ICP Test Report Certification Packet - Littelfuse · 2015. 3. 7. · I\rercury, Cadmium, Hexavalent...
Transcript of ICP Test Report Certification Packet - Littelfuse · 2015. 3. 7. · I\rercury, Cadmium, Hexavalent...
1
ICP Test Report Certification Packet
Company name : Littelfuse, Inc. Product Series: 2AG Cartridge Product #: 230xxxDRT1SSP Series Issue Date: December 13, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.
Issued by:
<Global EHS Engineer>
(1) Parts, sub-materials and unit parts
This document covers the 2AG Cartridge RoHS-Compliant series products manufactured by
Littelfuse, Inc. < Raw Materials Used
Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1
Remarks:
Form 585-047 Rev. A 2/21/06
2
Table 1: List of Raw Materials covered by this report
Total Parts Raw Material Part Number Raw Material Description Page(s) 1 HP-H (895-195) Sleeve – Heat shrinkable tube 3-9 2 082xxx Tin Coated Wire- Cu CDA 102 Sn Plated 10-14
4 3m-3779-PG (087244) Adhesive 15-19, 20-23
5 EP608 (087355) Glue 24-27, 28-31
6 YTW102
(692535-001 / 692471) Solder 32-36
7 910-537-3 Cap 37-40, 41-44
8 C909-369-001 BOSI Glass Tube - Body 45-48 9 C909-367-001 BOSI Glass Tube - Body 45-48 10 648106-001 Yarn 49-56 11 648115 Yarn 57-64 12 082xxx-001 Wire-99% Cu Sn Plated 65-71
TIANJIN BAIRUIJIE WELDING IJATERIAL CO.,LTD.
NO.38,BAOYUAN ROAD,EAST ZONE OF JINNAN DEVELPOPMENT ZONE,JINNAN DISTRICT,TIANJINCHINA
The following sample(s) was^/vere submitted and identified on behatf of the clients as : TIN-COATED COppERWIRE
Test Report
SGS Job No. :
Composition :Date ofSampl€ Received :Testing Period :
Test Requested :
Test Method :
Test Resulb :
Conclusion :
No. TSNEC1110357903 Date: 26 Oct 2011 Page 1of 5
TP1 1-0021 84 - TJCu
210d2011
21ocl2011 -26 ccl2011Selected test(s) as requested by client.
Please refer to next page(s).
Please refer to next page(s).
Based on the performed tests on submitted samples, the results of Lead,I\rercury, Cadmium, Hexavalent chromium, Polybrominated biphenyls (pBB),Polybrominated diphenyl ethe6 (PBDE) compty with the limits as set by RoHSDirective 2011l65/EtJ Annex ll; recasting 2002/95/EC.
scsM3B6,No..t,Yh.5n a-^J.rEDA.n.f i ch'E 3m457 r (e-z4ed8am
Signed for and on behalf ofscs-csTc Ltd.
;@-Reabeca ZhouApproved Signatory
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rbdi iriLrn.tsnor.rdiyroh.rmehlr)rftd
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M6nb€rorrhoscs couD {sos sA)
Test Report No. TSNEC1110357903 Date: 26 oct 2011 Page 2 of 5
Test Resulb :
Test Pad Descriotion :
Spodmen No. SGS Samde lD D6.*iptbnI TSN1 l -103579.002 sjtvery metatwire
Remal}6 :
(1) I mgftg= l PPm=0.0001%(2) MDL = lrethod Detedion Limit(3) ND = Not Detecled ( < MDL )(4)'-" = Not Regulated
RoHSI DllEdive 201 I,/8AEU
Test llethod : With reference to IEC 6232't:2008(1) Determination of Cadmium by tCp-OES.(2) Detemination of Lead by |CP-OES.(3) Determination of [,lefcury by tCp-OES.(4) Detemination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis.(5) Determination of PBBS / pBDEs by GC-MS.
Test ltem(s)
Cadmium (Cd)Lead (Pb)lllercury (Hg)Hexavalent Chromium (C(Vl))
MonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiphenylPentabromobiphenyl
HeptabromobiphenylOctabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBOESMonobromodiphenyl ether
tjDj! Unit
10O mS/Kg1,000 ms/Ks1,000 mg/kg
1,000 mg/kg- mg/Kg- mg/Kg- mg/Kg_ mg/xg- mg/(g- ms/Kg- mg/Kg- mgks- mdks- mgKg
1,000 msu4a- mgKg
sc3lLdlon,l{orl,Tn $r alcuTEoAThnltn,chtB 3&atfl.tlrilttitllflt*tlrrts€s*! ttr3o$r
r (s.22t6623gm r 1&24A4562| (e2a62sd l(*-?a5@ . .6jir'.OF@
MDt @2 N D2 N D2 N DC Negative
ND5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D- N D
5 N D
lo.d [email protected] b r.m d I tri,_rr!!,colrr!.'nt .,!ecu!rt!!1!!!i. diiii& ii ddni b-i'.lFnria.|d ttd Fehi i.d fiMr$hrnt hcdr 0rhr dsm.d r dndfiMii-h.rnt hcdr 0thr dsm.d t dnd h.l
tuhro'csrr 'iffia tmr .eal;l. Fd*-b. dBr,.-. d o d i g d b i . q d i 0 r f u n 6 @ ! . . d . 1 4 p | h | u l ' { b d D d . ' - h | i
rhoi ri si h rrd *r onrr ro rtu t6ph(.'r.rbd .
M€nb6' or rh6 scs o,o!p (sos sAj
Test ReportTesl ltem(s)
Dibromodiphenyl olherTdbromodiphenyt elherTetrabromodiphenyl etherPenlabromodiphenyl etherHexabromodiphenyl elherHeptabromodiphenyl ethe.Oclabromodiphenyl etherNonabromodiphenyl etherDecabromodjphenyl ether
Notes :
No. TSNEC1110357903 DaIe: 26 Od 2O11 Page 3 of 5
ti!r! UlImg/rgms/kgms/k9mgKsmgKgmg/rgmgftgmg/Kgmg/Kg
MDL
555555555
peNDN DNDNDNDNON DN DND
(1) The maximum permissible timit is quoted from directive 2011/65/ElJ. Annex .(2) o spot-test:Negative = Absence ofCr(Vl) coating, positive = presence ofC(Vt) coating;The tested sample should be further verified by boiling-wEter-€xtraction method ifthe spot test resutt asNegative or c€nnot be confimed,o Boiling-wateFextraction:Negative = Absence of Cr(Vl) coaling; positive = presence of C(Vt) coatingThe detecled concentration in boiling-watef-extraction solution is equalor greater than 0.02 mg/kg with 50cm2 sample surface area.For conosion protection coatings on metals: Information on stofage conditions and production date ofthetested sample is unavailable and thus results of Cr(VI) represent status of the sampte at the time oftesting
riLdc!d!i.,tdb'h.ffi b ffira hffir a u*:!llg4lrd r!4!e! h!!! ^dldbi tr di.
lq..dhrb' !.u. d..d rM^ &yMtoroi'r!Frrbtt. i |4ai
r 06-4252$52{ (s-4 25e95252
Memb.ror th.SGSG@rISOSSAl
Test Report
ATTASHMENTS
'l) Name2) Name3) Thsse(Cf* end
cdpb/t{g/cl./FBBs&pBDEr Tcsdng Ftow c-h.It
oflh6 porcon who mads tesiing: Aaron Wang/Jeson Li/Angell yeoofthe psrson in charge oftesting: Cindy yin,/Rsx Zhusamplss wer8 dissolved iotel ly by prs-condil ionjng method according to bslow f low chadPBBs/PBDEs iesl rnethod excluded)
I scs u.nrio,r{orar.Th. 5|| Avru1ED4Tt rth,chkE sas, I {a_2216*w I F,r?r5295252| +!::!$'et!11!g!Ili41!!9!*! !!i9erl |p&.e!ry r(!:a,5ry9
Page 4 of 5No. TSNEC1110357903 Date:26 Oct 2011
Sample Preparation
Sample lVeasurBmeil
Acid digeBlion w'thmicrc,,rave/ hotplale
Sample solv€ntextraclion
ConcenlraliorVDilution ofexlraciion
s0lution
1)Alkali Fusion /0ry Ashing2) Acid todissolve
Boil ing waterBxllacl,on
Adding 1 ,5-diphenylcarbazid€ for
color d9velopmenl
Ared color indicalgsthe presence ofCre.lf necessary, conlifm
N€gative
_{ dlld ll .d by b. 6@y &q.o 'o in c.tu.' cod 16. d e
rbc.iF.ri sh '6pdMn bb ,{6s.jbrhirqqcunxbrN'6ed.|dbryd!
[{olnb.rot rhs SGS GrolD (SOS SA)
Test Report
Sample photo:
I :9sl!j.atY11nE 5rr ̂ nu.rEoard4,n chtm 300.s7 , c4fiasqD trar46eereI
sr. tttI*IlErI*3r+scsrit tt fi.57 r {S_?2t662mr @r?2sa5a?
No. TSNEC1110357903 Date: 26 oct 2011 Page 5 of 5
TSN11-103579.002
SGS authentic€tethe photo on original reporl only'" End of Report -.
