GANPAT UNIVERSITY · 2017. 5. 13. · Quantum chemistry by R K Prasad Co -ordination chemistry by...

GANPAT UNIVERSITY

Faculty of Science

Teaching Scheme, Examination Scheme

&

Syllabus

M.Sc. Organic Chemistry

Semester I & II

(Effective from July 2017)

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1

GANPAT UNIVERSITY

FACULTY OF SCIENCE Programme Master of Science Branch/Spec. Chemistry

Semester I Version 2.0.0.0

Effective from Academic Year 2017 Effective for the batch Admitted in June 2017

Subject code MCHE1 IOC Subject Name Inorganic chemistry-I

Teaching scheme Examination scheme (Marks)

(Per week) Lecture(DT) Practical(Lab.) Total CE SEE Total

L TU P TW

Credit 4 0 0 0 4 Theory 40 60 100

Hours 4 0 0 0 4 Practical 00 00 00

Pre-requisites:

Before studying Inorganic chemistry, all students have basic knowledge of inorganic and organic

compounds, molecular structure, Molecular orbital theories and knowledge related to UG level chemistry.

Learning Outcome:

Basic knowledge of bonding in the metal complexes.

Understanding of V. B. and M. O. theories.

Understanding of quantum mechanics and its importance.

Knowledge of symmetry, groups, point groups and multiplication table.

Theory syllabus

Unit Content Hrs

1

Reaction Mechanism of Transition Metal Complex: Reactivity of metal complexes, ligand replacement reaction: classification of mechanism and energy

profile of reaction. Inert and labile complexes, interpretation of liability and inertness of transition

metal complexes on the basis of VBT and CFT. Factors affecting the liability of a complex,

transition state or activated complex, substrate, attacking reagents electrophilic and nucleophilic,

Nature of central atom. Kinetic application of CFT.

Kinetics of octahedral substitution, acid hydrolysis, factor affecting acid hydrolysis, base

hydrolysis, conjugate base mechanism, direct and indirect evidences in favor of conjugate

mechanism, reaction without metal ligand bond cleavage, and reaction of coordinated ligands.

Substitution reactions in square planner complexes the trans effect, mechanism of one electron

transfer reaction outerphere type reaction, cross reactions and Marcus-Hush theory, inner

sphere type reactions.

15

2

Symmetry And Group Theory In Chemistry And Its

Applications:

Representation of groups: • Preparation of matrices and vectors.

• Matrix notations for geometrical transformations.

• Orthogonality theorem and its consequences.

• Reducible and irreducible representations and their relation.

• Preparation of character table for C2v and C

3v point groups.

Application of group theory to - • Transformation properties of atomic crystals.

• Hybridization scheme for σ and π-bonding.

15

2

3

Quantum Chemistry: Discussion of solutions of Schrodinger equation to some model systems e.g. the one dimensional

harmonic oscillator, two particle rigid rotator.

Ordinary angular momentum, generalized angular momentum, eigen functions of angular

momentum, eigen values of angular momentum, different types of Operators and their uses,

addition of angular momentum, spin, antisymmetry & Pauli exclusion principle using Ladder

operators. Russel-Saunders terms and coupling scheme, Slater-Condon parameters, term separation

energies of the pn

and dn

configuration, magnetic effect: spin orbit coupling and Zeeman effect

(splitting).

15

4

Co-ordination Chemistry

Stability of co-ordination compound: Introduction, Thermodynamic stability, Kinetic stability,

Instability constant, Stability constant, Factors affecting the stability of complex ions, Methods for

determination of stability constant and composition of complex, Stereochemistry of Coordination

compounds with special reference to chelating ligands ( Optical activity of metal complexes with chiral

ligands). Metal Clusters. δ bond. Transition metal complexes of π acceptor (π- Acid) ligands.

15

Reference Books

1 2 3 4 5 6 7 8 9

Mechanism of Inorganic Reactions, F. Basolo and R. G. Persons, Wiley Pub

Reaction Mechanism of Coordination Compounds, C. H. Langford and H. B. Gray

Inorganic Reaction Mechanisms, M. L. Tobe, Nelson Pub

Inorganic Chemistry, K. F. Purcell and J. C. Kotz.

Quantum chemistry by R K Prasad

Co-ordination chemistry by Gurdeep Chatwal, M S Yadav

Chemical application of Gtroup theory by F A Cotton

Group theory & its application by P K Bhattacharya

Inorganic Chemistry –II, H.C.Khera

3

GANPAT UNIVERSITY

FACULTY OF SCIENCE Programme Master of Science Branch/Spec. Organic Chemistry


Effective from Academic Year 2017-18 Effective for the batch Admitted in June 2017

Subject code MCHE1 ORC Subject Name Organic Chemistry-I



L TU P TW

Credit 4 0 0 0 4 Theory 40 60 100


Pre-requisites:

Before studying organic chemistry, all students should have basic knowledge of organic compounds,

general organic chemistry, reactive intermediates and reaction mechanisms.

Learning Outcome:

Basic concept of reaction mechanisms and general organic chemistry.

Knowledge of aromaticity, substitution and elimination reactions.

Understanding of basic concepts of stereochemistry.

Understanding of conformation of various acyclic and cyclic organic molecules.

Understanding of the concept of tautomerism.

Theory syllabus

Unit Content Hrs

1

Nature of bonding in organic molecules

Delocalized chemical bonding- conjugation, cross conjugation, hyper conjugation, resonance.

Tautomerism, Aromaticity in benzenoid and nonbenzoid compounds, alternate and nonalternate

hydrocarbonds, Huckel’s rule, energy level of π-molecular orbitals, annulenes, antiaromaticity,

homoaromaticity, PMO approach. Bonds weaker than covalent-addition compounds, crown

ether complexes, cryptands and inclusion compounds.

15

2

Fundamentals of Stereochemistry

Strain due to unavoidable crowding. Elements of symmetry, conformational free energy,

chirality, molecules with more than one chiral center, thereo and erythro isomers, methods of

resolution, optical purity, enantiotopic and diastereotopic atoms, groups and faces.

