DRAFT PHASE III NANO- SCALE ZERO-VALENT IRON PILOT TEST … · 2020. 11. 17. · i EXECUTIVE...

DRAFT PHASE III NANO-SCALE ZERO-VALENT IRON PILOT TEST REPORT FORMER UNIDYNAMICS FACILITY PHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITE GOODYEAR, ARIZONA by Haley & Aldrich, Inc. Phoenix, Arizona for Crane Co. Stamford, Connecticut File No. 37639-000 28 February 2011

SDMS DOCID# 1142224

28 February 2011 File No. 37639-000 Arizona and Navajo Site Section SFD-6-2 Superfund Program U.S. Environmental Protection Agency – Region 9 75 Hawthorne Street San Francisco, California 94105 Attention: Ms. Catherine Brown, Remediation Project Manager Subject: Draft Phase III Nano-scale Zero-Valent Iron Pilot Test Report – Implementation, Results, Conclusions and Recommendations Former Unidynamics Facility Phoenix-Goodyear Airport-North Superfund Site Goodyear, Arizona Dear Ms. Brown: Haley & Aldrich, Inc. is pleased to submit this report on behalf of Crane Co. regarding the Phase III Nano-scale Zero-valent Iron Pilot Test. This report provides a summary description of the pilot test activities, presents the performance monitoring results, and provides a detailed evaluation, conclusions and recommendations. Jet-assisted injection of PolyMetallixTM nano-scale zero-valent iron was determined to be an effective technology for future in-situ treatment of trichloroethene in and nearby the source area at the site. Please review and address any comments or questions you may have to Paula Chang at [email protected]. Sincerely yours, HALEY & ALDRICH, INC. Paula R. Chang Mehdi Miremadi Remediation Program Manager Senior Vice President Enclosures G:\PHX Backup\37639 Crane Co PGA-North\37639_0228_HAI_ PIIInZVI PT Report_D.docx

Haley & Aldrich, Inc. 60 E. Rio Salado Parkway

Suite 900 Tempe, AZ 85281

Tel: 480.659.1814 Fax: 480.366.5801

HaleyAldrich.com

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EXECUTIVE SUMMARY This report was prepared on behalf of Crane Co. and provides a description of the implementation and results of the Phase III Pilot Test (PT) conducted as part of the nano-scale zero-valent iron (nZVI) field testing program at the Phoenix-Goodyear Airport-North Superfund Site. The PT was conducted in accordance with the Work Plan and subsequent Response to Comments and Amendments submitted to the United States Environmental Protection Agency on 31 August 2009, 16 November 2009, and 20 November 2009, respectively. The scope of work for the PT included: Installation of two blank-cased wells for use as injection points;

Installation of six downhole sensors and pressure transducers in nearby monitoring wells for real-time monitoring of groundwater elevation, temperature, oxidation reduction potential (ORP), and pH;

Injection of 1,400 pounds (lbs) of Polyflon Company’s PolyMetallix™ nano-scale zero valent iron and 7,421 gallons of anaerobic water at a concentration of 21 grams per liter into;

– Two injection wells; and

– Two injection intervals per well:

108 to 113 feet below ground surface (bgs), and

113 to 118 feet bgs;

Collection of groundwater samples to monitor the performance of the nearby wells. The objectives of the PT were to: Demonstrate that a pressurized injection method (jet-assisted injection) can increase the nZVI

mass applied at each point and increase the ROI of injected nZVI as compared to the Phase I and II PT results;

Reduce trichloroethylene (TCE) and perchlorate concentrations within the PT area; and

Evaluate the persistence of the nZVI in the PT area; and

Asses the technical and economic feasibility of using this injection technique with PolyMetallix for potential future treatment of the source area at the site.

The PT nZVI injections were performed 2 through 5 February 2010. The nZVI injections were conducted using a combination of a jet lance injection tool and pressurized packer isolation of the target injection zone. The jet-assisted injection of anaerobic water using a 10,000-pound per square inch (psi) tri-plex pump was alternated with injection of nZVI using a piston pump. The 10,000- psi jetted water was applied to the lance to carve approximately 1/16- to 1/8-inch diameter holes through the polyvinylchloride casing and through the grout to create ten jetted conduits into the formation. The injectate piston pump then pressurized the casing between the packers to 100 to 160 psi, forcing the nZVI into the jetted conduit and creating fractures as the injectate pressure exceeded the overburden pressure. These stresses are hypothesized to result in nucleation of hydraulic fractures, increasing the distribution of the nZVI into the surrounding soils. Periodic application of the water jets was used to

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create high pressure turbulence to further mix the nZVI with soil in the vicinity of the jetted conduit and clear the casing of nZVI particles. After completion of the lower injection interval, the packers were pulled up to the next injection interval and the process was repeated. Two intervals, 113 to 118 feet bgs and 108 to 113 feet bgs, were completed at each injection well. The wells were finished with a standard flush-mount well casing and both remain in place for potential reuse in future remediation activities. A total of 7,421-gallons of highly reducing (-500 to -800 mV) nZVI particles were injected into a deep alluvial water-bearing zone within the source area. PolyMetallixTM nZVI was provided by Polyflon, a Crane Co. company, as a 35.2 gram per liter aqueous solution contained in eighteen 275-gallon totes. Each tote of nZVI was batch-mixed with anaerobic water prior to subsurface injection. The injectate used at both locations contained a combined total of 1,400 pounds of nZVI.

Monitoring Program

Prior to injection, TemphionTM probes and pressure transducers were installed in six downgradient monitoring locations. The TemphionsTM and pressure transducers were programmed to record measurements of pH, ORP, temperature, and groundwater levels every five minutes for a 10-day period. The real-time monitoring probes were left in place during the PT injections and for one week after completion of the injections. The paired downhole probes were placed at mid-screen, approximately 115 feet bgs in IRZ-MW-B, IRZ-MW-C, IRZ-MW-D, IRZ-IW-02, IRZ-IW-04, and IRZ-IW-05. PT groundwater monitoring included a baseline round, conducted prior to injection of the nZVI particles, and groundwater sampling rounds performed at weeks one and two, and months one, three, and six after injection. The baseline sampling round was conducted a week and a half prior to the injection field work. Groundwater samples were analyzed for volatile organic compounds, perchlorate, chlorate, chlorite, and hydrogen during every sampling event. Periodic samples were taken during select monitoring rounds to monitor changes in total and dissolved iron, manganese, chloride, sulfate, nitrate, alkalinity, sodium, phosphate, and total organic carbon in groundwater during the monitoring period. In accordance with the comments on the Work Plan, passive diffusion bags were placed in select monitoring wells at two depths and deployed at the same locations and depths for the month three and month six groundwater monitoring events.

Results and Conclusions

Jet-assisted injection in blank cased wells proved to be an effective method to deliver large quantities of PolyMetallix nZVI particles to the subsurface;

Groundwater data within the treatment area shows a decrease in TCE mass ranging between 63 percent and 96 percent one month after injection;

Immediate (weeks 1 and 3) degradation effect were observed at least 29 feet from injection locations;

Iron and hydrogen data shows migration of nZVI and treated groundwater as far as 45 feet downgradient, six months after injections;

Injections also mobilized TCE concentrations downgradient of the injected nZVI particles for capture at downgradient extraction wells; and

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Jet-assisted injection of PolyMetallix nano-scale zero valent iron was determined to be an effective technology for future in situ treatment of TCE in and nearby the source area at the site.

HALEY& ALDRICH

TABLE OF CONTENTS

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EXECUTIVE SUMMARY i LIST OF TABLES vi LIST OF FIGURES vi

1. SCOPE AND OBJECTIVES 1

1.1 Scope of Work 1 1.2 Objectives 1 1.3 Rationale 2

2. PILOT TEST IMPLEMENTATION 3

2.1 Injection Well Installation 3 2.2 Baseline Sampling 3 2.3 Site Preparation 4

2.3.1 Anaerobic Water Preparation 4 2.3.2 Temphion and Pressure Transducer Installation and Programming 4

2.4 Injection Procedures 5 2.4.1 Injectate Dosage and Composition 5 2.4.2 Resuspension of nZVI 5 2.4.3 Injection Activities 6

2.5 Post-Injection Performance Monitoring Program 7 2.5.1 Locations 7 2.5.2 Frequency 7 2.5.3 Analytes 7

3. RESULTS 9

3.1 Injection Monitoring and Field Observations 9 3.2 Temphion and Pressure Transducer Data 9 3.3 Groundwater Performance Monitoring Data 10

4. DATA EVALUATION 11

4.1 Field Observations and Real-time Monitoring 11 4.2 Field Parameter Evaluation 11 4.3 Groundwater Performance Monitoring Results 12

4.3.1 Trichloroethene Mass Reduction 12 4.3.2 Perchlorate 13 4.3.3 Hydrogen 13 4.3.4 Reduction-Oxidation Indicating Parameters 13 4.3.5 Passive Diffusion Bag Results 14

5. LESSONS LEARNED 15

6. CONCLUSIONS AND RECOMMENDATIONS 16

TABLE OF CONTENTS

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6.1 Comparison to Previous Pilot Test Results 16 6.2 Mass Reduction 16 6.3 Persistence of the nZVI 16 6.4 Recommendations 16

REFERENCES 18 APPENDIX A – Boring Logs and Construction Diagrams for IRZ-BW-1 and IRZ-BW-2 APPENDIX B – Daily Field Injection Logs APPENDIX C – Laboratory Data Packages

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LIST OF TABLES Table No. Title I Baseline and Performance Monitoring Analyte List II Existing Well Construction Data III nZVI Injection Data IV Field Parameter Data V Volatile Organic Compound and Perchlorate Data VI Metals and Major Ion Data VII Passive Diffusion Bag Volatile Organic Compound Data VIII Parameter Response Summary IX Mass Reduction Summary X Distances from Injection Wells to Monitoring Wells XI Lessons Learned LIST OF FIGURES Figure No. Title 1 Site Location Map 2 Injection and Monitoring Well Location Map 3 Pilot Test Field Equipment Schematic 4 Jet-assisted Injection Sequence 5 TemphionTM and Hydraulic Pressure Charts 6 pH, Dissolved Oxygen and Oxidation Reduction Time Series Charts 7 Temperature, Specific Conductivity, and Turbidity Time Series Charts

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8 Trichloroethylene Time Series Chart 9 Perchlorate Time Series Chart 10 Hydrogen Time Series Chart 11 Sulfate Time Series Chart 12 Total Iron Time Series Chart 13 North-South Cross-Section 14 East-West Cross-Section

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1. SCOPE AND OBJECTIVES This report was prepared on behalf of Crane Co., and provides a description of the implementation and results of the Phase III Pilot Test (PT) which was conducted as part of the nano-scale, zero-valent iron (nZVI) field testing program at the Phoenix-Goodyear Airport-North (PGA North) Superfund Site (Figure 1) in Goodyear, AZ. The PT was conducted in accordance with the Work Plan (ERM 2009) and subsequent Response to Comments and Amendments submitted to the United States Environmental Protection Agency (EPA) on 31 August 2009, 16 November 2009, and 20 November 2009, respectively. A summary description of the scope of work and objectives for the PT is provided in the next two subsections. The third subsection discusses the rationale for the selection of the jet-assisted injection method. 1.1 Scope of Work The scope of work for the PT included: Installation of two blank-cased wells for use as injection points (Figure 2);

Installation of six downhole sensors and pressure transducers in nearby monitoring wells for real-time monitoring of groundwater elevation, temperature, oxidation reduction potential (ORP), and pH;

Injection of 1,400 pounds (lbs) of Polyflon Company’s PolyMetallix™ nZVI and 7,421 gallons of anaerobic water at a concentration of 21 grams per liter into;

– Two injection wells; and

– Two injection intervals per well:

108 to 113 feet below ground surface (bgs), and

113 to 118 feet bgs;

Collection of groundwater samples to monitor the performance of the nearby wells. 1.2 Objectives The objectives of the PT were to: Demonstrate that a pressurized injection method (jet-assisted injection) can increase the nZVI

mass applied at each point and increase the ROI of injected nZVI as compared to the Phase I and II PT results;

Reduce trichloroethylene (TCE) and perchlorate concentrations within the PT area;

Evaluate the persistence of the nZVI in the PT area; and

Asses the technical and economic feasibility of using this injection technique with PolyMetallix for potential future treatment of the source area at the site.

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1.3 Rationale

Historic bench tests and field PTs conducted at PGA-North showed that the permeability and variability of the fine-grained layers of site soil (sandy silts and clays) is inhibitory to gravity-fed nZVI injection. During the Phase I and Phase II PT efforts, the maximum injection mass of PolyMetallix™ nZVI was 50 lbs. The Phase I PT was conducted in January 2006; the Phase II PT was conducted in April through December of 2008. During the Phase II PT, 2,751 gallons of nZVI solution were injected at a concentration of 2.1 g/L, and under gravity-induced pressure head of 26 lbs per square inch (psi). The effects of the nZVI was measured in IRZ-IW-01, the well located 5 feet downgradient of the injection point, indicating an ROI of at least 5 feet with an estimated effective porosity of 0.07 (Arcadis 2006). The Phase II injection resulted in an order of magnitude decrease in permeability based on slug testing completed before and after injection (Arcadis 2008). In order to optimize nZVI distribution and treatment effectiveness for removing TCE and perchlorate from groundwater, the jet-assisted injection method was chosen for this PT.

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2. PILOT TEST IMPLEMENTATION The following is a summary of the PT field schedule: Field preparation was performed during weeks 11 and 18 January 2010;

The blank-cased wells were installed on 11 and 12 January 2010;

Baseline sampling was conducted on 18 January through 20 January 2010;

nZVI injection was completed on 1 through 5 February 2010;

Week 1 post-injection groundwater monitoring was completed 10 and 11 February 2010;

Week 2 post-injection groundwater monitoring was completed 17 through 19 February 2010;

Month 1 post-injection groundwater monitoring was completed 3 and 4 March 2010;

Month 3 post-injection groundwater monitoring was completed 5 and 6 May 2010; and

Month 6 post-injection groundwater monitoring was completed 4 and 5 August 2010. 2.1 Injection Well Installation The locations of the two injection points, IRZ-BW-1 and IRZ-BW-2, are depicted on Figure 2. These locations were chosen based on their proximity to existing downgradient and sidegradient monitoring well locations. The placement of IRZ-BW-1 allowed for radial tracking of the effects of both injections and the migration of nZVI. The configuration of the array of monitoring wells allowed for limited evaluation of preferential flow paths and will be discussed in Section 4.0 Data Evaluation. Well construction was performed in accordance with the Standard Operating Procedures (SOPs) provided in Appendix B of the Work Plan. In summary, the two blank-well injection points, IRZ-BW-1 and IRZ-BW-2, were installed to a total depth of 135.3 and 136.1 feet bgs, respectively. The installation locations are depicted on Figure 2. Following subsurface clearance, each borehole was advanced by Layne Christensen, Inc. using a Becker dual-wall percussion drill rig. Soil classification between ground surface and total depth was based on drilling returns collected from the hopper and soil core samples collected with a split-spoon sampler at approximately 5-foot intervals below the water table. The two injection wells are constructed of Schedule 40 4-inch PVC well casing within a 9-inch borehole. Stainless steel centralizers were placed within the annulus of each well-bore to ensure the placement of an equal thickness of grout to install as straight a well as possible. A cement grout was tremied into the annulus along the total depth of each well to the surface. The bottom of the well casing was capped with a PVC threaded cap. The cement grout mixture consisted of Sikagrout 212. Boring logs and construction diagrams for IRZ-BW-1 and IRZ-BW-2 are provided in Appendix A. 2.2 Baseline Sampling Baseline sampling consisted of groundwater samples collected from each of the PT monitoring wells (Figure 2), using the EPA-approved low-flow sampling method. Groundwater samples were analyzed for the parameters listed in Table 1.

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2.3 Site Preparation

Preparation of the site for nZVI injection included the placement and staging of the following equipment:

Installation of temporary security fencing;

Receipt and setup of anaerobic water holding tanks;

Receipt and setup of secondary containment;

Receipt and placement of nZVI totes;

Placement of roll-off bins for general site waste disposal; and

Receipt and securing of two nitrogen Dewars.

The configuration of site equipment is depicted on Figure 3. Major activities, including the preparation of anaerobic water and the installation of real-time monitoring equipment, are described in the next two subsections. 2.3.1 Anaerobic Water Preparation

Two 6,900-gallon black polyethylene tanks were sparged with nitrogen until the dissolved oxygen concentration was measured below 0.1 milligrams per liter (mg/L). The sparging procedure was performed in accordance with the Work Plan. Multiple air stones were connected in parallel and placed in each tank to achieve adequate gas partitioning efficiency. The nitrogen remaining in the Dewar was used to maintain a positive tank pressure in the 6,900-gallon tanks and within the primary mixing tank that contained the resuspended nZVI particles prior to downhole injection.

2.3.2 Temphion and Pressure Transducer Installation and Programming

A Temphion™ downhole sensor for real-time monitoring of pH, temperature, and ORP, and an open-vent pressure transducer were installed at monitoring locations IRZ-IW-01, IRZ-IW-02, IRZ-IW-04, IRZ-IW-05, IRZ-MW-C, and IRZ-MW-D on Monday, 1 February 2010. The instruments were installed to a depth of 115 feet bgs at each location. The installation of the Temphions™ was completed in accordance with the SOPs provided in Appendix B of the Work Plan. Both sets of instruments were initially programmed to take a measurement every 15 minutes, but this was changed to every 5 minutes after observation of the quick rate of change in ORP at IRZ-IW-2 in response to injection at IRZ-BW-1 on Wednesday, 3 February 2010.

The instruments were checked daily during injection activities to assure continuous operation. Data was downloaded to a computer as necessary, and a complete data download was performed just prior to removal. With the exception of the Temphion and pressure transducer located in monitoring well IRZ-IW-02, the instruments were removed after 10 days of data collection. The physical effects of the injection process at this location are discussed further in Section 3.1 of this report.

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2.4 Injection Procedures Jet-assisted injection has been successfully used in the oil and gas industry to improve yield from deep recovery wells. This method was adapted for remediation purposes and utilizes the kinetic energy of high-pressure water jets to distribute the injectate throughout the soil matrix. This process is similar to the jet grouting methods used by geotechnical engineers to strengthen and stabilize weak soils. This injection method simultaneously creates mixing and second porosity from hydraulic fracturing phenomena. Jet-assisted injection is used at many environmental sites to emplace slurries and dissolved solutions of various types of remediation amendments. Frx, Inc., located in Cincinnati, Ohio, provided the jet-assisted injection equipment and services for the PT. 2.4.1 Injectate Dosage and Composition

The nZVI used for this PT was formulated with sodium hexametaphosphate (SHMP). SHMP was added to PolyMetallix™ and processed through a colloid mill during the Phase II PT (Arcadis 2009) improving the ROI of the gravity-fed injection, and was proven in bench-tests to improve the dispersion of the nZVI particles. For this PT, SHMP was added to the nZVI prior to site transport. The addition of SHMP to the nZVI is expected to increase migration into the soil pore space after emplacement using the jet-injection method, without passivating the nZVI. A total of 7,421 gallons of highly reducing (-500 to -800 mV) nZVI particles were injected into a deep alluvial water-bearing zone within the source area. The PolyMetallixTM nZVI was provided by Polyflon, a Crane Co. company, as 35.2 grams per liter aqueous solution contained in eighteen 275-gallon totes. Each tote of nZVI was batch-mixed with anaerobic water prior to subsurface injection. The injectate contained a total of 1,400 pounds of nZVI. The Phase III PT nZVI dose was derived by calculating the stoichiometric hydrogen demand of major electron acceptors, including target volatile organic compounds (VOCs), sulfate, nitrate, and oxygen within a 25-foot radius of the injection point. The half reactions for the reduction of the compounds were matched with the oxidation half reaction for nZVI to calculate a ratio of electron equivalents. The maximum concentrations of these compounds from the most recent groundwater sampling event (June or December 2008) was used together with these ratios to calculate the mass of nZVI necessary to meet the electron demand exerted by the compounds. Calculation tables showing each step of this analysis were provided in Appendix A of the Draft Work Plan (ERM 2009).

2.4.2 Resuspension of nZVI

The nZVI was expected to settle during site transport. Resuspension was to be performed by recirculating the nZVI between access ports at the bottom and top of the tote with a transfer pump. The nZVI was pumped from the bottom access port back into the top port to create a closed loop and prevent exposure to air. The pressure rating of the tote liner was tested prior to attempting this procedure using the nZVI solution. The test involved recirculation of water within the tote at progressively higher flow rates. The tote was found to withstand flow rates much higher than the 10 gallons per minute specified in the Work Plan. Upon attempting this procedure during the PT, it was found that the nZVI had settled to the bottom of the totes and the energy from recirculation was not enough to promote resuspension; a mixing tool was therefore devised using a length of schedule 40 PVC attached to the transfer pump leading to the primary feed tank for the high pressure pump (Figure 4). Resuspension

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was achieved by manually inserting the tool into the tote through the top port and mixing the particles at the bottom of each tote. The entire contents of the tote, as necessary, were transferred to the primary feed tank during the mixing process as a suspension of nZVI nano-particles in water. Each tote was transferred in its entirety and the volume of anaerobic transferred to the mixing tank was carefully monitored to maintain control of the final particulate concentration in each batch of nZVI injectate. The daily field logs for each batch are provided in Appendix B. The primary feed tank was kept under a nitrogen gas headspace. Nitrogen gas flowed continually into the tank from the Dewar. Continued suspension of the nZVI particles in the primary feed tank was achieved by continuous recirculation of the solution using a sump pump. Suspended nZVI solution was transferred to the primary feed tank on an as needed basis. A flow meter gauge was placed in-line to monitor the pressure and recirculation rate.

2.4.3 Injection Activities

The nZVI injection was conducted using a combination of a jet-injection lance tool and pressurized packer isolation of the target injection zone. The target injection interval was paired with the screen intervals of the existing performance monitoring wells, in order to ensure that the injection activities could be adequately monitored. A schematic of the jet-assisted injection sequence is depicted in Figure 4. The jet-injection lance is comprised of a set of packers straddling an array of 10 high-pressure water nozzles. Separate nitrogen, water jet, and injectate feed lines were passed through the top packer. The packers and jet-injection lance was lowered into the well by a development rig. The lower 5-foot injection interval was completed first, and then the packers were deflated and moved to the upper injection interval at each injection well. The jet-injection lance was comprised of five sets of opposing jets, oriented to balance injection pressure and provide radial coverage. The 10,000-psi jetted water was applied to the lance to carve approximately 1/8-inch diameter holes through the PVC and out through the grout to create 10 jetted conduits into the formation. The jet-assisted injection of anaerobic water was alternated with injection of nZVI using the injectate pump. The injectate pump pressurized the casing between the packers to 100 to 160 psi, forcing the nZVI into the jetted conduit and creating fractures as the injectate pressure exceeded the overburden pressure. These stresses are hypothesized to result in nucleation of hydraulic fractures, increasing the distribution of the nZVI into the surrounding soils. Periodic application of the water jets were used to create high pressure turbulence to further mix the nZVI with soil in the vicinity of the jetted conduit. Pressure gradients created between the fractures and the aquifer matrix caused the injectate to flow into the surrounding soil pores through the fracture-created secondary porosity. After completion of the first injection interval, the packers were pulled up to the next injection interval and the process was repeated. Two intervals, 113 to 118 feet bgs and 108 to 113 feet bgs were completed at each injection well. The wells were finished with a standard flush-mount well casing and both remain in place for potential reuse in future remediation activities.

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2.5 Post-Injection Performance Monitoring Program The Phase I and II PT injections included the use of tracers and pressure transducers. Sodium bromide was used to determine the initial injection radius and groundwater velocity. Residual bromide from the previous injections made this tracer ineffective because it was difficult to distinguish background concentrations of bromide injected during the Phase II PT. The PT employed an alternative to a chemical tracer: the ROI and migration was tracked through real-time monitoring for the geochemical and physical effects of the active nZVI on groundwater. Post-injection groundwater monitoring was performed similar to that conducted after Phase I and II PT injections. The frequency of PT groundwater sample collection was based on the concentration trends of analytes measured during the Phase I and II PTs. The maximum changes in concentration during the Phase I and II PTs were observed within 2 weeks of injection, with gradual increases occurring over the 4- to 6-month performance monitoring period. Additionally, the activity of nZVI injection during the Phase II PT was estimated to last at least 22 weeks; the Phase III monitoring schedule therefore spanned a 6-month period. The analyte list (see Table I) was comprised of the target compounds, potential byproducts from chemical reduction of the target compounds, competing electron acceptors, and other geochemical indicators of the chemical reduction of TCE and perchlorate. 2.5.1 Locations

All of the existing IRZ wells were used as performance monitoring locations. The PT targeted the same depth interval as the existing monitoring well screens (108 to118 feet bgs) to ensure representative downgradient performance monitoring. Monitoring and injection well construction details are provided in Table II.

2.5.2 Frequency

A baseline monitoring round was performed prior to injecting the nZVI. After injection, groundwater samples were collected using the EPA-approved low flow sampling method at 1 week, 2 weeks, 1 month, 3 months, and 6 months after completion of final injection interval. Table III provides a detailed schedule of locations, analytes, and sampling frequency. The frequency of data collection for specific monitoring parameters was modified during execution of the performance monitoring program based on data trends or lack thereof. Field observations during injection and post-injection groundwater monitoring were also used to modify analysis for specific parameters on a location by location basis. These modifications will be discussed further in the data evaluation section of this report.

2.5.3 Analytes

Analytes in the performance monitoring program are listed in Table I. In summary, groundwater samples were analyzed for the following parameters: Target compounds: VOCs, including TCE, carbon tetrachloride, chloroform,

dichloromethane, and perchlorate;

Potential by-products: cis-1,2-dichloroethylene, vinyl chloride, chlorate, chlorite, chloride, hydrogen, methane, ethane, and ethane;

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Geochemical indicators: alkalinity, total organic carbon;

Metals and redox indicators: total and dissolved iron, manganese, sulfate, nitrate, and ammonia;

Ions for tracking injectate: sodium and phosphate; and

Field parameters: turbidity, specific conductivity, dissolved oxygen ([DO]; using an optical density meter), pH, temperature, and ORP.

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3. RESULTS Data collected during the performance monitoring program for groundwater and field events recorded during performance of the injections are provided in this section. Laboratory data packages for the groundwater data are provided in Appendix C. 3.1 Injection Monitoring and Field Observations The injection process was controlled using pressure gauges and flow meters to monitor the injectate volumes and injection rates. During injections, a water level meter was located in nearby monitoring wells to provide immediate data regarding any changes in water level elevation in response to the injections. Injection began into IRZ-BW-2 on Tuesday, 2 February 2010, and was completed the following day. IRZ-BW-1 was begun on Thursday, 4 February, and was completed on Friday. Injections began by lowering the injection tooling and packers into the well to the prescribed depth and sealing the packers to the casing by inflating them with nitrogen. After both packers were inflated, anaerobic water was jetted through the casing using the higher pressure pump to carve holes through the PVC. The lower pressure pump was then used to pump the nZVI solution out into the formation through these holes. After the initial process of puncturing the well-casing, the jet injection pump was used to alleviate pressure build-up by injecting anaerobic water in short 30-second high pressure bursts. This allowed for rapid delivery of the nZVI solution together with mixing with soil outside of the injection well casing at pressures ranging between 150 to 200 psi, and at a rate of approximately 45 minutes per 460-gallon batch. After completion of injection at each interval, the hoses, tooling, and casing were cleared with an additional injection of 250 to 300 gallons of anaerobic water. This process was repeated for each of the four injection intervals. The field injection sheets are provided in Appendix B. After injection of the second batch at IRZ-BW-2, an upwelling of groundwater containing ZVI was observed at IRZ-IW-2, and IRZ-MW-B. It was discovered that the well box for IRZ-IW-2 and IRZ-MW-B were connected with a PVC pipe located approximately 8 inches bgs and groundwater containing nZVI was passing between the well boxes through this conduit. Injection was halted while IRZ-MW-B was fitted with a cap and pressure gauge to prevent the recurrence of this condition during the ongoing injection. Pressure as high as 40 psi was recorded at the well cap during the injection into IRZ-BW-2. The increase and decreases in pressure recorded at IRZ-MW-B corresponded to the operation of the high pressure jet pump. Upwelling of nZVI laden groundwater was also observed within the casing at monitoring well IRZ-IW-4, and nZVI was observed on the water level tape retrieved from that well. Neither of these events resulted in aboveground releases of groundwater, as it was either contained in the well boxes, or did not rise above the top of the casing. 3.2 Temphion and Pressure Transducer Data Data from the downhole devices were uploaded to a portable computer on a daily basis. These data were compiled into data tables in Microsoft Excel and are provided in Appendix D. The data were graphed against the real-time measurements as shown in Figure 5. Evaluation of these data is provided in Section 4.1.

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3.3 Groundwater Performance Monitoring Data Data collected during the baseline and performance monitoring events were tabulated as listed below. The data were used to construct time series plots so that trends over the PT monitoring period can be evaluated (Section 4.0 Data Evaluation), unless there is a paucity of data for that particular analyte. The data are provided in the following tables and figures: Field parameter data, including pH, ORP, DO, specific conductivity, turbidity, and temperature

are provided in Table 4, and Figures 6 and 7;

TCE, perchlorate and associated daughter product data are provided in Table 5, and Figures 8 and 9;

Metals, other reduction-oxidation indicators, and major anion and cation data, including hydrogen are provided in Table 6;

Hydrogen, sulfate, and total iron time series charts are Figures 10, 11, and 12, respectively; and

VOC data collected using passive diffusion bags (PDBs) are shown together with the low-flow sampling results for each common sampling location in Table 7.

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4. DATA EVALUATION This section provides an evaluation of the data collected during the PT groundwater performance monitoring period. 4.1 Field Observations and Real-time Monitoring The field observations made during injection and the real-time changes in pH, ORP, temperature, and pressure show that the injection ROI was at least 29 feet from the point of injection. The data show a definitive response through increased temperature and pH, decreased ORP, and increased pressure at IRZ-IW-2 during injection at IRZ-BW-2. The temperature at IRZ-IW-2 peaked at 25.1 degrees Celsius (°C), up from a baseline of 24°C, during the injection into the upper interval at IRZ-BW-2. The ORP decreased from a baseline of 67.5 mV to -837 mV at IRZ-IW-2. Within the same timeframe, the pH increased from a baseline of 7.1 standard units (SU) to 9 SU at IRZ-IW-2. The pressure transducer recorded a visible response to the injection that increased from batch to batch (Figure 5). During injection of the first batch, the pressure increased from 10.9 psi to 19.6 psi; during the second batch, a maximum pressure of 40.2 psi was recorded at IRZ-IW-2. A less strong, but significant and similar response was evident at IRZ-IW-4 during injection at IRZ-BW-1. IZ-IW-4 is located 29 feet downgradient of IRZ-BW-1. The temperature at IRZ-IW-4 peaked at 24.6°C during injection into the upper interval. The ORP decreased from a baseline of 198 mV to -874 mV at IRZ-IW-4. The pH at IRZ-IW-4 increased from 6.3 SU to 11 SU at the end of the 10-day monitoring period. A response in pressure during injection at IRZ-BW-1 was recorded in all the monitoring wells containing transducers; the strongest response was recorded at IRZ-IW-2, IRZ-IW-5, and IRZ-IW-4. These data verify that nZVI travelled at least 29 feet from the injection performed at BW-1. It is likely that a similar ROI occurred during the injection at BW-2. 4.2 Field Parameter Evaluation The ORP, DO and pH field parameter data clearly show that groundwater in the vicinity of IRZ-IW-02, IRZ-IW-04, and IRZ-MW-B was effected by the nZVI injections. These data are similar to the real-time data, but with less resolution. Monitoring well IRZ-IW-05 shows little change in these parameters, likely due to the lingering presence of iron from the Phase I and II PT injections. The DO concentrations at IRZ-IW-03 show a distinct decrease; however, the ORP at this location did not decrease significantly, possibly indicating that anaerobic water reached this location, independent of nZVI. Unfortunately, this trend could not be followed through Month 6 due to a malfunction in the DO meter during that monitoring event. No data are available past Month 1 at IRZ-IW-02 due to the inaccessibility of the well screen. Prior to the injections, this well was screened from 110 feet bgs to 120 feet bgs. After injection, the bottom of the well was sounded at 109 feet bgs, indicating that this well had filled in, hypothetically with filter pack sand. PolyMetallix was observed in the groundwater samples from this well, providing visual confirmation of the presence of nZVI at this location. Specific conductance, turbidity, and temperature were also monitored during low-flow groundwater sampling at each monitoring well. These parameters were less sensitive to the injection activities, and did not show any significant trends. Groundwater temperature increased significantly over the course of the pilot test commensurate with the onset of summer.