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.r lfr i i ! l l . l !1'pn..i.|c']ylo6.[n'1.{r|hfi
rr.flb.r ol th. ScS O|o!p (SOS SAI
Test Report
3I,T CHINA LIMITED
222#T|AN LtN ROAD, SHANGHAT (200239)
No. SHAEC1018364101 Date: 23 Dec 201 0
rrb h |Irb(.,r-E
sP10-042093 - SH
21 Dec 201021 Dec 2010 - 23 Dec 2010
Selected test(s) as requested by client.
Pleas€ refer to next page(s).
Please refer to next page(s).
Based on the perfomed tests on submitted samples, the results comply with theRoHS Direclive 200Z9YEC and its subsequent amendments.
Page 1of 5
The following sample(s) wasi/vere submitted and identifed on behalf of the clients as : 3l!l 3779-PG
SGS Job No. :
Oate of Sample Rec€ived :
Testing Period :
Test Requested :
Test Method :
Test Results :
Conclusion :
Signed tor end on b€half ofSGgCSTC Ltd.
zQv""^Fan Jingiie, JJApproved Signatory
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cci{
Mrn$or or rh. SSS G|!up (S99 SA)
T€st R€port
Test R€sults :
Test Part Description :
Sp6d,n6n tlo. SGS Semde lD1 SHA10-143641.001
Remarks :
No. SHAEC10183g101 Date: 23 Dec 2010 Page 2 of 5
De6('iplionYellow translucent solid
(1) 1 mg,/kg= 1 PPm=00001%(2) l\rOL = lrethod Deteclion Limit(3) ND = Not Detected ( < MDL )(4) '-' = Not Regulated
Rol{S Exr€divo mo2/gs/Ec
T€6t Method : With reference to IEC 6232'12008(1) Determination of Cadrnium by ICP-OES.(2) Detemination of Lead by ICP-OES.(3) Detemination of Mercury by ICP-OES.(4) Determination of Hexavalent Chromium by Colorimetric liethod using W-Vis.(5) Determination of PBBS / PBDES content by GC-MS.
Test ltem(s)
cadmium (Cd)
Lead (Pb)Merclry (Hg)
Hexavalent Chromium (CrVl)
Sum of PBBSMonobrornobiphenylDibromobiphenylTdbromobiphenylTetrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphsnyloclabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobromodiphenyl ethet
ti!d! UlI100 mg/kg
1,000 mg/kg1,000 mg/kg1,000 mgr'kg1,000 mg/kg
- ms/Ks- msftg- m9K9- mg/Kg- mg/kg- mdks- mg/ru- mgftg- mgKg- mg/Kg
1,000 mg/kg- mgKg
MSt 0p12 N D2 N D2 N D2 N D- N D
5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D- N D
5 N D
scd b r. cn" c.dsr.i !'tlo trd- odr'.[|!r. d qu.r d -cff i h,!4- b r@ 5t cd'@ t. EMd4 oosFr d !a!tl!9!!r@t!a9s!4!!!
rhM 5 br d 4d e stE h r$Pb(.) bb.
tlrcllnl,t|$ionttudtlrtrorr 2D@3|l!.Il.lEalurra€8sil3ql ll: 2@
l6lE(6-r)611@ lEl€{E-?l)6(KA Boro.c!.nItF2l)614029a Hi{6-zlFa@! .rFii.€4M
u.nb.roltno sose.oup (sqss )
Test Report
Test ltem(s)Dibromodiphenyl etherTribromodiphenyl etherTetrabromodiphenyl otherPentabromodiphenyl etherHexabromodiphenyl etherHeptabromodiphenyl etherOctabromodiphenyl etherNonabromodiphenyl elherOec€bromodiphenyl elher
No. SHAEC1018364101 Date: 23 Dec2010
unit Mot aalmdkg 5 NDng/kg 5 NDmg/kg 5 NDmg/kg 5 NDmg/kg 5 NDmSikS 5 NDmg/kg 5 NDmS/kS 5 NDmS/kS 5 ND
Page 3 of 5
Notes :(1) The maximum pe.missible limit is quoted from the document 200t618/EC amending RoHS directive
2002t9stEc
Limit
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lloml.| ol0|s SG3 Orour (scs sa)
Test Report No. SH4EC10f8364101 Oate: 23 Dec 2010 Page 4 of 5
ATTACHMENTS
RoHS Testing Flow Chart'1) Name of the person who made testing: Allen Xiao/ Wesleywei/ Andy Zhao /Elim Lin2) Name of the per6on in cha.ge of testing: Jeff Zhang/ceoee XdTracy Yue3) These samples were dissolved lotially by pre-conditioning method according to below flow chart. (Cr"
and PBBS/PBDES test method excludeo
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Pb/cd,Hg PBBs/PBDES
Acid digestion withmic.owave/ hotplate
Concentration/Dilution of extEction
solution
Heating to 90-95Cior extraclion'| ) Alkali Fusion /
DryAshing2) Acid to dissolve Adding 1,5.
diphenylcarbazidefor color
developmentAdding t,5-
diphentcabazidefor color
developmentA red colorindicatesthe
presence of Cf'. fnecessary,confirm with
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M.nb.i ot !n€ SOS Oro{r lSGs SA)
Test Report
Sample photo:
No. SHAEC'1018364101 Date: 23 Dec 20'1 0 Page 5 of 5
sHA1G183641.001
SGS authenticate the photo on original report only't* End of Report '*
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SGS Job No. :Date of Sample Received :Testing Period :Test R€quested :
Test Method :
Test Results :
Test Report No. SHAECl018364102 Date: 23 Dec 2010 Page 1 of 4
3M CHINA LIMITED
222# T|AN LIN ROAD, SHANGHAT (200239)
The following sarnple(s) wasl^/ere submitted and identified on behatf of the clients as : 3M 3779_pc
sP'10-042093 - SH21Dec201O21 Dec 2010 - 23 Dec 2010Selected test(s) as requested by client.Please refer to next page(s).
Please refer to next page(s).
Signed for and on behalf ofSG$CSTC Ltd.
7QvFan Jingjie, JJApproved Signatory
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!"iru$.alrri.d)cri'.4ltltaoit 2ooarg rElE(dAid.@ lErE{caFffi)g mcn.{.@Hl{&"eld{i!!44 r{j(&"t)tl&L . {.d*roe.o,if l'J'f '*iEaltltl0+3t, a), M
M.nb.r ot rh6 sos o|!up (sos 3A)
Test Report No. SHAEC1018364102 Date: 23 Dec 2010 Page 2 of4
Test Results :
Test Part Descdotion :
Sp€dmqrNo. SGS Samde lD1 SHA1G.1$A|1.001
Remarks :
(1) 1 mgr'kg= 1 ppm=0.0001%
(2) MDL = Method Deteclion Limit(3) ND = Not Dereded ( < [4DL )(4) '-" = Not Regulated
Haloosl
Test Method : With reference to EN 145E2: 2007, analysis was performed by lon Chromatograph (lC).
D€cripto|lYellow translucent solid
Test ltem(s)Fluodne (F)Chbnne (Cl)Bromine {Br)lodine (l)
u!j!mg/KgmgkgmgKgmg/kg
MpL 00150 ND50 ND50 ND50 ND
db,bc.'ryr/t.rbr.o-'Jcddb.daaroddd.ft.r..vEEm,E ! i - nh .n !!Dr !!!:!r!,q!!t!!_!4!-E!!!!aa
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r Et€ 6+1)0l.|025aHr{n-a}a rE9a
rr.mb.r ot U|. SOg €mI' (SOa SA)
Test Report
ATTACHMENTS
No. SHAEC1018364102 Date: 23 Dec 2010 Page 3 of4
1) Name of the person2) Name of the person
Halogen Tesfln9 Ftow Chart
who made testing: Daisy Gongin charge oftesling:Alex Jiang
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Irbihr.ir.(.)brc
Sample measurement
Combustion in oxygen bomb
Dissolved an an absorptionsolution
Anal).zed by ionchromatog€phy. Double confirm
by other instruments, if
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M.nDef ot th. 3OS Otllp (scg SA)
Test R€port No. SHAECl018364t02 Dale: 23 Dec 2010 Page 4 of4
Sample photo:
SGS authentic€te the photo on original report only-' End of Report *..
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Momberolin SGSOruro(SOSSA)
Test Report
SGS Job No.Compositionlrodel No.Client Ref . lnformationDate of Sample Rec€ivedTesting Period
Test Requested
Test Method
Test Results
Conclusion
No. TSNEC1100107601
NEW MATERIALS CO.. LTD.ROAD, BADACHU HIGH-TECHZONE,BEIJING.
Dater2S Mar 201' l Page I of 4
BEIJING HYSTIC5 SHUANGYUAN100041, cHtNA
The follo.ling sample(s) was/lvere submitted and identified on behalf of the clients as :ADHESIVE
1060825 - TJEPOXY ADHESIVEEP6O8Model No : EP60623 Mar 201123 Mat 2011 - 28 Mar 2011
Selecl€d test(s) as r€quested by cli€nt.
Please refer to next page(s).
Please refer to next page(s).
Based on the perfomed tests on submitted sample(s), the results comFrywith the RoHS Direclive 2002/95/EC and its subsequent amendmenls.
