ecology ^nd environment, inc. -!• Specialist •••s in the ...TASK REPORT TO THE ENVIRONMENTAL...

FIELD INVESTIGATIONS OFUNCONTROLLED HAZARDOUS WASTE SITES\ •

FIT PROJECT

Prepared

TASK REPORT TO THEENVIRONMENTAL PROTECTION AGENCY

CONTRACT NO. 68-01-6056

A Site Inspectionof

KimbertonTDD No. F3-8203-22:;EPA NO. PA-423

Preperation Date: July 23, 1982

Presented to: Linda Y. Boornazian, Acting DPOEPA Region III

/

Ctegg Crystal 1

Joŝ pl/G. McGovern^flTL III

ecology ̂nd environment, inc.- • • • • " • • - • • •Internationa! Specialists in the Environmental Sciences

163100

KimbertonTDD No. F3-8203-22EPA NO. PA-423

TABLE OF CONTENTS

Section 1 Summary and Recommendations

Section 2 Field Trip Report

Section 3 Site Inspection Form

, Section 4 Analytical Data Summary

Section 5 Toxicological Review

Section 6 Maps

6.1 Map of Sample and Photograph Locations .6.2 7.5* Map of Floodprone Showing Sample and

Photograph Locations

Section 7 Photographic Log

Section 8 Appendixes

8.1 Wells Samples By PA DER And Results8.2 Analysis Data Sheets8.3 Sample Paperwork, Airbills and Chain of Custody

ARIOOI89

. • •' I


SUMMARY AND RECOMMENDATIONS

1.1 SUMMARY

The subject property, which is now owned by Monsey Products, Inc., anasphalt manufacturer, contains three lagoons previously used for disposal ofTCE and related process wastes by CIBA-GEIGY Corporation, the former realtyowners. These lagoons were installed and operated for approximately 10 yearsending in 1960 by CIEA-GEIGY Corporation. The three lagoons presently have athin soil and grass covering. There are no liners under the lagoons.

An area adjacent to the lagoons may have been used as a spray field fordisposal of contaminated process water by CIBA-GEIGY. However, there was noevidence of this at the time of the site visit.

Samples collected and analyzed by the PA DER from household wells in thevicinity of the property in question revealed high levels of TCE and dichloro-ethylene. The concentrations are great enough in one or two homes topotentially cause ill effects from inhalation exposure as a results of bathing(showering). Other samples including one from the Kimberton Country HouseRestaurant, had TCE and dichloroethylene levels considerably over what the PADER recognizes as a criteria level (45 up/1) for these compounds.

Lagoon samples collected by FIT Region III show high concentrations oflead (38,000 ug/1), arsenic (2400 ug/1) and chromium (13,000 ug/1) as well asTCE at a level of 710 ppb.

The downstream sample of the creek (tributary to French Creek) revealedcontamination by some potentially carcinogenic polynuclear aromatichydrocarbons such as benzo(k)fluoranthene, and benzo(a)arthracene among others.These compounds may have entered the creek via spills from Monsey rather thanthe lagoons since these compounds were not detected in the lagoon samples. v

1-1 ARIOOI90

KimbertonTDD No. F3-8203-22EPA No. PA-423Summary and Recommendations

1.2 RECOMMENDATIONS

o Due to the type and level of.contamination in the residential wells,an alternative water source should be used. Bottled water wouldsuffice in most cases, however, in the homes having higher levels ofcontaminants (where inhalation exposure from bathing could besignificant) an alternative water source is needed.

The Citizens Utility Water Company, which serves a portion ofKimberton, has submitted plans and cost estimates to the PA DER forconnecting homes having contaminated water to their system.

i , o It is recommended that remedial action should be undertaken to^^ • prevent the further contamination of the groundwater.

o In the interim, the lagoons should be immediately fenced in toreduce the potential for inadvertant exposure to the toxins.Furthermore, residents of homes adjacent to the creek and downstreamof Monsey should be warned not to let their children play in the •creek, due to the nature of the compounds found there.

o Since French Creek is used for recreational purposes, it isrecommended that additional sampling at the entrance to French Creekbe considered.

A R I O O I 9 I


FIELD TRIP REPORT

2.1 INTRODUCTION

FIT Region III was tasked to perform a high priority Site Inspection tocollect enough information to complete a Hazardous Ranking System (HRS) on theTCE lagoons located on property now owned by Monsey Products. The lagoons wereused by the previous property owner, CIBA-GEIGY Corporation for disposal of TCEand related wastes. The lagoons were in operation for approximately 10 yearsfrom 1950 to 1960. It has also been reported that CIBA-GEIGY also used a sprayfield on an adjacent property to dispose of TCE contaminated process water.FIT Region III conducted this Site Inspection on April 22, 1982. AccompanyingFIT Region III representatives Gregg Crystall and Beth Gross was Steve Jarvelaof EPA Region III. It should be noted that no wells were sampled since PA DERhad previously sampled them and were not required for the HRS.

2.2 CONTACTS

John Doyle, Vice President Steve Jarvela, EPA Region IIIMonsey Products, Inc. Philadelphia, PAColdstream RoadKimberton, PA 19442(215) 933-8888 Phil Retallic, EPA Region III

Philadelphia, PAAgden Fitzsimmons(area resident and formerengineer for CIBA-GEIGY)Hares Hill RoadKimberton, PA 19442(215) 933-9586

2.3 PERTINENT COMMENTS

o Mr. Fitzsimmons - "Used to work for CIBA-GEIGY in the 1950's andearly 1960's. They installed those lagoons and filled them with solvents.There are no liners there and they have to be the cause of all this groundwatertrouble."

2-1

ARIOOI92

KimbertonTDD No. F3-8203-22.EPA No. PA-423Field Trip Report

o Phil Retallic explained that there may have been a spray field whichis now across Route 113 from the lagoons. The spray field was operated byCIBA-GEIGY and is located on a probable fault line in the bedrock.

o John Doyle explained that prior to Monsey Products buying theproperty, CIBA-GEIGY owned it and used to have some waste solvent lagoons.Before CIPA-GEIGY another chemical company owned the property, but the lagoonswere installed by CIBA-GEIGY. Monsey has no immediate plans for the lagoonareas.

2.4 FIELD OBSERVATIONS

O FIT Region III arrived at the site at 1000 hours to interview therepresentatives of the present owner, Monsey Products, and conduct on-sitesampling. The weather was about 65*F and sunny.

Observations of the lagoon area revealed the following: There are threeold lagoons that are marginally covered with soil and vegetation. There didnot appear to be any leachate emanating from the lagoons. The lagoons areeasily accessible to the public (no fences).

Lagoon #1 (See Photograph 1) is approximately 10' x 35*. The areasurrounding this lagoon is fully vegetated. FIT Region III dug approximately 1foot into the lagoon and took a sample of a white sludge mixed with a blackresin-like material. There were no readings above background on the HNUphotoionizer. Lagoons #2 and (3 (See Photographs 2 and 3) measured 15* x 5'and 20* x 20', respectively. There was some evidence of stressed vegetationaround lagoon #3. It was noted that there were animal burrows into the side ofall three lagoons.

AR100193

KimbertonTDD No. F3-8203-22EPA No. PA-423Field Trip Report

FIT Region III left the site at 1130 hours to investigate the reportedspray field across Route 113 from the site of the lagoons, and obtain numerousoff-site samples.

•

The area that was allegedly a spray field was evidently being used for acorn field (See Photograph 4). There was no evidence of stressed vegetation inthis area.

The tributary to French Creek appeared to have the same algal growthsand aquatic flora on its banks both up and downstream without evidence ofadverse stream conditions.

2.5 SAMPLE LOG———————————

All samples were collected on April 22, 1982.

S-l Lagoon 1, Medium Concentration Solid, 10:20Organics sent to CRL, Annapolis, MDInorganics sent to Wheeling, WV Field Office

S-2 Lagoons 2 and 3, Medium Concentration Solid, 10:30Organics sent to CRL, Annapolis, MDInorganics sent to Wheeling, WV Field Office

S-3 Downstream Creek, Low Concentration Aqueous, 11:15TR #'s C1371/MC-8971Organics sent to Mead Technology LabsInorganics sent to California Analytical Labs

2-3

ARIOOI9U

KiirbertonTDD No. F3-8203-22EPA No. PA-423

S-4 Downstream Sediment, Low Concentration Solid, 11:15TR #'s C-1378/MC-8979Same Labs as S-3

S-5 Upstream Creek, Low Concentration Aqueous, 11:30TR tf's C-1370/MC8970Same Labs as S-3

S-6 Upstream Sediment, Low Concentration Solid, 11:30TR #'s C-1377/MC-8977Same Labs as S-3

S-7 Sediment in Ditch (spray field area), Low Concentration Solid, 12:05TR #'s C-1379/MC-8979Same Labs as S-3

S-8 Fitzsimmons Spring (used for drinking), Low Concentration Aqueous, 12:20TR #'s C-1373/MC-8973Same Labs as S-3

S-9 Fitzsimmons Pond, Low Concentration Aqueous, 12:20TR #'s C-1372/MC-8972Same Labs as S-3

S-10 Roberts Spring, Low Concentration Aqueous, 12:35TR #'s C-1374/MC-8974Same Labs as S-3

2-4

ARIOOI95

KimbertonTDD No. F3-8203-22EPA No. PA-423

S-ll Gotwalls Pond, Low Concentration Aqueous, 12:40TR #'s C-1375/MC-8975Same Labs as S-3

Sample Blank (Low Concentration Aqueous)TR #'s C-1369/MC-8969Same Labs as S-3

Sample Blank (Low Concentration Solid)TP #'s C-1376/MC-8976Same Labs as S-3

Sample Blank (Medium Concentration Solid)Organic sent to AFOInorganic sent to WFO

2.6 IMMEDIATE ACTION ITEMS

o An alternative water source should be given to homes havingconcentrations of TCE and dichloroethylene in toxic levels.

o Fencing of the lagons to preclude direct contact by the public.

o Inform the residents along the creek (tributary to French Creek) anddownstream of the site of the potential hazards of coming in contact with thecreek water.

2-5

ARIOOI96

From Pege t______________ TDD Np. F3-8203-22 EPA NO. PA-423X. WATER AND HYDROLOCICAL DATA 'continued;

LIST ALL DRINKING WATER WELLS WITHIN A r« MILE RADIUS OF SITE

1. WELL 1. OCPTHftptei/y unlij

t. LOCATION(prottmitr lo population,' talldint*!

