FIELD OF TESTING : Chemical and Biological Testing · Colour (Saybolt) ASTM D156-15 12. ......

Intertek Testing Services (S) Pte Ltd Certificate No. : LA-1997-0115-A Cargo and Analytical Assessment Singapore Technical Centre Issue No. : 25 1 Seraya Avenue Singapore 628208 Date : 07 February 2018

Page : 1 of 28

FIELD OF TESTING : Chemical and Biological Testing

MATERIALS/ PRODUCTS TESTED

TESTS/PROPERTIES STANDARD METHODS/

TECHNIQUES

I PETROCHEMICALS AND SOLVENTS A. Petrochemicals 1. Acetaldehyde of Vinyl Acetate ASTM D2191-06(12) and Solvents Monomer 2. Total Acid Acceptance ASTM D2942-02(13) 3. Acidity in Volatile Solvent ASTM D1613-17 4. Aldehyde ASTM D2119-09 5. Alkalinity in Acetone ASTM D1614-09 6. Aniline Point (Method A) ASTM D611-12(16) 7. Aromatics ASTM D1319-15 8. Ash ASTM D482-13 9. Chloride content In-House Method TPM 5.13 / Turbidimetric Techniques 10. Colour (Pt-Co Scale) ASTM D1209-05(11) 11. Colour (Saybolt) ASTM D156-15 12. Distillation range IBP and DP ASTM D86-17 ASTM D1078-11 ASTM D850-16 13. Doctor test ASTM D4952-12(17)

Certificate No. : LA-1997-0115-A Issue No. : 25 Date : 07 February 2018 Page : 2 of 28

MATERIALS/ PRODUCTS TESTED

TESTS/PROPERTIES STANDARD METHODS/

TECHNIQUES

14. Flash Point (Tag Close) ASTM D56-16a 15. Free Halogens ASTM D4755-95(15)e1 16. Iron content in Ethylene, Glycols ASTM E202-12 & Propylene Glycol 17. Non-Volatile Matter ASTM D1353-13 18. Permanganate ASTM D1363-06(11) 19. pH ASTM D2110-00(12) 20. Specific Gravity a) Digital Density Meter ASTM D4052-16 IP 365/97(04) ISO 12185-96 b) Hydrometer ASTM D891-09 21. Viscosity, Kinematic ASTM D445-17a IP 71/97 ISO 3104-94 22. Water by Karl Fischer ASTM E1064-16 23. Water Miscibility ASTM D1722-09 24. Acidity in Vinyl Acetate ASTM D2086-08(12) 25. Acidity - Alkalinity of Halogenated ASTM D2989-01(16) Organic Solvents 26. Acidity of Benzene ASTM D847-16 27. Acid Wash Colour of Xylene ASTM D848-14 28. Total Chloride In-House Method TPM 2.71C / Oxidative Microcoulometry ASTM D4929-16 ASTM D5808-09a(14) 29. Copper Corrosion of Industrial ASTM D849-15 Aromatic Hydrocarbons 30. Hydroquinone in Vinyl Acetate ASTM D2193-06(12)


MATERIALS / PRODUCTS TESTED TESTS / PROPERTIES

STANDARD METHODS / TECHNIQUES / EQUIPMENT

31. Iron in Trace Quantities ASTM E394-15 32. Inhibitor (TBC) in Styrene ASTM D4590-13 Monomer 33. MEHQ in Monomeric Acrylate ASTM D3125-06(12) Ester & Acrylate Acid 34. Non-Volatile Matter in ASTM D2109-01(16) Halogenated Organic Solvents & Admixtures 35. Sulphuric Acid Wash ASTM E346-08e1 36. Acid Value ASTM D1045-14 37. Alkalinity as NaOH ASTM 2106-07(12) 38. Appearance ASTM D3741-00(15)e1 39. Bromine Index of Petroleum ASTM D2710-09(13) Hydrocarbons by Electrometric Titration 40. Bromine Index of Aromatic ASTM D5776-14a Hydrocarbons by Electrometric Titration 41. Colour (Pt-Co Scale) – ASTM D2108-10(15) Halogenated Organic Solvents 42. Free Halogens ASTM D4755-95(15)e1 43. FTIR Scan In-House Method TPM 2.177 / FTIR Spectroscopy 44. Hydroxyl Number ASTM D4274-16 45. Odour of Volatile Solvents & ASTM D1296-01(12) Diluents 46. Refractive Index ASTM D1218-12(16) 47. Specific Gravity – Halogenated ASTM D2111-10(15) Organic Solvents


