Gluten Free Pulse Milling Wet and Dry Fractionation Applications of Peas Lentils and Chickpeas in...

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Pulse-milling: Wet and dry fractionation applications of peas, lentils and chickpeas in gluten-free foods Mehmet C. Tulbek, Ph.D. Technical Director Northern Crops Institute Fargo, ND Institute of Food Technologists 2010 Annual Meeting Gluten-free foods: Opportunities and challenges

Transcript of Gluten Free Pulse Milling Wet and Dry Fractionation Applications of Peas Lentils and Chickpeas in...

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Pulse-milling:Wet and dry fractionation

applications of peas, lentils andchickpeas in gluten-free foods

Mehmet C. Tulbek, Ph.D.

Technical Director

Northern Crops InstituteFargo, ND

Institute of Food Technologists 2010 Annual MeetingGluten-free foods: Opportunities and challenges

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DRY PEAS, LENTILS and CHICKPEAS

Base ingredient in gluten free foodsHigh protein & dietary fiber

Non GMO

Poor allergen

Low glycemic index

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COMPOSITION OF PEAS, LENTILS & CHICKPEAS

Dietary fiber ≅ 25‐35

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WORLD DRY PEA PRODUCTION (MT)

Source: FAOSTAT 2008

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Major Exporters

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WORLD LENTIL PRODUCTION (MT)

Source: FAOSTAT 2008

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Major Exporters

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WORLD CHICKPEA PRODUCTION (MT)

Source: FAOSTAT 2007

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Major Exporters

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FEASIBLE TO FRACTIONATE ?

Pin Milling, Air Classification and

Fractionation

Lentils and chickpeasStrong and growing market due to changingworldwide agricultural practices

Dry peas (yellow)Price & functional advantages

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GROWER PRICES – JULY 16th 2010

Lentils – $ 25-32 / CWT 

Chickpeas - $25-30 / CWT 

Green peas – 8-9.5 / CWT 

 Yellow peas – 6.25-8.00 / CWT 

CWT = 100 lbs = 44.5 kg

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LITERATURE OVERVIEW

Pin Milling & Air Classification

Significant research conducted in 1980s

Tyler (1982), Tyler (1984) and Tyler andPanchuk (1982).

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LITERATURE OVERVIEW

Air classification and protein-starchfractionation is similar in all pulses exceptchickpea (Han and Khan 1990).

High fat content

Based on variety 5-8% fat content

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DRY FRACTIONATION PROCESS

Fractionate protein, starch and fiber components indry milling process

Fractionation is conducted based on particle size.

Dehuller

Pin mill / jet mill

Air classification REQUIRED EQUIPMENT 

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DRY FRACTIONATION PROCESS

DehullingKey process for the removal of 97-98% of thefiber portion

Dry fractionation

Protein & starch separation

Pin mill OR jet milling

Air classification

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FLOWCHART 

Dehulling 

 – whole 

peas

Pin milling  – split (dehulled) 

peas

Air classification  – split 

(dehulled) pea flour   Packaging

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DEHULLING

Removal of outer kernel

Easier to conduct in peas and lentils

Much difficult process in edible beans andchickpeas due to crop characteristics

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DEHULLING

Impact dehulling

Stone dehulling

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DEHULLING

•1000 kg Dry Pea (%9 Hulls)•90 kg pea hulls removed

•910 kg dehulled or split peas

•Pea hulls are rich in terms of insoluble fiber.

•%85 Insoluble fiber

•%15 Soluble fiber

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DRY FRACTIONATION

•910 kg dehulled or split peas•Pin milled

•High speed pulverizer•%100 under 350 mesh (60 micron)

•Very fine material

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Pin mill

Courtesy 

of  

Particle 

Control LLC

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AIR CLASSIFICATION

•Fluidized tower system

•Particles in vacuum

•Separation based on particle size•2-20 micron - Protein concentrate

•20-40 micron – Starch concentrate

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Air

Classification

System

Courtesy 

of  

Particle 

Control LLC

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Air

Classification

System

Tower and 

Dust Bag

Courtesy 

of  

Particle 

Control LLC

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Heavy 

Fraction

Starch‐rich

Flour

Courtesy 

of  

Particle 

Control LLC

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Light 

Fraction

Protein‐rich

Flour

Courtesy of  Particle 

Control LLC

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PROCESS OUTCOME

•1 MT = 1000 kg

•90 kg pea hulls•546 kg starch concentrate

•364 kg protein concentrate

•Without any moisture loss (theoretical)

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PROCESS OUTCOME

•1 MT = 1000 kg•6% moisture loss

•940 kg pea flour

•84.6 kg pea hulls

•513.24 kg starch concentrate

•342.16 kg protein concentrate

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Moisture Ash Protein Starch Fiber Lipid APC Mold Yeast

(%) (%) (% dm) (% dm) (%) (%) (CFU/g) (CFU/g) (CFU/g)

Pea hulls 8.2 2.1 2.0 <1.0 >85 0.1 1200 50 20

Split Peas 12.1 2.5 26.5 50.5 1.0 2.2 1000 200 50

Pea Flour 7.2 2.5 26.3 50.1 0.9 2.2 6200 70 30

StarchConcentrate 9.2 1.7 12.4 73.1 0.8 0.7 820 30 10

ProteinConcentrate 8.7 4.6 53.5 8.0 1.0 2.2 500 200 40

DRY FRACTIONATIONINGREDIENT SPECIFICATIONS

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WET FRACTIONATION PROCESSES

Fractionate protein, starch and fiber components indry & wet milling process

Dehuller

Hammer mill

Soaking tanks REQUIRED EQUIPMENT 

Decanter

Spray / drum drier

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WET FRACTIONATION PROCESSES

Dehulling

Key process for the removal of 97-98% of thefiber portion / same as dry fractionation

