7 on Webspectra Intermediate I

CyHao

CnHzntztN X n C

Hea z HioHe42L2 units

H NMR Table of H Environments _4

8 spinppm Int Hoofneighbors assignment

2 2 3 s EWG CHz

5.83 I d

yc ciHx3

6 12 I d l

6.24 I dd 2 Iti

HABHB Jars Jose doubledoublet

H Ha

3z

t 3 61 dI t l t l

l l 1

NOaldehyde

Iexchange

Ado

noetchargeupfielddownfield

St

St St

sideshielded shielded

13C NMR Table of C Environments 4

Sppm assignment28 alkyl Cftz129 c C

138

200 c o

2saturation

GEE CH3solvent

0dc

Normalalkyl

Pieces

cfct

CHz

Hz0

it A tHgs

at y HSH CHzH

O

H H a s xH tats

0It itCHz 9.5X

L HH

to pHe

robot 13 ddsins 0

CHzHD Sa o zitz

A H Hcdddd B

13 6 12112

HisFIz 12 18 He

4Hey trans

13 6 12 He IsH double

Hy cis doublet23

It Se o 2 Hegemminal

The alkene systemtrans Cislarge SvalueJvalue

IT

1B D C

0 large d

yy Ho5pmiss.ng

ddHf Hcdusmall

Ar H

RI I t

Sdven t Thesdd

HNMR Table 5 Environments

ppm Int unit in assignment

6.2 I d 1542leg 14 2

7 2 I dish It

7.44 2 delta I Ar Hx 17.66 Z d He I

011.5 l S exchanges 1 off

Z yt Ioa EEti

2 I 4 7

15ha

Htrans

H

CqHa02 CqHyNoy

missing Hoz HozNitro group

EE Itis ES AABB

allottedx x

H

y7 r 49 at No

AA'BB 15He

Noctt

IROHHogg

INE

i tiite Iff yaffoHYo faarpthff 0 We

n 9 atHamar stonger Eatdoz

µ M Iwclose

CalmRAr IN

color

H I I ill HX gd

0

if Iat a Y

go