MATERIALS / PRODUCTS TESTED

TESTS / PROPERTIES STANDARD METHODS /

TECHNIQUES / EQUIPMENT

48. Suspended Matter ASTM D4670-17 49. Unsaturation of Polyols ASTM D4671-16 50. Water in Halogenated Organic ASTM D3401-97(12) Solvents 51. Trace Chloride in Aromatics ASTM D5808-09a(14) Hydrocarbons by Oxidative Microcoulometry 52. Carbonyl Number by Chemical UOP 624-14 Analysis 53. Chloride in Petroleum Distillates UOP 779-08 by Microcoulometry 54. Trace Chloride in Liquid ASTM D5194-13 Aromatic Hydrocarbons 55. Trace Quantities of Carbonyl ASTM E411-17a Compounds with 2, 4- Dinitrophenylhydrazine 56. Water in Volatile Solvents (Karl ASTM D1364-02(12) Fischer Reagent Titration Method) 57. *Sulfur Speciation by GC ASTM D5623-94(14) 58. *DHA by High Resolution GC ASTM D6730-01(16) 59. Color of Liquids by Tritimulus ASTM D5386-16 Colorimetry 60. *MTBE by GC ASTM D5441-98(17) 61. Iron by FerroZine Method ASTM E1615-16 62. Ultra Low Nitrogen in Aromatic ASTM D7184-15 Hydrocarbons 63. Total Fluorine, Chlorine and Sulfur ASTM D7359-14a In Aromatic Hydrocarbons and Their Mixtures by CIC Method





64. Determination of Halogenated In-House Method TPM 5.44C / and Sulfur Compounds in C.I.C. Hydrocarbon Samples by Combustion Ion Chromatography (C.I.C.) B. Caustic Soda 1. Carbonate In-House Method TPM 5.14 / Titrimetric techniques 2. Iron In-House Method TPM 5.16 / Colorimetric techniques 3. Hydroxide Content In-House Method TPM 5.14 Titrimetric techniques 4. Sulphate In-House Method TPM 5.17 / Gravimetric techniques 5. Sodium Hydroxide ASTM E291-09, Titrimetric 6. Chloride ASTM E291-09, Potentiometric 7. Iron ASTM E291-09, Photometric 8. Sulphate ASTM E291-09, Gravimetric

C. Ethanol 1. Clarity of Solution USP 32:2009

2. Color of Solution 3. Identification 4. FTIR Scan 5. SG @ 15.56°C 6. Acidity as Acetic Acid 7. Ultra Violet Absorption 8. Volatile Impurities 9. Non-Volatile Residue D. Ethanol Anhydrous 1. Appearance EP 6.0

2. Acidity or Alkalinity 3. Relative Density 4. Absorbance 5. Volatile Impurities 6. Residue on Evaporation

E. Denatured Ethanol 1. * Denatured Ethanol Content by In-house Method TPM 5.81 GC





II PETROLEUM TESTING A. Jet A-1 / Kerosene 1. Colour (Saybolt) ASTM D156-15 2. Total Acidity ASTM D3242-11(17) 3. Aromatics ASTM D1319-15 ASTM D6379-11 4. Olefins Content ASTM D1319-15 5. Total Sulphur ASTM D4294-16e1 IP 336/04(14) 6. Mercaptan Sulphur ASTM D3227-16 7. Distillation Range ASTM D86-17 8. Flash Point, Abel IP 170/14 9. Density / Specific Gravity / ASTM DF-12b(17) API Gravity IP 160/99 ISO 3675-98 ASTM D4052-16 IP 365/97(04) ISO 12185-96 10. Freezing Point ASTM D2386-15e1 11. Kinematic Viscosity @ -20°C ASTM D445-17a IP 71/97 ISO 3104-94 12. Aniline Gravity Product ASTM D611-12(16) ASTM D1298-12b(17) 13. Smoke Point ASTM D1322-15e1 14. Naphthalene Content ASTM D1840-07(17) 15. Copper Corrosion ASTM D130-12 16. Thermal Stability (JFTOT) Filter ASTM D3241-16a Pressure Differential Tube Deposit Rating (Visual)





17. Water Reaction Interface ASTM D1094-07(13) Rating Separation Rating 18. Water Separation Index ASTM D3948-14 Modified (MSEP) 19. Electrical Conductivity ASTM D2624-15 20. Char Value IP 10/12 21. Estimated of Net & Gross Heat of ASTM D4868-17 Combustion ASTM D3338-09(14e2) ASTM D4529-17 22. Existent Gum ASTM D381-12(17) IP 540/08(14) 23. Particle Counter IP 564/13 24. Freezing Point (Auto) IP 529/16 25. Freezing Point (Auto Laser Method) ASTM D7153-15e1 26. Particulate Contamination ASTM D5452-12 27. Heat of Combustion ASTM D4809-13 28. Inorganic Acidity IP 182/06 29. Sulphur ASTM D7039-15a 30. Color by Auto Tritimulus Method ASTM D6045-12(17) 31. * FAME Content by GCMS IP 585/10 32. Trace Elements in Middle ASTM D7111-16 Distillate Fuels by ICP-AES 33. Level of Cleanliness of Aviation IP565-13 Turbine Fuel- Portable Automatic Particle Counter Method 34. Vapor Pressure (VPX) (Triple ASTM D6378-10 Expansion Method)





