[GAS CHROMATOGRAPHY/MASS CALIBRATION TUNING ...g'-ea'.e' tia" 40.0'-- of mass 198 17.0 - 23 0', of...
40
002291
Transcript of [GAS CHROMATOGRAPHY/MASS CALIBRATION TUNING ...g'-ea'.e' tia" 40.0'-- of mass 198 17.0 - 23 0', of...
002291
smartin
Poor Quality Original
Case No- Contractor Gul-f ^out^Rgs^rch Irst. Contract No. ^I^IL^LI^^
InsTument ID /^W ^>/ „ Date ______t]/^^^£
Lab ID /•Tj^^y^^. Data Release Authorized By
m/e ION ABUNDANCE CRITERIA %RELATIVE ABUNDANCE
51
63
69
70
127
197
198
199
275
365
441
442
443
3C.O • 60.0°'o of mass 198
less man 2.0°; of mass 69
mass 69 relat ive aounoance
less Than 2.0°; of mass 69
40 0 - 60 0^ of mass 198
less than I.OS of mass 198
bay.' peak, 100s: '•a;a' ve abundance
50 - 9 0~: c* mass 1 9 8
10.0 - 300'-. of mass 198
3-eater tha- 1.00\ c* mass 198
pi-esen*. bu: •ess '.na'". mass 443
g'-ea'.e' tia" 40.0'-- o f mass 198
17.0 - 23 0', of mass 442
Ho. 7-
0 c^1
(.-.ۥ. 3
0 C^ '
5^, S"
0I c^o
6, -3^
l'?r^
S.o^
^.3X
'y/. 7S^l Cy^2
Value m pare-thesis is % mass 69,0
Va'ue ir pa'^nifiesis is % mass 442.THIS PERFORMANCE TU\E APPLIES TO THE FOLLOWiNGSAMPLES BLANKS Ar-iO STA^OAROS.
SAMPLE ID
y,/?^ sy ^r^tac^ ^ ^n>, ..l(/c:^ 5^ ^ro .^^^ !)l/ftp^ S^ ^TD
1
LAB ID
.^y^y^r^/^^^y^v^yz?/<^^^<y5^c/•s^'y^'/s^"^/^.•(i1 .1 <y ^'fc- ,g <!/<. rt-</'9 PC/^ /JK-'tf 'f Mt f " 7 »- / >^ V,> < / / ^ / 0 J t- 1
DATE OF ANALYSIS
v/Wr-r
'^/ ----
'/'
Y/^^/y^/ • /
TIME OF ANALYSIS
/.? -•-''?/,-^y
/6-7^
/7 .^ /
y-/-^^
FORM V 4/B4
Br««BiraBBMMBff»«i>tl«CM»f««t!WUIMUffiR!iffiiBBn«Bg««lHtgtfffiSanfl ^
002292
8^ ni p 1 e:Bond s . :
#554 to
I 3<?
444-, Mass
« 37.00?50. 00?
151- 00?52- OO?56. 00?
157. 00?63. 00?65. OO?69- 00173, 00
' 74. 0075. 00
J76.0077- 0078. 00
g79. 00B80-00"81. 00
82. 00
I1 B3.0065. 0071. 00
172. 0073. 0094. 0076. 00
B98. 00®77.00101 00
E4. 00' 5, 00107.00
gbOS. 00B10.00T11. 00117-00
SIQ2. 00Ss3. oo125. 00J827. 00lp8. 00127. 00130. 00§35. 00PG6. 00137.00gu. oo|t7. 0048. 00^3. 00
• • * *SV PERF STD (763-30M DB-5 FSCC (ft3^555 Summed " ^5
0, 00 0. 00
7. RA 7. RIC
2. 50 0. 319.65 1.20
40. 74 5, OQ2. 41 0. 30
S 1. 39 0. 17S 3. 73 0. 47
1.88 0.231. 47 0. 16
S 66,28 B.271. 06 0, 134. 27 0. 538. 18 1. 023. 07 0. 39
58. 93 7. 354. 45 0. 563. 56 0. 442. 80 0. 35
S 3. 21 0. 40S 0. 76 0- 12S 1. 03 0. 13S 1. 14 0. 14S 0, 83 0. 10
1. 15 0. 145. 31 0. 660. 05 0. 110. 70 0. 123. 42 0. 433. 72 0. 462. 17 0. 271. 15 0. 141 - 4 2 0- 18
14. 86 1. 852. 52 0. 31
35. 21 4. 395. 33 0. 677. 71 0. 991. 07 0. 131. 80 0. 221. 03 0. 13
55. 45 6 924. 14 0. 52
50. 04 2, 501.64 0.231.88 0.230. 87 0-113, 49 0 172. 25 0, 251-32 0. 172. 17 0. 270. 89 0. 11
t-di 1 :40-PERF-)3671) 2550 X I . 00
0.# 0In ten .
242,934.
3744.233-135.361.162.142.
6416.103.413772.299.
5704.431.345.271.311.93.
100.110.80.
111.514.82.95.
331.360.210.111.137.
143G.244.
3408.516.766.104.174.100.
5368.401-
1740.178.182.84.
144.21012G.210.06.
^S042485C
/4-300(?8 F
M i n i maMax ima
Mass
155.00156. 00161.00167.0016B,00174. 00175.00177.00180.00191.00185. 00166.00187. 00192,00193. 00196,00198.00179.00204. 00205. 00206.00207.00211.00217.00221.00223.00224.00225.00227.00229.00244.00246.00255.00256 00258. 00265.00273. 00274. 00275. 00276.00277.00296. 00323.00334.00365.00372. 00423.00441. 00442. 00443.00
^ ^ 2 R I C :^^ y ' / 7
INN 01 CALIB 04/S
Min i n t e n ; 79
7. RA 7. R I C
1. 46 0. 1B1. 93 0. 241. 25 0- 164. 54 0. 572 98 0. 371. 08 0. 141-57 0. 203, 65 0. 462. 00 0. 251- 16 0. 151. 52 0. 17
11.67 1.463. 24 0. 401. 81 0. 231. 11 0. 144. 13 0. 52
300.00 12. 486. 32 0. 792. 84 0. 354. 54 0. 57
18. 78 2. 342. 79 0, 351.66 0.234. 85 0. 607. 00 0. 871, 46 0. 187. 75 1, 222. 33 0. 274, 14 0. 520. 98 0. 128. 26 1. 031. 96 0. 24
35. 58 4. 444. 90 0. 612. 46 0. 311. 02 0. 131. 22 0. 153. 01 0. 38
17. 19 2. 152. 38 0. 301. 33 0. 174. 00 0. 501. 51 0. 191. 04 0 132. 09 0. 260. 96 0. 122. 79 0. 356. 32 0 79
49. 67 6- 208 81 1. 10
i. . J.-7CI '
77569,
34/05
I n t e n
143.1S7.121.439.288.105.152353.194.114.147.
1130.314.175.307.400.
9680-612.275.439.
1818,270.380.469.678.141.944.226.401.
95.800.170.
3444.474.238.
99,118.291.
1664.230.129.3S7.146101.202.93.
270.612.
4808.853.
U VffSSHWiKWuwia. i Jram
002293
CO
CO
LOcn
©COto(n
03
COC
T|U
3»-< inr-^-. r-MU
J -•
01 0
<r—<
CQ CK:
•V
-
min c^
• •«:
o o
in in
03 CO
•<r •rc^c-j•
TT
-Q
G)
1.1-1 i.na. a
,
00O-l •
ID<S>-C
^
VI
CO•s*3-0-^Y>rf-(SCC)
0•®
CM
o-ir\--
<r«—I-
-J<xC
J<r <rd
o
OCr&
1. '
®
-
S
J ^in
• <N
0
fc
CJ
Ct:
LJ ---
»-40- —
^C
I f-
& CO
<S>
•- <"<« in
•-
1 M
10
^ M
W
«:
"• l£> "--
<n r^. t
•^ LJ0
Q+
Q
IJ-I CJ LU
t-U-
£r: co o-i
• z:a
c& in o
3C
t; •• LL-
I LU
U-l
t- ©
Cxl <Xi Q<
->--» LU
Q
(0U
J
•• 0.
LD U
-iQ
_
ET
CD in
tn *-< ^> cs c^ 4c
mco
vi in
"o
w w "
" Q- »—
CC \
U
J " 3^
E: T
f ^J
1/1 UJ T3-
_
C^
CL
. 0 t—
lJ->
0 S
2^
2:
int- <r <r o
o w
£: 0
1^
0 0
co^d
tn-j0^4
r-(M-
©in
CO
UJ
LU
^»
LJJ
or
CS)-CS3
s-
inCOin
<f>.CO
COCO
r"«3>
®CO
^-P<sCO10
002294
"IB?™<u^^^ AND .^ASS CALIBRATIONDecafluorotriphenylphosphine (DFTPP)
^lUJL——^- ConrracTor C^:,5.:.;^ ; r, ...::l - . Comr.ct ,\'o.
lO^^tJL Date ___^4JJf ^^T^^r^^
UL' !C Pit-y^LL^L- 0313 Release Authorized 8y: , ^ ^ ^
m.e fC^ ABU^DA\C£ CRITERIA ^RELATIVE ABUNDANCE
51
6S
69
70
127———————
197
1 5 3
isg
275
365
441
442
443
30.0 - 60.O^ o* masi 198
less :"a-i 2.0°; o^ mass 69
nzsss c5 ^ta:,^^ a^u^nance
less i^a^ 2-0^ o' mass 69
40,0 • 60,0°;i of mass 198
'eis •^a" ^O^ of mass 193
base sea-., ICO^a ra . 5 :11 ,0 aDu-"cj-c&
5.0 - 5.^ ' - o* mass 1 ?S
10.C: - 3; ;": c' r"3->s 1 S 3
;-e.i:e' :,~^" I.CO'- -J mass 1 9 3
c-ess" ' . c-: 'ess "-i;n mass 443
S-ea-e- ^^-' 40 0\ -.' ,'nass T G 3
1 7 - 0 - 23 :'; o- n-,3'-.-. 442
%. 3
0 ^5'^/.^0 ^ )'
^-7. 30
[Oi-i
f c . S t1 ^ . ?
1 . ? ^(,.fc I
^ ^ . 'a'.'?'! C'-^^
t'3'
00
\0
m00
Va:'L,e in c3'e~"'es s is ~~. ^ay 653Vd'Je in pa'i'-f-es s .s •'; -n.iss 442.
THIS PSRFO.^'. 'A'.C^ ~J'J£ APP,;£S TO THE FOLLO.'.I^GSA-.'PLES. e^.'..<3 A- .^ srA-;c.--=os.
SAMPLE ID
^p^ 5v/ 3T^pJ^^. ^ -3
f f/1-,^- „ . .
---
^^
rtn""—-'——to1-"—-"" i - - - i i - iiii
B,-., „.„. -1 ^Y^^ V
LAB 10
^ ^4AS-^4t•> \.' .Trt^ ^L/^^^Ji^^?
.„ - , „ „ „ ,
i
DATE OF A N A L Y S I S
^bsly'r ~/ / / • • • •
I • - •
Tl.Mt OF A N A L Y S I S
/ ^ ' •L61
^../S"/^. . , .
/7^.9
Bwittfitnncwe""—.—---
002295
%^^
w-
Ut
s,fl
^t ^
-ft.
0 0
1 CD
^1
PJ
00
00
00
00
00
PJ —
PJ
—
—
0 C
J U
t '•-
—i-*
•s
J yi
>-*
!t
00
00
0
FJ —
PJ
— —
£J o
- ^ u
LJ
>- >
-. PJ
0'-
— i--
.fl
«fl
^ A
PJ
PJ
U1
A ^ ^
.& U
.&
.p.