NON-COM-M'JN'TYr.trk 'X'>

COMMON-IT.»_f«i«/* 'X')

see attachment A of Site Inspection report

1. RECEIVING WATER

1. NAME I I I I. SEWERS 00 »• STKE AMS/P. IVEHS

tribuary toFrenchCreek [ r~l 4. LAKES'NESEKVOIRS ! * s. OTME«'»p»e«r;

S. SPECIFY USE AND CLASSIFICATION OF RECEIVING WATERS

tributary is not used. French Creek is used for recreational purposes.

XI. SOIL AND VEGIT ATION DATALOCATION OF SITE IS IN:

[XJ A. KNOWN FAULT ZONE Q B. KARST ZONE O C. «00 YEAR FLOOD PL»«N ~ D. WETLAND

•33 C. A REGULATED FLOODWAY ! ! F. CRITICAL HABITAT j£ G^RCCMARCE IQNg^SB SOLt SJJ^it AOJi*ER

XII. TYPE OF GEOLOGICAL MATERIAL OBSERVEDHark 'X* to indicate the typef*) of ceoloeical material observed and specify where necessary, the cor-.̂ cr.r.-.* ̂ trtsX

A. OVERBURDEN•x

B. BEDROCK (tpicllr Itlow)X'

C. CTriER .•p»cl/J- bcloH-j

'•*ANO Stockton Formation-

loam coarse grain sandstone and cong onerateS. 6RAVCL

Xm. SOIL. PERMEABILITY

1 1 A. UNKNOWN ! 1 B. VERY HIGH fJOO.COO 1C JOOO em'»*t,) ' ' C. MISH fJOOO ic 10 cm '«.«.;!TP D. MODERATE flO ro .1 cm'»«eO P~l E. LOW {.I to .001 cm/tft.) f~1 r. VE»Y LOW r.OW «c .OOOOJ cn.'McOG. RECHARGE AREA

(~1 *. NO *. COMMENTS.-H. DISCHARGE AREAl~l 1. YES E *• K0 '• COMMENTS.I. SLOPE1. ESTIMATE * OF SLOPE I Z. SPECIFY DIRECTION OF SLOPE. CONDITION OF SLOPE. ETC.

___7%_____[slope is covered with grassJ. OTHER GEOLOGICAL DATA

There are t{*) fault lines in this area

"PA Ferin TJ070-3

TDD No. F3-S203-2; EPA No. PA-423XIV. PERMIT INFORMATION

List all applicable permits held by the site and provide the related information.

A. PERMIT TYRE B. ISSUINGAGENCYc. PERMITNUMBER

D. DATEISSUED

E. EXPIRATIONDATE

f. IN COMPLIANCEtmtttt 'X')

i.YES

a.MO

(.UN-KNOWN

No permits

XV. PAST REGULATORY OR ENFORCEMENT ACTIONS3 NONE I I YES (•unanlrix* In Ittlf »t>»t»)

NOTE: Based on the information in Sections III through XV, fill out the Tentative Disposition (Section II) informationon the first page of this form.

IfA Form T2070-J (JO-7?) PAGE 10 OF 10

ARIOOI98

Continue* FrcT,̂ .- TDD NO. F3-S203-22 EPA NO. PA-423. HAZARD^DESCRIPTIONrcontinuerf;

C~l N. flRE OR EXPLOSION

None

f""} O. SPILLS/LEAKING CONTAINERS/RUNG? F/STANDINC LIQUID

None

P. SEWER. STORM DRAIN PROBLEMS

No

Q. EROSION PROBLEMS

No

QJ R. INADEQUATE SECURITY

Lagoon area is not fenced in

f") S. INCOMPATIBLE WASTES

Not apparent

ARIOOI99

EPA Fen* TJ070-J (10>7f) PACE 7 OF 10 Continue On Reverse

TOD No. F3-8203-22 EPA No. PA-423

~~l T. MIDNIGHT DUMPING

No

[~~i U. OTHER f*p«e«w

N/A

•

VHI. HAZARD DESCRIPTION 'conrmued,

(Red)

IX. POPULATION DIRECTLY AFFECTED BY SITE

A. LOCATION OF POPULATION

t.lN RESIDENTIAL AREAS

- IN COMMERCIAL**OR INDUSTRIAL AREAS

. IN PUBLICLY'•TRAVELLED AREAS

. PUBLIC USE AREAS'•fp«r*». •eheet*. He,)

B. APPROX. NO.OF PEOPLE AFFECTED

100

30

variesnone

iC.APPHOX. NO. OF PEOPuE ' C.APPF

AFFECTED WITHIN OF BJIUNIT AREA i AFFE

i

1/4 mile ' 30

1/4 mile 5

Rt. 113 adjacent to site

ICX. KD. E. DISTANCEi-CINSE TO SITECTEC -tpfdly unit!)

4 1/4 mile< 1/4 mile

X. WATER AND HYDROLOGICAL DATAA. DEPTH TO GROUNDWATERf*p*c'fr

5 feetO. POTENTIAL YIELD OF AQUIFER

-unknown

l*>

p.*e< TDD No. F3-8203-22 EPA No. PA-423VTIl. HAZARD DESCRIPTION f continued;

fid B. NON-WORKER INJURY/EXPOSURE

Potential exists via direct contact since lagoon area is readily accessible to thepublic.

-it-'•••'. i

C. WORKER INJURY/EXPOSURE

None reported - but potential exists same as VIII B above.

D. CONTAMINATION OF WATER SUPPLY

Some drinking water in the area is contaminated by TCE and 1,2-dichloroethylene.

E. CONTAMINATION OF FOOD CHAIN

Potential exists since there is farming in the area.

F. CONTAMINATION OF GROUND WATER•

Some local residential wells and Robert's Spring were found to be contaminated,

G. CONTAMINATION OF SURFACE WATER

Downstream of the lagoons in the tribuary to French creek is contaminated with1,2-dichloroethylene, benzoanthracene, benzofluoranthene, chrysene.

fiRIOOZOIE PA F«*» T2070-3 (10-7») PAGE 6 OF 10 Continue On Reverse

Continued From Front__________ _________ TDD NO. F3-8203-22 EPA NO. PA-423. HAZARD DESCRIPTION fcontinuedj

;__I H. DAMAGE TO FLORA/FAUNA

Not apparant v )

i I I. FISH KILL

Nonereported ORIGINAL

[ I J. CONTAMINATION OF AIR

hnu readings over entire site showed no levels above background

[ ! K. NOTICEABLE ODORS

None

[~1 L. CONTAMINATION OF SOIL

None

[ I II. PROPERTY DAMAGE

None

ARI00202 rEPA Form T2070-3 (10-7W PAGE 6 OF 10 Conlinoe On

Continued From Front TDD NO. F3-S203-22 £PA f.'O. PA-423VD. WASTE RELATED INFORMATION 'confinm..

2. Estimate the amount (specify unit of measure) of waste by category, mark 'X' to indicate which wastes are present.a. SLUDGE

AMOUNT

185*UNIT OF MEASURE

cubic vards• j(~~ "'PIGMENTS

...METALS* SLUDGES

IS)POTW

ALUMINUM'•'SLUDGE

X. (l)OTHCRfep«cff>.):

sludge fromsolventtreatment andvastes^(quantityestimatedfrom size oflagoons)

b. OILAMOUNT

UNIT OF MEASURE

X •

~~ " WASTES

J,,OTHERr.p.ci/X,

c. SOLVENTSAMOUNT

UNIT OF MEASURE

X1..HALOCENATECSOLVENTS

. NON-M ALO6NTC.SOLVENTS

_ i|iOTHERf*pecifx;-

d. CHEMICALSAMOUNT

UNIT OF MEASURE

—— 1 AC'CS

I2, PICKLING

• »' CAUSTICS

14'. PESTICIDES

'9! CVES'INKS

16' CYANIDE

ITI PHENOLS

IS'HAUOeENt

i isi PCB

I1C>METALS

ill ; CTHER'tp»CI/)v

1

*. SOLIDS f. OTHERAMOUNT AMOUNT

KN:T OF MCASwIE .CN'T OF MEASURE1

- -— hH"pt;s::jSuT:i ASBESTOS '2IHOSPITAL

• ?*-,::::;--«-z:iisxM' — c—

NOM-FERXOUS i is. OTHER ftpeelly;:SMLTG. WASTES j ——

h

1

D. LIST SUBSTANCES OF GREATEST CONCERN WHICH ARE ON THE SITE (pUet in descending crder of hazard

1.SUBSTA

2. FORM J.TOXICITYmar* 'X') (murk 'X')

"CC 1. SO-LID

ITF

1,2-dichloroethvlene

b.DO.

X

x

C.VA. •.POR HIGH

b. c. d. "-MEC. 1.OK NONC

AS NUWBE* {AMOUNT 6. UNITi

X 710 pph

X . 10 ppb

VIII. HAZARD DESCRIPTIONFIELD EVALUATION HAZARD DESCRIPTION: Place an 'X' in the box to indicate that the listed hazard exists. Describe thehazard in the space provided.•~Xt A. HUMAN HEALTH HAZARDS

Drinking water is contaminated by TCE and 1,2-dichloroethylene.