35. Determination of Halogenated In-House Method TPM 5.44C / and Sulfur Compounds in C.I.C. Hydrocarbon Samples by Combustion Ion Chromatography (C.I.C.) 36. Dynamic Viscosity and Density of ASTM D7042-16e3 Liquids by Stabinger Viscometer B. Mogas / Reformate / 1. Copper Corrosion ASTM D130-12 Pyrolysis Gasoline 2. Distillation Range ASTM D86-17 3. Doctor Test IP 30/07(14) ASTM D4952-12(17) 4. Induction Period / Oxidation Stability ASTM D525-12a 5. Reid Vapour Pressure ASTM D323-15a 6. Sulphur ASTM D4294-16e1 IP 336/04(14) 7. Lead Content – Iodine ASTM D3341-16 Monochloride Method 8. Lead Content IP 224/02(14) 9. Density /Specific Gravity / ASTM D1298-12b(17) API Gravity IP 160/99 ISO 3675-98 ASTM D4052-16 IP 365/97(04) ISO 12185-96 10. Mercaptan Sulphur ASTM D3227-16 11. Aromatics, Olefins ASTM D1319-15 *ASTM D6839-17 12. Research Octane Number ASTM D2699-16e1 13. Motor Octane Number ASTM D2700-16a 14. Front End Octane Number ASTM D2699-16e1





15. * Trace Oxygenated Hydrocarbons In-House Method TPM 5.38 LowOx in Liquid Hydrocarbon Streams by GC (LOWOX) 16. Bromine Number ASTM D1159-07(17) 17. * Hydrocarbon Types, Oxygenated ASTM D6839-17 Compounds, and Benzene in Spark Ignition Engine Fuels 18. Acidity ASTM D974-14e2 19. Phosphorus ASTM D3231-13 20. Vapour Pressure of Petroleum ASTM D5191-15 Products (Mini Method) 21. Lead Content – Atomic ASTM D3237-17 Absorption Spectroscopy 22. Existent Gum ASTM D381-12(17) IP 540/08(14) 23. Corrosive Properties (NACE) TM 0172-01 [NACE International, The Corrosion Society] 24. Determination of Total Sulphur ASTM D5453-16e1 in Light Hydrocarbons, Motor Fuels and Oils by Ultraviolet Fluorescence 25. * Determination of MTBE, ETBE, ASTM D4815-15b TAME, DIPE, tertiary – Amyl Alcohol and C1 to C4 Alcohols in Gasoline by Gas Chromatography 26. * Determination of Benzene, Toluene, ASTM D5580-15 Ethylbenzene, p/m- xylene, o-xylene, C9 and heavier Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography 27. * Paraffin, Naphthene and Aromatic ASTM D5443-14 Hydrocarbon type analysis in Petroleum Distillates through by 200C Multi-Dimensional Gas

Chromatography





28. Manganese (except for Reformate) ASTM D3831-12(17) 29. Heat of Combustion: ASTM ASTM D4809-13 30. *Sulfur Speciation by GC ASTM D5623-94(14) 31. *DHA by High Resolution GC ASTM D6730-01(16) 32. *Oxygenates in Gasoline ASTM D5599-17 33. Sulphur ASTM D7039-15a 34. Chloride by Microcoulometry UOP 779-08 35. Color by Auto Tritimulus Method ASTM D6045-12(17) 36. *MTBE by GC ASTM D5441-98(17) 37. Vapor Pressure (VPX) (Triple ASTM D6378-10 Expansion Method) 38. Determination of Halogenated and In-House Method TPM 5.44C / Sulfur Compounds in Hydrocarbon C.I.C. Samples by Combustion Ion Chromatography (C.I.C.) C. Light Virgin Naphtha / 1. Colour (Saybolt) ASTM D156-15 Naphtha 2. Distillation Range ASTM D86-17 3. Lead Content IP 224/02(14) 4. * Hydrocarbon Types, Oxygenated ASTM D6839-17 Compounds, and Benzene in Spark Ignition Engine Fuels 5. Olefins ASTM D1319-15 6. Reid Vapour Pressure ASTM D323-15a 7. Sulphur ASTM D4294-16e1 IP 336/04(14) 8. Research Octane Number ASTM D2699-16e1