Signed for and on behalfofscs-csTc Ltd.
,**^
Summer BaiApproved Signatory
o,61 domdillld b r.m' 0d
I FA 66?330@ J ($,2?25e$252r (s2t66430c0 l{s-2a62$252 o sq.dii€s{im
h|cohF!|o|d@d'ii lytrl.
scs M3Bi4,No 41,Th. slh Av.nBTEDAt.nlin,CniE 300,t57
i +r.lr6&tq**tatiifi11!9$*!-. _ lt:i_3na9lM€nbs,or rh. 6cSG.ouo{SGS SA)
Test Report
Te6t Results:lD for specimen 1Description for specimen 1
RoHS Dlr€d1,6 2002/95/EC
Test ltem(s)cadmium (Cd)L€ad (Pb)lrerorry (Hg)Hexavalent Chrornium (CrVl) byalkaline extraclionSum of PBBSl\,lonobromobiphenylDibromobiphenylT bromobiphenylTelrablomobiphenylPentabromobiph€nylHexabromobiphenylHeptabromobiphenylOctabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobromodiphenyl elherDibro.nodiphenyl etherTribromodiphenyl etherTelrabromodiphenyl etherPentabromodiphenyl etherHexabromodiphenyl etherHeptabromodiphenyl etherOc{abromodiphenyl 6therNonabromodiphenyl etherOecabromodiphenyl ether
Note:
No. TSNEC1100107601
TSN1l-001076.001grey viscous liquid
Date: 281 ar2011 Page 2 of4
UnitmgKgmgKgmg/Kgngkg
mdksmsr(gmsftsmg/Kgmg/Kgmg/(9mgKgmgKgm9KSm9KSmg/K9mg/Kgmdkgmg/KgmgKgm9Kgmg/KgmgKgmgKgmgKgmgKgfigK9
N.D.N.D.N.D.N.D.N.D,N.D.N . D .N , D .N,D.N,D.N.D-N,D.N.D.N.D.N.D.N.D.N.D.N.D.N,D.N,D.N,D.N,D.
Test l4ethod (Reference)IEC 62321 Ed.1: 2008, ICP-OESIEC 62321 Ed.1: 2008, ICP-OESIEC 62321 Ed.1: 2008, ICP-OESIEC 62321 Ed.1:200€, UV-Vis
tEc 62321 Ed.1: 2008, GGMSIEC 62321 Ed.1: 2008, OC-MSIEC 62321 Ed.1: 2008, OC-MSIEC 62321 Ed.1i 2008, GC-lrSIEC 62321 Ed.1: 2m8, GC-MStEc 62321 Ed.1: 2008, GC-MSIEC 62321 Ed.1: 2008, cC-ltlsIEC 62321 Ed.l: 2008, cC-[,lSIEC 62321 Ed.1: 2008, GC-MSIEC 62321 Ed.t 2008, GC]\,!S
IEC 62321 Ed.1: 2008, cC MSIEC 62321 Ed.1: 2008, GC-MSIEC 62321 Ed.1: 2008, GC-[4SIEC 62321 Ed.1:2008, GGMSIEC 62321 Ed.1:2008, GGMSl€C 62321 Ed.1: 2008, GGMSIEC 62321 Ed.1:2004, GGMSIEC 62321 Ed.1:2008, GCMSIEC 62321 Ed.1:2008, GGMStEC 62321 Ed.1:2008, GC-MS
Result IIDL LimitN.D. 2 100N.D. 2 [email protected]. 2 1000N.D. 2 1000
- 10005555555555- 10005555555555
1. mg/kg = ppm2. N.D. = Not Detected (< l\4DL)3. MDL = llethod Deteclion Limit4. '-' = Not regulated5. The maximum permissible limit is quot€d fom the doqJment 2005/618/EC amending RoHS direc{ive200295tEc
Result shown is of the total weight of w€t sample
nr.n*ui.i i i i ;orhn @utud&bt d b r.mr r.d hdrdi I dnri btfiailhii.ib.ard judkh br{. &ii.d ri.'.h r
u|slfud'doiw'i l.^3'oldv.|oln.conll iy.id.db.io[!i&,rh.r.ir.rondeliri
1 SGS |\&Bion,ror1,Th. 5rh awnuerEo ,r.nrh,ord sa57 rle2aEat{@ , $-4?5a5e5?
I 4|.i!!!tFnl4g!ltf1t!s9sj!.-. .!aqs!51 !re-q65am r @-?4?5ee6?52M.mbe.ol Iho SGS G.o!p (SGS SA)
Test Report No. TSNEC1100107601 Date:28 Mar2011 Page 3 of4
ATTACHMETTS
cd/pbfi l/cf ?BBr&pEDE3 Ftow Chrft
1) Nams ofth6 person who made tssting: Skt Shi/Aaron Wang/Winnie Zhang/Atgell yao2) Name ofthe percon in chargB oftesting: Cindy yin/Rex Zhu3) These samplos $,src dissohed totsllt by pr€-conditioning msthod according to
b6low iow ched. (Cf and PEBS,/PBOES l€st meihod Bxcluded)
rhd4ui.dr..lv.dbrh.coirrr."4{irooc.i.rdcs4brlrs. 'n ,nr_3!d-!.o!('oi!h6 nd roq!4jl c lohn 6diut,.ubi.d ro t mr nd codrbd .d
tthinlh.''t|o'cl|ir|iifuei!. idobloei!udd.ll i .nii.. l lm.
SGS Mansion,No a1 Tho 5th Avenu. TEDA.fdnth,Ch'6 1Dt57+l tl6etfi44l8li^F1lCscs1tr |!lli300457
r 1s-4656&00 r1s-4529$252 M ci sq! oolt&.4e62!0!o i (36-42545252 e rs!.rrsg!!36
Membororrho SGS Cfolp ISGS SA)
Sample Preparal ion
Sempls Msasufsm€nl
Acid digeslion withmicroraYs/ holplale
Adding digesiion rcagsnt
Concsnlralion/Dilution of€xtfaction
golution
Filiration and pHadjustment
1)Alkali Fusion /DryAshing4 A.id todissoFg
Adding | 5-diphenylcarbazid€ for
color dsvelopment
Pbr'Cd/H9 FBB'PBDE3
Test Report No. TSNEC1 100107601 Datet28Mat201l Page 4 of4
Sample photo:
TSN11-001076.001
SGS auth€nticate the photo on original report only'*' End of Report '-
tB @tud it r.u.d ty s. cd'ir .utor ro d 3.i.,.r cdLh. dr 3.d! sd.t't_!!d!& &hn [email protected] c b r6t .na cdfl..r rdr €bd,6ro ostud d !*.6.*i4.fr .&uhrii
b.hoai r'dr.r.r@n.,..otrtro
scsu..rion,No.al,Tn $n adoTEDAItrnjin,chitu !00457 r is-22)3'l3${0 I ls-22)254e52 ,*..i !c..@c!.tltgtf,{*taliit?rqscs*t lli 3e.57 r (&a)65400 r t35-22'299s252 e {!.hktr{l.sM
M.mb€rorrh. sGS Gouo ISGS SA)
SGSTe€t Reoort
SGS Job No.CompositionModel No.Date of Sample ReceivedTesting Period
Test Requested
Test lvethod
Tesl Results
1062747 -TJEPOXY RESINEP6O811 Apr 201111 Apt 2011 - 14 Apt 2011
Selected test(s) as requested by client.
Please refer to next page(s).
Please reier to next page(s).
Dafe: 14 Apr 2011 Page 1ol4
r (s-2216?3!rr0 | l6-22)?5?!5i]er 1a-2455?3m ' €G2l5A5?52
No. TSNEC1100135201
CO,, LTD.HIGH.TECH ZONE,BEIJING,
BEIJING HYSTIC NEW I\4ATERIALS5 SHUANGYUAN ROAD, SADACHU'100041, cHtNA
The following sample(s) was/were submitted and identified on b€hatf of the dients as :EPOXY STRUCTURAL ADHESIVE
Signed for and on behalfofscs-csTc Ltd.
Reabeca ZhouApproved Signatory
yebj.cl|o4!G.i.trLconddoitds.hld rd.ojq!!!.E io'ri docld nr'r rdo(unFr h,i iin.iEl I dh{ 'o-ii.n',rron dr,!mr4g|!!!t{.d r Jaddoib ltdsron o'yr$rtrhh h. rne'irtt6r hrris.i][hrft olrltF.Mdbrn dr,r9t 6,e.ry o
scsMa6bn,No.4l,Th. sth Av.nu.lEoA,nanjh.cniu 3004t+ | . *itii€tffi*It8tE*fr41rlscs*l i|| 3001s?
