FREEZE DRYER - LABFREEZ - Laboratory & Industry ... · PDF filespace among common sample tray...

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Transcript of FREEZE DRYER - LABFREEZ - Laboratory & Industry ... · PDF filespace among common sample tray...

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CONTENTS

FD SeriesLab Scale Freeze Dryer (Lyophilizer) .................................................................................................... 3

LAB-Series Lab Freeze Dryer (Lyophilizer) .......................................................................................................... 9

FD Series Pilot scale automatic freeze dryer ...................................................................................................... 13

FD-P Series Process Freeze Dryer .................................................................................................................. 21

FD-FP series Vacuum Freeze Dryer (Lyophilizer) ............................................................................................... 24

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FDSERIESLab Freeze Dryer/Lyophilizer

FD SeriesLab ScaleFreeze Dryer(Lyophilizer)DESCRIPTIONVacuum freezing dryer is widely used in the medical, pharmaceutical, biological, chemical and food and other fields, FD series is suitable for laboratory use or low-volume production to meet the requirements of most laboratories conventional lyophilization.

FEATURES Microprocessor control & LCD touch display which

can display drying curve, vacuum, condenser temp., run time, ambient temperature.

Pre-freezing function for samples. Large refrigerating capacity and slight noise of

DANFOSS(SECOP) compressor with CFC-FREE refrigerant.

304 stainless steel of condenser, table-top, racks & shelves to ensure corrosion-resistant and easy to clean; shelves height adjustable.

Transparent drying chamber is safe and easy to observe;

Novel design, small size and easy operation; For water based samples, the -55°C condenser is the

perfect choice with effective cost. For samples containing solvents or with low eutectic points, the -80 C dual cascade refrigeration condenser provides maximum performance(optional).

For labs that needs quick turn-around, electric heating defrost is optional. Nitrogen inflation valve is available. It includes the following types: Normal type, Top-press type, multi-manifold T type and multi-manifold Top-press type to meet the

various requirements. Normal type suitable for bulk raw products like food, fruit, herbal medicine and other bio material, Top-press(stoppering) type suitable for vials comes with cap, to stoppering caps into the vials.

CE/ISO 9001 13485 14001 certificated.

FD-10 Bench-top typeModel FD-10-R FD-10-MR FD-10-TP FD-10-MTP FD-10-MT

Image

Dry chamber size (D*H) Ф260×430mm Ф260×465mm Ф260×490mm Ф260×540mm /

Total shelf area 0.12 m2 0.12 m2 0.08m2 0.08m2 /

Shelf size(mm) Ф200*4pcs Ф200*4pcs Ф180 * 3pcs Ф180 * 3pcs /

Shelf space height (mm) 70 70 70 70 /

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FDSERIESLab Freeze Dryer/Lyophilizer

Shelf number 4 pcs 4 pcs 3 pcs 3 pcs /

Trays number 4 pcs 4 pcs 3 pcs 3 pcs /

Vials load

capacity

Ф12mm 920 Pcs 920 Pcs 560 Pcs 560 Pcs24 ports

430×480mm (H*L)Ф16mm 480 Pcs 480 Pcs 285 Pcs 285 Pcs

Ф22mm 260 Pcs 260 Pcs 165 Pcs 165 Pcs

Sample load capacity 1.2L 1.2L 0.8L 0.8L /

Flask / 8 pcs / 8 pcs /

Dry rack Included Included Included Included /

Cold trap rack Included Included Included Included Included

Condenser Temp. <-55°C (-80°C or even lower is optional)

Cold trap size. Ф215 * 140 mm (Depth * Height)

Ice remove capacity 3~4kg/24hours

Cold type Air-cooled

Defrost type Natural (Electric is optional)

Ultimate Vacuum <5 Pa (empty)

Vacuum pump Included

Pump rate 2L/S

Install Power 970W

Voltage 220v/50Hz or 110v/60Hz

Dimensions 460*625* (370+430)(mm)

Weight 100 kg 110kg 105kg 120kg 65kg

FD-12 FLOOR TYPEModel FD-12-R FD-12-MR FD-12-TP FD-12-MTP FD-12-MTImage

Dry chamber size (D*H) Ф260×430mm Ф260×465mm Ф260×490mm Ф260×540mm /

Total shelf area 0.12 m2 0.12 m2 0.08 m2 0.08m2 /

Shelf size (mm) Ф200*4pcs Ф200 * 4pcs Ф180 * 3pcs Ф180 * 3pcs /

Shelf space height (mm) 70 70 70 70 /

Vials load quantity

Ф12mm 920 Pcs 920 Pcs 560 Pcs 560 Pcs24 ports

430×480mm (H*L)Ф16mm 480 Pcs 480 Pcs 285 Pcs 285 Pcs

Ф22mm 260 Pcs 260 Pcs 165 Pcs 165 Pcs

Sample load capacity 1.2L 1.2L 0.8L 0.8L /

Flask / 8 pcs / 8 pcs /

Dry rack Included Included Included Included /

Cold trap rack Included Included Included Included Included

Condenser temp. <-55°C (-80°C or even lower is optional)

Cold trap size Ф215 * 140 mm (Depth * Height)