9. Specific Gravity / Density / ASTM D1298-12b(17) API Gravity IP 160/99 ISO 3675-98 ASTM D4052-16 IP 365/97(04) ISO 12185-96 10. Motor Octane Number ASTM D2700-16a 11. Chlorides ASTM D4929-16 12. Aromatics *ASTM D6839-17 ASTM D1319-15 13. * Trace Oxygenated Hydrocarbons In-House Method TPM 5.38 LowOx in Liquid Hydrocarbon Streams by GC (LOWOX) 14. Determination of Trace Nitrogen ASTM D4629-12(17) by Oxidative Combustion 15. Vapour Pressure of Petroleum ASTM D5191-15 Products (Mini Method) 16. Determination of Total Sulphur in ASTM D5453-16e1 Light, Hydrocarbons Motor Fuels and Oils by Ultraviolet Fluorescence 17. Total Mercury and Mercury UOP 938-10 Species in Liquid Hydrocarbons 18. Existent Gum IP 540/08(14) ASTM D381-12(17) 19. Vapor Pressure (VPX) (Triple ASTM D6378-10 Expansion Method) 20. Heat of Combustion ASTM D4809-13 21. *Sulfur Speciation by GC ASTM D5623-94(14) 22. *DHA by High Resolution GC ASTM D6730-01(16) 23. Color by Auto Tritimulus Method ASTM D6045-12(17)





24. Determination of Halogenated and In-House Method TPM 5.44C / Sulfur Compounds in Hydrocarbon C.I.C. Samples by Combustion Ion Chromatography (C.I.C.) D. Fuel Oil / Low Sulphur 1. Ash ASTM D482-13 Wax Residue / Decant Oil / Light Cycle Oil 2. Calorific Value (Fuel Only) ASTM D240-17 3. Conradson Carbon Residue ASTM D189-06(14) 4. Micro Carbon Residue ASTM D4530-15 5. Flash Point, PMCC ASTM D93-16a IP 34/16 ISO 2719-16 6. Pour Point ASTM D97-17a 7. Water by Distillation ASTM D95-13e1

IP 74/00(14) ISO 3733-99 8. Sediment by Extraction ASTM D473-07(17)e1 9. Sulphur ASTM D4294-16e1

IP 336/04(14) 10. Kinematic Viscosity ASTM D445-17a IP 71/97 ISO 3104-94 11. Total Sediment, Existent IP 375/11

ASTM D4870-09(14) 12. Total Sediment, Accelerated IP 390B/11 13. Total Sediment, Potential IP 390A/11 14. Compatibility Test ASTM D4740-04(14) 15. Asphaltenes IP 143/04 16. Water and Sediment ASTM D1796-11(16) 17. Hydrogen Sulphide IP570-15





18. Fusion + Elements In House Method TPM 5.34 I.C.P.E.S IP 377/95(14) ASTM D5184-12(17) 19. Aniline Point ASTM D611-12(16) 20. Trace Nitrogen by Oxidative ASTM D4629-12(17) Combustion 21. Density ASTM D1298-12b(17) IP 160/99 ISO 3675-98 ASTM D4052-16 IP 365/97(04) ISO 12185-96 22. Hydrogen Sulphide ASTM D5705-15 23. Al, Si, V, Ni, Fe, Na, Ca, Zn, & P IP501/05 24. Carbon, Hydrogen & Nitrogen ASTM D5291-16 25. *Simulated Distillation ASTM D2887-16a 26. Heat of Combustion: ASTM D4809-13 27. Asphaltenes ASTM D6560-12 28. *Boiling Point Distribution ASTM D7169-16 29. Sulphur ASTM D7039-15a 30. Chloride by Microcoulometry UOP 779-08 31. Nitrogen ASTM D5762-12(17) 32. n-Heptane Insolubles ASTM D3279-12e1 33. K Factor and Molecular Weight UOP 375-07 Estimation 34. Determination of Halogenated and In-House Method TPM 5.44C / Sulfur Compounds in Hydrocarbon C.I.C. Samples by Combustion Ion Chromatography (C.I.C.)





35. Dynamic Viscosity and Density of ASTM D7042-16e3 Liquids by Stabinger Viscometer 36. Specific Energy ISO 8217-17 Annex H 37. CCAI Calculation ISO 8217-17 Annex C

E. Base Oil 1. Determination of Trace Nitrogen ASTM D4629-12(17) by Oxidative Combustion 2. Water by Karl Fischer ASTM D1533-12 3. Sulphur ASTM D7039-15a 4. Nitrogen ASTM D5762-12(17) 5. Chloride by Microcoulometry UOP 779-08 6. Apparent Viscosity (CCS) ASTM D5293-17a 7. Determination of Halogenated and In-House Method TPM 5.44C / Sulfur Compounds in Hydrocarbon C.I.C. Samples by Combustion Ion Chromatography (C.I.C.)