Stereospecific and stereo selective synthesis. Optical activity in the absence of chiral carbon

(biphenyls, allenes and spirane) chirality due to helical shape, stereochemistry of the

compounds containing nitrogen, sulfur and phosphorous.

15

3

Reaction mechanism: Structure and reactivity

Type of mechanism, types of reactions, thermodynamic and kinetic requirement, kinetic and

thermodynamic control. Hammonds postulates. Curtin-Hammett principle, potential energy

diagram, transition states and intermediates, methods of determining mechanism, kinetic

isotopes effect.

Generation, structure, stability and reactivity of carbocations, carbanions, free radicals,

carbenes and nitrenes. The Hammett equation and linear free energy relationship; substituents

and reaction constants.

15

4

4

Aliphatic nucleophilic substitution

The SN2, SN1, mixed SN1 and SN2 and SET mechanism. The neighbouring group mechanism,

neighbouring group participation by p and s bonds, anchimeric assistance, Classical and

Nonclassical carbocations, phenonium ions, norbornyl systems, common carbocation

rearrangements. Application of NMR spectroscopy in the detection of carbocations. The SNi

mechanism. Nucleophilic substitution at an allylic, aliphatic trigonal and a vinylic carbon.

Reactivity effects of substrate structure, attacking nucleophile, leaving group and reaction

medium, phase transfer catalysis and ultra sound, ambident nucleophile, regieoselectivity.

15

Text Books

1 Advanced organic chemistry-Reactions, Mechanism and Structure by Jerry March, John Wiley and

Sons

Reference Books

1 Advance Organic Chemistry by F.A. Carey and R.J.Sunderg, Plenum.

2 A Guide Book to Mechanism in Organic Chemistry by Peter Sykes & Longman

3 Structure and Mechanism in Organic Chemistry by C.K.Ingold, Comell University Press

4 Organic Chemistry, by R.T.Morrison and R.N.Boyd , Prentice Hall

5 Modern Organic Reactions, by H.O. House, Benjamin.

6 Principles of Organic Synthesis, by R.O.C. Norman and J.M.Coxon, Blackie Academic & Professions

7 Reaction Mechanism in Organic Chemistry by S.M.Mukherji and S.P.Singh, Macmilian

8 Pericyclic Reaction by S.M.Mukherji, Macmilian, India

9 Stereochemistry of Organic Compounds by D.Nasipuri, New Age International Publication

10 Stereochemistry of Organic Compounds by P.S.Kalsi, New Age International Publication

5

GANPAT UNIVERSITY

FACULTY OF SCIENCE Programme Master Of Science Branch/Spec. Organic Chemistry


Effective from Academic Year 2017-2018 Effective for the batch Admitted in July-2017

Subject code MCHE1 PHC Subject Name Physical Chemistry - I



L TU P TW

Credit 04 00 00 00 04 Theory 40 60 100

Hours 04 00 00 00 04 Practical 00 00 00

Pre-requisites:

Before learning Physical chemistry, student should aware about basic principles and theories of

physical chemistry, thermodynamics, electrode potential, chemical reactions and other UG level

chemistry. Learning Outcome:

Knowledge of the phenomena of adsorption and related theories.

Understanding of the theories of thermodynamics.

Knowledge of activity and fugacity.

Basic concept of liquid crystals and their classification.

Knowledge of the concept of chemical kinetics and its theories.

Understanding of the theories of unimolecular gaseous reactions.

Theory syllabus

Unit Content Hrs

1

Chemical kinetics and reaction dynamics :

Recapitulation- order of reaction, rate law, zero, first, second (a=b, a≠b), third (a=b=c), nth

order rate equation, molecularity.

Complexities in simple kinetics – Reversible reactions, parallel (side) reactions, consecutive

(sequential) reactions, principle of microscopic reversibility, steady state approximation,

elucidating mechanism using SSA. Chain reactions, Numerical

15

2

Quantum Chemistry

Introduction to exact quantum mechanical results:

The Schrodinger equation and the postulates of Quantum Mechanics, discussion of solutions

of the Schrodinger equations to some model systems viz., particle in a box, the harmonic

oscillator, the rigid-rotor, the hydrogen atom

Molecular orbital theory:

Huckel theory of conjugated systems, bond-order and charge density calculations, application

to ethylene, butadiene, cyclopropyl radical, cyclobutadiene.

15

3

Theories of Reaction Rates :

Effect of temperature on reaction rates, Arrhenius equation, Activation energy, Kinetic salt

effect (primary and secondary), enthalpy, free energy and entropy of activation, correlation of

steric factor in collision theory and entropy of activation, Kinetic of thermal H2+ Br2

reactions, Numerical

08

Liquid Crystals (The mesomorphic state):

Liquid crystals, Vapour pressure-temperature diagrams, Thermography, LCDS and the seven

segment cell, Classification of thermotropic liquid crystals, Smectic liquid crystals, Nematic

07

6

liquid crystals, Cholesteric liquid crystals, Disc shaped liquid crystals, Polymer liquid

crystals, Polymorphism in thermotropic liquid crystals, Pressure-induced mesomorphism,

Molecular arrangements in various states of liquid crystals, The glass state.

4

Statistical Thermodynamics:

Concept of distribution, thermodynamic probability and most probable distribution, ensemble

averaging, postulates of ensemble averaging. Canonical, grand canonical and micro canonical

ensembles, corresponding distribution laws (using Langrange’s method of undetermined

multipliers), partition functions, translational, rotational, vibrational and electronic partition

functions, calculation of thermodynamic properties in terms of partition functions,

applications of partition functions.