12

4.3 Groundwater Performance Monitoring Results The effectiveness of the nZVI in reducing TCE concentrations, together with an analysis of the effects of the injections on groundwater geochemical parameters, is summarized in Table VIII. A more detailed analysis is provided in the subsections below. 4.3.1 Trichloroethene Mass Reduction

The TCE mass reduction in monitoring wells located within the injection ROI of 29-foot ranges between zero and 96 percent (Table IX); this includes all of the monitoring wells with the exception of IRZ-MW-C and IRZ-MW-D. Table X shows the distances of the monitoring wells from each of the injection locations. Maximum percent mass reduction is observed at IRZ-IW-B, where concentrations decreased from 46 µg/L to non-detect and at IRZ-IW-03, where the TCE decreased from a baseline concentration of 5,100 µg/L to 200 µg/L. Both changes in concentration represent a 96 percent decrease in TCE concentration during the performance monitoring period. TCE concentrations rebounded at several locations after showing significant decreases in the concentration. For example, at IRZ-IW-02, TCE concentrations decreased by 82 percent, from 510 µg/L to 93 µg/L the first week after injection, but then rebounded to 620 µg/L one month after injection. This phenomenon can be explained through the dissolution of sorbed phase mass resulting in the release of TCE back into the treated area and the continual migration of TCE-impacted groundwater into areas previously treated by nZVI. Increases in TCE concentration without a preceding decrease can be attributed to displacement of TCE-impact groundwater from the incoming volume of injectate; however, the injection volume is calculated to be 9 percent of the porewater volume within the ROI of both injection wells, indicating that a minimal volume of groundwater was displaced during the injection process. The ten foot injection interval relative to stratigraphy is shown on north-south and east-west trending cross-sections (Figures 13 and 14, respectively). These figures were constructed from boring logs of the blank-cased injection wells and the existing monitoring wells. Generally, the Subunit A saturated zone beneath the Main Drywells Source Area extends from 85 to approximately 155 feet bgs and is comprised of interbedded layers of sand dominant deposits; comprised of silty sand to clayey sand with >15% fines; and well to poorly sorted sand with <5% fines. These deposits are interbedded with layers and lenses of silt/clay intermixed with sand. Additionally, within the screened intervals of IW-01 and IW-05 localized gravel dominant deposits comprised of silty to clayey gravels with >15 % fines were noted. It is difficult to ascertain whether the presence of higher and lower density soil types affected the ROI, since all of the performance monitoring data was generally collected downgradient of the injection wells and in the vicinity of the Phase I and II PT test injection points. IRZ-IW-05 is located within the injection ROI but showed an increase in TCE concentration from a baseline of 140 µg/L to a maximum concentration of 1,800 µg/L one month after injection. It is understood from the results of the previous nZVI injection at this location that the permeability of the formation decreased significantly. It is therefore reasonable to suspect injectate was diverted around this location, and potentially around IRZ-IW-01 located directly behind IRZ-IW-05, due to the reduction in permeability. At monitoring locations outside of the injection ROI, effects of the jet-injection process are likely observed due to the migration of displaced and/or treated groundwater through these wells.

13

At IRZ-MW-C and IRZ-MW-D, the monitoring wells located furthest from the injection wells, treated groundwater can be seen to be migrating through these wells by the decrease in TCE concentrations, even after an initial increase. At IRZ-MW-C, the TCE concentration increased from the baseline measurement of 220 µg/L to 480 µg/L in the one week groundwater sample. The TCE concentration at this location eventually decreased back to 250 µg/L six months after injection. At IRZ-MW-D, the baseline TCE concentration was 290 µg/L, and increased to 760 µg/L one week after injection. At six months after injection the TCE concentration decreased to below baseline by 31 percent and to a concentration of 200 µg/L.

4.3.2 Perchlorate

The trends in perchlorate concentration are shown on Figure 9; the perchlorate, chlorate and chlorite data are shown in Table V. Perchlorate concentrations decreased slightly in the monitoring wells closest to the injection wells, and in other monitoring wells increased in response to the nZVI injections. At most monitoring locations, perchlorate returned to baseline concentrations between the three- and six-month sampling events. Chlorate concentrations did not change significantly over the PT monitoring period. Chlorite was consistently detected only in groundwater samples from IRZ-IW-01: the concentrations of chlorite decreased slightly after the injection, but returned to baseline concentrations at the six-month monitoring event.

4.3.3 Hydrogen

Hydrogen is released as the nZVI is oxidized and serves as an indicator of the ongoing activity of the nZVI. Groundwater samples were analyzed for molecular hydrogen during performance monitoring, and it was detected consistently in groundwater after injection. Figure 10 shows a rapid increase in hydrogen concentration at most of the performance monitoring wells after the injection, and then a decrease, but not to baseline concentrations. Hydrogen concentrations continued to remain elevated above baseline concentrations six months after completion of the nZVI injections. At IRZ-IW-03, hydrogen continued to increase in concentration commensurate with decreases in TCE concentration. This is likely an indication of the downgradient migration of treated groundwater from the PT treatment area.

4.3.4 Reduction-Oxidation Indicating Parameters

Sulfate concentrations remained relatively stable throughout the performance monitoring period, with the exception of data from MW-B (Figure 11). Sulfate decreased from a baseline concentration of 950 mg/L to 390 mg/L, indicating a decrease of 59 percent. Sulfate is a concern because it is an electron acceptor that can take electrons from the nZVI, rendering it inactive and making it a competitor to the TCE. The fact that only a 59 percent reduction in sulfate was measured indicates that it is less susceptible to reduction than previously thought. This has further implications for calculation of the nZVI dosage for potential future application to the source area. Previous calculations included all sulfate as a competing electron acceptor to the nZVI. This data provides evidence that including all the sulfate in the stoichiometric dosage calculation is an overestimation of the electron demand.

Figure 12 shows a rapid increase in total iron concentration at most of the performance monitoring wells after the injection, and then a decrease, but not to baseline concentrations. Total iron concentrations continued to remain elevated above baseline concentrations at IRZ-

14

IW-01, IRZ-IW-03, IRZ-MW-B, and IRZ-IW-04 six months after completion of the nZVI injections.

4.3.5 Passive Diffusion Bag Results

In general, the TCE concentrations were lower in the groundwater samples collected using passive diffusion bags in comparison to the low flow TCE data (Table VII). Two exceptions to this observation are at the six month sample for IRZ-MW-B; both the upper and lower PDBs were very close in concentration to the low-flow sample result. At IRZ-MW-D, the six month PDB result from the 125 feet bgs sample interval was significantly higher than both the low flow sample and the upper interval PDB sample. At IRZ-MW-C, there appears to be no trend in whether the deeper or shallower PDB yielded higher or lower TCE concentration. At IRZ-MW-D, the lower PDB, located at a depth of 125 feet, was consistently higher in concentration than the PDB hung at the upper interval of 115 feet bgs.

15

5. LESSONS LEARNED Lessons learned during execution of the PT were primarily in regards to the physical design and implementation of the injection procedure. The issues that arose and the subsequent changes in response to those issues are provided in Table XI.

16

6. CONCLUSIONS AND RECOMMENDATIONS This section provides a discussion of conclusions drawn from the evaluation of the PT results in context of the PT objectives set forth in the Work Plan, and additionally provides some recommendations for continued optimization of the application of this remediation technology at PGA North. 6.1 Comparison to Previous Pilot Test Results When compared to previous pilot test efforts, there is no doubt that this pilot test was successful in meeting the objective of delivering the planned large quantity of mass and volume of nZVI into the Dry Wells Area. Several major drawbacks associated with the prior nZVI injection process were overcome during execution of the PT. Through the use of jet-assisted injection, a technology adapted from use in the oil fields, it is evident that the nZVI was distributed to distances as far as 29 feet from each injection well. A maximum of 50 pounds of nZVI was delivered to the subsurface during the Phase I and II PT efforts, while 1,400 pounds were easily delivered to treat source area concentrations of TCE during this PT. The use of high pressure injection methods and robust injection tooling during this pilot test enabled limitations imposed upon the process by the varied lithology and depth of the water table to be overcome. 6.2 Mass Reduction The comparison between the baseline TCE concentrations and post-injection TCE concentrations shows that between 63 percent and 96 percent of the TCE within the ROI of the injection wells was degraded by the nZVI. Although some displacement of dissolved and likely sorbed phase mass likely occurred, the volume of the injectate was only 9 percent of the total volume of groundwater within the 29-foott ROI observed for the PT. Additionally, it is generally acknowledged that the PolyMetallix nZVI is extremely effective in chemically reducing TCE and with the delivery of 1,400 lbs of nZVI the likelihood of displacement being the root cause of the observed decreases in TCE concentration is very small. 6.3 Persistence of the nZVI Although elevated concentrations of hydrogen and iron continued to persist in downgradient monitoring wells six months after the injections, the data show that the iron remained active for at least one month after injection. 6.4 Recommendations The results of this PT lead to the recommendation for further full-scale use of this remediation technology to treat TCE in the Main Dry Wells Area at PGA North. This groundwater remedy has proven to be effective in quickly reducing TCE mass that may have lingered in the source area and continues to contribute to the downgradient dissolved TCE groundwater plume. Areas for improvement and optimization in the implementation of the jet-assisted injection of nZVI include development of a better understanding of the distribution of the nZVI as part of future planned full-scale injection phases and whether the ROI from jet-assisted injection is subject to changes in the lithologic characteristics of the formation. Answering these questions will lead to smarter and more effective application of this technology. Suggestions for furthering the development and optimization of this technology includes developing a program to collect additional data regarding nZVI distribution, refinement of the injection

17

port configuration on the jet lance tooling, and development of a mechanism by which the orientation of the ports may be prescribed prior to implementation. G:\PHX Backup\37639 Crane Co PGA-North\37639_0228_HAI_ PIIInZVI PT Report_D.docx

HALEY& ALDRICH

18

REFERENCES 1. Arcadis. February 2006. Draft Technical Memorandum for the Nano-Scale, Zero-Valent Iron

Field Pilot Test. Phoenix-Goodyear Airport-North Superfund Site.

2. Arcadis. May 2008. Draft Technical Memorandum #4 – Injection Procedure for the Phase II Nano-Scale, Zero-Valent Iron Field Testing Program. Phoenix-Goodyear Airport-North Superfund Site.

3. Arcadis. January 2009. Final Technical Memorandum #5 – Summary of Field Implementation and Results for the Phase II Nano-Scale, Zero-Valent Iron Field Testing Program. Phoenix-Goodyear Airport-North Superfund Site.

4. Army Corps of Engineers. May 2009. Environmental & Munitions Center of Expertise – Review Comments on Draft Work Plan for the Phase III Nano-Scale, Zero-Valent Iron Injection. Phoenix-Goodyear Airport-North Superfund Site.

5. ERM. April 2009. Draft Work Plan for the Phase III Nano-Scale, Zero-Valent Iron Injection Program. Phoenix-Goodyear Airport-North Superfund Site.

6. ERM. July 2009. Nano-Scale, Zero-Valent Iron PT Conceptual Design Approach. Phoenix-Goodyear Airport-North Superfund Site.

7. Hydutsky, Bianca W., Mack, Elizabeth J., Beckerman, Benjamin B., Skluzacek, Joanna M., and Mallouk, Thomas E. 2007. Environmental Science & Technology, Vol. 41, pp 6418-6424. Optimization of Nano- and Microiron Transport through Sand Columns Using Polyelectrolyte Mixtures.

8. Kanel, S.R. and Choi, H. Water Science & Technology, Vol 55 No 1-2, pp 157-162, 2007. Transport Characteristics of Surface-Modified Nanoscale, Zero-Valent Iron in Porous Media.

9. Kanel, S.R., Goswami, R.R., Clement, T.P., Barnett, M.O., and Zhao, D. Environmental Science & Technology. 2008, vol. 42, pp 896-900. Two Dimensional Transport Characteristics of Surface Stabilized Zero-Valent Iron Nanoparticles in Porous Media.

10. Schrick, Bettina, Bianca W. Hydutsky, Jennifer L. Blough, and Thomas E. Mallouk. 2004. Chem. Mater. 2004, 16, 2187-2193. Delivery Vehicles for Zerovalent Metal Nanoparticles in Soil and Groundwater

TABLE IBASELINE AND PERFORMANCE MONITORING ANALYTE LISTPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 1

Parameter Analytical Method Bottles Hold Time Bottle Type Preservative

VOCs 8260B 3 14 days 40 mL vials HCl

Perchlorate 314 1 2 days 500 mL Poly None

HydrogenMicroSeeps AM

15.011 28 days

Bubblestrip Method, Glass vial with

septumNone

Chlorate 300.1 1 28 days 500 mL Poly None

Chlorite 300.1 1 28 days 500 mL Poly None

Sulfate 28 days None

Chloride 28 days None

Nitrate 2 days None

Alkalinity M2320B 1 14 days 500 mL Poly None

Phosphate M4500-P B, E 1 28 days 500 mL Poly H2SO4

Sodium

Total Fe and Mn

Dissolved Fe 200.7 1 180 days 500 mL Poly Field Filtered, HNO3

Total Organic Carbon SM5310B 4 28 days 40 mL amber vial H2SO4

Sample Locations:All wells include: IRZ-IW-01, IRZ-IW-02, IRZ-IW-03, IRZ-IW-04, IRZ-IW-05, IRZ-MW-B, IRZ-MW-C, and IRZ-MW-D

Sample Frequency:Baseline, 1 week, 2 weeks, 1 month, 3 months, and 6 months

Abbreviations:

Fe - iron

Mn - manganese

H2SO4 - sulfuric acid

HNO3 - nitric acid

HCl - hydrochloric acid

mL - milliliter

L - liter

VOCs - volatile organic compounds

Notes:

Low flow sampling method will require collection of field parameters including: turbidity, pH, dissolved oxygen, specific conductivity, temperature, and redox potential

1 500 mL Poly300

200.7 1 180 days 500 mL Poly HNO3

HALEY & ALDRICH, INC.2011_0217_HAI_Tbls I thru III_D.xlsx DRAFT FEBRUARY 2011

TABLE IIEXISTING WELL CONSTRUCTION DATAPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 1

Name Well TypeTotal

Depth (feet bgs)

Borehole Diameter (inches)

Well Diameter (inches)

Screen Slot Size (inches)

Screen TypeScreen Interval

(feet)Drilling Method Filter Pack Method

Filter Interval (feet bgs)

IRZ-BW-1 Injecion 135 9 4 -- polyvinyl chloride None Pneumatic Hammer None NA

RZ-BW-2 Injection 136 9 4 -- polyvinyl chloride None Pneumatic Hammer None NA

IRZ-MW-A Monitoring 132 8 4 0.03 stainless steel wire wrap 110 - 130 Rotary-Sonic Colorado silica 6/9 NA

IRZ-MW-B Monitoring 130 9.5 4 0.03 polyvinyl chloride 110 - 130 Pneumatic Hammer Colorado silica 6/9 NA

IRZ-MW-C Monitoring 132 8 4 0.03 stainless steel wire wrap 110 - 130 Rotary-Sonic Colorado silica 6/9 106.5 - 131

IRZ-MW-D Monitoring 132 8 4 0.03 polyvinyl chloride 111 - 131 Rotary-Sonic Colorado silica 6/9 106 - 131.75

IRZ-IW-1Injection/

Monitoring341 5 4 0.03 stainless steel wire wrap 110 - 120 Rotary-Sonic Colorado silica 6/9 105 - 120.5

IRZ-IW-2 Injection 120 5 4 0.03 stainless steel wire wrap 110 - 120 Rotary-Sonic Colorado silica 6/9 NA

IRZ-IW-3 Monitoring 151 9 4 0.03 stainless steel wire wrap 108 - 118 Rotary-Sonic Colorado silica 10/20 105 - 119

IRZ-IW-4 Monitoring 120 9 4 0.03 stainless steel wire wrap 110 - 120 Rotary-Sonic Colorado silica 10/20 105 - 120

IRZ-IW-5 Injection 125 9 4 0.03 stainless steel wire wrap 109 - 118.5Dual-Wall Percussion

Hammer#4 sand 108 - 121

NOTES:

bgs - below ground surface

NA - not available


TABLE IIInZVI INJECTION DATAPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 1

Injection Location IRZ-BW-1 IRZ-BW-2

Well Type Blank-cased injection Blank-cased injection

Total Depth (feet bgs) 135 136

Borehole Diameter (inches) 9 9

Well Diameter (inches) 4 4

Injection Intervals (feet bgs) 108 - 103 and 113 - 118 108 - 103 and 113 - 118

Injection Method Jet-assisted injection Jet-assisted injection

Dosage 700 pounds of PolyMetallix nZVI 700 pounds of PolyMetallix nZVI

Dispersant Content 5% SHMP 5% SHMP

Water Volume 3,984 gallons 3,984 gallons

Drilling Method Dual-wall percussion hammer Dual-wall percussion hammer

Grout Sikagrout 212 Sikagrout 212

NOTES:

bgs - below ground surface

SHMP - sodium hexmetaphosphate


TABLE IVFIELD PARAMETER DATAPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 3

Location Event Sample Date Day Depth to Water**

Screen Interval pH Specific

Conductance Turbidity Dissolved Oxygen*** Temperature

Oxidation Reduction Potential

(ft bgs) (ft bgs) (SU) (mS/cm) (NTU) (mg/L) (°C) (mV)

IRZ-IW-05 Baseline 1/18/10 -15 91.49 109 - 118.5 8.26 3851 7.601 0 25.25 -336

IRZ-IW-05 1 week 2/10/10 6 90.88 109-117.48 8.53 3289 0 0 19.16 -367

IRZ-IW-05 2 week 2/18/10 14 90.66 109-117.48 8.31 3758 19.77 0 24.96 -330

IRZ-IW-05 1 month 3/3/10 28 90.35 109-117.59 8.03 4483 30.12 0 25.12 -339

IRZ-IW-05 3 month 5/5/10 92 88.88 109-117.15 8.07 4566 174.1 0.29 25.13 -255

IRZ-IW-05 6 month 8/4/10 214 89.74 109-117.15 8.32 3369 <999 #N/A 30.1 -184

IRZ-IW-04 Baseline 1/18/10 -15 91.29 110 - 120 7.63 3963 198.1 1.35 22.27 166

IRZ-IW-04 1 week 2/11/10 7 90.98 110 - ? 8.76 6278 5 0.01 24.31 -431

IRZ-IW-04 2 week 2/19/10 15 90.78 110 - 117.55 8.72 3865 1.4 -.04* 23.11 -632

IRZ-IW-04 1 month 3/3/10 28 90.44 110 - 117.54 8.07 4197 59.14 0.98 25.12 -238

IRZ-IW-04 3 month 5/5/10 92 88.99 110-118.91 8.05 4298 224.4 -0.02 28.62 -325

IRZ-IW-04 6 month 8/4/10 214 89.80 110-118.91 8.00 3249 >999 #N/A 29.86 -179

IRZ-IW-03 Baseline 1/19/10 -15 91.67 108 - 118 7.06 4234 731 4.97 23.91 153

IRZ-IW-03 1 week 2/11/10 7 91.24 108 - 118 6.95 4361 2926 2.06 24.9 67

IRZ-IW-03 2 week 2/19/10 15 91.04 108 - 118 7.16 4232 1219 1.86 26.32 50

IRZ-IW-03 1 month 3/3/10 28 90.80 108 - 118 6.76 4553 457 2.02 26.65 49

IRZ-IW-03 3 month 5/5/10 92 89.24 108-118.34 6.97 4290 1323 2.70 29.15 172

IRZ-IW-03 6 month 8/4/10 214 90.10 108-118.34 7.14 3100 >999 #N/A 32.3 15

IRZ-IW-02 Baseline 1/20/10 -15 91.92 110 - 120 7.21 3685 1514 0.49 21.16 105

IRZ-IW-02 1 week 2/11/10 7 68.45 -1 8.66 4464 167 0.01 24.91 -391

IRZ-IW-02 2 week 2/19/10 15 75.36 -1 8.38 1155 176.4 0.05 25.13 -293

IRZ-IW-02 1 month 3/4/10 29 90.46 -1 8.92 5630 177.5 0.01 25.84 -554

HALEY & ALDRICH, INC.2011_0217_HAI_Tbl IV_Figs 6&7 PT Field Parameters_D.xlsx DRAFT FEBRUARY 2011


Page 2 of 3






IRZ-IW-01 Baseline 1/18/10 -15 91.63 110 - 120 7.70 4233 1.828 0.58 25.22 58

IRZ-IW-01 1 week 2/11/10 7 91.13 110 - 120 7.61 4242 6.295 0.45 24.79 79

IRZ-IW-01 2 week 2/19/10 15 90.93 110 - 120 7.63 4200 15.13 0.46 26.33 -33

IRZ-IW-01 1 month 3/4/10 29 90.62 110 - 120 7.59 4328 24.01 0.75 26.17 -4

IRZ-IW-01 3 month 5/5/10 92 89.15 110 - 119.50 7.52 4486 19.49 0.72 28.71 99

IRZ-IW-01 6 month 8/5/10 215 90.00 110 - 119.50 7.22 4523 10.1 0.6 30.38 73

IRZ-MW-B Baseline 1/19/10 -15 91.36 110 - 130 7.11 3662 91.36 7.64 21.5 158

IRZ-MW-B 1 week 2/10/10 6 90.63 110 - 112.15 8.58 3318 1.556 0 22.25 -478

IRZ-MW-B 2 week 2/19/10 15 90.98 110 - 112.15 8.80 4009 35.14 0.01 24.11 -420

IRZ-MW-B 1 month 3/3/10 28 90.67 110 - 112 8.83 5858 35.15 0 25.87 -469

IRZ-MW-B 3 month 5/5/10 92 89.02 110 - 112.00 8.81 5917 112.4 -0.01 27.64 -413

IRZ-MW-B 6 month 8/5/10 215 90.05 110 - 111.91 8.48 5581 >1200 #N/A 26.34 -54

IRZ-MW-C Baseline 1/19/10 -15 90.55 110 - 130 7.09 3892 1197 6.45 25.36 183

IRZ-MW-C 1 week 2/10/10 6 90.71 110 - 130 7.04 3794 369.9 7.13 22.31 65

IRZ-MW-C 2 week 2/17/10 13 90.54 110 - 130 7.16 3987 303.5 6.98* 24.94 64

IRZ-MW-C 1 month 3/4/10 29 90.23 110 - 130 6.98 3776 130.1 7.44 21.2 36

IRZ-MW-C 3 month 5/5/10 92 88.75 110 - 126.15 7.08 4843 104.9 5.46 34.45 69

IRZ-MW-C 6 month 8/5/10 215 89.60 110 - 126.15 7.18 4450 432 4.9 32.35 47

IRZ-MW-D Baseline 1/19/10 -15 90.88 111 - 131 7.27 3928 32.77 6.31 24.06 148

IRZ-MW-D 1 week 2/11/10 7 90.90 111 - 131 7.15 3901 85.46 6.08 23.58 173

IRZ-MW-D 2 week 2/17/10 13 90.73 111 - 131 7.20 4018 15.58 6.39* 25.24 138

IRZ-MW-D 1 month 3/4/10 29 90.44 111 - 131 7.13 3589 31 7.13 19.4 35

IRZ-MW-D 3 month 5/5/10 92 88.92 111 - 128.74 7.15 4202 37.82 5.78 27.91 71

IRZ-MW-D 6 month 8/5/10 215 89.60 111 - 128.74 7.04 4203 98.6 5.5 31 74



Page 3 of 3






Average Baseline 1/19/10 -15 7.42 3931 471.72 3.47 23.59 79.38

Average 1 week 2/11/10 7 7.91 4206 445.15 1.97 23.28 -160.38

Average 2 week 2/17/10 13 7.92 3653 223.24 1.96 25.02 -182.00

Average 1 month 3/3/10 28 7.79 4552 118.00 2.29 24.42 -185.50

Average 3 month 5/5/10 92 7.66 4657 285.16 2.13 28.80 -83.14

Average 6 month 8/5/10 215 7.63 4068 180.23 3.67 30.33 -29.66

NOTES:S/cm - microSiemen per centimeter

mg/L - milligram per liter

mV - millivolt

SU - standard unit

°C - degrees Celsius

PDB - passive diffusion bag

NTU - Nephelometric turbidity units

#N/A - Parameter not measured, no data available for this date.

* Data considered anomalous and was not used to compute average.

**Depth to water measured before start of purging.

***DO Probe was not operating properly on first day (4 August 2010) of sampling event.


TABLE VVOLATILE ORGANIC COMPOUND AND PERCHLORATE DATAPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 2

Location Event Sample Date Day Screen Interval PCE TCE cis-1,2-DCE Vinyl

Chloride Perchlorate Chlorate Chlorite Other Detected VOCs

(ft bgs) ( g/L) g/L) g/L) g/L) g/L) g/L) g/L) g/L)IRZ-IW-05 Baseline 1/18/10 -15 109 - 118.5 < 0.5 140 1.6 < 0.5 < 2 < 100 < 100

IRZ-IW-05 1 week 2/10/10 6 109 - 118.5 < 5 250 6.3 < 5 < 4 22 < 100

IRZ-IW-05 2 week 2/18/10 14 109 - 117.48 < 5 480 3.8 < 0.5 < 4 < 200 < 200 carbon disulfide = 0.8, 1,1-dichloroethene = 1.2

IRZ-IW-05 1 month 3/3/10 28 109 - 117.59 0.68 1800 3.2 < 0.5 7.8 < 40 < 200 benzene = 0.51, carbon disulfide = 0.71, chloroform = 0.82, 1,1-dichloroethene = 1.6

IRZ-IW-05 3 months 5/5/10 92 109-117.15 < 5 1400 < 5 < 5 12 #N/A #N/A

IRZ-IW-05 6 months 8/4/10 214 109-117.15 < 5 150 3.3 < 5 < 4 < 400 < 40 carbon disulfide = 1.5

IRZ-IW-04 Baseline 1/18/10 -15 110 - 120 0.98 2,300 < 0.5 < 0.5 14 93 < 200 chloroform = 0.80

IRZ-IW-04 1 week 2/11/10 7 110 - ? < 5 270 7.5 < 5 16 < 100 < 400

IRZ-IW-04 2 week 2/19/10 15 110 - 117.55 < 2.5 280 7.7 < 2.5 16 < 40 < 200 1,1-dichloroethene = 4.1

IRZ-IW-04 1 month 3/3/10 28 110 - 117.54 < 0.5 750 2.3 < 0.5 14 < 40 < 200 1,1-dichloroethene = 1.1

IRZ-IW-04 3 months 5/5/10 92 110-118.91 < 5 1100 < 5 < 5 12 #N/A #N/A

IRZ-IW-04 6 months 8/4/10 214 110-118.91 < 5 580 < 5 < 5 6.1 < 400 < 40 carbon disulfide = 1.5

IRZ-IW-03 Baseline 1/19/10 -15 108 - 118 2.3 5,100 < 0.5 < 0.5 20 100 < 200 carbon disulfide = 0.77 ug/L, chloroform 1.6 ug/L

IRZ-IW-03 1 week 2/11/10 7 108 - 118 < 50 3,600 < 50 < 50 23 84 < 40 duplicate TCE = 3,800 ug/L, duplicate perchlorate = 18 ug/L

IRZ-IW-03 2 week 2/19/10 15 108 - 118 2.3 5,800 < 0.5 < 0.5 23 93 < 200 benzene = 0.72, chloroform = 1.7, 1,1,dichloroethene = 3.7,

IRZ-IW-03 1 month 3/4/10 29 108 - 118 < 10 2,700 < 10 < 10 20 89 < 200

IRZ-IW-03 3 months 5/5/10 92 108-118.34 < 2.5 1200 < 2.5 < 2.5 5.9 #N/A #N/A

IRZ-IW-03 6 months 8/4/10 214 108-118.34 < 0.5 200 < 0.5 < 0.5 < 2 < 40 < 40

IRZ-IW-02 Baseline 1/20/10 -15 110 - 120 < 0.5 510 2.0 < 0.5 3.6 < 40 < 200 1,1-dichloroethene = 1.2, MTBE = 67

IRZ-IW-02 1 week 2/11/10 7 -1 < 0.5 93 2.3 < 0.5 < 4 < 100 < 400 acetone = 57, benzene = 0.72, bromodichloromethane = 0.90, 2-butanone (MEK) = 9.4, 1,1-dichloroethene = 0.67, methylene chloride = 1.8, and toluene = 1.8

IRZ-IW-02 2 week 2/19/10 15 -1 < 0.5 190 3.2 < 0.5 6.2 < 100 < 400 duplicate trichloroethene = 190, acetone = 32/30, benzene = 0.81/0.66, 2-butanone (MEK) = 4.4/4.0, chlorobenzene = 0.98/0.96, 1,1-dichloroethene = 0.93/0.75, and toluene = 1.0/0.87, duplicate perchlorate = 5.8

IRZ-IW-02 1 month 3/4/10 29 -1 < 2.5 630 < 2.5 < 2.5 9.7 #N/A #N/A

IRZ-IW-01 Baseline 1/18/10 -15 110 - 120 3.0 6,300 1.4 < 0.5 27 68 1,300benzene = 0.91, chloroform = 2.1, and 1,1-dichloroethene = 10

IRZ-IW-01 1 week 2/11/10 7 110 - 120 1.9 6,700 1.6 < 0.5 27 < 100 930benzene = 0.82, chloroform = 2.0, and 1,1-dichloroethene = 8.4

HALEY & ALDRICH, INC.2011_0217_HAI_Phase III PT VOCs Metals and Ions.xlsx DRAFT

FEBRUARY 2011

TABLE VVOLATILE ORGANIC COMPOUND AND PERCHLORATE DATAPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 2 of 2


Chloride Perchlorate Chlorate Chlorite Other Detected VOCs

(ft bgs) ( g/L) g/L) g/L) g/L) g/L) g/L) g/L) g/L)

IRZ-IW-01 2 week 2/19/10 15 110 - 120 2.4 6,700 1.4 < 0.5 27 74 830benzene = 0.85, chloroform = 1.9, and 1,1-dichloroethene = 8.8

IRZ-IW-01 1 month 3/4/10 29 110 - 120 < 50 4,500 < 50 < 50 23 77 900

IRZ-IW-01 3 months 5/5/10 92 110 - 119.50 < 25 6,700 < 25 < 25 27 #N/A #N/A

IRZ-IW-01 6 months 8/5/10 215 110 - 119.50 < 25 7,800 < 25 < 25 25 130 1,000

IRZ-MW-B Baseline 1/19/10 -15 110 - 130 < 0.5 46 < 0.5 < 0.5 4.4 85 < 200

IRZ-MW-B 1 week 2/10/10 6 110 - 112.15 < 5 < 5 < 5 < 5 < 2 < 100 < 100

IRZ-MW-B 2 week 2/19/10 15 110 - 112.15 < 0.5 1.7 < 0.5 < 0.5 < 4 < 100 < 400 acetone = 46, 2-butanone = 7.4 (MEK), toluene = 1.3

IRZ-MW-B 1 month 3/3/10 28 110 - 112 < 0.5 1.7 < 0.5 < 0.5 < 6 180 < 400 acetone = 30, 2-butanone (MEK) = 9.9, toluene = 1.7

IRZ-MW-B 3 months 5/5/10 92 110 - 112.00 < 0.5 560 1.7 < 0.5 < 10 #N/A #N/A

IRZ-MW-B 6 months 8/5/10 215 110 - 111.91 < 0.5 1100 6.4 < 0.5 4.5 69 <1,000 acetone = 34, benzene = 1.6, carbon disulfide = 0.56, chloroform = 0.63, 1,2-dichloroethane = 0.50, 1,3-dichloropropane = 0.65, 2-hexanone = 3.4, 4-methyl-2-pentanone (MIBK), Methyl-tert-butyl ether (MTBE) = 0.68, toluene = 2, 1,2,3-trichloropropane = 1.1

IRZ-MW-C Baseline 1/19/10 -15 110 - 130 < 0.5 220 < 0.5 < 0.5 5.0 89 < 200

IRZ-MW-C 1 week 2/10/10 6 110 - 130 < 0.5 480 < 0.5 < 0.5 10 86 < 100

IRZ-MW-C 2 week 2/17/10 13 110 - 130 < 0.5 360 < 0.5 < 0.5 9.3 87 < 200

IRZ-MW-C 1 month 3/4/10 29 110 - 130 < 2.5 370 < 2.5 < 2.5 7.9 85 < 200 duplicate TCE = 470

IRZ-MW-C 3 months 5/5/10 92 110 - 126.15 < 2.5 370 < 2.5 < 2.5 8.7 #N/A #N/A duplicate TCE = 330

IRZ-MW-C 6 months 8/5/10 215 110 - 126.15 < 0.5 250 < 0.5 < 0.5 5.4 92 < 40

IRZ-MW-D Baseline 1/19/10 -15 111 - 131 < 0.5 290 < 0.5 < 0.5 6.0 90 < 200 1,1-dichloroethene = 0.82

IRZ-MW-D 1 week 2/11/10 7 111 - 131 < 0.5 760 < 0.5 < 0.5 12 89 < 100 1,1-dichloroethene = 0.96, toluene = 0.54

IRZ-MW-D 2 week 2/17/10 13 111 - 131 < 0.5 310 < 0.5 < 0.5 31 87 < 200

IRZ-MW-D 1 month 3/4/10 29 111 - 131 < 2.5 210 < 2.5 < 2.5 6.3 85 < 200

IRZ-MW-D 3 months 5/5/10 92 111 - 128.74 < 5.0 230 < 5.0 < 5.0 8.6 #N/A #N/A

IRZ-MW-D 6 months 8/5/10 215 111 - 128.74 < 0.5 200 < 0.5 < 0.5 4.7 80 < 40 duplicate TCE = 220

NOTES:

g/L - micrograms per liter

mg/L - milligram per liter#N/A - Parameter not measured, no data available for this date.


