h. sGE GrcuP (8GS SA)
Test R€port No. SHAECl216714748 Date: 25 Sep 2012 Pag€ 4 of 5
ATTACHMENTS
RoHS Testing Flow Chart
1) Name of the person who made testing: Jan Shi/Yoyo Wangr'Allen XiaolGaryXu2) Name of the person in charge of testing: Jeff Zhanglceorge Xu/ Linda Li3) These sampleswere dissolved lotally by pre-conditioning method according to betow flow chart. (Cf'
and PBB!,/PBDES test method excluded)
Sample PrepaEtion
1) Alkali Fusion /DryAshing
2) Acid to dissolve
Heating to 90-957for extraction
Adding 1,5-diphenylcalbaAde
for colordevelopment
Adding 1,5-diphenylcarbaade
for colordevelopment
A rcd colorindicatesthe
presence of cr8t.necessary,
Pb/CdHg PBBs/PBDES
t6&tttY|laf{dpdtrd,st{iatr @'Fr.-*.ltrEtdttidotsr+l lr:2@3
r ErE F2!) 8r@53rll Fzl6lil&5aa
I€EF{|FMDrij F€i)i6063
lLint r ot th.sos Gro{p (8GS s,l)
Teet Report
Sample photo:
No. SHAEC1216714748 Oate: 25 Sep 2012 Page 5 of 5
sHA12-167147.041
SGS authenticate the photo on odginal report only
". End of Report '_
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Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SH AH00334352
AUTHORIZED BY: FOR INTERTEK TESTING SERVICES LTD., SHANGHAI
JACOB LIN GENERAL MANAGER
PAGE 1 OF 8
APPLICANT: LITTELFUSE,INC. DATE: AUG 15, 2012 800 E. NORTHWEST HWY ATTN: A. CESISTA/ K. BACILA
SAMPLE DESCRIPTION: One (1) submitted sample said to be White Yarn. Part Description : Yarn. Part Number : 648102.
***************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SH AH00334352
TESTS CONDUCTED
PAGE 2 OF 8
1 ( Ⅰ) Test Result Summary:
TESTING ITEM R ESULT (ppm)
HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MonoBB) ND DIBROMINATED BIPHENYLS (DiBB) ND TRIBROMINATED BIPHENYLS (TriBB) ND TETRABROMINATED BIPHENYLS (TetraBB) ND PENTABROMINATED BIPHENYLS (PentaBB) ND HEXABROMINATED BIPHENYLS (HexaBB) ND HEPTABROMINATED BIPHENYLS (HeptaBB) ND OCTABROMINATED BIPHENYLS (OctaBB) ND NONABROMINATED BIPHENYLS (NonaBB) ND DECABROMINATED BIPHENYL (DecaBB) ND POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MonoBDE) ND DIBROMINATED DIPHENYL ETHERS (DiBDE) ND TRIBROMINATED DIPHENYL ETHERS (TriBDE) ND TETRABROMINATED DIPHENYL ETHERS (TetraBDE) ND PENTABROMINATED DIPHENYL ETHERS (PentaBDE) ND HEXABROMINATED DIPHENYL ETHERS (HexaBDE) ND HEPTABROMINATED DIPHENYL ETHERS (HeptaBDE) ND OCTABROMINATED DIPHENYL ETHERS (OctaBDE) ND NONABROMINATED DIPHENYL ETHERS (NonaBDE) ND DECABROMINATED DIPHENYL ETHER (DecaBDE) ND HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) ND BROMINE (Br) ND IODINE (I) ND
REMARKS: ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
RESPONSIBILITY OF CHEMIST: DENT FANG / KEN HE *****************************************************************************************************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SH AH00334352
TESTS CONDUCTED
PAGE 3 OF 8
(Ⅱ) ROHS REQUIREMENT:
RESTRICTED SUBSTANCES LIM ITS
CADMIUM (Cd) CONTENT 0.01% (100ppm) LEAD (Pb) CONTENT 0.1% (1000ppm) MERCURY (Hg) CONTENT 0.1% (1000ppm) CHROMIUM VI (Cr6+) CONTENT 0.1% (1000ppm) POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm) POLYBROMINATED DIPHENYL ETHERS (PBDEs) 0.1% (1000ppm)
THE ABOVE LIMITS WERE QUOTED FROM ROHS DIRECTIVE 2002/95/EC AND AMENDMENT 2005/618/EC FOR HOMOGENEOUS MATERIAL.