15

Text Books

1 Textbook of physical chemistry – W.J.Moore

2 Textbook of physical chemistry – Glasstone

3 Textbook of physical chemistry – P.Atkins

Reference Books

1 Advanced physical chemistry – Gurdeep Raj

2 Principles of Physical Chemistry – Puri, Sharma, Pathania

3 Advanced physical chemistry – J.N.Gurtu, A.Gurtu

4 Thermodynamics for chemists –Glasstone

5 Statistical thermodynamics – M.C.Gupta

6 Physical chemistry – S. Castellian

7 Chemical Kinetics- Laidler

8 Chemical Kinetics – Frost and Pearson

7

GANPAT UNIVERSITY

FACULTY OF SCIENCE Programme Master of Science Branch/Spec. ORGANIC CHEMISTRY



Subject code MCHE1 SST Subject Name Selected Spectroscopic Techniques-I



L TU P TW

Credit 4 0 0 0 4 Theory 40 60 100


Pre-requisites:

Before learning analytical chemistry, student should aware about basic principles and theories of

analytical chemistry, instrumental methods of analysis and other UG level chemistry. Learning Outcome:

Basic knowledge of various spectroscopic techniques and their instrumentation.

Interpretation of organic/inorganic compounds using spectroscopic techniques.

Knowledge of atomic and molecular spectroscopy.

Principle and applications of absorption and emission spectroscopy.

Theory syllabus

Unit Content Hrs

1 UV – Visible spectroscopy: Types of transitions; Factors affecting spectra characteristics

(structural and non-structural); Effect of conjugation; Instrumentation, applications, Calibration

of UV Visible Spectrophotometer as per Pharmacopoeia, Absorption of dienes, polyenes,

carbonyl compounds and α,β- unsaturated carbonyl compounds. Woodward rule and its

application. Aromatic compounds.

IR Spectroscopy: Vibration modes and bond stretching, Absorption of common functional

groups, electrical and steric effects, effects of Hydrogen bonding, Fingerprint region and

interpretation of IR spectra, qualitative interpretation of I.R. spectra, recent advances in I.R.

spectroscopy including FTIR, ATR, etc.

Numerical based on UV-visible and IR.

20

2 X-Ray Diffraction: Diffraction of X-rays by crystals, The Laue equations and Bragg’s law,

Definitions related to crystal structure, crystallographic direction and crystallographic phases,

X-ray diffraction experiments: The powder method and the single crystal method. Reciprocal

lattice, Structure factor and its relation to intensity and Electron density. The phase problem.

Description of procedure for an X-ray structure analysis, Applications of X-ray diffraction.

10

3 Nuclear Magnetic Resonance Spectroscopy: Fundamental principles of NMR (Magnetic

properties of nuclei, applied field and precession, absorption and transition frequency),

chemical shifts concept, factors affecting chemical shift, isotopic nuclei, reference standards,

Proton magnetic spectra, their characteristics, presentation, terms used in describing spectra and

their interpretation (signal no., position, intensity), signal multiplicity phenomena in high

resolution PMR; Spin spin coupling, application of signal splitting and coupling constant data

to interpretation of spectra, decoupling and shift reagent methods. Brief outline of principles of

FT-NMR with reference to 13C NMR: Spin-spin and spin lattice relaxation phenomena, free

induction decay (FID), nuclear overhauser enhancement; 13C NMR spectra; their presentation,

characteristics, interpretation, examples and applications. Brief indication of application of

15

8

magnetic resonance spectral data of other nuclei by modern NMR instruments

4 Mass Spectrometry: Basic principles and brief outline of instrumentation, ion formation and

types: molecular ions, meta stable ions, fragmentation processes, fragmentation patterns and

fragment characteristics in relation to parent structure and functional groups, relative

abundances of isotopes and their contribution to characteristic peaks, mass spectrum; its

characteristics, presentation and interpretation, chemical ionization mass spectrometry, GC-MS

including recent advances in MS, Fast atom bombardment mass spectroscopy.

15

Text Books

1 Instrumental Methods of Analysis – Scoog and West

2 Spectrometric Identification of Organic Compounds – Silverstein et., al.

Reference Books

1 Instrumental Method of Analysis – Willard Dean & Merrit

2 Text Book of Inorganic Chemistry — A.I. Vogel

3 Pharmaceutical Chemistry Vol. I & Vol. II — Becket and Stanlake

4 Pharmaceutical Chemistry Vol. I & Vol. II — L.G.Chatten

5 Text Book of Pharmaceutical Analysis – K.A. Connors

6 Pharmaceutical Analysis — Hiquchi, Bechmman, Hassan

7 Methods of Drug Analysis — Gearien, Graboski

8 Text Book of BioPharmaceutic Analysis — Robert Smith and James Stewart

9 Pharmaceutical Analysis — Modern methods — Part A and B — Munson James. W

10 Quantitative Analysis of Drugs — Garrot

11 Quantitative Analysis of Drugs in Pharmaceutical Formulations — P. D. Sethi

12 IP/BP/USP

13 Application of Absorption Spectroscopy of Organic Compounds — Dyer

14 Analytical Profiles of Drug Substances — Florey [Volume 13]

15 Spectroscopy of Organic Compound – P. 5. Kalsi, Wiely Eastern Ltd., New Delhi

16 Absorption Spectroscopy of Organic Molecules — V. M. Parikh, Addision — Wesley Publishing

Company, London

9

GANPAT UNIVERSITY




Subject code MSEL1 NCH Subject Name Nano-Chemistry



L TU P TW

Credit 2 0 0 0 2 Theory 40 60 100


Pre-requisites:

Basic knowledge and understanding of material science and UG level chemistry.

Learning Outcome:

Understanding of fundamental principles of nanotechnology.

Knowledge of various nanomaterials. Theory syllabus

Unit Content Hrs

1

Fundamentals Of Nanotechnology:

Introduction to Nano-science and Nano-technology, Nano-scale material, implications

for Physics, Chemistry, Engineering & Biology, and Motivation for Nanotechnology

study. Histroy & development of Nano-science and Nano-technology with the emphasis

on history of Nano-metals, Chalcogenides & Boron Nitrite and Carbon Nanomaterials.

15

2

Structures & Classification Of Nanomaterials:

Nano-structures: various types of nano-structures and nano-crystals. Classification of

bulk Nano-structured materials, 0D, 1D, 2D structures- Size Effects-Fraction of Surface

Atoms-specific Surface Energy anf Surface Stress- Effect on the Lattice Parameter-

Photon Density of States Nano-particles, Quantum dots, Nano-wires, Ultra thin films,

Multi-layered materials.