FEBRUARY 2011

TABLE VIMETALS AND MAJOR ION DATAPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 2

Location Event Sample Date Day Screen Interval Hydrogen Total Iron Dissolved

IronTotal

ManganeseTotal

SodiumTotal

Phosphorus Phosphate Sulfate Nitrate as N Bicarbonate Alkalinity Chloride TOC

as CaCO3

(ft bgs) (nM) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L)

Tank Pre-Injection 1/20/10 -13 #N/A #N/A < 0.05 #N/A < 0.05 220 #N/A #N/A 770 16 140 660 #N/A

IRZ-IW-05 Baseline 1/18/10 -15 109 - 118.5 11 1,300 6.6 5.3 320 140 430 800 3.3 160 750 1.4

IRZ-IW-05 1 week 2/10/10 6 109 - 118.5 5,000 6,900 4,200 32 460 #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-05 2 week 2/18/10 14 109 - 117.48 1,700 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-05 1 month 3/3/10 28 109 - 117.59 840 500 3.3 3.3 420 52 160 1000 12 190 800 1.4

IRZ-IW-05 3 months 5/5/10 92 109-117.15 5,600 1,600 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-05 6 months 8/4/10 214 109-117.15 930 170 2 #N/A 380 #N/A #N/A 1000 #N/A #N/A 770 #N/A

IRZ-IW-04 Baseline 1/18/10 -15 110 - 120 25 14 < 0.05 0.16 410 < 0.1 < 0.3 1,100 21 220 770 < 1.0

IRZ-IW-04 1 week 2/11/10 7 110 - ? 320,000 6,200 2,100 25 1,300 #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-04 2 week 2/19/10 15 110 - 117.55 130,000 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-04 1 month 3/3/10 28 110 - 117.54 36 100 1.6 0.67 460 5.1 16 1,100 7.7 220 810 1.2

IRZ-IW-04 3 months 5/5/10 92 110-118.91 640 1000 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-04 6 months 8/4/10 214 110-118.91 59 720 9.2 #N/A 390 #N/A #N/A 970 #N/A #N/A 750 #N/A

IRZ-IW-03 Baseline 1/19/10 -15 108 - 118 9.8 68 1.8 0.49 470 1 3.1 1,100 20 210 820 1.3

IRZ-IW-03 1 week 2/11/10 7 108 - 118 4,200 910 100 9.5 470 #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-03 2 week 2/19/10 15 108 - 118 300 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-03 1 month 3/3/10 28 108 - 118 23 91,000 2.4 11 380 6.5 20 1,100 19 220 790 4.9

IRZ-IW-03 3 months 5/5/10 92 108-118.34 5,300 49 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-03 6 months 8/4/10 214 108-118.34 8,800 210 < 0.05 #N/A 470 #N/A #N/A 810 #N/A #N/A 700 #N/A

IRZ-IW-02 Baseline 1/20/10 -15 110 - 120 13 1.40 < 0.05 0.09 430 < 0.1 < 0.3 980 9.8 200 730 < 1.0

IRZ-IW-02 1 week 2/11/10 7 -1 #N/A 79 #N/A 0.22 1900 #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-01 Baseline 1/18/10 -15 110 - 120 16 0.11 < 0.05 0.019 420 < 0.1 < 0.3 1,100 15 91 800 1.0

IRZ-IW-01 1 week 2/11/10 7 110 - 120 66 0.15 < 0.05 0.018 450 #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-01 2 week 2/19/10 15 110 - 120 41 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-01 1 month 3/4/10 29 110 - 120 42 14 < 0.05 0.046 430 < 0.1 < 0.3 1,100 16 110 810 < 1.0

IRZ-IW-01 3 months 5/5/10 92 110 - 119.50 34 0.58 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-IW-01 6 months 8/5/10 215 110 - 119.50 100 0.62 < 0.05 #N/A 430 #N/A #N/A 1,100 #N/A #N/A 800 #N/A

HALEY & ALDRICH, INC.2011_0217_HAI_Phase III PT VOCs Metals and Ions.xlsx DRAFT FEBRUARY 2011

TABLE VIMETALS AND MAJOR ION DATAPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 2 of 2

Location Event Sample Date Day Screen Interval Hydrogen Total Iron Dissolved

IronTotal

ManganeseTotal

SodiumTotal

Phosphorus Phosphate Sulfate Nitrate as N Bicarbonate Alkalinity Chloride TOC

as CaCO3

(ft bgs) (nM) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L) (mg/L)

IRZ-MW-B Baseline 1/19/10 -15 110 - 130 5.2 < 0.05 < 0.05 < 0.01 510 < 0.1 < 0.3 950 20 180 740 < 1.0

IRZ-MW-B 1 week 2/10/10 6 110 - 112.15 38,000 4,000 150 9.7 390 #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-MW-B 1 month 3/3/10 28 110 - 112 #N/A 26 < 0.05 0.075 1700 1.9 5.8 500 < 0.2 < 6* 1,700 10

IRZ-MW-B 3 months 5/5/10 92 110 - 112.00 #N/A 3.3 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-MW-B 6 months 8/5/10 215 110 - 111.91 #N/A 490 < 0.05 #N/A 1300 #N/A #N/A 390 #N/A #N/A 1,400 #N/A

IRZ-MW-C Baseline 1/19/10 -15 110 - 130 11 130 < 0.05 0.31 490 0.61 1.9 980 21 180 750 1.1

IRZ-MW-C 1 week 2/10/10 6 110 - 130 30 30 < 0.05 0.058 460 #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-MW-C 2 week 2/17/10 13 110 - 130 31 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-MW-C 1 month 3/4/10 29 110 - 130 5,900 11 0.45 0.021 450 < 0.3 < 0.3 940 20 180 730 < 1.0

IRZ-MW-C 3 months 5/5/10 92 110 - 126.15 640 35 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-MW-C 6 months 8/5/10 215 110 - 126.15 170 57 0.15 #N/A 430 #N/A #N/A 930 #N/A #N/A 730 #N/A

IRZ-MW-D Baseline 1/19/10 -15 111 - 131 19 1.90 < 0.05 0.014 490 < 0.1 < 0.3 990 20 180 750 1.0

IRZ-MW-D 1 week 2/11/10 7 111 - 131 29 2.80 < 0.05 0.031 480 #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-MW-D 2 week 2/17/10 13 111 - 131 33 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-MW-D 1 month 3/4/10 29 111 - 131 32 2.30 < 0.05 0.026 470 < 0.1 < 0.3 940 20 180 730 < 1.0

IRZ-MW-D 3 months 5/5/10 92 111 - 128.74 22 0.50 #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A #N/A

IRZ-MW-D 6 months 8/5/10 215 111 - 128.74 130 2.10 < 0.05 #N/A 470 #N/A #N/A 930 #N/A #N/A 730 #N/A

NOTES:


mg/L - milligram per liter

ft bgs = feet below groundwater surface

*Alkalinity as CaCO3 was measured at 1,500 mg/L, Carbonate Alkalinity = 1,000, Hydroxide Alkalinity = 450 mg/L, and Alkalinity via Phenolphthalein = 960 mg/L

TOC = total organic carbon

#N/A = no data available


TABLE VIIPASSIVE DIFFUSION BAG VOLATILE ORGANIC COMPOUND DATAPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 1


Chloride Other Detected VOCs

(ft bgs) ( g/L) g/L) g/L) g/L) g/L)IRZ-MW-C Baseline 1/19/10 -15 110 - 130 < 0.5 220 < 0.5 < 0.5

IRZ-MW-C 1 week 2/10/10 6 110 - 130 < 0.5 480 < 0.5 < 0.5

IRZ-MW-C 2 week 2/17/10 13 110 - 130 < 0.5 360 < 0.5 < 0.5

IRZ-MW-C 1 month 3/4/10 29 110 - 130 < 2.5 370 < 2.5 < 2.5 duplicate TCE = 470

IRZ-MW-C-115 1 month 3/3/10 28 110 - 130 < 0.5 99 < 0.5 < 0.5 acetone = 22, benzene = 73

IRZ-MW-C-125 1 month 3/3/10 28 110 - 130 < 0.5 140 < 0.5 < 0.5 acetone = 17, benzene = 41, bromoform = 1.0

IRZ-MW-C 3 months 5/5/10 92 110 - 126.15 < 2.5 370 < 2.5 < 2.5 duplicate TCE = 330

IRZ-MW-C-115 3 months 5/5/10 92 110 - 126.15 < 0.5 110 < 0.5 < 0.5 benzene = 28

IRZ-MW-C-125 3 months 5/5/10 92 110 - 126.15 < 0.5 97 < 0.5 < 0.5 benzene = 29

IRZ-MW-C 6 months 8/5/10 215 110 - 126.15 < 0.5 250 < 0.5 < 0.5

IRZ-MW-C-115 6 months 8/5/10 215 110 - 126.15 < 0.5 230 < 0.5 < 0.5 acetone = 10, benzene = 7

IRZ-MW-C-125 6 months 8/5/10 215 110 - 126.15 < 0.5 250 < 0.5 < 0.5 acetone = 12, benzene = 4.7

IRZ-MW-D Baseline 1/19/10 -15 111 - 131 < 0.5 290 < 0.5 < 0.5 1,1-dichloroethene = 0.82

IRZ-MW-D 1 week 2/11/10 7 111 - 131 < 0.5 760 < 0.5 < 0.5 1,1-dichloroethene = 0.96, toluene = 0.54

IRZ-MW-D 2 week 2/17/10 13 111 - 131 < 0.5 310 < 0.5 < 0.5

IRZ-MW-D 1 month 3/4/10 29 111 - 131 < 2.5 210 < 2.5 < 2.5

IRZ-MW-D-115 1 month 3/3/10 28 111 - 131 < 0.5 53 < 0.5 < 0.5 acetone = 17, benzene = 4.4

IRZ-MW-D-125 1 month 3/3/10 28 111 - 131 < 0.5 68 < 0.5 < 0.5 acetone = 18, benzene = 3.7

IRZ-MW-D 3 months 5/5/10 92 111 - 128.74 < 5.0 230 < 5.0 < 5.0

IRZ-MW-D-115 3 months 5/5/10 92 111 - 128.74 < 0.5 69 < 0.5 < 0.5 benzene = 3.6

IRZ-MW-D-125 3 months 5/5/10 92 111 - 128.74 < 0.5 78 < 0.5 < 0.5 benzene = 3.8, 2-butanone = 2.9

IRZ-MW-D 6 months 8/5/10 215 111 - 128.74 < 0.5 200 < 0.5 < 0.5 duplicate TCE = 220

IRZ-MW-D-115 6 months 8/5/10 215 111 - 128.74 < 0.5 130 < 0.5 < 0.5 acetone = 14, benzene = 5.2, 1,2-dichloroethane = 0.53, 1,3-dichloropropane = 0.67, Methyl-tert-butyl ether (MTBE) = 0.93, 1,1,2,2-tetrachloroethane = 0.74, 1,1,2-trichloroethane = 0.66, 1,2,3,-trichloropropane = 1.3

IRZ-MW-D-125 6 months 8/5/10 215 111 - 128.74 < 0.5 260 < 0.5 < 0.5 acetone = 11, benzene = 0.81

NOTES:



Depth of passive diffusion bag indicated in location identification - for example, the "-115" in IRZ-MW-C-115 indicates that the passive diffusion bag was stationed at 115 feet below the top of the well casing.


TABLE VIIIPARAMETER RESPONSE SUMMARYPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 1

Well Distance from OrientationNo. Injection Point, ft 6 7 13 14 15 28 29 92 214 215 ORP Pressure Temperature pH Hydrogen Sulfate Iron

IW‐2 12.5' from BW‐02 Downgradient 82 63 ‐24

MW‐B 19' from BW‐02 Downgradient 89 96 96 ‐1117 ‐2291C

‐‐‐ ‐‐‐

IW‐4 29' from BW‐01 Downgradient 88 88 67 52 75 ‐‐‐

22' from BW‐01; 18'

Change in TCE Concentration after x Days, % Parameter Response

Could not be sampled for these parameters

HALEY & ALDRICH, INC.2011_0217_HAI_Tbl VIII_Parameter Response Summary_D.xlsx DRAFT FEBRUARY 2011

IW‐522 from BW‐01; 18

from BW‐02Cross‐gradient ‐79 ‐243 ‐1186 ‐900 ‐7 ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐

IW‐128' from BW‐01; 24'

from BW‐02Cross‐gradient ‐12 ‐12 ‐25 ‐12 ‐12 ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐

MW‐C32' from BW‐01; 25'

from BW‐02Cross‐gradient ‐118 ‐64 ‐68 ‐68 ‐14 ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐

IW‐332' from BW‐01; 29'

from BW‐02Cross‐gradient 29 ‐14 47 77 96 ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐

MW‐D45' from BW‐01; 36'

from BW‐02Cross‐gradient ‐162 ‐7 28 21 31 ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐

Notes: 1. Injected 7,400 gallons of nZVI solution in two wells (IRZ‐BW‐01 and BW‐02) on or around the 2nd of February.2. Estimated time for advective front to move from upgradient stagnation point past most downgradient monitoring well ‐ roughly 30 to 40 days.3. Bold black font indicates observed decrease in TCE concentration from baseline; red font in italics indicates increase in TCE concentration.4. Green arrows indicate post‐injection response; yellow indicates delayed response; ‐‐‐ indicates no response or no data available.

HALEY & ALDRICH, INC.2011_0217_HAI_Tbl VIII_Parameter Response Summary_D.xlsx DRAFT FEBRUARY 2011

TABLE IXMASS REDUCTION SUMMARYPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 1

Location Event Day TCE

g/L)

IRZ-MW-D Baseline -15 290

IRZ-MW-D 1 week 7 760

IRZ-MW-D 2 week 13 310

IRZ-MW-D 1 month 29 210

IRZ-MW-D 3 months 92 230

IRZ-MW-D 6 months 215 200

IRZ-MW-C Baseline -15 220

IRZ-MW-C 1 week 6 480

IRZ-MW-C 2 week 13 360

IRZ-MW-C 1 month 29 370

IRZ-MW-C 3 months 92 370

IRZ-MW-C 6 months 215 250

IRZ-IW-03 Baseline -15 5,100

IRZ-IW-03 1 week 7 3,600

IRZ-IW-03 2 week 15 5,800

IRZ-IW-03 1 month 29 2,700

IRZ-IW-03 3 months 92 1200



IRZ-IW-01 1 week 7 6,700

IRZ-IW-01 2 week 15 6,700

IRZ-IW-01 1 month 29 4,500

IRZ-IW-01 3 months 92 6,700

IRZ-IW-01 6 months 214 6,700

IRZ-IW-05 Baseline -15 140

IRZ-IW-05 1 week 6 250

IRZ-IW-05 2 week 14 480

IRZ-IW-05 1 month 28 1800





IRZ-IW-04 2 week 15 280




IRZ-MW-B Baseline -15 46

IRZ-MW-B 1 week 6 < 5

IRZ-MW-B 2 week 15 1.7

IRZ-MW-B 1 month 28 1.7

IRZ-MW-B 3 months 92 560

IRZ-MW-B 6 months 214 1100

IRZ-IW-02 Baseline -15 510


IRZ-IW-02 2 week 15 190


NOTES:




FEBRUARY 2011

TABLE XDISTANCES FROM INJECTION WELLS TO MONITORING WELLSPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 1

Existing Wells IRZ-BW-1 IRZ-BW-2IRZ-IW-1 27'-7" 24'-0"IRZ-IW-2 26'-6" 12'-6"IRZ-IW-3 31'-9" 28'-6"IRZ-IW-4 29'-1" 19'-4"IRZ-IW-5 21'-9" 18'-2"

IRZ-MW-B 32'-9" 19'-1"IRZ-MW-C 36'-5" 25'-0"IRZ-MW-D 45'-3" 35'-8"

NW Fence Corner South 15'-1" 3'-0"NW Fence Corner West 20'-8" 29'5"

NOTE:

Distance between Phase III injection wells is 15'-0"

Injection Wells

HALEY & ALDRICH, INC.2011_0217_HAI_Table IX_D.xlsx DRAFT FEBRUARY 2011

TABLE XILESSONS LEARNEDPHOENIX-GOODYEAR AIRPORT-NORTH SUPERFUND SITEGOODYEAR, ARIZONA

Page 1 of 1

ISSUE RESPONSE

Monitoring wells were rendered unusable during injection procedure. Install monitoring wells after performing the injection to preserve utility of the monitoringwells. Baseline data can be collected during installation of injection wells if necessary.

Ratio of anaerobic water injection using high‐pressure pump to nZVI injection pump was unknown prior to performance of the pilot test.

Jet‐assisted injection was required for 30 seconds after 5 minute of pumping with thelower pressure nZVI pump.

Resuspension of the nZVI particles after shipping was not possible using the recirculation technique specified in the Work Plan.

A mixing tool is required to resuspend the nZVI particles within the totes prior to injection.

Longevity of the anaerobic status of the nitrate‐purged water. Once prepared, anaerobic water was fairly stable for at least four weeks.

Influence of sulfate on calculating nZVI dosage.At one monitoring location, sulfate concentrations decreased by 59%. The chemical interaction between the nZVI and sulfate is less than expected; therefore the nZVI dosage can be lowered during future injections.

HALEY & ALDRICH, INC.Table XI.xlsx DRAFT FEBRUARY 2011

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U.S.G.S. 7.5 MinutB Series Quadrangle, (Tolleson, Arizona) Map Veralon: 1982 CUnent aa of: 1978

0 1000

SCALE IN FEET

2000

HALEY& ALDRICH

PHASE Ill OF THE nZV1 FIELD TEST PROGRAM PHOENIX·IlOODYEAR AIRPORT NORTH SUPERFUND SITE GOODYEAR. ARIZONA

SITE LOCATION MAP

SCALE: AS SHOWN FEBRUARY 2011 FIGURE 1

IRZMW-D-$-

IRZMW-C-$-

• .IRZ-1W~

IRZ-IW-04 * IRZ-IW-()1

* • * IRZ-IW-«1

IRZ-IW-05

IRZ-aW-2-$- •

• Groundwater Flow Direction •

Soil Vapor Extraction Well

+ Proposed Injection location

Installed Injection Well s

Installed IRZ Monitoring Well 0 10 20

Drywelllocation SCALE IN FEET

SVESystem Compound

HALEY& ALDRIOI

PHASE Ill OF THE nZVI FIELD TEST PROGRAM PHOENIX-GOODYEAR AIRPORT NORTH SUPERFUND SITE GOODYEAR, ARIZONA

INJECTION AND MONITORING WELL LOCATION MAP


G:\37839-CRANE_CO\GLOBAL\CAD\3783&-000-0000-PROCESS-FLOW-DIAGRAM.DWG

RECIRCULATION

• • • • • • •

2X ANAEROBIC WAlERTANK

4,500 GALLONS

LEGEND

•

~ FLOWMETER

NITROGEN DEWAR

9 PRESSURE GUAGE

®VALVE

SECONDARY CONTAINMENT

~HI' FRP TRASH PUMP

SO PSI

WATER INJECTION

1"HOSE 12,5001'51

nZVI INJECTION

1.5"HOSE 1,500 PSI

POLYLINE 1000 PSI

NITROGEN CYUNDER 2,500 PSI

BASIC MD-2.5

PACKERS 900PSI

HALEY& ALDRICH


PILOT TEST FIELD EQUIPMENT SCHEMATIC

SCALE: NO SCALE FEBRUARY 2011 FIGURE 3

G:\3

7639

-CR

AN

E_C

O\G

LOB

AL\

CA

D\3

7639

-000

-000

0-E

RM

-SC

HE

MA

TIC

.DW

G

FIGURE 4

PHASE III OF THE nZVI FIELD TEST PROGRAMPHOENIX-GOODYEAR AIRPORT NORTH SUPERFUND SITEGOODYEAR, ARIZONA

JET-ASSISTED INJECTIONSEQUENCE

SCALE: NOT TO SCALEFEBRUARY 2011

FIGURE SOURCE: ERM, FIGURE 2 SEQUENTIALJET-ASSISTED INJECTION SCHEMATIC, 08/200 9

I·

a) Install blank-cased well to depth of ten feet post targeted injection interval

b) Lower dual packer assembly with jet injection tool to seal off injection interval. Jet injection tool located between packers.

v , o.ooo psi· "' ~f _, 2oo-3oo psi water hose--~IW.I III--++---nZVI injectate

hose ....___....,.._~-IPqss thru

c) Packers straddle injection interval and 10,000 psi water stream penetrates well casing and formation

lc: Opposing pairs injecting into and --i+-lel out of the page

- Opposing pairs of water jets injecting along the plane of the page

·.

d) Pressure in the formation must be allowed to relax before packers can be deflated and moved to next 5- foot interval

0 · u ··- __ ·_._· __ _,o£__ ____ _

'----

1--4-inch schedule 40 PVC casing

-- 9- inch borehole

Tremmied grout cernent-bosed

- containing shrinkage compensa_tion agent

End Cop

-

nZVI Distributed in Pore Space

Top View

------

~Jot-o-.. conduit

Subfroctures

0.! ~

2.2. ~~===-

0 =---·----=--=

~ ---

-

""-- 1/8 to 1/4-inch holes remain In PVC

.____

e) Blank-cased well will remain in place with traditional well completion for reuse in future injection activities or additional injection intervals

·'-

--~ 0

0

--

LEGEND

\7 Water Table

- Water

c::J PolyMetollix nZVI

HALEY& ALDRICH

DRAFT

FIGURE 5 - TEMPHIONTM AND HYDRAULIC PRESSURE CHARTS

22.5

23.0

23.5

24.0

24.5

25.0

25.5

Deg

rees

Cel

sius

Temperature

IW-1 IW-2 IW-4 IW-5 MW-C MW-D

-1000

-800

-600

-400

-200

0

200

400

Mill

ivol

ts


10

12pH

BW-1 Injection PeriodBW-2 Injection Period

0

2

4

6

8

10

Sta

ndar

d U

nits

10

15

20

25

30

35

40

45

2/1

0:0

0

2/1

12

:00

2/2

0:0

0

2/2

12

:00

2/3

0:0

0

2/3

12

:00

2/4

0:0

0

2/4

12

:00

2/5

0:0

0

2/5

12

:00

2/6

0:0

0

2/6

12

:00

2/7

0:0

0

2/7

12

:00

2/8

0:0

0

2/8

12

:00

2/9

0:0

0

2/9

12

:00

2/1

0 0

:00

2/1

0 1

2:0

0P

ound

s P

er S

quar

e In

ch

Date

Pressure Head

DRAFTFIGURE 6 - pH, DISSOLVED OXYGEN AND OXIDATION REDUCTION TIME SERIES CHARTS

-700

-500

-300

-100

100

300

OR

P (

mill

iVo

lts)

IRZ-IW-05 IRZ-IW-04 IRZ-IW-03 IRZ-IW-02

IRZ-IW-01 IRZ-MW-B IRZ-MW-C IRZ-MW-D

1

2

3

4

5

6

7

8

isso

lved

Oxy

gen

(m

g/L

) DO probe not operational on 4 August 2010.

0

1Di

6.5

7.0

7.5

8.0

8.5

9.0-20

0 20 40 60 80 100

120

140

160

180

200

220

pH

(S

tan

dar

d U

nit

s)

Days

DRAFTFIGURE 7 - TEMPERATURE, SPECIFIC CONDUCTIVITY, AND TURBIDITY TIME SERIES CHARTS

0

1,000

2,000

3,000

4,000

5,000

6,000

7,000

Sp

ecif

ic C

on

du

ctan

ce (

uS

/cm

)

IRZ-IW-05 IRZ-IW-04 IRZ-IW-03 IRZ-IW-02

IRZ-IW-01 IRZ-MW-B IRZ-MW-C IRZ-MW-D

1,000

1,500

2,000

2,500

3,000

3,500

Tu

rbid

ity

(NT

U)

0

500

19

21

23

25

27

29

31

33

35

-20

0 20

40

60

80

10

0

12

0

14

0

16

0

18

0

20

0

22

0T

emp

erat

ure

(d

egre

es C

)

Days

--~/\~ f

L " ....... "

~ ---- · - -- - \

r~]~ -- -------------· -

--......::::· \ I v

__ .. ,

DRAFTFIGURE 8 - TRICHLOROETHYLENE TIME SERIES CHART

100

1,000

10,000

TC

E C

once

ntra

tion

(ug/

L)

IRZ-IW-05 IRZ-IW-04 IRZ-IW-03 IRZ-IW-02 IRZ-IW-01 IRZ-MW-B IRZ-MW-C IRZ-MW-D

1

10

-20

0 20 40 60 80 100

120

140

160

180

200

220

Days

DRAFTFIGURE 9 - PERCHLORATE TIME SERIES CHART

12

16

20

24

28

32

Con

cent

ratio

n (u

g/L)


0

4

8

-20

0 20 40 60 80 100

120

140

160

180

200

220

Days

DRAFTFIGURE 10 - HYDROGEN TIME SERIES CHART

100

1,000

10,000

100,000

1,000,000

ar H

ydro

gen

Con

cent

ratio

n (n

M)


1

10

100

-20

0 20 40 60 80 100

120

140

160

180

200

220M

olec

ula

Days

DRAFTFIGURE 11 - SULFATE TIME SERIES CHART

100

1,000

10,000

Con

cent

ratio

n (m

g/L)


1

10

-20

0 20 40 60 80 100

120

140

160

180

200

220

Days

DRAFTFIGURE 12 - TOTAL IRON TIME SERIES CHART

1 0

10.0

100.0

1,000.0

10,000.0

Con

cent

ratio

n (m

g/L)


0.0

0.1

1.0

-20

0 20 40 60 80 100

120

140

160

180

200

220

Days

-...J CJ)

~ <( 1-u. -z 0 i= :; w ...J w

s

1000

975

950

.... :·~.; ~ ·.,;·:··:::>:<;:·:~·\i·:::.~-~~~:~~~::~-->~·~::~~;·.~,\~.:. ·: \·~-:·::<~Y:~ .. .-.: t:_:: .:_.:~· .:~~. 925 . ~· .,. ~ .... : • .:. ••• :·:: .,:: ! ... ~· ::

900

875

LEGEND

MW-A - WELL DESIGNATION

--- SEALEDINTERVAL

--- SCREENED INTERVAL

D D ~ ~

SILT/CLAY

SILTY SAND I CLAYEY SAND WITH GRAVEL

SAND WITH GRAVEL

GRAVEL WITH SAND

HORIZ. 0

VERT. 0

15

25 APPROXIMATE SCALE IN FEET

30

50

N

1000

975

950

925

900

875

HALEY& ALDRICH

SITE MAP

N


NORTH-SOUTH CROSS-SECTION


SITE MAP

N

w

IRZ-BW-2

SVE System

• Compound

• IRZ-.A N .IIIE.(I8

A s -...J 0 20 40 en

~ SCALE IN FEET <C

1-LL. -z 0

~ w ...J w

LEGEND

MW-B - WELL DESIGNATION

--SEALED INTERVAL

--SCREENED INTERVAL

D SILT/CLAY

D SILTY SAND I CLAYEY SAND WITH GRAVEL

QJ SAND WITH GRAVEL

~ GRAVEL WITH SAND

w E

1000 c¥' 1000 ov

$'9J ~~ ~ ~

975 975

950 950

925 925

900 900

875 875

850 850

825~------------------------~825

HORIZ. 0

VERT. 0

HALEY& AIDRICI-1

15 30

25 ~ APPROXIMATE SCALE IN FEET


EAST-WEST CROSS-SECTION


APPENDIX A

Injection Well Boring Logs

MW

2 TO

40

FT B

V -

- 19

/4/1

0 15

:29

- F:\E

RM

FIL

ES

\AZ\

PR

OJE

CTS

FY

10\0

1039

65 -

PG

A N

OR

TH\P

HA

SE

III P

ILO

T TE

ST\

PG

A-N

OR

TH.G

PJ

Blo

wC

ount

s

GW

SP

SM

ML

CL-ML

SM

Fiel

dS

cree

ning

(ppm

)

J-plug

Sika Grout 212

ML

7272 East Indian School Road, Suite 100Scottsdale, AZ 85251Phone: (480) 998-2401Fax: (480) 998-2106

LOG OF SOIL BORING: IRZ-BW-1

SP

Sam

ple

Inte

rval

US

CS

Cod

e

Gra

phic

Log

1 of 2

WELL DIAGRAM

Date Started: 1/11/2010Date Completed: 1/12/2010Total Depth: 135.3 feetBorehole Diameter: 8.75"Initial Water Level: Not encountered

Project Number: 103965Project Name: PGA-NorthClient Name: Crane Co.Location: Goodyear, AZContractor: Layne Drilling Co.Drilling Method: Becker RigLogged By: J. Hilker

ERM

Notes: ADWR #: 55-911572. Logged from cuttings unlessnoted.

Dep

th (f

t)

5

10

15

20

25

30

35

40

45

50

55

60

65

SANDY SILT. ~15% Sand. ~85% Silt. Sand is fine to very finegrained. Dry. Reddish Brown. Trace fine gravel.

SILT. ~10% Sand. ~90% Silt. Sand is fine to very fine grained.Brown. Damp.

POORLY GRADED SAND WITH GRAVEL. ~35% Gravel. ~60%Sand. Gravel is fine to coarse grained, subrounded. Sand isfine to medium grained. Trace fines. Damp.

WELL GRADED GRAVEL WITH SAND. ~20% Sand. ~75%Gravel. Sand is medium to fine grained. Gravel is coarse tofine grained, subangular to subrounded. ~5% Cobbles (3"+).Trace fines. Damp.

POORLY GRADED SAND. ~5% Gravel. ~10% Silt. ~85% Sand.Gravel is fine grained, subrounded. Sand is fine to mediumgrained. Brown to reddish brown. Damp.

SILTY SAND WITH LITTLE GRAVEL. ~5% Gravel. ~25% Silt.~70% Sand. Sand is fine to medium grained. Gravel is finegrained, subangular. Brown to light brown. Damp.

SILTY CLAY. ~10% Sand. ~10% Carbonate nodules. ~20% Silt.~60% Clay. Sand is fine to very fine grained. Reddish brown.Clay has low plasticity. Damp.

SILTY SAND. ~40% Silt. ~60% Sand. Sand is fine to mediumgrained. Brown to Dark Brown. Damp.

@20' - 15% carbonate nodules, white, well cemented.

@15' - Trace cemented carbonate nodules

Soil Description and Observations

Blank 4" SCH-40PVC

1850

MW

2 TO

40

FT B

V -

- 19

/4/1

0 15

:29

- F:\E

RM

FIL

ES

\AZ\

PR

OJE

CTS

FY

10\0

1039

65 -

PG

A N

OR

TH\P

HA

SE

III P

ILO

T TE

ST\

PG

A-N

OR

TH.G

PJ

Slough

ML

SM

SW

SP

SWML

ML

SP

SW

GP

SP

GP

SP

3050

Threaded End Cap

50

273234

50

505050

456

8912


ERM

2 of 2



Dep

th (f

t)

Fiel

dS

cree

ning

(ppm

)WELL DIAGRAM

Blo

wC

ount

s



Sam

ple

Inte

rval

Gra

phic

Log

75

80

85

90

95

100

105

110

115

120

125

130

135

US

CS

Cod

e

SILT WITH SAND. ~10% Carbonate lenses. ~15% Sand. ~70%Silt. Sand is fine to very fine grained. Carbonate lenses up to1/2" thick. Reddish brown to brown. Medium stiff. Damp.

POORLY GRADED SAND WITH FINES. ~10% Silt. ~10% Clay.~20% Carbonate lenses. ~60% Sand. Sand is fine to very finegrained. Carbonate lenses are 1/2" to 1/4" thick. Reddishbrown to brown. Medium dense. Damp.

POORLY GRADED GRAVEL WITH SAND AND CLAY. ~10%Clay. ~20% Sand. ~70% Gravel. Sand is fine to mediumgrained. Gravel is coarse to fine grianed, subrounded. Clay isbrown to reddish brown. Trace cobbels (3"+). Damp.

WELL GRADED SAND WITH GRAVEL. ~5% Fines. ~15%Gravel. ~80% Sand. Gravel is fine grained, subrounded. Sandis fine to coarse grained. Very dense. Wet.

SILT WITH SAND. ~75% Silt. ~15% Sand. Sand is fine tomedium grained. Reddish brown to grey mottling. ~10%Carbonate nodules. Moderate cementation. Wet.

POORLY GRADED SAND WITH CLAY. ~20% Clay. ~75% Sand.Sand is fine to medium grained. Low plasticity. Trace gravel.Brown to reddish brown. Moist.

WELL GRADED SAND WITH FINES. ~15% Fines. ~80% Sand.Sand is fine to coarse grained. Brown to reddish brown. Weakcementation. Dense. Wet.

WELL GRADED SAND WITH GRAVEL. ~10% Fines. ~20%Gravel. ~70% Sand. Gravel is fine to coarse grained. Sand isfine to coarse grained. Reddish brown. Damp.

POORLY GRADED GRAVEL WITH SAND AND CLAY. ~10% Silt.~20% Sand. ~70% Gravel. Sand is fine to medium grained.Gravel is coarse to fine grained, subrounded. Silt is brown toreddish brown. Trace cobbles (3"+). Damp.

POORLY GRRADED SAND WITH GRAVEL. ~35% Gravel. ~60%Sand. Gravel is fine grained, subrounded. Sand is coarse tomedium grained. Trace fines. Damp.