(Ⅲ) TEST METHOD:
TESTING ITEM TE STING METHOD REPORTING LIMIT
CADMIUM (Cd) CONTENT
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.
2 ppm
LEAD (Pb) CONTENT
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.
2 ppm
MERCURY (Hg) CONTENT WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.
2 ppm
CHROMIUM VI (CR6+) CONTENT
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX C, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER.
1 ppm
POLYBROMINATED BIPHENYLS (PBBs)
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.
5 ppm
POLYBROMINATED DIPHENYL ETHERS (PBDEs)
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.
5 ppm
REMARK:REPORTING LIMIT = QUANTITATION LIMIT OF ANALYZE IN SAMPLE
Date Sample Receive:AUG.9, 2012 Test Period: AUG.9, 2012 To AUG.15, 2012 RESPONSIBILITY OF CHEMIST: KEN HE
***************************************************************************************************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SH AH00334352
TESTS CONDUCTED
PAGE 4 OF 8
(Ⅳ) MEASUREMENT FLOWCHART: TEST FOR Cd/ Pb/ Hg/Cr (VI)/ PBBS/PBDES CONTENTS REFERENCE STANDARD: IEC 62321 EDITION 1.0:2008
***************************************************************************************************************************************************** TO BE CONTINUED
Sampling/grinding or cutting
Weigh sample and for different material,
digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized water and add Diphenyl-
carbazide solution
Cr6+
Weigh sample and add organic
solvent
Soxhlet extractionor
Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
Spot test
Get 50cm2 samples
Boiling water extraction
Metal Polymers / electronics
Positive*2
Confirm the tested samples are totally
dissolved
No
Cool and filter the extract
Yes
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SH AH00334352
TESTS CONDUCTED
PAGE 5 OF 8
REMARKS: *1: LIST OF APPROPRIATE ACID: MATERIAL ACID ADDED FOR DIGESTION POLYMERS HNO 3,HCL,HF,H2O2,H3BO3 METALS HNO 3,HCL,HF ELECTRONICS HNO 3,HCL,H2O2,HBF4
*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED.
***************************************************************************************************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SH AH00334352
TESTS CONDUCTED
PAGE 6 OF 8
2 ( ) Ⅰ Test Result Summary :
Testing Item Result (ppm)
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND
Remarks: ppm = Parts per million = mg/kg ND = Not detected
(Ⅲ) Test Method:
Testing Item T esting Method R eporting Limit
Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography 50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
***************************************************************************************************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SH AH00334352
TESTS CONDUCTED
PAGE 7 OF 8
(Ⅳ) Measurement Flowchart:
Test For Halogen Content Reference Standard: EN 14582
*****************************************************************************************************************************************************
TO BE CONTINUED
add absorbent in a combustion flask & place weighed sample in equipment
fill the combustion flask with oxygen
ignite then leave the flask at room temperature
transfer the absorbent into a volumetric flask
make up with deionized water
sampling/grinding or cutting
analyzed by ion chromatography
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SH AH00334352
TESTS CONDUCTED
PAGE 8 OF 8
*****************************************************************************************************************************************************
END OF REPORT
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
TEST REPORT NUMBER: SH AH00355828
AUTHORIZED BY: FOR INTERTEK TESTING SERVICES LTD., SHANGHAI
JACOB LIN GENERAL MANAGER
PAGE 1 OF 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
APPLICANT: LITTELFUSE,INC. DATE: DEC 13, 2012 800 E. NORTHWEST HWY AT TN: A.DIVIETRO/D.UNTIEDT
SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE WHITE POWDER. ITEM NAME : FILLER. PART NO. : 090187.