15

Reference Books

1 C.Bre’ chignac P. Houdy M. Lahmani, Nanomaterials and Nanochemistry, Springer Berlin

Heidelberg, Germany (2006).

2 Kenneth J. Klabunde, Nanscale materials in chemistry, Wiley Interscience publications(2001).

3 Hans Lautenshlager, Emulsions, Kosmetik International,(2002).

4 Roque Hidalgo-Alvarez, Structure and Functional properties of Colloids, CRC Press.

5 Richard J. Fann, Chemistry and Technology of Surfactants, Wiley-Blackwell, (2006).

10

GANPAT UNIVERSITY




Subject code MCHE1 PRA Subject Name Practical Module - I



L TU P TW

Credit 0 0 6 0 8 Theory 00 00 00

Hours 0 0 12 0 12 Practical 00 200 200

Pre-requisites:

Before performing these practicals, students have basic knowledge of laboratory chemicals, inorganic

& organic compounds and their properties, theories related to chemical kinetics, conductometry,

organic estimations, apparatus and instruments which are used in performing chemistry practicals.

Learning Outcome:

Understanding of synthetic inorganic chemistry.

Characterization of synthesized inorganic complexes.

Qualitative analysis of inorganic ions.

Knowledge of basic techniques like crystallization, distillation etc.

Understanding of synthetic organic chemistry.

Practical knowledge of conductometer.

Practical knowledge and application of theories. Theory syllabus

Unit Content Hrs/week

1 Inorganic Chemistry Practical 04

(A)Qualitative Analysis. (A mixture containing total 6 radicals and one rare

element) ( Minimum 10 )

(a) Less common metal ions – TI, Mo, W, Ti, Zr, Th, V, U (Three metal ions

in cationic and three anionic form)

(b) Insoluble – oxides, sulphates and halides

(B) Volumetric and Gravimetric Analysis

Separation and determination of two metal ions Cu-Ni, Ni-Zn, Cu-Fe etc. involving

volumetric and gravimetric methods. ( Minimum 3 )

2 Organic Chemistry Practical 04

(A) Preparation of organic compounds : (ALL) i) Nitration

ii) Bromination

iii) Acylation

iv) Reduction

v) Oxidation

vi) Condensation reaction

vii) Diazotization reaction

viii) Friedel-Craft’s reaction

11

ix) Cannizzaro reaction

x) Aldol condensation

(B) Quantitative Estimations (Any Two) a. Estimation of ester

b. Estimation of alcohol/phenol

c. Estimation of glycine

d. Estimation of amide

3 Physical Chemistry Practical 04

(Perform any 10 practical)

(A)Determine the effect on velocity constant of hydrolysis of an ester/ionic

reactions

1. Change of concentration of catalyst (HCl)

2. Change of concentration of reactant (Ester)

3. Change of temperature

4. Effect of ionic strength

5. Reaction in micellar media

(B) Chemical Kinetics

1. To study the reaction between H2O2 and HI at two different temperature and

calculate the temperature coefficient and the energy of activation.

2. To study the rate constant of the reaction between K2S2O8 and KI and study the

influence of ionic strength on the rate constant.

(C) Conductometric Analysis

1. Determine the amount of HCl and CH3COOH in given solution by

conductometric titration against 0.1N NaOH

2. Determine the degree of dissociation and dissociation constant in water for

the acetic acid conductometrically

3. Determine the amount of HCl and CH3COOH in given solution by pH-

metric titration against 0.1N NaOH

(D) Potentiometry

1. Titration of mixture of strong (HCl) and weak (HAC) acid with NaOH / NH4OH

and find the strength of the acids in mixture.

2. Determination of Solubility product of silver halides.

Text Books

1 A text book of practical organic chemistry – A. I. Vogel

Reference Books

1 Vogel’s Qualitative Inorganic Analysis, Revised by G Svehla, Sixth Edition, Longman, 1987

2 Advanced Practical Inorganic Chemistry, Gurdeepraj, Goel Publishing House, 2001

3 Practical organic Chemistry – Mann and Saunders

4 A handbook of quantitative and qualitative analysis – H. T. Clarke

5 Comprehensive Practical Organic Chemistry : Qualitative Analysis V K Ahluwalia & S. Dhingra.

6 Comprehensive Practical Organic Chemistry : Preparations and Quantitative Analysis V K Ahluwalia

& R. Aggarwal Universities Press.

7 An Advance Course in practical Chemistry, A K. Nad, B. Mahapatra and A. Ghoshal.

8 Practical physical chemistry –J.B.Yadav

9 Practicals in physical chemistry – P.S.Sindhu

10 Experimental physical chemistry – R.C.Das, B.Behera

11 Experiments in physical chemistry- P.H.Parsania, F. Karia

13

GANPAT UNIVERSITY

FACULTY OF SCIENCE Programme Master of science Branch/Spec. Chemistry

Semester II Version 2.0.0.0

Effective from Academic Year Effective for the batch Admitted in June 2017

Subject code MCHE2 IOC Subject Name INORGANIC CHEMISTRY-II



L TU P TW

Credit 4 00 00 00 4 Theory 40 60 100

Hours 4 00 00 00 4 Practical 00 00 00

Pre-requisites:

Before studying Inorganic chemistry, all students have basic knowledge of inorganic and organic

compounds, molecular structure, non-transition elements, co-ordination compounds and knowledge

related to UG level chemistry.

Learning Outcome:

Basic knowledge of bonding in the metal complexes.

Knowledge of non-transition elements.

Knowledge on Inorganic polymers.

Understanding of ion exchange, its mechanism and knowledge of Inorganic ion exchangers.