F. Gas Oil 1. Ash ASTM D482-13 ISO 6245-01 2. Conradson Carbon Residue ASTM D189-06(14) 3. Micro Carbon Residue ASTM D4530-15 ISO 10370-14 4. Colour (ASTM) ASTM D1500-12(17) 5. Cetane Index ASTM D976-06(16) ISO 4264-13 6. Copper Corrosion ASTM D130-12 7. Distillation Range ASTM D86-17 8. Flash Point, PMCC ASTM D93-16a ISO 2719-16 IP 34/16





9. Pour Point ASTM D97-17a ISO 3016-94 10. a) Cloud ASTM D2500-17 b) Cloud Point ISO 3015-92 11. Cold Filter Plugging Point IP 309/16 12. Strong Acid Number ) ASTM D974-14e2 13. Total Acid Number ) 14. Specific Gravity / Density / ASTM D1298-12b(17) API Gravity IP 160/99 ISO 3675-98 ASTM D4052-16 IP 365/97(04) ISO 12185-96 15. Sulphur ASTM D4294-16e1 IP 336/04(14) ASTM D7039-15a ISO 8754-03 16. Kinematic Viscosity ASTM D445-17a IP 71/97 ISO 3104-94 17. Water by Distillation ASTM D95-13e1

IP 74/00(14) ISO 3733-99 18. Oxidation Stability, Accelerated ASTM D2274-14 IP 388/97 ISO 12205-95 19. Particulate Contaminant ASTM D2276-06(14) 20. Water and Sediment ASTM D2709-16 21. Determination of Trace Nitrogen ASTM D4629-12(17) by Oxidation Combustion 22. Aromatics IP 391/07





23. Trace Elements in Middle Distillate ASTM D7111-16 Fuels by ICP-AES 24. Determination of Total Sulphur in ASTM D5453-16e1 Light Hydrocarbons, Motor Fuels and Oils by Ultraviolet Fluorescence 25. Filter Blocking Tendency of IP 387/17 Distillate Fuel Oils ASTM D2068-17 26. Derived Cetane Number ASTM D6890-16e1 27. Kinematic Viscosity at 40°C ASTM D445-17a IP 71/97 ISO 3104-94 28. Total Sediment, Existent ISO 10307-1-09 29. Density at 15°C ASTM D4052-16 ISO 12185-96 ISO 3675-98 30. Aluminium and Silicon ISO 10478-94 31. Lubricity by HFRR IP 450/00 ASTM D6079-11(16) ISO 12156-1-06(E) CEC-F-06-A-96 32. Cloud Point (Auto) ASTM D5771-17 IP 444/09 33. Pour Point (Auto) ASTM D5950-14 34. Heat of Combustion ASTM D4809-13 35. *Boiling Point Distribution ASTM D7169-16 36. CFPP BS EN 116:2015 IP 309/16 ASTM D6371-17 37. Chloride by Microcoulometry UOP 779-08 38. Nitrogen ASTM D5762-12(17)





39. FAME Content by FTIR IP 579/14 EN 14078-14 40. Color by Auto Tritimulus Method ASTM D6045-12(17) 41. Ramsbottom Carbon Residue ASTM D524-15 42. K Factor and Molecular Weight UOP 375-07 Estimation 43. Acid Petroleum Products ASTM D664-17 44.

Cetane Index - Calculated ASTM D4737-10(16)

45.

Determination of Halogenated and Sulfur Compounds in Hydrocarbon Samples by Combustion Ion Chromatography (C.I.C.)

In-House Method TPM 5.44C / C.I.C

46. Dynamic Viscosity and Density of

Liquids by Stabinger Viscometer ASTM D7042-16e3

47. Specific Energy ISO 8217-17 Annex H 48. CCAI Calculation ISO 8217-17 Annex C 49. Particulate Contaminant ASTM D6217-11(16) IP 415/07 50. Free Water and Particulate ASTM D4176-04(14) Contamination in Distillate Fuels (Visual Inspection Procedures)

G. Crude Oil 1. Specific Gravity / Density / API ASTM D1298-12b(17) Gravity IP 160/99 ISO 3675-98 2. Water by Distillation ASTM D4006-16e1 3. Sediment by Extraction ASTM D473-07(17)e1 4. Sediment by Membrane Filtration ASTM D4807-05(15) 5. Water by Karl Fischer ASTM D4377-00(11)