WELL GRADED SAND WITH GRAVEL. ~10% Sand. ~30%Gravel. ~60% Sand. Gravel is fine grained, subangular. Sandis fine to coarse grained. Dense. Wet.

SILT WITH SAND AND CARBONATE LENSES. ~20% Sand.~30% Carbonate lesnes. ~50% Silt. Sand is fine to very finegrained. Carbonate lenbses are up to 1/4" thick. Brown to lightbrown. Very stiff. Damp.

SILTY SAND WITH TRACE GRAVEL. ~5% Gravel. ~45% Silt.~50% Sand. Sand is fine to medium grained. Brown toreddish brown. Very dense. Wet.


Total Depth - 135.3 feet bgs

Fiel

dS

cree

ning

(ppm

)

Blo

wC

ount

s

SW

SP

SP

SM

ML

MW

2 TO

40

FT B

V -

- 19

/4/1

0 13

:02

- F:\E

RM

FIL

ES

\AZ\

PR

OJE

CTS

FY

10\0

1039

65 -

PG

A N

OR

TH\P

HA

SE

III P

ILO

T TE

ST\

PG

A-N

OR

TH.G

PJ

Sika Grout 212

J-plugML

US

CS

Cod

e

WELL DIAGRAM

LOG OF SOIL BORING: IRZ-BW-27272 East Indian School Road, Suite 100Scottsdale, AZ 85251Phone: (480) 998-2401Fax: (480) 998-2106

Sam

ple

Inte

rval

Gra

phic

Log


5

10

15

20

25

30

35

40

45

50

55

60

65


1 of 2

ERM


Dep

th (f

t)

@15' - ~20% Gravel. Gravel is fine, subangular to subrounded.Damp.

@55' - Gravel is fine to coarse.

POORLY GRADED SAND WITH GRAVEL. ~35% Gravel. ~60%Sand. Gravel is fine grained, subrounded. Sand is fine tomedium grained. Trace fines. Damp.

SILTY SAND. ~20% Silt. ~80% Sand. Sand is fine to mediumgrained. Reddish brown. Damp.

SILT WITH LITTLE CLAY. ~5% Sand. ~10% Clay. ~85% Silt.Sand is fine to very fine grained. Dark reddish brown. Moist.

@35' - Damp.

@30' - Weak to moderately cemented. Light grey to light brown.Dry.

@25' - Trace clay. Weak cementation. Light brown. Dry

SANDY SILT. ~15% Sand. ~85% Silt. Sand is fine to very finegrained. Trace carbonate nodules. Reddish brown. Dry.

@10' - light brown to tan. Weak to moderate cementation.

POORLY GRADED SAND WITH GRAVEL. ~10% Fines. ~35%Gravel. ~60% Sand. Gravel is fine to coarse grained,subrounded. Sand is medium to coarse grained. Reddishbrown. Damp.

@20 - ~15% carbonate nodules, white, weak to moderatelycemented.


WELL GRADED SAND WITH GRAVEL. ~5% Fines. ~20%Gravel. ~70% Sand. Gravel is fine to coarse grained. Sand isfine to coarse grained. Reddish brown. Damp.

Threaded End Cap

7912

MW

2 TO

40

FT B

V -

- 19

/4/1

0 13

:02

- F:\E

RM

FIL

ES

\AZ\

PR

OJE

CTS

FY

10\0

1039

65 -

PG

A N

OR

TH\P

HA

SE

III P

ILO

T TE

ST\

PG

A-N

OR

TH.G

PJ

SM

SP

GP

GWSW

ML

Blank 4" SCH-40PVC

SP-SM

GP

GW

SW

GW

SM

50

Slough

50

111925

152125

1150

81316

1450

6711

ERM

2 of 2


Date Started: 1/12/2010Date Completed: 1/13/2010Total Depth: 136.1 feetBorehole Diameter: 8.75"Initial Water Level: Not encounteredNotes: ADWR #: 55-911574. Logged from cuttings unlessnoted.

Fiel

dS

cree

ning

(ppm

)WELL DIAGRAM

Blo

wC

ount

s


Dep

th (f

t)


Sam

ple

Inte

rval

Gra

phic

Log

75

80

85

90

95

100

105

110

115

120

125

130

135

US

CS

Cod

e

WELL GRADED SAND WITH GRAVEL. ~5% Fines. ~25% Sand.~70% Sand. Gravel is fine to coarse, subrounded. Sand isfine to coarse grained. Reddish brown. Very dense. Wet.

SILTY SAND WITH LITTLE CLAY. ~10% Clay. ~30% Silt. ~60%Sand. Sand is fine to medium. Reddish brown. Mediumdense. Wet

@110' - Hard. Dry.

WELL GRADED GRAVEL WITH LITTLE SAND. ~5% Fines.~15% Sand. ~80% Gravel. Gravel is fine to coarse grained,subrounded. Sand is fine to medium grained. Moist.

WELL GRADED GRAVEL WITH SAND. ~5% Fines. ~20% Sand.~75% Gravel. Sand is medium to coarse. Gravel is fine tocoarse, subrounded. Reddish brown. Dense. Wet.

SILT WITH SAND AND CLAY. ~10% Clay. ~15% Sand. ~75%Silt. Sand is fine to very fine grained. Reddish brown. Verystiff. Moist.

POORLY GRADED GRAVEL WITH SAND. ~10% Fines. ~20%Sand. ~70% Gravel. Sand is fine to coarse grained. Gravel iscoarse grained, subrounded. Very dense. Wet.

POORLY GRADED SAND WITH FINES. ~5% Gravel. ~15%Fines. ~80% Sand. Sand is fine to medium grained. Reddishbrown. Very dense. Wet.

SILTY SAND. ~35% Silt. ~65% Sand. Sand is fine to mediumgrained. Weak cementation. Reddish brown. Wet.

POORLY SORTED SAND WITH SOME SILT. ~15% Silt. ~85%Sand. Sand is fine to coarse grained. Reddish brown. Wet.

POORLY GRADED GRAVEL WITH SAND AND FINES. ~20%Fines. ~25% Sand. 55% Gravel. Sand is fine to coarsegrained. Gravel is fine grained, subrounded. Brown. Moist.

@108 - 10% Carbonate lenses up to 1/4" thick. Very stiff. Damp.

WELL GRADED SAND WITH GRAVEL. ~5% Fines. ~30%Gravel. ~70% Sand. Sand is fine to coarse grained. Gravel isfine to coarse grianed, subangular. Reddish brown. Moist.

WELL GRADED GRAVEL WITH SAND. ~35% Sand. ~60%Gravel. Gravel is fine to coarse grained, subrounded. Sand isfine to medium grained. Trace fines. Damp.


Total Depth - 136.1 feet bgs

APPENDIX B

Daily Field Logs

' /4)

k

nZVITote Batch nZVI .. miXIng Number Tote.ID time (min)

v-.(<. tAl ( I 1 -

Ott) Jol il

f G'w•-

s-Se{ 10 ....,t..J

,j 'f'wPcf'-

Q, •• ~-'1

?_ \J-~ uv-\v-

t{.cl-~ tiS' 'b-olo

3 t. J £.\. I

.11

Injection Well: IRZ-BW- ;}..

Packer Depth Interval: /I 3 ft to / I ?2 ft

Data Collection Field Personnel: 72_{,.1-c· , , / H J:~~.~~------------

Date: (),- ~-I 0

Weather I Ambient Temperature: PC G Q 's ll> 7 0 15.

Note: 5 batches lower 11ft & 4 batches upper lift (460 gallons/batch)

Anaerobic Anaerobic Water Water Anaerobic Batch Totalizer Totalizer En<! Water Injection Injection Injection Injection Volume Start Reading Reading (Target is Start Finish Flow rate Pressure Injected (gallons) (gallons) 185 gallons) Time Time (gpm) (psi) i (gallons)

Z.::l. i..1) :~ U,V; a) '65 IOH{ 1.1-+Lr "> ',Y,o 7~·> ;?-~ ;:p<;1-1:3Z I 5'

d. ''2'Jv' '78 )~d /

·1JicGr. z. ' IZ.: '-tJ '~cS ~-o ?.3f. {} /{5~/hvo 13:Lfl1 p~ 4S'S""

.1- H 1-::z.o'l -?0

J;J3'i(p '2-'Lc.Oq 1.\.91,¥- - ---Je..<- 1.\I.PO

1.3 r.o q '2._ -~3V/ !<65' iS"'!.> 'L r &J-d- r"'"= l\oi.J'Zb t.j (o 0

qq$

zz~ao<t 'd--£). /'¥, i rlf)f - - - - ·-

[,_ 'Lj {1-l--,.-y v

I 85' n:-z.c.. 18/'J.- '-~ (t.'tw ~ Z-2.~ -zr . .;l 4/oO - u~JY ~7.:2 1--? ).)-'lLJ) - - - -

.. ···

PGA-North Injection Field Form Crane Company

Goodyear, Arizona

ERM Project Number 0103965

Notes/Comments (ex: number, duration, & pressure of pulses)

/~,._, ~ I;Jl L -r-2 )"'f'"

.30-'&11<1-:;~ ~p/.,r· ~1",.· l .,..._,..) ?)C.-0v..-'l ?'.JI..'>-1' /#MJ.V/k.._ 't_ p ~ pa-.Lp V\... S--{

~ _l

1 "'~ f.' r<"''-"- ;-... ~v,,:&; 1- Sho.l- ,\'.,., I'D .leu .

e_-."(J ~"' s-,/ ·:~~~K-~J-\-..1"\ 'P-- .

e.I.VJ- >(Y\. \,. 3a 51? c. ~*- ~""\;.__

Page __ of __

'J

Injection Well: IRZ-BW- ;)__

Packer Depth Interval: II "3 ft to 118 ft

Data Collection Field Personnel: ·:Jl.lr [L ~ ~~~~------------------

Date: L_-]-- £.QI\J Weather I Ambient Temperature: ~C. L) o'<, ·~'0 ~oo)'

Note: 5 batches lowerlift & 4 batches upper lift (460 gallons/batch)

Anaerobic Anaerobic Water Water Anaerobic Batch

nZVITote Totalizer Totalizer End Water Injection Injection Injection Injection Volume Batch nZVI .. Start Reading Reading (Target is Start Finish Flow rate Pressure Injected nuxxng Number ToteiD time (min) (gallons) (gallons) 185 gallons) Time Time (gpm) (psi) (gallons)

<;?- i "' i1 Ji'% 8!-/0 9'13 0 >13_!_-m

~ 5"1'?

·~~ i

~~ L\ 'ref-.~ 8:zo · )\.joio'-V-\:?.&0 fO.~{.,.

.,_~

-z.:z.:J" + 1/\\< . \$ ....,_.._ -z.:> r+B .Jw.,'>,y l··i rLD.L

q;oo ?-li. I{ e "' / 9'J41 tO::J-f!, '-/I,D( '17 nu;,o-o "c(IP<:J to l14::loo I ,_44'0'>\

./~

5" I.V '1 "' ! 10 \8) 9::.6_

v-1..'-\ I '-l '-( :j+ ;...,..)a 1-<-- 1..-:,nB ?.33?---;C

:(( 'J.Lj~ ").L\. vZ,) (Od-') [0 '-I'{ 1')0(1 1.1 i 70/tOC

t "" tS'O I')$ v _; /-,

~ ;;233J.J.. J3)'t'\ ·;;,1 9-T


Goodyear, Arizona


Notes/Comments (ex: numberr dur_ation, & pressure of pulses)

3c Se~ \'<- ,\<-, ~ ~ r•·L~

.\-\-< . ..._ "-'-") s,.-.,__\....- Jo i£:'<:_

f5< ""'- :DI'-'~- {Vow -IL>

h.M i'-< !..t- ·to ·~.-l.[b p ';.; ~ 0

ctW:.J.- -i'l.:t.J..,.,_ \h..+ ...

StA IYii v-l G..b~u<..

FLi.J5 l.f' ~ IJfl..:r.....z b7:L

.4--' ~ F-<>·- (..,.J tfQ_U(._

Page ___ of ___

nZVI Tote Batch nZVI ' ' InlXIng

Number Tote!D time (min)

10 :;-s-3o"-Cf il O'J

'h ...

k t</>J 'fO

~< ~r {/~{:))'

I . V

'r-4~ 1)::$0

·.·. s w:'

,e - (-,'\(... II'! : 'l.o

q 4 oC- C\ l'f.3~

:f'-cv

'v- ~)s..' I--. .., ~

-<!.. ~\.?

Injection Well: IRZ-BW- }-

Packer Depth Interval: tog ft to i I 5 ft

Data Collection Field Personnel_,>J-1-'i~"-· ,1,_..]2""--. ult£.._ _______ _

Date: ;;) - 3 -.)o l 0

Weather I Ambient Temperature: ?G 'to's ·r;;, & o-i Note: 5 batches lower lift & 4 batches upper lift (460 gallons/batch)

Anaerobic Anaerobic Water Water Anaerobic Batch Totalizer Totalizer End Water Injection Injection Injection Injection Volume Start Reading Reading (Target is Start Finish Flow rate Pressure Injected (gallons) (gallons) 185 gallons) Time Time (gpm) (psi) (gallons)

~~!:5) ~

18-~ IJ:i.S- j!:')( IZ s•f ·~ "f&TJ 'J.Y?Ja-o ~ fV1J..- tC

J 3 "'"' l "2'> s-:7-J -z_z..L{ - - - - -\\'·)8 n:n- /i.¥ ~ 2_'(22D

( .ZSUI>£ \ \'b.? LffuO Ill• <I- ~ 0 / ..

I.

Z.:>S')--..1 '1...-'3 ~~ lo /IJ - -- - -·z...>\'<'o J~

t:~L 5'{ 1Lf;Sl? ~~ I1.5DOG ~ .· .· ,zy jJ.$'~ L/S'q <Ell•

'L )i.C 'l, \o 1.,38'1l.f J-oR .- - - - -ll{ J4L[ IS :1o ;O.ZJ"I \~

'25\.'trl 1125'5?.\o\ ·0 (,

4 lt' ( & f(h ~ ' ~~ 'i>" <t,'-\COO jOI:

Q'..))l,fl{ ~~\. ' t ~ - - -

/)..'-\ ooo L-L\_ \~ \S$' _:::::::,_ ""' 1' /

I~

PGA-North Injection Field Form · Crane Company

Goodyear, Arizona


Notes/Comments (ex: numberr dura~gn .. &pressure of pulses)

3D l.k- ~ \·l--'~ rv-1\'J ;I fyv,:''' <il leV \,., <t\~V;l ~

¢;y- .:> "'•'i = ,., """- .. -l' c) l k

L...xt, ~ 'f-j__

$'0.(\"< -s c. !..K_ h ~ 1-eJ'--

~=t-

u~¥-- ~<.J.

50rvv ~ d.~

wo:~ fJ.

1...)0~ C\.J¥-' ¥\ -eui-IY\. 1 ~

OUI"f' {J-'1-A

Page~of~

\ -J.J

nZVITote Batch nZVI .. m1x1ng Number Tote ID time (min)

>~\--U'l. :1

oklr- ~ ~')

\U"\'-~ f\'2j!

~<t ~"'

2 I

[\'';£>') xv-' .t

Injection Well: IRZ-BW- :L Packer Depth Interval: \ \'3 ft to \I f ft

Data Collection Field Personnel: ~ ~~--------------~--~--

Date: -z--:1-10 ~ Weather/ Ambient Temperature: S'--'"''7 1 4Y:':...(.,s_:"'

Note: 5 batches lower lift & 4 batches upper lift (460 gallons/batch)


'£...>55:> II~. / r":l , \~0 "I( l .... 11..:7;, "b"J

2.'-1\ >5'

Z.%:>.5- Z5 ~s.""S' \KP

.

Z<::<o£5-

~ -t;: ~A~ s" '

PGA-North Injection Field Fonn Crane Company

Goodyear, Arizona


N otes(Comments (ex: numberr duration, & pressure of pulses)

L.) ~ il'o"'- ,'-'·ha \ ~ vee -\e- .:y:·J-., .C.,Jt..

\.~ -)rvt~>u«>\+c:, ~huYdav•

4

()'1~uJ- +o

-Jl-(11\h '-'-plY'- I· ~ 13' p..V"' ()) "'1' j..;

PageL-- of 2.. ------

Batch nZVI Number Tote ID

~

l l "'"'-

C]J-'1

\,.)IJ-\P)

c,J-cr 0~

ltoV\ \..)lAo\;

\-\v

Injection Well: IRZ-BW- :l.

Packer Depth Interval: _ _,I.:_I::::_J __ f:.:.t..::to:._-'-1 _:_:/ ,5:__· _.:;ft.:__

Data Collection Field Personnel: ']"1-t , ilL<~~~--------------

Date: ;}_ - 4 - J D

Weather I Ambient Temperature: _5u"-"7 - 4.£ - ~r' s'-""","

Anaerobic Water

nZVI Tote Totalizer mixing Start Reading time (min) (gallons)

., 0 {)\Y' :). ::, '3 8 s

~t.i-- 1?4(/51-

)00">~

')_S$'-JD

f* 124$"}1

:J;:; ('A ltv ·z0 ruLr:' .... ./

p"-- ~so\~

'3Dr 1,\D'l). I)

2--''-- 1.))\ ~ \Q

\"""'-y 1-s 1}_/~

Note: 5 batches lower lift & 4 batches upper lift (460 gallons/batch)

Anaerobic Water Anaerobic Totalizer End Water Reading (Target is (gallons) 185 gallons)

24~+( 71\{

1..J>r.fV ?.-., 1Tzr -> <'?'"/ ,.-.1J'r t2L

?~wl0 144.

lv ·z.,o . ../'

\~S.

7_')\ ~G

~ \C\.'L

'•• L)lll 1..1--

\v 5"\~ l. -s-·:r=~-t

Batch Injection Injection Injection Injection Volume Start Finish Flow rate Pressure Injected Time Time (gpm) (psi) (gallons)

-

- ....-- -

!! l'f~'IC % '1-t:! - 1-N(, D './.;'o

- - - ~ -•··

14:'3 0 t5·oz. v --ell \t 0

--- - ~

l$':'0£ I) ":'-io i~·>,)"-1 -~ y ~'1\J

"' - -- -- -


Goodyear, Arizona


Notes/Comments

bc ... \-<.k v u-i---11.~'-t-, OlU-L -~ J~ b('l''-l<...y._ l"'- k ihw<dioy-

. >;~1.-Ll\<.-. ~ - .

'-'

f-.SG\ (L{_ (/-- /n..fd tl=Z.

€f* vav\eA - ::;p.o--t 0.) ia~!._ *<-

{"' Wu..L_

11---~ ~ k...,~ ,±- ~

r-*- l;J tiL~

Page -1__ ot_i_

nZVITote Batch nZVI ' ' mnang Number ToteiD time (min)

tJ:.-<1 'J,O

I rrc."'-

Zl Q_ .1,. \,_ G,\,_,/

?xJ-'1 1-?n\..._

'l 5ol ') '?b .. , II,

~~

7o~9 ' ~D

lf _,----- ,/""'

r:.r .. h -..) ,.,'f

- R.l Jkr.·t

Injection Well: IRZ-BW-

Packer Depth Interval: I 08 ft to Jl'3 ft

Data Collection Field Personnel: 3\\-, IS Date:·"!__-c=...: _ _,_Lt ___ l_o_/--::>::.---S---, 0::----

Weather /Ambient Temperature: 5v.-"l'} 1'\ ~L......... v"' Note: 5 batches lower lift & 4 batches upper lift (460 gallons/batch)


i g~ I(, D 5 I b ~D \)\ ~l~ 1!?}:;, ~+~I 1.J.p'{Ol.-. '9-\t~Jr ~ L\\.Q-0

J

tis>1'\ ~<;sg 0 ( q <"'' - ·- ~

-

173\l ~~ lGS&+- ,ii6d \-sy-- 1/. L\\J."" i(5 Z.l.. '1-~l.- ;,1

..))5 q 0 ;;~7~/ - ~

I '1/ ~ ~. ~

) b 7'7J- )(y 9S-:t 1?£ o<r~o :? 'Qet; il

\'-{s~"' I'~ l\loi ,~~J .;,.-,

.::>C,9 g 0 :?JS 15/ j, ') 1 - -.... - ....-- -:':J5 7?: d J''IOQ imv 7 V{) :.1

:J. r; 9s2? It~ ... ;ell I;{ "1-l :::, 7 t5'f. v·s::r ....

~ ~

~ ~ - - - -

~ ~ IJ!!\) a b t 51 \5'{

::>I~~~/ '::. ':7 .l ~ 'j' ,/

\))

.


Goodyear, Arizona


Notes/Comments (ex: number, duration1 & pressure of pulses)

~411; t'f1$V-fp>~j"f/ ""( '"""fb/ ~ Ds;, bf&:r

f''P.-y 5 ... ,r, "> ) D SPL ;""~'!-;.,

s." •1'\f " :, :::fJ_ d._

~ ,. i:;f."'j "', _,.r,.r A. II <'iv"5tv,

h -+obJ ~'1. '-""'-k -= 2:21 ~ ' ~\;._;L

Page __ of __

APPENDIX C

Laboratory Data Packages

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)

454-9303

LABORATORY REPORT

Prepared For: Environmental Resources Management Inc.-West

7272 E. Indian School Rd. Ste 100

Scottsdale, AZ 85251

Attention: Paula Chang Sampled:

Received:

Issued:

01/18/10

01/18/10

02/02/10 16:13

The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report

were performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unless

otherwise noted in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. This

report shall not be reproduced, except in full, without written permission from TestAmerica. The Chain(s) of Custody, 2 pages, are

included and are an integral part of this report.

This entire report was reviewed and approved for release.

Project: PGA North/103965.00

NELAP #01109CA Arizona DHS#AZ0728

CASE NARRATIVE

MATRIXCLIENT IDLABORATORY ID

PTA0778-01 IRZ-IW-05-01182010 Water

PTA0778-02 IRZ-IW-05-01182010 Water

PTA0778-03 IRZ-IW-05-01182010 Water

PTA0778-04 Trip Blank Water

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily

<Page 1 of 44>


454-9303

Environmental Resources Management Inc.-West



Attention: Paula Chang

Sampled:

Received:

01/18/10

01/18/10Report Number:

Project ID:

PTA0778

PGA North/103965.00

SAMPLE RECEIPT: Samples were received intact, at 4°C, on ice and with chain of custody documentation.

HOLDING TIMES: All samples were analyzed within prescribed holding times and/or in accordance with the TestAmerica

Sample Acceptance Policy unless otherwise noted in the report.

PRESERVATION: Samples requiring preservation were verified prior to sample analysis.

QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data qualifiers.

N1a-Method 300.0-Results exceeded the linear range in the MS/MSD and therefore are not available for

reporting. The batch was accepted based on acceptable recovery in the Blank Spike (LCS).

N1a - Sample PTA0778-04 (a trip blank) had a detectable amount of carbon disulfide above the reporting

limit. The carbon disulfide was likely from the analytical system. There was no additional sample available

for reanalysis. Note: The source of the carbon disulfide has been identified and eliminated.

R1-The RPD exceeded the acceptance limit.

COMMENTS: No significant observations were made.

SUBCONTRACTED: Refer to the last page for specific subcontract laboratory information included in this report.

Reviewed By:

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily

The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica. <Page 2 of 44>


454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

VOLATILE ORGANICS BY GC/MS (EPA 5030B/8260B)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0778-01 (IRZ-IW-05-01182010 - Water) D1

Reporting Units: ug/l

Trichloroethene 1/19/20101/19/201010A0509 5.0 10EPA 8260B 140

100 %Surrogate: Dibromofluoromethane (80-130%)

92 %Surrogate: Toluene-d8 (80-120%)

90 %Surrogate: 4-Bromofluorobenzene (80-125%)

Sample ID: PTA0778-01RE1 (IRZ-IW-05-01182010 - Water)


1/21/20101/21/2010EPA 8260BAcetone 1010A0618 1ND

1/21/20101/21/2010EPA 8260BBenzene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BBromobenzene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BBromochloromethane 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BBromodichloromethane 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BBromoform 1.010A0618 1ND

1/21/20101/21/2010EPA 8260BBromomethane 1.010A0618 1ND

1/21/20101/21/2010EPA 8260B2-Butanone (MEK) 2.510A0618 1ND

1/21/20101/21/2010EPA 8260Bn-Butylbenzene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260Bsec-Butylbenzene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260Btert-Butylbenzene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BCarbon disulfide 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BCarbon tetrachloride 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BChlorobenzene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BChloroethane 1.010A0618 1ND

1/21/20101/21/2010EPA 8260BChloroform 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BChloromethane 1.010A0618 1ND

1/21/20101/21/2010EPA 8260B2-Chlorotoluene 0.5010A0618 1ND


1/21/20101/21/2010EPA 8260BDibromochloromethane 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260B1,2-Dibromo-3-chloropropane 2.510A0618 1ND

1/21/20101/21/2010EPA 8260B1,2-Dibromoethane (EDB) 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BDibromomethane 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260B1,2-Dichlorobenzene 0.5010A0618 1ND



1/21/20101/21/2010EPA 8260BDichlorodifluoromethane 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260B1,1-Dichloroethane 0.5010A0618 1ND


1/21/20101/21/2010EPA 8260B1,1-Dichloroethene 0.5010A0618 1ND

cis-1,2-Dichloroethene 1/21/20101/21/201010A0618 0.50 1EPA 8260B 1.6

1/21/20101/21/2010EPA 8260Btrans-1,2-Dichloroethene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260B1,2-Dichloropropane 0.5010A0618 1ND


Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0778-01RE1 (IRZ-IW-05-01182010 - Water) - cont.



1/21/20101/21/2010EPA 8260B1,1-Dichloropropene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260Bcis-1,3-Dichloropropene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260Btrans-1,3-Dichloropropene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BEthylbenzene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BHexachlorobutadiene 1.010A0618 1ND

1/21/20101/21/2010EPA 8260B2-Hexanone 2.510A0618 1ND

1/21/20101/21/2010EPA 8260BIodomethane 2.510A0618 1ND

1/21/20101/21/2010EPA 8260BIsopropylbenzene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260Bp-Isopropyltoluene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BMethylene Chloride 1.010A0618 1ND

1/21/20101/21/2010EPA 8260B4-Methyl-2-pentanone (MIBK) 2.510A0618 1ND

1/21/20101/21/2010EPA 8260BMethyl-tert-butyl Ether (MTBE) 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BNaphthalene 2.510A0618 1ND

1/21/20101/21/2010EPA 8260Bn-Propylbenzene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BStyrene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260B1,1,1,2-Tetrachloroethane 0.5010A0618 1ND


1/21/20101/21/2010EPA 8260BTetrachloroethene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BToluene 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260B1,2,3-Trichlorobenzene 1.010A0618 1ND


1/21/20101/21/2010EPA 8260B1,1,1-Trichloroethane 0.5010A0618 1ND


1/21/20101/21/2010EPA 8260BTrichlorofluoromethane 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260B1,2,3-Trichloropropane 1.010A0618 1ND

1/21/20101/21/2010EPA 8260B1,2,4-Trimethylbenzene 0.5010A0618 1ND


1/21/20101/21/2010EPA 8260BVinyl Acetate 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BVinyl chloride 0.5010A0618 1ND

1/21/20101/21/2010EPA 8260BXylenes, Total 1.010A0618 1ND




Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0778-04 (Trip Blank - Water)


1/19/20101/19/2010EPA 8260BAcetone 1010A0509 1ND

1/19/20101/19/2010EPA 8260BBenzene 0.5010A0509 1ND










Carbon disulfide 1/19/20101/19/201010A0509 0.50 N1a1EPA 8260B 1.4



















1/19/20101/19/2010EPA 8260Bcis-1,2-Dichloroethene 0.5010A0509 1ND










Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0778-04 (Trip Blank - Water) - cont.











1/19/20101/19/2010EPA 8260BStyrene 0.5010A0509 1ND




1/19/20101/19/2010EPA 8260BToluene 0.5010A0509 1ND





1/19/20101/19/2010EPA 8260BTrichloroethene 0.5010A0509 1ND











Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0778-01 (IRZ-IW-05-01182010 - Water)

Reporting Units: mg/l

Boron 1/20/20101/19/201010A0524 0.20 1E200.7 55

Calcium 1/20/20101/19/201010A0524 2.0 1E200.7 280

Iron 1/20/20101/19/201010A0524 0.050 1E200.7 1300

Magnesium 1/20/20101/19/201010A0524 2.0 1E200.7 100

Manganese 1/20/20101/19/201010A0524 0.010 1E200.7 5.3

Sodium 1/20/20101/19/201010A0524 2.0 1E200.7 320

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

DISSOLVED METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 1/22/20101/21/201010A0620 0.050 1E200.7 6.6

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Alkalinity as CaCO3 1/21/20101/21/201010A0597 6.0 1M2320 B 160

1/20/20101/19/2010SM4500-NH3DAmmonia-N 0.5010A0519 1ND

Bicarbonate Alkalinity as CaCO3 1/21/20101/21/201010A0597 6.0 1M2320 B 160

1/21/20101/21/2010M2320 BCarbonate Alkalinity as CaCO3 6.010A0597 1ND

1/21/20101/21/2010M2320 BHydroxide Alkalinity as CaCO3 6.010A0597 1ND

Nitrate-N 1/19/20101/19/201010A0489 0.20 1EPA 300.0 3.3

Phosphate 1/22/20101/22/201010A0639 0.30 1SM 4500-P B, E 430

Phosphorus,Total - P 1/21/20101/20/201010A0562 25 250M4500-P B, E 140

1/21/20101/21/2010M2320 BAlkalinity, Phenolphthalein 6.010A0597 1ND



1/21/20101/21/2010EPA 314.0Perchlorate 2.010A0602 E41ND



Chloride 1/22/20101/22/201010A0648 20 10EPA 300.0 750

Sulfate 1/22/20101/22/201010A0648 20 10EPA 300.0 800

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL ORGANIC CARBON (SM 5310B)

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Total Organic Carbon 1/20/20101/19/201010A0510 1.0 1M5310B 1.4

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS (EPA 300.1)

Data

QualifiersBatch

Reporting

Limit

Sample

Result



1/21/20101/21/2010EPA 300.1Chlorate 10010A2026 D15ND

1/21/20101/21/2010EPA 300.1Chlorite 10010A2026 D15ND

97 %Surrogate: Dichloroacetate (DCA) (90-115%)

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

SHORT HOLD TIME DETAIL REPORT

Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: IRZ-IW-05-01182010 (PTA0778-01) - Water

2 01/18/2010 12:35 01/18/2010 17:27 01/19/2010 08:45 01/19/2010 11:34EPA 300.0

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte


METHOD BLANK/QC DATA

Data

Qualifiers

Batch: 10A0509 Extracted: 01/19/10

Blank Analyzed: 01/19/2010 (10A0509-BLK1)

Acetone ug/l10ND

Benzene ug/l0.50ND

Bromobenzene ug/l0.50ND

Bromochloromethane ug/l0.50ND

Bromodichloromethane ug/l0.50ND

Bromoform ug/l1.0ND

Bromomethane ug/l1.0ND

2-Butanone (MEK) ug/l2.5ND

n-Butylbenzene ug/l0.50ND

sec-Butylbenzene ug/l0.50ND

tert-Butylbenzene ug/l0.50ND

Carbon disulfide ug/l0.50ND

Carbon tetrachloride ug/l0.50ND

Chlorobenzene ug/l0.50ND

Chloroethane ug/l1.0ND

Chloroform ug/l0.50ND

Chloromethane ug/l1.0ND

2-Chlorotoluene ug/l0.50ND


Dibromochloromethane ug/l0.50ND

1,2-Dibromo-3-chloropropane ug/l2.5ND

1,2-Dibromoethane (EDB) ug/l0.50ND

Dibromomethane ug/l0.50ND

1,2-Dichlorobenzene ug/l0.50ND



Dichlorodifluoromethane ug/l0.50ND

1,1-Dichloroethane ug/l0.50ND


1,1-Dichloroethene ug/l0.50ND

cis-1,2-Dichloroethene ug/l0.50ND

trans-1,2-Dichloroethene ug/l0.50ND

1,2-Dichloropropane ug/l0.50ND



Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene ug/l0.50ND

cis-1,3-Dichloropropene ug/l0.50ND

trans-1,3-Dichloropropene ug/l0.50ND

Ethylbenzene ug/l0.50ND

Hexachlorobutadiene ug/l1.0ND

2-Hexanone ug/l2.5ND

Iodomethane ug/l2.5ND

Isopropylbenzene ug/l0.50ND

p-Isopropyltoluene ug/l0.50ND

Methylene Chloride ug/l1.0ND

4-Methyl-2-pentanone (MIBK) ug/l2.5ND

Methyl-tert-butyl Ether (MTBE) ug/l0.50ND

Naphthalene ug/l2.5ND

n-Propylbenzene ug/l0.50ND

Styrene ug/l0.50ND

1,1,1,2-Tetrachloroethane ug/l0.50ND


Tetrachloroethene ug/l0.50ND

Toluene ug/l0.50ND

1,2,3-Trichlorobenzene ug/l1.0ND


1,1,1-Trichloroethane ug/l0.50ND


Trichloroethene ug/l0.50ND

Trichlorofluoromethane ug/l0.50ND

1,2,3-Trichloropropane ug/l1.0ND

1,2,4-Trimethylbenzene ug/l0.50ND


Vinyl Acetate ug/l0.50ND

Vinyl chloride ug/l0.50ND

Xylenes, Total ug/l1.0ND

25.0 80-130Surrogate: Dibromofluoromethane ug/l26.0 104

25.0 80-120Surrogate: Toluene-d8 ug/l23.2 93

25.0 80-125Surrogate: 4-Bromofluorobenzene ug/l23.1 93

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/19/2010 (10A0509-BS1)