M.nb.ror rh6 SGSGrolp(SGS SA)
Test Report
Test Results:lD for specimen 1Description for specimen 1
Haloo€n
Test ltem(s)
Fluodne (F)chbnne (Cl)Bromine (Br)lodine (l)
Note:1. mg/kg = ppm2. N.D. = Not Detected (< IVDL)3. MDL = l\,ilethod Detection Limit
No. TSNEC1100135201
TSNl l-001352.001light gray liquid
Date: 14 Apr2011 Page 2 ol4
Unit Test Method (Reference)
EN 14582:2007, lCEN 14582:2007, lCEN 14582:2007, lCEN 14582:2007, lC
Result tulDL
65 508076 5096 50
N.D. 50
ms/Kgmg/(gmg/Kgms/Ks
Result shown is of ihe total weight of w€t sample
/.d!yu.corriiy&q.dbrbG.(c 5rF.' iour.ob.n$d b r.fl . jrwerMe, Her.d n; a'q'; r .ru ro_F! n.umi olb.ntt dbr.Tr.nocodrdr ro. e Her.d n; a'q,; r .ru ro_F! n.rrDr d
||u.|@.ii.. i i^ryb|d'o,6'D.itr;ro.rru.iordd.D.il; 'o.ned.ioi
rireir.G)rn'd
SGSU.@ioi,No.a1,Tho $n AhuorcOA,TidnJh,chie 3e.57 t($-?2f593enql.I|r €tF^ftgftif4rgscsl! {l;3m157 1186"221654&
| 136 24254t5r52 m.cd lgscohr {8naa295ae r 43.t'M@r$@
M8mb€roi th€ SGSGroJ! ISGS SA)
Test Report
AT?ACHMENTS
1) Name oflhe psrson who made t€sting:Angell Yeo2) Name oflhe person in charge oftesl ing: Rsx Zhu
' |ryft.c.frp,|yr!.i.'6@|od
bE4q6!i ic.0oio' lh.€d.do
r {60-?aames r 06-a?te96e521136-2165430(o lOFAl25295e52 e.!!.rE@s!6m
No. TSNEC1100135201 Date: 14 Apr 2011 Page 3 of4
Halogcn T.sthg Flow Chad
Sample cutt ing/pfeparal ion
Semple measur€msnt
Combustion an oxygen bomb
Dissoh'ed in an absorpl ions0 ,J!0n
Analyzsd by ionchrcmaiography. Double
conlim by olher instrumsnts, i fn6ce66ary
ri| leuh.di.!.u.dbyu.
scsM.n!ton,No.41,Th. 5rh AvsnuclEDA,fianlrn,ChlM 300a57+q.*tit€*Et{A8lrtf4lCscs^! ll3m4s7'
Mehbsrol rh6 SGS Glolp {SGS SA)
Test Roport
Sample photo:
No. TSNEC1100135201 Dale: 14 Apr 2011 Page 4 of4
TSN11-0013s2.001
SGS authentic€te the photo on original report only'*' End of Report '*
D Brld b, 6r conr.ry r6rd ro.bEt!6ni. r06n doeuNio.ubld b tm h; ManiE;li *N; b-iFa-rt;i.6n?
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.ndob|i.&irunfi|6.6.d..cu[m|.'
r (s 22)25?!525? M.o.r!! @hr (3ta25a9cs2 e s!s.&Eol{..s
SOa M.Nlon.ilo.41,$€ 5in Aq@T€D,\1tanjtn,Chi@ 3iras7 | (M2r652836!)0{l.tflt?tlli}laln*f4rqscs ! {i:3m457 r0r2)06a&00
b.horninsr.bdnFnrtuortb
Msm!€ror rfe scs GouD lscs sA)
Test Report
SGS Job No. :
l,Iodel No. I
Composition :
Date of Sample Received :
Testing Period :
Test Requested :
Test Method :
Test Results :
Condusion :
No. SHAEC1116009838 Date: 14 Oct 2011 Page 1of 5
ZHEJIANG ASIA GENERAL SOLDERING & BRAZING MATERIAL CO.,LTDXIHU INDUSTRIAL PARK,SANDUN,HANGZHOU CITY.ZHEJIANG PROVINCE.CHINA
The following sample(s) was/u/ere submitted and identifed on b€hatf of the clients as : LEAD-FREE SOLDERWRE
sP11-030781 -SH
YTW102(692535-00 t,692535-002,692535-003)
Sn2.0CuRE
09 Oct 2011
09Oc t2011-13Oc t2011
Selecied test(s) as requested by client.
Please refer to next page(s).
Please lefer lo next page(s).
Based on the performed tests on submitted samples, the results of Lead,Mercury, Cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB),Polybrominated diphenylethers (PBDE) comply wilh the limits as set by RoHSDiredive 201 1/65/EU Annex ll; recasting 200295/EC.
Signed for and on behalf ofSGgCSTC Lrd.
,zQr''Fan Jingjie, JJApproved Signatory
cdEd ar-r b tu ondr co'v,uo. ds.dd rnd .,.,h.r, .nr| . m q!$' 4 tarrbr. j hdA/hw er.oiw!!-!44!d!trNd;fi;L-;ii;;'tu;a-e-a;fr;;;; 'tu; DA;;F. i*!tEa@r:419!s4!sja!.Eii r {.I'-r. i. *oflq,d;iirrii€ b tu. ts c.icrba b Edisr DoMFF . !Etl@[email protected]*hd.arhl*r!rd.d.a'.dLdtdrdiffidRhf,i$rrss.c4m"/. I'drie' nhrm'd$.hado'.*. i'.nvd.d, ,b. rh.c!.lar rd. '.r.ddDri rb|bc||fndnui.d..dil6 d o9n;";;;d;;d;'d t$aidqiagDi.f . ntu'nm'it ad b FFd,{d.€!r h tun *'hod F!sFtbtu6db@h'd
Lun .hMri*hrntsnhtudrbib.6!i.(r)in!.
fArhthn9l|red&|,a.{9r9roh @lnt.!:.ltral&1830+$ lrl2@3
lEt(H1)8'lqA r$EF-?r)04€ryt9 l*.d.aicmHLO-el)611@t Hlj(10-21p15@ .sd'lerFq
r .nbdol tr'. SGS GmrP (gGS SA)
T€st Report No. SHAECl116009838 Date: 14 Ocl2011 Page 2 of 5
Test Results :
Test Part Descriotion :
Sp€dhen tlo. SGS &mdo lD Dscridion1 SHA1 1-160098.033 Sitvery metatwire
Remarks :(1) 1 mg/kg = 1 PPm = 0 0001%(2) MDL = Method Deteciion Limit(3) ND = Not Detected ( < tvDL )(4) "-' = Not Regulated
RoHS Dir€div€ 2011lbs/Eu
Test Method: With reference to IEC 62321:2008(1) Determination ofCadmium by ICP-OES.(2) Determination of Lead by ICP-OES.(3) Determination of Mercury by ICP-OES.(4) Determination of Hexavalent Chromium by Spot test / Colodmetdc Method using IJV-Vis.(5) Determination ofPBBS/ PBDES by GC-MS.
T€st ltem(s)Cadmium (Cd)Lead (Pb)Merorry (Hg)Hexavalent Chromium (Cr(Vl))Sum of PBBSMonobbmobiph€nylDibromobiphenylTribromobiphenylT€trabromobiphenylPentabromobiphenylHexabromobiphenylHeptabrornobiphenylOctabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESlllonobromodiphenyl ether
ti!!t Ud!100 mg/kg
1,000 mg/kg1,000 mg/kg
1,000 mg/kg- mgKs- mgKs- mg/Kg- ms/Ks
mdks- ms/KS- ms/Kg- mg/Kg- mgKs- mg/Kg
1,000 mg/kg- mg/Kg
MDt 0332 N D2 1672 N DO Negative- N D
5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D. N D
5 N D
dun .h.s6nirdn dr|rrsrrbbsir.Glbbd.
rh!dgr'ibb&-t'|h. ry&uEr b r. or-rcdt'|m.l !.'vr6dh Dcsr{rb.r tGrrr!Ar!!&t!!ll&s0,al@
-*rirEt id&n.h*did.i^dri.ah rdw detudt..dddMliFd6affih.noi.i'rtbs.c!rt,. imne..rhrhdb.a-iEiifi*rhntur rdchdr hdd.!, dE. n.cMrt or.o.4lbrlUr6k c lx{rnuirlh4Mr.6'd-.fi|
t.irdpbaYrtutodxll$ci1d,9rldOlr 20Gt'il 'lt .*Jr6tttragllstl lti 2@3
rEuFa)arlo€!5lrEl€(6-AFffi7t nr.4.$cml!{fi.2t)6l]@Sa Hr06-ql)5a5060 .!$dmGFs
fr.mbor ol U. AOS Goup (8GsS )
Test ReportTest ltem{s)
Dibromodiphenyl etherTdbromodiph€nyl eiherTetrabromodiphenyl eiherPentabromodiphenyl elherHexabromodiphenyl etherHeplabromodiphenyl etherOctabromodiphenyl etherNonabromodiphenyl eiherDecabromodiphenyl elhe.
