FALL 2012ORGANIC CHEMISTRY LAB

CHML212

Lab Schedule, Course Policies, and Safety

Information

PREREQUISITE/REQUIRED MATERIALS

PREREQUISITE: Grade of “C” or better in CHML211!

REQUIRED TEXTS/SUPPLIES: 1.LAB MANUAL:

Organic Chemistry: Chemistry 211-212 Laboratory Manual Fall 2010 Edition—previous editions are unacceptable

2.LAB NOTEBOOK: Organic Chemistry Laboratory Notebook

3.SAFETY GLASSES/GOGGLES: Can be glasses or goggles, as long as

they form a complete seal around eyes!

COURSE WEBSITE

https://learn.uncw.edu/webapps/login/

LAB SCHEDULEDate Exp.

#Experiment Title Pre-Lab

Assignment 8/29,30 13a* Lab Intro–Calculation, Chromatographic, and Spectral

Applications NONE

9/5,6 13b* Calculation, Chromatographic, and Spectral Applications NONE9/12,13 15 Substituent Effects on the Rate of Electrophilic Aromatic

SubstitutionExp. 15 Pre-

Lab9/19,20 17a Nitration of p-methylacetanilide (Synthesis and

Purification)Exp. 17 Pre-

Lab9/26,27 17b Nitration of p-methylacetanilide (Product Analysis)

Quiz 1 (Exp. 13, 15, 17)NONE

10/3,4 18 The Grignard Reaction Exp. 18 Pre-Lab

10/10,11

19 Oxidation of 9-Fluorenol Exp. 19Pre-Lab

10/17,18

*20* Reduction of p-vanillin Exp. 20* Pre-Lab

10/24,25

*26* Synthesis and Analysis of Commercial Polymers Exp. 26* Pre-Lab

10/31,11/1

21 Ester Synthesis: Flavors and Fragrances Quiz 2 (Exp. 18, 19, 20, 26)

Exp. 21 Pre-Lab

11/7,8 22 The Solventless Aldol-Type Condensation Exp. 22 Pre-Lab

11/14,15

23 Theory of Color in Organic Compounds: Preparation of Organic Dyes

Exp. 23Pre-Lab

11/21,22

*** NO LAB—Thanksgiving Break Holiday NONE

11/28,29

24 Synthesis and GC Analysis of Fatty Acid Methyl Esters—Lab Checkout Quiz 3 (Exp. 21, 22, 23, 24)

Exp. 24 Pre-Lab

ATTENDANCE POLICY All labs are mandatory.

No make-up labs for any reason.

Missed lab = zero (regardless of reason). 

Missing 3+ labs = F for course.

Athletic events are NOT excused absences.

GRADING Lab is graded separately than lecture!

Quizzes (45%) Final Lab Reports (55%)

Course Grading: A = 90-100, B = 80-89, C = 70-79, D = 60-69, F

= 59 and below. Plus (+) or minus (-) grades may be awarded at

the discretion of the instructor.

LAB QUIZZES 3 lab quizzes , 3-5 experiments on each.

Full experiment after all quizzes! Plan on staying for the entire lab period!

Make up quizzes will only be allowed for excused absences. To have a quiz absence excused, the student

must: Email before beginning of lab Bring doctor’s note

MAKE UP QUIZZES MUST BE TAKEN PRIOR TO THE NEXT LAB MEETING!

FINAL LAB REPORTS All lab assignments will be available on

the course website. Final Lab Reports consist of:

Pre-Lab Assignments (20 pts) In-Lab Assignments (20 pts) Post-Lab Assignments (50 pts) Lab Technique/Preparation (10 pts)

Due dates announced by instructor. Late reports = 5% penalty per day

Once lab reports are returned to students graded, NO MORE WILL BE ACCEPTED!

LAB TECHNIQUE You are responsible for your own

safety! Be prepared and familiar with safety

hazards! Wear proper shoes and eye protection! Common sense and thinking are

REQUIRED.

You are responsible for cleaning up after yourself! YOU. Not your lab instructor. If we clean,

you pay.

PERSONAL ELECTRONICS Cell phone use WILL NOT BE tolerated.

Turn ON SILENT OR VIBRATE before lab and PUT IT AWAY!

YOURS rings = you leave = ZERO Cannot use phone as calculator during quizzes!

Laptops and desktop computers use is allowed for lab related activities ONLY.

Ipod use is not acceptable in lab!

OTHER ISSUES Please refer to the online

syllabus for information regarding: Learning Outcomes Academic Integrity Students with Disabilities Violence and Harassment

SAFETY IN THE ORGANIC LAB

Follow instructions at all times!

Act responsibly at all times!

No food or drinks on lab benches!

Dress appropriately for lab!

Come prepared! Know what you are going to do, and what the hazards are!

Report all accidents to the instructor, no matter how small.

ACCEPTABLE CLOTHING FOR LAB…

DO wear Goggles/safety glassesClosed-toe shoesTie back long hair

DON’T wearSandals/flip-flops JewelryLoose or baggy clothing

LAB SAFETY EQUIPMENT Safety Shower Eyewash

Safety Goggles/glasses

LAB SAFETY EQUIPMENTFire Extinguisher Fume Hood

ACCIDENTS AND INJURIES

Report ALL injuries to lab instructor IMMEDIATELY, no matter how minor.

Be aware of hazards associated with each chemical and technique you will use in the experiment!

Complete an Injury Report Form.

FIRST AID Eye accidents: Wash eyes in stream of

water using eyewash station for 15 minutes!

Chemical burns: Immediately flush the affected area with a large amount of water in the sink! Use safety shower if necessary!

Thermal burns: Determine the type and extent of the burn. Take appropriate action. 1st degree: red skin, no blisters.

Immerse in cold water/apply ice. 2nd degree: blisters.

Immerse in cold water, then apply clean gauze. 3rd degree: broken skin, tissue damage.

Cover with clean gauze. Visit the Health Center.

FIRST AID Bleeding, cuts, and abrasions:

Clean wound with soap and warm water. Apply pressure with clean gauze pad

until bleeding stops. Cover wound with bandage or clean

gauze pad and secure.

Poisoning: If, after contact with, inhalation of, or

accidental ingestion of a chemical, you experience discoloration of the lips, a burning sensation in the throat, stomach cramps, nausea and vomiting, or confusion, seek treatment IMMEDIATELY for chemical poisoning!

UNCW SAFETY CONTRACT

READ Laboratory Rules and Guidelines (p. vii) CAREFULLY!

READ, SIGN, AND SUBMIT safety contract (p. xiii) to instructor!

WASTE DISPOSAL Waste disposal procedures are at

end of the procedure for each experiment.

If you do not know which waste goes where, ASK!

NOTHING DOWN THE SINK!

QUESTIONS?