Ice remove capacity 4 Kg/24h

Cold type Air-cooled

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FDSERIESLab Freeze Dryer/Lyophilizer

Defrost type Natural (Electric is optional)

Ultimate Vacuum <5 Pa

Vacuum pump Included

Pump rate 2L/S

Install Power 970 W

Voltage 220v/50Hz or 110v/60Hz

Dimensions 460×556×(720+465)(mm)

Weight 120 kg 135kg 130kg 140kg 76 kg

FD-18 FLOOR TYPEModel FD-18-R FD-18-MR FD-18-TP FD-18-MTP FD-18-MT

Image

Dry chamber size (D*H) Ф300×445mm Ф300×465mm Ф300×540mm Ф300×570mm /

Total shelf area0.18 m2

0.27 m2

0.18 m2

0.27 m2

0.09 m2 0.09 m2 /

Shelf size (mm)Ф240 * 4pcs

Ф240 * 6pcs

Ф240 * 4pcs

Ф240 * 6pcsФ200 * 3pcs Ф200 * 3pcs

/

Shelf space height (mm)70

50

70

5070 70

/

Vials load capacity

Ф12mm1320 Pcs

1980 pcs

1320 Pcs

1980 pcs990 Pcs 990 Pcs 24 ports

T-manifold

430×480mm (H*L)

Flask rack:

610×600mm

Ф16mm740 Pcs1110 pcs

740 Pcs1110 pcs

555 Pcs 555 Pcs

Ф22mm360 Pcs

540 pcs

360 Pcs

540 pcs270 Pcs 270 Pcs

Sample load capacity1.8L

2.7L

1.8L

2.7L0.9L 0.9L

Flask / 8 pcs / 8 pcs /

Dry rack Included Included Included Included /

Cold trap rack Included Included Included Included Included

Condenser Temp. <-60°C (-80°C or even lower is optional)

Cold trap size Ф270 * 400 mm (Depth * Height)

Ice capture capability 6 Kg/24h

Cold type Air-cooled

Defrost type Natural (Electric is optional)

Ultimate Vacuum <5 Pa

Vacuum pump Included

Pump rate 4L/S

Power 1400W

Voltage 220v/50Hz or 110v/60Hz

Dimensions 540×610×(963+445)(mm)

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FDSERIESLab Freeze Dryer/Lyophilizer

Weight 170 kg 185kg 185kg 195kg 105 kg

Standard Configuration Stainless steel condenser with opening, stainless steel operation tops, seamless welding with round cornerwhich is anti-corrosion

and easy to clean Stainless steel shelf & rack, 4 or 6 pcs shelves optional, shelf removable and spacing height adjustable Stainless steel pre-cooling rack with metal cover Integrally molded glass dried barrel adopted special plastic will not break Used SECOP (DANFOSS) quality compressor, high performance condenser fan, LCD touch display, history data can be stored,

searched and exported to computer.Model R TP MR MTP MT

Image

Description Normal type Stoppering Manifold Stoppering + Manifold Multi-ports manifold

Freeze Dryer ● ● ● ● ●

Transparent dry chamber

● ● ● ●

Vacuum pump ● ● ● ● ●

Stoppering device ● ●

Manifold Ports 8 ports (28/ 32mm) 8 ports (28/ 32mm) 24 ports

Freezing rack ● ● ● ● ●

Drying rack ● ● ● ●

Tray 4 pcs 3 pcs 4 pcs 3 pcs

FD-10S, FD-12S, FD-18S Series Shelf heating & program controlling (optional) Electric heating element for each shelf, Auto + Manual operation; 36 Segment programs can be set used for kind of different raw material Temperature sensor ensure to monitor temperature of each shelf Data can be export to computer for analysis 7’’ LCD touch display, easy to operate on machine Real-time alarm display and historical alarm query function to facilitate fault diagnosis and equipment maintenance. Users can set the level and password, decentralized operation and management. Sensor calibration to ensure long-term accuracy of the measured value

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FDSERIESLab Freeze Dryer/Lyophilizer

Optional itemsItem No. Item Name Item No. Item Name

FD1001 -80°C Condenser FD10091000 1000ml flask

Fd1002 Defrost dev ice FD1010 Eutectic point test dev ice

FD1003 Refrigerant R404a, R502, R23 and etc FD1011 Vacuum regular dev ice

FD1004 Oil mist filter FD1012 Jar bottle

FD1005 Shelves heating & Program segment control

Can stored 16 programs, each program can be set up 36segments, correct program data in computing, memorize

the drying curve

FD1013 Change to SS316 condenser &

shelves

FD1006 6pcs shelves instead of 4 pcs FD1014 Capacitance type vacuum gauge

FD1007 Leybold vacuum pump FD1015 Backfill filter

FD1008 Anti-back oil dev ice FD1016 Auto backfill / drainage system

FD1009100 100ml flask

FD1009250 250ml flask

FD1009500 500ml flask

Vacuum Pump for FD series freeze dryer

Adapter Quick-release pipe Small-bore pipe Oil mist collector

Specifications of vacuum pump

Model 2XZ-0.5 2XZ-1 2XZ-2C 2XZ-4C 2XZ-6C 2XZ-8C 2XZ-15C

Pumping Speed: L/S 0.5 1 2 4 6 8 15

Ult.