No. SHAEC1116009834 Date: 14 Oct 2011 Page 3 of 5
Limit ldrm9Kgmdksmgkgmsn<9mg/Kgmg/Ksmg/KgmgK9mgKs
fitED&nrhrrhrD.l4LC'ao de33Sl.-tt.*fiAldt|€€efl+l :*2@r
MDt555555555
033NONDNDNDN DNDNDNDND
Notes :(1) The maximum permis,sibte timjt is quoted from direciive 2011/65/EU, Annex ll(2) o spottest:Negative = Absence of C t coating, positive = presence of CrVl coating;The tested sample shoutd b€ furthor verified by boiting-wateFextraction method if the spot test result isNegative or cannot be confrmed.o Boiling-water-extraction:Negative = Absence of CrVl coating; Positive = presence of CrVt coatingThe detected concentration in boiting-waterextraction solution is equat or greater than O.O2 mg/kg with S0cm2 sample surface area.For corrosion prctection coatings on metals: Infomation on storage conditions and produclion date of thetested sample is unavailable and thus results of Cr(Vl) represent status of the sample at the time oftestino
rE€(6-?1)11{@5! |E€F6-AF{S?! ||r4.rfl.cooH!i&ala11q04 |l0n-21)6aa!d|.3 .r6d'h&9.qr
M6ln!6. or ho 8GS Oro(9 {8OS S.$
Test Report No. SHAEC1116009838 Date: 14 Oct 2011 Page 4 of 5
,rtu.rM h r* bi npd rrrr o r b rr tmpr.(r) 'obd
ATTACHMENTS
RoHS Testing Flow Chart
1) Name of the person who made tesling: Jan Shi/yoyo Wang/A en Xiao/Gary Xuz) Name or me person in charge oftesling: Jefi zhang/George xu/ Elim LinJ) | nese samples w€re dissolved totaltv bv oreconditioning method according lo below flow chart.(Cl6+ and PBBS/PBDES test method'ex;tuoeo,
Sample Preparation
Sample l\Ieasurcment
Acid digestion withmacrowave/ hotplate
1) Alkali Fusion /DryAshing
2) Acid to di66olve
Nonmetallicmaterial
Heating to 90-95Cfor extraction
Adding 1,5-diphenylcarbazide
forcolordevelopment
Adding 1,5-diphenylcarbazide
for colordevelopment
A red colorindicatesthe
presence of Cr6'.necess€ry,
Pb/Cd/Hg PBB9/PBDES
.rbrd n T.m. d c.{drb * uidr Dd'M d fti..dt{rB..d.ol,dl'6:,{61-l-i6-n 66-Ii!1ii'd.-i-dbrr4f,iki.drrdiehxa&hd hrii.^ny[&db eour! ddHEffiEEFii|lsF-Eb afrlrb di-riinh fr l'trrd G.ll|t h*!d.F, td.ihloollaItllsltd*{.rdilkbrd.b!.. .Iihrhffi-i{rb.aturrq..rE rhturr.{6M.n'tuDrdo,rr.clqry.D/$.ffidrtr i{F.bE-yt
JbfBlsraY!$blrri urt4Strtllch 2m33+l 'tl . *iE8Atll89!13t! l* 2@c
rEcFa)6rc45* lE E(S{I6SD tw.ojra@ru{n-21)6L@s1 HirF2l)5a5{rE! . 3i.hi|or4@
M6hblr o, $o SGS Grolp l8GS 5,^)
Test Report
Sample photo:
No. SHAEC1116009838 Date: 14 Oct 20t l Page 5 of 5
SGS authenticate the photo on original r€port only'- End of Report "*
br. o.'|'rc.d!{rd l.d{ prr@d er.t, ud.nbd oqrd d -rrdtr n!414!!49!!qo44_!!!_a!q!aa
tr.hcd.D, ,d. rn.Cdrrvt -r. dn.*llt iblbcrd jdr'Lrn t ucr{a@rd|!.ft460ffi'nsrdb.nrDdo!.dE lhMlrldDdrdqrtls...pDB.roi$r
dub.hMhdrhinrddroi,rb'hrnp.i4lELc.
ftrEll$rDYa.f.i[ilrrBErlrfirr 2o@3 rEEl6-er)oertuEpeajo*vn wo,ra.MeI -tl.*EqldfiFrl6r?|l ll.2@3 fiLti-2r)6 e5e4 rLls-a)5.5@53 ..Fd'dcl.o
[.m!.. otlh. 8GS Orcqp (aOS S )
Test Report No. SHAEC1018971802 Date: 06 Jan 2011
The following sample(s) was/u/€re submitted and identified on behalf of the clienb as : FUSE CAP
Page 1 of4
DONGGUAN CIryXNHAI METAL PRODUCTS CO.,LTD.
1ST WEIMIN ROAD HENGZENG AV,XINAN COI,/IMUNITY CHANGAN TOWN DONGGUAN CITYGUANGDONG PROVINCE
SGS Job No. :Date of Sample Received :
Testing Period :Test Requested :
Test Method :
Test Results :
sP10-043287 - SH
30 Dec 201030 Dec 201 0 - 06 Jan 201 '1
Selecled te6t(s) as requested by dient.
Pleas€ €fer to nExt page(s).
Please refer to next page(s).
Signed for and on behalf ofSGgCSTC Ltd.
zQv'"^Fan Jingjie, JJApproved Signatory
!e d,tr!!ffi bim ffiiriE n tr rn c6arM |' €16... o.d'ft d r.a.dtfrm..dodmnrtii ldG6.-I-dffiFifiEiii6-lb,riE n rd f,n cal.rM |' €16... o.d'ft d r.a.dtfrm..dodmnrtii ldG6.-ltd
.tah{t hdrrd.D, ,n n!.C..mrt d. ds|Ury bbr.O].r,ib.n ar6ddrah@dEhcdF/r d.n dhdmdr.b r. c d rd ut! d.olmr.6 d
hr'rrroE6 'l{rnon $r6vdotm. coi'..rydi.r r. dqrgl d6!r hturroE6 'l{rnon $r6vdotm. coir
|I.mlor ot iha SOS g|urD (soa SA)
fltrbl9n'.bxrilttlrdlOar 2@B+l '}|.ljE8ruft.el3+l l*M
rErE&2rj6ra@rErEt64rt6n *.or,'dHL{t-a)d.l!s lt(l!a)6am . .Fd'|lo.r6
Test Report No. SHAEC1018971802 Date: 06 Jan 2011 Page 2 of 4
Test Results I
Test Part Desdiotion :
Spo.ime|| tlo. SGSS plelD De6.ridion1 SHA1G189718.002 Silvermetal(base)
Remarks :
(1) 1 mg/kg = 1 PPm=0 0001%(2) MDL = Melhod Detection Limit(3) ND = Not D€tected ( < MDL )(4) --" = Not Regulated
RoHS Dli€diw 200295/EC
Test M€thod : With r€ferenc€ to IEC 62321 :2008(1) Determin€tion of Cadmium by ICP-OES.(2) Determination of Lead by ICP-OES.(3) Detemination of Merorry by ICP-OES.(4) Determination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis.
Test ltem(s)Cadmium (Cd)Lead (Pb)Mercury (Hg)H€xavalent Chromium (CrVl)
Limit !d!100 ms/ks
1,000 ngfl(g1,000 mg/kg
UDt OA2 N D2 1 52 N DO Negative
Notes :(1) The maximum permissible limit is quoted from the docum€nt 200t618/EC amending RoHS dircctive
200z95tEC(2) " spot'test:Negative = Absence of CrVl coating, Positive = Presence of CrVl coating;The tested sample should be further verifed by boiling-wateFextraciion method if the spot test result isNegative or cannot be confirmed.. Boiling-water-extraction:Negative = Al6€nc€ of Crvl coating; Positive = Presence of CrVl coatingThe detected concentration in boiling-wateFextraction solution is equal or greater than 0.02 mg/kg with50 crn" samole surface aree.For conosion protec-tion coatings on metals: Information on stoEge conditions and produc-tion date ofthe tested sample is unavailable and thus results of Cr(Vl) represent status of the sample at the time oftestang.
br.dMIn.!brrbcdDqitdbrro-dlsfl .rIryk F!t!ryrrr-.rrd.{trqlli{$!fr the:r!n. @mqrrl€ t Ihr ra
id ri.-th oo.r..r'. ii.hr ibhdri.hq.rcrnrl r'i.!rroD, ,n ln.Cmyt * ddl|lnr a! qsbtsdrbrirldd'.r'aorrtrrd.ud,litrtr *raoM||,it tldmdd'rl !.n9o.!'{d.r-tIntul, nrMrrh.rilb.!rdr.|fisno.iib4qd'i.||db(nniehte
dh rhsl h s b..rd nirr6rt6h 6rr.(.)bb.
lr.m!.r of lns SGS Oroup (SGS SA)
ttr$ri'rrnhtrirLrt$ndrlnr 20@33+1.I|.ltrgldrllr9l3tl l*2@
rElE{6-a)fia!2161} IE!E(6{|FSA m.o.4..!6H.j 6-21)i1a@s i{.:{F2l)6a6@ . rFr*r0.Ntr
SGSTest Report
ATTACHMENTS
RoHS Tssting Flow Chart
1) Name of lhe person who mad€ tosting: Allen Xiac, Wesley Wei/ Andy Zhao2) Name of the pe6on in charge of testing: Jeff Zhang/George xu3) These sampl€6 w€re dissolved totally by preconditioning method according t5 below flow afiad. (Cfl
test method excluded)
,ndn o$r.l d$b 6.t!.nq *4bb n nq]44!4!4!b!a,b!! d dir tu4r{- r rF! rt oornm t E n4b ooolffi d E[tEs6ar4!!99!!!!!4^|h&id n.rraidtu.4eddt'hi-466 -r|n6
dfi ffi GEEEiiF.nd-fr Eft cs,' r ni
in &r.d d* h t n crdirtdrd|.. nir fidfrdoid h. DE tuorr rd!! h nn,lnnsdrrh.rytdddMdhdt
No. SHAEC1018971a02 Date: 06 Jan 2011
.M h*dn d-L16'rbtu16!bl.)ar.