RR 100203'EPA Farm TJ070-3 (10-79) PAGE « OF 10 Continue On Pefe 5

F r o m , » » _ 3 T D D No. F3-8203-22 EPA No. PA-423

\

IV. SAMPLING INFORMATION (continued) '.,......C. PHOTOS. TYPE OF PHOTOS 2. PHOTOS IN CUSTOOV OF

3 a. GROUND H2 b. AERIAL Ecology and Environment, Inc. -Region IIID. SITE MAPPED*

JtJ YES. SPECIFY LOCATION OF MAPSEnclosed in report

E. COORDINATESi. LATITUDE fdef.-min.-sec..)

40° 08' 00"2. LONGITUDE .'def .-nin.-sec.;

75° 35 ' 20"V. SITE INFORMATION

A. SITE STATUS"""} 1. ACTIVE (Thott induct"*' omunicipal sites which are beinf usfor waste treatment, tiormgr. or dison a continuing bfttt, even if infre

r X 2. INACTIVE fThetfrd sites which no longer receiveposal wastes.;

• 3. OTHERfspeeifyi-(Thott sites that include such incidents like "midnight dumping"u-here no ttgultr or continuing use of the site for waste disposalhas occurred.,)

B. IS GENERATOR ON SITE1~JT' 1. NO ' 2. YES'specify generator's iour-difii SIC Code;-

C. AREA OF SITE fin acres,

disposal area yĵ acre

D. ARE THERE BUILDINGS ON THE SITE'^;».NO jj[ 2. YES'speciiv.i- Plant works, garage, offices

VI. CHARACTERIZATION OF SITE ACTIVITYIndicate the major site activityfies) and details relating to each activity by marking 'X* in the appropriate boxes.•X1— A. TRANSPORTER

1.RAIL2. SHIP

S. BARGE4. TRUCK

S. PIPELINE

S.OTHKRfspacifyj:

— B. STORER

I. PILE

2. SURFACE IMPOUNDMENT

S. DRUMS

4. TANK. ABOVE 6ROUNC

S.TANK. BELO* CROUNS

e. OTHER (specify;.-

XI )-4 C. THEATER

1 1 . FILTRAT'ON

2. INCINERATION

9. VOLUME REDUCTION

- 0. DISPOSER

1..AN=r._.

i -*N = '»'"'-

i.OPES C-JMP

4.RECYCLIN6'RECCVER* |y '* l.-'-CE :wC£_.s^MENT

B.CHEM.'PHVS.'TREATMES- j

(.BIOLOGICAL TREATMENT

T. WASTE O-L REPROCESS'-.^

(.SOLVENT RECOVER^

S.OTHER(specify;:

t.vrN.S-T CUV«-SG

€. NC-NE«i A* C%

'• »N; EB ;=c -%r INJECTION6. S "ME" -speci/y

E. SUPPLEMENTAL REPORTS: tf the site fails within any of the categories listed below. Sv*>pl«mer.:ai Reports must be completed. Indicatewhich SvvpUaental Reports you have filled out and attached to this for..

C] 1. STORAO £3 2. INCINERATION !~~! 3. LANDFILL QQ •• ?MPOI?N*DMENT "~l *• DEEP WELL

D •• PMVSTREATMENT d '• LANDFARM [̂ «. OPEN DUMP F] f. TRANSPORTER !̂ 10. RECYCLOR/RECLAIMER

V1L WASTE RELATED INFORMATIONA. WASTE TYPE[53 1. LIQUID 1 1 2. SOLID (3D 3. SLUDGE ! 1 «. GAS

». WASTE CHARACTERISTICS

£3 '• CORROSIVE D 2. IGNITABLE 1 1 3. RADIOACTIVE KJ 4. HIGHLY VOLATILEnjl ». TOXIC 1 1 S. REACTIVE 1 ! 7. INERT i I 1. FLAMMABLE

( | 9. OTHER f»p»cl/r>-WASTE CATEGORIES

.. Are records of wastes available? Specify items such aa manifests, InventoHes. etc. below.

v No records available»rHI T207M (10-79) PAGE S OF 10 Uontmue On «everseAR10020U

Continued From Front Tnn Mn F*3 c?m 9° EPA No. PA-423ID. INSPECTION INFORMATION (-continued;

D. GENERATOR INFORMATION 'sources af wmttt) • ' '-'1. NAME

ciba Geiov

t. TELEPHONE NO.

ino lonoer on s•

S. ADDRESS '

te)

' • • • ' • "i °̂

E. TRANSPORTER/HAULER INFORMATION1. NAME

N/A

t. TELEPHONE NO. S. ADDRESS

F. IF WASTE IS PROCESSED ON CITE AND ALSO SHIPPED TO OTHER SITES. IDENTIFY OFF-SITE FACILITIESt. NAME

N/A

C. DATE OF INSPECTION

t. TELEPHONE NO.

H. TIME OF INSPECTION

10:00-12:30

I.KASTE TVPE CENERATED

I.MASTE TVPE TRANSPORTED

USED FOR DISPOSAL.s. ADDRESS

-

1. ACCESS GAINED B Y:f credentials aiust be shon-n in all cases;GO t. PERMISSION I I 2. WARRANT

J. WEATHER fdescrtAs;

r7RO p_ and camnvIV. SAMPLING INFORMATION

A. Hark 'X* (or the types of samples taken and indicate where they have been sent e.g., regional lab, other EPA lab. contractor,etc. and estimate when the results will be available.

1. SAMPLE TYPE

a. CROUNDWATCR

b. SURFACE WATER

C. WASTE

d. AIR

a. RUNOFF

t SPILL

e. COIL

B. VE6CTATION

1. CTHERfepecJfr>

S. SAMPLETAKENmark 'X')

X

X

X

X

, - . . , . ! S . SAMPLE SENT T O :

Organic to Mead Technology LabsTn/MTifl'tife *r> faT^T^nrnia Apaly^^pA^ |^a

Same as aboveOrganics to AFOInnrganlre. to WFO

^ I •'

Same a? for ground and surface water

:" :.::tf\

4. DATERESULTS

AVAILABLE

bs

B. FIELD MEASUREMENTS TAKEN fe.f.. radioactivity, eiplosivity, PH, etc.;1.TVPE

hnu

(.LOCATION OF MEASUREMENTS S.RI

Lagoon .area, entire site no readinos abovI

. i-

ESULTS

e background

f\Rinn?05EPA Fare. TJ070-J (10-T«) PACE 2 OF 10 Continue On P««e y

TDD No. F3-S203-22 EPA No. PA-423—————————— TrrrrrwEPA i»«< P01 «'IAL HAZARDOUS WASTE SITE' SITE INSPECTION REPORT

REGION SITE NUMBER (la 6* sssfjn-sdbvjfq)

III

GENERAL INSTRUCTIONS: Complete Sections 1 and III through XV of this form as completely as possible. Then use the inform*'»ion oa this form to develop • Tentative Disposition (Section 11). File this form ia its entirety in the regional Hazardous Waste Log

la. Be sure to include all appropriate Supplemental Reports in the file. Submit a copy of the forms to: U.S. Environments! Pro*action Agency; Site Tracking System; Hazardous Waste Enforcement Tack Force (EN-335), 401 II St., SW; Washington, DC 20460.

I. SITE IDENTIFICATIONA. SITE NAME

KimbertonC. CITY

Kimberton6. SITE OPERATOR INFORMATIONt. NAME

_^ previously, operatedS. STREET

same address

B. STREET (or elher Idemlfiarj

Rt. 113 & Coldstream RoadO. STATE. IE. ZlP~COBE

PA 1 19442(former)

by. Clba-Geigy_.Cqr2oratio

SAMPLE DATA SUMMARY

Site Karne: fc,̂- TDD No. : n-siOl 2-7_______

EPA No.: ?A-»U2 _____Date of Sample; ._y/a./g7. ' -

a ORGANIC!}COMPOUNDS IDENTIFIED IN SAMPLE RESULTS

-J< I MORGAN 1C J ——————————————————————————Concentrations in: ppb » ug/1 - L (aqueous); ppb = ug/kg - S (solid)

(For tentatively identified compounds see Analytics] Data Sheets in the appendixes)

Eit-nient/Compound ?>'firne

Sheet | of 2-

SAMPLE DATA SUMMARY

Site Kane: k\r-,\V-.r*,rk"v

0 ORGAI'

TDD No.:EPA No . :

Date of S

del> COMPOUNDS

Concentrations in: ppb * ug/1

(For tentatively identified compounds

P3>-VX*/.^ 2.7.f>A-«t'ZS.

trnpJe: •Jla.z.X'il.

IDENTIFIED IN SAMPLE

• • i 4'"

RESULTS

- L (aqueous); ppb s ug/kg - S (solid)

see Analytical Data Sheets in the appendixes)

Element /Compound Kame

/ / / / •//-I 1 I .i/ */ W i/Sample I.D. No. C/ •*£/ -M C *T ^/ P4 / Cj /

Types and Location \7 x/ vJ / \J , \/ ^ / /

Sarrple Blank (biJCfvCj,

Lab Blank

7 r3 !SJ

W*WJ

2«00

/IOW

2' ' - ~2CCW

^iTirc

.iscec'tawtf'

*

1

irsp«C.od

il'JĈ

/ Cor~.ents

550O

tl6Bi>1 y »*./fflA.» li.!00

*

"

'.

J«klif.N L,Hl/J,t.k̂ U.-h

AKI.002JSheet ^ of

353

Complied hi A A Sfir

*"VV "^ a ; - : '/.'

448

v - .*••, •±"C£ , '• V--" - / I-__.——— , .^ ^ « . ̂

-' '":: -cu *• V̂ f '*?

* -,, . • ' -• 1 » * •' " " • • - .

Comoiledbv T IW BERG andA .sfirmnw 1978

SAMPLE DATA SUMMARY

^ OR5A.' Dlf.'ORGA'

Cone i- nt rat ions i

(For tentatively identi

r.xr.ple 1 .D. No. KTypes and Location

£*r:Ple ?2ank(vw'̂

Lab PUnk

s-:.....bp,.i..._

S-*;' .•{•- ••••'.'.,- -̂-.Vc_A- c,-)if..-. r:,L

i-£ r!--. s J ̂ 7̂-

Ai .

6-y cj.̂ .i,,-. iwki-̂̂ fl̂ VA.rtt.̂ ^ .M,

——————— ————— JL>-)» ŴMkik̂ fjix

TDD ?io. :EPA No . :

f i •iii'.i-xaPA -H 1.3

Date of Sample: Ski\^t;

> COMPOUNDS IDENTIFIED IN SAMPLE RESULTS^CJ

n: ppb • ug/1 - L (aqueous); ppb * ug/kg - S (solid)

fied compounds see Analytical Data Sheets in the aj.'pt-ridi>e-s)

£u El t-yent /Compound )*wne ̂ J

/ jV ;^J/ .j-s,y-oo ' ̂/ •£ sj

> / _/ / *• / , / ̂M ^/ ^ / ^ / 4

I *< 1 •*$ 1 ••* ̂ / ̂i

1 -10i_r ..:. .j._ ..

Sa,^VUcnVb>x«Ac^cMsr-it VlvW(lw ct̂ s«uH

i!K/:TOO

•

. ... . .

\\oOI ^>

|1U^

•

IJ

1 I

It

\l

.

.. .. _...V̂

- 1ARI002II '

j

;

Sheet . of

SAMPLE DATA SUMMARY

Site Kime:

«t OR3A

' DINORGAConcentrations i

(For tent fit ively identi

•>"V

?.•-:•.;• le 1 .D. No. JTvp'.-« end Location ^ ^

/ \\_S*-ple BUnk (Uĵ x̂ ll

Lfb FUnk

'* ' I/ •• 1'̂.' . . Kft'r'H ' ...