6. Sulphur ASTM D4294-16e1 IP 336/04(14) ASTM D7039-15a 7. Reid Vapour Pressure ASTM D323-15a 8. Water and Sediment ASTM D4007-11(16)e1 9. Total Mercury and Mercury UOP 938-10 Species in Liquid Hydrocarbons 10. Crude Distillation ASTM D2892-17a (15-Theoretical Plate Column) 11. Distillation of Heavy Hydrocarbon ASTM D5236-17 Mixture(Vacuum Potstill Method) 12. Carbon, Hydrogen & Nitrogen ASTM D5291-16 13. Salts in Crude ASTM D3230-13 14. Pour Point of Crude Oils ASTM D5853-17 15. Heat of Combustion ASTM D4809-13 16. *Boiling Point Distribution ASTM D7169-16 17. Asphaltenes ASTM D6560-12 18. Density of Crude Oils ASTM D5002-16 19. Chloride by Microcoulometry UOP 779-08 20. N Heptanes Insolubles ASTM D3279-12e1 21. Total Mercury by Lumex ASTM D7622-10(15) 22. Total Mercury by NIC ASTM D7623-10(15) 23. K Factor and Molecular Weight UOP 375-07 Estimation





24.

Determination of Halogenated and Sulfur Compounds in Hydrocarbon Samples by Combustion Ion Chromatography (C.I.C.)

In-House Method TPM 5.44C / C.I.C.

H. Hydraulic Oil / 1. Water Content ASTM D95-13e1 Lubricating Oil IP 74/00(14) ISO 3733-99 2. Kinematic Viscosity ASTM D445-17a IP 71/97

ISO 3104-94 3. Pour Point ASTM D97-17a 4. Viscosity Index ASTM D2270-10(16) 5. Flash Point ASTM D93-16a ASTM D92-16b 6. Strong Acid Number ASTM D664-17 7. Total Base Number ASTM D2896-15 8. Total Solids IP 316/93(05) 9. Colour ASTM D1500-12(17) 10. Water by Karl Fischer ASTM D1533-12 11. Carbon, Hydrogen and Nitrogen ASTM D5291-16 12. Flash Point ASTM D3828-16a (Method A) 13. Sulphur ASTM D7039-15a 14. Trace Elements ASTM D5185-13e1 Aluminium, Cadmium, Chromium, Copper, Iron, Lead, Manganese, Molybdenum, Nickel, Silver, Tin, Titanium, Boron, Sodium, Silicon. Barium, Calcium, Magnesium, Phosphorus, Zinc





15. Evaporation Loss by Noack Method ASTM D5800-15a (Procedure B) 16. Chloride by Microcoulometry UOP 779-08 17. Nitrogen ASTM D5762-12(17) 18. Color by Auto Tritimulus Method ASTM D6045-12(17) 19. Apparent Viscosity (CCS) ASTM D5293-17a 20. Pentane Insolubles by Membrane ASTM D4055-04(13) Filtration 21. Water by Karl Fischer Titration ASTM D6304-16e1 22. Total Acid Number ) IP 177/13 23. Strong Acid Number ) 24. Determination of Halogenated and In-House Method TPM 5.44C / Sulfur Compounds in Hydrocarbon C.I.C. Samples by Combustion Ion Chromatography (C.I.C.) 25. Dynamic Viscosity and Density of ASTM D7042-16e3

Liquids by Stabinger Viscometer

I. Marine Fuel Oil/Marine 1. Kinematic Viscosity ASTM D445-17a Diesel Oil/Marine Gas Oil IP 71/97 ISO 3104-94 2. Density @ 15°C ASTM D4052-16 IP 365/97(04) ISO 12185-96 3. Water Content IP 74/00(14) 4. Ash Content @ 550°C IP 4/05(12) 5. Ash Content @ 775°C IP 4/05(12) 6. Micro Carbon Residue ASTM D4530-15 7. Sulphur Content ASTM D4294-16e1 IP 336/04(14)





8. Total Sediment Existent IP 375/11, ASTM D4870-09(14) 9. Total Sediment Accelerated IP 390 B/11 10. Total Sediment Potential IP 390 A/11 11. Pour Point IP 15/95(14) 12. Flash Point IP 34/16 13. Cold Filter Plugging Point IP 309/16 14. Carbon, Hydrogen & Nitrogen ASTM D5291-16 15. Derived Cetane Number ASTM D6890-16e1 16. Hydrogen Sulphide IP570-15

J. Liquid Petroleum Gas 1. *Composition ASTM D2163-14e1 (LPG) 2. *Density at 15°C ASTM D2598-16 3. *Vapour Pressure Absolute 37.8°C ASTM D2598-16 4. *Octane Number ASTM D2598-16 5. Hydrogen Sulfide ASTM D2420-13 6. Weathering ASTM D1837-17 7. Residue on Evaporation at 37.8°C, ASTM D2158-16a O-number 8. Copper Corrosion ASTM D1838-16 9. Oily Residue IP 427/97(04) 10. Total Sulfur ASTM D6667-14

11. Determination of Halogenated and In-House Method TPM 5.44D / Sulfur Compounds in LPG and C.I.C. Natural Gas Samples by Combustion Ion Chromatography (C.I.C.)