Acetone 25.0 10-150ug/l1026.8 107

Benzene 25.0 80-120ug/l0.5025.0 100

Bromobenzene 25.0 80-120ug/l0.5025.4 102

Bromochloromethane 25.0 80-125ug/l0.5027.2 109

Bromodichloromethane 25.0 80-120ug/l0.5022.9 92

Bromoform 25.0 75-130ug/l1.024.9 100

Bromomethane 25.0 55-150ug/l1.022.0 88

2-Butanone (MEK) 25.0 40-150ug/l2.529.7 119

n-Butylbenzene 25.0 80-130ug/l0.5025.1 101

sec-Butylbenzene 25.0 80-125ug/l0.5025.4 101

tert-Butylbenzene 25.0 80-120ug/l0.5025.4 101

Carbon disulfide 25.0 70-140ug/l0.5029.4 117

Carbon tetrachloride 25.0 75-130ug/l0.5023.8 95

Chlorobenzene 25.0 80-120ug/l0.5025.0 100

Chloroethane 25.0 70-130ug/l1.023.0 92

Chloroform 25.0 75-120ug/l0.5024.2 97

Chloromethane 25.0 60-140ug/l1.021.3 85

2-Chlorotoluene 25.0 80-120ug/l0.5024.1 96


Dibromochloromethane 25.0 80-120ug/l0.5022.1 88

1,2-Dibromo-3-chloropropane 25.0 50-150ug/l2.527.0 108

1,2-Dibromoethane (EDB) 25.0 80-120ug/l0.5025.6 103

Dibromomethane 25.0 75-120ug/l0.5024.0 96

1,2-Dichlorobenzene 25.0 80-120ug/l0.5025.4 102



Dichlorodifluoromethane 25.0 60-150ug/l0.5022.1 88

1,1-Dichloroethane 25.0 70-125ug/l0.5024.4 98


1,1-Dichloroethene 25.0 75-125ug/l0.5026.2 105

cis-1,2-Dichloroethene 25.0 80-120ug/l0.5027.1 108

trans-1,2-Dichloroethene 25.0 80-120ug/l0.5026.3 105

1,2-Dichloropropane 25.0 80-120ug/l0.5023.6 94



Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/19/2010 (10A0509-BS1)

1,1-Dichloropropene 25.0 75-120ug/l0.5024.7 99

cis-1,3-Dichloropropene 25.0 80-120ug/l0.5023.1 92

trans-1,3-Dichloropropene 25.0 80-125ug/l0.5023.3 93

Ethylbenzene 25.0 80-120ug/l0.5024.2 97

Hexachlorobutadiene 25.0 40-150ug/l1.026.7 107

2-Hexanone 25.0 20-150ug/l2.526.3 105

Iodomethane 25.0 80-130ug/l2.524.7 99

Isopropylbenzene 25.0 80-130ug/l0.5024.5 98

p-Isopropyltoluene 25.0 80-130ug/l0.5026.4 105

Methylene Chloride 25.0 70-120ug/l1.025.2 101

4-Methyl-2-pentanone (MIBK) 25.0 60-135ug/l2.524.4 98

Methyl-tert-butyl Ether (MTBE) 25.0 70-130ug/l0.5025.0 100

Naphthalene 25.0 40-150ug/l2.527.6 110

n-Propylbenzene 25.0 75-130ug/l0.5024.7 99

Styrene 25.0 80-120ug/l0.5024.1 96

1,1,1,2-Tetrachloroethane 25.0 75-125ug/l0.5024.4 98


Tetrachloroethene 25.0 70-130ug/l0.5025.7 103

Toluene 25.0 80-120ug/l0.5023.8 95

1,2,3-Trichlorobenzene 25.0 55-150ug/l1.028.3 113


1,1,1-Trichloroethane 25.0 75-125ug/l0.5023.6 94


Trichloroethene 25.0 80-120ug/l0.5024.4 98

Trichlorofluoromethane 25.0 70-150ug/l0.5022.7 91

1,2,3-Trichloropropane 25.0 70-130ug/l1.026.4 106

1,2,4-Trimethylbenzene 25.0 80-120ug/l0.5024.4 97


Vinyl Acetate 25.0 40-150ug/l0.5023.8 95

Vinyl chloride 25.0 70-130ug/l0.5023.6 94

Xylenes, Total 75.0 60-140ug/l1.073.2 98




Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Dup Analyzed: 01/19/2010 (10A0509-BSD1)

Acetone 25.0 3510-150ug/l1018.9 76 35

Benzene 25.0 1580-120ug/l0.5024.3 97 3

Bromobenzene 25.0 1580-120ug/l0.5025.3 101 1

Bromochloromethane 25.0 1580-125ug/l0.5025.6 103 6

Bromodichloromethane 25.0 1580-120ug/l0.5022.5 90 2

Bromoform 25.0 2075-130ug/l1.023.9 96 4

Bromomethane 25.0 2055-150ug/l1.021.9 88 0

2-Butanone (MEK) 25.0 3540-150ug/l2.524.7 99 18

n-Butylbenzene 25.0 1580-130ug/l0.5025.2 101 0

sec-Butylbenzene 25.0 1580-125ug/l0.5025.3 101 0

tert-Butylbenzene 25.0 1580-120ug/l0.5025.6 102 1

Carbon disulfide 25.0 1570-140ug/l0.5028.3 113 4

Carbon tetrachloride 25.0 2075-130ug/l0.5023.3 93 2

Chlorobenzene 25.0 1580-120ug/l0.5024.7 99 1

Chloroethane 25.0 1570-130ug/l1.022.4 89 3

Chloroform 25.0 1575-120ug/l0.5023.6 94 3

Chloromethane 25.0 2060-140ug/l1.020.9 84 2

2-Chlorotoluene 25.0 1580-120ug/l0.5024.4 97 1


Dibromochloromethane 25.0 1580-120ug/l0.5024.1 96 9

1,2-Dibromo-3-chloropropane 25.0 3550-150ug/l2.525.0 100 8

1,2-Dibromoethane (EDB) 25.0 1580-120ug/l0.5024.3 97 5

Dibromomethane 25.0 1575-120ug/l0.5022.7 91 6

1,2-Dichlorobenzene 25.0 1580-120ug/l0.5025.1 100 1



Dichlorodifluoromethane 25.0 3060-150ug/l0.5021.1 85 4

1,1-Dichloroethane 25.0 1570-125ug/l0.5023.7 95 3


1,1-Dichloroethene 25.0 2075-125ug/l0.5024.9 100 5

cis-1,2-Dichloroethene 25.0 1580-120ug/l0.5026.2 105 3

trans-1,2-Dichloroethene 25.0 1580-120ug/l0.5025.4 102 4

1,2-Dichloropropane 25.0 1580-120ug/l0.5023.2 93 2



Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 1575-120ug/l0.5024.1 96 3

cis-1,3-Dichloropropene 25.0 1580-120ug/l0.5022.2 89 4

trans-1,3-Dichloropropene 25.0 1580-125ug/l0.5022.5 90 4

Ethylbenzene 25.0 1580-120ug/l0.5023.9 95 1

Hexachlorobutadiene 25.0 3540-150ug/l1.027.0 108 1

2-Hexanone 25.0 3520-150ug/l2.523.8 95 10

Iodomethane 25.0 1080-130ug/l2.524.2 97 2

Isopropylbenzene 25.0 1580-130ug/l0.5024.2 97 1

p-Isopropyltoluene 25.0 1580-130ug/l0.5025.7 103 2

Methylene Chloride 25.0 1570-120ug/l1.024.3 97 4

4-Methyl-2-pentanone (MIBK) 25.0 2560-135ug/l2.523.3 93 5

Methyl-tert-butyl Ether (MTBE) 25.0 2070-130ug/l0.5022.9 92 9

Naphthalene 25.0 3040-150ug/l2.526.1 105 5

n-Propylbenzene 25.0 1575-130ug/l0.5025.4 102 3

Styrene 25.0 1580-120ug/l0.5023.9 96 1

1,1,1,2-Tetrachloroethane 25.0 1575-125ug/l0.5024.6 98 1


Tetrachloroethene 25.0 2070-130ug/l0.5025.2 101 2

Toluene 25.0 1580-120ug/l0.5023.8 95 0

1,2,3-Trichlorobenzene 25.0 3555-150ug/l1.027.6 110 2


1,1,1-Trichloroethane 25.0 1575-125ug/l0.5023.2 93 2


Trichloroethene 25.0 1580-120ug/l0.5024.5 98 0

Trichlorofluoromethane 25.0 2570-150ug/l0.5021.3 85 6

1,2,3-Trichloropropane 25.0 2070-130ug/l1.025.0 100 6

1,2,4-Trimethylbenzene 25.0 1580-120ug/l0.5024.2 97 1


Vinyl Acetate 25.0 2540-150ug/l0.5021.6 87 9

Vinyl chloride 25.0 2070-130ug/l0.5022.4 89 5

Xylenes, Total 75.0 1560-140ug/l1.073.8 98 1




Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 01/19/2010 (10A0509-MS1) Source: PTA0786-02

Acetone 25.0 10-150ug/l1011.1 ND 44

Benzene 25.0 70-125ug/l0.5024.3 ND 97

Bromobenzene 25.0 75-120ug/l0.5025.2 ND 101

Bromochloromethane 25.0 75-130ug/l0.5026.2 ND 105

Bromodichloromethane 25.0 75-125ug/l0.5022.6 ND 90

Bromoform 25.0 65-125ug/l1.024.0 ND 96

Bromomethane 25.0 45-150ug/l1.016.0 ND 64

2-Butanone (MEK) 25.0 15-150ug/l2.517.2 ND 69

n-Butylbenzene 25.0 70-130ug/l0.5024.2 ND 97

sec-Butylbenzene 25.0 70-125ug/l0.5025.3 ND 101

tert-Butylbenzene 25.0 70-125ug/l0.5025.2 ND 101

Carbon disulfide 25.0 65-145ug/l0.5029.4 0.750 114

Carbon tetrachloride 25.0 65-135ug/l0.5023.6 ND 94

Chlorobenzene 25.0 75-120ug/l0.5024.6 ND 98

Chloroethane 25.0 65-140ug/l1.023.5 ND 94

Chloroform 25.0 70-130ug/l0.5023.4 ND 94

Chloromethane 25.0 55-145ug/l1.019.8 ND 79

2-Chlorotoluene 25.0 70-125ug/l0.5023.7 ND 95


Dibromochloromethane 25.0 70-130ug/l0.5024.0 ND 96

1,2-Dibromo-3-chloropropane 25.0 50-150ug/l2.524.0 ND 96

1,2-Dibromoethane (EDB) 25.0 70-125ug/l0.5024.8 ND 99

Dibromomethane 25.0 70-120ug/l0.5023.8 ND 95

1,2-Dichlorobenzene 25.0 75-120ug/l0.5024.9 ND 100



Dichlorodifluoromethane 25.0 60-150ug/l0.5019.5 ND 78

1,1-Dichloroethane 25.0 70-130ug/l0.5023.3 ND 93


1,1-Dichloroethene 25.0 70-130ug/l0.5025.9 ND 104

cis-1,2-Dichloroethene 25.0 70-125ug/l0.5025.8 ND 103

trans-1,2-Dichloroethene 25.0 75-125ug/l0.5025.5 ND 102

1,2-Dichloropropane 25.0 75-125ug/l0.5022.5 ND 90



Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 65-130ug/l0.5024.2 ND 97

cis-1,3-Dichloropropene 25.0 75-130ug/l0.5022.0 ND 88

trans-1,3-Dichloropropene 25.0 70-130ug/l0.5022.1 ND 88

Ethylbenzene 25.0 70-125ug/l0.5023.4 ND 94

Hexachlorobutadiene 25.0 40-150ug/l1.025.5 ND 102

2-Hexanone 25.0 20-150ug/l2.520.8 ND 83

Iodomethane 25.0 60-150ug/l2.522.4 ND 90

Isopropylbenzene 25.0 75-130ug/l0.5023.9 ND 96

p-Isopropyltoluene 25.0 70-130ug/l0.5025.3 ND 101

Methylene Chloride 25.0 65-130ug/l1.024.6 ND 98

4-Methyl-2-pentanone (MIBK) 25.0 55-135ug/l2.521.3 ND 85

Methyl-tert-butyl Ether (MTBE) 25.0 65-140ug/l0.5023.6 ND 94

Naphthalene 25.0 40-150ug/l2.525.9 ND 104

n-Propylbenzene 25.0 70-130ug/l0.5024.8 ND 99

Styrene 25.0 55-135ug/l0.5022.5 ND 90

1,1,1,2-Tetrachloroethane 25.0 70-125ug/l0.5024.2 ND 97


Tetrachloroethene 25.0 65-130ug/l0.5025.2 ND 101

Toluene 25.0 70-125ug/l0.5023.3 ND 93

1,2,3-Trichlorobenzene 25.0 50-150ug/l1.027.0 ND 108


1,1,1-Trichloroethane 25.0 70-130ug/l0.5023.0 ND 92


Trichloroethene 25.0 70-125ug/l0.5025.2 2.01 93

Trichlorofluoromethane 25.0 65-150ug/l0.5022.1 ND 88

1,2,3-Trichloropropane 25.0 70-130ug/l1.025.2 ND 101

1,2,4-Trimethylbenzene 25.0 70-125ug/l0.5023.7 ND 95


Vinyl Acetate 25.0 40-150ug/l0.5020.0 ND 80

Vinyl chloride 25.0 60-140ug/l0.5023.4 ND 94

Xylenes, Total 75.0 75-120ug/l1.072.0 ND 96




Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 01/19/2010 (10A0509-MSD1) Source: PTA0786-02

Acetone 25.0 3510-150ug/l1021.0 R1ND 84 62

Benzene 25.0 2570-125ug/l0.5025.1 ND 101 3

Bromobenzene 25.0 2075-120ug/l0.5027.1 ND 108 7

Bromochloromethane 25.0 2075-130ug/l0.5027.4 ND 110 4

Bromodichloromethane 25.0 2075-125ug/l0.5023.2 ND 93 2

Bromoform 25.0 2565-125ug/l1.025.5 ND 102 6

Bromomethane 25.0 3545-150ug/l1.021.1 ND 85 28

2-Butanone (MEK) 25.0 3015-150ug/l2.526.3 R1ND 105 42

n-Butylbenzene 25.0 3070-130ug/l0.5025.8 ND 103 6

sec-Butylbenzene 25.0 3070-125ug/l0.5027.2 ND 109 8

tert-Butylbenzene 25.0 2570-125ug/l0.5026.7 ND 107 6

Carbon disulfide 25.0 2565-145ug/l0.5031.1 0.750 121 6

Carbon tetrachloride 25.0 2565-135ug/l0.5024.9 ND 100 6

Chlorobenzene 25.0 2075-120ug/l0.5025.5 ND 102 4

Chloroethane 25.0 2565-140ug/l1.023.6 ND 95 1

Chloroform 25.0 2070-130ug/l0.5024.4 ND 98 4

Chloromethane 25.0 3555-145ug/l1.021.5 ND 86 8

2-Chlorotoluene 25.0 2570-125ug/l0.5025.6 ND 102 8


Dibromochloromethane 25.0 2070-130ug/l0.5025.2 ND 101 5

1,2-Dibromo-3-chloropropane 25.0 3050-150ug/l2.529.7 ND 119 21

1,2-Dibromoethane (EDB) 25.0 2070-125ug/l0.5026.5 ND 106 7

Dibromomethane 25.0 2070-120ug/l0.5025.0 ND 100 5

1,2-Dichlorobenzene 25.0 2075-120ug/l0.5026.7 ND 107 7



Dichlorodifluoromethane 25.0 3060-150ug/l0.5021.3 ND 85 9

1,1-Dichloroethane 25.0 2070-130ug/l0.5024.4 ND 98 5


1,1-Dichloroethene 25.0 2570-130ug/l0.5027.2 ND 109 5

cis-1,2-Dichloroethene 25.0 2070-125ug/l0.5027.2 ND 109 5

trans-1,2-Dichloroethene 25.0 2575-125ug/l0.5027.2 ND 109 6

1,2-Dichloropropane 25.0 2075-125ug/l0.5023.8 ND 95 5



Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 2565-130ug/l0.5025.8 ND 103 7

cis-1,3-Dichloropropene 25.0 2075-130ug/l0.5023.1 ND 92 5

trans-1,3-Dichloropropene 25.0 2070-130ug/l0.5023.0 ND 92 4

Ethylbenzene 25.0 2570-125ug/l0.5024.5 ND 98 4

Hexachlorobutadiene 25.0 3040-150ug/l1.028.0 ND 112 9

2-Hexanone 25.0 3020-150ug/l2.526.6 ND 106 25

Iodomethane 25.0 3060-150ug/l2.525.5 ND 102 13

Isopropylbenzene 25.0 2575-130ug/l0.5025.2 ND 101 5

p-Isopropyltoluene 25.0 3070-130ug/l0.5027.2 ND 109 7

Methylene Chloride 25.0 2065-130ug/l1.025.4 ND 101 3

4-Methyl-2-pentanone (MIBK) 25.0 2555-135ug/l2.526.5 ND 106 22

Methyl-tert-butyl Ether (MTBE) 25.0 2565-140ug/l0.5025.5 ND 102 8

Naphthalene 25.0 3040-150ug/l2.530.1 ND 120 15

n-Propylbenzene 25.0 3070-130ug/l0.5026.5 ND 106 7

Styrene 25.0 3555-135ug/l0.5023.6 ND 94 5

1,1,1,2-Tetrachloroethane 25.0 2070-125ug/l0.5025.2 ND 101 4


Tetrachloroethene 25.0 2565-130ug/l0.5026.6 ND 106 5

Toluene 25.0 2070-125ug/l0.5024.4 ND 98 5

1,2,3-Trichlorobenzene 25.0 3550-150ug/l1.029.7 ND 119 9


1,1,1-Trichloroethane 25.0 2570-130ug/l0.5023.9 ND 96 4


Trichloroethene 25.0 2570-125ug/l0.5025.8 2.01 95 2

Trichlorofluoromethane 25.0 2565-150ug/l0.5023.5 ND 94 6

1,2,3-Trichloropropane 25.0 2570-130ug/l1.029.2 ND 117 15

1,2,4-Trimethylbenzene 25.0 3070-125ug/l0.5025.7 ND 103 8


Vinyl Acetate 25.0 3040-150ug/l0.5021.1 ND 84 5

Vinyl chloride 25.0 2560-140ug/l0.5024.8 ND 99 6

Xylenes, Total 75.0 1575-120ug/l1.075.2 ND 100 4




Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/21/2010 (10A0618-BS1)

Acetone 25.0 10-150ug/l1031.5 126

Benzene 25.0 80-120ug/l0.5024.4 98




Bromoform 25.0 75-130ug/l1.024.2 97


2-Butanone (MEK) 25.0 40-150ug/l2.532.6 130








Chloroform 25.0 75-120ug/l0.5023.3 93




















Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/21/2010 (10A0618-BS1)






2-Hexanone 25.0 20-150ug/l2.530.0 120

Iodomethane 25.0 80-130ug/l2.524.1 96






Naphthalene 25.0 40-150ug/l2.528.5 114


Styrene 25.0 80-120ug/l0.5024.0 96




Toluene 25.0 80-120ug/l0.5023.2 93
















Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1020.7 R683 41

Benzene 25.0 1580-120ug/l0.5024.1 96 1




Bromoform 25.0 2075-130ug/l1.022.2 89 9


2-Butanone (MEK) 25.0 3540-150ug/l2.524.0 96 31








Chloroform 25.0 1575-120ug/l0.5023.4 94 0




















Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3520-150ug/l2.523.3 93 25

Iodomethane 25.0 1080-130ug/l2.524.6 98 2






Naphthalene 25.0 3040-150ug/l2.526.1 104 9


Styrene 25.0 1580-120ug/l0.5023.3 93 3




Toluene 25.0 1580-120ug/l0.5023.3 93 0
















Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1018.2 ND 73

Benzene 25.0 70-125ug/l0.5025.3 ND 101




Bromoform 25.0 65-125ug/l1.023.7 ND 95






Carbon disulfide 25.0 65-145ug/l0.5030.0 ND 120
























Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.523.0 ND 92









Styrene 25.0 55-135ug/l0.5019.6 ND 78



Tetrachloroethene 25.0 65-130ug/l0.5026.4 0.380 104

Toluene 25.0 70-125ug/l0.5024.0 ND 96





Trichloroethene 25.0 70-125ug/l0.5025.4 ND 102











Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1016.8 ND 67 8

Benzene 25.0 2570-125ug/l0.5023.2 ND 93 8




Bromoform 25.0 2565-125ug/l1.022.8 ND 91 4


2-Butanone (MEK) 25.0 3015-150ug/l2.524.0 ND 96 13




Carbon disulfide 25.0 2565-145ug/l0.5026.9 ND 108 11
























Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3020-150ug/l2.523.8 ND 95 4









Styrene 25.0 3555-135ug/l0.5017.5 ND 70 11



Tetrachloroethene 25.0 2565-130ug/l0.5023.9 0.380 94 10

Toluene 25.0 2070-125ug/l0.5022.0 ND 88 9





Trichloroethene 25.0 2570-125ug/l0.5022.6 ND 90 12











Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Boron mg/l0.20ND

Calcium mg/l2.0ND

Iron mg/l0.050ND

Magnesium mg/l2.0ND

Manganese mg/l0.010ND

Sodium mg/l2.0ND

LCS Analyzed: 01/20/2010 (10A0524-BS1)

Boron 1.00 85-115mg/l0.200.991 99

Calcium 21.0 85-115mg/l2.021.2 101

Iron 1.00 85-115mg/l0.0501.04 104

Magnesium 21.0 85-115mg/l2.021.9 104

Manganese 1.00 85-115mg/l0.0101.01 101

Sodium 20.0 85-115mg/l2.020.3 101


Boron 1.00 2085-115mg/l0.200.961 96 3

Calcium 21.0 2085-115mg/l2.021.3 101 0

Iron 1.00 2085-115mg/l0.0501.04 104 0

Magnesium 21.0 2085-115mg/l2.021.2 101 3

Manganese 1.00 2085-115mg/l0.0100.987 99 3

Sodium 20.0 2085-115mg/l2.019.6 98 3


Boron 1.00 75-125mg/l0.201.09 0.106 99

Calcium 21.0 75-125mg/l2.067.3 45.9 102

Iron 1.00 75-125mg/l0.0501.55 0.492 105

Magnesium 21.0 75-125mg/l2.039.4 17.9 102

Manganese 1.00 75-125mg/l0.0100.992 0.0137 98

Sodium 20.0 75-125mg/l2.0142 122 104

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Boron 1.00 75-125mg/l0.201.06 ND 106

Calcium 21.0 75-125mg/l2.0541 M2534 33

Iron 1.00 75-125mg/l0.0501.18 0.130 105

Magnesium 21.0 75-125mg/l2.077.6 57.0 98

Manganese 1.00 75-125mg/l0.0100.967 0.00179 97

Sodium 20.0 75-125mg/l2.065.1 45.2 100


Boron 1.00 1075-125mg/l0.201.13 0.106 103 4

Calcium 21.0 1075-125mg/l2.068.7 45.9 109 2

Iron 1.00 1075-125mg/l0.0501.56 0.492 107 1

Magnesium 21.0 1075-125mg/l2.040.7 17.9 108 3

Manganese 1.00 1075-125mg/l0.0101.02 0.0137 101 3

Sodium 20.0 1075-125mg/l2.0147 M1122 128 3


Boron 1.00 1075-125mg/l0.201.07 ND 107 1

Calcium 21.0 1075-125mg/l2.0557 534 111 3

Iron 1.00 1075-125mg/l0.0501.21 0.130 108 3

Magnesium 21.0 1075-125mg/l2.079.2 57.0 106 2

Manganese 1.00 1075-125mg/l0.0100.981 0.00179 98 1

Sodium 20.0 1075-125mg/l2.066.1 45.2 105 1

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

DISSOLVED METALS


Data

Qualifiers



Iron mg/l0.050ND


Iron mg/l0.050ND

LCS Analyzed: 01/22/2010 (10A0620-BS1)

Iron 1.00 85-115mg/l0.0500.983 98


Iron 1.00 2085-115mg/l0.0500.976 98 1


Iron 1.00 75-125mg/l0.0500.966 ND 97


Iron 1.00 75-125mg/l0.0502.83 1.76 107


Iron 1.00 1075-125mg/l0.0500.957 ND 96 1


Iron 1.00 1075-125mg/l0.0502.92 1.76 117 3

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Chloride mg/l2.0ND

Nitrate-N mg/l0.20ND

Sulfate mg/l2.0ND

LCS Analyzed: 01/19/2010 (10A0489-BS1)

Chloride 20.0 90-110mg/lNA20.1 100

Nitrate-N 4.00 90-110mg/lNA4.08 102

Sulfate 20.0 90-110mg/lNA20.6 103


Chloride 20.0 1590-110mg/lNA20.1 100 0

Nitrate-N 4.00 1590-110mg/lNA4.13 103 1

Sulfate 20.0 1590-110mg/lNA20.6 103 0


Chloride 20.0 80-120mg/l2.058.4 39.0 97

Nitrate-N 4.00 80-120mg/l0.204.94 0.785 104

Sulfate 20.0 80-120mg/l2.074.9 56.7 91


Chloride 20.0 1580-120mg/l2.058.3 39.0 96 0

Nitrate-N 4.00 1580-120mg/l0.204.86 0.785 102 2

Sulfate 20.0 1580-120mg/l2.074.4 56.7 89 1



Ammonia-N mg/l0.50ND

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers


LCS Analyzed: 01/20/2010 (10A0519-BS1)

Ammonia-N 10.0 85-115mg/l0.5011.3 113


Ammonia-N 10.0 2085-115mg/l0.5010.8 108 4


Ammonia-N 10.0 70-130mg/l0.509.39 0.500 89


Ammonia-N 10.0 2070-130mg/l0.509.57 0.500 91 2



Phosphorus,Total - P mg/l0.10ND

LCS Analyzed: 01/21/2010 (10A0562-BS1)

Phosphorus,Total - P 0.300 90-110mg/l0.100.327 109


Phosphorus,Total - P 0.300 2090-110mg/l0.100.330 110 1


Phosphorus,Total - P 0.300 80-120mg/l0.100.224 M20.0670 52



Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Phosphorus,Total - P 0.300 2080-120mg/l0.100.219 M20.0670 51 2


Phosphorus,Total - P 0.300 2080-120mg/l0.100.547 0.194 118 3



Alkalinity as CaCO3 mg/l6.0ND

Bicarbonate Alkalinity as CaCO3 mg/l6.0ND

Carbonate Alkalinity as CaCO3 mg/l6.0ND

Hydroxide Alkalinity as CaCO3 mg/l6.0ND

Alkalinity, Phenolphthalein mg/l6.0ND

LCS Analyzed: 01/21/2010 (10A0597-BS1)

Alkalinity as CaCO3 250 90-110mg/l6.0256 102


Alkalinity as CaCO3 250 2090-110mg/l6.0257 103 0

Duplicate Analyzed: 01/21/2010 (10A0597-DUP1) Source: PTA0680-01

Alkalinity as CaCO3 20mg/l6.080.7 82.0 2

Bicarbonate Alkalinity as CaCO3 20mg/l6.080.7 82.0 2

Carbonate Alkalinity as CaCO3 20mg/l6.0ND ND

Hydroxide Alkalinity as CaCO3 20mg/l6.0ND ND

Alkalinity, Phenolphthalein 20mg/l6.0ND ND

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Alkalinity as CaCO3 20mg/l6.0175 175 0

Bicarbonate Alkalinity as CaCO3 20mg/l6.0175 175 0






Perchlorate ug/l2.0ND

LCS Analyzed: 01/21/2010 (10A0602-BS1)

Perchlorate 25.0 85-115ug/lNA27.0 108


Perchlorate 25.0 1585-115ug/lNA24.7 99 9


Perchlorate 15ug/l2.011.2 11.7 4




Perchlorate 25.0 80-120ug/l2.025.1 1.13 96


Perchlorate 25.0 80-120ug/l2.025.6 1.91 95

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Perchlorate 25.0 1580-120ug/l2.022.9 1.13 87 9


Perchlorate 25.0 1580-120ug/l2.026.2 1.91 97 2



Chloride mg/l2.0ND

Sulfate mg/l2.0ND

LCS Analyzed: 01/22/2010 (10A0648-BS1)

Chloride 20.0 90-110mg/lNA19.6 N1a98

Sulfate 20.0 90-110mg/lNA20.2 N1a101


Chloride 20.0 1590-110mg/lNA19.6 N1a98 0

Sulfate 20.0 1590-110mg/lNA20.2 N1a101 0


Chloride 20.0 80-120mg/l2.029.6 M227.4 11


Chloride 20.0 1580-120mg/l2.027.0 M227.4 -2 9

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Total Organic Carbon mg/l1.0ND

LCS Analyzed: 01/20/2010 (10A0510-BS1)

Total Organic Carbon 20.0 80-120mg/l1.019.4 97


Total Organic Carbon 20.0 2080-120mg/l1.019.4 97 0


Total Organic Carbon 20.0 80-120mg/l1.020.9 ND 104


Total Organic Carbon 20.0 2080-120mg/l1.019.2 ND 96 8

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorate ug/l20ND

Chlorite ug/l20ND

1.00 90-115Surrogate: Dichloroacetate (DCA) ug/l1.00 100

LCS Analyzed: 01/21/2010 (10A2026-BS1)

Chlorate 100 75-125ug/l2098.0 98

Chlorite 100 75-125ug/l2097.7 98


Matrix Spike Analyzed: 01/21/2010 (10A2026-MS1) Source: ITA1034-01

Chlorate 100 75-125ug/l40100 ND 100

Chlorite 100 75-125ug/l4097.7 ND 98


Matrix Spike Dup Analyzed: 01/21/2010 (10A2026-MSD1) Source: ITA1034-01

Chlorate 100 2575-125ug/l4098.7 ND 99 1

Chlorite 100 2575-125ug/l4093.0 ND 93 5


Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

DATA QUALIFIERS AND DEFINITIONS

D1 Sample required dilution due to matrix.

E4 Concentration estimated. Analyte was detected below laboratory minimum reporting limit (MRL).

M1 Matrix spike recovery was high; the associated blank spike recovery was acceptable.

M2 Matrix spike recovery was low; the associated blank spike recovery was acceptable.

N1 See case narrative.

R1 The RPD/RSD exceeded the method acceptance limit.

R6 LFB/LFBD RPD exceeded the method acceptance limit. Recovery met acceptance criteria.

Relative Percent DifferenceRPD

Analyte NOT DETECTED at or above the reporting limit or MDL, if MDL is specified.ND

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily




454-9303





Sampled:

Received:

01/18/10


Project ID:

PTA0778

PGA North/103965.00

Certification Summary

Method Matrix Nelac Arizona

TestAmerica Phoenix

Water XE200.7

Water XEPA 300.0

Water XEPA 314.0

XWater XEPA 8260B

Water XM2320 B

Water XM4500-P B, E

Water XM5310B

WaterSM 4500-P B, E

Water XSM4500-NH3D

Nevada and NELAP provide analyte specific accreditations. Analyte specific information for TestAmerica may be obtained by contacting

the laboratory or visiting our website at www.testamericainc.com

Subcontracted Laboratories

Microseeps/Univ of Pittsburgh App Research Center

220 William Pitt Way - Pittsburgh, PA 15238

Analysis Performed: HydrogenSamples: PTA0778-03

TestAmerica - Irvine, CA NELAC Cert #01108CA, California Cert #1197, Arizona Cert #AZ0671, Nevada Cert #CA72-2002-63

17461 Derian Ave. Suite 100 - Irvine, CA 92614

Method Performed: EPA 300.1Samples: PTA0778-01

Project Manager

TestAmerica Phoenix

PTA0778

Kylie Emily



SENDING LABORATORY:

TestAmerica Phoenix 4625 East Cotton Center.Bivd. Ste 189 Phoenix, AZ. 85040 Phone: (602) 437-3340 Fax: (602) 454-9303 Project Manager: Kylie Emily Client: Environmental Resources Management Inc.-West

Analysis Units Due

SUBCONTRACT ORDER TestAmerica Phoenix

PTA0778 -:J TA r::r t l RECEIVING LABORATORY:

TestAmerica Irvine

17461 Derian Ave. Suite 100 Irvine, CA 92614 Phone :(949} 261-1022 Fax: {949} 261-1228 Projeyt Location: AZ. - ARIZONA Receipt Temperature: oc

Expires lnterlab Price Surch Comments

Ice: Y I N

Sample 10: PTA0778-01 (IRZ-IW-05-01182010- Water) Sampled: 01118110 12:35 Chlorate (300.1) mg/1 02/02/10 02/15/10 12:35 $30.00 0%

Chlorite (300 .1) - 0 · mg/1 02/02/10 02101/10 12:35 $30.00 0%

Containers Supplied: .