A P
J 0-
CJ m
—
CJ •
•Jl
00
00
00
00
00
-&03 ^
1>
PJ —
-~J y
i &•
• -0
03
s0 r
'..| —
—
"0
— yi
o o
c0
0 -
^ U
M0
CD
m C
J PJ
u"J
i m
PJ
—u
o u
i •&
y—
-fr 0
PJ
-^
J?a
.& U
CJ
•-••
•sJ C
J1
00
00
00
»—• o
>-*
-0 -
0 -
^CD
i>
-^
00
0
PJ —
M
U —
0
1-t
!—
.
l> C
O ^
tul 0
^1
CJ U
RJ
CJ P
J <1
-& C
J 0-
00
00
00
0 —
CJ
-£) ^
<t
^3 S
i CO
00
0
»— »
-* .&
1- ^
FJ
1
- C
JCO
PJ
CJPJ
PJ
—
^ U 0 0 0 •— •c 0 0 PJ PJ »-t y. m PJ • 0 0 i—t PJ 0 0 h— cn r* 0 ^
'P^J
B1
PJ P
J pJ
r»
J fJ
^0 C
O ^
LJ
E-J
00
00
00
00
00
ru
v—• ^
^ •-
' ost
LI
LJ >
- *a
'"
CJI
1—
' 0
PJ o
cr- o
o-&>
•Jl ^ "
>—
03 0
^ L
J 0
^
^CD
CJ
'sf0
E>-
C'
'0 -
^I>
PJ
CD M
Li
PJ P
J F-J
PJ
PJ'sl
' s
f 0
[> L
f •C*
LJ
IJI
00
00
00
00
00
IU 0
~ CJ -
0
CJ
P
J -a
CO C
J 0
-&
0
0-0
00
iU -
0 U
<-
—•
»-*
m ^
* 0
»~*
^ U
PJ
h-
0 '
O e
-n 0
-^4
CO P
J CO
CJ '.I
^ 0
. ^
^*
^1
0-
00
00
00
CD 0
-&
'O C
O<] 0
03
00
0
•s3 •
—
tJi
'sf 0
i>
^t
A0
^f 0
0" U
T C-
PJ P
J FU
m (J
I mCO 0
(Jl
00
00
00 CJ
PJ U
l ^
ro -
%i
CO ^t
—
0 0
U
PJ U
I ^
0- O 0 fJ
»- -
C* 0
3)
CJ c
n0 0
CO
ff >~* 0 0 0 CJ ^ 'sJ <1 -C» U CJ i-* ^ A PJ -! 0 0 0 »-* PJ •sf
0 f—t
c-n i- 0 0"
ffll
00
00
(
en0
00
00
0
»-*
PJ ^
•~1
0^ 0
^>
<1
-^
•--
0-0
u -a
—f"
A
Cr
-
>-t
PJ -
fc. -
l
ru >
- •—
-> 0
PJ P
J PJ
-& -
F* f
JU
' -?*
'sl
00
00
00
0 ^
LJ
CU L
J ^
<l
—
-&
00
0
—
CG C
J0
U <
1
0 F
J^J o
mJS
. CO
0-
ft 4
0 0
.&
—
0 0
0 0
•-* P
J
— C
J)0
CO
0 0
- f
J^
-J ru
0 -
s[J U
1
PJ P
JfJ
PJ
Ul
+1
0 0
0 0
PJ <
1
E> ^t
- 0
0 -
CJ -
Q ^
PJ C
D-
0^
-si
B <J -0 0 0 CJ 0 0 0 .£* C- u CJ PJ PJ PJ £J 0 0 >-• 0 PJ 0 »-* r'J CG Ul«
0
<!<
;<[
CO L
J FJ
00
00
00
D U
T -t
UT •
sJ >
"<i
rJ
—
00
0
— m u
M A
0 ^
<S
-0 &
- PJ
PJ F
U rJ
PJ •
" •—
*^
',4 K
—
00
00
00
Ch
-& P
J
\t C
D CJ
Ul 0
CJ
00
0
SJ
U7 rJ
^ 0
"4
U1
-P*
—Ch 0
-0
PJ ^
^
« 0 >-•• 0 0 0 0 0 1—
t
CQ E.J tU 0 ''J 0 0 iU ^ 01 0 GJ 1—-
PJ fJ •3
fiffll
0 C
D £0
o c
n u
00
00
00
- '0
-£?
P-J £
> U1
00
0
LJ —
^
-0 C
O PJ
CJ 0
•-
PJ P
J PJ
00
00-
(Jl
-^
00
00
00
!—»
ED -
& P
J
1J1
0s &
-i—
;>
'-•
PJ 0
0
•-l
Ul
CJ—
CJ 0
»—•
U1 U
PJ
-C-,
03 —
0 L
O ^
» CO PJ 0 0 PJ h— 0 -& ^ 0 t-t
PJ 0 u 0 0 >-t 0 0 0 >— PJ m iJI
asei
SBSS
vs
sa
sC
OC
D^
Sl^
'sl'
^-^
O'C
-O'-
tJIi
JlU
I—
O'a
CO
-JO
CJ
I^.^
lUlE
J-^
iOF
'J
00
00
00
00
00
00
00
00
00
00
00
00
00
00
•s)
•vJ
•^
0 •
s)
•
03^
CJ
LJ
-P
-O
CJ
-O
i^—
^P
J^
—L
I
Cr
-M
-^
^O
O-
O—
(J
T^
—'^
CO
-^CJ
yi 0
0 "
-f 0
(J1
0 -
& -
* U
I PJ ^
LJ
00
00
03
0—
00
00
00
0
yfD
UtJ
IOU
—U
lCJ
—
PJE
JIP
JCJ
LJ
^^
^O
.frL
JS
)0
0"U
l->
PJ
-a
UT
0s
U r
J P
J CJ
CO
PJ C
O *>
^1
— —
CJ
—
PJC
T^a3
<iC
J[.J
^nJpJr
o'—
'sis
omcn
d 0
CJ -
0 0
ED
-fa -
& ^
s0
CJ ^
Ui
o^o
-^-o
-a-a
mco
cae
ocD
^^^
—
•-O C
O E>
U
PJ
-s;
Ch 0
1 >- 0
-0 ^
UT
00
00
00
00
00
00
00
00
00
00
00
00
00
00
>~*
0
-O
O^
OL
JO
—
CJ
—
—
—rU
iCJ
—
—
'OC
OO
'0-0
—O
PJ
UtF
OC
JU
lOU
lo
—o
iu-^
'-^
uio
m—
oc
oo
-o
00
-0
00
0—
00
00
00
^-*
'sl*
»-&
'--—
'L}R
J'-
*'~
*PJ
-b—
*——
coo
ul—
uu
icn
a-^
ci^—
— c
o
COU
t LJ 0
PJ
'O
—
—
—
PJ
—m
Cr-
fJ P
J --
t <1
E.J
I CJ
PJ
0 -
0 -
0 03
CJ
o -^
f o o
ro '
•i A
Ni •^
— —
CG u
PJ
«ffla
UI
U'
CJ— 0
-^
00
00
00
•^
•s)
•0
m —
1> C
J LJ
PJ C
O 0
y P
J CD
1> -
0
A U
I ^*
— en
PJ
.fr
—&-
—
£Jca
01 o
00
0
O1 &-
0-
-^ C
O ^
00
00
00
0 t
U A
-0
••0
Ul
<] 0
CO
00
0
— C
J U
I—
A
PJ
M C
JED
-^
CDn.i
'o —
attsra ff
iu CO 0 0•^
»-*
0 »-* 0 1-* PJ CD ?•»
E^ h- 0 0 t-^ >-* yi 0 —
CJ -0 17'
rcB
uwan
MW
fi
BQ
flB
SB
3 QJ
j.
(A
A C
JW
Ji. U
.
p33
0>
0
^0
75 -.
oC
l 0
*- f
t3 .'1
-(0 3
00
:? 3
Oi
»^-
x
3(->
. i
.3 3
OJ
Ell3 QS 01 i/'
3:
i-
3 1^-
3^
^- rc
33
3> ^ S3 w
vt
0
p
•—<
3 •-t-
It 3
sa^i
BS
9
rfl
at o
U1 3
U1
C3.
^» Ifl
1 ••
fl: C
Jc.n 0
-& z
"•;0
X t
3—
(
- rJ
l0 o
"n en 0 0 A:
U U CO ^t—
•"• PJ Ul
• ^> CJ 0 0 r? CD -n »-< z H 0 ^-* 0 3> r i~* en A • PJ ^> 's.
CO <J1
BSil
SBBB
OJ 3 •a ^i m En'
<i
T? •
m ;C i
-n • (
en c
-( a Eh •
!^ - t
-1-C
.0 f -0 m
c33
0-TT
^ ^ -< I
^- '--
<'N
f
P • c- p f i:
00
56
85
002296
MID mSS SPECTRUM - • • - , . ,. .^P4.-'28.'&5 11:45:0» + 3 :14 < • • - < ' _-.- . - . ,SAMPLE; SU FERF STD <763-40-r-FF.F>
OATR; F5042335A1 S554CALI: F'S042^3A1 t?2
Cn^OS.: 30M DP-5 FSCC <S33&n/ 2?.--4-30C@3 FimOl CftLIB 4/24/85GC TEr'F: 2Pb DFG-. C^^l - s^ ;••;£, 00
EH^E n/'S: 13;?RIC: 72350.
109.Q^
50.0-
ri-?1Q?,@ -i
"
-
sa a ~w'"' • '-'
,
T*-
^1
„ , , 0 n 5 6 R ^
f00J. —•u
^9
^l
"
'
tq ?? f. . „-,„..' ,;L^«' I.;.
4422?5
i25^
sa
-^f •-'
[, 2S5 .' ' '\ < r^
^ . . - ^——^-^.••"l". ji».i.t.r.^.t>)-*Jf.,J,t.,
109
'>-e-e
'-ih i ' '"r-'
h i
no
93 |( • f -'.. ! « •
qeL . -3 ^ . 3.
["• -r—!——'——T-'7-
3??
if
l-V1 ^•'11 (
;
II?
^ i'" t " • < f f
REVIEWED
APR2 '-1985/^•/z
GSRf
•'.^. -
-:-^ 490
E 20?ISb ;
t'?^ ^0 !?I (, I79 , !iLj— . ^—^J^- . .—tJ.Li *4*^J^—f.ll,,. f>yLL..i.i M. i—,. ^ >.f.L. ^-^- ^n
130 200
334 ^5 -:.}?—[—^—;—i—]-—,—,—,—,———.-—r—^— ,-.-,-t
-ti
420 ifi • ( ' r
22L , J I .
-
-
450
4
( 23b !
i—J
002297
002298
U1 yi
-h ^
A
.&
A U
U U
FJ
fJ M
PJ
fJ -
>-
^- "
0 0
'^
0 0
'0
-0
0 -
0 -0
CD
fB C
O CO
ED
^1 ^ ^
---i
-^ ^ 0
l>
C-
0- ^
(Jt
Ul
U1 yi
LJ0
(Jl ^
CO
^J P
.) ^-
'.1
U
l 0
-0
03
^J U
M C
O '-l - 0
L.)
-^ '
. A
— .0
CD
U M -
1"-
L.
'') -
0 -
G m
~J
Ct-
CJ'
. ~C
m
CJ
i 0
n-) -
0 -
0
3
gg
gg
gg
gg
gg
gg
gg
Sg
gs
'Sg
SS
^g?
§§
? §
§§
8 §
§§
§§
§§
§§
§§
§§
§§
,§§
SS
gJ
J -'J
•J
•s)
-\>
v "
J \>
pJ
yi
u"
' '
^e
o m
-*M -' 0
M 1^
)"* P
J ^-
»-•
P.I
M •
& C
- 1^
^" "
-0
V O
- rij
IT-
— "•
PJ ^
C*
t.n
»"
--• •"
*--
—
A U
U -
t» 0
U -
<1 ''.n
"• ^ -
' PJ
**
'"* C
J? U
' PJ
U
>'
0
O^
^^
^O
O^
J1
CD
^P
J^
^A
OO
O^
<l^
Un
JU
I^
^O
CT
OO
Jf
'JU
•^
<1
0•
t>C
30
V''
00
-&
^-
•U
PJ
^O
^•
C:*
0•
0-
0 33
0^-
fJ 0
0 U
---1
0'
C* 0
'
'0 ^
0-
i,^ 0
••si 0
0 • . 0
a
iJ
£.