Wet fractionation

Protein & starch separation – high purity

Hammer milling

Soaking and acid-base treatment

Decanter – filtration - spray or drum drying

Packaging

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Dehulling  – whole peas

Hammer milling  – split 

(dehulled) peas

Soaking  – split (dehulled) 

pea flour

 (pH

 = 10)

Removal of  starch

& protein

Precipitate 

solubilized protein

 

(pH=4.5)

Drying 

Starch

&

Protein

Drying 

Protein

Packaging

#I#2

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WET FRACTIONATION

•1000 kg peas•Dehulling – remove 90 kg hulls

•910 kg dehulled or split peas•Milling

•High speed pulverizer, or hammer mill

•%100 under 100 mesh

•Fine material

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DEHULLING

Impact dehulling

Stone dehulling

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WET FRACTIONATION

Solubilization of pea proteins, sugars and lipids bybase solution (NaOH solution, pH=10.5-11.0 for 1h.extraction)

Removal of starch & protein by decanter orultrafiltration

Protein can also be held at pH=4.5 for

precipitation

Protein and starch are dried by fluidized bed drieror spray drier.

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Decanters

Starch &protein removal

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Decanters

Starch &protein removal

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Separation

decanters

16 level

99.9% starch and85%protein purity

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Spray drier

Proteindehydration -

drying

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Drum drier

Starchdehydration -

drying

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Moisture Ash Protein Starch Fiber Lipid APC Mold Yeast

(%) (%) (% dm) (% dm) (%) (%) (CFU/g) (CFU/g) (CFU/g)

Peahulls 8.2 2.1 2.0 <1.0 >85 0.1 1200 50 20

Split

Peas 12.1 2.5 26.5 50.5 1.0 2.2 1000 200 50

Peafiber 10.0 2.2 2.1 <1.0 >85 0.2 6200 70 30

Pea

starchisolate 11.0 0.1 0.4 >98.0 0.1 0.1 820 30 10

Peaprotein

isolate 11.2 4.2 >85.0 <1.0 1.1 2.1 500 200 40

WET FRACTIONATIONINGREDIENT SPECIFICATIONS

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CHINESE VERMICELLI NOODLE MAKING

Traditional & long process

Mung bean or dry pea

Soaking in tap water

Then acid addition

h Gl b l k l

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CHINESE VERMICELLI NOODLE MAKING

C i i h Gl b l M k l

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CHINESE VERMICELLI NOODLE MAKING

C ti i th Gl b l M k t l

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CHINESE VERMICELLI NOODLE MAKING

Liquid starch sent directly to starchnoodle process

Extrusion

C ti i th Gl b l M k t l

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CHINESE VERMICELLI NOODLE MAKING

Starch is gelatinized

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CHINESE VERMICELLI NOODLE MAKING

Drying vermicellinoodles

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PEA HULLS (PEA FIBER ISOLATE)

GLUTEN FREE END USE

High water binding capacity

Modifies texture

Veggie burges, hamburgers, sausages,nutritional bars, sauces, fillings, bakedproducts

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PEA PROTEIN RICH FLOUR

(PEA PROTEIN CONCENTRATE)

High level of functionality,

bioavailability and lysine content.Bland taste

Good alternative to soy flour/proteinconcentrate (Non GMO and non allergen)

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PEA PROTEIN CONCENTRATE

Beverages

Granola bars

Baby foods

Pasta

TVPs

Meat products - sausages

Veggie burgers

Baked goods

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PEA STARCH RICH FLOUR(PEA STARCH CONCENTRATE)

Rich source of starch (>%72)

Good source of protein (%12)

Acid, retort and shear stable similar tomany modified starches

Improves texture in gluten free bakedproducts

Increases volume/expansion in extrudedproducts

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PEA STARCH CONCENTRATE

PastaBaked products

Batters and coatingsExtruded snacks

Fillings and dressings

Soups, sauces

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PEA PROTEIN ISOLATE

High level of functionality, bioavailabilityand lysine content.

>%85 Protein, %3 Fat, %4 Ash

Good alternative to soy protein isolate(Non GMO and non allergen)

TVPs, beverages, granola bars, babyfoods, pasta, baked products, dressings,

meat products, veggie burgers

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g p

PEA STARCH ISOLATEExcellent gel strength and bland taste

>%98 purityGelling and film forming properties

Vermicelli noodle

Excellent acid, retort and shear stable similar tomany modified starches

Improves crispness in baked products

Increases volume/expansion in extruded products

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g p

CONCLUSION

Pin milling, air classification and wet fractionation

processes can be used in dry pea, lentil and chickpeaprocessing.

Raw material availability, sustainability and price

Dry yellow peas can be utilized based on marketneeds

Vermicelli noodles, TVPs

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g p

THANK YOU

Mehmet Caglar Tulbek, Ph.D.Technical Director

Northern Crops Institute

North Dakota State University1240 Bolley Dr. Fargo, ND 58102

Phone: 701-231-5493

Fax: 701-231-7235

Email: [email protected]

http://www.northern-crops.com