Theory syllabus

Unit Content Hrs

1 Chemistry of Non-Transition Elements

General discussion on the Properties of the non – transition elements, special features of

individual elements, synthesis, properties and structure of halides and oxides of the non –

transition elements, polymorphism in carbon, phosphorous and sulphur, synthesis,

properties and structure of boranes, carboranes, silicates, carbides, phosphazenes, sulphur,

- nitrogen compounds, peroxo compounds of boron, carbon, sulphure, structure and

bonding in oxyacids of nitrogen, phosphorous, sulphure and halogens, interhalogens,

pseudohalides

15

2 Solid State Reaction:

General principles, experimental procedure, co-precipitation as a precursor to solid state

reaction, kinetics of solid state reactions.

Crystal Defects and Non- Stoichiometry:

Perfect and imperfect crystal, intrinsic and extrinsic defects – point defects, line and plane

defects, vacancies – Schottky defects and frenkel defects. Thermodynamics of Schottky

and frenkel defects formation, Colour centres, non – stoichiometry and defects.

Organic Solids:

Electrically conducting solids, organic charge transfer complex, organic metals, new

superconductor.

15

3 Bio-inorganic Chemistry Metalloporphyrins (enzymes) definition, hemoglobin and myoglobin, cytochrome, vitamin

B12

(cyano cobalamin), zincmetallo enzymes, nitrogen fixation, essential and trace

elements in biological system, biochemistry of non metals K, Na pump (action of bath

ions), toxic metals and their toxicity.

Co-ordination compounds in medicine:

Chelation therapy, gold compounds and rheumatoid arthritis, anticancer drugs –platinum

complexes, gold complexes, metallocenes etc, antimicrobial agents, metal complexes as

radiodiagnostic agents, magnetic resonance imaging.

15

14

4 Organometallic Compounds

Organometallic compounds of transition elements, stability of metal carbon bond in

complexes. Synthesis, uses and structure of organometallic compounds of π bonding

organic ligands, 2-electron ligands, olifinic and acetylinic complexes, compound with 3

electron ligand – allylic complexes, compounds. With 4- electron ligands butadiene

complexes, n4 complexes of cyclopentadiene, compounds with 5 electron ligands –

cyclopantadionyl, compounds with 6 electron ligands, n6 complexes of benzene and its

derivatives.

Role of organometallic compounds in catalytic reaction.

15

Reference Books

1 2 3 4

5

6

7 8 9

10 11

12

Advanced Inorganic Chemistry, F. A. Cotton and Wilkinson, John Wiley,

Inorganic Chemistry, J. E. Huhey, Harpes & Row.

Chemistry of the Elements, N. N. Greenwood and A. Earnshow, Pergamon.

C. E. Harland 1994 Ion exchange theory and practice, 2nd

edn, Royal society of Chemistry Cambridge.

J. Korkisch 1989 Handbook of ion exchange resins, their application to inorganic chemistry CRC Press,

Boca Raton FL.

Principles of Instrumental Analysis” by Douglas A. Skoog, 3rd

Edition, Holt- Saunders International Edition

Advanced Inorganic Chemistry Vol. 1, Gurdeep Raj, Krishna Publication Meerut.

Principles of Bioinorganic Chemistry, S. J. Lippard and J. M. Bers

Bioinorganic Chemistry, I. Bertini, H. B. Gray and S. J. Lippard

Principals of Biooganic Chemistry, S. J. Lippard and J. M. Berg, University Science Books. Bioinorganic

Chemistry, I. Bertini, H. B. Gray, S. J. Lippard and J. S. Valentine, University Science Books.

Inorganic Biochemistry vols I and II ed. G. L. Eichhorn, Elsevier

Advanced Inorganic Chemistry: (Vol.1)Satya Prakash ,Tuli, Basu and Madan; S. Chand

Advanced Inorganic Chemistry Vol. 1, Gurdeep Raj, Goel Publishing House,23rd Edition(1998)

Essential of Bioinorganic Chemistry, By Neerja Gupta , Monal Singh

15

GANPAT UNIVERSITY




Subject code MCHE2 ORC Subject Name Organic Chemistry-II



L TU P TW

Credit 4 0 0 0 4 Theory 40 60 100


Pre-requisites:

Before studying organic chemistry, all students should have basic knowledge of organic compounds,

general organic chemistry, reactive intermediates and reaction mechanisms and other UG level

organic chemistry. Learning Outcome:

Knowledge of reaction mechanisms and general organic chemistry.

Knowledge of aromatic substitution, addition, elimination and free radical reactions.

Theory syllabus

Unit Content Hrs

1

(A) Aromatic Electrophilic Substitution Reactions

The arenium ion mechanism, orientation and reactivity, energy profile diagrams. The

ortho/para ratio, ipso attack, orientation in other ring systems. Quantitative treatment of

reactivity in substrates and electrophiles. Diazonium coupling, Vilsmeir reaction, Gatterman-

koch reaction.

(B) Aromatic Nucleophilic Substitution Reactions

The SNAr SN1, benzyne and SN1 Mechanism, Reactivity effect of substrate structure, Leaving

group and attacking nucleophile. The Von Richte , Sommelet – Hauser, and Smiles

Rearrangements.

15

2

(A) Addition Reactions

Mechanistic and stereo-chemical aspect of addition reactions involving electrophiles,

nucleophiles and free radicals. Regio - and Chemo-selectivity, orientation and reactivity.

Addition to cyclo propane ring. Hydrogenation of double and triple bounds. Hydrogenation of

aromatic rings, Hydroboration, Michael Reaction, Sharpless asymmetric epoxidation.

(B) Elimination Reactions

The E2, E1, E1cb mechanisms and their spectrum. Orientation of double bond, Reactivity effect

of substrate structures, attacking base. The leaving group and the medium mechanism and

orientation in pyrolytic elimination.

15

3

Addition to Carbon – Hetero Multiple Bonds

Mechanism of metal hydride reduction of saturated and unsaturated carbonyl compounds, acid

ester and nitriles. Addition of Grignard reagents, organozinc and organolithium reagents to

carbonyl and unsaturated carbonyl compounds. Mechanisms of condensation reactions

involving enolates –Aldol., Knoevenagel, Claisen, Mannich, Benzoin, Perkin, Witting and

Stobbe reactions. Hydrolysis of esters and amides, ammonolysis of esters.