K. Asphalt 1. Specific gravity at 25 / 250°C ASTM D70-09e1 2. Ductility ASTM D113-07 3. Loss on heating ASTM D6-95(11)e1 4. Thin film over test 3.2mm at ASTM D1754-09(14) 163°C for 5 hours 5. Penetration ASTM D5-13 6. Softening Point ASTM D36-14e1 7. Solubility in Trichloroethylene ASTM D2042-15 8. Flash Point ASTM D92-16b 9. Kinematic Viscosity of Asphalts ASTM D2170-10 10. Viscosity of Asphalts by Vacuum ASTM D2171-10 Capillary Viscometer 11. Determination of Paraffin Wax EN 12606-1:2007 Content 12. Determination of Halogenated and In-House Method TPM 5.44C / Sulfur Compounds in Hydrocarbon C.I.C. Samples by Combustion Ion Chromatography (C.I.C.)

L. Biodiesel 1. Ester content, Linolenic acid EN 14103:2011 methyl ester 2. Methanol content EN 14110:2003 3. Monoglyceride, Diglyceride, EN 14105:2011 triglyceride, free glycerol, total glycerol 4. Sulfur content EN ISO 20846:2011 5. Oxidation Stability 110°C EN 14112:2016





6. Density @ 15°C ASTM D4052-16 IP 365/97(04) EN ISO 12185:1996 7. Viscosity @ 40°C ASTM D445-17a IP 71/97 EN ISO 3104:1994 8. Sulfated Ash ISO 3987:2010 9. Water content EN ISO 12937:2000 10. Copper strip corrosion EN ISO 2160:1998 11. CFPP BS EN 116:2015 IP 309/16 ASTM D6371-17 12. Acid Value EN 14104:2003 13. Iodine value EN 14111:2003 14. Free and Total Glycerine ASTM D6584-17 15. Total Contamination EN 12662-14 16. Fuel Filter Blocking Potential ASTM D7501-12a 17. Oxidation Stability by EN 15751-14 / IP 574/14 Accelerated Oxidation Method 18. Ca, K, Mg and Na Content by EN 14538-06 / IP 547/07 ICP-OES 19. Acid Petroleum Products ASTM D664-17 20. Determination of Halogenated and In-House Method TPM 5.44C / Sulfur Compounds in Hydrocarbon C.I.C. Samples by Combustion Ion Chromatography (C.I.C.) 21. Dynamic Viscosity and Density of ASTM D7042-16e3

Liquids by Stabinger Viscometer





M. Fuel Oil 1. Kinematic Viscosity at 50°C ASTM D445-17a IP 71/97 ISO 3104-94 2. Total Sediment, Potential ISO 10307-2-09 3. Density at 15°C ASTM D4052-16 ISO 12185-96 ISO 3675-98 4. Flash Point, PMCC ASTM D93-16a IP 34/16 ISO 2719-16 5. Pour Point ISO 3016-94 6. Micro Carbon Residue ISO 10370-14 7. Ash ISO 6245-01 8. Water by Distillation ASTM D95-13e1

IP 74/00(14) ISO 3733-99 9. Sulphur ISO 8754-03 10. Aluminium and Silicon ISO 10478-94 11. Saybolt Universal Viscosity (SUS) ASTM D2161-17 by Calculation 12. Ramsbottom Carbon Residue ASTM D524-15 13. Acid Petroleum Products ASTM D664-17 14. Specific Energy ISO 8217-17 Annex H 15. CCAI Calculation ISO 8217-17 Annex C





N. Refinery Gas 1. *Refinery Gas Analysis by GC UOP 539-12 2. Determination of Halogenated and In-House Method TPM 5.44D / Sulfur Compounds in LPG and C.I.C. Natural Gas Samples by Combustion Ion Chromatography (C.I.C.)