Page 3 of4
59mple Preparation
Sample Measurement
Acid digestion withmidowave/ hotplate
1) AlkaliFusion /DryAshing
2) Acad to dissolveAdding 1,&
diphenylcarbazide forcolor development
Adding 1,5-diphenylcarbazide
for colordevelopment
A aed color indicatesthe presence ofcf'.lf necessary, confrm
PbtcdrHg
Positive
Negative
f!lbrLtl| bd,ohillmrciotl zdzst+l .Il .trdldrlqD||efl l* 2@
lElC&r)614!!6glElE6-?lFaet9 a.4.!amHro.2tlala@{ l{j{F-AFeEa . $dtroq6
Monlerolrt so8 Gbup (sossa)
Test Report No. SHAEC1018971802 Date: 06 Jan 20 1 1 Pag€ 4 of 4
Sample photo:
sHA10-189718.002
SGS authenticateth€ photo on original report only
"' End of Report ""
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il.mbor ol lno 8OS omur (8OS S )
DONGGUAN CIryXNHAI METAL PRODUCTS CO,,LTD.
1ST WEIMIN ROAD HENGZENG AV.XINAN COMMUNITY CHANGAN TOWN DONGGUAN CITYGUANGDONG PROVINCE
Test Report No. SHAEC1018971801 Date: 06 Jan 201 1 Page 1 ol4
The following sample(s) was/w€ro submitled and identifed on behalf of the clients as : FUSE CAP
SGS Job No. :
Date of Sample Received :
Testjng Period :Test Requested :
Test Method :
Test Results :
sP10-043287 - SH30 Dec 2010
30 Dec 20'10 - 06 Jan 2011Selected test(r) as requested by di6r(.
Pleas€ refer to next page(s).
Please refer to next page(s).
Signed for and on behalf ofSGgCSTC Ltd.
,23r"-Fan Jingjie, JJApproved Signatory
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l|mb!. or 0|o SCS Sroup (SGg SA)
Test R€port
Test Results :
No. SHAECl018971801 Date: 06 Jan 2011 Page 2 of 4
Test Part Description :
SpednsrNo. SGSSandelD Ds6cdpdon1 SHA10-1897'18.001 Silvormetal(pleting)
Remarks :
(1) 1 mgikg= 1 PPm=0.0001%(2) MDL = Method Detection Limit(3) ND = Not Detected ( < MDL )(4) '-" = Not Regulaled
Rol{S DNl€ Jve 2d}2/95/EC
Test Method : (1)lEC 62321:2008 application of modilied digestion by surface etcfiing for Cadmium, Lead andMercury. analysis by ICP-OES(2)Wth reference to IEC 62321:2008 for Hexavalert Chromium by spot test / Colorimehic Method.
Test ltem(s)
Lead (Pb)Cadmium (Cd)Mercury (Hg)Hexavalent Chromium (CrVl)
!!d! ud!1,000 mg/kg10O mgikS
1,000 mg/kg
MDt 0p11 0 N D10 ND10 NDo Negative
Notos :(1) The maximum permissible limit is quoted from the document 2005/618/EC amending RoHS directive2002,9stEc(2) " spot-lest:Negalive = Abs€nc€ of CrVl coating, Positive = Presence of CrVl coatingiThe testgd sample should be further verifed by boiling-wateFextraction method if the spot test result isNegative or cannot b€ confirmed.o Boiling-water-extraction:Negative = Absence of CrVl coatjng; Positive = Presence of CrVl coatingThe detected concentration in boiling-waterextraction solution is equal or greater than 0.02 mg/kg with50 cm2 sample surface area.
eunr.iMIl 6bb.nrd nJtr6rtb tu MDr.(.)bbd .
fi&rntrl bdea|r.4ltfiOri 2@B+l .-tl .lf6ltftnq|{|l l l|: z@r
t EIE (S-ti) 614@563 lE|EFllFaA6tl me..e.mHl''{E-a}a(@a Hi{l-A)aeKl . $.dli{s@
M.mbd ol lno SOS O|uD (SOS SA)
Platlng Pb/Cd/Hgrcre Testing Flow Chart
1 )2)
Test Report
ATTACHMENTS
Nam€ of the pe6on who made te€ting:Wesley WeiName of the person in charge of testing: Jeff Zhang
[email protected]!l.cbr.oi-rcdire.rrrtiornftd.!nn,st!r.dds.{did{bl.n!bd,b *ftdc dm doi..6,rqdr.Tmr rt c.draF b ELdurr. oo&mr d *$.ffim.4.!'td
No. SHAEC'1018971801 Date: 06 Jan 2011 Page 3 of4
Acid washing ofplating layer
Precisely weighingsample after acid
wasnrng
Adding 1,$diphenYcarbazide for
color development
A red color indic€lesthe presence of cr8t.lf necess€ry, confirm
t'lltt itYtudlln lhb,lj.idijoir [email protected]'l.l[At|I|li30tstl ll:2@
rEtEF{t)611@r* Fala!402!04
IE|E&a)6g3tDi&ln-all5,LlB
{.rDorofDo SOg C|ouD (saNl S }
Test Repon
Sample photo:
No. SHAECl01897'l801 Date: 06 Jan 2011 Page 4 of 4
sHA10-189718.001
SGS authenticatethe photo on original report only'*' End of Repon '*
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rndoa|(r|..t ucd0rr$t ctn nrrldrod"Dlhn .drEdrnr
rrb h |5Db(.)bb. .
t'lr.Er$.dl|rbEn|tidt daorr 2@3 rE E(6-21)ita0?!50 tEt€(6-AF$St ||r.!!..!rcohTl .ll.if,Ellrla€r9lor+t ll 2d!A, Hr{i-al6 @. rr(6-2rF@ . sd*re.rs
M.mborol0ro SOa Oroup lgog S )
Test Report No.: GZ1 106081316/CHE[.{ Date: JUN 24, 2011 Page 1 ol 4
XIAMEN LICHUN ELECTRONIC ELEMENT CO., LTD42.2 XINGLIN WEST RD,361OO2 JIMEI OISTRICT, XIAMEN FUJIAN. P.R.C
The following sample(s) was/were submitted and identified on behatf ol the applicant as BOS| GLASS TUBE
SGS Job No.
SGS Inte.nal Rof erence No.Dat€ ol Sample ReceivedTesting Period
Test Requestod
Tesl Method
xM13205987EC
JUN 23, 2011
JUN 23, 2011 TOJUN 24, 2011
Selected test (s) as requested by ctient.
Please refer to next page(s).
Please refer to next page{s).
Based on the perlomed lests on submitted sampte(s), the results comptywilh the RoHS Directive 20O2/95/EC and its subsequent amendmentg.
Test Bosult(s)
Conclusion
Signed for and on behalf olscs-csTc Lrd.
rk .roldr 8ssqq?ieo8€^)
Test Report No.: GZl 106081316i/CHEM Dale: JUN 24, 2011 Page 2ol 4
Test Results:Description tor specimen 1 : Transparent glass tube
RoHS Directive 2OO2yS5/EC
Test ltem(s)
Cadmium (Cd)Lead (Pb)lrercury (Hg)Hexavalent Chromium (CrVl) byalkaline extraction
MonobromobiphenylDibromobiphenylTdbromobiphenylTetrabromobiphenylPentabroftobiph€nylHoxabromobiphenylHeptabromobiphenylOctabromobiphenylNonabromobiphenylDecabromobiphenyl
Monobromodiphenyl etherDibromodiphenyl elherTdbrornodiphenyl etherTetrabromodiphenyl elherPentabromodiphenyl etherHexabromodiphenyl elherHeptab(omodiphenyl etherOclabromodiphenyl etherNonabromodiphenyl elherDecabromodiphenyl ether
Note:L mq/kg = ppm2. N.D. = Not Detected (< tuDL)3. MDL = Method Detection Limit4. '-" = Not regulated
Test Method (Reference)
IEC 62321: 2008, ICP-OESIEC 62321: 2008, ICP-OESIEC 62321: 2008, ICP-OES
IEC 62321:2008, UV-Vis
IEC 62321:2008, GC,MSIEC 62321: 2008, GC-MStEc 62321: 2008, GC-MSIEC 62321: 2008, GC-MSIEC 62321:2008, GC-LrSIEC 62321: 2008, GC-[.4SIEC 62321: 2008, GC-[,!SIEC 62321:2008, GC-MSIEC 62321:2008, GC-MSIEC 62321:2008, GC'MS
IEC 62321: 2008, GC-MSIEC 62321: 2008, GC-MSIEC 62321: 2008, GC-MSIEC 62321: 2008, GC-MSIEC 62321:2008, GC-MSIEC 62321:2008, GC-MSIEC 62321:2008, GC-frSIEC 62321:2008, GC-MSIEC 62321:2008, GC-MSIEC 62321:2008, GC-IIS
Unit
mgKgmg/kgmgikgmgag
Resull
N.D.N.D.N.D.