i-U 0
'^
'-
£•
•-J
C"
r" -
b L
J -?-
-0
-<3
-^
U
l -t
.&
•—
—
U
CJ 0
'0
• 0
-to ^
>
0
^0
00
00
00
00
0 P
JO
O-
OO
O-
'O.&
O—
00
00
00
00
OO
OO
OO
O's
iO
—O
^O
OO
OO
OO
O^
O
0P
J^
^^
y^
^^
pJ
^p
^^
tJ
^^
^^
~^
O^
^t'J
CD
^^
^J
U'^
C^
^^
^^
•-U
'U(J
^C
DA
^-
ly
'^--
t^
^^
•P
JU
'PJ
Cj'
^t&
-ft•
•-(
0U
[>>
--•^
4(^
r'^
U'^
'-"-
C>
C'O
CT
i>•"
(',
'l—
•s|(
Ji-
^A
.£*C
,P'O
Ul^
"LP
E'J
U'-
£>
^0
' c
.i-2
'<3
(J'-
^0
^-^
I(J
ir>
Ji-
PU
l'J
'0'O
Cn
'JlU
1
0
0
PJ
E^
'-
^A
—
•^
•^
<1
^t^
^^
^^
^^
^^
^^
^^
^^
^^
ow
p^
^^
^^
^w
^^
^^
^^
^^
i^u
^-s
-^
^^
^^
^^
^^
u'^
-^
-f*
^J
C^
O^
E^
nJ
U^
"A
LJ
O^
C^
^P
J^
J^
O^
U^
&^
<I^
^(>
C-^
C^
^^
C^
O^
^<
JU
^&
•0
('J
^^
l\i(
J^
UlU
^O
<i•
P>
'^4
y'
03 w
'0
U U
<~
& C
Jl ^-
&-
PJ i
-f ni
••n A
PJ r
i <i 0
U 0
- 0
^J
0
••) C
lOC
OC
'Uc
Jl
^O
Cn
Cr
-i>
OC
JO
LJ
Cn
'>^
LJ
'4U
-&
CD
O^
^A
^^
AlJ
U0
^1
^^
JlP
J^
;^J
^J
^^
ry
^^
lPJ
PJ
^'J
PJ
l('J
PJ
t'J
PJ
PJ
P^
(\J
^J
•-••-^
•^
^•-"'-
^-
t^
-•--•-
fc-"-^
•-"^
•-
t
A^
fc
^f>
J^
O^
^^
^^
^^
^^
^C
JA
A^
PJ
PJ
^J
^P
J^
^O
OO
O^
<l^
^<
3C
Oe
aC
nC
DE
XlC
D'^
'^I^
E>
E>
(>
(>
AL
J^
J^
UP
J^
U£
^^
C^
U•
AU
CT
C^
•^
J1
C^
^^
^^
^^
"^
^^
C^
^A
<1
03
&•
UP
J0
3^
&'•
^^
O^
OU
^•
C*
C3
^C
^'-
A
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oo
oO
OO
OO
OQ
OO
OO
OO
CO
OO
OO
OO
OO
O0
00
00
00
00
00
00
00
00
00
00
00
00
.&
^-
CJ
-'
^-
'O
'-
1
3M
^a
lC"C
^^
JO
PJ
^^
^P
J^
PJ
"[l
JU
'y^
^^
m"4
»fU
OC
^(^
PJ
PJ
'0•fc
>^
l-^
0•&
>--•-O
CJ
PJ
•-•^
•-P
JC
J^
-l•-
t•^
•&
0>
--
^
^
0ft'
>^
M^
^C
^<
l^
l^
U^
^('J
-a
A^
^O
^^
'J'^
U'^
<!^
^^
'^^
^C
DO
OO
^^
<lP
J^
^C
Jr\l^
^^
CJ
ES
-O
U
3t
3
r"U
O^
LJ
O^<
l^^
J^
(>
<IP
JA
lJlU
•-C
^&
r^
PJ
O^
PJ
U^
^J
^P
JO
^^
J^
J^
^O
^^
U^
^O
UO
'•^
<lr
^'^
•^
•-*
-f
:*
•O
C^
• >
••
•-*
3)CT
i-* n
—
s^
•c»O
OU
'0
00
00
00
0"
OO
OO
UO
OO
OO
O>
-O
OO
OM
00
0-
00
00
0—
00
00
00
00
00
\.
.,
..
, .
. .
. .
. .
. ,
. ,
..
. .
. .
- -
X
—
PJ^
^P
J^
CJ
^[U
^^
^^
i^U
^f
tJ
£^
<i^
^^
^^
^P
J^
^^
PJ
U^
U'L
)^
PJ
^^
"^
L.)L
J"•
t--P
JC
J•
rf•
)-
t-C
*U
^'r
f•'-
t•
-^
0
•£*
UP
J^
I>
O^
Ul^
^^
C3
^U
^C
^^
A^
^^
^"
<l^
^C
3^
^^
"rJ
^U
^U
CJ
^C
r'C
>a
3'^
t>
0-C
Di.J
eD
Ai-*
U1
0
0
's CO Ul
>-*
h-»
^iJI
»-*
CJ
1—
PJ
-l
--
3
PJ"^
PJ
^O
^P
J•-^
^^
lJ
<lU
"F
lJf>
^^
^^
^U
tPJ
PJ
^(J
tPJ
C^
^^
UC
OU
•ts
•^
••--
(-•l.
l)^
J^
••-
t^
)C
J^
••--•-P
*U
1•-
A^
- ^
0^
LJ
^C
hO
^U
l^
^fr
mc
J'U
O^
Cr
-l^
CQ
^U
^^
^^
^^
SU
^^
^P
JO
^^
lJ
U^
C^
^^
^O
-U
'^
CJ
^y
^^
m
CD P
-J PJ ^
PJ
!\1 •- 0
Ul
.0 C
r- T
l •
t^)
PJ 0
0 (
f -0
PJ ^
U1 f
J 01
•?
• CJ
<!
••^
PJ
Ul
O--
— 0
•-G
LJ
1-- E
^J CJ
CO
-^ '0 0
<!
CD 0
C 0
M •L
.n 3
00
56
88
002299
sas ssc ws was
MID MASS04/2S/85SAMPLE:CONDS.:GC TEMP:
^50;=- T,1
100.9-1
-
^.0-
M^1P?.^ "i
J, REVIEWED
'30.0-
*?9
^
39< »• '
•5@
275|i,L 28'-, .^L ^^-
57..i .r . ,
-»qc••. — 31'
SBS
SPECTR2:2?:
SU PEPF30M DB-20? nrtt^h •?
( 'tt
h
liy !
81It);..-.
SBS ffiSB ^BXT B^S VSSS SBBS OH 001 fl
J^ / ^ ,/ / 7 CIMTA: SJFi?429e?Al tt"Pti?. + 5: 1^ ' "l" :Mll: • .iF'. : ;1? ! S:-
STD <?i:.?.-4P(-PERF •? FSCC -.»:::;,'-;; 1 ' :^'4-'^fi^ FIW'l C^LIc 4•;•4'8C'.Q. L.t^FD - a^^^ "1 .0^
^'^
1
.93 ; ;
ii i •. . it t.... 1 1 •• - t •
l6o
334 u
!.',
1 1 " '1
W ;'
»
^ ^t^ J.t4 4-'-^ ' f1-^—^——^—»—,-— „..-..-,.. ,. „„ ,., .. ———.-A.——,——.——-*ttk,——-
28^iee
1^ [4? -c,i . 17-3iti . " ,, .1 . . . . ' • • - . ...i-. it. iit,, -„ f
MAY ; - m^
6sm
•i .i,,
442
i
Btt OM
35 BASEPIC:
224 ^
. 1 . 1 1 .
4i?6
—— BOB ffW UOS
M/-2: 19810112i?.
r- 11368.
255
»a
r •; i^, t25e
4§6
•
:
r 113^?.
0 0 5 6 8 9002300
06
9S
OO
i-' •»<*»,'.
^:
M0•
^ .
s
o ST
^~.«—
— .«
!< & 5 J^gs \ re 1
°i,oi ^
' , '\
w o i '-> J
< .C
c
'/»
OB
^ a
: >-
2Q ? : <
IZ
C-
v
- °
ffi -c
<~-
<* ••
-c
•
S•i o. .j
<^
•^
—
e*
•y
fc- ^
£S
-
^
3y 0
3
<*
-
t- "I
CC3 03
»- »•
0
"B
r»
0
^ -\1-032•»0£.
'a<e*<»J?«*(TS
<
3
£»-
^Jft0^>-€0n
»
3
E UJ
1-t•r<0301<«fti
Uf
e:
V
(Cu«u<J-•'<0.--^ca<£o
0tT>
^
}•OOt^<•
'54i--00O
f
081
*--»en«s—
/
<3^
^
s-4
?0*-0f4r—<-•5
0v
^^«•
u(:1'«»1»
11w*J>——
••
01•4J1S
^~»'J<
S«•
?0•wpCMr—r»»0IF*.
'?-•\
<»
iok«A••--it«•"1'O•*
0y00•V^~r«
0
;
^/"v«
^--flOAwk
W100C"1<«r••ft)
r~tf*
N>
0
*-€.
?3ai»•»•*•
0<•>•>*-USfJJ
«t
(ft
^tA^
•r •
•Vfc0L>
CT'
0Wl
0o*
r.^w•n*rn< >
< »<-»
«-»0*n»-CM
rnr^<*>ir'«*«»•»(<•*
0rM1*•^«1t»
m•O«-»
0r-^.i•»-sI*"•f
•<»
^*>tfl1••
—
h•—•9-9
^^-
„„01m"if*'
<J0'»1«ii*•t«?*,
IN]
•«•»
«1^<T^
0-
r,
\?^*
^r^•t•€"it:0i »
nrs0r^n•»•a
-—
- -
002301
a"9gmpCond
1"1 "
3^
It'O
5152
|63
1 65606^74
1;:7 7
1 '°"'
1:1 I".
1°'-•b •C'r;'- 0 0 P •
I1?:'::'tf'l
• '1 "vi .. ,
1 0 '
1 i t-I 1 1
<* 1 7
1 9K'-I
1 2 7
IZO^9
130g!35|37.^t41
fc142ft 4 7il48
1 5 5
I5£.59
• i» •* » i9/85It S\% 3C6 - tt"
36444a&ti
oo-?00?00^00-00"00--00--0000-OC-0.0.,'c<00C.r.-occ":*00r-o'.cc"'0'.0-
O'"c'c0<c<o//~",
00 1 ^ ^.Or0;00c^-0(-00OC 56 3/-000000000000OC0000000000
- 1 » *.
7 27 00 •»^ PERF STC3M DB-5 PSS>5C X I 00
0 00
•/. RA
3 291 1 0253 0?2 ©21 *»04 2J2 241 3-?1 09
77 7<-4 0:9 1 ^
6t 0''4 74; 1 ^< ??';4 L"1 1 ^1 ? /C ,.}-': ^lC '';
c 47
-? 4''• o "-
? 3 '1 i I: 1 ^
^ ^ I-'c 3:
4 a^e 3:0 941 ?.'''
4 0'-51 1 5
1 741 441 I?2 060 921 032 211 1 1i ei0 9R
f 9) (7>CC
0
%
01600000090107001"'0C'0CC000('•
000C104000060-1
000' 24000000
1663-4(<«33E
00
RIC
39382\33??50^f.161 31 35607^n> 75-33-t4c,.
1 31'-.; fi 11 Z10i,.a4i47
^; ^
1 3Cl-.>-f -
311 ^57931 0t c
6C434S
^01 7< '",
1 1IF?&I 3i«
1 1
UC
3-PE371 >
HIn
16
9(J
1f
ei-•«
6^043750030111
19903e?£?
4'30 46 1 4
I04Q1«i
70ftC5 1 4
2660?191!2591130 423378 44112^71^3
JItJ
«] 1RF »
25/
0 10 ^
t(?n
4 1 440;.67..35523^53.'20.:1 7 0137&oe&04
15^38156059&39^36:&3E4:7'.0^-1 4.'a0^^ '
3944
066?
8144
16
39
P50429cPS0429Ec^^4-300<?E:
Himma^rf i IfflJ
M
1 6 11616C1 7 41 7 517^1 8 CieiIBS18^1 0 -\^t19:19i.19^19'-20420"WL20 •-n i^^22 i1-^-1I. C- „
2^422?-,- -,C C- '
^2'?24^.24 S241i-^-IC ie- ^ i»
25C26l:.273?7427527^.^7r29..3?3334365:?72
44?442
^Bl N5B1 «
^//7riN
M
d ^ T
0000000000000000000000r>r"><'•0-:'0." ' , "
^~-y.r.r
( ~
€•:J 'f...•- .(K-000'''Orr. -
/" --
.
OC•X'''-r.OC0--'00^0^J";-0''/000-,/• ,'-/ -.
000-"c^000^00
&56 Ba2 RI
>
N01 CAL1B
in iriten
•/. RA
1 124 583 280 99I 613 042 131 301 51
1 1 773 461 001 013 56
100 006 56,2 634 4 ^
\ff 212 371 '905 O6.6 631 2b9 6^2 433 5B 0 4:0 677 751 031 1 7
3^ 1 15 1 91 7? . ...1 Oc n ir>1 03? 74
Ifo 70? 1 61 303 8I 561 061 730 835 433 70
45 107 9?
S(?
C
4/
7.
00000000010000
1 100C?0000010
0000400
00100000C0G050
m / 11
24, 9
103
RIC
. 1 3543Cir1 ^3-.2T1 ^ie3&4 1irit4,:7177315"21
23•T-t-C
5";7f;1 11 3?!?
1 C9]IP1 41 361?!
J Ek
12329 .251 544181230102067?fi9-1
19607392
5
Inten
1 4 15764 1 312s20 Z36^26816J190
148C4.;'1;^\i '44,
12^-8^33.55-
24:(.30 '—/ •T .
23'-k —'
63'-8.'^-lt;
12l i30'";-4^,':ic^97"12-1 4 -
4 4 1 1Jl,®!'-0^ -
cli- =.
12'-13.:^atLu~ -•
2!OC-,-.-e- f-
l&d
47o19<!;13^f HJ -J
^ 1 P& J LJ
105105*J\y ^/
71'7
5672100^;
002302
HID MASS SPECTPLIM w^: ps^^ei ft?^C^l-I: ^S^-t:?^^! ft 204-'2S--85 7:27:^0 + 9::i=; ,. <" < ^- / / '7
SAMPLE: SU PEPF ^TD <7^?:;-49-=•EF)r •OMtS.: 3011 D^-^ F?CC •^~.^l' :•c-4-?^l?9 FI^^i •' UF. 4-:4.-::;5G'' TEMP: 2(?e DEr,. i.ft^^ - ft?^.'1 v: .^^
BASE tl/Z; 19&PIC: l07'?92.