500 ml Poly w/EDA (L) 125ml Brown Poly w/ EDA (M)

0 .

'! I

~~-Released By

Released By Datemme

G/w Dl-lfJ-/D 17-:0V Received By ) Datemme a;;) ~C.

~V~w~b:;Leutfi= _ ___::,£t6~:w/o 11 ~t7o c:Y3,2 Received By 1Datemme Page 1 of 1

rest America CHAIN OF CUSTODY FORM

[ 1 Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 THE LEADER IN ENVIRONMENTAL TESTING [ 1 Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803

\ [ 1 Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 7~~"""-ef·n~·v,~"ft-..OC\A\f'Tt· vJ21~JT98-36'1H-----AL·DD13·5SD (12/08) 1 . .i\ :\1 1)'- / .....1:.. ~ .Page of

ClientName/Address: - ~v '.>~\;'t" t;'(~~/~O(V~~m./~rio:· .•. -c.OD r ~~.'~;[~Analysis Required ,) ~\ t=ft(Y\;· 1-'1]_1(._.1:::.. ~ ._ . . \ 'VIT V )('f\. lf}J' II..!... """" r' I-R~ ~'! C-<=,\ t-• (I". I

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-----------........,-S-am-p-:-le-r-C:-o-nt-ai-ne-r-t-#-o-f -.-S-a-m-pl~in-g ,-Sa_m_p_lin-g.,----. -1 fJ, ch~ c;-J · ~N \ Jo $)··· ..$ -? Sample Description Preservatives V ~ .> .>. ~

Matrix Type Cont. Date Time CJ (J \.L 2 Speciallnstructions

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0 Ld By: Date/Time: :~::r:~;d Time: (Check;2 hours---

Rpfinjui'she'd By: Date/Time: • y.eceived By: Date/Time: 24 hours 5 days

/ / 48 hours normal

Relinquished By: Date/Time: ( .:/Lab By: ihYJJ/(J r:ID~I J( ']_ ~::~le~egrity: (Che~nice 3 , SCJL-Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on t~is chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

Lab SamQie# P1001274-01

Client Name: Test America Contact: Kylie Emily Address: 4625 East Cotton Center Blvd.

Page: Page 1 of 3 Lab Proj #: P1001274

Report Date: 02/02/1 o Client Proj Name: PTA0778

Client Proj #: PT A0778 Suite 189 Phoenix, AZ.. 85040

Client Sample ID PTA0778-03

Laboratory Results ,;} Total pages in data package: -t-

Microseaps test results meet all the req ·1rements of the NELAC standards or provide reasons and/or justification if they do not.

Approved Bv:

Project Manager: Debbie Hallo

The analytical results reported here are reliable and usable to the precision expressed In this report. As required by some regulating authorities, a full discussion of the uncertainty in our analytical results can be obtained at our web site or through customer service. Unless otherwise specified, all results

are reported on a wet weight basis.

Case Narrative:

As a valued client we woufd appreciate your comments on our seNice. Please calf customer seNice at (412)826-5245 or email [email protected].

220 William Pitt Way • Pittsburgh, PA 15238 • Tel 412·826-5245 • Fax 412-826-3433

website www.microseeps.com email [email protected]


Suite 189 Phoenix, AZ 85040

Sam1:2le Descrigtion Matrix Lab Sample#


Report Date: 02/02/1 0 Client Proj Name: PT A0778

Client Proj #: PT A0778

SamQied Date/Time Received PTA0778-03 Vapor P1001274-01 18 Jan. 10 13:30 22 Jan. 10 15:27

Analyte(s) Flag Result PQL Units Method# Analysis Date By RiskAnalysis N Hydrogen 11.000 0.600 nM AM20GAX 2/1/10 sl

f~·~ Data Qualifiers: J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery!RPD poor for MS/MSD, SAMP/DUP, B- detected :fm8~ in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N- NELAC certified analysis

Client Name: Test America Contact: Kylie Emily

Address: 4625 East Cotton Center Blvd. Suite 189 Phoenix, AZ 85040

Prep Method:

Analysis Method:

M100201023~MB

Result n-ueSgikeConc. RDL

Hydrogen < 0.600 nM 0.600

M1 00201 023-LCS

Result TrueSeikeConc.

Hydrogen 10.000 nM 9.78

M1 00201 023-LCSD

Result TrueS]2ikeConc.



Report Date: 02/02/10 Client Proj Name: PT A0778


Hydrogen by Bubble Strip


%Recove!Y Ctl Limits

- NA


102.00 75-125

%Recove!Y Ctl Limits RPD

102.00 75-125 0.00

RPD Ctl Limits

0-20

1---------~~ Outlined Results indicate results outside of Control limits

Data Qualifiers; J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B- detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N- NELAC certified analysis

SENDING LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 189 Phoenix, AZ 85040 Phone: (602) 437~3340 Fax: (602} 454~9303 Project Manager: Kylie Emily


PTA0778

RECEIVING LABORATORY:


220 William Pitt Way Pittsburgh, PA 15238 Phone :(412)826-5245 Fax: (412}826-3433 Project Location: AZ- ARIZONA Receipt Temperature: oc Ice: Y I N

Standard TAT is requested un,Iess specific due date is requested. => Due Date: ---- Initials: __ _

Analysis Units Expires

Sample JD: PTA0778-03 (IRZ-IW-05-01182010 ·Water) Sampled: 0111811013:30

Hydrogen

Containers Supplied:

NA (A}

(tL ...

Released By

n~•-- ... ~..J r"' ••

% 02/15/1 0 13:30

{I ;),0 I I D [/:6\J r(j) &---

::::::~1\ Datemme

n ... L ... rr.--

Comments

Microseeps

n y A . Jt>vu '- ./ Paae 1 of 1


454-9303

LABORATORY REPORT





Received:

Issued:

01/19/10

01/19/10

01/27/10 15:53




report shall not be reproduced, except in full, without written permission from TestAmerica. The Chain of Custody, 1 page, is included and

is an integral part of this report.


Project: PGA North 103965.00


CASE NARRATIVE


PTA0845-01 IDW-Soil Soil


Sample recieved in a stainless sleeve.





N-1 = The Laboratory Control Sample / Laboratory Control Sample Duplicate and Matrix Spike / Matrix

Spike Duplicate recovered high and outside of acceptance limits for 2-Butanone. All associated samples

are non-detect for this compound and therefore are not impacted.

L3-Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above the

acceptance limits. Analyte not detected, data not impacted.


SUBCONTRACTED: No analyses were subcontracted to an outside laboratory.

Reviewed By:

Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily

<Page 1 of 15>


454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

VOLATILE ORGANICS BY GC/MS (EPA 5035/8260B)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0845-01 (IDW-Soil - Soil)

Reporting Units: ug/kg

1/23/20101/20/2010SW8260B1,1,1-Trichloroethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,1,2,2-Tetrachloroethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,1,2-Trichloroethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,1-Dichloroethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,1-Dichloroethene 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,1-Dichloropropene 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,2,3-Trichlorobenzene 10010A0547 0.994ND

1/23/20101/20/2010SW8260B1,2,3-Trichloropropane 10010A0547 0.994ND

1/23/20101/20/2010SW8260B1,2,4-Trimethylbenzene 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,2-Dibromoethane (EDB) 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,2-Dichlorobenzene 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,2-Dichloroethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,2-Dichloropropane 5010A0547 0.994ND

1/23/20101/20/2010SW8260B1,3,5-Trimethylbenzene 5010A0547 0.994ND





1/23/20101/20/2010SW8260B2-Butanone (MEK) 50010A0547 L30.994ND

1/23/20101/20/2010SW8260B2-Chlorotoluene 5010A0547 0.994ND

1/23/20101/20/2010SW8260B2-Hexanone 25010A0547 0.994ND

1/23/20101/20/2010SW8260B4-Chlorotoluene 5010A0547 0.994ND

1/23/20101/20/2010SW8260B4-Methyl-2-pentanone (MIBK) 25010A0547 0.994ND

1/23/20101/20/2010SW8260BAcetone 50010A0547 0.994ND

1/23/20101/20/2010SW8260BBenzene 5010A0547 0.994ND

1/23/20101/20/2010SW8260BBromobenzene 5010A0547 0.994ND

1/23/20101/20/2010SW8260BBromochloromethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260BBromodichloromethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260BBromoform 5010A0547 0.994ND

1/23/20101/20/2010SW8260BBromomethane 25010A0547 0.994ND

1/23/20101/20/2010SW8260BCarbon tetrachloride 5010A0547 0.994ND

1/23/20101/20/2010SW8260BChlorobenzene 5010A0547 0.994ND

1/23/20101/20/2010SW8260BChloroethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260BChloroform 5010A0547 0.994ND

1/23/20101/20/2010SW8260BChloromethane 25010A0547 0.994ND

1/23/20101/20/2010SW8260Bcis-1,2-Dichloroethene 5010A0547 0.994ND

1/23/20101/20/2010SW8260Bcis-1,3-Dichloropropene 5010A0547 0.994ND

1/23/20101/20/2010SW8260BDibromochloromethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260BDichlorodifluoromethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260BEthylbenzene 5010A0547 0.994ND

Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0845-01 (IDW-Soil - Soil) - cont.

Reporting Units: ug/kg

1/23/20101/20/2010SW8260Bm,p-Xylenes 10010A0547 0.994ND

1/23/20101/20/2010SW8260BMethyl-tert-butyl Ether (MTBE) 5010A0547 0.994ND

1/23/20101/20/2010SW8260BMethylene Chloride 10010A0547 0.994ND

1/23/20101/20/2010SW8260Bn-Butylbenzene 5010A0547 0.994ND

1/23/20101/20/2010SW8260Bn-Propylbenzene 5010A0547 0.994ND

1/23/20101/20/2010SW8260Bo-Xylene 5010A0547 0.994ND

1/23/20101/20/2010SW8260Bp-Isopropyltoluene 5010A0547 0.994ND

1/23/20101/20/2010SW8260Bsec-Butylbenzene 5010A0547 0.994ND

1/23/20101/20/2010SW8260BStyrene 5010A0547 0.994ND

1/23/20101/20/2010SW8260Btert-Butylbenzene 5010A0547 0.994ND

1/23/20101/20/2010SW8260BTetrachloroethene 5010A0547 0.994ND

1/23/20101/20/2010SW8260BToluene 5010A0547 0.994ND

1/23/20101/20/2010SW8260Btrans-1,2-Dichloroethene 5010A0547 0.994ND

1/23/20101/20/2010SW8260Btrans-1,3-Dichloropropene 5010A0547 0.994ND

1/23/20101/20/2010SW8260BTrichloroethene 5010A0547 0.994ND

1/23/20101/20/2010SW8260BTrichlorofluoromethane 5010A0547 0.994ND

1/23/20101/20/2010SW8260BVinyl Acetate 5010A0547 0.994ND

1/23/20101/20/2010SW8260BVinyl chloride 5010A0547 0.994ND




Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: IDW-Soil (PTA0845-01) - Soil

2 01/19/2010 16:07 01/19/2010 17:31 01/20/2010 12:58 01/23/2010 05:05SW8260B

Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1,1-Trichloroethane ug/kg50ND

1,1,2,2-Tetrachloroethane ug/kg50ND

1,1,2-Trichloroethane ug/kg50ND

1,1-Dichloroethane ug/kg50ND

1,1-Dichloroethene ug/kg50ND

1,1-Dichloropropene ug/kg50ND

1,2,3-Trichlorobenzene ug/kg100ND

1,2,3-Trichloropropane ug/kg100ND

1,2,4-Trimethylbenzene ug/kg50ND

1,2-Dibromoethane (EDB) ug/kg50ND

1,2-Dichlorobenzene ug/kg50ND

1,2-Dichloroethane ug/kg50ND

1,2-Dichloropropane ug/kg50ND

1,3,5-Trimethylbenzene ug/kg50ND





2-Butanone (MEK) ug/kg500ND

2-Chlorotoluene ug/kg50ND

2-Hexanone ug/kg250ND

4-Chlorotoluene ug/kg50ND

4-Methyl-2-pentanone (MIBK) ug/kg250ND

Acetone ug/kg500ND

Benzene ug/kg50ND

Bromobenzene ug/kg50ND

Bromochloromethane ug/kg50ND

Bromodichloromethane ug/kg50ND

Bromoform ug/kg50ND

Bromomethane ug/kg250ND

Carbon tetrachloride ug/kg50ND

Chlorobenzene ug/kg50ND

Chloroethane ug/kg50ND

Chloroform ug/kg50ND

Chloromethane ug/kg250ND

Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



cis-1,2-Dichloroethene ug/kg50ND

cis-1,3-Dichloropropene ug/kg50ND

Dibromochloromethane ug/kg50ND

Dichlorodifluoromethane ug/kg50ND

Ethylbenzene ug/kg50ND

m,p-Xylenes ug/kg100ND

Methyl-tert-butyl Ether (MTBE) ug/kg50ND

Methylene Chloride ug/kg100ND

n-Butylbenzene ug/kg50ND

n-Propylbenzene ug/kg50ND

o-Xylene ug/kg50ND

p-Isopropyltoluene ug/kg50ND

sec-Butylbenzene ug/kg50ND

Styrene ug/kg50ND

tert-Butylbenzene ug/kg50ND

Tetrachloroethene ug/kg50ND

Toluene ug/kg50ND

trans-1,2-Dichloroethene ug/kg50ND

trans-1,3-Dichloropropene ug/kg50ND

Trichloroethene ug/kg50ND

Trichlorofluoromethane ug/kg50ND

Vinyl Acetate ug/kg50ND

Vinyl chloride ug/kg50ND

1250 60-130Surrogate: Dibromofluoromethane ug/kg1430 114

1250 65-125Surrogate: Toluene-d8 ug/kg1250 100

1250 65-125Surrogate: 4-Bromofluorobenzene ug/kg1330 107

LCS Analyzed: 01/22/2010 (10A0547-BS1)

1,1,1-Trichloroethane 1250 75-120ug/kg501270 102

1,1,2,2-Tetrachloroethane 1250 60-125ug/kg501280 102

1,1,2-Trichloroethane 1250 65-125ug/kg501250 100

1,1-Dichloroethane 1250 70-125ug/kg501350 108

1,1-Dichloroethene 1250 50-135ug/kg501390 111

1,1-Dichloropropene 1250 75-120ug/kg501190 95

1,2,3-Trichlorobenzene 1250 55-140ug/kg1001350 108

1,2,3-Trichloropropane 1250 60-130ug/kg1001330 107

Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/22/2010 (10A0547-BS1)

1,2,4-Trimethylbenzene 1250 75-120ug/kg501220 97

1,2-Dibromoethane (EDB) 1250 70-120ug/kg501230 99

1,2-Dichlorobenzene 1250 80-120ug/kg501240 99

1,2-Dichloroethane 1250 70-130ug/kg501410 113

1,2-Dichloropropane 1250 80-120ug/kg501270 101

1,3,5-Trimethylbenzene 1250 80-130ug/kg501210 97





2-Butanone (MEK) 1250 40-150ug/kg5002030 L3162

2-Chlorotoluene 1250 80-120ug/kg501170 94

2-Hexanone 1250 20-150ug/kg2501260 100

4-Chlorotoluene 1250 80-120ug/kg501240 99

4-Methyl-2-pentanone (MIBK) 1250 50-130ug/kg2501400 112

Acetone 1250 10-150ug/kg5001810 145

Benzene 1250 75-120ug/kg501230 99

Bromobenzene 1250 80-120ug/kg501240 99

Bromochloromethane 1250 75-125ug/kg501390 111

Bromodichloromethane 1250 75-120ug/kg501220 98

Bromoform 1250 60-120ug/kg501230 98

Bromomethane 1250 20-140ug/kg2501140 91

Carbon tetrachloride 1250 70-130ug/kg501180 95

Chlorobenzene 1250 80-120ug/kg501230 98

Chloroethane 1250 10-130ug/kg501140 91

Chloroform 1250 75-120ug/kg501360 108

Chloromethane 1250 25-140ug/kg2501020 81

cis-1,2-Dichloroethene 1250 70-125ug/kg501220 98

cis-1,3-Dichloropropene 1250 75-125ug/kg501320 105

Dibromochloromethane 1250 75-120ug/kg501230 99

Dichlorodifluoromethane 1250 10-150ug/kg50699 56

Ethylbenzene 1250 80-120ug/kg501180 95

m,p-Xylenes 1250 60-140ug/kg1001230 98

Methyl-tert-butyl Ether (MTBE) 1250 65-130ug/kg501420 113

Methylene Chloride 1250 65-125ug/kg1001380 110

Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/22/2010 (10A0547-BS1)

n-Butylbenzene 1250 65-130ug/kg501200 96

n-Propylbenzene 1250 75-130ug/kg501220 97

o-Xylene 1250 80-120ug/kg501190 95

p-Isopropyltoluene 1250 75-130ug/kg501200 96

sec-Butylbenzene 1250 75-125ug/kg501160 93

Styrene 1250 80-120ug/kg501230 99

tert-Butylbenzene 1250 80-120ug/kg501140 91

Tetrachloroethene 1250 70-130ug/kg501160 93

Toluene 1250 75-120ug/kg501210 97

trans-1,2-Dichloroethene 1250 70-130ug/kg501420 114

trans-1,3-Dichloropropene 1250 65-130ug/kg501340 107

Trichloroethene 1250 80-120ug/kg501240 99

Trichlorofluoromethane 1250 50-150ug/kg501120 89

Vinyl Acetate 1250 35-150ug/kg501320 105

Vinyl chloride 1250 10-150ug/kg50552 44





1,1,1-Trichloroethane 1250 1575-120ug/kg501270 102 0

1,1,2,2-Tetrachloroethane 1250 3060-125ug/kg501280 102 0

1,1,2-Trichloroethane 1250 3065-125ug/kg501240 99 1

1,1-Dichloroethane 1250 2070-125ug/kg501360 108 1

1,1-Dichloroethene 1250 2050-135ug/kg501400 112 1

1,1-Dichloropropene 1250 1575-120ug/kg501130 90 5

1,2,3-Trichlorobenzene 1250 2555-140ug/kg1001330 107 1

1,2,3-Trichloropropane 1250 3060-130ug/kg1001270 102 5

1,2,4-Trimethylbenzene 1250 1575-120ug/kg501220 97 0

1,2-Dibromoethane (EDB) 1250 2070-120ug/kg501220 98 1

1,2-Dichlorobenzene 1250 2080-120ug/kg501240 99 0

1,2-Dichloroethane 1250 2070-130ug/kg501410 113 0

1,2-Dichloropropane 1250 2080-120ug/kg501280 102 1

1,3,5-Trimethylbenzene 1250 1580-130ug/kg501220 97 1



Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers





2-Butanone (MEK) 1250 3540-150ug/kg5001940 L3155 4

2-Chlorotoluene 1250 1580-120ug/kg501170 94 0

2-Hexanone 1250 3520-150ug/kg2501220 97 3

4-Chlorotoluene 1250 1580-120ug/kg501200 96 4

4-Methyl-2-pentanone (MIBK) 1250 3550-130ug/kg2501390 111 1

Acetone 1250 3510-150ug/kg5001460 117 21

Benzene 1250 1575-120ug/kg501240 99 0

Bromobenzene 1250 2080-120ug/kg501230 98 1

Bromochloromethane 1250 2075-125ug/kg501420 113 2

Bromodichloromethane 1250 1575-120ug/kg501240 99 1

Bromoform 1250 2560-120ug/kg501190 95 3

Bromomethane 1250 3520-140ug/kg2501180 95 4

Carbon tetrachloride 1250 2070-130ug/kg501180 94 0

Chlorobenzene 1250 1580-120ug/kg501200 96 2

Chloroethane 1250 3010-130ug/kg501130 91 1

Chloroform 1250 2075-120ug/kg501400 112 3

Chloromethane 1250 3525-140ug/kg2501020 82 1

cis-1,2-Dichloroethene 1250 1570-125ug/kg501250 100 3

cis-1,3-Dichloropropene 1250 1575-125ug/kg501320 105 0

Dibromochloromethane 1250 2075-120ug/kg501240 99 0

Dichlorodifluoromethane 1250 3510-150ug/kg50688 55 2

Ethylbenzene 1250 1580-120ug/kg501180 94 0

m,p-Xylenes 1250 1560-140ug/kg1001180 94 4

Methyl-tert-butyl Ether (MTBE) 1250 2065-130ug/kg501460 117 3

Methylene Chloride 1250 2065-125ug/kg1001390 111 1

n-Butylbenzene 1250 2065-130ug/kg501200 96 1

n-Propylbenzene 1250 1575-130ug/kg501210 97 1

o-Xylene 1250 1580-120ug/kg501190 95 0

p-Isopropyltoluene 1250 1575-130ug/kg501180 95 1

sec-Butylbenzene 1250 1575-125ug/kg501130 90 3

Styrene 1250 1580-120ug/kg501190 95 3

tert-Butylbenzene 1250 1580-120ug/kg501130 90 1

Tetrachloroethene 1250 1570-130ug/kg501160 92 0

Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Toluene 1250 1575-120ug/kg501230 98 1

trans-1,2-Dichloroethene 1250 2070-130ug/kg501410 112 1

trans-1,3-Dichloropropene 1250 2065-130ug/kg501310 105 2

Trichloroethene 1250 1580-120ug/kg501210 96 3

Trichlorofluoromethane 1250 2550-150ug/kg501110 89 1

Vinyl Acetate 1250 3535-150ug/kg501350 108 2

Vinyl chloride 1250 3510-150ug/kg50544 43 2





1,1,1-Trichloroethane 1240 50-125ug/kg501160 ND 94

1,1,2,2-Tetrachloroethane 1240 50-130ug/kg501130 ND 91

1,1,2-Trichloroethane 1240 55-120ug/kg501140 ND 92

1,1-Dichloroethane 1240 55-125ug/kg501220 ND 98

1,1-Dichloroethene 1240 25-140ug/kg501230 ND 99

1,1-Dichloropropene 1240 55-125ug/kg501080 ND 87

1,2,3-Trichlorobenzene 1240 35-140ug/kg1001230 54.4 95

1,2,3-Trichloropropane 1240 35-140ug/kg1001140 ND 92

1,2,4-Trimethylbenzene 1240 50-130ug/kg501130 ND 91

1,2-Dibromoethane (EDB) 1240 55-120ug/kg501100 ND 89

1,2-Dichlorobenzene 1240 60-120ug/kg501150 ND 92

1,2-Dichloroethane 1240 55-130ug/kg501270 ND 102

1,2-Dichloropropane 1240 60-120ug/kg501160 ND 94

1,3,5-Trimethylbenzene 1240 45-135ug/kg501130 ND 91





2-Butanone (MEK) 1240 40-150ug/kg5002010 N1ND 162

2-Chlorotoluene 1240 60-120ug/kg501100 ND 89

2-Hexanone 1240 20-150ug/kg2501250 ND 101

4-Chlorotoluene 1240 55-130ug/kg501140 ND 92

4-Methyl-2-pentanone (MIBK) 1240 40-130ug/kg2501280 ND 103

Acetone 1240 10-150ug/kg5001960 M1ND 158

Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Benzene 1240 55-120ug/kg501140 ND 92

Bromobenzene 1240 60-125ug/kg501120 ND 90

Bromochloromethane 1240 50-135ug/kg501230 ND 99

Bromodichloromethane 1240 60-120ug/kg501140 ND 92

Bromoform 1240 40-125ug/kg501100 ND 88

Bromomethane 1240 10-140ug/kg2501030 10.5 82

Carbon tetrachloride 1240 40-135ug/kg501120 ND 90

Chlorobenzene 1240 65-120ug/kg501120 ND 91

Chloroethane 1240 10-140ug/kg501010 ND 81

Chloroform 1240 60-125ug/kg501230 ND 99

Chloromethane 1240 10-140ug/kg250881 ND 71

cis-1,2-Dichloroethene 1240 55-125ug/kg501120 ND 91

cis-1,3-Dichloropropene 1240 55-120ug/kg501190 ND 96

Dibromochloromethane 1240 55-125ug/kg501120 ND 90

Dichlorodifluoromethane 1240 10-150ug/kg50575 ND 46

Ethylbenzene 1240 60-125ug/kg501110 ND 90

m,p-Xylenes 1240 55-125ug/kg1001130 ND 91

Methyl-tert-butyl Ether (MTBE) 1240 50-130ug/kg501260 ND 101

Methylene Chloride 1240 50-120ug/kg1001240 ND 100

n-Butylbenzene 1240 40-135ug/kg501150 22.5 91

n-Propylbenzene 1240 55-130ug/kg501150 ND 93

o-Xylene 1240 60-125ug/kg501120 ND 90

p-Isopropyltoluene 1240 45-135ug/kg501140 ND 92

sec-Butylbenzene 1240 50-130ug/kg501100 ND 89

Styrene 1240 55-125ug/kg501150 ND 93

tert-Butylbenzene 1240 55-125ug/kg501090 ND 88

Tetrachloroethene 1240 60-130ug/kg501120 ND 90

Toluene 1240 55-125ug/kg501100 ND 89

trans-1,2-Dichloroethene 1240 50-130ug/kg501250 ND 101

trans-1,3-Dichloropropene 1240 55-125ug/kg501200 ND 96

Trichloroethene 1240 40-145ug/kg501190 ND 96

Trichlorofluoromethane 1240 20-150ug/kg50987 ND 80

Vinyl Acetate 1240 10-150ug/kg50707 ND 57

Vinyl chloride 1240 10-150ug/kg50517 ND 42


Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers






1,1,1-Trichloroethane 1250 1550-125ug/kg501180 ND 95 2

1,1,2,2-Tetrachloroethane 1250 2550-130ug/kg501170 ND 94 3

1,1,2-Trichloroethane 1250 2555-120ug/kg501210 ND 97 6

1,1-Dichloroethane 1250 2555-125ug/kg501230 ND 98 1

1,1-Dichloroethene 1250 3525-140ug/kg501270 ND 101 3

1,1-Dichloropropene 1250 2555-125ug/kg501080 ND 87 0

1,2,3-Trichlorobenzene 1250 3035-140ug/kg1001310 54.4 100 6

1,2,3-Trichloropropane 1250 3535-140ug/kg1001210 ND 97 6

1,2,4-Trimethylbenzene 1250 2050-130ug/kg501150 ND 92 2

1,2-Dibromoethane (EDB) 1250 2555-120ug/kg501180 ND 94 7

1,2-Dichlorobenzene 1250 2560-120ug/kg501200 ND 96 5

1,2-Dichloroethane 1250 2555-130ug/kg501300 ND 104 3

1,2-Dichloropropane 1250 2560-120ug/kg501180 ND 94 2

1,3,5-Trimethylbenzene 1250 2045-135ug/kg501160 ND 93 2





2-Butanone (MEK) 1250 3540-150ug/kg5002110 N1ND 168 4

2-Chlorotoluene 1250 2060-120ug/kg501100 ND 88 0

2-Hexanone 1250 3520-150ug/kg2501280 ND 102 2

4-Chlorotoluene 1250 2055-130ug/kg501170 ND 93 2

4-Methyl-2-pentanone (MIBK) 1250 3040-130ug/kg2501400 ND 112 9

Acetone 1250 3510-150ug/kg5001900 M1ND 152 3

Benzene 1250 2555-120ug/kg501140 ND 92 0

Bromobenzene 1250 2560-125ug/kg501140 ND 91 2

Bromochloromethane 1250 3050-135ug/kg501280 ND 102 4

Bromodichloromethane 1250 2060-120ug/kg501180 ND 94 3

Bromoform 1250 3540-125ug/kg501150 ND 92 5

Bromomethane 1250 3510-140ug/kg2501040 10.5 82 1

Carbon tetrachloride 1250 3040-135ug/kg501100 ND 88 2

Chlorobenzene 1250 2065-120ug/kg501170 ND 94 4

Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chloroethane 1250 3510-140ug/kg50975 ND 78 4

Chloroform 1250 2560-125ug/kg501250 ND 100 2

Chloromethane 1250 3510-140ug/kg250872 ND 70 1

cis-1,2-Dichloroethene 1250 2555-125ug/kg501120 ND 90 0

cis-1,3-Dichloropropene 1250 2055-120ug/kg501220 ND 98 3

Dibromochloromethane 1250 3055-125ug/kg501190 ND 95 6

Dichlorodifluoromethane 1250 3510-150ug/kg50510 ND 41 12

Ethylbenzene 1250 2060-125ug/kg501140 ND 91 2

m,p-Xylenes 1250 2055-125ug/kg1001170 ND 94 4

Methyl-tert-butyl Ether (MTBE) 1250 3550-130ug/kg501320 ND 105 5

Methylene Chloride 1250 3050-120ug/kg1001270 ND 102 2

n-Butylbenzene 1250 2540-135ug/kg501150 22.5 90 0

n-Propylbenzene 1250 2055-130ug/kg501150 ND 92 0

o-Xylene 1250 3060-125ug/kg501160 ND 93 4

p-Isopropyltoluene 1250 2545-135ug/kg501150 ND 92 1

sec-Butylbenzene 1250 2050-130ug/kg501110 ND 89 1

Styrene 1250 2055-125ug/kg501190 ND 95 3

tert-Butylbenzene 1250 2555-125ug/kg501110 ND 89 2

Tetrachloroethene 1250 2060-130ug/kg501130 ND 90 1

Toluene 1250 3555-125ug/kg501170 ND 94 6

trans-1,2-Dichloroethene 1250 2550-130ug/kg501320 ND 105 5

trans-1,3-Dichloropropene 1250 2555-125ug/kg501240 ND 99 3

Trichloroethene 1250 3540-145ug/kg501190 ND 95 1

Trichlorofluoromethane 1250 3520-150ug/kg50972 ND 78 1

Vinyl Acetate 1250 3510-150ug/kg50832 ND 67 16

Vinyl chloride 1250 3510-150ug/kg50516 ND 41 0




Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00


L3 The associated blank spike recovery was above method acceptance limits.





Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0845

PGA North 103965.00



TestAmerica Phoenix

Soil XSW8260B



Project Manager

TestAmerica Phoenix

PTA0845

Kylie Emily



Test America THE LEADER IN ENVIRONMENTAL TESTING

TAL-0013-550 (12/08)

Project Manager:\)v__ .... .\A G"' G-1\.. ..j

Sampler::S, \-h \\Le,.-. / '11 Sc.huJ/1 d.er-Sample Container

'-----

CHAIN OF CUSTODY FORM

[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602} 437-3340 FAX (602} 454-9303 [ ) Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520} 807-3801 FAX (520) 807-3803 [ ) Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Proje~t/P.ONumber: · P(oA--~ (IJO . .

103~~£10°

Analysis Required

Phol)!il Number: 4o-O ~q't9- 'Z.4o I

Fax Num~e~ __ q-o,~ ~7_\0~

Page l 0 I

Sample Description Matrix Type # of Sampling Sampling Preservatives

Cont. Date Time Special Instructions

.:r:::Dw - So ~ I

/7171 Received By:

()l'!f ) Date/Time: Turnaround Time: (Check)

same day 72 hours

/1~ist ed By: Date/Time: Date/Time: 24 hours 5 days

48 hours normal

lt/T~r; )f) ) 1 ~ ,j-r Sample Integrity: (Check)

intact o'---. on ice do... ~linquished By: Date/Time: / Received in Lab B() ~

""~ late: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. 'ayment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days. }

0 d_Cac.

·I


454-9303

LABORATORY REPORT





Received:

Issued:

01/19/10

01/19/10

02/05/10 14:51









CASE NARRATIVE


PTA0848-01 IRZ-MW-B-01192010 Water

PTA0848-02 IRZ-MW-B-01192010 Water

PTA0848-03 IRW-IW-03-01192010 Water

PTA0848-04 IRW-IW-03-01192010 Water

PTA0848-05 IRZ-MW-C-01192010 Water

PTA0848-06 IRZ-MW-C-01192010 Water

PTA0848-07 IRZ-MW-D-01192010 Water

PTA0848-08 IRZ-MW-D-01192010 Water

PTA0848-09 IRZ-MW-D-011910-R Water

PTA0848-10 Trip Blank (Cooler1) Water

PTA0848-11 Trip Blank (Cooler2) Water

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily

<Page 1 of 81>


454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

SAMPLE RECEIPT: Samples were received intact, at 1°C and 3°C, on ice and with chain of custody documentation.



PRESERVATION: Samples requiring preservation were verified prior to sample analysis. Results were qualified where the

sample container did not meet the method preservation requirements.


N1a-PTA0848-10 and PTA0848-11 Carbon Disulfide-There was lab contamination and the samples were

re-analyzed for conformation. Due to both samples being Trip blanks the re-anaysis was done with

headspace. Both the original and re-analysis are reported.

N1a-300.0-Results exceeded the linear range in the MS/MSD and therefore are not available for reporting.

The batch was accepted based on acceptable recovery in the Blank Spike (LCS).

N1a-Batch 10A0559-MS1/MSD1- Due to an oversight, the Matrix Spike and Matrix Spike Duplicate were

analyzed outside of the 12-hour analytical clock (3 minutes and 34 mintues respectively). The data has

been provided for informational purposes. The Laboratory Control Sample / Laboratory Control Sample

Duplicate provide acceptable precision and accuracy data for the batch.

N1a-Batch 10A0646-MSD1-The Laboratory Control Sample / Laboratory Control Sample Duplicate and

Matrix Spike Duplicate recovered high and outside of acceptance limits for 1,3-Dichlorobenzene. All

associated samples are non-detect for this compound and therefore are not impacted.