Vacuum

Pa

Without gas ballast ≤6×10-2

With gas ballast ≤6.5 ≤1.33

Speed: r/min(50HZ) 1400

Power Required: Kw 0.18 0.25 0.37 0.55 0.75 1.1 1.5

Diameter of inlet port: mm 16 16 25 25 40 40 40

Temp. rise of pump oil: °C ≯40 ≯45 ≯45 ≯65 ≯70

Oil capacity : L 0.60 0.70 0.10 1.2 2.0 3.0 4.0

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FDSERIESLab Freeze Dryer/Lyophilizer

Overall Dimensions: mm

447

168260

469

168260

514

168282

514

168282

565

200342

650

240430

770

240430

Weight: kg 16 17 20 22 40 60 75

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LABSERIES Standard Freeze Dryer/Lyophilizer

LAB-Series LabFreeze Dryer (Lyophilizer)Features Touch LCD display with microprocessor controller, easy to use. Dry chamber using aircraft grade acry lic materials, non-adhesive, high strength, and no leaks.

Condenser pre-cooling function.

Used DANFOSS compressor.

Vacuum pump in Japan or Korea brand, with oil-mist filter can trapping oil mist in the exhaust

gas, reduce env ironmental and health hazards. Can charge nitrogen or inert gas to save after dry ing.

Programmable, freezing, dry ing and defrosting will be program controlled.

Automatic control system: Temperature heating control for each shelves, heating circulation

monitoring protect, fuzzy PID control algorithm.

Defrost system: Auto Non-electric heating defrost, more safety and fast. Vacuum regular system: vacuum degree regular in sublimation and dry ing process to avoid

special material foaming or blowing, accelerate lyophilized efficiency (Optional)

Pulse backfill system: slow, medium, fast three kinds of backfilling mode selection, avoiding the

granular material and flocculent material being blown out effective loss problem inflatable

pro duce. (Optional) Automatic drainage system: interlock with vacuum system after draining to prevent any

failure in vacuum system. (Optional)

Can be work in automatic or manual operation, manual mode is used to explore the process

parameters, automatic mode for process maturity.

Data recording system: 1) data can be stored in machine in 3 months; 2) External U-disk storage (Optional); 3) PC-database storage (Optional)

Monitoring system: real time system temperature and vacuum degree monitored, acquisition

frequency 50ms / time.

Lyophilization process recipe storage function: can store 500 set of fixed or user-defined

lyophilized formulation process. PC remote monitor system: remote monitor working status of machine, max 1.5km distance

(Optional)

Eutectic point test function (Optional)

Calibration function: temperature and vacuum calibration ensures long-term accuracy of the

measured values. Freeze-dry ing curve searchable.

Safety Protection Over-current protection

Over-load protection Over-heating of temperature

Vacuum defense in processing

36V safety voltage for heating system

Vacuum pump protection

Configuration Instruction

Freeze dryer with manifold & stoppering

system

Freeze dryer with -80°C condenser

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LABSERIES Standard Freeze Dryer/Lyophilizer

Normal type(R): suitable for bulk material Stoppering type(S): suitable for sealing

v ials material

Flask-mount type(F): suitable for

external flask material

Stoppering with flask-mount type(FS):

suitable for bulk, external flask and v ials material

T-manifold type(T): Suitable for

external v ials or flasks material

-80°C condenser type

SpecificationsModel LAB-1R-50

LAB-1R-80LAB-1S-50LAB-1S-80

LAB-1F-50LAB-1F-80

LAB-1FS-50LAB-1FS-80

LAB-1T-50LAB-1T-80

Type Normal Stoppering Flask-manifold Stoppering & Flask-

manifold

T-manifold

Control Programmed Programmed Programmed Programmed Programmed

Display LCD touch LCD touch LCD touch LCD touch LCD touch

Condenser temperature

-55°C

-85°C

-55°C

-85°C

-55°C

-85°C

-55°C

-85°C

-55°C

-85°C

Water/ice capture

3L

4L

3L

4L

3L

4L

3L

4L

3L

4L

Compressor power

7/8HP

2/3HP * 2

7/8HP

2/3HP * 2

7/8HP

2/3HP * 2

7/8HP

2/3HP * 2

7/8HP

2/3HP * 2

Defrost Yes Yes Yes Yes Yes

Dry area (m2) 0.12 0.08 0.12 0.08 -

Shelf 4 pcs 3 pcs 4 pcs 3 pcs -

Vacuum < 8 Pa < 8 Pa < 8 Pa < 8 Pa < 8 Pa

Power 900W

1400W

900W

1400W

900W

1400W

900W

1400W

900W

1400W

Voltage 220/50

110/60

220/50

110/60

220/50

110/60

220/50

110/60

220/50

110/60

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LABSERIES Standard Freeze Dryer/Lyophilizer