J34 34^. ^•c
—'^——r" —~r*~ •f"' "T———r— - -»*-~
^i't^
5 6 9 2
002303
VJ\.^ m i iwnirmi ^rBL? f»A9^ ^AUbKATION
D«caf!uorotriphenylphosphine (DFTPP)Case No. .M I i r—————— Contractor Gulf ^ourJL- ^Lir tL-Iu^L^ Contract No. 68-^1-^^^ j"
r- / ir I l 'Instrument ID r M.A. (| 1 Date ^L'2"? (:-Y.Time -iL-LAl
Lab ID P^-^-Z^r^J- Daia Release Authorized By;
m/e l0\ ABUNDANCE CRITERIA
I 511 68
69
70
1 2 7
197
198
199
275
365
441
442
443
1 w - , . - : —
300 - 600% of mass 198
less lhan 2.OS of mass 69
mass 69 relative abundance
less "ban 2.0''; of mass 69
40.0 - 600°° of mass 198
(ess -ban I.O0; of mass 198
base sea",. lOO'a reial.ve abundance
5.0 9.0^ of mass 198
10 C 300- of mass 198
Q'-ea'er lha- 1 00's of mass 198
Drese-'t, bu*. 'ess than mass 443
great?' lhar- 4; O'u of mass 198
17.0 - 230^ o' mass 442
•w, , *-i-i-y/i • L. r^U^ill-IJAI1! Li f,
^<-.^.
i .J. C/&7)1
—}<•) ?-
c- ( ... )'S^.-7
L.
' C C-
^ / (c ^
"? \- '
/— c, ^'- / •*
U -. !'-' '*
7 i-. ('^-)2
^Value in pare-:nes s is % mass 442.
THIS PERFORMANCE TUNE APPLIES TO THE FOLLOWINGSAMPLES, BLANKS AND S^'-DARDS.
002304
1 7 69
S 0 0
di — fn rj " o- <i •'
\.r ;•* r
^ i., i.' --. ./ ,.
, •• .,• i ,• .... •., (>• .-, : . .-i ,- .. — r
^. ;_: , < , , ^. ^ ^
' T-) o n
"•' ('. CO 0 c in^
10 ^i 1.1 in ;\ r- t"i u"i in n ro ur- !J ^ '3- o
m •n .n •o 1-.' o
r^ 4.1 in -o •:J iii co -o q •r <i '-i -o 'J- o
in o u"i '0 r.i n
r"j o in
<-<<-' i- 1-1
'--< o'- t\) '— —* r' —' '-' '"J
^i ^- --i (i~i if ciJ
.-i i .-,
, ,
_ T-i fi) ^- n
n
-
_
o <y CJ ro T r.. C-L' -,J -•.) u--. i-;) -.J 03 r'; ;"J ru <;' in '-J ^
CD n o
i-'' ^ u"- :'-
J — T r^ ^ o i.-. ~. r. ^i co .n a
L'') L^ o o
r^ c- yi^
^^
^rJ
^r^
^r^
^^
no
^r^
^r^
r^^
Ln
N^
^n
^o
^^
c^
'orJ
^^
nc
or^
^^
Jr^
^rti^
^n
^ic
sQ
J'-^
do
oo
oo
'-o
oo
o^
oo
o r^ o
oo
oo
—o
o—
oo
no
oc
'oo
-*
oo
oo
o6
o6
oo
<ro
o«—'
"' GS r'u o (o OJ in &•• 0.1 i"i t.r o
EJ.I — "- -o 'T ^ ^ '.c' o
^ <?• p' ^ n
n o- in 03 — ni _ (-J ^- ^-J ^
.
^ p^ 03 ,y >s. rv (
03f^ ru co if; rj a-- o- ^
•q n <r o
o o
r-- o
n r^ o
-.0 fiJ r^ rJ o c^ u'' r'- IT! — in rii t)'-. r. GO u^ o' u"i n
\n n n
<?• 17- in '3 n•- •-' n
rii '- '-• •- n —• •— r^ o
i\ n
o I'd -^ T r'-. — o
r>J *.?' o- — — in ^
ri T-i — n s0 rd —
q- rii —' ru — --< n
irt r') ^ —
*-* o
rii
-^ n
•—
IT•—<
'Ji
0 0
0 0
0 0
0 0
0 0
0 •:.•
0 0
0 •^
';' C
C' 0 0
0 0
0 0
0 0
0 0
0 0
0 ;- 0
0 0
0 0
0 0
C 0
0 0
0 0
00
00
00
00
0 C
CO
QO
C'O
OO
OO 0
00
00
00
00
00
00
00
00
00
00
00
00
00
0
IT) r-^ o' o 1- ITJ -o ^. FJ n
o '-."i o y- u^ --':•-' o
r- -' n T u"i f^- <r u~i -o L'-J o
c-i u^ n o- ir. •<) r^ •o n
*y tT) rJ " n
"• r^ ri «T1 s' ]
r^ co CO 03 03 o 0
s o 1- i> 0' o o
o o
c; — •" rij (\J ru riJ r^ <r T
r ^ ifi m
o i-s
fs r^ r. o rn n
-43 ^ fij CM "a- <r '4- •a--^ _-, _,
, _^ ^
, -^ i ^
^ „
r^ ^ i-u ^
(-J j-y ru fd rJ nJ fij rJ ^1 rii ro ru (\i rd .J ry r^ rii rd n o
n o
<t ca- <• «T <r '«3'
0 [^
0 '0
>-''' 0
C-- ^
FJ (;) t--. I.] y"/
P'J G* -' 0
~< 0
T-- Q
U —
' <s i.''
0 •^
tJ tTi U
rj "- C-
0 FJ •?•
-" n 0^
CO 0 '-' CT
T T
03 (\ 1
oM
ory
—^
lOu
^^
^^
'^o
^—
os
^^
^^
^^
^^
ao
^^
J^
'^o
^^
r^D
'mL
So
r^-a
o'o
o'-o
as
in'o
rij ^ »- fiJ
i —i fij t* —
r" rM — —' ^
riJ — " —«
-o — in rJ ri r^ "* GO —i
'—rti
r'J cu
"
(•>J
— "- CD n '."ii i> -d •-3 u-
-u i L'i •'•- ::} r. i-,i r- c n
n
[^ i-d •i i"J L- -<) ;-', I-J cu -J -^ <r ^
--3 — •n ^ FJ o^ ca ^
^- ai i -<i '
~i n ru o
n — — r^- in —' ri b"i ir; T I"J ^'.i — I'J —' r.J —i — r^ s- u^ i"ij •" ^
;'') ru IT] t> -^ •' n
iri t rij r^ —• r^ --< rii '- CIJ -^ -<
•o
oo
oo
oo
ro
o-
o^
c oo
o o
oo
oo
oo
o o
oo
^o
^-o
oo
o-o
o fi] oo
oo
oo
oo
oo
['.J v -' ?•• ,-•• J c3 [.'J ''k, t" -.- .-' u'i ,- •„•
'J --< a L.'. .-3 o
c
•' ••J i'J -in-- r.' c' N
<i ;") ^ ^
ri. -< L 1- ij — ". n '.'J ^
'- sQ -ofij n
.o <- cc r^ tr fu n •a- <3- ii'i --' u-i o" J'. ir- r'- r'j ^
fu fii u; y- ' s' <, <r <i G! r^ c' ^ 'ii ^- in --':i — - r' &• f^ in 10 <3- o
•" <r if)r'J n
ru in I'J — '- o- ifi c- c") I.J iri r-t fiJ •i .-,--, ^ — — o 1-3 ^- ^ .' ^. r^ 03 o
LL* -' <- r' ^- ru r>] • — r>] —' ru '-• ry —
'-'in
N
— ^J
— n
iri
fij
o c,. <-.. i. ,-•
.:•., i-o o
o o
o c. o
o o
^. ':•• '-/ -^' •;• f-. ^- c o o
o o
c' o ^
o c; c
c' o c
c o
o o
.:; o o
o o
o o
o o
o o
o o
oo
oo
oo
o o
co
o c
-o
oo
oo
oo
oo
oo
oo
oo
co
oo
oo o
oo
oo
oo
oo
oo
oo
o"' I'll <) '•'•
I'J Lf. 0 IT- '
"'"•i
..•.) '^ CO r^
^
—
CJ r", u"; '! -•'
:J C^ I0 ','-
— •-''''
•X 0
—
^- i\ 1
i r^
CJ l> C
' in N
'- ' sk
GO Li <, —
lU
in in IT) in o <! ^ <» r- ?'- r 1- r- ?^ r-s o
ro a c''i 03 GI L» ^
c- (-•" '- o
^ '-"•• o " "
— '"u r,, f\, fi; r-u n n
ri •y '<T <r yi IT' o 0
002305
r'UD mSS SPECTRUMoa.-J9/$5 1 6 : 1 1 : ? ^ + "3: 14:-WLE: PERF STO ?^-^-FW CK:.F- 4 1 1 "CCiHDS.: 30M DEi-^ FS.J" • ^ ^ 7 P ;•':• 4-^n^Gr TEMP: 2^ DF:'-,. i
±±",4 - ft^ ";.o-.?
CnSE r'l : 19SFIL,: 36Q32.
'IliNnl L^-i^ 4 ^.•^
I""!ff 1
B 59-^P 1
H -"-i^
fc ' ^sis
US ' 0 0 5 6 9
^
| M'2
E&.
1as'sj
| 5^.@-
^sH !
^" "^' - i 'g l» -':-,, .-^—
§ f'1 7 •:;t??t ''ir11'1 •^
R?
.?9 J—. -J-i—i—4
1
\
( : ; i
ff~"w'-{ ; ] 1 .-.f, f i ....
?
->c-
^9<?i'
^
!^;
i l; ' i • ' ' |
1^-J l^-'" ^r?^
REVIEWED
MAY G 2 198^/^ 4A?
r'
'?!- , :':;4 .- ^' ^^ 4:::;
i ' ' ' ' ' ' ' ' ' ! E ' i '
1!. ;
!i ; 1 '
i ! '' l0^^ i i v7 ' 1.- ,- ", , 5E T „ ;, ' l-- I-;-? 11:" 1 , 4
F f t l n . . • ^ 1 1 i . 1 1 > u ' ,. . . , t , ! * ' ; . 1 1 . i ( i i: ! [ i . i . l . i f i . If- ' ] iii i. i
——————^^———————————————
(SSRI
2CiF.
i, ,J
T 24i , > 2/:!cr
[- f . ^ ' r ' 'r'-Li-'——'1 .——1
;!
5
l ' ;
^i?4
i ' ' ''J.^^
14
i'
25^
•~i—'—
3394,
002306
""~?^w?^^^ v^m.ionM l lUMD«cafluorotriphenylphosphine (DFTPP)
Case No. „.",.' U______ Contractor Gulf .Snuch _Resear.ch._Inst. extract No. ^8-01- WG7
Instrument ID F^ ' ^ Date ^ ^______________ TL^ ^ ^0i ^ < - /•
L^b ID P^Q^ 3J ':^ '.. Data Release Authored By;
m/e y^LATTVE ABUNDANCE ION ABUNDANCE CRITERIA
51
68
69
70
127
197
198
199
275
365
441
442
443
30,0 - 60.00-. of mass 198
less than 2.0°i, of mass 69
mass 69 relative abuncance
less man 2.00;: of mass 69
400 - 60 0^ of mass '98
tess t^an }.0% of mass 198
D^se oeak, lOO^ relate abundance
5.0 - 90'- of mass 196
10.0 • 300- of mass '98
yea:er ;han 1.00°; of Tiass '98
p'sseni, bui less mar, ,'nass 443
g'eB'e' than 40.0^ of nass 198
1 7 , 0 23,0^ 0< mass 442
^.>
LZL C^1
"?v .^
0 ( ^ )'
S^^t
c1 . c
^ cc^ c?
->• :' I/
3 L^
<- • ^
^ ^ O 1 1 - ] 2
Value 'n pa'-enthes s is \ mass 69.Value 'r' parenthesis •s ^ mass 442.
THIS PERFORMANCE TUNE APPLIES TO THE FOLLOWINGSAMPLES, BLANKS ^"-D STANDARDS.
SAMPLE 10 LAB ID DATE OF ANALYSIS TIME OF A N A I V S 1 S
^ fa^ e^^t porp<.^-> ,>^^ A)or^^Brt»,/7i;^o^M v
002307
^np Iednds
<»552 to
499te ^S-S
I•JS 00''
39 00"*
141 00?44 00'"50, 00^
151 00"'5.? 00?56 00"57 00-
•£>3 00 ••65 OC'
68 00"
(^ CO7 4 0075 00
176 00'7. 007u 00^7 OC
13. 0:-.<? : 00"- 00
1 ^3 00^5 00& 00^ i or;
8^3 OCB-^ C-c
0 ^ 00
1" 1 00- -J r.o1 C £; GC
« '": 7 00| 00^ i 0 00
1 1 1 00
1; 7 00;g oo
!-*3 00§27 00g29 00129 00
^30 00|35.00137. 001 4 3 00147 00[48 00155 00^6 00
5V r£RF ST30M DB-5 F^553 Sumrn
0 00
% RA
1 264 701 3C.