***************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************
TO BE CONTINUED
TEST REPORT NUMBER: SH AH00355828
TESTS CONDUCTED
PAGE 2 OF 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
1 (Ⅰ) Test Result Summary:
TESTING ITEM R ESULT (ppm)
HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MonoBB) ND DIBROMINATED BIPHENYLS (DiBB) ND TRIBROMINATED BIPHENYLS (TriBB) ND TETRABROMINATED BIPHENYLS (TetraBB) ND PENTABROMINATED BIPHENYLS (PentaBB) ND HEXABROMINATED BIPHENYLS (HexaBB) ND HEPTABROMINATED BIPHENYLS (HeptaBB) ND OCTABROMINATED BIPHENYLS (OctaBB) ND NONABROMINATED BIPHENYLS (NonaBB) ND DECABROMINATED BIPHENYL (DecaBB) ND POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MonoBDE) ND DIBROMINATED DIPHENYL ETHERS (DiBDE) ND TRIBROMINATED DIPHENYL ETHERS (TriBDE) ND TETRABROMINATED DIPHENYL ETHERS (TetraBDE) ND PENTABROMINATED DIPHENYL ETHERS (PentaBDE) ND HEXABROMINATED DIPHENYL ETHERS (HexaBDE) ND HEPTABROMINATED DIPHENYL ETHERS (HeptaBDE) ND OCTABROMINATED DIPHENYL ETHERS (OctaBDE) ND NONABROMINATED DIPHENYL ETHERS (NonaBDE) ND DECABROMINATED DIPHENYL ETHER (DecaBDE) ND
REMARKS: ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(Ⅱ) ROHS REQUIREMENT: RESTRICTED SUBSTANCES LIM ITS
CADMIUM (Cd) CONTENT 0.01% (100ppm) LEAD (Pb) CONTENT 0.1% (1000ppm) MERCURY (Hg) CONTENT 0.1% (1000ppm) CHROMIUM VI (Cr6+) CONTENT 0.1% (1000ppm) POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm) POLYBROMINATED DIPHENYL ETHERS (PBDEs) 0.1% (1000ppm)
THE ABOVE LIMITS WERE QUOTED FROM ROHS DIRECTIVE 2002/95/EC AND AMENDMENT 2005/618/EC FOR HOMOGENEOUS MATERIAL.
***************************************************************************************************************************************************** TO BE CONTINUED
TEST REPORT NUMBER: SH AH00355828
TESTS CONDUCTED
PAGE 3 OF 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
2 (Ⅰ) Test Result Summary:
TESTING ITEM R ESULT (ppm)
HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) ND BROMINE (Br) ND IODINE (I) ND
REMARKS: ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
(Ⅲ) TEST METHOD:
TESTING ITEM T ESTING METHOD REPORTING LIMIT
HALOGEN CONTENT WITH REFERENCE TO EN 14582:2007 BY COMBUSTION FLASK WITH OXYGEN AND DETERMINED BY ION CHROMATOGRAPHY 50 ppm
***************************************************************************************************************************************************** TO BE CONTINUED
TEST REPORT NUMBER: SH AH00355828
TESTS CONDUCTED
PAGE 4 OF 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅲ) TEST METHOD:
TESTING ITEM T ESTING METHOD REPORTING LIMIT
CADMIUM (Cd) CONTENT
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.
2 ppm
LEAD (Pb) CONTENT
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.
2 ppm
MERCURY (Hg) CONTENT WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.
2 ppm
CHROMIUM VI (CR6+) CONTENT
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX C, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER.
1 ppm
POLYBROMINATED BIPHENYLS (PBBs)
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.
5 ppm
POLYBROMINATED DIPHENYL ETHERS (PBDEs)
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.