Dimensions(W*D*H)mm

470*600*400640*640*1000

470*600*400640*640*1000

470*600*400640*640*1000

470*600*400640*640*1000

470*600*400640*640*1000

OptionalItem ref. Item name Item ref. Item name

LAB10001 Vacuum regular system, Vacuum trimming needle

* 1 + v acuum solenoid valve +1

LAB10024 Paperless recorder, with USB interface

LAB10002 Eutectic point tester (economic ty pe), measuring

temperature & resistance v alue

LAB10025 Remote controlling & monitoring system, RS485

LAB10003 Eutectic point tester (standard), measuring

temperature & resistance v alue online & offline,

w ith softw are

LAB10026 Anti-back oil solenoid v alve, SEGV brand

LAB10004 T ty pe 16 port manifold LAB10027 6 shelv es with tray dry chamber

LAB10005 T ty pe 24 port manifold LAB10028 8 shelv es with tray dry chamber

LAB10006 T ty pe 52 port manifold LAB10029 4 shelv es with trays, 12 port manifold-flasks

LAB10007 T ty pe 104 port manifold LAB10030 6 shelv es with trays, 12 port manifold-flasks

LAB10008 Ampoules sealer, sealing torch with tank LAB10031 8 shelv es with trays, 12 port manifold-flasks

LAB10009 Vial capper, suitable for 12~30mm LAB10032 3 shelv es with trays, 12 port manifold-flasks with

stoppering dev ice

LAB10010 Jars adapter (Wide neck) LAB10033 Auto w ater drain dev ice, include solenoid valve, drain

pipe & interface

LAB10011 Pulse backfill system, Backfill solenoid valve *1+

pipe and adapter

LAB10034 Mini dot matrix printer

LAB10012 Backfill filter, 0.2u filter LAB10035 Oil mist filter, SEGV

LAB10013 Backfill interface, USA APG, 8mm LAB10036 Oil mist filter, BWVAC

LAB10014 PC-database storing system LAB10037 Oil mist filter, ULVAC

LAB10015 U-disk data recording system, for online/offline

analy sis

LAB10038 Oil mist filter, Ley bold

LAB10016 BWVAC Vacuum pump 1.5L/S LAB10039 ULVAC Vacuum pump 1L/S

LAB10017 BWVAC Vacuum pump 3L/S LAB10040 ULVAC Vacuum pump 2L/S

LAB10018 BWVAC Vacuum pump 6L/S LAB10041 ULVAC Vacuum pump 4L/S

LAB10019 BWVAC Vacuum pump 8L/S LAB10042 Sample temperature monitor, display range -50~100°C

LAB10020 Ley bold Vacuum pump 2L/S

LAB10021 Ley bold Vacuum pump 4L/S

LAB10022 Ley bold Vacuum pump 6L/S

LAB10023 Ley bold Vacuum pump 8L/S

Built-in freezing container Ampoules sealer Oil-mist filter 6~8 shelves with dry chamber

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LABSERIES Standard Freeze Dryer/Lyophilizer

Eutectic point tester Vial capperLeybold

vacuum pump6~8 shelves with dry chamber

and flaks mount

T-16/24/52/104 manifold Jars adapter Oil anti-back system Backfill filter

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FDSERIES Pilot Freeze Dryer/Lyophilizer

FD Series Pilot scale automaticfreeze dryer

Features:Chamber Rectangular type dry chamber, Pre-freezing, drying in same chamber without any manual operation. Drying chamber & shelves made by polished SS 304 or material contact parts SS316 is optional, adopted high strength, high

transmittance plexiglass door, easy to observe, inside round corner, easy to clean. Oil circulation heating type with high temperature precision control, usually suitable for medical, bio field, electric heating type

suitable for food field. GUNDFOS shielded circulating pump and PID control electric heating component; circulation liquid used Low-temperature low-

viscosity silicone oil. Shelves heating system uses safe voltage, while heating rate controllable. (Electric heating type)

Condenser (cold trap) Made by SS304 drum-type cold trap, with high transmittance plexiglass door, Integrity or separately condenser and chamber

can be chosen. Patented gas diversion technology, cold trapping ice even, ice-catching ability.

Refrigeration Dual-stage cooling, famous hermetic compressor which is low noise, capillary throttling technology, air-cooled or water-cooled

is available. Brazed plate heat exchanger. Environmental-friendly refrigerant.

Control Flexible manual + automatic control, manual groping process, automatic

batch production. PLC control with 7’ LCD touch graphic display, can be operated in auto,

semi-auto and manual mode. Shelf temperature adjustable, controllable, explore suitable for pilot and

production processes.

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FDSERIES Pilot Freeze Dryer/Lyophilizer

32 programs, each program can be set as 36 segments, curve can be stored, processing parameters can be modified in real time.

Built with recorder, with USB interface data can be exported to computer for analysis, FD-LYO software & computer is optional for controlling by remote way.

sensor calibration function, to ensure long-term use of the accuracy of the measured value.

Real-time alarm display and historical alarm inquiry function, convenient fault diagnosis and equipment maintenance.

Users can set the level and password, decentralized operation and management.

Vacuum Two-stage rotary vane vacuum pump, vacuum is automatic adjust and can be set (optional). Ultimate vacuum can reach 5 Pa, in order to reach highest vacuum, Leybold brand vacuum pump is optional.