S 1 3714 OZ&e ic:3 2^2 2?5 702 411 4C1 2^
S 76 154 9J9 463 02
65 4 -" 4 ;3 142 fcl4 :ic-i 5"i ^:1 141 -^! 21? 463 4',-2 e.'-1 —1C(=- C- -/
1 3^-1 4 1
15 c"-S :<4
32 9J4 639 341 1 11 65
53 934 37
20 Q71 971 771 512 161 322 571 651 91
0 <763-40SCC <tt33Sed - ft 54 5
0 00
•/. R J C
0 140 530 150 151 5S6 S30 360 250 640 ?70 170 148 73
0 5*^1 060 3^7 3"?C c. •"L
.)\.'
0 3^o 3r'C. 4?0 ; 7c isC 1 ?C' J 40 140 6.10 3^0 43o 2r/' 1 Civ/ J 3
0 161 75f} ""'/U c-l-;
3 700 5.-i /'. "•.i \.- ^0 130 1 S~\I 86 060 4Jr' 34 c0 2?0 ^00 170 240. 150 29o ia0 21
-PERF ••71) 25
X I 00
011. /"ft CInter .
12345^127134
1376568E?315•^-i,'*.c-e.^55723614'-i T:1 c.. ,-
764^4G2925301
6 4 C C4J :'")" /*J - •
27^4^."14'1"^1 I!Ic-'t;'
,! IS5341 1 1» '34./3722C.13Z13^
1 C, '~~* /*,?=.'•'T-T3t c: 'f
32^445391^109161
527241 /
204019317314821 1129251161!&-'
C^w. t///7/4-300@e F I N N O
Mi r- if[)QMa x i m a
M a s ?
161 00167 00168 00174 00375 0017" 00180 00185 00196 00187 00192 00193 00196 0019G 00199 00202 00204 OL'20^ 00206 OC207 OC21 1 OC'">*'' ."Vc- I - ' •J ' -
2.? 1 00'"t " • 1 /^ r*223 OC2?4 O.:.I-IC. /-,/'.c-e. -' -"-TT? r\ r.e.c- / ..i..-22"? 00242 00244 00245 00246 00255 00256 00256 00265 00273 00274 00275 00276 OC277 00296 00323 OC36 5 00372 00423 00441 00442 00443 00444. 00
20 172 9-?
10 37 i i / . i / - • ^
4 2C-
1 371 54
37 1 15 \^2 J61 1&
16 902 571 714 761 572 501 263 717 69
51 3^9 521 23
M i n
c; N i L . " 87040
1 CALIS 4/24/85
i n t e n
•/. RA
I 234 592 991 241 703 342 471 73
11 743 2^1 221 443 83
100 007 001 282 764 4.L
1 2/-5 0-i.6 371 33
2 55
1 3?1 2C6 39
1 ^3 41
100
•/. R I C
0. 140. 920. 340. 140 I?0 300 200 191 320 3/0 140 160 43
1 1 2^0 790 14C/ ^1C 5'-'2 270 3?0 140 5/0 72
- — -. - . ,..C 15
0 290 470 160 I?0 "o i r0 I /4 170 500 270 130 160 3P3 900 270 190 530 100 280 140 300. 865 771 070 14
I n t s n
120449292121l & r327241169
114S3221 1914:374
97-66@-12;27-.43:-
i^-r--••»-& •12-d'?-,fr^~i "•
J W ^
24-^: :136I I 7
5-.c- —
13^1 51
50'231< • ••1 i .-
1^
3 .r'16";'-'^ •c- - .
16'45S15J24:123265752
502493112C'
002308
i11
B^ Icvll S&i-""
vasssSi, wwso hriHBB
§§| **":• T^
H '^-l
§1
VS 9
II1 51?•e•'
| ' • '•^ r- "
I M/2 ci
| l^.n-t
i i1n. i
i&t^ a-!1 '1 t . '
i J •B 1 ' ••MCi f ' '
SS i Bif ' i ' 'i ' • -H L. ,——^ .. .
.
R?1
-
I.,
39
BM
f^ID Wt^4'3e-SHMPLECOtiDS.GC TE:M
51
;
57 ,L J,n
";<. •• -T--^
::0t3
« 1 . » » » » — — « — — • . » 1 « W — — — —
SS SPECTRUM C^'A: ^^•l? '?^: ^cc:; P ' E r85 7:40:^ + •3:l:: / ^ . t / / ' 7 ^.^ ^"^P^.'-^i ?: ^l,::: SU PEPF STD •7^?-4F--PFr=. '' '- ^ r /
: 3eri OB-? F?|: •tf'-i^rp ;"• 4--.mi?'-- ^^^1 r^i iFv 4 ;4 ."D: :' ceQ. -
t
I
-J
pJ— '
ft^^J: ;::'"^ '''l - ^ "1 ."•'»
1
. - - . ; j, ' T?'" 4^ .-. ^ JiuLi--.- , i 11 • • •
i...:.i.''
i-»i
1 1.3:-
< i .-. !'i r )i
' •-tit£-
A'y6»' iq. 1 ; l- ',. i i ':' i ?5q,-? ;
- - - - - •-.i 1 ' 1 ,^——,—————>———^-^ ..JJ..-L i.,Jt, .i.., .^^ ^^t -L^ . ^ . - - • t - ~ ,-ll. .... 1,. |JI-.... 1 ^L1 , 1 ' i [ . ^ •
r
1 ' 1
\y' 3^~i ''
REVIEWED
MAY -. : ?. 198^. /' •l<^^?'/
..fiSRf ;i -- .
"? "'*' 1 1 • '•' r •.,-> • , * -L -i ' .'.'-• • ;-1- '" : 4i1 • *
.!-••.->
^^c^
**"
'4 244. 1 , "'•>€- ) i
lL^-L^iL.—-' ^, f
^
A 39
^2; 19887949.
-»J
t ;?ec"T—'—r^-
•
'.
002309
GC/MS TIDING AND MASS CALIBRATIONDacofluorotriphenylphosphine (DFTPP)
Case Nc. ^ 1 ^_____ Coniracior '^.:: 5.:.: --.c-.-.::-. . JLr.S;.,. . Csnir<=;: ,\o 66- :. f^ ^
insiru^en: 3 l7^^ 4 1 Date ^^/^
Lab ir^PSCM^^'ft ' Da:a Release Authorized By
m/< 10\ ABUNDANCE CRITERIA •'.ftEL51 30 S 60-0^ ol man ^98
68 iet» •-.an 2.0*»o( man 69
69 man 69 'e.n-ve at:i.";a"ee
70 lest •-an 20") 0* fTun 69
4 C O 6CO f l.o« matt T98127
'?it "an I.O6- of m ii 1981 9 7
199 5 2 - - 3': o< fms 199
275 1 C : 3C :': o* n-asi '33
\'i .^.e n pa'fi'':'''! s i :; man 6ai
IVa J? '^ Da''er't^'^i * s ^s •^'ais 4^2.
^'S PEPPOR*. '" ' .C^ "•J'.E A^^L S3 TO THE ^OLLG••.t•^GSA'.'PLES. eLA'. ' -S -'.^ ST.\- .2A?^S
002310
3SB t^
ffi *
•r ^
?- ^
'
• ^ ^
LJ
LJ U
fJ
"J
."',1
i'.i
-•
—
• 1-
•-;•
1.,'
-..
' -J
.,-
^ -I
J
.1 ^.
' •"
'.
. .)
. •
. -i
'•i
-
--
0-
•> '.'
C*
- ••
•-" O
'-."' U
' U
'.."
-3
3^
C:
'13
-•^ -
- Cr
- i.J
l CO
•••
-<••-
"M y
0 0
,';''
-^
^ •
Tl
-^
* •--
• I '
-•'
-.'
^ -
n
I'--
(-1
i
• --
."••
.. •
--
•..
;'
i71
- »
•• ;"
^
.1:.
ir.
,•-. t
.i -
^ (
.- PJ
-
C '
0
2
/>.
0.
12 u
• •
1 A
0 »
** t- 0
2o
o o
c' o o
0 0
0 0
0 o
o ^
o •
r' o
•>
'..i •-
" c
o '
o r
-i r1 •
-'' "'
':' •
\- •'-
c -i o
c
'." ^
^ o
€••
o 1
••;'
o o
o o
o o
o
/• A u
TI
\ a-
0 0
0 0
0 0
0 0
0 0
0 0
C 0
r'' C
•-,'
•
•"-*
•''
• .
•
• 0
•'i
''"' 0
.
' --•
C
. •'
•'
• • '
^ •'
'.. 0
-:
--•
•'-• 0
0
'•> 0
0 C
0 0
0 0
.i
rft
C
(
• CD
^•
• J
.• -^ ^
J ^
U»
*P
31- U
(Jl
Im
o o
tu r
'LO
U 2
0 -
<,".
T
-a
-o
P) r
tcu
-1
i.'
-• rr
•J J^
*-*
x CD
3 '0
& ^
>-.
-. 1
-* fu.
»-
i«* "
— p
j i:
it
ci ^-
•.
ip .
-- ,
f-, .
, ..-
-. r
;-,
..} i.
/i ...
--
f • »-
^. f
, "i
i,j
ft . j»
r)
-o <
• i."
»•* "
'--
fc PJ
r"J
i> >
^ PJ
.s-*
o
*—
i m in
oa
.'
o -
o -E*
•& "
-o ^
^ \
: <•
.J
-,1 '.k •
"''•• '
-•, :..
~1:. •'
.'"-
."',
,."•
-i
••• '
•.•• -
i -'
~' "
— -
.' — ^
c.')
1-; •
J' c"; c
''.'
fJ r
t.1 u
'o
"n
o
o
< o
•0 C
' -<"
C-
t-
C
' C ^
-'» ^
^n
L'
' '
<..; '
:•• ..
i '
" <
• .-
.'.
,-
! ti,
-
. •
--
•i ,
,.
.,
, :•*
0-
; ••;
^-
r
••
'"
••
.•
")
—
••
ri
0 " (J)
in +
n -<
>•
0 0
0 0
0 0
0 0
0 0
••3 0
0 F
-J i"
' 0-
."• 0
':-
i
& c
1 —
•:•
• C 0
0 .
-' 0
.:.
•'.
''•'
' ."•
..1
.-;
0
^ r-> ^
:.» ill ^
0 0
0 0
• ' 0
— 0
0
'O
33
^•r
A
-^
"J
— r;
—
"J —
r'.
; "J
.J
A
f.-
— "
„
• r1 I;
-.1
— "
i.j
'J-
{.;
r-.
. >-
i—
-.
—
c.
.i
i.i
• •'
,-,, I
J 0
(i
C^ --
—
'*
! •C»
"J
f1-'
M ''J
(J
—
0
» —
0
.;•• c
••.-
'•-- -
^ r'
'-;•
•• r
-- o
:•-
u.' .
£* ~c<
) "'
' tii
-/•
;• &
• ..i
& <
.-i r"-
P)
A r
:. i •
•' i.
': i-
;;
— i./
i*
r.* r
.' lv ir
-• (
- iJt
i> o
- a
L.I
^
o
LJ ^
oL
J t>
on u
-1
I—
«•
^ (J
i•-
U
P,
I LJ
•fr
PJ
3
—
(*J
Ft 0
pJ H
J _
»-
. ,„
w
t-t
pJ p
j ,-
£.
1 1 0
— ^
" i
J —
U
. fJ
«—
" P
J 'sJ "
t.n
PJ
L,'
•—•
PJ —
—
0-
&• —
'
I
Qt
&CD
^ 0
•-
ED A
E^
—
CD 0
LJ
•-
& P
- •O
fr
r-
1 '
'>
S^ 0
"> ^
iJi
-i ^
u [>
vJ
o ^
-
A •
.^ ^
03
C'- i>
"J
C'
• i -
~0 0
U P
-' U
0-
Ut 0
" 'B
U)
'— r
*P.
; -. U
U -
^ FJ
CD
fJ —
)J 0
O C
^ '1 ^ "
^
1'
fr
•::)
•..
^1
•'.,;
PJ
- ; ^
f..; C
•I '
•• CJ
L.
' '•
• ""
' ",'
• ':'
L- ^
IJ I
- n 0
'-.
^-
••i
-to
CO "
J C
'."1 3
00
PJ <
••
if(J
1 ^
3 z
-&
yi
inCJ
>- i
r» <
<*
3
CJ >
•D Tl
- -
0 U
l 0 0
-h ^
A A
A
U
U U
U P
J PJ
fJ
PJ
PJ P
J P
; PJ
PJ
M P
J PJ
PJ
PJ P
J PJ
PJ
P:
P.-
CL'
"J P
.- PJ
FJ
P.'
PJ —
— " "
— ^-
— "
—
—
—
— •"
—
99
0 m
A
•&^
AA
Ar
iJ^
O^
UP
J^
^^
^^
^C
^C
Pt.'l
iJ'A
A^
p.p
^n
Jfr
Jn
J^
-^
^.-
^o
OO
O'd
'O^
O^
O'O
CO
OC
DC
OC
O-
stN
i's
IC
'^
EliO
) ro
L
JE
J-c
' IJ
rJ
— U
PJ
y A
CJ 0
^ 1
^ iJ
i A
LJ
(J» 0
'?•
^i C
" C-
' A
'.i
IJI
£.