\-: jc t.-.i..-̂'«,y tpW.rr.b

/ 1 L-^ W* f f 7> *̂'* I ̂V*\̂ «̂ J

--

— —— —

}ifUu

-> ĵ̂ .f̂ a.UvlN Ĵ̂ ,̂ >*r>.̂ '̂ COMPOUNDS

F̂ J JjyJ'i-'i'*l>A H 12.

Hlf pi e : HUiVfe/,

IDENTIFIED IN SAMPLE RESULTSNJCJ

n: ppb * ug/1 - L (aqueous)J ppb « up/kg - S (solid)

fied compounds see Analytical Data Sheets in the appendices)

El I'jrent /Compound I'Ajne

I/ ^

7

Ij/ ^J/ x{J./ // ^ / • / /

§ -N§/ ?/ /

——— _~

—— —— .

it0

.._. .....

.«0«>

.

i

HOP,

'

, .,. . • ..

-: ;

•

|

._..

5- 31

f.212

2̂ 1

t-=.•

• - - — - ~ —

I—— - ——— •

!

J Ccr r.-t-nt S

—————— .

_... _ .... ... .

i-an! .00212

Sheet .̂ of JjL

ECOLOGY AND ENVIRONMENT, INC.TOXICOLOGICAL ASSESSMENT

SITE: Kimberton__________TDD NO.: F3-8203-22EPA NO.: PA-423DATE: July 23. 1982

Based on review of Background Information, Site Observations and Laboratory AnalyticalData, the following conclusions are indicated:

I I There is no indication of an imminent or severe adverse toxicological impactto public health or the environment.

There are possible indication(s) of potential adverse toxicological and/orenvironmental impact. A more compreshensive Site Investigation and SamplingProgram is recommended.

| Xx| A review of the information presented herein is sufficient to indicatea potential adverse impact on human health and/or the environment. AToxicological Impact Assessment is advised.

Comments:Sample analyzed by the PA DER show a number of household drinking wells in the

vicinity of the TCE lagoons to be contaminated with 1,2-dichloroethylene, trichloro-ethylene (TCE), 1,1-dichloroethylene and 1,1,1,-trichloroethane. Of greatest concern arethe wells serving the Davis household (1,200 ppb-DCE and 600 ppb TCE), Ludwig household(1,200 ppb-DCE and 500 ppb TCE), Manger's home and the Kimberton Country House Restaurance(400 ppb-DCE and 200 ppb TCE). Although these compounds have low acute toxicities, TCE isa suspected carcinogen. Inhalation as a results of showering in Davis', Ludwig's andManager's horres i**v provide s «itrific«Pt additiorfl exposure to these volatile compounds.

Samples collected by FIT Region III reveal relatively high concentrations of varioustoxic metals in the lagoon samples. Lead was detected at 38,000 ug/1 in lagoon #'s 2 and 3(Sample S-2). The potentially carcinogenic metals, arsenic at 2,400 ug/1, and chromium at13,000 ug/1 were also detected in lagoon #1 (S-l). These compounds were not detected inthe surface or ground water at this time. TCE found at the concentration of 710 ug/1 wasalso found in lagoon #'s 2 and 3 (S-2).

The downstream creek sample (S-3) shows concentrations of various carcinogenicpolynuclear aromatice hydrocarbons (benzo(a)anthracene 12 ug/1, benzo(k)fluoranthene 13ug/1). The sediment sample S-4) shows concentration of these compounds in the 11QC-1500ug/1 range. Although the creek is not used at present, it does flow through a nur r ofbackyards and may pose a problem to children playing in the creek.

A complete toxicological assessment for this site is in process.\̂

Gregg Crystal 1

ARI002I3

SITE NAME:TDD NO.:EPA NO.:

TITLE: gAmlt \QgecrijrvS «-

\

FIGURE NO.

wSOLE:

——-————— ftRI002U

SITE NAME: K^NO. ; PJTDD NO. ; PJ xWduftr* {kirk *• gâ U- j A, '.

r FIGURE NOT J \1 '

SOURCE : . ft uJKfn « ̂jmurrilie )>A

Kimberton..- TDD No. F3-8203-22

EPA NO. PA-423

PHOTOGRAPHIC LOG

ALL PHOTOGRAPHS TAKEN ON APRIL 22, 1982.

Photograph 1 - View of Lagoon #1. Photograph 2 - View of Lagoo.-,

7-1 RR 1 002 1 6

KimbertonTDD No. F3-8203-22EPA No. PA-423Photographic Log

?m%*®gf*3&3

HRI002I7

KimbertonTDD No. F3-8203-22EPA No. PA-423 V •>! , £Photographic Log

u

Photograph 3 - View of Lagoon #3. Photograph 4 - Area where sprayfield may have been (thisis not stressed vegetation,but a corn field)

7"3 HR1002I8


7-4

ARI002I9

Kimberton ;"TDD No. F3-8203-22EPA No. PA-423 ^ , s .,Photographic Log '*" ! '•

Photograph 5 - Sampling downstream Photograph 6 - Upstream creek (S-5;creek (S-3)

7-5

ARI00220


jkiW&L.

7-6

ARI0022I

KimbertonU T D D No. F3-8203-22

EPA No. PA-423Photographic Log

Photograph 7 - Fitzsimmons Pond (S-9) Photograph 8 - Gotwalls Pond (S-ll)

7-7

ARI00222


ARI00223

v\ARI00221*

; :i'^ ?\ f.

ft

J " • » £ : ! - £ - *;:v ~ ;: - - ~ ^

I I

5

*\.

;V ;V

j i -i- i — i-

! I

t- i- '• ; : ! . '• '" ftR 100226

y5 UNITED STATES ENVIRONMENTAL PROTECTION AGENCYJ REGION III

.„ jcT CENTRAL REGIONAL LABORATORY839 BESTGATE ROAD 301-224-2740

ANNAPOLIS. MARYLAND 21401 FTS-922-3752

DATE : May 4, 1982SUBJECT: Kimberton, VOAs by GC/MS

Superfund; 820427-01 - 03 (4/30/82 - 5/3/82) .,,-....

FROM: : Rick DreischChemist

TO: : Daniel K. DonnellyChief, Lab Section

THRU : John Austin Vf^Team Leader,"Organic Analysis Unit

The above samples were analyzed by purge and trap methodology for volatileorganics using the mass spectrometer as the detector. The samples weresolids, therefore a representative subset was taken and analyzed accordingto the procedures established for solids in the fish and sediment analysisof last year. The values reported are in ng/g of material. The nominaldetection limit was 1 ppb.

Table 1Sample ? Identification

820427-01 Kimberton, #1 Lagoon #102 Kimberton, #2 Lagoon 2 & 3-03 Blank-^e^. COAC

Table 2

Compounds Found (ng/g) S«\820427 -01 -02

Trichloroethylene O" T\0Unknown (57) 0.4cis-l,2-Dichloroethylene — 1-10

RO/ad

cc: P. J. KrantzQAO, CRL

ARI00227

U.S. ENVIROWEKTAL PROTECTION AGENCY-HWI Sample Management OfficeP.O. Box 818, Alexandria, 22313 - 703/683-0885 ' Me Number

ORGANICS ANALYSIS DATA SHEET

Laboratory Nome Mead CompuChem____ §> •• ̂Lab Sample ID NO. \^\\^i JfrlS,':*.'.-OCR

21A

22A

24A

31A34A

57A

58A

59A

60A

64A

65A

IB98

esSB

12B18B

20B

25826B

27B

28B

35B

368

37B

396

403

•port NO. it'£7fi1~tr

f Sample Number3» 2 KORGANICS ANALYSIS DATA SHEET-Page 2 fr4J\D>̂ -C.lrVH i

Laboratory Name Head CompuChemLab Sample ID NO. \^}J) 0k - • - . . »

QC Report NO. //-S7. /7-t/k. 37-97

2V

3V

4V

6V

TV

10V

11V

13V.

14V

13V

16V

19V

23V

29V

30V

32V33V38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V87V

83V

f

VOLATILES

aerolefnaerylonltrllebenzenecarbon tetrachlorldeeh 1 orobenzene1 ,2-d leh 1 oroethane1,1,1-trlchloroethane

1 , 1-d 1 eh 1 oroethane1, 1,2-trlehloroethane1, 1,2,2-tetraehloroethane

chloroethane2-ch loroethyl vinyl etherchloroform

1, 1-41 eh 1 oroethy 1 ene1 , 2-tr ans-d 1 ch 1 oroethy 1 ene1 , 2-d 1 ch 1 oropropane1,3-dlchloropropyleneethyl benzenemethyl ene chloride

methyl chloride•ethyl bromidebromoformdlchlorobromomethane

tr 1 ch 1 orof 1 uoromethaned 1 eh 1 orod 1 f 1 uoromethaneeh 1 orod 1 bromomethanetetraeh 1 oroethy 1 enetoluenetr 1 eh 1 oroethy 1 enevinyl chloride

ug/1NDND

NO

ND

ND

ND

ND

ND

ND

NO

ND

ND

NO

ND

cl̂ > -ND

ND

ND

ND

ND

NO

ND

NO

ND

ND

NO

ND

NDi#

ND

PESTICIDES

89P aldrln90P dleldrtn91P ehlordane92P 4,4»-DOT

93P 4.4'-ODE

94P 4,4«-ODD

95P a 1 pha-endosu 1 f an96P beta-endosulfan

97P endosulfan sulfate96P endrln

99P endrln aldehyde100? heptacMor101P heptachlor epoxide

102P alpha-BHC103P beta-SHC104P delta-BHC105P gamna-BHC

106P PCS- 1242

107P PCS- 1254

108P PCS- 1221

109P PC8-I232

HOP PCS- 1248

111P PC8-1260

112P PCS- 101 6

1 13P toxaphene

DIOXINS

1293 2,3,7.8-tetrachlorodlbenzo-

p-dloxln

ug/1NDND

ND

ND

ND

ND

NO

ND

ND

NO

ND

ND

ND

ND

NO

ND

ND

ND

NO

ND

ND

ND

NO

ND

ND

ND

*La$» than 10 ug/1

NO » NOT DETECTED (pesticides less than, lug/I) A n O 0 QI 00££j

ORGANICS ANALYSIS DATA SHEET - Page 4

Lab Name; MEAD CQMPUCHEH ' '