5 ppm
REMARK:REPORTING LIMIT = QUANTITATION LIMIT OF ANALYZE IN SAMPLE
***************************************************************************************************************************************************** TO BE CONTINUED
TEST REPORT NUMBER: SH AH00355828
TESTS CONDUCTED
PAGE 5 OF 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅳ) MEASUREMENT FLOWCHART: TEST FOR Cd/ Pb/ Hg/Cr (VI)/ PBBS/PBDES CONTENTS REFERENCE STANDARD: IEC 62321 EDITION 1.0:2008
REMARKS: *1: LIST OF APPROPRIATE ACID: MATERIAL ACID ADDED FOR DIGESTION POLYMERS HNO 3,HCL,HF,H2O2,H3BO3 METALS HNO 3,HCL,HF ELECTRONICS HNO 3,HCL,H2O2,HBF4
*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED.
***************************************************************************************************************************************************** TO BE CONTINUED
Sampling/grinding or cutting
Weigh sample and for different material,
digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized water and add Diphenyl-
carbazide solution
Cr6+
Weigh sample andadd organic
solvent
Soxhlet extractionor
Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
Spot test
Get 50cm2 samples
Boiling water extraction
Metal Polymers / electronics
Positive*2
Confirm the tested samples are totally
dissolved
No
Cool and filter the extract
Yes
TEST REPORT NUMBER: SH AH00355828
TESTS CONDUCTED
PAGE 6 OF 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅴ) MEASUREMENT FLOWCHART: TEST FOR HALOGEN CONTENT REFERENCE STANDARD: EN 14582
*****************************************************************************************************************************************************
TO BE CONTINUED
Add absorbent in a combustion flask & place weighted sample in equipment
Fill the combustion flask with Oxygen
Ignite then leave the flask at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by Ion Chromatography
TEST REPORT NUMBER: SH AH00355828
TESTS CONDUCTED
PAGE 7 OF 7 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
*****************************************************************************************************************************************************
END OF REPORT
This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
TEST REPORT NUMBER: SH AH00355836
AUTHORIZED BY: FOR INTERTEK TESTING SERVICES LTD., SHANGHAI
JACOB LIN GENERAL MANAGER
PAGE 1 OF 8 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
APPLICANT: LITTELFUSE,INC. DATE: DEC 13, 2012 800 E. NORTHWEST HWY AT TN: A.DIVIETRO/D.UNTIEDT
SAMPLE DESCRIPTION: ONE(1) SUBMITTED SAMPLE SAID TO BE BEIGE POWDER. ITEM NAME : FILLER. PART NO. : 090184. ******************************************************************************************************************************************************
TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
****************************************************************************************************************************************************** TO BE CONTINUED
TEST REPORT NUMBER: SH AH00355836
TESTS CONDUCTED
PAGE 2 OF 8 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
1 ( Ⅰ) Test Result Summary:
TESTING ITEM R ESULT (ppm)
HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MonoBB) ND DIBROMINATED BIPHENYLS (DiBB) ND TRIBROMINATED BIPHENYLS (TriBB) ND TETRABROMINATED BIPHENYLS (TetraBB) ND PENTABROMINATED BIPHENYLS (PentaBB) ND HEXABROMINATED BIPHENYLS (HexaBB) ND HEPTABROMINATED BIPHENYLS (HeptaBB) ND OCTABROMINATED BIPHENYLS (OctaBB) ND NONABROMINATED BIPHENYLS (NonaBB) ND DECABROMINATED BIPHENYL (DecaBB) ND POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MonoBDE) ND DIBROMINATED DIPHENYL ETHERS (DiBDE) ND TRIBROMINATED DIPHENYL ETHERS (TriBDE) ND TETRABROMINATED DIPHENYL ETHERS (TetraBDE) ND PENTABROMINATED DIPHENYL ETHERS (PentaBDE) ND HEXABROMINATED DIPHENYL ETHERS (HexaBDE) ND HEPTABROMINATED DIPHENYL ETHERS (HeptaBDE) ND OCTABROMINATED DIPHENYL ETHERS (OctaBDE) ND NONABROMINATED DIPHENYL ETHERS (NonaBDE) ND DECABROMINATED DIPHENYL ETHER (DecaBDE) ND
REMARKS:ppm = PARTS PER MILLION = mg/kg
ND = NOT DETECTED
RESPONSIBILITY OF CHEMIST: DENT FANG / LEAF LIU (Ⅱ) ROHS REQUIREMENT:
RESTRICTED SUBSTANCES LIM ITS
CADMIUM (Cd) CONTENT 0.01% (100ppm) LEAD (Pb) CONTENT 0.1% (1000ppm) MERCURY (Hg) CONTENT 0.1% (1000ppm) CHROMIUM VI (Cr6+) CONTENT 0.1% (1000ppm) POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm) POLYBROMINATED DIPHENYL ETHERS (PBDEs) 0.1% (1000ppm)
THE ABOVE LIMITS WERE QUOTED FROM ROHS DIRECTIVE 2002/95/EC AND AMENDMENT 2005/618/EC FOR HOMOGENEOUS MATERIAL.