1..1
— ^
-^
0 '','
•..
L-' ^
A
-^3
CC
*> U
P.;
'M t
- C
" —
C ^
^ A
<'
2
0) •
C* 0
0a*
"• E
D CO
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
00
0
•-"
^•U
'tJi
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
C 0
0 0
C
"I 0
•-'' 0
0 •
:' 0
0 0
0 0
C 0
0 0
0 0
0 0
0
>"
TI
"4 C
T '3
•4
f
h^
2
2>-
2
» H
-3
0 •—.
(J\
>-•
I"
^CJ
l -
.^
J,
-.
^o
^*
3
PJ
O^
-^0
^-
£>
CJ
—
—
>->
»-A
^-r,t
^iu
>-t-
t— (J
IQ^
-^.
^A
ftJ
i-i—
cr--^
^-,
>- -.
LJ
IJ ^
IJ
C1- 0
LJ
•~1 *-
CJ 0
•—
—
PJ
I*1
'-'•-*
*^
^
ft-
0ft
J>
U^
<t3
)U
O^
(U
^U
U'^
^^
AQ
^P
lOI^
^J
CD
•-*
^.P
'-IJ
C^
•-•'J
'•-.^
00
'J'e
^O
•y
O'(
)P
JP
Jl,
Jl'
O^
PJ
U^
OO
^O
O
3)
:)
r~U
..- ^
.-*
— ^ ^
^ •
<]. C
J A
CO
(-1 0
C
r* L
-n
•,; -i
11
IJ ^
f •J
Q i
U o
£,
^> ^
..i ^
.0
p i
rr. IJ
1.1
o •
i- u
Q Q
-0 U
CD
(Jl
L.'
'O 0
1»
*-<
33
d)
03
»-*
tt>(•-
) tfi
^-
: A
re
O—
E." 0
00
00
00
00
PJ
OO
OO
OA
OO
00
0—
0
00
0':
'00
."iO
'"3
Ci—
O
C-
00
—0
00
00
00
^x
M
a
>— 0
•O ' U
•— (
U
rJ
•&
—•
rJ 0
CJ
—
•—
f-t
f> U
•"
•"
•^ ;.
fJ
i—
>-
sJ C
.D "
—
—
!.J r
' '.'t IJ
'.t
LJ
A ^-
^-
-to
"J
PJ
^- P
J' l.
h-
-* •
—
•—
0
-E*
^/"
••J 0
^1
C-l
PJ r
'J ^
0 <
Cn
'."•
h C
" ۥ
- "J ^
0 L
; '^
^-*
C
; •-
i .3
1>
t-'1 1.1
<
\ '-J
r>
~ •
•,i ri
C .
->
'<;
s;
(.1
A
fa
C"'
•£>• '"
-^
^1
i-
'O
"J
PJ
^
0
^
•s*CO 'J
t (J
l0
*^
-^J
'-•PJ
•-
M
i~
m
-»
(J
I -0
Ut
^3 L
J *—
^-*
—
PJ
-
• 0
•-
—
IJ "
A
PJ "
f.P
LJ
r !
-- -*
P.)
—
C*
-J M
PJ 0
<-•
— --
rr
PJ
HI
^ -p*
•<:
•A .
a 0s -
'• • o
i.i1 (
i} ,.J
1,1
fr> '"
n n
— o
J-
-.1 -^
i,n u
fa i,
n •.J
;i' ^
en
•J cr-
-J
,'; *»
• --^ ^
c'-
^i -
'-i o
ro o
&
-i
'o i>
o
TO^ t
) (•- I.I
—
PI
P.)
OJ U
0
i1 :
• t-
)-
-•
i"-
t-
C. •
:'• rr-
•-
fi
0)
-O
-..
'.n i.,
i.'''
i -i'
•
' U
'l •;'
.".
•J1
•--
;:;! ^
) 0
-^
FJ ^ U
—
JT,
fy-
A*
t.J •
- 3
00
57
00
002311
-1 '^
_..-
-L_-
——
1.—
—-.
,-l_
-——
-A...
.. .I.
^ .s,i
•s'
-J
•-J
'£'
'-'1i
L:'' i
i i.ri
c.i ri
n: '—
' •z-
- f
* >-
4
.n
z: -
-,
cr'
^. ^ o
•TI r
.<t.',.1
'n >
.n r"
Q :•
?=£
•
m -
, 3>
I -T
J ••
"
ro u
-1cn
tntt-
o-
' LI
i fi r
. <&
's
u'i
'.(i '
f '
i '•
'• ri'i
c1 'r'
r-.-* r
^r^'
•T)
^-
;A;l
—)
f • '
•n
i -•
-1.1
f 'l
0 c^ •so
-{•* r-.'
50 m ^ m m 0
•~)
-^ C
D-<
X>
0 i.
ri••
m '3i
"\ rvJen
•-.s> -J
-.
^n L
Or-^
' ':c«
.'l -J cn a"'
002312
GC/^S TUMING AND ^ASS CALIBRATIOND^cafiuorotriDhenylDnosDhme (DFTPP)
002313
I D Mass/oi. 'e?
S a T p 1 e :QSTI d a
1^1 -
36
!497; Ms ?• s
139 00^50 00^51 00->
52 CO-gS 6 00?8 5 7 00"
63 00"
1 6 5 00'69 007 4 00
n75 00B7^ OOH 7 ,'" 00
7S 00
1 79 00L'-': 00
£ 1 C'C
1 ;?;: CO
L- 3 0'..'•? 1 0092 0^
gsJ 00" /c; OJ'
99 00
B ;, 1 •"003 0'.
i C4 •:--m •'<'-:. 005 ' " ' CK '^ :'d 0'--: 1 •J OC'
1 1 ! C'Ui i OJ
1 1 ;•' 00
J ^^ 09.-•J 0':'
1 2 7 0:'BR ; 00g 29 00^30 00
1 3 5 00
B37 004 1 00
1 4 2 00g47 00g4& 00
1 5 ':• 00) 56 00
B/-'\ 006t,7 00
Ll5t
7: 5 :••SV PE^30M D£-ti53l A l
0tt 0 Max
•/,
-><9
42•~ic.
1333
-14
E3
*- --'^3-3'•A
*
•:
^
3
1
^
'.'
i
*
' t-
(-"
-;:;•
c.
c"r1
C,f
4'i.-,c. -•
111"1e-
01•
e.»itJ
34
Data: PS05000 +
STD (5 f^SCC. 00
00
RA •/.
249639404:-659o1 00"
. <-' --'!•<'-•'4,-•£.' •^
c)'!
^ ;'--.' -'7:;/. l--.0"'0 ;'"'/-:. ;.,r '. •
~> -
JO'i.-'i ^i .1 :-'?..:5-
. li;/ • •
i' '6r-97a .'9l r '•-»>-
7054
1 10:.-9907<:'4?;1
B(Cl:i:M
9763-4C/-
(ti3387l) 25/4-300
0
0•\500.^\
0cR/-i1i''700c,'
'^,'
,'"
.'"-
1^.
'...
00c1^
0104C000c6r-
•ic-
00000000000
^^^R
- 01
00
RIC
^27c?l
. 1 5^9ig44.?41 3^4
t:-l0^4^1
t ;.'.. ..''-'?^-„• -•3 3-i"J •?< •
1 •"'
1 r.'
(,,C:/^ -1.IT
4^.-ip
1 ^1 ^1*'-&1-"'" iL-' 1
/;<
('
1 1
93lr
i&
(JO
'• /-
4 -.,2\1 91 3r-1^is1 3V71 5..'.!/'53
^SiB^1 !) ^
Cal i PS050185A1PERF) CASE 4 1 1 7
0. Mm
Inten
3B1l<b9fc7216
409247622337IS'7
1^0967^-C
14c'£ )
593lOS'^r?.
^/J
^ ' ..
4 c.- ••63 -! •"-'} " ' ^1 ::1 ''r ^COC.4'.•L3^39:! ^1 9 - ,1 9 ^
(=; . c;
^.3-L
6i d4
B...';.1 4 9
1 3 OBl/.^249
9^.,, G70^
344^28'---26?1B934 b16818338.:-S?OG317193739
i ma Mm i n t e n ,ima
111 7 5 001180 00118^ 001119? 00193 0011120^ 00204 00r^O-'- 00•~i">c:,•"1
C-
£-.
2•i—'^':. 002^'" 00&.2?:', 00Sc-11"? 00•"t&>.
c'.
24,-,, 002b'- 00c.
?^6^ 00273 00274 00£-
276 0022323 00334 00365 0037? OG423 00441 0044<"1 00443 00444 00
1 6 5 A 1
@5 FINN01 CALIB
Mass
68 0074 00
79 00
81 00
06. 00P7 00
96 009;J 0099 00
0^- 000 . 00:'? OC'i i oc1 - 00^•i' 00
?5 00
44 004^' 00
56 005& 00
/') 00
77 0096 00
^ 541^ 2
'/.
301 .21 .11
1 1310.•~i
100602.4
1 9n
01±
461 ,
10'->c.
4181i
354,1013
1 7t14.1 .110
S 27.
4800
BasR 1 C
RA
1 19055959906211 41 51 593750061S9472 i016287
627790100146000333123':'24
96098620060119430766037785361 36S3690
e m/z .140032
4/24/85
13Q.
% R 1 C
0 380, 1 10. 190 360, 240, 1 30 1 51 - 350 300 1 40 1 10 46
1 2 1 6o. y'0 i 30 30U 5 1." 310 320, 1 10 200 5^.0 840 1 31 -ni C. (.
0 300. 490 1 3; 010 1 40 164 230 600 230 100. 1 50 372 070 260 1 70 490 200 120, 230 100, 290 875 921 020 1 1
198
Inter,
52^1 5 4264503339ISO206
189653&19t,15c -6?c-•
3 70.;^1 1 2 6
1 5 24207li
1-3 £ •-j fc
44.:;14::
•-1-7 .c. • -,
S 1 .1 1 "''-
•[ q -
1 7 0 4
4 1 8& S 1 ,1 7 6
1 4 1 ^19023C
6C"X84^32r1 4 -20-'.e; -•, t.
289^.37124369328217530114?406.
1 2 1 482S61424
1 5 4
002314
a ?;
§
£
»-<
*——
'——
'——
1—
—1
——
1—
—'
• -
1....
1 .
..
.05 r
!CTl 0
-'»-i G
'(S
-• 'd-t\J
-—
, /-,S
/—
^
IJ'
^-
CJ
00
LLJ
0^
LiJ —
^LH 0
^"
'-Q
<r -< U
J ,—
,CD
Ct.
—~
-—
'>•
>-i
'/•u^
^.\ [
tv
-^y
v, \
\G
C
-^\\)
\Y
^,J
' \\\
\s '-\l
ii •--j
',
11= ft '\
—;
. -S
'J=-
b ' U
• (<.:<—
——
—-:
'"'':• 0:1 ir'
i-.< --:
— --:•
0;- 13:1
IJ i,
-a '^
J"
""
"'"
^—
••
——
——
——
——
-^•^'','
<••-,IJ
-I U-l
^
:l-'l-
IJ- *••+-
. .
••c'
;..
..
QJ
i:C'-—
-==
<•
»•
;—
<»
-•
-, -
t- -i
-J
^ .
-J
Ct -X
t - -
l.~i '—'
''—.'i
l~t
•
tj-'<-0C
J
ll-)ll-i —
——
—.—
—„—
——
.
\'a-
(X:
^ —
-C
^ C
-l0./'
^
—
t'j—
—^
•-"'1
^
Q—
is"'C
-l
--0r'l
Li.
crii'1'ivt
i''J•J'''4
-
L
'^' •-•' 4
t•i
h-
L^
'i
fK:
1-
1-)
liJQ-
IJ'I
i/1111<r?-0*"-«f
»—'
CTi
+i-;iG
1
•r
iSl
tT'
ftJ
r-^>
<Sr
u-iCO--< ^J 'yi<s-"•-.IT-'S
^t i' 1
C*
LLJ CJ
;L
1C
^ T'•
U'l
- r^
tiL't-:LiJ
-C
L •—••t
f -
•^- '-•-.1
•-•''
IJ-,
.-•
r -- L-i
C,-
Q i./i
L'lir*
Ll- t
Ct; C
uLAJ 00-
E-
U^ CO
uJ '^CL. 0E
" <C 0
U'f 0
1
'—
'
r^i
• 1'*.'
f •I .
LU --•*
CJ --.
£:• —
r&
• '
f'--< u"...
:tt" •ri
a- i
1^£:
LU -
•1— tir
<•• -fto
IT'
ۥ''cn
"
r^IT'.
ll*'
r.-.i'C
'nI.';
Ju'-:
mr.i•'•"i
ll^'.T
' -'"••i(i •
0-1-ۥ>
"-r'<^c^ll-*
ir*r'-c-;
Cr
ll''
002315
Case ^a.