N.D,
N.D.N.D.N.D,N.D,N.D.N.D.N,D.N.D.N.D.N.D.N.D,N . D ,N.D.N,D.N,D.N,D.N,D.N.D.N.D.N,D.N.O.N,D.
MDL Limit2 1002 10002 10002 1000- 10005555555
55- 1000
555555
5
m9Kgmg/KgmgKgm9KgmdkgmgKgmsiksmgftsmgikgmgftgmgesmgKgmg/KgmgKgmgKgmgKgm(yKgMEKgmgKgms/kgms/ksm9{(g
|{ard,rlqrr.lf.rFi.ldL C.An
rk.rladf,849qt|p|ao9€A)
Test Report No.: G21106081316/CHEM Date: JUN 24, 2oi1 page 3 ot
ATTACHMENTSRoHSTesting Ftow Chart
1) Name of the person who made testing: Be a Wang / Cutey yu / Ross Zhan2) Name ol the person in charge ot Fsting: Adams yu / Ryan yangJ)r nese sampEs w€re d|ssotved lolally by pre-conditioning method according to below flow chart(C6+ and PBBS/PBDEs test method €xctudeo,.
Acid digeslion withmicrowave/ hoiplate
'1 ) Alkali Fusion /Dry Ashing
2) Acid toAdding 1,tdiphenylcarbazide
Adding 1,$'diphenylcarbazide
development indicates thepresence of cF.. lf
Pb/Cd/Hg PBBS/PBDEs
Negative
rrf,ta..rrabi E-.an lbair-. L-.ryr.!r {qtd4.. aa-aa
tc-t-x!.ri.' rr ! ortr r- r*'d|l r$rai|-...F..!..4-..! +! r!ji!s.! !!a!r.t ffi -i( -r.r.
r-a.hrt r..rr.F..dglr.h-.r.rnlr,3rr{||.tl.|x.lnaa.rn*lart-qaEirS rt.rL4.rdd-c.ei,
x.||l!..Cnr s8AC.r?{8gag )
Test Report No.: G21 106081316/CHEMDate:JUN 24,2011 Page 4 ot 4
Sample photo :
SGS authenticate the photo on original report onty
"' End ot Repon "'
.hrr.r.drr-trlrnda.rbtne-rliatrF*tar.{d.it5r.a.t*a'-dbti.a'..a.,qrr14 -r.i}rrid J-c.-.+
& ri! Ir5fltry*r {Ddr.6!E rp{0tE tt{t[na *...ra*?r,n lll.ft.atlblltlgl+&lltltli$i ltlr rFdls rF{nt6 . rd{r.a-(-
r.'I..r.-.r.n,''
rhr!.rC ||!. 8EaC!.r trlcgE^l
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00251051
PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI
MYRA LV STEPHEN TSANG CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER
PAGE 1 OF 8
APPLICANT: LITTELFUSE,INC. DATE: APR 13, 2011 800 E. NORTHWEST HWY
ATTN: A. CESISTA/ K. BACILA
SAMPLE DESCRIPTION: One(1) submitted sample said to be White yarn. Part Description : Yarn. Part Number : 648106-001. Date Sample Received : Apr.7, 2011. Date Test Started : Apr.7, 2011. ***********************************************************************
TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
*********************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00251051
TESTS CONDUCTED
PAGE 2 OF 8
(I) Test Result Summary :
Testing Item Result (ppm)
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
*********************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00251051
TESTS CONDUCTED
PAGE 3 OF 8
Testing Item Result (ppm)
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND
Remarks: ppm = Parts per million = mg/kg ND = Not detected
Responsibility Of Chemist :Dent Fang / Ken He
(II) RoHS Requirement: Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. ***********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00251051
TESTS CONDUCTED
PAGE 4 OF 8
(III) Test Method:
Testing Item Testing Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Date Sample Received : APR.7, 2011 Testing Period : APR.7, 2011 TO APR.11, 2011 ***********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00251051
TESTS CONDUCTED
PAGE 5 OF 8
(IV) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008
*********************************************************************** TO BE CONTINUED
sampling/grinding or cutting
weigh sample and for different
material, digest the sample with
make up with deionized water
Cd/Pb/Hg
analyzed by ICP-OES
weigh sample and add alkaline solution
definite temp.
make up with deionized water and add diphenyl-
carbazide solution
Cr6+
weigh sample and add organic
soxhlet extraction or
solvent extraction
concentrate the extract and make up with organic
PBBs/PBDEs
analyzed by UV-VIS
analyzed by GC-MSD
spot test
get 50cm2 samples
boiling water extraction
metalpolymers / electronics
negative*2confirm the tested samples are totally
dissolved No
cool and filter the extract
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00251051
TESTS CONDUCTED
PAGE 6 OF 8
REMARKS: *1: List of appropriate acid:
Material Acid added for digestion
Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*********************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00251051
TESTS CONDUCTED
PAGE 7 OF 8
Test For Halogen Content Reference Standard: EN 14582
***********************************************************************
TO BE CONTINUED
add absorbent in a combustion flask & place weighed sample in equipment
fill the combustion flask with oxygen
ignite then leave the flask at room temperature
transfer the absorbent into a volumetric flask
make up with deionized water
sampling/grinding or cutting
analyzed by ion chromatography
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00251051
TESTS CONDUCTED
PAGE 8 OF 8
***********************************************************************
END OF REPORT
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 E-mail: [email protected] www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00240565
PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI
MYRA LV STEPHEN TSANG CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER
PAGE 1 OF 8
APPLICANT: LITTELFUSE,INC. DATE: JAN 25, 2011 800 E. NORTHWEST HWY
ATTN: A. CESISTA/ K. BACILA
SAMPLE DESCRIPTION: One(1) submitted sample said to be White yarn. Part Description : Yarn. Part Number : 648115. Date Sample Received : Jan.20, 2011. Date Test Started : Jan.20, 2011. ***********************************************************************
TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
*********************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 E-mail: [email protected] www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00240565
TESTS CONDUCTED
PAGE 2 OF 8
(I) Test Result Summary :
Testing Item Result (ppm)
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
*********************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 E-mail: [email protected] www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00240565
TESTS CONDUCTED
PAGE 3 OF 8
Testing Item Result (ppm)
Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND
Remarks: ppm = Parts per million = mg/kg ND = Not detected
Responsibility Of Chemist :Dent Fang / Ken He
(II) RoHS Requirement: Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. ***********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 E-mail: [email protected] www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00240565
TESTS CONDUCTED
PAGE 4 OF 8
(III) Test Method:
Testing Item Testing Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
Date Sample Received : JAN.20, 2011 Testing Period : JAN.20, 2011 TO JAN.24, 2011 ***********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 E-mail: [email protected] www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00240565
TESTS CONDUCTED
PAGE 5 OF 8
(IV) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008
*********************************************************************** TO BE CONTINUED
sampling/grinding or cutting
weigh sample and for different
material, digest the sample with
make up with deionized water
Cd/Pb/Hg
analyzed by ICP-OES
weigh sample and add alkaline solution
definite temp.
make up with deionized water and add diphenyl-
carbazide solution
Cr6+
weigh sample and add organic
soxhlet extraction or
solvent extraction
concentrate the extract and make up with organic
PBBs/PBDEs
analyzed by UV-VIS
analyzed by GC-MSD
spot test
get 50cm2 samples
boiling water extraction
metalpolymers / electronics
negative*2confirm the tested samples are totally
dissolved No
cool and filter the extract
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 E-mail: [email protected] www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00240565
TESTS CONDUCTED
PAGE 6 OF 8
REMARKS: *1: List of appropriate acid:
Material Acid added for digestion
Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*********************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 E-mail: [email protected] www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00240565
TESTS CONDUCTED
PAGE 7 OF 8
Test For Halogen Content Reference Standard: EN 14582
***********************************************************************
TO BE CONTINUED
add absorbent in a combustion flask & place weighed sample in equipment
fill the combustion flask with oxygen
ignite then leave the flask at room temperature
transfer the absorbent into a volumetric flask
make up with deionized water
sampling/grinding or cutting
analyzed by ion chromatography
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 E-mail: [email protected] www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00240565
TESTS CONDUCTED
PAGE 8 OF 8
***********************************************************************
END OF REPORT
scsI
Test ReportPOLYFIL AGOBERALLMENDSTMSSE 2OA,
was/w6re submitted and identified by/on behalfofthe client as:
Validit nownForQueStiPlease Co ith scs
No. : CE/2011/84950 D e | 2011112101
CH€3OO ZUG / SWITZERLAND
Cu99.9MSn'1'14595
2011t1lt25201 1t11/25 rO 201I |1',01
Page: 1 or 7
rr|| [ltt!|||tlt[t
The following sample(s)
S€mple DescriptionBuyer/Order No.Sample Receiving DateTesting Period
lest Result(a) Plea6eefer to next page(s).
prqt iadsd Ds Gn ,epd eind bComFiy -r ,: !;t lLr. . . i ; l :r l i l l{ i l rt lrd r qti ' r^rl l i9i: l+,11\- em+,i , -,:r. ift",rl.