15

16

4

Free Radical Reactions

Types of free radical reactions, Free radical substitution mechanism, mechanism at an

aromatic substrate, neighboring group assistance. Reactivity for aliphatic and aromatic

substrate at a bridgehead. Reactivity in the attacking radicals. The effect of solvents on

reactivity. Allylic Halogenation (NBS), Oxidation of aldehydes to carboxylic acids, auto-

oxidation, coupling of alkynes and arylation of aromatic compounds by diazonium salts,

Sandmeyer reaction, Free radical rearrangement, Hunsdiecker reaction

15

Text Books

1 Advanced organic chemistry-Reactions, Mechanism and Structure by Jerry March, John Wiley and

Sons

Reference Books

1 Advance Organic Chemistry by F.A. Carey and R.J.Sunderg, Plenum.

2 A Guide Book to Mechanism in Organic Chemistry by Peter Sykes & Longman

3 Structure and Mechanism in Organic Chemistry by C.K.Ingold, Comell University Press

4 Organic Chemistry, by R.T.Morrison and R.N.Boyd , Prentice Hall

5 Modern Organic Reactions, by H.O. House, Benjamin.

6 Principles of Organic Synthesis, by R.O.C. Norman and J.M.Coxon, Blackie Academic & Professions

7 Reaction Mechanism in Organic Chemistry by S.M.Mukherji and S.P.Singh, Macmilian

8 Pericyclic Reaction by S.M.Mukherji, Macmilian, India

9 Stereochemistry of Organic Compounds by D.Nasipuri, New Age International Publication

10 Stereochemistry of Organic Compounds by P.S.Kalsi, New Age International Publication

17

GANPAT UNIVERSITY



Effective from Academic Year 2017-2018 Effective for the batch Admitted in July-2017

Subject code MCHE2 PHC Subject Name Physical Chemistry - II



L TU P TW

Credit 04 00 00 00 04 Theory 40 60 100

Hours 04 00 00 00 04 Practical 00 00 00

Pre-requisites:

Before learning Physical chemistry, student should aware about basic principles and theories of

physical chemistry, thermodynamics, electrode potential, chemical reactions and other UG level

chemistry. Learning Outcome:

Understanding the chemistry of macromolecules and their physical properties.

Knowledge of surface chemistry.

Knowledge of electrochemistry and related theories.

Knowledge of nuclear chemistry.

Understanding of thermodynamics.

Understanding of polarization, types of over voltage and related theories.

Theory syllabus

Unit Content Hrs

1

Surface Chemistry :

Adsorption Surface tension, capillary action, pressure deference across curved surface

(Laplace equation), vapour pressure of droplets (Kelvin equation), Adsorption isotherms

(Classical Freundlich, Langmuir, BET equation), Gibbs adsorption isotherm, insoluble

surface films on liquids. Surface active agents, classification of surface active agents,

micellization, hydrophobic interaction, critical micellar concentration (CMC), factors

affecting the CMC of surfactants, numerical.ss

15

2

Macromolecules:

Introduction, Classification of polymers, Molecular weight and size, Number and weight

average molecular weight, Sedimentation method, Viscosity method, Light scattering

method, Ultra centrifugation method, The Zimm plote, Kinetics of polymerization, Free-

radical chain reactions, Cationic polymerization, Anionic polymerization, Free-radical

co-polymerization, Glass transition temperature, Importance of glass transition

temperature, Numerical

15

3

Chemical Thermodynamics :

Recapitulation- Free energy change and equilibria, Calculation of H, S, G and K.

Effect of temperature and pressure dependence for various and types of chemical

reaction partial molar quantities, concept of activity, dependence of activity and activity

coefficients on pressure and temperature, fugacity and its dependence on pressure and

temperature, fugacity in a mixture, determination of activity and fugacity, Numerical

07

18

Nuclear chemistry:

Nuclear properties-nuclear radius, coulombic and nuclear potential radius, nuclear spin

and angular momentum, magnetic moment, nuclear binding energy, nuclear models-

shell model, liquid drop model, Fermi gas model, collective model, radioactive decay,

nuclear reactions, evaporation, spallation, fragmentation, fission and fusion reactions,

accelerators, reaction cross section, use of radioisotopes as tracers.

08

4

4.1 Electrochemistry:

Debye-Huckel theory, Mathematical derivation of Debye-Huckel theory, Tests of

Debye-Huckel theory, The complete Debye-Huckel equation, Debye-Huckel-Bronsted

equation, Debye-Huckel Onsagar equation, Wien effect, Thermodynamics of electrified

interfaces (Lippmann’s equation), Electrical double layer, Theories of structure of

Electrical double layer, Helmoholtz-Perrin theory, Goug-Chapman theory, Stern’s

theory

09

Over-potential:

Decomposition voltage and its measurement, Polarization, Types of over voltages,

Hydrogen overvoltage, Oxygen overvoltage, Metal overvoltage, Measurement of

overvoltage, Factors affecting overvoltage, Theories of overvoltage (mechanism of

Hydrogen over-voltage), Tafel equation, Butle Volmen equation, Diffusion overvoltage

06

Text Books

1 Textbook of physical chemistry – W.J.Moore

2 Textbook of physical chemistry – Glasstone

3 Textbook of physical chemistry – P.Atkins

Reference Books

1 Advanced physical chemistry – Gurdeep Raj

2 Principles of Physical Chemistry – Puri, Sharma, Pathania

3 Advanced physical chemistry – J.N.Gurtu, A.Gurtu

4 Thermodynamics for chemists –Glasstone

5 Surface chemistry – Adamson

6 Surface chemistry – Osipov

7 Polymer chemistry – Gowariker

8 Polymer chemistry – Billmayer

9 Principles of polymer science – Bahadur & Sastry

10 Polymer science & technology – Fried

11 Polymer chemistry- Malcolm P. Stevens

12 Nuclear chemistry – Arniker

13 Nuclear and radio chemistry – J.W. Kannedy, G.Friedlander

14 Electrochemistry – Bockris and Reddy

19

GANPAT UNIVERSITY

FACULTY OF SCIENCE Programme Master of Science Branch/Spec. ORGANIC CHEMISTRY



Subject code MCHE2 SST Subject Name Selected Spectroscopic Techniques-II



L TU P TW

Credit 4 0 0 0 4 Theory 40 60 100


Pre-requisites:

Before studying these techniques, all students should have basic knowledge of organic/inorganic

compounds, general organic, inorganic and physical chemistry.