QC REPORT NO: lt'£7,/7-

U.S. ENVIRONMENTAL PROTECTION "̂ NCY-HNI Sample Management OfficeP.O. Box 813, Alexandria, VA ,13 - 703/633-0885 Sample Number

ORGANICS ANALYSIS DATA SHEET - Page ' 1 | |

Laboratory Name Mead CompuChem Case Number 1 0 1 *S

LaboratoryLab Sample

107-02-6

107-13-171-43-2

56-23-5108-90-7

107-06-2

71-55-6

75-34-3

79-00-579-34-5

75-00-3

110-75-8

67-66-3

75-35-4

156-60-5

78-87-5

10061-OX-XX

100-41-4

75-09-2

74-87-3

74-83-9

75-25-2

75-27-4

75-69-4

75-71-8

124-48-1

127-18-4

106-88-3

79-01-6

75-01-4

ORGANICS ANALYSIS

I

torn* Mead CompuChem

ID NO. t ̂ 1 £3i \

VOLATILES ug/gacroleln 0.10U ieery Ion Itr lie 0.10U

benzene 0.01U *carbon tetrach lor Ide 0.01Uehlorobenzene 0.01U1,2-dlchloroethane 0.01U1,1,1-trlchloroethane ' 0.01U

1,1-dlchloroethan« 0.01U1,1,2-trlehloroethane 0.01U1,1,2,2-tetrechloroethane O.OIUchl oroethane 0.01U

2-ch loroethyl vinyl ether 0.01Uchloroform O.OIU1,1-dlchleroethene 0.01U1,2-trans-dlchloroethene 0.01U1,2-dlehloropropane O.OIU1,3-dlehloroproplene 0.01Uethyl benzene 0.0 1U•ethyl ene chloride 6£5Lehloromethane C.01UbroBomethane Q.01Ubroaoform . O.OIUdlehlorebroMomethane 0.01UtrlehlorofluoroMthane 0.01Udlchlorodlfl uoromethane 0.01UchlorodlbronoMthane O.OIU

tetraehleroethylene O.OIUtoluene O.'OIUtrlehloroethylene 0.01Uvinyl chloride O.OIU

DATA SHEET-Page. . Sample Number

Case Number | Q \ *^~

CC Report to. y/-//5,«'/-/Af,

I

31tu

3 a

«/»

glib

|

d

1H.•—. uV>

Uj "- ^

If cvVI

I$

~HV

1?

• 7a- e

in

ARI00233

* -

U.S. ENVIRONMENTAL PROTECTION AGENCY-HWI Sample Management Office CliiQlS*- C.\ST O ^P.O. Box 816, Alexandr VA 22313 - 703/683-0885

ORGANICS ANALYSIS DATA

Laboratory Name Mead CompuChem

iemple Number -^

SHEET , l/t>47T>£»VH. £f*C4l/C

!' s-sLab Sample 10 NO. _JS_IJ 1QC Report NO. tf.S7. /7-«/fe, *7-phthalatabutyl benzyl phthalatedl-n-butyl phthalatedl-n-octyl phthalatedlethyl phthalatedimethyl phthalatebenzo(a )anthrecenebenzo(e)pyrene3,4-benzof luoranthenebenzo (k)f luoranthenechrysene

acenaphthylene

anthracenebenzo (ghl )perylanefluorenephenanthrenedl benzo (e,h)enthracenelndeno(1,2,3-cd)pyrene

pyrene

-,*'.ug/lND

ND

ND

ND

ND

ND

ND

» ^NA /— - /: /ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ARI00234

Sample NumberORGANICS ANALYSIS DATA SHEET-Page 2


Lab Sample 10 NO. | ̂ | \ \

CC Report NO. ifS7. /?~9*. ̂7-y

2V

3V

4V

6V

TV

10V

11V

13V

14V

13V

16V

19V

23V

29V

30V

32V33V38V

44V

43V

46V.

47V

48V

49V

50V

31V

85V

86V

87V

88V

VOLATILES

acrolelnacrylonltrllebenzenecarbon tetrachlorldeeh 1 orobenzene1 ,2-d 1 ch 1 oroethane

1,1,1-trlchl oroethane1 . 1-d 1 ch 1 oroethane

1*1, 2-tr 1 ch 1 oroethane1*1,2, 2-tetrach 1 oroethanechl oroethane «.2-ch 1 or oethyl vinyl etherchloroform1.1-dlchloroethylene

1 • 2-trans-d 1 ch 1 oroethy 1 en*

1,2-dlchloropropana1 , 3-d 1 eh 1 oropropy 1 eneethyl benzenemethyl ene chloride

methyl chloridemethyl bromidebromoforndlchlorobroraomethane

tr 1 ch 1 orof 1 uoromethaned leh 1 orod If 1 uoromethaneeh 1 orod 1 br omomethan*tetrach 1 oroethy 1 ene

toluenetrl chl oroethy lenevinyl chloride

7

ug/1NDND

ND

ND

ND

ND

ND

ND

ND

ND

NO

ND

ND

ND

ND

ND

ND

NO

NO

ND

ND

ND

NO

ND

ND

ND

ND

ND

ND

ND

.:>:.; |\

•


Lab Name; MEAD COMPUCHEM

QC REPORT NO: / f -S7f /T-Dl. 2l-U 7 1

B. TENTATIVELY IDENTIFIED COMPOUNDS °''•' v '

SAMPLE

12

34

5

6

7

8

9

1011

12

13/14

15

16

17

18

19

20

21222324

25

26

27

28

29

y30

CAS t

CD

©>

COMPOUND NAME

Ancs4

U.S. ENVIRONMENTAL PROTECTION AGENCY-HWI Sample Management OfficeP.O. Box 313, Alexandria, V. .2313 - 703/633-0835

ORGANICS ANALYSIS DATA SHEET - Pag


Lab Sample ID NO. \C>\^O ^1 —Signature of Person Authorized to Release Data: (JL.rd

ACID COMPOUNDS

88-06-2 2,4,6-trlchlorophenol59-50-7 p-chloro-*-cresol

95-57-8 2-chlorophenol122-83-2 2,4-dlchlorophenol105-67-9 2,4-dlmethylphenol

88-75-5 2-nltrophenol

100-02-7 4-nltrophenol

31-68-3 2,4-4 In Itrophenol

534-32-1 4,6 dlnltro-o-cresol87-86-5 pentach lorophenol108-95-2 phenol

BASE/NEUTRAL COMPOUNDS

83-32-9 acenaphthene

92-37-3 benzldlne120-82-1 1,2.4-trlchlorobenzene1 1 8-74- 1 hexach 1 orobenzene

67-72-1 hexaeh 1 oroethane111-44-4 bls(2-chl oroethy nether91-58-7 2-chloronaphthalene95-50-1 1,2-dl chl orobenzene541-73-1 1,3-dlchlorobenzene106-46-7 1,4-dlchlorobenzene91-94-1 3,3'-dlehlorobenzldlne121-14-2 2,4-dlnltrotoluene606-20-2 2,6-dlnltrotoluene

1 , 2-d 1 pheny 1 hydraz 1 ne122-66-7 (as azobenzene)206-44-0 f luoranthene7005-72-3 4-chlorophenyl phenyl ether

"9/9

0.2U 101-55-3

0.4U 39633-32-9

0.2U 111-91-10.2U 87-63-3

0.2U 77-47-4

0.2U 78-59-1

1.8U 91-20-3

0.8U 98-95-3

0.4U NA

0.5U 86-30-6

0.2U 621-64-7

117-81-7

85-68-7

84-74-2

0.2U 117-84-0

0.5U 84-66-2

0.2U 131-11-30.2U 56-55-3

0.2U 50-33-8

0.2U 205-99-20.2U 207-08-9

0.2U 318-01-9

0.2U 208-96-3

0.2U 120-12-7

0.2U 181-24-2

0.2U 86-73-7

0.2U 85-01-8

0.2U 33-70-3

0.2U 183-39-3

0.2U 129-00-0

SampTe Number

Case Number \ O| f̂

CC Report N». y/̂ //3. IZ-foJ.Vd-fCil


4-bronophenyl phenyl etherbls-(2-chlorolsopropyl Jether

bl s ( 2-ch 1 oroethoxy Imethanehexach 1 orobutad 1 enehexach 1 orocye 1 opentad 1 eneIsophoronenaphthalene

nitrobenzene

N-n i trosod 1 methy 1 am 1 ne

N-n 1 trosod 1 pheny 1 an 1 ne

NHI 1 trosod 1 -n-propy 1 an 1 neb 1 s ( 2-ethy | hexy 1 )phtha 1 atebutyl benzyl phthalatedl-n-butyl phthalatedl-n-oetyl phthalatedl ethyl phthalatedimethyl phthalatebenza(a )anthracenebenzo(a)pyrene3, 4-benzof 1 uorantheneben zo(k)f luoranthenechryseneacenaphthyleneanthracenebenzo(ght )perylenefloor ene

phenanthrene

dlbenzo(a,h)antnracenelndeno( 1,2,3-cd)pyrene

pyrene

VICINAL•i-r^i

"9/90.2U

0.2U

0.2U0.2U

0.2U

0.2U

0.2U

0.2UNA

0.2U

0.2U

0.2U

0.2U

0.2U0.2U

0.2U

0.2U £

0,? tf"

0.2U

0.3 t£to.? i/J0.2 ifj0.2U ̂

0.2- «TT0.5U0,2- eTo.y 4-J0.5U

0.5U

0.5

Sample NumberORGANICS ANALYSIS DATA SHEET-Page 2 '

Laboratory Name Mead CompuChem____ • Case Number \ CM 5^____

Lab Sample 10 NO. If̂ -̂O & ReP°rt *>• V/'Iff.M-fty M-feS ': ''-il /

107-02-8

107-13-1

71-43-2

56-23-5106-90-7

107-06-2

71-55-6

75-34-3

79-00-5

79-34-5

75-00-3110-75-8

67-66-3

75-35-4

156-60-5

78-87-5

10061-OX-XX

100-41-4

75-09-2

74-87-3

74-83-9

75-25-2

75-27-4

75-69-4

75-71-8

124-48-1

127-18-4

108-88-379-01-6

75-01-4

VOLATILES

acrolelnacrylonltrlle

benzenecarbon tetrach lor Idachl orobenzene1,2̂ Jlchloroethane

1,1, t-tr 1 ch 1 oroethane1 , W leh loroethane1, 1,2-tr Ichloroethane1* 1, 2, 2-tetrech loroethane

eh loroethane2-ch lor oethyl vinyl etherchloroformUWI eh loroethene1,2-trans-̂ lchloroethene1,2-dlehleropropane1 , 3-d lehloroprop lene•thy (benzene

•ethyl ene chloride O>t>(»\ehloromethanebroMmethanebromofom

d 1 eh lorobromomethanetr leh 1 orof 1 uoromethaned leh lorod 1 f 1 uoromethanech lorod 1 bromoMthanetetrach 1 oroethy 1 enetoluenetr 1 eh 1 oroethy 1 enevinyl chloride

0.10U0.101)O.OIU

0.01U0.01U f

O.OIU

0.01U I -

0.01U I

O.OIU0.01U

o.otu0.01U

0.01U

0.01U •

0.01U '0.01U

O.OIU •'0.01U

1* • i0.01U

0.01U i

o.oiu ;0.01U

o.oiu !0.01U ;

0.01U ;0.01U0.01U

0.01U

0.01U

309-00-2

60-57-1

57-74-9

50-29-372-55-9

72-54-8

115-29-7

115-29-7

1031-07-878-20-8

7421-43-4

76-44-6

1024-57-3

319-84-6

319-85-7

319-66-8

58-89-9

53469-21-911097-69-7

11104-28-2

11141-16-5

12672-24-6

11096-82-5

12674-11-2

8001-35-2

1746-01-6

PESTICIDES

aldrln

dleldrlnchlordane4,4«-OOT

4,4'-DC€

4,4

(ASi

UtO

a

^

UJ

3 3

, 3UJ

C/}

gu!

dI

3

3 « P"o2 -.