Others Normal type suitable for bulk raw products like food, fruit, herbal medicine and bio material. Stoppering type suitable for vials

comes with cap, to stoppering caps into the vials. Inflatable (water) valve with a safety diaphragm valve can be connected to the inert gas source, dry and filled with inert gas, to

extend the shelf life of the material. CE/ISO 9001 13485 14001 certificated. Can be conforms to GMP standard.

Main characteristics:FD-10F Series

FD-10F SeriesModel

FD-10F-R (Silicon oil heating)FD-10-RE (Electric heating)

FD-10F-TP (Silicon oil heating)FD-10F-TPE (Electric heating)

Specification Normal With stoppering

Picture

Drying chamber

Shelf area 0.2 m2 0.1 m2

Shelf quantity 2 pcs 1pcShelf temp. range -70°C ~ +65°C

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FDSERIES Pilot Freeze Dryer/Lyophilizer

-50°C ~ 70°CShelf space height 70mmShelf dimension 400×270mmФ22mmvials(piece) 440 220Ф16mm vials (piece) 868 434Ф12mmvials (piece) 1554 777Tray dimensions 395×265mm 395×265mmTray quantity 2 1Sample loaded capacity 2L 1LStoppering device No YesMaterial SS304 (chamber, shelves, trays)

Condenser

Max temp.≤-80°C

≤-60°C (-80°C is optional)Ice capture capacity 6Kg/24hsDefrost Natural (Electric heating is optional)Material SS304

VacuumVacuum pump IncludedVacuum rate 4L/SVacuum degree ≤5 Pa

Basic parameters

Style of cooling Air-cooledDimension(L*W*H) 655×640×1200mm 655×640×1200mmWeight 210kg 210kgControl method PLC auto + manualInstallation power 2KwVoltage 220V/50Hz (can be change to 110V/60Hz)

FD-20F Series

FD-20F SeriesModel FD-20F-R FD-20F-TP

Specification Regular Top-press

Pictures

Drying chamber

Freeze-drying area 0.3 m2 0.2 m2

Heating method Circulation oil heating Circulation oil heatingShelves quantity 3 pcs 2+1 pcs

Shelves temp. range -50°C ~70°C -50°C ~70°CTemp. difference 1°C 1°CShelves space 70mm 70mm

Dimensions of shelves 400*270 mm 400*270 mmSize of tray 395×265mm * 3 pcs 395×265mm * 2 pcs

Ф22 Bottle (piece) 440 440

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FDSERIES Pilot Freeze Dryer/Lyophilizer

Ф16Bottle (piece) 868 868Ф12 Bottle (piece) 1554 1554

Sample loaded capacity 3L 3LStoppering device No Yes

Material SS304 (chamber, shelves, trays) SS304 (chamber, shelves, trays)

Cold trapCold trap temperature ≤-75°C ≤-75°C

Water-capture capability 6 Kg/24h 6 Kg/24hMaterial SS304 SS304

Basic parameters

Ultimate Vacuum ≤5 Pa ≤5 PaPump rate 4L/s 4L/s

Style of cooling Air Cooling room temperature≤25°CAir Cooling room temperature≤25°C

Power supply 220V/50Hz or 110V/60Hz 220V/50Hz or 110V/60HzPower 3000W 3000WWeight 300kg 310kg

Dimension 770x750x1520 mm 770x750x1650 mm Control method PLC auto + manual PLC auto + manual

FD-30F SeriesFD-30F Series

Model FD-30F-RE FD-30F-R FD-30F-TP

Heating type Electric heatingSilicon oil circulation

heatingSilicon oil circulation

heating

Picture

Drying chamber

Freeze-drying area 0.4 m2 0.4 m2 0.306 m2Shelf quantity 4+1 pcs 4+1 pcs 3+1 pcsShelf temp. range -50 ~ 70°C -50 ~ 70°C -50~70°CTemp. Difference +/-1°C (balance) +/-1°C (balance) +/-1°C (balance)Shelf size 300×340mm 300×340mm 300×340mmSample loaded capacity 4L 4L 3LShelf spacing 50mm 50mm 70mmTray size 295×335mm 295×335mm 295×335mmTray quantity 4 pcs 4 pcs 3 pcsMaterial of chamber Polish SS304 Polish SS304 Polish SS304Material of Shelves Polish SS304 Polish SS304 Polish SS304Material of trays SS304 SS304 SS304

Vial load capacity

(pcs)

Ф22 vials 728 728 546Ф16 vials 1440 1440 1080Ф12vials 2600 2600 1950

Cold trapCold trap temperature ≤-60°C ≤-75°C ≤-75°CIce capture capability 8 Kg/24h 8 Kg/24h 8 Kg/24hDefrost Nature Nature Electric or hot gas

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FDSERIES Pilot Freeze Dryer/Lyophilizer

Cold type Air-cooled Air-cooled Air-cooledMaterial SS304 SS304 SS304

Basic parameters

Style of top-press - - Hydraulic pressureUltimate vacuum ≤ 5 Pa ≤ 5 Pa ≤ 5 PaVacuum rate 6L/S 6L/S 6L/SDimension (mm) 890×660×1210 920×780×1350 1280*900*1630Weight 280 kg 400 kg 450 kg