Learning Outcome:

Basic knowledge of various spectroscopic techniques and their instrumentation.

Knowledge of advance chromatographic techniques.

Interpretation of organic/inorganic compounds using spectroscopic techniques.

Theory syllabus

Unit Content Hrs

1 Raman spectroscopy: Basic Principle, Instrumentation, Application of Raman

spectroscopy, Comparison of IR & Raman spectroscopy, Application of Raman spectra

for inorganic compounds in structure determination, pure rotational, vibrational and

vibrational rotational Raman spectra and selection rule, Advantages and limitations of

Raman spectra.

10

2 Electron Spin Resonance Spectroscopy:

Hyperfine coupling, spin polarization for atoms and transition metal ions, spin-orbit

coupling and significance of g-tensors, application to transition metal complexes (having

one unpaired electron) including biological systems and to inorganic free radicals such

as PH4, F2- and [BH3]

-.

Mossbauer Spectroscopy:

Basic principles, spectral parameters and spectrum display. Application of the technique

to the studies of

(1) Bonding and structures of Fe+2 and Fe+3 compounds including those of intermediate

spin ,

(2) Sn+2 and Sn+4 compounds- nature of M-L bond, coordination number, structure

(3) Detection of oxidation state and inequivalent MB atom

20

3 Atomic Absorption Spectroscopy (AAS), Flame Photometry (FES): Principle of

AAS & FES, Instrumentation of AAS & FES, Relationship between AAS & FES,

Application of AAS & FES, advantages and disadvantages and limitations of AAS &

FES. Atomic Emission Spectroscopy (AES) & Fluorescence Spectroscopy: Principle of

AES & Fluorescence, Instrumentation, Analytical uses of X-ray fluorescence,

Applications.

15

20

4 TGA & DSC: Principles, Introductions of TGA & DSC, Instrumentation of TGA &

DSC, Advantages and disadvantages of TGA & DSC, Applications of TGA & DSC,

Factor affecting of TGS & DSC curves.

15

Text Books

1 Instrumental Methods of Analysis – Scoog and West

2 Instrumental Methods of Chemical Analysis – Gurdeep R. Chatwal & Sham K. Anand

3 Spectrometric Identification of Organic Compounds – Silverstein et., al.

Reference Books

1 Instrumental Method of Analysis – Willard Dean & Merrit

2 Text Book of Inorganic Chemistry — A.I. Vogel

3 Pharmaceutical Chemistry Vol. I & Vol. II — Becket and Stanlake

4 Pharmaceutical Chemistry Vol. I & Vol. II — L.G.Chatten

5 Text Book of Pharmaceutical Analysis – K.A. Connors

6 Pharmaceutical Analysis — Hiquchi, Bechmman, Hassan

7 Methods of Drug Analysis — Gearien, Graboski

8 Text Book of BioPharmaceutic Analysis — Robert Smith and James Stewart

9 Pharmaceutical Analysis — Modern methods — Part A and B — Munson James. W

10 Quantitative Analysis of Drugs — Garrot

11 Quantitative Analysis of Drugs in Pharmaceutical Formulations — P. D. Sethi

12 IP/BP/USP

13 Application of Absorption Spectroscopy of Organic Compounds — Dyer

14 Analytical Profiles of Drug Substances — Florey [Volume 13]

15 Spectroscopy of Organic Compound – P. 5. Kalsi, Wiely Eastern Ltd., New Delhi

16 Absorption Spectroscopy of Organic Molecules — V. M. Parikh, Addision — Wesley

Publishing Company, London

21

GANPAT UNIVERSITY




Subject code MSEL2 RMD Subject Name Research Methodology


(Per week) Lecture(DT)

Practical(Lab.)

Total CE SEE Total

L TU P TW

Credit 02 00 00 00 02 Theory 40 60 100

Hours 02 00 00 00 02 Practical 00 00 00

Pre-requisites:

Before studying these techniques, all students should have basic knowledge of Research

Methodology Learning Outcome:

Basic concepts of research, Selecting the problem , literature survey.

Knowledge of different types of research method and methodology. Theory syllabus

Unit Content Hrs

1

Research - meaning, purpose, types (educational, clinical, experimental,

historical descriptive, basic, applied and patent oriented research), & objective of

research.Literature survey-use of library, books and journals – MEDLINE - internet,

patent search,and reprints of articles as a source for literature survey.

Selecting a problem and preparing research proposals,Methods and tools used in

research –Qualitative & quantitative studies, Simple data organization & descriptive

data analysis, Limitation & sources of error, Inquiries in form of questionnaire, etc

Documentation- “How” of documentation, Techniques of documentation,

Importance of documentation, Use of computer packages in documentation.

15

2

The Research Report Paper writing/ thesis writing: Title –title of project with

authors name, Abstract- statement of the problem, background list in brief, purpose &

scope, Key Words, Methodology - subject, apparatus, instrumentation & procedure,

Results- tables, graphs, figures & statistical presentation. Discussion support or non

support of hypothesis, practical & theoretical implications, Conclusion,

Acknowledgements, References, Errata, Importance of Spell check for entire project,

Uses of footnotes, Presentation (especially for oral presentation), Introduction and

importance, types of different skills, contained, format of model, poster, gestures, eye

contact, facial expressions, stage fright, volume- pitch, speed, pause & language,

visual aids & seating, questionnaire, etc.

Cost analysis of the project – cost incurred on raw materials, procedure,

instrumentations and human resources. Sources for procurement research grants –

international and national agencies, government and private bodies. Industrial -

institution interaction- industrial projects, their feasibility reports, interaction with

industries.