00

1500

\nooCM in to

ARI00239

U.S. ENVIRONMENTAL PROTECTION AGENCY-Htfl Sample Management OfficeP.O. Box 818, Alexandria, f V 22313 - 703/683-0885

ORGANICS ANALYSIS DATA SHEET - Pai


Lab Sample ID NO. l£y| Q^ S7

Sample Number

Vt CLIolnje 1 ' * j

Case Number \ (~̂\ ^" ^ » *J

OC Report ND. y/.//3,V2-/oJ.V̂ -r*ĈSignature of Person Authorized to Release Data: $$*$ ̂ f̂fld&S

ACID COMPOUNDS

88-06-2 2,4,6-trlchlorophenol

59-50-7 p-chloroHR-cresol

95-57-6 2-chlerophenol122-83-2 2,4-dlchlorophenol

105-67-9 2,4-dlmethy (phenol

88-75-5 2-nltrophenol100-02-7 4-n i tropheno 1

51-88-5 2,4-dlnltrophenol534-52-1 4,6 dlnltro-o-cresol87-66-5 pentach lorophenol108-95-2 phenol


83-32-9 acenaphthene92-67-5 .benzldlne120-82-1 1.2,4-trlehlorobenzene118-74-1 hexachlorobenzene

67-72-1 hexach loroethaneH1.44-4 bis (2-ch loroethyDether91-58-7 2-ch 1 oronaphtha lene95-50-1 1,2-dlchlorobenzene

541-73-1 1,3-dlchlorobenzene106-46-7 1,4-41 eh 1 orobenzene91-94-1 3,3'-dlchlorobenzl

NumberORGANICS ANALYSIS DATA SHEET-Page 2

Laboratory Name Mead CompuChem Case Number \ Q\Lab Sample '0 NO. \ ̂ \ £>7V CC Report Ms.

VOLATILES ug/g PESTICIDES ug/g

107-02-8 acroleln___________0.10U 309-00-2 aldrln____________O.Q1UJQ7-13-1 acrylonltrlle________O.IOU 60-57-1____dleldrln___________0.01U71-43-2 benzene____________0.01U 37-74-9____chlordane__________0.01U56-23-5 carbon tetrach I or I de 0.01U 50-29-3____4,4«-DDT___________Q.Q1U108-90-7 chl orobenzene________O.OIU 72-55-9____4,4«-ODE___________0.01U

107-06-2 1.2-dlchloroethane_____O.Q1U 72-54-8____4,4»-DDO___________0.0 IU

71-55-6 1,1,1-trlchloroethane 0.01U 115-29-7 endosulfan I 0.01U

75-34-3 1,1-̂ I eh I oroethane_____O.Q1U 115-29-7 endosulfan II________0.01U79-00-5 1,I,2-trIchloroethane 0.01U 1031-07-8 endosulfan sulfate 0.01U79-34-3 1,1,2,2-tetrachloroethane 0.01U 78-20-8____endrln________._____0.01U75-00-3 chl oroethane______ O.Q1U 7421-43-4 endrln aldehyde______0.01U110-75-8 2-chloroethylvlnyl ether 0.01U 76-44-8 heptachlor__________0.01U , j67-66-3 chloroform 0.01U 1024-57-3 heptachlor epoxlde 0.01U75-35-4 1,1-dlehloroethene_____O.Q1U 319-64-6 BHC-Alpha___________0.01U

156-60-5 1,2-trans-dlchloroethene O.Q1U 319-83-7 BHC-Beta___________0.01U78-87-3 1,2-dlchloropropane 0.01U 319-86-8 BHC-Oalta 0.01U

10061-OX-XX 1,3-dlchloroproplene 0.01U 58-89-9 BHC-Gama 0.01U

100-41-4 ethyl benzene_________0.01U 53469-21-9 PCS-1242___________0.01U

75-09-2 aethylene chloride Qo?Z 11097-69-7 PCS-1254___________0.01U

74-87-3 chloromethane 0.01U 11104-28-2 PCS-1221 0.01U74-83-9 bronoMthane 0.01U 11141-16-3 PCB-1232 O.OIU

75-25-2 bromofom 0.01U 12672-24-6 PCS-1248 0.01U

75-27-4 dlchlorobromomethane 0.01U 11096-82-5 PCS-1260 0.01U75-69-4 tr leh I orof I uoromethane 0.01U 12674-11-2 PCS-1016 0.01U75-71-8 dlchlorodlfluoromethane O.OIU 8001-35-2 toxapnene 0.04U124-48-1 chlorodlbromoaethane O.Q1U127-18-4 tetrachIoroethyIene____Q.Q1U OIOXIHS108-88-3 toluene 0.01U79-01-6 tr I eh I oroethy I ene_____0.01U 2,3,7,8-tetrachlorodlbenzo-75-01-4 vinyl chloride______ 0.01U 1746-01-6 p-dloxln__________ 0.01U

•Uss than 0,2 ug/l(pesticides less than, 0.01

CO

rJrW

**» i 01 «i «ci «ei ari _g

wgb!

£ fe

•M

^Ui

§1 tn

CSJ

RI.002U2

U.S. ENVIRONMENTAL PROTECTION AGENCY-HMI Sample Management OfficeP.O. Box 813, Alexandria. 22313 - 703/683-0885


Laboratory Name Mead CompuChemLab Sample ID NO. \F?\l«ACC Report NO. 18-37. /7~ Hk. &7-U7

21A

22A24A

31A

34A

37A

58A

59A

60A

64A

65A

19

5989

99

129

189209

259269

279

289

359369378

399

403

AC 10 COMPOUNDS

2, 4, 6-tr 1 eh 1 oropheno 1

p-ch 1 oro-o-cr eso 12-ch 1 oropheno 1 .

2,4-dlchlorophenol

2,4-dlmethylphenol

2-nltrophenol4-nltrophenol

2,4-dlnltrophenol

4,6-dlnltro-o-cresolpentach 1 oropheno 1

phenol


acenaphthenebenzldlne1,2,4-trlchlorobenzenehexach 1 orobenzenehexaeh loroethanebls(2-chloroethyl 3 ether2-ch 1 oronaphtha 1 ene1,2-dlchlorobenzene1,3-dlchlorobenzene1,4-dlchlorobenzena3,3'-dlchlorobenzldlne2,4-dlnltrotoluene2,6-dlnltrotoluene1 , 2-d 1 pheny 1 hydr az 1 ne(as azobenzene)f luoranthene4-chlorophenyl phenyl ether

ug/1ND

NO

NO

ND

ND

ND

ND

ND

ND

NO

NO

NO

ND

NO

NO

. NO

NA

ND

ND

ND

ND

ND

NO

ND

NO

ND

NO

419

429

438

528

539549

553568

618629

638663

678

688

698

703719

729

739

749

753

768

778

788

798

808818

828838

848

r^Wlnrv^AiS-2


4-oromophenyl phenyl etherbls-(2-

•*•# r»

F Sample NumberORGANICS ANALYSIS DATA SHEET-Page 2


Lab Sample ID NO. J^JJj-1

CC Report NO. /ff. ST. /1'tff.. St7-lf1

2v -

3V4V

6V

7V

10V

11V

13V

14V

15V

16V

19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

65V

66V

87V

B8V

VOLATILES

aero lainaery Ion Itr Hebenzenecarbon tetrach lor Ida

eh 1 orobenzene

1 , 2-d 1 ch 1 oroethane1 , 1 , 1 -tr 1 eh 1 oroethane1,1̂ 1 chl oroethane

1 , 1 , 2-tr 1 ch 1 oroethane1,1,2, 2-tetrach 1 oroethaneeh loroethane2̂ hl oroethy 1 vinyl ether

chloroform

1,1-4lchloroethylene

1 ,2-trans-4 leh 1 oroethy 1 ene1 » 2-4 leh loropropane1 , 3-d 1 eh 1 oropropy laneethyl benzene

•ethyl ene chloride•ethyl chloride

•ethyl bromidebrofflofornd 1 eh 1 orobromomethanetr leh lorof 1 uoromethaned leh i erod 1 f 1 uoromethaneeh 1 orod 1 bromomethane

tetrach 1 oroethy 1 enetoluene*trl chl oroethy lene

vinyl chloride

•g/jND

ND

ND

ND

ND

ND

ND

ND

ND

ND. jo

ND' ND"ND

ND

NDND

. ND

ND

ND

ND

ND

'"" ND.. ,.,,.̂.. .