Voltage Freeze dryer220V/50Hz110V/60HZ

220V/50Hz110V/60HZ

220V/50Hz110V/60HZ

Power 2700W 4500W 5500WControl method

PLC auto + manual

FD-50F SeriesFD-50F Series Model FD-50F-RE FD-50F-R FD-50F-TP

Heating type Electric heating Silicone oil circulation Silicone oil circulation

Picture

Drying chamber Freeze-drying area 0.6 m2 0.7 m2 0.5 m2

Shelf quantity 6 pcs 4+1 pcs 3+1 pcsShelf temp. range -50°C ~70°C -50°C ~70°C -50~70°CTemp. Difference +/-1°C (balance) +/-1°C (balance) +/-1°C (balance)Shelf size 300×340mm 480×360mm 410×410mmShelf spacing 50mm 50mm 70mmSample load capacity 6L 7L 5LTray quantity 6 pcs 4 pcs 3 pcsTray size 295×335mm 475×355mm 405×405mmMaterial of chamber Polish SS304 Polish SS304 Polish SS304Material of Shelves Polish SS304 Polish SS304 Polish SS304Material of trays SS304 SS304 SS304

Vial load capacity Ф22 vials (piece) 1408 1408 1050Ф16 vials (piece) 2728 2728 2058Ф12vials (piece) 4920 4920 3705

Cold trap Cold trap temperature ≤-60°C ≤-75°C ≤-75°CIce capture capability 10 Kg/24h 10 Kg/24h 10 Kg/24hElectric defrost Nature Nature Electric or hot gasCool type Air cooled Air cooled Air cooledMaterial SS304 SS304 SS304

Basic parameters Style of top-press - - Hydraulic pressureUltimate vacuum ≤5Pa ≤5Pa ≤5PaVacuum pump Included Included IncludedPump rate 8L/S 8L/S 8L/S

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FDSERIES Pilot Freeze Dryer/Lyophilizer

Dimension (mm) 890×670×1410 1000×785×1420 1490×850×1620+240Weight 450kg 600kg 800 kgVoltage Freeze dryer 380V±10%50Hz/60Hz 380V±10%50Hz/60Hz 380V±10%50Hz/60HzPower 4500W 5500W 6500W

FD-100F SeriesFD-100F Series Model FD-100F-R FD-100F-TP

Heating type Silicone oil circulation Silicone oil circulation

Picture

Drying chamber

Drying area 1.0 m2 1.15 m2Shelf quantity 6+1 layer 4+1 layerShelf Temp range -50°C ~70°C -50~70°CShelf temp. difference ±1°C (balance) ±1°C (balance)Shelves size 480*360mm 480×600mmTray size 475×355mm 475×595mmTray quantity 6 pcs 4 pcsRaw material loaded capacity 10L 11LHeight space 70mm 70mmMaterial of chamber Polish SS304 Polish SS304Material of Shelves Polish SS304 Polish SS304Material of trays SS304 SS304

Vials load capacityФ22 vials (PCS) 2112 2460Ф16 vials(PCS) 4092 4788Ф12vials (PCS) 7920 8624

Cold trap

Condenser temp. ≤-75°C ≤-70°CCondenser capability 15 Kg/24h 15 Kg/24hDefrost Electric heating Electric heatingMaterial SS304 SS304

Basic parameters

Vacuum pump Included IncludedUltimate Vacuum ≤5 Pa ≤5 PaPump rate 15L/S 15L/SStyle of top-press - Hydraulic pressureCooling type Air cooled Air cooledDimension (mm) 1170×830×1665 1640×1100×1630+350Voltage 3p-380~400V/50Hz 3p-380~400V/50HzInstall Power 6500W 7500WWeight 700kg 1000kg

Control method PLC auto + manual

FD-200F Series

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FDSERIES Pilot Freeze Dryer/Lyophilizer

FD-200F

Series

Model FD-200F-R FD-200F-TP

Heating type Silicone oil circulation Silicone oil circulation

Picture

Dry ing

chamber

Freeze-dry ing area 2.25 m2 1.98 m2

Shelves quantity 5+1pcs 4+1pcs

Shelf Temperature -50°C ~70°C -50°C ~70°C

Shelf Temp. Accuracy ± 1°C ± 1°C

Shelf spacing 80~100mm 80~100mm

Size of shelves 500*900*20 mm 610*810*20 mm

Raw material load capacity (be better) 22L 20L

Material of chamber Polish SS304 Polish SS304

Material of Shelves Polish SS304 Polish SS304

Material of trays SS304 SS304

Vials load capacity

Ф22 v ials (PCS) 4100 3600

Ф16 v ials (PCS) 7800 6800

Ф12 v ials (PCS) 14400 12600

Condenser

Max temperature ≤-75°C ≤-75°C

Water-capture capability 40 Kg/24h 40 Kg/24h

Defrost water soaking water soaking

Material SS304 or SS316 SS304 or SS316

Basic

parameters

Vacuum degree ≤5 Pa ≤5 Pa (Range:1~300Pa)