15

Reference Books

22

1 Research In Education- John V. Best, John V. Kahn 10th edition, Allyn & Bacon Publisher,

2005

2 Practical Introduction of copyright.by Gavin Mcfarlane, McGraw-Hill Inc.,US, 1982

3 Thesis projects in Science & Engineering – Richard M. Davis, St. Martin's Press, 1979

4 Assignment And Thesis Writing, Jonathan Anderson, Millicent Poole, Juta Academic

Publisher, 4th ed, 2008

5 Writing a technical paper- Donald H. Menzel, Mcgraw Hill Higher Education, 1961

6 Effective Business Report Writing –Leland Brown, Prentice Hall College Div, 4th ed., 1961

7 Manual for evaluation of industrial projects, by United Nations Industrial Development

Organization.; Vienna: United Nations Industrial Development Organization, United Nations,

1986

8 Manual for the preparation of industrial feasibility studies, United Nations; Rev Exp Su

edition, 1991

9 Biomedical Research by G. Jagadeesh, Sreekant Murthy, Y.K. Gupta and Amitabh Prakash,

2010

23

GANPAT UNIVERSITY




Subject code MCHA2 PRA Subject Name Practical Module - II



L TU P TW

Credit 0 0 8 0 8 Theory 00 00 00

Hours 0 0 12 0 12 Practical 00 200 200

Pre-requisites:

Before performing these practicals, students have basic knowledge of laboratory chemicals, inorganic & organic compounds and their properties, theories related to chemical kinetics, conductometry, organic estimations, apparatus and instruments which are used in performing chemistry practicals.

Learning Outcome:

Understanding of synthetic inorganic chemistry.

Characterization of synthesized inorganic complexes.

Qualitative analysis of inorganic ions.

Knowledge of basic techniques like chromatographic techniques.

Understanding of separation and identification of organic compounds.

Practical knowledge of conductometer, colorimeter, potentiometer and polarimeter.

Practical knowledge and application of theories.

Theory syllabus

Unit Content Hrs/week

1 Inorganic Chemistry Practical 04

(A) Preparation and determination of purity

Preparation and determination of purity of double and complex salts. At least

ten preparations should be done. Synthesis Of Metal Complexes, Double Salts

And Estimation By Gravimetry or volumetric.

1.Hexa ammine nickel(II) chloride.

2.Ferrous ammonium sulphate.

3.Mercury tetrathiocyanatocobaltate.

4.Tris-acetylacetonato Manganese(II) chloride.

5.Pottasiumtrioxalatoferrate

6.Prussian blue

7.Hexaure chromic chloride.

8.Tetra ammine copper sulphate

9.Cis – trans- bis oxalate, diaquo chromate(III)

10.Ni (dmg)2

(B)Chromatography (Minimum Five) Separation of cations and anions by :

(a) Paper Chromatography

(b) Column Chromatography - Ion Exchange

2 Organic Chemistry Practical 04

24

(A) Qualitative Analysis Of Organic Mixture (Minimum 12)

Mixture analysis: ternary mixture to be given. (S+S+S) or (L+L+L). Type

determination. Separation by physical and chemical methods. (both permitted

in case of liquids) (minimum 5 ether separation)

3 Physical Chemistry Practical 04

(Perform any 10 practical)

1. To study the absorption of Acetic Acid on Charcoal and prove the

validity of freundlich equation.

2. To determination of molecular weight of high polymer (i.e.

polystyrene) by Viscosity measurement.

3. To determine the distribution coefficient of Iodine between

CCl4/CHCl3 & water at a given temperature.

4. To determine the distribution coefficient of acetic acid between

Benzene & water at a given temperature.

5. Determine the amount of HCl and H2C2O4 in given solution by

conductometric titration against 0.1N NaOH

6. To determine the Solubility product and solubility of sparingly soluble

salt of BaSO4 by Conductometry.

7. Determine the instability constant of the complex ions between

Fe3+and salicylic acid by Job’s method (spectrophotometry)

8. To determine the concentration of unknown solution from given

KMnO4 solution by Colorimetry.

9. Determine the specifir rotation of given substance (d-Glucose/d-

Sucrose) by polarimeter

10. Determine the rate constant for hydrolysis of inversion of

canesugar/ d-sucrose using polarimeter 11. To determine the solubility of AgCl, Agbr, AgS, Ag2CrO4 using

potentiometer.

12. Redox titration Ferrous ammonium sulfate –KMnO4 , K2Cr2O7 using

potentiometer.

Text Books

1 A text book of practical organic chemistry – A. I. Vogel

2 Textbook of Quantitative Chemical Analysis, A. I. Vogel 6th

Edition, 2002.

Reference Books

1 Qualitative Inorganic Analysis. – A. I. Vogel, 6th Edition revised by G. Svehla ELBS – London

2 Qualitative Chemistry semi micro analysis – edited by P. K. Agasyan CBS Publisher-Delhi.

3 Advanced Practical Inorganic Chemistry, Gurdeepraj, Goel Publishing House, 2001

4 An Advanced Course in Practical Chemistry, A.K. Nad, B. Mahapatra, A. Ghosal, New Central

Book Agency, 2004

5 Practical organic Chemistry – Mann and Saunders

6 A handbook of quantitative and qualitative analysis – H. T. Clarke

7 Comprehensive Practical Organic Chemistry: Qualitative Analysis V K Ahluwalia & S. Dhingra.

8 Comprehensive Practical Organic Chemistry: Preparations and Quantitative Analysis V K

Ahluwalia & R. Aggarwal Universities Press.

9 An Advance Course in practical Chemistry, A K. Nad, B. Mahapatra and A. Ghoshal.

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GANPAT UNIVERSITY · 2017. 5. 13. · Quantum chemistry by R K Prasad Co -ordination chemistry by...

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Transcript of GANPAT UNIVERSITY · 2017. 5. 13. · Quantum chemistry by R K Prasad Co -ordination chemistry by...