Instrume-: ID £lf/^..^.L
^h.n er^r-T^
Contractor -Culf ^.r.'.:^ Pp.qp.-'-rh T^rf^T^ci No. ^8-0'- ^•o^' ^
Dale _ ^LlU£______ T.me-^rl_/2i Z/ / ^^.-^- '
Data Release Authorized By:
fn/c IC*^ A B U N D A N C E C R I T E R I A
50
75
95
96
173
174
175
176
1 7 7
1 S - 0 • 40.0% o^ the t33-,e oeak
30 C • 60.0"a Qi the base ^eak
6as< peak. WC0;. relat ive abundiince
5.0 • 9,0°;; of ;he base peak
L?;! Ifian 1.0"',) o* the basfi peak
G'e^^e' than £0.0'''o of ihe base peak
5.0 - 9.G3; of mass 1 7 4
G'este' than 95.0%, but !ess than 101 .0% of mass 1 7 4
5.C - 9,0^ of 'nass 776
{?<t^. i y
^^.0
)00.
^.33
<^
^^ /
5:3o ^^1
^-;/ 3 ^y.^ '
^7^6 C?. - / / )Value in p3re"'L*''esis is ^ r-iass 1 7 4 .
*V.ilue \r\ paren'.hesis ii % n-ais 1 7 6 .
THIS PERFORMANCE TU.\£ APPLIES ro THE FOLLOWINGSAMPLES. BLA\ *<S AND STANDARDS.
SAMPLE 10
ftLrtM^ 1
^^pp^-.v^^7?.L^p ... ,,, ^ „„W^b yi:^ srD..^OOPpb^t.^T^..
' ^•> Mi-^ ^n>fsJA^ z
J — l . - l - ,- ^r-ni-i in ini.riLiiiL.
LAB 10
——^LJ lllj /?
———l^UJJ^L^^(/V/.7^/3 .V^M.LiiA' /^-^/1^J> . . .
..\to/,l^'./,7^'^ „^ L S ^ M J ^ i Q . : „
DATE OF ANALYSIS
^/ / ?-/ ^ i"
-^——J
/
^
. ...-i /27^' ./
TIME OF A N A L Y S I S
/3-,- ^ f/
A- ; ?^
/7,'^<,'
/5" /^/^,^'7/y-^sJ?6?;4 c/
4 /Q4
FORM V
- . ^ . .h.,•. ,- ...—-*-'..-'"l-l""^"^"Bttlr fT-^i-':••"""'u:"""l >1''",„>t», ^^^^•"^— ' w^•-""•~"l•a
002316
E/17/85i m p l e :Conds. :^»144 -
• 36Pi ^&1 iJ
6 Mass
36. 00?
137.00?38.00?39.00?40.00?| 41,00?S 43.00?
44. 00?| 45.00?S 46.'00?
47. 00?to 48.00?| 49.00?9 50.00?
51. 00?| 53.GO?D 55.00?
56.00?| 57.00?| 58.00?
60.00?.61.00?|62.00?B 63.00?
64.00?1 65.00?S 68.00?
69. 001 70.00[ 71 00' 72. 00
73. 00! 74.001 75. 00
76. 0077. 0078. 0079. 0000. 0061. 0082. 0004. 0085. 0086. 0087. 0069. 0091. 0092. 0093. 0094. 00
13:50NG1%SP#130
ft O M a x i m a
S 1. 20S 7. 10S 6. 82S 3. 78S 2. 68S 2. 32S 1. 97S 3. 92S 2. 98S 0. 26S 1. 67S 0. 66S 4. 64S 22 81S 7. 14S 0. 08S 0. 27S 2. 14S 3. 18S 0 20S 0. 60
5. 415. 26
S 3. 50S 0. 48S 0. 11S 11- 11S 10.61S 1. 06S 0. 44S 0. 42S 3. 40S 14. 70S 44-97
SSSSSSSS5SSS
SS 10. 93
51:004-BFB
1000 CX I . 00
0. 00
X RA
5. 680. 290. 414. Q82. 124. 411. 690. 080. 440. S56. 684. 930. 753. 573. 61
+ 7: 12INT
ARB B
0. 00
X R I C
0. 24t. 421. 360. 760. 530. 460. 390. 780. 590. 050. 370. 130. 934. 551. 430. 020. 050. 430. 640. 040. 121. 001. 050. 700. 100. 022. 222. 120. 370. 090. 030. 6B2. 936 981. 130. 060. OQ0. 970. 420.650. 340. 050. 090, 051. 330. 980. 150. 710. 722. 16
C a l i :CALIB ^45/4-220@8
0.
Inten.
88.520.499.277.196.170.144.287.218.
19.137.48.
340.1670.523.
6-20.
157.233.
15.44.
396,385.256.35.8.
813.777.136.32.31.
249.1076.3292.416.21.30.
357.155.323.124.
6.32.18.
489.361.
55.261.264.900.
BF041785A^J^. ^ / / 7
FINN 01
M i n i m a
Mass
95. 0096. 0099. 00
103.00104-00105. 00106.00107. 00108.00110.00113.00117.00l ie .oo119.00121.00123.00124.00128.00129.00137.00141.00143.00147.00159.00163.00169.00174.00175.00176.00177.00207.00215.00
i, * r-r odae n i / z :S 2 R I C :
CALIB 4/17/85
Min in ten:
% RA
S 100-00S 6. 33S 0. 40S 0. 79
1. 38S 0. 15
1. 00S 0. 19S 0. 38S 0. 79S 0. 51
1. 930, 68
S 0. 560. 71
S 0. 200. 670. 980. 77
S 0. 331. 481. 500. 49
S 0. 230. 520. 52
66. 095. 30
67. 325. 66
S 0. 480. 05
0.
% R I C
19 961. 260. 080. 160. 280. 030. 200. 040. 080. 160. 100. 380. 140. 110. 140. 040. 130. 200. 150. 070. 290. 300, 100. 050, 100. 10
13. 591. 06
13. 441. 130. 100. 17
*y^ -
36672.
In fcen
7320.463.29.58.
101,11.73.14.28.58.37.
14150.41.52.15.49.72.56.24.
108.110,36.17.38.38.
4984.388.
4928.414.
35,62.
rfHfWJt BhIUKUlIktAuiu •IL, . E. u.. f -fiL L..-. ..
002317
F1A5S SPECTRUM DATAs BF041785A ftl44CALI; BFQ41785ft ^204/17/85 13:51:00 + 7:12
SAMPLE; 50NG 4-BFB INT CALIB ^A ^cl - / / / ?COHOS.; l^SPieee CftRB B 45/4-22e@8 FII 01 CALIB 4/17/85GC TEMP: 218 DEC. Cftl44 - ^130 ?<1.00
95
BASE M/2: 95RIC; 36672.
APR 2 5 ^985174
f I
- Gsm ^
75
^ ;i 57 n» 79.* . 1 . 1 1 1 f1 iL-[•iil.'lHI!;- ifE-llll-hii.-ll Illlll !..,.! ,121 2@7 215
123 148t ' " '•i
168 1881 1 E - • • • ' • • • • l290 220
0 0 5 7 0 7
002318
Case No. Contractor nuK. ^^"h ppqp.-^r-h ri^cf^ntrgr-t ^o. -&^Q1_L^L .7.
Instrument SO EiX^Z-_ Date .._____I/ J^i S^
//-<.<'/? -/———-——-——s^- '' " ''7 /gg3- '7 Data Release Authorized B ^ ^ ^ ALab ID
m/e 10\ A B U N D A N C E C R I T E R I A ^RELATIVE A B U N D A N C E
50
75
95
96
173
1 7 4
1 7 5
176
1 7 7
15 ,0 - '10.0^ of the base oeak
30.0 - 60.O^ of the base peak
Base ?eak, lOO^ relat ive abundance
5.0 - 9.0°o of the base peak
Less :"ian l.O^ of the base peak
Grea'e- than 50.0°o o^ the base peak
5.0 • 9 0°3 of mass 1 7 4
Grea-0 ' man 95.00';;. bu' 'ess !han 101.0% of mass 1 7 4
5.0 • 9.0^ of mass 1 7 6
?5".
5-V.^
i00
f.iv
&'^.S-
-/. /^ (7s^ '
^^ ^^'
^.t'^- ^^.S'^2
Value in parent ' -ssis ;i % mass 1 7 4 .-Va'ue in pa/fnthes's n % mass ;76.
THIS P E R f O R ^ A ' . C e T U N E A P P L I E S TO T H E F O L L O W I N GSAMPLES. BLAr;.<S A N D S T A N D A R D S .
SAMPLE ID
b^pb v^A -^'^rA^f^^OIV OcA^/ 3,
.f/l - ^^fA •^^<}^^^^^^ -^S.^Wf)
rd^?r;
LAB ID
V ^ t ^ ^ / i<>--.7?
^OJ6-2^. . ^^Ib^A .. ,..
^Jo^/^/^'/<-•• J 0 /
.-\L'..r. ./ ,,, .... .„ „ . ,\ ] O J ' ^ ) i ' f ^Sl>
VL\I.Q^..i-- ^ - - - : - -
DATE OF ANALYSIS
-///^ <K'^ ..„.„. ,-.*.-.. ,K»...» , ,.„ „. l,,r
==±=11 1 ' " • " " / " "rr7——==n——
rHhr/^
TIME OF A N A L Y S I S
S A>^<7.</^,
/6>; 5 ^'/ / . ^
/ '
„ . / ^ • / b
/ y . c ? . ./ ^ • o y .,...
4/84
FORM V
002319
- • _ _ •» w k n ^ bf C.X /18/85 8:22;00 + 6:36 Call: BF041885B ft 2mple; 50 NG 4-BFB CASE ^ / / ?
odse m / 1 : 95R 1 C : 13968.
Conds. : 1%SP1000 CARB B 45/4-22006 FINN 01 CALIB 4/17/85,^132 - #109 XI. 00l" 37
177H Mass
37. 00?
J 39.00?, 39.00?
40. 00?41. 00?
K43. 00?®44. 00?
45. 00?
B47.00?49. 00?50. 00?
a51 00?g56 00?—57. 00?
53, 00?
861,00?62. 00?63. 00?
»66.00?i69-00
73 00a.74 °°§75.00"76.00
79. 00881 00§87.00
88 00a 93. 00g94.00"95 00
96 00&31 00t74.00175. 00&76 00J177. 00
0, 00
% RA
11 6510. 497. 39
6 0. 56S 0. 99Q 1. 97S 1. 55S 1. 09
2 757. 54
35. 4610. 703. 45
S 5 775 0 74
6. 766. 514. 89
14 65S 1 1. 48
6. 9017. 7854. 585 775 114. 617. 08
S 5, 424. 75
11-20100 00
8 10S 0. 81
52 754. 12
52 194 08
0. 00
% R I C
2. 372, 131. 500. 110. 200, 400. 320. 220 561. 537. 212. 180. 701. 170. 151. 371. 321- 002. 982. 331. 403. 62
11. 101. 171. 040. 94l. 441, 100. 972. 28
20, 331. 650. 16
10 720. 84
10. 610. 83
0.ft 0Inten.
331.398.210
16.28.56.44.31.78.
214.1007-304.98
164.21.
192.185.139.416.326.196.505.
1550164.145.131.201,154.135.318.
2840.230.23.
1490.117.
1402.116
M i n i mafla a i ma
Min in ten
002320
PtftSS SPECTRUM84/18/85 8s22:Q0 + 6s3SSAMPLE; 59 NG 4-BFB CASE ^ / / /COHDS.s 17SP18ee CARB B 45/4-220@8GC TEE : 218 0£G. C
#132 - »109 ^1.0095
DATA? BF@4t885B 132CALI: BF8418858 f2
Fim 01 CALIB 4/17/85
BASE M/2s 35RICs 13968.
75174
58
68
7987
131T"f>"^ T"T< ^ •n' , i I '
80 186i 1 i i i " r r - r 'T 1 r T'T'T
120 140 160n n ^ 7 i o
002321
Contrac^or f^ l f gr^r.h .c'p.q.i-'.-irr-h. ^gri^pf-gct NO. . .rjll.-.. '' _
Date ^^Ar____________ T.rnp ^; g'/_lUStrume-: 1 0 P'.f^..^.^.
L^ ID f li ^*' - .-.__ .^ ^»^/_ .^ ~ '~~" ri-
Data Release Authorized R y_ -^- '_7 :~::::' '• '
m/e t0\ A B U N D A \ C E C R I T E R ! A ./^PELATIVE A B U N D A N C Ein .u-n^iiifc.1 —-
50
75
95
96
1 7 3
1 7 4
1 7 5
1 7 6
1 7 7
1 5 - 0 • -10.OS of The base oeak
30.0 • 60.0°;; of t^e base peak
Bdi<* peak, lOO^o 'eia:ive abunaance
5,0 • S.O6-- of ine &ase orak
Lesi in<)-i t.O^o of the Oase w^k
Grea'.e1' tha" 50.0'; o* '^e bas? peak
5.0 • 9.0% of mass 1 7 . 1
Grea'e ' rha" 95.0::•-. but less than lO^O^ of mass 1 7 4
5.0 • 9.0% of mass 1 7 6
y^S-^.L-
/OO
^ . /
0
. ^ - / - oV. S' (7,^)1
^o^ w-n\
H.Z^ C'^^) 2
Value in pare ' - '^es is is '\» rnjss 1 7 4 .'Value ui pdrenthei's 1 1 % mais pg.