****************************************************************************************************************************************************** TO BE CONTINUED
TEST REPORT NUMBER: SH AH00355836
TESTS CONDUCTED
PAGE 3 OF 8 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅲ) TEST METHOD:
TESTING ITEM T ESTING METHOD REPORTING LIMIT
CADMIUM (Cd) CONTENT
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.
2 ppm
LEAD (Pb) CONTENT
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.
2 ppm
MERCURY (Hg) CONTENT WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.
2 ppm
CHROMIUM VI (CR6+) CONTENT
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX C, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER.
1 ppm
POLYBROMINATED BIPHENYLS (PBBs)
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.
5 ppm
POLYBROMINATED DIPHENYL ETHERS (PBDEs)
WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.
5 ppm
REMARK:REPORTING LIMIT = QUANTITATION LIMIT OF ANALYZE IN SAMPLE
****************************************************************************************************************************************************** TO BE CONTINUED
TEST REPORT NUMBER: SH AH00355836
TESTS CONDUCTED
PAGE 4 OF 8 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅳ) MEASUREMENT FLOWCHART: TEST FOR Cd/ Pb/ Hg/Cr (VI)/ PBBS/PBDES CONTENTS REFERENCE STANDARD: IEC 62321 EDITION 1.0:2008
REMARKS: *1: LIST OF APPROPRIATE ACID: MATERIAL ACID ADDED FOR DIGESTION POLYMERS HNO 3,HCL,HF,H2O2,H3BO3 METALS HNO 3,HCL,HF ELECTRONICS HNO 3,HCL,H2O2,HBF4
*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED.
****************************************************************************************************************************************************** TO BE CONTINUED
Sampling/grinding or cutting
Weigh sample and for different material,
digest the sample with appropriate acid*1
Make up with deionized water
Cd/Pb/Hg
Analyzed by ICP-OES
Weigh sample and add alkaline
solution
Definite temp. Extraction
Make up with deionized water and add Diphenyl-
carbazide solution
Cr6+
Weigh sample andadd organic
solvent
Soxhlet extractionor
Solvent extraction
Concentrate the extract and make up with organic
solvent
PBBs/PBDEs
Analyzed by UV-VIS
Analyzed by GC-MSD
Spot test
Get 50cm2 samples
Boiling water extraction
Metal Polymers / electronics
Positive*2
Confirm the tested samples are totally
dissolved
No
Cool and filter the extract
Yes
TEST REPORT NUMBER: SH AH00355836
TESTS CONDUCTED
PAGE 5 OF 8 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅴ) MEASUREMENT FLOWCHART: TEST FOR HALOGEN CONTENT REFERENCE STANDARD: EN 14582
****************************************************************************************************************************************************** TO BE CONTINUED
Add absorbent in a combustion flask & place weighted sample in equipment
Fill the combustion flask with Oxygen
Ignite then leave the flask at room temperature
Transfer the absorbent into a volumetric flask
Make up with deionized water
Sampling/grinding or cutting
Analyzed by Ion Chromatography
TEST REPORT NUMBER: SH AH00355836
TESTS CONDUCTED
PAGE 6 OF 8 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
2 ( ) Ⅰ Test Result Summary :
Testing Item Result (ppm)
Halogen Content Fluorine (F) ND Chlorine (Cl) 100 Bromine (Br) ND Iodine (I) ND