S10-Surrogate recovery was above acceptance limits.



Reviewed By:

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-01RE1 (IRZ-MW-B-01192010 - Water)


1/22/20101/22/2010EPA 8260BAcetone 1010A0646 1ND

1/22/20101/22/2010EPA 8260BBenzene 0.5010A0646 1ND























1/22/20101/22/2010EPA 8260B1,3-Dichlorobenzene 0.5010A0646 L31ND
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-01RE1 (IRZ-MW-B-01192010 - Water) - cont.











1/22/20101/22/2010EPA 8260BStyrene 0.5010A0646 1ND




1/22/20101/22/2010EPA 8260BToluene 0.5010A0646 1ND
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-03 (IRW-IW-03-01192010 - Water)


1/20/20101/20/2010EPA 8260BAcetone 1010A0559 1ND

Benzene 1/20/20101/20/201010A0559 0.50 1EPA 8260B 0.66










Carbon disulfide 1/20/20101/20/201010A0559 0.50 1EPA 8260B 0.77




Chloroform 1/20/20101/20/201010A0559 0.50 1EPA 8260B 1.6

























Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-03 (IRW-IW-03-01192010 - Water) - cont.











1/20/20101/20/2010EPA 8260BStyrene 0.5010A0559 1ND



Tetrachloroethene 1/20/20101/20/201010A0559 0.50 1EPA 8260B 2.3

1/20/20101/20/2010EPA 8260BToluene 0.5010A0559 1ND















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-03RE1 (IRW-IW-03-01192010 - Water) - cont.


Trichloroethene 1/21/20101/21/201010A0618 50 100EPA 8260B 5100




Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-05 (IRZ-MW-C-01192010 - Water)


1/20/20101/20/2010EPA 8260BAcetone 1010A0559 1ND

1/20/20101/20/2010EPA 8260BBenzene 0.5010A0559 1ND







































Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-05 (IRZ-MW-C-01192010 - Water) - cont.











1/20/20101/20/2010EPA 8260BStyrene 0.5010A0559 1ND




1/20/20101/20/2010EPA 8260BToluene 0.5010A0559 1ND















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-05RE1 (IRZ-MW-C-01192010 - Water) - cont.






Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-07 (IRZ-MW-D-01192010 - Water)


1/20/20101/20/2010EPA 8260BAcetone 1010A0559 1ND

1/20/20101/20/2010EPA 8260BBenzene 0.5010A0559 1ND




























1,1-Dichloroethene 1/20/20101/20/201010A0559 0.50 1EPA 8260B 0.82











Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-07 (IRZ-MW-D-01192010 - Water) - cont.











1/20/20101/20/2010EPA 8260BStyrene 0.5010A0559 1ND




1/20/20101/20/2010EPA 8260BToluene 0.5010A0559 1ND















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-07RE1 (IRZ-MW-D-01192010 - Water) - cont.






Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-09 (IRZ-MW-D-011910-R - Water)


1/21/20101/21/2010EPA 8260BAcetone 1010A0618 1ND

1/21/20101/21/2010EPA 8260BBenzene 0.5010A0618 1ND







































Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-09 (IRZ-MW-D-011910-R - Water) - cont.











1/21/20101/21/2010EPA 8260BStyrene 0.5010A0618 1ND




1/21/20101/21/2010EPA 8260BToluene 0.5010A0618 1ND
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-10 (Trip Blank (Cooler1) - Water)


1/20/20101/20/2010EPA 8260BAcetone 1010A0559 1ND

1/20/20101/20/2010EPA 8260BBenzene 0.5010A0559 1ND







































Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-10 (Trip Blank (Cooler1) - Water) - cont.











1/20/20101/20/2010EPA 8260BStyrene 0.5010A0559 1ND




1/20/20101/20/2010EPA 8260BToluene 0.5010A0559 1ND
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-10RE1 (Trip Blank (Cooler1) - Water) - cont. Q2






Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-11 (Trip Blank (Cooler2) - Water)


1/20/20101/20/2010EPA 8260BAcetone 1010A0559 1ND

1/20/20101/20/2010EPA 8260BBenzene 0.5010A0559 1ND







































Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-11 (Trip Blank (Cooler2) - Water) - cont.











1/20/20101/20/2010EPA 8260BStyrene 0.5010A0559 1ND




1/20/20101/20/2010EPA 8260BToluene 0.5010A0559 1ND
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-11RE1 (Trip Blank (Cooler2) - Water) - cont. Q2






Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0848-01 (IRZ-MW-B-01192010 - Water)


Boron 1/21/20101/20/201010A0569 0.20 1E200.7 2.7

Calcium 1/21/20101/20/201010A0569 2.0 1E200.7 230

1/21/20101/20/2010E200.7Iron 0.05010A0569 1ND

Magnesium 1/21/20101/20/201010A0569 2.0 1E200.7 84

1/21/20101/20/2010E200.7Manganese 0.01010A0569 1ND

Sodium 1/21/20101/20/201010A0569 2.0 1E200.7 520



Boron 1/21/20101/20/201010A0569 0.20 1E200.7 3.2

Calcium 1/21/20101/20/201010A0569 2.0 1E200.7 380

Iron 1/21/20101/20/201010A0569 0.050 1E200.7 68

Magnesium 1/21/20101/20/201010A0569 2.0 1E200.7 130

Manganese 1/21/20101/20/201010A0569 0.010 1E200.7 0.49

Sodium 1/21/20101/20/201010A0569 2.0 1E200.7 470



Boron 1/21/20101/20/201010A0569 0.20 1E200.7 3.5

Calcium 1/21/20101/20/201010A0569 2.0 1E200.7 290

Iron 1/21/20101/20/201010A0569 0.050 1E200.7 130

Magnesium 1/21/20101/20/201010A0569 2.0 1E200.7 100

Manganese 1/21/20101/20/201010A0569 0.010 1E200.7 0.31

Sodium 1/21/20101/20/201010A0569 2.0 1E200.7 490



Boron 1/21/20101/20/201010A0569 0.20 1E200.7 3.3

Calcium 1/21/20101/20/201010A0569 2.0 M31E200.7 280

Iron 1/21/20101/20/201010A0569 0.050 1E200.7 1.9

Magnesium 1/21/20101/20/201010A0569 2.0 M11E200.7 100

Manganese 1/21/20101/20/201010A0569 0.010 1E200.7 0.014

Sodium 1/21/20101/20/201010A0569 2.0 M31E200.7 490

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

DISSOLVED METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



1/22/20101/21/2010E200.7Iron 0.05010A0620 1ND



Iron 1/22/20101/21/201010A0620 0.050 1E200.7 1.8



1/22/20101/21/2010E200.7Iron 0.05010A0620 1ND



1/22/20101/21/2010E200.7Iron 0.05010A0620 1ND

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result








Nitrate-N 1/20/20101/20/201010A0584 1.0 5EPA 300.0 20

1/22/20101/22/2010SM 4500-P B, EPhosphate 0.3010A0639 1ND

1/21/20101/20/2010M4500-P B, EPhosphorus,Total - P 0.1010A0562 1ND




Perchlorate 1/21/20101/21/201010A0602 2.0 1EPA 314.0 4.4

Sample ID: PTA0848-01RE1 (IRZ-MW-B-01192010 - Water)


Chloride 1/22/20101/22/201010A0648 40 20EPA 300.0 740

Sulfate 1/22/20101/22/201010A0648 40 20EPA 300.0 950




Ammonia-N 1/21/20101/21/201010A0616 0.50 1SM4500-NH3D 1.2




Nitrate-N 1/20/20101/20/201010A0584 1.0 5EPA 300.0 20

Phosphate 1/22/20101/22/201010A0639 0.30 1SM 4500-P B, E 3.1

Phosphorus,Total - P 1/21/20101/20/201010A0562 1.0 D110M4500-P B, E 1.0




Perchlorate 1/21/20101/21/201010A0602 4.0 D12EPA 314.0 20

Sample ID: PTA0848-03RE1 (IRW-IW-03-01192010 - Water)


Chloride 1/22/20101/22/201010A0648 40 20EPA 300.0 820

Sulfate 1/22/20101/22/201010A0648 40 20EPA 300.0 1100

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result




Ammonia-N 1/21/20101/21/201010A0616 0.50 1SM4500-NH3D 0.65




Nitrate-N 1/20/20101/20/201010A0584 1.0 5EPA 300.0 21

Phosphate 1/22/20101/22/201010A0639 0.30 1SM 4500-P B, E 1.9

Phosphorus,Total - P 1/21/20101/20/201010A0562 0.10 1M4500-P B, E 0.61





Sample ID: PTA0848-05RE1 (IRZ-MW-C-01192010 - Water)


Chloride 1/22/20101/22/201010A0648 40 20EPA 300.0 750

Sulfate 1/22/20101/22/201010A0648 40 20EPA 300.0 980




Ammonia-N 1/21/20101/21/201010A0616 0.50 1SM4500-NH3D 1.0




Nitrate-N 1/20/20101/20/201010A0584 1.0 5EPA 300.0 20

1/22/20101/22/2010SM 4500-P B, EPhosphate 0.3010A0639 1ND






Sample ID: PTA0848-07RE1 (IRZ-MW-D-01192010 - Water)


Chloride 1/22/20101/22/201010A0648 40 20EPA 300.0 750

Sulfate 1/22/20101/22/201010A0648 40 20EPA 300.0 990

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



1/26/20101/26/2010M5310BTotal Organic Carbon 1.010A0725 1ND










Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



Chlorate 1/29/20101/29/201010A2918 40 2EPA 300.1 85






Chlorate 1/29/20101/29/201010A2918 40 2EPA 300.1 100






Chlorate 1/29/20101/29/201010A2918 40 2EPA 300.1 89






Chlorate 1/29/20101/29/201010A2918 40 2EPA 300.1 90




Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: IRZ-MW-B-01192010 (PTA0848-01) - Water

2 01/19/2010 08:34 01/19/2010 17:31 01/20/2010 09:00 01/20/2010 10:57EPA 300.0

Sample ID: IRW-IW-03-01192010 (PTA0848-03) - Water

2 01/19/2010 10:23 01/19/2010 17:31 01/20/2010 09:00 01/20/2010 11:15EPA 300.0

Sample ID: IRZ-MW-C-01192010 (PTA0848-05) - Water

2 01/19/2010 13:09 01/19/2010 17:31 01/20/2010 09:00 01/20/2010 11:33EPA 300.0

Sample ID: IRZ-MW-D-01192010 (PTA0848-07) - Water

2 01/19/2010 14:48 01/19/2010 17:31 01/20/2010 09:00 01/20/2010 11:52EPA 300.0

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/20/2010 (10A0559-BS1)

Acetone 25.0 10-150ug/l1031.7 127

Benzene 25.0 80-120ug/l0.5026.0 104




Bromoform 25.0 75-130ug/l1.024.8 99


2-Butanone (MEK) 25.0 40-150ug/l2.529.9 119








Chloroform 25.0 75-120ug/l0.5025.4 101




















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/20/2010 (10A0559-BS1)






2-Hexanone 25.0 20-150ug/l2.529.3 117

Iodomethane 25.0 80-130ug/l2.524.8 99






Naphthalene 25.0 40-150ug/l2.527.5 110


Styrene 25.0 80-120ug/l0.5026.2 105




Toluene 25.0 80-120ug/l0.5025.3 101
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1033.1 133 4

Benzene 25.0 1580-120ug/l0.5025.7 103 2




Bromoform 25.0 2075-130ug/l1.026.4 106 6


2-Butanone (MEK) 25.0 3540-150ug/l2.533.2 133 10








Chloroform 25.0 1575-120ug/l0.5024.8 99 2




















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3520-150ug/l2.531.4 126 7

Iodomethane 25.0 1080-130ug/l2.524.6 98 1






Naphthalene 25.0 3040-150ug/l2.530.1 121 9


Styrene 25.0 1580-120ug/l0.5025.8 103 2




Toluene 25.0 1580-120ug/l0.5024.8 99 2
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 01/21/2010 (10A0559-MS1) Source: PTA0847-01 N1a

Acetone 25.0 10-150ug/l1022.5 ND 90

Benzene 25.0 70-125ug/l0.5025.9 ND 104




Bromoform 25.0 65-125ug/l1.024.8 ND 99






























Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 01/21/2010 (10A0559-MS1) Source: PTA0847-01 N1a






2-Hexanone 25.0 20-150ug/l2.523.8 ND 95









Styrene 25.0 55-135ug/l0.5025.0 ND 100




Toluene 25.0 70-125ug/l0.5024.2 ND 97
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 01/21/2010 (10A0559-MSD1) Source: PTA0847-01 N1a

Acetone 25.0 3510-150ug/l1025.2 ND 101 12

Benzene 25.0 2570-125ug/l0.5025.2 ND 101 3




Bromoform 25.0 2565-125ug/l1.024.8 ND 99 0






























Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 01/21/2010 (10A0559-MSD1) Source: PTA0847-01 N1a






2-Hexanone 25.0 3020-150ug/l2.524.5 ND 98 3









Styrene 25.0 3555-135ug/l0.5024.5 ND 98 2




Toluene 25.0 2070-125ug/l0.5024.1 ND 96 1
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/21/2010 (10A0618-BS1)

Acetone 25.0 10-150ug/l1031.5 126

Benzene 25.0 80-120ug/l0.5024.4 98




Bromoform 25.0 75-130ug/l1.024.2 97


2-Butanone (MEK) 25.0 40-150ug/l2.532.6 130








Chloroform 25.0 75-120ug/l0.5023.3 93




















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/21/2010 (10A0618-BS1)






2-Hexanone 25.0 20-150ug/l2.530.0 120

Iodomethane 25.0 80-130ug/l2.524.1 96






Naphthalene 25.0 40-150ug/l2.528.5 114


Styrene 25.0 80-120ug/l0.5024.0 96




Toluene 25.0 80-120ug/l0.5023.2 93
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1020.7 R683 41

Benzene 25.0 1580-120ug/l0.5024.1 96 1




Bromoform 25.0 2075-130ug/l1.022.2 89 9


2-Butanone (MEK) 25.0 3540-150ug/l2.524.0 96 31








Chloroform 25.0 1575-120ug/l0.5023.4 94 0




















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3520-150ug/l2.523.3 93 25

Iodomethane 25.0 1080-130ug/l2.524.6 98 2






Naphthalene 25.0 3040-150ug/l2.526.1 104 9


Styrene 25.0 1580-120ug/l0.5023.3 93 3




Toluene 25.0 1580-120ug/l0.5023.3 93 0
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1018.2 ND 73

Benzene 25.0 70-125ug/l0.5025.3 ND 101




Bromoform 25.0 65-125ug/l1.023.7 ND 95






























Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.523.0 ND 92









Styrene 25.0 55-135ug/l0.5019.6 ND 78




Toluene 25.0 70-125ug/l0.5024.0 ND 96
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1016.8 ND 67 8

Benzene 25.0 2570-125ug/l0.5023.2 ND 93 8




Bromoform 25.0 2565-125ug/l1.022.8 ND 91 4






























Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3020-150ug/l2.523.8 ND 95 4









Styrene 25.0 3555-135ug/l0.5017.5 ND 70 11




Toluene 25.0 2070-125ug/l0.5022.0 ND 88 9
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/22/2010 (10A0646-BS1)

Acetone 25.0 10-150ug/l1032.8 131

Benzene 25.0 80-120ug/l0.5025.3 101




Bromoform 25.0 75-130ug/l1.024.8 99


2-Butanone (MEK) 25.0 40-150ug/l2.533.0 132








Chloroform 25.0 75-120ug/l0.5024.1 96









1,3-Dichlorobenzene 25.0 80-120ug/l0.5030.5 L3122











Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/22/2010 (10A0646-BS1)






2-Hexanone 25.0 20-150ug/l2.530.8 123

Iodomethane 25.0 80-130ug/l2.527.5 110






Naphthalene 25.0 40-150ug/l2.532.2 129


Styrene 25.0 80-120ug/l0.5024.2 97




Toluene 25.0 80-120ug/l0.5024.2 97
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1025.4 102 25

Benzene 25.0 1580-120ug/l0.5024.5 98 4




Bromoform 25.0 2075-130ug/l1.024.8 99 0


2-Butanone (MEK) 25.0 3540-150ug/l2.530.0 120 10








Chloroform 25.0 1575-120ug/l0.5023.1 92 4




















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3520-150ug/l2.527.4 109 12

Iodomethane 25.0 1080-130ug/l2.525.1 100 9






Naphthalene 25.0 3040-150ug/l2.532.8 131 2


Styrene 25.0 1580-120ug/l0.5023.2 93 4




Toluene 25.0 1580-120ug/l0.5023.5 94 3
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1019.5 ND 78

Benzene 25.0 70-125ug/l0.5023.8 ND 95




Bromoform 25.0 65-125ug/l1.022.1 ND 88






























Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.520.9 ND 84





4-Methyl-2-pentanone (MIBK) 25.0 55-135ug/l2.522.7 1.05 87




Styrene 25.0 55-135ug/l0.5021.1 ND 85




Toluene 25.0 70-125ug/l0.5021.8 ND 87
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1023.6 ND 94 19

Benzene 25.0 2570-125ug/l0.5025.1 ND 101 6




Bromoform 25.0 2565-125ug/l1.023.9 ND 96 8



















1,3-Dichlorobenzene 25.0 2575-120ug/l0.5030.4 N1aND 122 9











Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3020-150ug/l2.524.0 ND 96 14





4-Methyl-2-pentanone (MIBK) 25.0 2555-135ug/l2.525.9 1.05 99 13




Styrene 25.0 3555-135ug/l0.5023.0 ND 92 9




Toluene 25.0 2070-125ug/l0.5023.5 ND 94 7
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND


2-Butanone (MEK) ug/l2.5ND V1




























Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers













4-Methyl-2-pentanone (MIBK) ug/l2.5ND V1




Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/26/2010 (10A0749-BS1)

Acetone 25.0 10-150ug/l1030.0 120

Benzene 25.0 80-120ug/l0.5026.8 107




Bromoform 25.0 75-130ug/l1.028.3 113


2-Butanone (MEK) 25.0 40-150ug/l2.532.0 V1128








Chloroform 25.0 75-120ug/l0.5026.3 105




















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/26/2010 (10A0749-BS1)






2-Hexanone 25.0 20-150ug/l2.535.3 141

Iodomethane 25.0 80-130ug/l2.525.7 103




4-Methyl-2-pentanone (MIBK) 25.0 60-135ug/l2.533.5 V1134


Naphthalene 25.0 40-150ug/l2.526.3 105


Styrene 25.0 80-120ug/l0.5028.3 113




Toluene 25.0 80-120ug/l0.5026.2 105
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1031.0 124 3

Benzene 25.0 1580-120ug/l0.5026.9 108 0




Bromoform 25.0 2075-130ug/l1.027.6 110 3


2-Butanone (MEK) 25.0 3540-150ug/l2.532.3 V1129 1








Chloroform 25.0 1575-120ug/l0.5026.7 107 2




















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3520-150ug/l2.533.9 136 4

Iodomethane 25.0 1080-130ug/l2.526.8 107 4




4-Methyl-2-pentanone (MIBK) 25.0 2560-135ug/l2.531.9 V1127 5


Naphthalene 25.0 3040-150ug/l2.525.6 103 2


Styrene 25.0 1580-120ug/l0.5028.0 112 1




Toluene 25.0 1580-120ug/l0.5025.7 103 2
















Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1052.0 15.3 147

Benzene 25.0 70-125ug/l0.5028.0 2.81 101


Bromochloromethane 25.0 75-130ug/l0.5028.1 0.810 109

Bromodichloromethane 25.0 75-125ug/l0.5031.6 0.420 125

Bromoform 25.0 65-125ug/l1.026.8 1.74 100


2-Butanone (MEK) 25.0 15-150ug/l2.536.9 V12.14 139

n-Butylbenzene 25.0 70-130ug/l0.5035.6 5.08 122

sec-Butylbenzene 25.0 70-125ug/l0.5031.2 4.02 109






Chloroform 25.0 70-130ug/l0.5032.4 0.290 129



4-Chlorotoluene 25.0 70-125ug/l0.5032.2 M1ND 129

Dibromochloromethane 25.0 70-130ug/l0.5029.7 1.24 114

1,2-Dibromo-3-chloropropane 25.0 50-150ug/l2.538.4 M1ND 154


Dibromomethane 25.0 70-120ug/l0.5029.6 1.11 114





1,1-Dichloroethane 25.0 70-130ug/l0.5032.8 M1ND 131








Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers






Ethylbenzene 25.0 70-125ug/l0.5050.3 18.9 125


2-Hexanone 25.0 20-150ug/l2.537.1 0.490 146


Isopropylbenzene 25.0 75-130ug/l0.5034.1 6.17 112

p-Isopropyltoluene 25.0 70-130ug/l0.5033.1 M1ND 132


4-Methyl-2-pentanone (MIBK) 25.0 55-135ug/l2.536.7 V1, M10.550 145


Naphthalene 25.0 40-150ug/l2.550.0 M111.0 156

n-Propylbenzene 25.0 70-130ug/l0.5032.7 3.85 116

Styrene 25.0 55-135ug/l0.5027.8 ND 111




Toluene 25.0 70-125ug/l0.5033.7 7.51 105



1,1,1-Trichloroethane 25.0 70-130ug/l0.5033.3 M1ND 133





1,2,4-Trimethylbenzene 25.0 70-125ug/l0.5029.8 1.60 113


Vinyl Acetate 25.0 40-150ug/l0.5030.4 0.230 121


Xylenes, Total 50.0 75-120ug/l1.086.4 29.2 114



25.0 80-125Surrogate: 4-Bromofluorobenzene ug/l32.3 S10129

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1038.9 15.3 94 29

Benzene 25.0 2570-125ug/l0.5029.3 2.81 106 5


Bromochloromethane 25.0 2075-130ug/l0.5027.1 0.810 105 3

Bromodichloromethane 25.0 2075-125ug/l0.5026.7 0.420 105 17

Bromoform 25.0 2565-125ug/l1.031.2 1.74 118 15


2-Butanone (MEK) 25.0 3015-150ug/l2.535.0 V12.14 131 5

n-Butylbenzene 25.0 3070-130ug/l0.5033.3 5.08 113 7

sec-Butylbenzene 25.0 3070-125ug/l0.5030.0 4.02 104 4






Chloroform 25.0 2070-130ug/l0.5026.5 0.290 105 20




Dibromochloromethane 25.0 2070-130ug/l0.5028.6 1.24 109 4

1,2-Dibromo-3-chloropropane 25.0 3050-150ug/l2.539.1 M1ND 156 2


Dibromomethane 25.0 2070-120ug/l0.5028.8 1.11 111 3




Dichlorodifluoromethane 25.0 3060-150ug/l0.5024.6 R1ND 99 36


1,2-Dichloroethane 25.0 2065-140ug/l0.5027.3 R1ND 109 35







Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers






Ethylbenzene 25.0 2570-125ug/l0.5046.7 18.9 111 7


2-Hexanone 25.0 3020-150ug/l2.535.9 0.490 142 3


Isopropylbenzene 25.0 2575-130ug/l0.5035.1 6.17 116 3



4-Methyl-2-pentanone (MIBK) 25.0 2555-135ug/l2.534.6 V1, M10.550 136 6


Naphthalene 25.0 3040-150ug/l2.544.6 11.0 134 11

n-Propylbenzene 25.0 3070-130ug/l0.5033.1 3.85 117 1

Styrene 25.0 3555-135ug/l0.5027.3 ND 109 2


1,1,2,2-Tetrachloroethane 25.0 2570-125ug/l0.5031.8 M1ND 127 8


Toluene 25.0 2070-125ug/l0.5032.0 7.51 98 5






Trichlorofluoromethane 25.0 2565-150ug/l0.5025.2 R1ND 101 33


1,2,4-Trimethylbenzene 25.0 3070-125ug/l0.5029.2 1.60 110 2


Vinyl Acetate 25.0 3040-150ug/l0.5027.5 0.230 109 10


Xylenes, Total 50.0 1575-120ug/l1.081.5 29.2 105 6




Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Boron mg/l0.20ND

Calcium mg/l2.0ND

Iron mg/l0.050ND

Magnesium mg/l2.0ND


Sodium mg/l2.0ND

LCS Analyzed: 01/21/2010 (10A0569-BS1)

Boron 1.00 85-115mg/l0.200.969 97

Calcium 21.0 85-115mg/l2.021.0 100

Iron 1.00 85-115mg/l0.0501.00 100

Magnesium 21.0 85-115mg/l2.021.1 100

Manganese 1.00 85-115mg/l0.0101.04 104

Sodium 20.0 85-115mg/l2.019.6 98


Boron 1.00 2085-115mg/l0.200.971 97 0

Calcium 21.0 2085-115mg/l2.020.9 99 1

Iron 1.00 2085-115mg/l0.0500.985 98 2

Magnesium 21.0 2085-115mg/l2.021.0 100 0

Manganese 1.00 2085-115mg/l0.0101.03 103 1

Sodium 20.0 2085-115mg/l2.019.6 98 0


Boron 1.00 75-125mg/l0.204.31 3.26 106

Calcium 21.0 75-125mg/l2.0303 279 117

Iron 1.00 75-125mg/l0.0502.99 1.88 112

Magnesium 21.0 75-125mg/l2.0124 101 112

Manganese 1.00 75-125mg/l0.0101.05 0.0135 104

Sodium 20.0 75-125mg/l2.0516 492 121

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Boron 1.00 1075-125mg/l0.204.38 3.26 112 1

Calcium 21.0 1075-125mg/l2.0321 M3279 202 6

Iron 1.00 1075-125mg/l0.0503.06 1.88 118 2

Magnesium 21.0 1075-125mg/l2.0130 M1101 137 4

Manganese 1.00 1075-125mg/l0.0101.05 0.0135 104 0

Sodium 20.0 1075-125mg/l2.0533 M3492 207 3

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

DISSOLVED METALS


Data

Qualifiers



Iron mg/l0.050ND


Iron mg/l0.050ND

LCS Analyzed: 01/22/2010 (10A0620-BS1)

Iron 1.00 85-115mg/l0.0500.983 98


Iron 1.00 2085-115mg/l0.0500.976 98 1


Iron 1.00 75-125mg/l0.0500.966 ND 97


Iron 1.00 75-125mg/l0.0502.83 1.76 107


Iron 1.00 1075-125mg/l0.0500.957 ND 96 1


Iron 1.00 1075-125mg/l0.0502.92 1.76 117 3

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers




LCS Analyzed: 01/21/2010 (10A0562-BS1)



Phosphorus,Total - P 0.300 2090-110mg/l0.100.330 110 1






Phosphorus,Total - P 0.300 2080-120mg/l0.100.219 M20.0670 51 2





Chloride mg/l2.0ND


Sulfate mg/l2.0ND

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers


LCS Analyzed: 01/20/2010 (10A0584-BS1)


Nitrate-N 4.00 90-110mg/lNA4.12 103

Sulfate 20.0 90-110mg/lNA20.9 N1a104



Nitrate-N 4.00 1590-110mg/lNA4.14 103 0

Sulfate 20.0 1590-110mg/lNA20.9 N1a104 0


Nitrate-N 4.00 80-120mg/l0.2014.2 10.4 94


Chloride 100 80-120mg/l10484 397 87

Nitrate-N 20.0 80-120mg/l1.044.7 23.5 106

Sulfate 100 80-120mg/l10164 56.0 108


Nitrate-N 4.00 1580-120mg/l0.2014.1 10.4 92 0


Chloride 100 1580-120mg/l10483 397 86 0

Nitrate-N 20.0 1580-120mg/l1.044.5 23.5 105 0

Sulfate 100 1580-120mg/l10163 56.0 107 0








Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers


LCS Analyzed: 01/21/2010 (10A0597-BS1)



Alkalinity as CaCO3 250 2090-110mg/l6.0257 103 0








Alkalinity as CaCO3 20mg/l6.0175 175 0

Bicarbonate Alkalinity as CaCO3 20mg/l6.0175 175 0







LCS Analyzed: 01/21/2010 (10A0602-BS1)


Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers









Perchlorate 25.0 80-120ug/l2.025.1 1.13 96


Perchlorate 25.0 80-120ug/l2.025.6 1.91 95


Perchlorate 25.0 1580-120ug/l2.022.9 1.13 87 9


Perchlorate 25.0 1580-120ug/l2.026.2 1.91 97 2




LCS Analyzed: 01/21/2010 (10A0616-BS1)

Ammonia-N 10.0 85-115mg/l0.509.81 98

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Ammonia-N 10.0 2085-115mg/l0.509.69 97 1


Ammonia-N 10.0 70-130mg/l0.508.96 0.390 86


Ammonia-N 10.0 2070-130mg/l0.509.08 0.390 87 1



Chloride mg/l2.0ND

Sulfate mg/l2.0ND

LCS Analyzed: 01/22/2010 (10A0648-BS1)


Sulfate 20.0 90-110mg/lNA20.2 N1a101



Sulfate 20.0 1590-110mg/lNA20.2 N1a101 0


Chloride 20.0 80-120mg/l2.029.6 M227.4 11


Chloride 20.0 1580-120mg/l2.027.0 M227.4 -2 9

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers




LCS Analyzed: 01/26/2010 (10A0725-BS1)


LCS Analyzed: 01/26/2010 (10A0725-BS2)







Total Organic Carbon 20.0 80-120mg/l1.019.3 0.731 93


Total Organic Carbon 20.0 2080-120mg/l1.019.7 0.731 95 2

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorate ug/l20ND

Chlorite ug/l20ND



LCS Analyzed: 01/29/2010 (10A2918-BS1)

Chlorate 100 75-125ug/l2097.7 98

Chlorite 100 75-125ug/l2097.8 98




Chlorate 240 75-125ug/l200307 90.0 90

Chlorite 240 75-125ug/l200218 ND 91




Chlorate 240 75-125ug/l200316 93.1 93

Chlorite 240 75-125ug/l200206 ND 86




Chlorate 240 2575-125ug/l200301 90.0 88 2

Chlorite 240 2575-125ug/l200213 ND 89 2



Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorate 240 2575-125ug/l200302 93.1 87 5

Chlorite 240 2575-125ug/l200211 ND 88 3



Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00






M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike

level. The associated blank spike recovery was acceptable.


Q2 Sample received with head space.



S10 Surrogate recovery was above laboratory and method acceptance limits. See case narrative.

V1 CCV recovery was above method acceptance limits. This target analyte was not detected in the sample.



Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily




454-9303





Sampled:

Received:

01/19/10


Project ID:

PTA0848

PGA North/103965.00



TestAmerica Phoenix

Water XE200.7

Water XEPA 300.0

Water XEPA 314.0

XWater XEPA 8260B

Water XM2320 B

Water XM4500-P B, E

Water XM5310B

WaterSM 4500-P B, E

Water XSM4500-NH3D






Analysis Performed: HydrogenSamples: PTA0848-01, PTA0848-03, PTA0848-05, PTA0848-07



Method Performed: EPA 300.1Samples: PTA0848-01, PTA0848-03, PTA0848-05, PTA0848-07

Project Manager

TestAmerica Phoenix

PTA0848

Kylie Emily



,.

·SENDING LABORATORY:

TestAmerica Phoenix


PTA0848


TestAmerica Irvine

4625 East Cotton Center Blvd. Ste 1 89 Ph~nix, AZ 85040

17461 Derian Ave. Suite 100 Irvine, CA 92614

Phone: (602) 437-3340 Phone :(949) 261-1022

Fax: (602) 454-9303 Fax: (949) 261-1228 Project Manager: Kylie Emily Project Location: AZ. - ARIZONA Client: Environmental Resources Management Inc.-West · Receipt Temperature: .. · oc ·· · · Ice: .Y I . N · . ~ ·

Analysis Units Due Expires lnterlab Price Surch Comments

Sample ID: PTA0848-01 (IRZ-MW-B-01192010- Water) Sampled: 01119110 oa:34 Chlorate (300.1) mg/1' 02/03/10 02/16/10 08:34 $30.00 0%

Chlorite (300.1) - 0 mg/1 02/03/10 02/02/1 0 08:34 $30.00 0%


500 ml Poly w!EDA (L) 125ml Brown Poly w/ EDA(M

Sample ID: PTA0848-03 (IRZ-IW-03-0119201 0 - Water) Sampled: 0111911 o .1 o:23 Chlorate (300.1) mg/1 02/03/10 02/16/10 10:23 $30.00 0%

Chlorite (300.1) - 0 mg/1 02/03/1 0 02/02/10 1 0:23 $30.00 0%


500 rril Poly w!EDA (L) 125ml Brown Poly w/ EDA(M)

Sample ID: PTA0848-05 (IRZ-MW-C-01192010 ·Water) Sampled: 01119110 13:09 Chlorate (300.1) mg/1 02/03/10 02/16/1013:09 $30.00 0%

Chlorite(300.1)-0 mg/1 02/03/10 02/02/1013:09 $30.00 .0%


500 ml Poly w/EDA (L) 125mL Brown Poly w/ EDA M)

Sample 10: PTA0848-07 (IRZ-MW-D-01192010- Water) Sampled: 0111911014:48 Chlorate (300.1) mg/1 02/03/10 02/16/10 14:48 $30.00

Chlorite (300.1) - 0 mg/1 02/03/10 02/02/10 14:48


500 ml Poly w/EDA (L) 125ml .Brown Poly w/ EDA(M

$30.00

0%

0%

L. f. 1-'2..-2.-1 D .

~n r , 'If; t:;D <1-JC!f, Ltv ~ /)oW/ J o ;1: /)0 .