THIS PEPFOR'. 'ANCE TU^E APPHES TO THE FOLLOWINGSAMPLES, ELAf . f ; 5A \0 STANDARDS.
SAMPLE 1U
^ h.-,- ,,,.. .,-a^nh- ^ ^ri>
i p JpAL. ,..,l^p^^ sn)
^ .JL ^n}
''
•»m ——»w»m •n.-iMM i. . JM^m
LAB ID
^ ±Ll iV^y^^^C.Vs^j^ •rfS i)
F- fLlL. . ^L—.-—^ .. L^^^ - »^^
•
DATE OF ANALYSIS
V/'••//.?<7-4 T-^-—"
~~£:————————. ^/ '•^————^-^(———————
TtM£ OF A N A L Y S I S
/•/.^/
..../'.f 5,,,,.,. ,, ,„.„,.„..-..-/^^y...„,,...„. /^ .•y^/^.' 3 t- /
,, .-..-.,..,,,. -.,.,,.,,,,,»,,..,-.,.J4 /84
PQftM V
002322
Iamp Ie;a n d s . :ftl33 to
i 36
207Mass
B 36.00?37.00?
«
3Q.00?39.00?41.00?
,g 42.00?g 44.00?w 4?.00 ?
47. 00?
!49. 00?50. 00?51.00?
156.00?, 5?.00?
58.00?61.00?
g 62.00?" 63.00?
66.00?
169.0073. 0074. 00
175.0076. 0079. 0081. 00
I Q7-00
® 89.0092. 00
193.0094. 0095. 00
Aft 96 00
gl74,00"17^. 00
176.00
K77. 0007. 00
501-/.SP1000 CARB £#135 Summed ~ #1
G
SSS
SS
S
100.00
-- »- . . w " • " " 0. -»«a \^Q 11'.W 4-BFB CASE- ^ / / ' ?
0. 00
% RA
1. 4612. 4511. 244. 032. 420. 776. 931. 141, 447.23
35. 3310. 272. 705. 430. 296. 056.214. 02
13. 4913.416. 52
18. 60S2.634. 934. 494. 746. 295. 990. 974. 10
10. 85
0. 1860. 95
4. SO60. 07
4. 251. 39
0. 00
% RIC
0. 292. 462. 220. 800. 4Q0. 151.370. 230. 281. 436. 902. 030. 531. 070. 061. 191. 230. 952. 662. 651. 293. 71
10. 400. 980. 890. 941. 241. 180. 190. Gi2. 15
19. 751. 61
12. 040. 89
11. 870, 040. 27
45/4-220613 X I . 0 0
0.^ 0Infcen .
160.1364.1232.442.265.64I f c T T h
760.1 O^iJt. e£\J.158.792.
3072.1126.296.595.32.
663.651.528.
1478.1470.715.
2060.5768.
543,4921 1 ha. i
519.689.657.106.449.
1192.10960.
89666QO.
493.6584.
466.152.
BF0419
8 FINN
MinimaM a x i m a
002323
PtftSS SPECTRUM DATA; BF04f985A fl34CALI: BF841985A S264/19/85 8:24:60 + 6:42 . -
SiWL£; 50 HG 4-EFB CASE ^ -' i
COHDS.: 17.5P10e9 CARS B 45//4-22^@8 FIMH Ql CALIB 4/17/85GC TEMPs 218 DEG. CTO3 TO ^135 SUMMED - # 1 1 3 ^1.00
9^
REVIEWED
APR25385^-
GSRI
BASE H/Z; 95RIC: 55488.
174
75
59
69
57 81 87
£9 80 190 120 140 160 18Q
0 0 5 7 1 5
207' \ l * ' ' n ' i ' t i
200
002324
Case No. ___^ // f Contractor c.^^.^.^'.i- o.p.F.^rr.h ^^ConT^ct No. irOl ' '
lns:rumeri ID Ef^ i 1 ... Date ,.^./•
Ub in ' c^^^ Data Retease Authorized By;
m/e IOM ABUNDANCE CRITERIA %RELATTVE ABUNDANCE
50
75
95
96
173
1 7 4
1 7 5
ne
1 7 7
15 .0 • 40.OS of the base oeak
30 0 60 C^ of the base peak
Bale peak. 100% relat ive dDundance
5.0 - 9.0''o c' t^e trase peak
Lesi ihdi l-C^s of the base De3h.
Gfea'er fa" 50 0^ o* '.ne oase peaK.
£.0 - 9.OS of mass 17.1
G'-ea-0 ' :ha~ 95.OS, but !ess "^an 1 0 1 . 0 % o' mass 1 7 4
5.0 • 9-OS c* r"ass 1 7 6
^ \.
^o 3/u c-
^"-.L^
r-
^^ 3
c ^ ^ ( ; ? 7 } 1
-, ^ C- t ) '
< ', c '-^2
Value in parsr thes 's li mais 174 .-Va'ue in parenif'ei's ii % masi i;6.
THIS PERFC^VANCE TUNE APPLIES TO THE FOLLOWINGSAMPLES, BLA'.^S A^D STANDARDS.
SAMPLE ID
-;' ,,, ^ L'.'/. ^r/^\u^ . ^rfl^^.rA-^i^ 1
LAB ID
.'• ^ ';-'-"C-i^rY"''^ •'^
\Lv •J^^/^^ .
^m-^ims^^
DATE OF ANALYSIS
<-// -,
.^..,,-^Y//.. .. ...„-,y '.. -J^f/
T(Mt OF AI^ALVSIS
'/ ^ -'t
-' •< ^ ,""
0 . ^ 7^;-?y
4/84FORM V
002325
1/19/85fnp 1 e:
Conds :fl^l44 -
370 l77
fi M.355
37. 00?
138.00?39. 00?40. 00?
^43.00?B45.00?B 47. 00?
49. 0<r>
150. 00?51, 00?57. 00?
158. 00?61. 00'762. 00?63. 00?
fl 68.00?8 69.00
73. 00
174. 0075. 0076 00
J 79. 0081. 0087. 0088 00
193 00' 94. 00
95 00
(96.0074. 00
175.00....176 00?77. 00
21:44:00 +50 NG 4-BFB1XSP1000 CA#i30 X I . 00
SS
100 00
SS
S
0. 00
% RA
12. 5011-464. 251- 130. 872. 042 308. 38
35. 4210. 297. 471 486. 296 124 21
12 5913 025 03
17. 5850 26
4. 605. 956 646 219 072 73
10. B5
8 6474. 22
5. 4772 83
5 12
7: 12CASE
RB 19
0. 00
% RIC
2. 382. 180. 810. 210. 170. 390. 441. 606, 751. 961. 420 281. 201 170. 802. 402 480 963. 359. 570, 801. 131 261 181 730 522 07
19 051 65
14 141 04
13 870 98
C a l l : BF0419E^yw^ c///7
45/4-2^088 FINN
1158
116
1710
0ft 0In t en
28826498262047.53
19381&237.17234
145141
97-290,300116405
106137.15314320963
2502304
199
1263678
M i n i m a Mm in ten:M a x i m a
uf W 4J
35B
01
T>
ft
t -r-T
2
CALIB
Ofa-avR I C :
4/17/85
ni/ i. *y312096
0.
002326
•*»-
COnC M
-*——
——
——
—l-—
——
——
—I_______L
iniJOcncn<s »CM••
v~tfxl\£:
LU -
too
<rfr-O
Qt^
'tf-st--. CM»
«•
mco
mm
CO 00
(ncn•y-< i~«•<!- tt0
(SLL.LLC
QO
Q
tn00.. ..
\<!:•-•
r-v-h- -J
^
<r a: \
QU
-<rOQ^J<X0U
.
&
^^
®
'
tM- ^
>"
-' m•<*-
(St LiJ-« U-l.. <rcair^- o
(XI
^+
CD <r oLL o
co
<S» OQ - <S>
CD I
<S C3 .
•• •<1' 0 LU
»-<^a
:/.™
0
K i^
(3
-> •• 2£ Q
- CO S)
a: »-« in
—« Mi—
(M ®
c^ <M .—0
1
0—
*,
lutp
0- CO
••
" &
. 1
01 \
Ifct
•£
. cn—
iy^lli •srw
•^ 4 0-Q
>- •fu-i s
s:^:
-*S
tr <x:o o (»
E: CO
(J C3
00CO-;——
r m
co
}—
co
in1s-
(Tt10
fc-
<.——
——
——
—^—
^--^„
<s?
S
cain
002327
Case No. Contractor (^1C . .-ir-11 Pp-^e.z.-rh. ^[•(^"^'•301 No. 68-0' - C^o^'^
Instrument !D h^^ (? I Date
Lab ID J^£J}JilLl£/l^ Data Release Authorized By:
m/e ION ABUMDAN-CE CRITERIA
50
75
95
96
173
174
1 7 5
176
1 7 7
15.0 - 40-CS of The base peak
30.0 - 60.0°a of ihe tsasc peak
Base sea1'.. IOCS rela::ve abundance
5 0 • S.O"; ot :ne base oeak
Less :r.an l.C^a of the base peak
G''e3'e.' lha" 50 O^o of ine base peak
5.0 - c 0°! of f^ass 1 7 4
G'ea:"' ina" S^.O^, but fess than 101 .2% of mass 174
5.0 • S O-o of fnass 1 7 6
3^,^•r/Jl00..
7. y-2.
6-7-3. y.i,^ ^n^7A ^ ( (•) '
' 25" ^- 7- ^T-^' ' '•- '"-/ /'.? /
Va'ue in parenihe^s is % "nass 174.-Va'ue in parcnihes!! 11 \ ~ass 1 7 6 .
THIS PERFORMANCE TL"<£ APPLIES TO TH£ FQLLC'.'.iNGSAMPLES. BLANKS AND STAr<OAROS.
SAMPLE ID
(3<^/^ ^ ^,?fil. \/.A STPfS'-'-^
^rrt -'i
LAB 10
v'fi^^^/^s^V-^^^l^ft\cTc r^ ^^-\J (.' re' i fc i<' ^
•
DATE OF ANALYSIS
^hi . . . . . .• ""• / ~ . . . . . - -^^—J
TIME OF A N A L Y S I S
( 0 : .?£>
./.?'- 1 ^ . i'S
.,...J,L.^. . ,..,,,,..,.
4/84
FORM V
002328
. ?^/^l/^ma m p 1 e :Conds :ttl42 -
B 37207i— \^ l
fi Mass
37. 00?
( 38.00?39. 00?40. 00?4 S. 00?
1 43.00?44.00^45. 00?
J 49. 00750.00?51 .00?
„ 56 00?IJ 57-00?• 6 1 . 0 0 ^
62. 00->
1 63.00?68 00?69. 00
1 73 00, 74. 00
75. 0076. 00
H 79.00* 8 1 . 00
87. 00
B 88 0092. 0093 00
a 74-00
§ 95.00B 96 00
1 7 4 , 0 0
1175 00176.00177 00
r-"07. 00'
9 - 1 1 : 0 050 NC 4-BF1-/.SP1000 Cftl26 >;!. 00
0. 00
•/ RA
13, 6113- 16
S 4. 08S 0 41
1 50S 1 . 335 2. 79S 2. 18
7. 8636 5310 48l 707. 967. 4Q6, 124. 56
1 4 , 5913. 336 46
17. 7651 09
5, 005. 656 635. 82
5 6 022. 074. 76
10. 31100 00
7 827 1 , 9-^
5. 6571 29
5 271 97
+ 7:06B CASEARB B 4
0. 00
% RIC
2 542 460. 760 080, 280. 250 520. 411 . 476. 821 . 960. 321 . 491 . 401 140, 652 722, 491 . 213 329. 540. 931 . 091 . 241. 091 120. 390. 891 92
18 671 46
13 441 05
13 310 980. 37
Call;^//75/4-220@
0.# 0Inten.
400387.120t2.44,39.8264.
231.1074.308
50.234220ISO134.429392190522
1502147172.11?^t l \J .
1 7 1 .177.61
140.303.
2940230.
2 1 1 6166
209615558
BF0421
8 FINN
M i n i maMaxima
ft«, * ~»c-
2case m/zRIC:
01 CALIB 4/17/85
Min inten
002329
MASS SPECTRUM04/'2!/85 9:11:00 + 7;0£ / , . . _ - - _SAMPLE: 50 NG 4-BFB CASE V // /CONOS.: 1^SPS990 CARB B 45^4-220@8 FINN 01 CALrB 4/17/85GC TEMP; 218 DEC. CSI42 - »i28 XI.00
95
DATA; BF042185A #142CALI: BF0421@5A ft2 BASE t1/'2; 95
RIC: l5?44.
002330