Remarks: ppm = Parts per million = mg/kg N D = Not detected
Responsibility Of Chemist : Grace Wang
(Ⅲ) Test Method:
Testing Item T esting Method R eporting Limit
Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography 50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Date Sample Received : Dec.5, 2012 Testing Period : Dec.5, 2012 To Dec.11, 2012
****************************************************************************************************************************************************** TO BE CONTINUED
TEST REPORT NUMBER: SH AH00355836
TESTS CONDUCTED
PAGE 7 OF 8 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
(Ⅳ) Measurement Flowchart:
Test For Halogen Content Reference Standard: EN 14582
****************************************************************************************************************************************************** TO BE CONTINUED
add absorbent in a combustion flask & place weighed sample in equipment
fill the combustion flask with oxygen
ignite then leave the flask at room temperature
transfer the absorbent into a volumetric flask
make up with deionized water
sampling/grinding or cutting
analyzed by ion chromatography
TEST REPORT NUMBER: SH AH00355836
TESTS CONDUCTED
PAGE 8 OF 8 Intertek Testing Services Ltd., Shanghai
Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司
上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740
www.intertek.com www.intertek.com.cn
******************************************************************************************************************************************************
END OF REPORT This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.
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Cuslomer: Suzhou FuHong Electronic IndustriatCo., 16.
Addr6s: NO.89 \/ElDU ROAD, WANGTING TOVIN, XTANGCHENG DISTR|CI SUZHOU. CHINARepod on the submltted samrl€ said to be
sample name: Lead wife coppershell
Modol:/
Itefi/Lot Io.: /Matonal:/Buyen/ :S u p p l i e r : / ,
l i lanufacturE:/- . _ - i
- fSample recelved date: Gq _08, 2012 :t*,tn o"n.o, t.. o".;;,,013
"."r.-,.,,613, 1 ,]
&glirs-Bgsccsgq i
As specifed by dienl, to determine the L€ad, Cadrium, l,tercury & tiexayabntChrcmium conle in the 6ubmitted sampte inaccodance with Directive 2OO2I95/EC {RoHS). j
l\OV'BF.F.q,A
TEST REPORTNO.: 4002R121008024-2R02 Oate: Oct.1 0, 2012
Testing ltem Measufing instrument ,MQL
Lead (Pb) IEC 62321:2008. section I rcP-oEs a!gagcadmium (Cd) IEC 62321:2008, s€ction 9 tcP-oEs 2 mg/kg
[,lercury (Hg) IEC 62321r2008, s€ction 7 rcP-oEs 2 mg/kg
Chromium (CrM) IEC 62321: 2008, Annex B 0.02mg/kg*
Testino method:
lsqj 0.02 mg/tg rcturs to the MQL olsample exlraction liquid.
Conclu3ion:-\ryhen tested as specified lhe submilied sample compried with th€ requircments of commission D€cision of 18 Aug 2005
amending Dircctive 2002/95/EC notilied under docum€nt 2005/618/EC.
LiTingting, Maggie
Chemical Test Direclor
Yuan Qi, l,lickey
LabManager
Sign€d ior and on behallol
Shenzhen AOV Testing Technology Co., Ltd, Kunshan 8ran6h
ea"arc"a"r, A?1 W a l b n OrO."*0r44
."*FOR FURTHER DETAILS, PLEASE REFERTOT
Technical Di€clor
STIENZIIEN AOVTE$Tl'{G I€CHI!OLOGY CO,.I.TD,KUNSHAN BRANCI]
(,10",'ll,,u*
l\ov"BF,?sn
NO.: A0O2R12100802+2R02
T63l Flow:
Cooling the vessel, fiitei washed and
fllled lo the mafK with distilled waler.