Dimension 1200*2100*1700 (mm) 1300*3300*2500 (mm)

Max Power 13.5kw 15kw

Weight 2300 kg 2600 kg

Data Process RS232 Interface or USB

Control method PLC auto + manual

Refrigeration

unit

Compressor Bitzer or TECUMSEH, 2 set

Power 7 Kw

Refrigerant R507 & R23

Cooling type Air cooled

Pressure controller DANFOSS

Expansion valve DANFOSS

Optional items for FD Pilot typeItem No. Item Name

FDF1001 Stainless steel shell (SS304 or SS316)

FDF1002 Rotary Device

FDF1003 Control software

FDF1004 PC

FDF1005 Eutectic point tester

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FDSERIES Pilot Freeze Dryer/Lyophilizer

FDF1006 Leybold vacuum pump

FDF1007 Defrost device (for special model)

FDF1008 Air compressor (for Pneumatic door opening)

FDF1009 Vacuum pump solenoid valve

FDF1010 External material change to SS304

FDF1011 Condenser, trays, shelves change to SS316

FDF1012 6 port manifold system (extra port customizable)

FDF1013 Data logger

FDF1014 Backfill filter

FDF1015 Capacitance type vacuum gauge

FDF1016 Vacuum regulation system

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FD-P SERIESProcess Freeze Dryer/Lyophilizer

FD-P Series Process Freeze DryerFor medicine useMain Functions Shelf pre-freezing function. Can be filled with nitrogen or inert

protect machine after working. lyophilized automatic control system:

procedural programming, both freeze-dried and defrost control procedures.

Shelf: adopting international advanced welding technology without leak (three-year warranty).

Lyophilized end point test system: automatic lyophilized end testing parsed end of the drying stage, to ensure that the moisture content of the material to reach the standards.

Vacuum regulator systems: sublimation and vacuum drying process analytical adjustment, avoid special material to foaming & blowing, accelerate lyophilization efficiency.

Pulse backfill system: slow, medium, fast three backfill mode selection, avoiding the issue for the end of the freeze-dried granular material and flocculent inflatable produce effective substances are blown away loss.

Large industrial touch screen, human-computer interaction is good, easy to understand, no instructions are also available for easy operation.

Monitoring system: real-time monitoring system temperature, vacuum, acquisition frequency 50ms / times. Lyophilization process recipe storage function: can store 2000 group fixed or user-defined lyophilized

formulation process. PC remote monitoring system: remote monitoring equipment operating conditions, as far as monitoring

distance 1.5KM. Eutectic point test function (optional). Process data recording system (optional). Calibration function: temperature and vacuum calibration ensures long-term accuracy of the measured

values. Lyophilized curve inquiry function (available temperature and vacuum degree curve, convenient process

optimization and lyophilized effect verification). Features◎ Cabinet: Cabinet design according to GB150-2011 / PED ASME standards, in line with FDA and GMP standards. Internal cabinet with large rounded design, with mirror polished surface, bottom of the box with tilt design, also i n line with CIP and SIP drainage requirements. It can withstand: 0.15Mpa to 0.5Pa full range of positive and negative pressure.

1~5 m2

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FD-P SERIESProcess Freeze Dryer/Lyophilizer

◎ Shelf: adopts international advanced welding process. Internal welding, TIG welding and orbital welding technology ◎ Condenser: with polishing technology, surface bright and smooth. Water vapor channel optimized design to ensure small molecule surge resistance, more efficient water capture. ◎ Refrigeration system uses world famous refrigeration compressors, refrigeration system security and stability. ◎ Vacuum system: vacuum pipe with automatic orbital welding, ensure welding firm appearance. Using helium vacuum leak detector testing to ensure vacuum system to achieve high vacuum requirements. ◎ CIP system CIP system valves and pneumatic actua tors are imported original, to ensure stable operation, safe and reliable. CIP system piping with automatic orbital welding, ensure welding firm appearance. CIP vacuum system piping using helium leak detector testing to ensure vacuum system to achieve high vacuum requirements. water pump imported from Germany to remove residual moisture after cleaning, cleared completely. ◎ SIP system uses a pulsating pre-vacuum steam sterilization, with Fo value display and recording, with complete safety interlock and interlock functions, box comes with a cooling function. Triple overpressure protection, to ensure absolute safety. Case high pressure vessel design, manufacturing process, all components of industrial X-ray machine detected by testing, ensure that the overall firm, resistant to high pressure. Valves are used in place disinfection system temperature up to above 350 °C of the original imports. Pneumatic actuators are imported original, ensure stable operation, safe and reliable. Reign disinfection system with automatic orbital pipe welding, welding to ensure strong and beautiful. SIP system piping using helium vacuum leak detector testing to ensure vacuum system to achieve high vacuum requirements. Remove residual moisture after sterilization imported from Germany, water ring pumps, pumping speed, completely clear. Maximum sterilization temperature up to 150 °C. ◎ Process Control System, meet FDA 21 CFR PART 11 electronic records, electronic signatures cannot be modified requirements. Precisely controlled, repeatable, can be restored. ◎ Plate heat exchanger, using the world-class plate heat exchanger, heat transfer efficiency. SIP type suitable for the use of the pharmaceutical sector. CIP type suitable for use in the field of biological engineering. Common type suitable for industrial, food and other fields use