ND

ND

ND

ND

ND

• ND

PESTICIDES

89P aldrln90P dleldrln91P ehlordane92P 4,4 '-DOT

93P 4,4'-OC€

94P 4,4'-DOD

95P alpha-endosulfan96P bete-endosulfen97P endosulfan sulfate

98P endrln

99P endrln aldehyde(OOP heptachlor

101P heptachlor epoxlde102P alpha-BHC103P beta-BHC104P delte-BHC105P gamma -BHC106P PCS- 1242

107P PCS- 1254

108P PCS-1221

109P PCB-1232

HOP PCS- 1248

11 IP FCB-1260

112P FC8-1016

113P toxaphene

DIOXINS

1298 2.3,7,8-tetrachlorodlbenzo-

p-dloxln

ug/1NDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

- - *Lass than 10 ug/1

ND « NOT DETECTED n».«+i.i— •.», than, lug/I) A R I 0 0 2 U H

ORGANICS ANALYSIS DATA SHEET - Page t

Lab Name: MEAD COMPUCHEM \ *51 \

REPORT NO: l9-f7.tJ~tlk,37~V7 SAMPLE NUMBER

3. TENTATIVELY IDENTIFIED COMPOUNDS

\

2

3

4

5

6

7

3

9

10

H

12

13

14

13

16

17

18

19

20

21

22

23

24

25

26

27

28

9

30

CAS i

CD

COMPOUND NAME

PUPAlCi- Q b-fiISM l-TYCMCTf\YL£THYLV̂ M£7/#t

•

.

FRACTION

ftlu

•

) MAXtMLM SCORE ATTAINEDMASS MATCHING ROUTINESPur fa(SPECIFY)1

50 9o

^

*

v

J

U.S. ENVIRONMENTAL PROTECTION AGENCY-HWI Sample Management Office



Lab Sample ID NO. \*?>\\3>QC Report NO. //-̂ 7; /7-«/4;̂ 7- V?

VOLATILES

2V acroleln

3V aerylonltrlle

4V benzene

6V carbon tetrachlorlde7V chl orobenzene

10V 1,2-4 leh loroethane

11V 1,1,1-trlchloroethane13V 1,1-d leh loroethane14V 1,1.2-tr leh loroethane1 5V 1,1.2. 2-tetrach 1 oroethane

16V chl oroethane19V 2-ch 1 oroethy 1 vinyl ether23V chloroform29V 1,1-d I chl oroethy lene

30V 1, 2-tr an s-41 chl oroethy lene

32V 1,2-dlchloropropene

33V 1,3-dlchloropropylane

38V ethyl benzene44V methyl ene chloride

45V methyl chloride46V methyl bromide

47V bromoform

48V dlchlorobromomethane

49V tr 1 eh lorofl uoromethane50V dlehlorodlfluoromethane51V chl orod Ibromomethane

85V tetrach 1 oroethy lene

86V toluene87V trlehloroethylene88V vinyl chloride

ug/1NO

ND

NO

ND

ND

NO

NO

ND

NO

NO

NO

NO

ND

NO

NO

ND

NO

NO

ND

NO

NO

ND

ND

ND

NO

ND

ND

NO

NO

ND

V • . -

:

' : :T '• '' ;3 *•""; * • ' . . - ' , 'ORGANICS ANALYSIS DATA SHEET - Page 4

Ub Name; MEAD COMPUCHEM

QC REPORT NO: SAMPLE NUMBER

B. TENTATIVELY IDENTIFIED COMPOUNDS-̂S

{ '

(

12

34

56

7

6

9

10

11

12

13/I4

15

1617

16

1920

21222324

25

2627

28

29

V)

CAS t COMPOUND NAME

ŴK, ̂ tVw —— ttL,

* , - . • - •

.......

r - •=..

,. , .... .

"

e

„.

FRACTION

•

% MAXIMUM SCORE ATTAINEDMASS MATCHING ROUTINES

(SPECIFY)

.

•

*(

•

•

ARI002148

U.S. ENVIRONMENTAL PROTECTION AGENCY-HWI Sample Management OfficeP.O.' Bex 818, Alexandria, v* 22313 - 703/683-0885 Srmole Number

ORGANICS ANALYSIS DATA SHEET

Laboratory Name Mead CompuChemLab Sample 10 NO. t̂ rf .,.." K0&'7* •!?' "*4OC Report NO. If- Si, /7-

NumberORGANICS ANALYSIS DATA SHEET-Page 2

Sample Ninif?-pi


Lab Sample ID NO.

QC Report NO. f f-5y//7-Jffc/J7«

lab ferny: MEAD COMPUCHEM


\s\\s

COMPOUND NAME

-?£»̂ «. -4— -VL.~

,

,

FRACTION

•

.

i MAXIMA SCORE ATTAINEDMASS MATCHING ROUTINES

(SPECIFY)

e

v

-

/

J

/

ARI0025I

U.S. ENVIRONMENTAL PROTECTION AGENCY-HHI Sample Management Office ££ 1 Ql*7— Ojr'il̂ SP.O. Box 816, Alexandria A 22313 - 703/683-0885


Laboratory Name Mead CompuChem Jti



Lab Sample ID NO. \r^\\CJ;

CC Report NO. / f-Sf. /?.

ORGANICS ANALYSIS DATA SHEET - Rage 4

Lab Name; MEAD COMPUCHEM ' :.

QC REPORT NO: jg-se. l7>Vt.2l-U7 SAMPLE NUMBER

^

i2

34

56

7

e9

10

1112

13y'u1516

17

18

19

20

21222324

25

26

27

28

29

V)

CAS f

£D

•

B. TENTATIVELY IDENTIFIED COMPOUNDS 'pB!- •

COMPOUND NAME

; —p . 77 n

,. • -:!:

. .•. '

" ,

' • •

FRACTION

Aê &.

•

% MAXIMUM SCORE ATTAINEDMASS MATCHING ROUTINESP '-te.(SPECIFY)/

*?2*7o

AR 100251*

U.S. ENVIRONMENTAL PROTECTION AGENCY-HWI Sample Management Office ______P.O. Box 818, Alexandria, 22313 - 703/683-0885 "I la Number

ORGANICS ANALYSIS. DATA SHEET ,.tvw~ ~ .,}**&*

Laboratory Name Mead CompuChemLab Sample ID NO. | PS \ \ H CCSW*'ĵ ,\!\; • /- ~?CC Report NO. (f-S7. 17-tH*. -»7-V7 .•*„.,. . bl s(2-ch 1 oroethoxy )mtftr{ah»ladelphia NOhexach 1 orobutad 1 enehexaeh 1 orocyc 1 opentad 1 eneIsophoronenaphtha lanenitrobenzeneN-n 1 trosod 1 methy 1 am 1 neN-n 1 trosod 1 pheny 1 amlne

N-n Itrosod 1 -fl-propy 1 am 1 nebls(2-ethylhexyl )phthalatabutyl benzyl phthalatedl-n-butyl phthalatedl-n-octyl phthalatedl ethyl phthalatedimethyl phthalate

benzo (a ) anthracenebenzo(a)pyrene3, 4-benzof 1 uorantheneben zo(k)f luoranthene

chryseneaeanaphthyleneanthracene

benzo (ghl )perylenefluorenephenanthrened 1 benzo(a,h ) anthracenelndeno( 1,2,3-ed)pyrene

pyrene

NO

ND

ND

ND

ND

NA

ND

ND

NO

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

NO

ND

ND

NO

NO

ND

ND

ND

...rĉ AIM00255

Sample NumberORGANICS ANALYSIS DATA SHEET-Page 2 n


Lab Sample ID NO. \5"| \OOC Report NO. /f-57, lT-*ttf /7-V7

VOLATILES

2V acroleln3V acrylonltrlle

4V benzene6V carbon tetrach lor Ida

TV eh 1 orobenzene10V 1,2-dlchloroethene

11V 1,1,1-tr leh loroethane13V 1,1-4 leh loroethane

14V 1,1,2-tr leh loroethane

15V 1,1,2,2-tetrachloroethane16V eh loroethane19V 2-chloroethyl vinyl ether23V chloroform

29V 1,1-d leh loroethy lene

30V 1,2-trans-d leh loroethy lane32V 1 , 2-4 1 ch 1 eropropane33V 1 , 3-41 eh loropropy lene38V ethyl benzene

44V methyl ene chloride45V methyl chloride46V methyl bromide *.

47V bromoform48V d 1 eh 1 erobromomethane

49V tr leh lorofl uoromethane50V dlehloreOlfluoroaethane51V chl orod tbrotnomethene65V tetrach loroethy leneB6V toluene67V trl chl oroethy lene68V vinyl chloride

ug/1ND

NDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

NDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

• • • ' . t *'M.\

r r;. •

PESTICIDES

89P aldrln90P dleldrln

91P ehlordane92P 4,4'-OOT

93P 4,4«-DDE

94P 4,4«-DOD

95P alpha-endosulfan96P beta-«ndosulfan

•97P endosulfan sulfete98P endrln99P endrln aldehyde100P heptaehlor101P heptachlor epoxlde102P alpha-BHC103P beta-BHC104P delta-BHC105P gamma -BHC106P- PC8-1242

107P PCS- 1254

108P PCS- 1221

109P PCB-1232

HOP PCS- 1248

HIP PCS- 1260

112P PCB-1016

. I13P toxaphene

OIOXINS

1296 2,3,7,8-tetrechlorodlbenzo-

p-4loxln

ug/1ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

*Less than 10 ug/1

ND * NOT DETECTED (pesticides lass than, lug/I) • n I 00956


Lab Name; MEAD COMPUCHEM

QC REPORT NO: lf-S7.l7-tiL. 27-V7 SAMPLE NUMBER

12

34

567

a9

10

11

12

1314

15

16

17

18

19

20

21

22

23

24

23

26

27

28

29

30

CAS i

snCOMPOUND NAME

1 7. n-TrtJc.ce.+^fe.ntYn+rile. * e î -*"f . A ' * /

'

'

•

FRACTION

-/J

•

•

t MAXIMLM SCORE ATTAINED"MASS MATCHING ROUTINES

(SPECIFY*/

55%

.