Add the digestion solulionj thevess€l is heated until the sample
TEST REPORTDate Oci .10,2012
L To Detemine/lead, Cldmium Content (Metal substrale)lestedbY
L7.^otq,
-*".irl,"*J "r,to,"t|,
Add lhe digestion soluUon, closelhe microwave vessel.
f---- -].-
(Plating)
The sample is digested in the
micrcwave oven tollowing a specinc
deoomposilion progrcm.
Test the sample solulion and ihe 0.02
mg/kg slandard solution by uv-vls.
' H o t l r n e40a 700 8600
Cooling the vessel, frller;washed and
filled to the maft wilh dislilled waler.
Remove lhe sample, and cool
the beak€r lo room temperature,
and do the color reaclion
______-l "*rn nrte,.washedand l_____*p;-r, f;;-1
I rilled lo$e mark with Dlwaler I
ShENZH€N AOV I6STII {G T 'C NOIOGY CO.. ITD.XUNSHAN OEANCH
/\OV"BF#,HN
NO.i A002R121008024-2R02
Sample Doscripilon:
TEST REPORTOate :Oc l10 2012
5. To Deiermine Hexavalent Chromium Content in colorless and colorcd chromate coaling on metals: (Plating)
r e s t e d b v : l ) ^ ,' L/A^U,4.
5.1 Spotlesl (
f l;"')l;**SN€$ZHEN AOVI :STING T€C NOIOGY CO' ' ITD.XUNSI lAN BBANCI I
lf the lest result is posiiive,
ihe sample is considered lo
have hexavalenl chromium
Place 1-5
and the 0.02 mg/kg
Boiling- water- extracton
procedurc shall be us€d tolf the test reslrlt
lltherc is intederence or it is had to decide
whetherlhe sample have the hexavalent
5.2 Boilin9- water- enractronRemove the sample, and cool
the beaker to rcom temperalu€,
and do the color rcaolion
Take the (50i5)cm2
sample in the beaker.Heat 50 ml ol Dl waler in the
beak€r to boiling lof 10 min
Code Sample Desc{iplion Code
copper shell subslfate
Lead wire Plating 24 Copper shell Platng
Unit RoHS Limit Result
2-3
Lead {Pb) mg/l(g 1000 N.D. N.D. N.D. N.O
Cadmium (Cd) mg/k9 100 N.D. N.D. N.D, N.D.
Meroury (Hg) mg/kg 1000 N.D. N.D. N.D, N D .
Chromum (Crl'I) mg/K9 1000 Negalive Negalrve Negaliv€ Negative
TEST REPORToare: oct.10,2012
-:fh€ new RoHS di€ctive 2011/65/EU, on Jul. 21,2011 come inlo force, on Jan. 03, 2013 ths formal implementation, Direcliv€
200295/EC ahall be repeal€d simultaneously-
Sp€cimens, which ggqeted to d€temine Lead, Cadmium and Mercury conient have been dissolved completelv.
NO.: A0O2R12100802+2R02
-mg/Kg=ppm
--The iest is bas€d on the following
ce of C_rl\,I)lif"veiry/y6hetp ttef.limere sr{.q!.be/rurTr v ii'iffyiT-''
*'q:*lhe spot test result is uncertain or
each pad is unifom. The tesl rcsult
maybe cannot stand for the physical truth-Photo is included
Lead wir€ copper shell
"'End of Repod""
sHEI\tZH:ir AOVrlsrr'tc IECNl'lO!OeY CO.,ITD KUNSHAN SRANCIi
r.r i35.1J:55i0eo0o Fd.3F1t?55roEr$ hrr ,w.d{.di' Fodrdo 1r.r00/ , Hot l rne
I , 400 700 8600