Safety: Independent Overcurrent protection for various facilities Independent overload protection for various facilities Conditions allow individual facilities operating Heating overtemperature protection Product vacuum freeze-drying process protection

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FD-P SERIESProcess Freeze Dryer/Lyophilizer

Vacuum pump protection System logic interlock Meet the GMP standard Model Shelf

area

(㎡ )

Shelf

qty

Shelf size (mm) Temp. accuracy(°C) Condenser

water capacity

(L)

Vials load

(�22)

Shelf

temp. (°C)

Condenser

temp. (°C)

Power

(KW)

FD-P1 1.08 4+1 450*600 ±1.0 20 2100 -60-80 <-85 9

FD-P2 2.19 4+1 600*900 40 4200 12

FD-P3 3.24 6+1 600*900 60 6300 21

FD-P5 4.86 6+1 900*900 100 9450 24

FD-P7 7.56 7+1 900*1200 150 15750 44

FD-P10 9.72 9+1 900*1200 200 19950 58

FD-P13 12.96 9+1 1200*1200 260 26250 67

FD-P15 16.1 9+1 1200*1490 320 33600 75

FD-P20 19.67 11+1 1200*1490 400 42900 104

FD-P25 25.0 14+1 1200*1490 500 52500 125

FD-P30 31.5 14+1 1490*1490 600 60900 134

FD-P40 42 14+1 1490*1990 800 84000 174

FD-P50 51.0 17+1 1490*1990 1000 105000 210

15 m2 20m2

25m2 40m2

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FD-FP SERIES Process Freeze Dryer/Lyophilizer

FD-FP Series Vacuum Freeze Dryer(Lyophilizer)For food processing

Main application of food freeze dryer:Vacuum freezing and drying technology is currently themost advanced technology for food dehydrationprocessing in the world. Compared with the commonlyused drying method, the freeze-dried food produced withthis technology features long period of quality assurance,good re-hydration nature, good-looking color, good flavor,taste and high content of nutritious components. Thedried food basically remains unchanged in its volume andshape, looks like sponge and has no shrinking. Thisdrying technology can be widely used in process ofvegetables, fruits, condiments, aquatic products,biological products, medicine, beverage, exemplar etc.

Main part of food freeze dryer:FD-FP series vacuum cryogenic drying equipment mainly includes food pre-freezing system, drying bin system, heating system, vacuumsystem, refrigerating system, material conveying system, medium system, pneumatic system, cleaning and sterilizing system.

Main technical parameters of food freeze dryer:Model FD-FP1 FD-FP5 FD-FP10 FD-FP20 FD-FP30 FD-FP40 FD-FP60 FD-FP75 FD-FP90 FD-FP100

Shelf area (m2) 1 5.5 11.4 22.4 35.6 45.6 59.28 74.88 89.8 100

Chamber size

(mm)

Diameter Φ600 Φ1200 Φ2300 Φ2300 Φ2300 Φ2400 Φ2500 Φ2500 Φ2500

Depth 700 1480 1300 2250 3300 4300 3170 4200 5200

Shelf quantity (pcs) 4+1 8+1 10+1 10+1 10+1 10+1 13+1 13+1 13+1

Shelf size

(mm)

W 400 360 600 600 600 600 600 600 600

D 625 1000 950 1900 2850 3800 3800 4800 5800

H 20 20 15 15 15 15 15 15 15

Shelf height space (mm) 60 60 80 80 80 80 80 80 80

Carts quantity (pcs) 0 1 1 2 3 4 4 5 6

Tray size

(mm)

W 395 330 460 460 460 460 460 460 460

D 625 350 640 640 640 640 640 640 640

H 30 20 40 40 40 40 40 40 40

Tray quantity 4 48 40 80 120 160 208 260 312

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FD-FP SERIES Process Freeze Dryer/Lyophilizer

Heating medium Silicone oil

Temp. range (℃) RT -120℃

Ice capture capacity (KG) 20 100 200 400 600 800 1000 1500 2000

Condenser temp. (℃) -50 or -70

Condenser cooling method Direct evaporation

Def rost type Hot water spray

Def rost water capacity (Kg) 230 1000 200 400 600 800 1000 1500 2000

Ultimate vacuum (Pa) 10Pa 10Pa 10Pa 10Pa 10Pa 10Pa 10Pa 10Pa 10Pa

Install power (KW) 6.5 12 24 46 70 85 110 160 200

Cooling ty pe Air cooled Water cooled

Cooling water (T/H) / 8 20 30 40 50 60 80 100

Cooling water pipe diameter (mm) / DN40 DN50 DN50 DN65 DN65 DN65 DN65 DN80

Dimensions (mm)

W 2010 2500 4000 6000 9000 9000 9000 1300 16000

L 1300 1400 2100 2100 2100 2400 2900 2900 2900

H 1720 1600 2300 2300 2300 2600 3200 3200 3600

Weight (T) 1 4.8 8.6 17.5 26 32 40 40 80

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