O. All Petroleum & 1. Elements By ICP-MS In-House Method TPM 5.01B Petrochemical Products

P. All Petroleum Products 1. Vacuum Distillation ASTM D1160-15 2. Determination of Halogenated and In-House Method TPM 5.44C / Sulfur Compounds in Hydrocarbon C.I.C. Samples by Combustion Ion 3. Sulfur in Petroleum Products by ASTM D1552-16e1 Procedure A High Temperature Combustion and IR Detection or TCD

Q. Gas 1. Total Mercury in Gas In-House Method TPM 5.40 2. *Analysis of Natural Gas and ASTM D1945-03(10) Gaseous Mixtures by GC GPA 2261-2013 3. *Extended Analysis of Natural Gas GPA 2286-2014 and Similar Gaseous Mixtures by Temperature Programmed GC 4. Determination of Halogenated and In-House Method TPM 5.44D / Sulfur Compounds in LPG and C.I.C. Natural Gas Samples by Combustion Ion Chromatography (C.I.C.)

III TRANSFORMER OIL A. Transformer Oil 1. Electrical Breakdown Voltage IEC 60156-95 2. Relative Permittivity, Dielectric IEC 60247-04 Dissipation Factor & D.C. Resistivity





3. Water Content by Coulometric KF IEC 60814-97 Titration 4. Corrosive Sulfur by Silver Strip DIN 51353-85 5. Corrosive Sulfur ASTM D1275-15 IEC 62535-08 6. Oxidation Stability IEC 61125-04 (Method C) 7. Specified Additives in Mineral IEC 60666-10 Insulating Oils 8. Interfacial Tension ASTM D971-12 9. *Gases Dissolved in Electrical ASTM D3612-02(09) (Method C) Insulating Oil by GC

IV COAL AND COKE A. Coal and Coke Sulfur in the Analysis Sample of ASTM D4239-17 Procedure A Coal and Coke Using High- Temperature Tube Furnace Combustion Determination of Sulfur by IR ISO 19579-06 Spectrometry

V ANIMAL AND VEGETABLE FATS AND OILS A. Animal and Vegetable Determination of Acid Value and ISO 660-09 Fats and Oils Acidity Determination of Moisture and

Volatile Matter Content ISO 662-16

Determination of Insoluble Impurities

Content ISO 663-17

Determination of polyethylene-type

Polymers ISO 6656-02

Determination of Iodine Value ISO 3961-13 * GC-related Tests


Approved Signatories

1. Ms Ngoh Mei Heong ) For all tests in Sections I, II, III, IV and V 2. Ms Lee Shiau Yeng ) 3. Ms Wong Ji Sim ) For all tests in Sections I, II L, III, IV and V

4. Ms Yap Hui Wen ) 5. Ms Lin Zhong Qian )

For all tests in Section II and IV

6. Mr Lau Chia Chiun )

7. Ms Goh Siew Wei ) 8. Mr Mohammad Firdaus Bin Ridzwan ) 9. Mr Mahkali Bin Selamat ) 10. Ms Neo Lay Hoon, Winnie ) 11. Mr Abdul Rahman B. Mohd Yasin – For all tests in Sections II, III and IV 12. Mr Manfus Yam – For all *GC-related tests 13. Mr Tee Soon Guan, Melvin )

For all mercury-related tests 14. Mr Jai Kumar Sharma ) 15. Mr Mohammad Bin Sawifi – For tests in Section II G10-11 16. Mr Tan Lee Hong, Mark )

For all tests in Section II and IV 17. Ms Ten Chaw Hsia ) 18. Mr Ng Bang Tong ) 19. Mr Lim He Lok, Joy ) 20. Ms Tung Xiao Dan ) For all tests in Section II except *GC-related tests 21. Ms Lee Fuei Khim ) For all tests in Section I, II, III, IV and V except *GC-related

tests 22. Ms Samatha Cheng )

For all tests in Section II (A, D to I, K to M, O & P), Section II (B, C & J) and IV except *GC-related tests

23. Ms Becky Chang ) 24. Ms Vanessa Lee ) 25. Ms Tan Wei Zhou, Rachel – For all tests in Section I, IV and V 26. Mr Wang Meng Choon )

For all tests in Section II D, F, I and M 27. Ms Lee Mei Lian ) 28. Mr Peng Kian Yong ) 29. Ms Aimi Sarah Bte Mohd Razali )


Note : This laboratory is accredited in accordance with the recognised International Standard ISO/IEC 17025. A laboratory's fulfilment of the requirements of ISO/IEC 17025 means the laboratory meets both the technical competence requirements and management system requirements that are necessary for it to consistently deliver technically valid test results. The management system requirements in ISO/IEC 17025 are written in language relevant to laboratory operations and operate generally in accordance with the principles of ISO 9001.

FIELD OF TESTING : Chemical and Biological Testing · Colour (Saybolt) ASTM D156-15 12. ......

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Transcript of FIELD OF TESTING : Chemical and Biological Testing · Colour (Saybolt) ASTM D156-15 12. ......