.ysuq8d b b cs€rcond rbns d ssubrd lo Tems ad cd@ l.l:
o n L y a i d w l h L n h . t m B d c | € d l n !
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Test ReportPOLYFILAGOBERALLI\4ENDSTRASSE
T66i R.6ultls)
PART t.lAME No.1
No.: CE/2011/84950 Dale :2O114ZO1
2OA, CH63OO ZUG / SWITZERLAND
Page'.2 of 7
t I] t l
SILVER COLORED METAL WIRE (INCLUDING THE PLATING LAYER)
Te3t lt6m(s) Unit Method MDLR.3ultNo,l
Cadmium (Cd) mg/KgWith reterence to IEC 62321r 2008 andperfomed by ICP-AES.
n.d.Lead (Pb) mgKg 24Mercury (Hg) mS/kS n.d.Hexavalent Chromium Cr(Vl) With reference to IEC 62321: 2008 and
pedormed by Boiling \r€ter ext€ctionMethod.#
Negative
Sum of PBBS
mgikS With reference to IEC 62321: 2008 andperfomed by GC/MS.
n.d.Monobromobiphenyl 5 n.d.Dibromobiphenyl 5 n.d.Tribromobiphenyl 5 n.d.Tetrabromobiphenyl 5 n.o.Pontabromobiphenyl n.d,Hexabrcmobiphenyl 5 n.o.Heptabromobiphenyl n.d.Octabromobiphenyl 5 n.d.Nonabrornobiphenyl 5 n.d.Dec€bromobiphenyl 5 n .d .Sum of PBOEa n.d.Monobromodiphenyl ether n.d.Dibromodiphenyl ether 5 n.o.Tribromodipheny! ethe. 5 n.d.Tetrabromodiphenyl ether n.d.Pentabromodiphenyl ether n.d.Hexabrcmodiohenvl ether 5 n.d.Heptabromodiphenyl ether 5 n.o,Octabromodiphenyl ether n.o,Nonabromodiphenyl ether 5 n.d.Decabromodiphenyl ether 5 n.d.
eGlG{d rh s ied @d €nrclb Bpdcn€ry 'l+ !r ! rlrl . .n 1!ts,:r1,rtilr. ;l'!l* rrn . imri+Al'r-\r jrl4.f4! 1r€11hsdocmdssdby'h€c.mpany&bldlobcffi6|codibGo's*to. e.d'mc romal dmstu suq
d ^ t ' n d w l h L n h r m B d c r . d ! n d p o B d r t s t o G c s r a n d r h 3 d Mldrrgh6add]Ed'on6un6lh6'm
t',i!r: :d, dri:_ 11rs6rorPre
Test Report No. : CE/2011/84950 Date | 2011h21O1 Page: 3 of 7
tl]tIlltltfltttltPOLYFILAGOBERALLMENDSTRASSE 2OA, CH€3OO ZUG / SWITZERLAND
Test ltem(s) Unit method MDLResultNo.1
HalogenHalogen-Fluorine (F)(CAS No.: 14762-94-8)
mg/Kg With reference to BS EN M5A2,2007.Analysis was perfomed by lC.
50 n,o,
HalogenChlodne (Cl)(CAS No.: 22537-1s1)
50 n.d.
Halogen-Brcmine (Br)(CAS No.r 10097-32-2)
50 n.d.
Halogen-lodine (l)(CAS No.i 14362-44-8)
50 n.d.
Note :1. mg/kg = ppm : 0.1wf/6 = 1o00ppm2. n.d. = Not Detected3. MDL = Method Detection Limit4 - " - "=No tRegu la led5. '" = Qualitative analysis (No unit)6. # = a. Positive means the presence of CrVl on the tested areas
b. Negative mgans the absence of C l on the tested areasThe dgteci€d concentration in boiling-lvater-ext€ction solution is equalor greaterthan 0.02 mg/kg with 50 cm,tested areas.
7. The sample(€) was/wer6 analyzed on behalfof the applicant as mixing sample in one testing. The above result(s)was^^/€re only giv€n as the informality value.
'nrhstar€Fnd€f ontrorbsmpq3)Idd rhEbd,etsn6ndbGComFny f l t r , l r i 9 ! r . , r l i ] l : r r ! l { : : l : : ; l i ' ! i : l j i A r i i F -5 ! , [ 1 ' e t r ; ' f ' , , ' l ] l t ) [ l i 1 'n3dumd ts6su6d ' l hscomtsny5u*db t csccond1 t r sds
sib iv 6 10 6 o er 5d b6 @mntft,ltrrsandd odd3undrth€ta mol & €pdud depr 'n ju r, ftd
+l r l *J l : r (+s610r ) re t7e f +sitlfuirL!{:,r rr ir: i - i.hsror
IlF
Test Report No. : CE201'1/84950 OaL .2011h2,01 Pager 4
according to belo\ / flo /
POLYFILAGOBERALLMENDSTRASSE 2OA, CH63OO ZUG / SWITZERLAND
1) These sample6were da66olved totally by pre-conditioning methoda Cf' test method excluded )
Name of the pe6on who made measurement: Climbg€at YangName ofthe pe6on in charge of measurement: Troy Chang3)
ICP-AES
Sample Material Dige€tion Acid
S1eel, copper, aluminum, sold€r Aqua regia, HNO3, HCl, HF, HrO,
Glass HNO3/HF
cold, platinum, palladium, ceramic Aqua regia
Silver HNO3
Plastic H2SO1, HrOr, HNq, HCI
Othe.s Any acid to totral digestion
ii. irei,.or if *q oy t . cop-r " ,g .oo-maa"J ' * .6b i " - ' *dco^d ' * "6 .Edrcn ico@isbdM!os@]bi.*ddb" -'d l,nsdd 6 *,* i5r
*l iq:i";* @"* -;d.." **o.ooissr,s.ry - r"
"rd;^ a * -nd .
rtf:r:: r1lirtii+ 1l i s6 io,t,e tTe t r s lo:)2e 'r7 ffiar(om
Acid digestion by suitable aciddepended on difierent samplemderial (as belo\ , iable)
Micro\rave digestion with
HNO/HCVHF
Heat to appropriat€
temperature to e,\tract
Cool, filter digestate
through filter1) Alkal iFusion2) HCltodissolve
at 540 nm by UV-VIS
Test ReportPOLYFILAGOBERALLI\4ENDSTRASSE 2OA,
No. : CE2011184950 Oale'. 201 lh2lo1
CH43OO ZUG / SWITZERLAND
Page: 5 of 7
t l | l [ ] | | I t t | l
PBB/PBDE1) lllanE of the person2) MnE of the person
analytical FLOW cHARTwho nEde npasurenEnt: Ronran Wongin charge of nEasurenent Troy Chang
Scrcen analysis
" " " " " 1 " " " " " "
Sanple extraction/So*rlet rEthod
ConcentratdDiluteE)dracbd solution
First testing process -----t
Optional screen process -.--
Confinmtion process - .>
-s."pb---_-]--------r-------[S-r-tp]-j-a"arn"-_l-----r----
Ft ler
Analysis by GC/liS
cm€ry r r ' r j l j r ) t r . : r i l i " . : . l ! i * i , ; i i l ' r l t : e l . t i l : i l r t / . 1 \ ' l r Fn . r ' j : 1 . ' t l 6+
to €sd'o'c ramd dm6tu suq
d^t ,nd vihin rb rmis ot cr€d s i3'lbr.ohbadd€donsu.ddsera od b. repdued eiceol itul wiher
! idsnrzorNe-tu!acirrrer/*l:r/f,!.r +!!4J1i:irlre 02)r!e
I
Test ReportPOLYFIL AGOBERALLMENDSTRASSE
No. : CE/2011/84950 Daie | 2011h21O1
2OA. CH-6300 ZUG / SWITZERLAND
Analytical flow chart of halogen content
1) Name of the p€rson who lmde rneasuredEntr Rita Chen2) llan€ of the person in charge of nEasurerEdt: Troy Chang
Page: 6 of 7
comoad N]r]F,j!:ir.. I tiir lt{!l; ;]]rltl.1!- . r. irtsih-{} I 11 FiT . f!l r19i!+l
fi"JHl"l;liiii',i!',i.iwi;c"ry"';ti"-"c*""tc"t.^a sriu*-t i*n d..",; ''jbl.n bi... .d c.d*" 6, €. a " ' ' i i a - - o e , " a a . ^ * * ' ; . n b a d " i s d l b d i b m a i o ; d k . d h ;
; ; ; q ; ; ; ; oo ,4a t ; . : 6 . ? .€6@- -hsd ; "db . - "b1 .
r L - I I i d l L a i
Sarple pretreatrnent / Separation
Weighting and putting safipte in cell
Orygen Bomb Cofibustion / Absorption
Dilution to fixed volurne
Analysisw€s perfornEd by lC
Test Report No. : CE/2011/84950 D€te 2011h2101 Paget 7 of 7
tl] tlt II][]lPOLYFILAGOBEMLLMENDSTRASSE 2OA, CH63OO ZUG / SWITZERLAND
* The teeted sample / pa is maaked by an arrow if ifs shown on ih€ pholo. '
" End of Report -
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