•

^

v

ARI00257

U.S. ENVIRONMENTAL PROTECTION «NCY-HHI Sample Management OfficeP.O. Box 818, Alexandria, VA ̂ 313 - 703/683-0885 E ample Number

î nu?ORGANICS ANALYSIS DATA SHEET - Page ^» i'l *.y t

*-* V ' W * • • ^^B

Laboratory Name Mead CompuChem -. . Case Number _J O ^ ?S

Lab Sample ID NO. \?S"\ \Q x-)/-\$Ĉ «Porr No. f/-//S.*/2*e3M-tCtfSignature

88-06-2

39-50-7

95-57-8

122-83-2

105-67-9

88-75-5

100-02-7

51-66-5

534-52-1

87-66-5

108-95-2

63-32-9

92-87-5

120-82-1116-74-1

67-72-1111-44-4

91-58-7

95-50-1

541-73-1106-46-7

91-94-1

121-14-2

606-20-2

122-66-7

206-44-07005-72-3

of Person Authorized to Release

ACID COMPOUNDS

2,4,6-trlchlorophenol

p-ch 1 oroHft̂ reso 1

2-ch 1 oropheno 1

2,4-4lchlorophenol

2, 4-41 methyl phenol

2-nltrophenol4-nltrophenol

2,4̂ In Itrophenol4,6 dlnltro-o^resol

pentach 1 oropheno 1phenol


acenaphthenebenzldlne1 ,2,4-tr leh lorobenzenehexach 1 oroben zene

hexach loroethanebls(2-chloroethyl)ether2-ch 1 oronaphtha lene1,2-4lch»crobenzene

1 , 3-d leh lorobenzene1,4-4 leh lorobenzene3,3»-4lchlorobenzldlne

2,4-dlnltrotoluene

2,6-d In Itrotol uene1* 2-d Ipheny 1 hydrazlne

(as azobenzene)f luoranthene4-chlorophenyl phenyl ether

Data:

"9/fl0.2U0.4U

0.2U0.2U

0.2U

0.2U

1.BU

0.8U0.4U

0.5U

0.2U

0.2U

0.5U

0.2U0.2U

0.2U0.2U

0.2U0.2U0.2U

0.2U0.2U

0.2U

0.2U

0.2U

0.2U

0.2U

0.2U

101-55-3

39638-32-9

111-91-187-68-377-47-4

78-59-1

91-20-5

98-95-3NA

86-30-6

621-64-7

117-81-7

85-68-7

84-74-2117-84-0

64-66-2

131-11-356-55-3

30-33-8

205-99-2

207-08-9318-01-9

208-96-8120-12-7

181-24-2

B6-73-7

85-01-8

53-70-3

183-39-5

129-00-0

/WI&&S

BASE/ICUTRAL COMPOUNDS

4-bromophenyl phenyl ether

b 1 s -( 2-ch 1 oro 1 sopropy 1 )ether

b 1 s ( 2-ch 1 oroethoxy tawthanehexach 1 orobutad t enehexach 1 orocyc lopentad 1 eneIsophorone

naphthalene

nitrobenzeneN-n i trosod Imethy 1 am 1 ne

N-n 1 trosod 1 pheny 1 an 1 ne

N-n 1 trosod 1 -n-propy 1 am 1 ne

b 1 s ( 2-ethy 1 hexy 1 )phtha 1 ate

butyl benzyl phthalatedl-n-butyl phthalatedl-n-octyl phthalate

dl ethyl phthalatedimethyl phthalatebenzo(a )anthracene

benzo (e)pyrene

5, 4-benzof 1 uoranthenebenzo ( k ) f 1 uoranthene

ehryseneacenaphthylene

anthracene

benzo(ghl )perylene

fluorene

phenanthrene

d 1 benzo(e * h)anthracene

1 ndeno (1,2, 3-cd >pyrene

pyrene

AF

0.2U

0.2U

0.2U

0.2U

0.2U

0.2U

0.2U

0.2UNA

0.2U-

0.2U

0.2U

0.2U

0.2U0.2U

0.2U

0.2U0.2U

0.2U

0.5U

0.2U0.2U

0.2U

0.2U

0.5U

0.2U

0.5U0.5U

0.5U

0.5U

\ \ 00


Laboratory Name Mead CompuChem *'"?'&!& A,. Case Number ____\Q

Lab Sample ID NO. ^\\Q *Ke(f.1 CC Report No. V/-//3 V2V0*,

VOLATILES ug/g PESTICIDES ug/g

107-02-B acroleln___________0.10U 309-00-2 aldrln .____________O.OIU

J07-13-1 acrylonltrlle________0.10U 60-57-1____dleldrln___________Q.Q1U

71-43-2 benzene____________0.01U 57-74-9____eh I or dan e___________Q.Q1U

56-23-5 carbon tetrachlorlde 0.01U 50-29-3____4,4«-DDT___________Q.Q1U

108-90-7 chlorobenzene O.OIU 72-55-9 4,4'-00£ 0.01U

107-06-2 1,2-dlehloroethane_____0.01U 72-54-8____4,4»-ODD___________0.01U

71-55-6 1,1,1-trichloroethane O.OIU 115-29-7 endosulfan I O.OIU

75-34-3 1,1-41 ch I oroethane 0.01U 115-29-7 endosulfan II O.OIU

79-00-5 1,1,2-trlchloroethane 0.01U 1031-07-3 endosulfan sulfate_____0.01U79-34-5 1,1,2,2-tetraeh I oroethane 0.01U 78-20-8 endrln 0.01U

75-00-3 ch t oroethane ________ • O.OIU 7421-43-4 endrln aldehyde _______ O.OtU

110-75-8 2-chloroethylvlnyl ether O.OIU 76-44-8 ____ heptaehlor __________ 0.01U

67-66-3 chloroform __________ 0.01U 1024-57-3 heptachlor epoxlde _____ 0.01U

75-35-4 1,1-dlchloroethene 0.01U 319-84-6 BHC-Alpha 0.01U

156-60-5 1,2-trans-dlchloroethene 0.01U 319-85-7 BHC-Beta O.OIU78-87-3 1,2-dlchloropropane____0.01U 319-36-8 BrC-Oelta___________O.OIU

10061-OX-XX 1,3-dlchloroproplene 0.01U 58-89-9 BHC-Gama 0.01U

100-41-4 ethyl benzene_________O.OIU 53469-21-9 PCS-1242___________0.01U75-09-2 methyl ene chloride ftfelf____ 11097-69-7 PCS-1254___________O.OIU

74-87-3 chloromethane________0.01U 11104-28-2 PCS-1221___________O.OIU

74-83-9 bronenethane 0.01U 11141-16-5 PCS-1232 0.01U

75-25-2 bromofora 0.01U 12672-24-6 PCS-1248 0.01U

75-27-4 dlehlorobromonethane 0.01U 11096-82-5 PCS-1260 0.01U

75-69-4 trlehlorofluoromethane 0.01U 12674-H-2 PCS-1016___________0.01U75-71-8 dlchlorodlfluorornethane 0.01U 8001-35-2 toxaphene___________0.04U

124-48-1 chlorodlbroaoaethane O.OIU127-18-4 tetrachIoroethyIene 0.01U OIOXINS108-88-3 toluene____________0.01U79-01-6 trlchloroethylene_____0.01U 2,3,7,8-tetrach'orodlbenzo-

75-01-4 vinyl chloride_______0.01U ' 1746-01-6 p-dloxin___________0.01U*Less than 0.2 ug/1

(pesticides less than, 0.01(#¥00259

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STORET STATION NO.« SC, , Q DEPTH» D (DATE-TIME YYMHDDTTTT]D GRABtDATE-TIHB JJcOH? (2)__________L ____________l ________COHPOSITlQ Flow Prop., Q Sequential, Qsiaiple SAMPLE SPLIT NoQ Co, pjSTATE

ANALYSISP10T«w. (Wat«r)*C. P400oHP95

d. t timhos/ea3

D.O., ax|/lP30i%D.O. SAT.P61Flow, cfsP58Flow. goaP?6£6dAcidity, mg/1 (H)P410Alkalinity, zag/1P9OOHardness, mg/1P945Sulfate, mgAP80Color PT-CO 0.P70Turbidity, JCOP940Chloride, ing AP310BODS, rao;AP324* ?0. TnO/J

>fW), HKT/J

P$80TOC. m̂ /1P31&01Tot. Coli/100P31S16

RESULTS

1 1

ANALYSISPSOOTotal, 09/1 SP703CO ODissol. inq/1 LPS30 ZSrsoend. nxi/l DP50̂ SVol., ag/1P38260MBAS, og/1P32730Phenols, ue/1P720Cvanids > swr/1P1032Rex. Cr. uo/1PS50Oil-Grease, mg/1P950Fluoride, ng/1P665Total, 189/1 PP666 HDis. , rxj/1 OP660 SOĵ tho, PO4. W»/l̂P62STXN, 09/1P610NH3-N, eg/1P60SORG.-H, mg/1P620KO3-N , ITI9/1P615NO2-M. ma/1P916Tot . Ca , og/1P927

RESULTS

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ANALYSIS REQUEST AND RESULT FORM

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INORGANICS ANALYSIS DATA SHEET

1.2.3.4.5.6.*

9.10.

1.2.3.

LABORATORY NAMELAB SAMPLE ID. NO.

AluminumChromiumBariumBerylliumCadmiumCobaltCopperIronLeadNickel

ArsenicAntimonySeleniumThallium

CAL LABSS'3l%

TASK 1 (Elements to beXig/U* mg/kg' Cdfeifcle one)

^ IQ̂ 2̂>< 5^ MO

TASK 2 (Elements to beifc/J or mg/kg

US ENVIRONMENTAL PROTECTION AGENCY '1HWI Sample Management Office r _U

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1.2.3.4.5.6.

9.10.

1.2.3.4.

LABORATORY NAME CAL LABSLAB SAMPLE ID. NO. £ ZlG

TASK 1 (Elements toug/1 or rfg/ta)(circle one?

Aluminum *£&&Chromium £. \Barium 3£Beryllium ^ .-S"Cadmium ^ « /Cobalt 8*OCopper ^ SIron /4t)OLead //Nickel . -̂ */

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Arsenic *£ iAntimony î.Selenium *£ \ i.Thallium ^ \

TASK 3 (Elements to

1. Ammonia2. Cyanide3. Sulfide

CASE NO. /0/5" /5"̂

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INORGANICS ANA

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j . • s-sLYSIS DATA SHEET

CASE NO. /0/5~ /5Y

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Sample No.


LABORATORY NAME CAL LABS CASE NO. /O 1


INORGANICS ANA

1.2.3.4.5.6.

9.10.

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CAL LABS

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LYSIS DATA SHEET

CASE NO. /0/5" I5ZC,

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US ENVIRONMENTAL PROTECTION AGENCYHWI Sample Management Of fice

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TASK 1 (Elements to be/?©}) or mg/kgv — -(circle one)

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Sample No.

1.2.3.4.5.6.4

9.10.

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CAL LABS^̂ O ̂ J ̂\Ĵ 3 PN.0K.

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CASE NO. 101 *? /5$£sOC REPORT NO. S'/Ŝ f

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ecology ^nd environment, inc. -!• Specialist •••s in the ...TASK REPORT TO THE ENVIRONMENTAL...

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