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Released By . Datemme .

Datemme Released By


TAL-0013-550 (12/08)


[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ. 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ. 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Analysis Required

Project Manager: ~G...v1o.... ch. (H._ 5 Pho~ ~()m.!:_e~:q ~- L LL 0 I

Sampler:'S', 1-b\\~/17 _s ch vtl'l'LV-..C(.ef'-

:j c:; t

Sample Description Sample Container Matrix Type

Fax Number: 0 1 :; a l\~o- q qa-L.\ Eh.o ~~ ::6

# of Sampling Sampling Preservatl"ves 9- L. Cont. Date Time \lj · ~

.:C\Ll-mw - () -o\ \ q~ \D I%\) \JO 1\-~v·"""l..

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Turnaround Time:

same day

24 hours

48 hours

Sample Integrity:

intact '"""

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Special Instructions

' \

(Check)

72 hours

5 days

normal

(Check)

on ice ..J

Note: By rehnqu1shmg samples to TestAmenca, cl1ent agrees to pay for the services requ~sted on this cham of custod/form ~nd ~ny additional analyses performed on th1s proJect. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.


rAL-0013-550 (12/08)

Client Name I Address:

Project Manager:

Sample~ P r--

-----------------~---··--------


[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Project/ PO Number:

Phone Number:

~ po;JL + Fax Number:

~ ~ 3 ~ 0. ")

Analysis Required

~~ ~ -------------------------,S-a_m_p-le"c-o-nt-a-in-er~-#-of-.-S-a-m-pl-in_g,_S_a_m-pl-in-g.------.~9- ~

Sample Description Matrix Type Cont. Date Time Preservatives UJ d-

'1\<1;)~

\ ( \ I \-\-N°3

l I " ( X ( L~\er Y\'[)'f\ e__

~~~;;,y £\)(-\ \.1..) -""'L- ~/ e~~ \..lPIY'L '\}Oft t{ \\GL

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/ 48 hours normal

Reli'\)1 isned~By:

Date/Time: L -'7~ -lved in t'l.IZ_ Date/Time: Sample Integrity: (Check)

I J J 1 IJ t\ /1 { 11 intact I on ice _,_

Relinquished By:

I I Note: By relinqu1shmg samples to TestAmenca, client agrees to pay for the serv1ces requested on this cham of custody form and any additional analyses performed on this project. · Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.


rAL-0013-550 (12/08) Client Name/Address:

Y-L 9QJ-<- 1--Project Manager:

Sampler: 0-e_ f~Q__

Sample Container


[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602)454-9303 [ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 8~120 (702) 798-3620 FAX (702) 798-3621

· Project/ PO Number: .d Analysis Required

P.~J<:- ~ i/ " J

~ __::/ s:ez_ ~ d ~J 'j ~ ,t"2 \i 0__, Phone Number: C::1 ~ ~ - ~J, j_

SflL p~-:]__ 0 E_ 'i j f ~ j 5 Q

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JlrJ(~ ) same day 72 hours

Reltq'u\slted By: Date/Time:

/ ~eceived By: Date/Time: 24 hours 5 days ·

,) 48 hours normal

Refinquished By: Date/Time: "- ~ived in(Y !/ l rr~T;7~

Sample Integrity: (Check)

fi~:Yt intact V' on ice i

l ( ........ v-u. .. Note: By relinqurshmg samples to TestAmerrca, client agrees to pay for the servrces requested on thrs cham of custody· form and any additiOnal analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

L

1 CHAIN OF CUSTODY FORM Test America ~cl 'f>TAO@~~-

[ ] Phoe"" , 4625 E. Cotto" Ce,tei Blvd., SoHe 189, Phoe";,, AZ 85040 (602]43Nl340 FAX (602) 454:.003 r (J1 Jog, 01 [ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 THE LEADER IN ENVIRONMENTAL TESTING

IAL-0013-550 (12/08) [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621 ~· . 'r' age ~ of l( J {)

Client Name I Address: Project/ PO Number: Analysis Required I 'C. j

5eL p ctJZ J- 54 ~)f- +- ~ .Lt . 1~ : ["" i~ ~

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~ ;$

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/ 48 hours normal

Relinquished By: Date/Time: t' veaa;By: /J )~aT~~e: Sample lntJrity: (Check)

ln~:~, intact on ice ' ~

' -'· I .. Note. By relrnqUishrng samples to TestAmenca, client agrees to pay for the services requested on this charn of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

·-- --------~~-----

I

I

)

Lab Sample#

P1001275-01

P1 001275-02

P1 001275-03

P1001275-04



Report Date: 02/05/1 0 Client Proj Name: PTA0848

Client Proj #: PTA0848 Suite 189 Phoenix, AZ 85040

Client Sample ID

PTA0848-01

PTA0848-03

PTA0848-05

PTA0848-07

Laboratory Results Total pages in data package: 7

I

Microseeps test results meet all the requiref\l nts of the NELAC standards or provide reasons and/or justification if they do not. "

Approved By:


The analytical results reported here are reliable and usable to the precision expressed in this report. As required by some regulating authorities, a full discussion of the uncertainty In our analytical results can be obtained at our web sl!e or through customer service. Unless otherwise specified, all results


As a valued client we would appreciate your comments on our service. Please call customer service at ( 412)826-5245 or email customerservice@m/croseeps. com.

Case Narrative:

220 William Pitt Way • Pittsburgh, PA 15238 • Tel 412-826-5245 • Fax 412-826-3433



Suite 189 Phoenix, AZ. 85040

Sam(;!le Descri1;2tion Matrix Lab Sample#



Client Proj #: PTA0848

SamQied Daternme Received PTA0848"01 Vapor P1 001275M01 19 Jan. 10 8:34 22 Jan. 1 o 15:35

Analyte(s) Fla~ Result PQL Units Method# Analysis Date

RiskAnalysis N Hydrogen 5.200 0.600 nM AM20GAX 2/2/10

Data Qualifiers: J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovezy/RPD poor for MS!MSD, SAMP/DUP, B- detected in blank, S - field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N "NELAC certified analysis

By

sl



SamQie DescriQtion Matrix Lab Sample#




SamQied Date/Time Received PTA0848-03 Vapor P1 001275-02 19 Jan. 10 10:23 22 Jan. 10 15:35

Analyte(s) Flag Result PQL Units Method# Analysis Date RiskAnalysis N Hydrogen 9.800 0.600 nM AM20GAX 2/2/10

Data Qualifiers: J ·estimated value, U -Non detect, R ·Poor surrogate recovery, M- Recovery!RPD poor for MSIMSD, SAMP/DUP, B -detected in blank, S- field sample llS received did not meet NELAC san1ple acceptance criteria, L ·Subcontracted Lab used, N- NELAC certif1ed analysis

By

sl


Sample Description PTA0848-05

Analyte(s) RiskAnalysis N Hydrogen


Matrix Vapor

Flag

Lab Sample# P1 001275-03

Result PQL

11.000 0.600




Sampled Date/Time 19 Jan. 10 13:09

Received 22 Jan. 10 15:35

Units Method# Analysis Date By

nM AM20GAX 2/2/10 sl

Data Qualifiers: J- estimated value, U- Non detect, R ·Poor surrogate recovery, M- Recovery!RPD poor for MS/MSD, SAMP/DUP, B- detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L -Subcontracted Lab used, N • NELAC certified analysis


Suite 189 Phoenix, P\Z. 85040

Samgle Descri[;!tion Matrix Lab Sample#

Page: Page 5 of 6 Lab Proj #: P1 001275



Samgled Date/Time Received PTA0848-07 Vapor P1001275-04 19 Jan. 10 14:48 22 Jan. 1 0 15:35

Anal~te(s) Flag Result PQL Units Method# Analysis Date By RiskAnalysis N Hydrogen 19.000 0.600 nM AM20GAX 2/2/10 sl

Data Quali 1ers: -estimate value, U- Non detect, R- Poor surrogate recovery, M- Recovery: D poor or MS/MSD, SAMP/DUP, B ·detected

-

\I,,. .. .:r:t~<1r fi J . d 1RP ti

f \ in blank, S - field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N- NELAC certified analysis


Suite 189 Phoenlx, AZ 85040

Prep Method:

Analysis Method:

M1 00202011-MB

Result TrueSpikeConc. RDL

Hydrogen < 0.600 nM 0.600 M1 00202011-LCS

Result TrueSQikeConc.


M1 00202011-LCSD

Result TrueSpikeConc.







%Recovery Ctl Limits

- NA


99.00 75-125

%Recovery Ctt Limits RPD

101.00 75- 125 2.04

RPD Ctl Limits

0-20

L.........----....11 Outlined Results lndlcate results outside of Control limits

Data Qualifiers: 1 ·estimated value, U- Non detect, R ·Poor surrogate recovery, M - Recovery/RPD poor for MSIMSD, SAMP/DUP, B - detected in blank, S ·field sample as receiyed did not meet NELAC sample acceptance criteria, L ·Subcontracted Lab used, N • NELAC certified analysis

SUBCONTRACT ORDER TestAmerlca Phoenix

SENDING LABORATORY:

TestAmerica Phoenix 4625 East Cotton Center Blvd. Ste 189 Phoenix, AZ. 85040 Phone: (602) 437-3340 Fax; (602) 454-9303 Project Manager. Kylie Emily

PTA0848


Microseeps/Univ of Pittsburgh App Research Center 220 William Pitt Way Pittsburgh, PA 15238 Phone :(412)826-5245 Fax; (412)826-3433 Project Location: AZ. -ARIZONA Receipt Temperature: °C Ice: Y I N

.··

Standard TAT is requested unless specific due date is requested. => Due Date: ___ _ Initials: ___ _

Analysis Units

Sample 10: PTA0848-01 (IRZ-MW-8-01192010 ·Water}

Hydrogen


NA (N)

%

Sample ID: PTA0848·03 (IRZ·IW-03-01192010 ·Water}

Hydrogen %


NA (N)

Sample 10: PTA084B-05 (IRZ-MW-C-01192010 ·Water)

Hydrogen


NA (N)

%

Sam pie ID: PTA0848-07 (IRZ-MW-D-0119201 0 ·Water}

Hydrogen


NA (N)

%

Expires

Sampled: 01/19/10 08:34 0211611 0 08:34

Sampled: 01/19/10 10:23 02/16/1 0 10:23

Sampled: 01/19/10 13:09 02/16/10 13:09

Sampled: 01/19/10 14:48 02/16/1014:48

~ LIJD/!~ t't:tfil ""'R-e~le-as""e..t.d._B-y-------'-+-1..... Datemme

Released Bv Datemme

Comments

Microseeps

Microseeps

Microseeps

Microseeps

Page 1 of 1


454-9303

LABORATORY REPORT





Received:

Issued:

01/20/10

01/20/10

02/10/10 09:45









CASE NARRATIVE


PTA0936-01 IRZ-IW-02-01202010 Water

PTA0936-02 IRZ-IW-02-01202010 Water

PTA0936-03 IRZ-IW-01-01202010 Water

PTA0936-04 IRZ-IW-01-01202010 Water

PTA0936-05 IRZ-IW-01-01202010-R Water

PTA0936-06 Trip Blank Water

PTA0936-07 IRZ-IW-04-01202010 Water

PTA0936-08 IRZ-IW-04-01202010 Water

PTA0936-09 IRZ-IW-04-01202010 Water

PTA0936-10 IRZ-IW-04-01202010-D Water

PTA0936-11 Tank Water

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily

<Page 1 of 84>


454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

SAMPLE RECEIPT: Samples were received intact, at 0°C and 3°C, on ice and with chain of custody documentation.










N1a-method 300.0-Results exceeded the linear range in the MS/MSD and therefore are not available for

reporting. The batch was accepted based on acceptable recovery in the Blank Spike (LCS).

N1a-PTA0936-06 Carbon disulfide- Due to lab conatmination the trip blank had a detect of Carbon

disulfide. The sample was re-analyzed with head space and both results are reported.

N1a-10A0646-MSD1-The Laboratory Control Sample / Laboratory Control Sample Duplicate and Matrix

Spike Duplicate recovered high and outside of acceptance limits for 1,3-Dichlorobenzene. All associated

samples are non-detect for this compound and therefore are not impacted.

N1a-Batch 10B0083 tert-Butylbenzene-Tert-Butylbenzene was recovered high and outside laboratory limits

in the second source curve verification sample and recovered high and outside laboratory limits in the CCV.

Tert-Butylbenzene was high and outside laboratory limits in the Laboratory Control Sample/Laboratory

Control Sample Duplicate. All associated samples were not detected for tert-Butylbenzene and therefore

should not be impacted.



Reviewed By:

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



1/22/20101/21/2010EPA 8260BAcetone 1010A0622 1ND

1/22/20101/21/2010EPA 8260BBenzene 0.5010A0622 1ND



























1,1-Dichloroethene 1/22/20101/21/201010A0622 0.50 1EPA 8260B 1.2












Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0936-01 (IRZ-IW-02-01202010 - Water) - cont.







Methyl-tert-butyl Ether (MTBE) 1/22/20101/21/201010A0622 0.50 1EPA 8260B 67



1/22/20101/21/2010EPA 8260BStyrene 0.5010A0622 1ND




1/22/20101/21/2010EPA 8260BToluene 0.5010A0622 1ND















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result







Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



1/22/20101/21/2010EPA 8260BAcetone 1010A0622 1ND

Benzene 1/22/20101/21/201010A0622 0.50 1EPA 8260B 0.91



























1,1-Dichloroethene 1/22/20101/21/201010A0622 0.50 1EPA 8260B 10












Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result











1/22/20101/21/2010EPA 8260BStyrene 0.5010A0622 1ND




1/22/20101/21/2010EPA 8260BToluene 0.5010A0622 1ND















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result







Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0936-05 (IRZ-IW-01-01202010-R - Water)


1/22/20101/21/2010EPA 8260BAcetone 1010A0622 1ND

1/22/20101/21/2010EPA 8260BBenzene 0.5010A0622 1ND







































Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0936-05 (IRZ-IW-01-01202010-R - Water) - cont.











1/22/20101/21/2010EPA 8260BStyrene 0.5010A0622 1ND




1/22/20101/21/2010EPA 8260BToluene 0.5010A0622 1ND





Trichloroethene 1/22/20101/21/201010A0622 0.50 M21EPA 8260B 9.4











Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0936-06 (Trip Blank - Water)


1/22/20101/21/2010EPA 8260BAcetone 1010A0622 1ND

1/22/20101/21/2010EPA 8260BBenzene 0.5010A0622 1ND







































Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0936-06 (Trip Blank - Water) - cont.











1/22/20101/21/2010EPA 8260BStyrene 0.5010A0622 1ND




1/22/20101/21/2010EPA 8260BToluene 0.5010A0622 1ND
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0936-06RE1 (Trip Blank - Water) - cont. Q2






Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



1/22/20101/21/2010EPA 8260BAcetone 1010A0622 1ND

1/22/20101/21/2010EPA 8260BBenzene 0.5010A0622 1ND







































Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result











1/22/20101/21/2010EPA 8260BStyrene 0.5010A0622 1ND




1/22/20101/21/2010EPA 8260BToluene 0.5010A0622 1ND















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result







Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0936-10 (IRZ-IW-04-01202010-D - Water)






Sample ID: PTA0936-10RE1 (IRZ-IW-04-01202010-D - Water)


2/2/20102/2/2010EPA 8260BAcetone 10010B0083 10ND

2/2/20102/2/2010EPA 8260BBenzene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BBromobenzene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BBromochloromethane 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BBromodichloromethane 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BBromoform 1010B0083 V110ND

2/2/20102/2/2010EPA 8260BBromomethane 1010B0083 10ND

2/2/20102/2/2010EPA 8260B2-Butanone (MEK) 2510B0083 10ND

2/2/20102/2/2010EPA 8260Bn-Butylbenzene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260Bsec-Butylbenzene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260Btert-Butylbenzene 5.010B0083 V1, N1a10ND

2/2/20102/2/2010EPA 8260BCarbon disulfide 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BCarbon tetrachloride 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BChlorobenzene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BChloroethane 1010B0083 10ND

2/2/20102/2/2010EPA 8260BChloroform 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BChloromethane 1010B0083 10ND

2/2/20102/2/2010EPA 8260B2-Chlorotoluene 5.010B0083 10ND


2/2/20102/2/2010EPA 8260BDibromochloromethane 5.010B0083 V110ND

2/2/20102/2/2010EPA 8260B1,2-Dibromo-3-chloropropane 2510B0083 10ND

2/2/20102/2/2010EPA 8260B1,2-Dibromoethane (EDB) 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BDibromomethane 5.010B0083 10ND

2/2/20102/2/2010EPA 8260B1,2-Dichlorobenzene 5.010B0083 10ND



2/2/20102/2/2010EPA 8260BDichlorodifluoromethane 5.010B0083 10ND

2/2/20102/2/2010EPA 8260B1,1-Dichloroethane 5.010B0083 10ND


2/2/20102/2/2010EPA 8260B1,1-Dichloroethene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260Bcis-1,2-Dichloroethene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260Btrans-1,2-Dichloroethene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260B1,2-Dichloropropane 5.010B0083 10ND


Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTA0936-10RE1 (IRZ-IW-04-01202010-D - Water) - cont.


2/2/20102/2/2010EPA 8260B2,2-Dichloropropane 1010B0083 10ND

2/2/20102/2/2010EPA 8260B1,1-Dichloropropene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260Bcis-1,3-Dichloropropene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260Btrans-1,3-Dichloropropene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BEthylbenzene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BHexachlorobutadiene 1010B0083 B110ND

2/2/20102/2/2010EPA 8260B2-Hexanone 2510B0083 10ND

2/2/20102/2/2010EPA 8260BIodomethane 2510B0083 10ND

2/2/20102/2/2010EPA 8260BIsopropylbenzene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260Bp-Isopropyltoluene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BMethylene Chloride 1010B0083 10ND

2/2/20102/2/2010EPA 8260B4-Methyl-2-pentanone (MIBK) 2510B0083 10ND

2/2/20102/2/2010EPA 8260BMethyl-tert-butyl Ether (MTBE) 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BNaphthalene 2510B0083 10ND

2/2/20102/2/2010EPA 8260Bn-Propylbenzene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BStyrene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260B1,1,1,2-Tetrachloroethane 5.010B0083 10ND


2/2/20102/2/2010EPA 8260BTetrachloroethene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BToluene 5.010B0083 10ND

2/2/20102/2/2010EPA 8260B1,2,3-Trichlorobenzene 1010B0083 10ND


2/2/20102/2/2010EPA 8260B1,1,1-Trichloroethane 5.010B0083 10ND


2/2/20102/2/2010EPA 8260BTrichlorofluoromethane 5.010B0083 10ND

2/2/20102/2/2010EPA 8260B1,2,3-Trichloropropane 1010B0083 10ND

2/2/20102/2/2010EPA 8260B1,2,4-Trimethylbenzene 5.010B0083 10ND


2/2/20102/2/2010EPA 8260BVinyl Acetate 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BVinyl chloride 5.010B0083 10ND

2/2/20102/2/2010EPA 8260BXylenes, Total 1010B0083 10ND




Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Boron 1/22/20101/21/201010A0609 0.20 1E200.7 4.3

Calcium 1/22/20101/21/201010A0609 2.0 M11E200.7 310

Iron 1/22/20101/21/201010A0609 0.050 1E200.7 1.4

Magnesium 1/22/20101/21/201010A0609 2.0 1E200.7 120

Manganese 1/22/20101/21/201010A0609 0.010 1E200.7 0.090

Sodium 1/22/20101/21/201010A0609 2.0 M11E200.7 430



Boron 1/22/20101/21/201010A0609 0.20 1E200.7 4.2

Calcium 1/22/20101/21/201010A0609 2.0 M11E200.7 360

Iron 1/22/20101/21/201010A0609 0.050 1E200.7 0.11

Magnesium 1/22/20101/21/201010A0609 2.0 1E200.7 100

Manganese 1/22/20101/21/201010A0609 0.010 1E200.7 0.019

Sodium 1/22/20101/21/201010A0609 2.0 M11E200.7 420



Boron 1/22/20101/21/201010A0609 0.20 1E200.7 2.9

Calcium 1/22/20101/21/201010A0609 2.0 1E200.7 340

Iron 1/22/20101/21/201010A0609 0.050 1E200.7 14

Magnesium 1/22/20101/21/201010A0609 2.0 1E200.7 130

Manganese 1/22/20101/21/201010A0609 0.010 1E200.7 0.16

Sodium 1/22/20101/21/201010A0609 2.0 1E200.7 410

Sample ID: PTA0936-11 (Tank - Water)


Boron 1/22/20101/21/201010A0609 0.20 1E200.7 0.80

Calcium 1/22/20101/21/201010A0609 2.0 1E200.7 300

1/22/20101/21/2010E200.7Iron 0.05010A0609 1ND

Magnesium 1/22/20101/21/201010A0609 2.0 1E200.7 120

1/22/20101/21/2010E200.7Manganese 0.01010A0609 1ND

Sodium 1/22/20101/21/201010A0609 2.0 1E200.7 220

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

DISSOLVED METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



1/22/20101/21/2010E200.7Iron 0.05010A0620 1ND



1/22/20101/21/2010E200.7Iron 0.05010A0620 1ND



1/22/20101/21/2010E200.7Iron 0.05010A0620 1ND

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result








Nitrate-N 1/20/20101/20/201010A0584 0.20 1EPA 300.0 9.8

2/1/20102/1/2010SM 4500-P B, EPhosphate 0.3010B0015 1ND








Chloride 1/25/20101/25/201010A0700 40 20EPA 300.0 730

Sulfate 1/25/20101/25/201010A0700 40 20EPA 300.0 980








Nitrate-N 1/20/20101/20/201010A0584 1.0 5EPA 300.0 15









Chloride 1/25/20101/25/201010A0700 40 20EPA 300.0 800

Sulfate 1/25/20101/25/201010A0700 40 20EPA 300.0 1100

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result








Nitrate-N 1/20/20101/20/201010A0584 1.0 5EPA 300.0 21









Chloride 1/25/20101/25/201010A0700 40 20EPA 300.0 770

Sulfate 1/25/20101/25/201010A0700 40 20EPA 300.0 1100

Sample ID: PTA0936-10 (IRZ-IW-04-01202010-D - Water)



Sample ID: PTA0936-11 (Tank - Water)






Nitrate-N 1/20/20101/20/201010A0584 0.20 1EPA 300.0 16


Sample ID: PTA0936-11RE1 (Tank - Water)


Chloride 1/25/20101/25/201010A0700 40 20EPA 300.0 660

Sulfate 1/25/20101/25/201010A0700 40 20EPA 300.0 770

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result










Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



1/29/20101/29/2010EPA 300.1Chlorate 4010A2918 D12ND






Chlorate 1/29/20101/29/201010A2918 40 2EPA 300.1 68

Chlorite 1/31/20101/31/201010A3035 400 20EPA 300.1 1300





Chlorate 1/29/20101/29/201010A2918 40 2EPA 300.1 93




Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)


2 01/20/2010 09:30 01/20/2010 17:21 01/20/2010 17:45 01/20/2010 19:24EPA 300.0


2 01/20/2010 11:25 01/20/2010 17:21 01/20/2010 17:45 01/20/2010 20:19EPA 300.0


2 01/20/2010 14:35 01/20/2010 17:21 01/20/2010 17:45 01/20/2010 20:38EPA 300.0

Sample ID: Tank (PTA0936-11) - Water

2 01/20/2010 16:04 01/20/2010 17:21 01/20/2010 17:45 01/20/2010 20:56EPA 300.0

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/21/2010 (10A0622-BS1)

Acetone 25.0 10-150ug/l1032.5 130

Benzene 25.0 80-120ug/l0.5025.5 102




Bromoform 25.0 75-130ug/l1.023.4 94


2-Butanone (MEK) 25.0 40-150ug/l2.532.5 130








Chloroform 25.0 75-120ug/l0.5024.7 99




















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/21/2010 (10A0622-BS1)






2-Hexanone 25.0 20-150ug/l2.530.1 120

Iodomethane 25.0 80-130ug/l2.524.6 98






Naphthalene 25.0 40-150ug/l2.528.6 114


Styrene 25.0 80-120ug/l0.5024.8 99




Toluene 25.0 80-120ug/l0.5024.5 98
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1033.0 132 2

Benzene 25.0 1580-120ug/l0.5026.2 105 3




Bromoform 25.0 2075-130ug/l1.025.4 102 8


2-Butanone (MEK) 25.0 3540-150ug/l2.534.5 138 6


sec-Butylbenzene 25.0 1580-125ug/l0.5028.3 113 0.1






Chloroform 25.0 1575-120ug/l0.5025.4 101 3










1,4-Dichlorobenzene 25.0 1580-120ug/l0.5028.9 115 0.03


1,1-Dichloroethane 25.0 1570-125ug/l0.5024.6 99 0.5








Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers






Ethylbenzene 25.0 1580-120ug/l0.5025.0 100 0.4


2-Hexanone 25.0 3520-150ug/l2.532.6 131 8

Iodomethane 25.0 1080-130ug/l2.526.4 105 7


p-Isopropyltoluene 25.0 1580-130ug/l0.5028.9 115 0.2




Naphthalene 25.0 3040-150ug/l2.531.3 125 9


Styrene 25.0 1580-120ug/l0.5025.1 101 1




Toluene 25.0 1580-120ug/l0.5025.2 101 3
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1020.4 ND 82

Benzene 25.0 70-125ug/l0.5026.3 ND 105




Bromoform 25.0 65-125ug/l1.025.2 ND 101






























Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.525.6 ND 103









Styrene 25.0 55-135ug/l0.5025.0 ND 100




Toluene 25.0 70-125ug/l0.5025.3 ND 101





Trichloroethene 25.0 70-125ug/l0.5026.6 M29.35 69











Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1019.1 ND 76 7

Benzene 25.0 2570-125ug/l0.5026.2 ND 105 0.3




Bromoform 25.0 2565-125ug/l1.024.5 ND 98 3






Carbon disulfide 25.0 2565-145ug/l0.5031.4 0.430 124 0.8







4-Chlorotoluene 25.0 2570-125ug/l0.5027.6 ND 110 0.5


1,2-Dibromo-3-chloropropane 25.0 3050-150ug/l2.528.8 ND 115 0.6



1,2-Dichlorobenzene 25.0 2075-120ug/l0.5027.3 ND 109 0.3





1,2-Dichloroethane 25.0 2065-140ug/l0.5021.4 ND 86 0.1




1,2-Dichloropropane 25.0 2075-125ug/l0.5024.6 ND 98 0.4



Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers





trans-1,3-Dichloropropene 25.0 2070-130ug/l0.5022.6 ND 91 0.04



2-Hexanone 25.0 3020-150ug/l2.524.9 ND 100 3







Naphthalene 25.0 3040-150ug/l2.530.3 ND 121 0.5

n-Propylbenzene 25.0 3070-130ug/l0.5027.9 ND 112 0.07

Styrene 25.0 3555-135ug/l0.5024.6 ND 98 2




Toluene 25.0 2070-125ug/l0.5024.5 ND 98 3

1,2,3-Trichlorobenzene 25.0 3550-150ug/l1.030.2 ND 121 0.4




Trichloroethene 25.0 2570-125ug/l0.5025.8 M29.35 66 3

Trichlorofluoromethane 25.0 2565-150ug/l0.5023.4 ND 94 0.04

1,2,3-Trichloropropane 25.0 2570-130ug/l1.029.3 ND 117 0.3

1,2,4-Trimethylbenzene 25.0 3070-125ug/l0.5026.7 ND 107 0.9

1,3,5-Trimethylbenzene 25.0 2575-130ug/l0.5027.3 ND 109 0.2







Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/22/2010 (10A0646-BS1)

Acetone 25.0 10-150ug/l1032.8 131

Benzene 25.0 80-120ug/l0.5025.3 101




Bromoform 25.0 75-130ug/l1.024.8 99


2-Butanone (MEK) 25.0 40-150ug/l2.533.0 132








Chloroform 25.0 75-120ug/l0.5024.1 96









1,3-Dichlorobenzene 25.0 80-120ug/l0.5030.5 L3122











Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/22/2010 (10A0646-BS1)






2-Hexanone 25.0 20-150ug/l2.530.8 123

Iodomethane 25.0 80-130ug/l2.527.5 110






Naphthalene 25.0 40-150ug/l2.532.2 129


Styrene 25.0 80-120ug/l0.5024.2 97




Toluene 25.0 80-120ug/l0.5024.2 97
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1025.4 102 25

Benzene 25.0 1580-120ug/l0.5024.5 98 4




Bromoform 25.0 2075-130ug/l1.024.8 99 0.04


2-Butanone (MEK) 25.0 3540-150ug/l2.530.0 120 10








Chloroform 25.0 1575-120ug/l0.5023.1 92 4




















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers





trans-1,3-Dichloropropene 25.0 1580-125ug/l0.5022.6 90 0.4



2-Hexanone 25.0 3520-150ug/l2.527.4 109 12

Iodomethane 25.0 1080-130ug/l2.525.1 100 9






Naphthalene 25.0 3040-150ug/l2.532.8 131 2


Styrene 25.0 1580-120ug/l0.5023.2 93 4




Toluene 25.0 1580-120ug/l0.5023.5 94 3







1,2,3-Trichloropropane 25.0 2070-130ug/l1.030.7 123 0.4



Vinyl Acetate 25.0 2540-150ug/l0.5023.0 92 0.4






Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1019.5 ND 78

Benzene 25.0 70-125ug/l0.5023.8 ND 95




Bromoform 25.0 65-125ug/l1.022.1 ND 88






























Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.520.9 ND 84





4-Methyl-2-pentanone (MIBK) 25.0 55-135ug/l2.522.7 1.05 87




Styrene 25.0 55-135ug/l0.5021.1 ND 85




Toluene 25.0 70-125ug/l0.5021.8 ND 87
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1023.6 ND 94 19

Benzene 25.0 2570-125ug/l0.5025.1 ND 101 6




Bromoform 25.0 2565-125ug/l1.023.9 ND 96 8



















1,3-Dichlorobenzene 25.0 2575-120ug/l0.5030.4 N1aND 122 9











Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3020-150ug/l2.524.0 ND 96 14

Iodomethane 25.0 3060-150ug/l2.526.4 ND 106 0.2




4-Methyl-2-pentanone (MIBK) 25.0 2555-135ug/l2.525.9 1.05 99 13




Styrene 25.0 3555-135ug/l0.5023.0 ND 92 9




Toluene 25.0 2070-125ug/l0.5023.5 ND 94 7
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







LCS Analyzed: 01/22/2010 (10A0652-BS1)













25.0 80-120Surrogate: Toluene-d8 ug/l13.0 S652





25.0 80-120Surrogate: Toluene-d8 ug/l11.0 S644


Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND


2-Butanone (MEK) ug/l2.5ND V1




























Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers













4-Methyl-2-pentanone (MIBK) ug/l2.5ND V1




Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/26/2010 (10A0749-BS1)

Acetone 25.0 10-150ug/l1030.0 120

Benzene 25.0 80-120ug/l0.5026.8 107




Bromoform 25.0 75-130ug/l1.028.3 113


2-Butanone (MEK) 25.0 40-150ug/l2.532.0 V1128








Chloroform 25.0 75-120ug/l0.5026.3 105




















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/26/2010 (10A0749-BS1)






2-Hexanone 25.0 20-150ug/l2.535.3 141

Iodomethane 25.0 80-130ug/l2.525.7 103




4-Methyl-2-pentanone (MIBK) 25.0 60-135ug/l2.533.5 V1134


Naphthalene 25.0 40-150ug/l2.526.3 105


Styrene 25.0 80-120ug/l0.5028.3 113




Toluene 25.0 80-120ug/l0.5026.2 105
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1031.0 124 3

Benzene 25.0 1580-120ug/l0.5026.9 108 0.4




Bromoform 25.0 2075-130ug/l1.027.6 110 3


2-Butanone (MEK) 25.0 3540-150ug/l2.532.3 V1129 0.9





Carbon tetrachloride 25.0 2075-130ug/l0.5026.6 106 0.2



Chloroform 25.0 1575-120ug/l0.5026.7 107 2



















2,2-Dichloropropane 25.0 1575-130ug/l1.027.1 108 0.2

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 1575-120ug/l0.5027.1 109 0.2





2-Hexanone 25.0 3520-150ug/l2.533.9 136 4

Iodomethane 25.0 1080-130ug/l2.526.8 107 4

Isopropylbenzene 25.0 1580-130ug/l0.5028.2 113 0.7



4-Methyl-2-pentanone (MIBK) 25.0 2560-135ug/l2.531.9 V1127 5

Methyl-tert-butyl Ether (MTBE) 25.0 2070-130ug/l0.5029.4 118 0.8

Naphthalene 25.0 3040-150ug/l2.525.6 103 2


Styrene 25.0 1580-120ug/l0.5028.0 112 1

1,1,1,2-Tetrachloroethane 25.0 1575-125ug/l0.5027.2 109 0.9



Toluene 25.0 1580-120ug/l0.5025.7 103 2
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1052.0 15.3 147

Benzene 25.0 70-125ug/l0.5028.0 2.81 101


Bromochloromethane 25.0 75-130ug/l0.5028.1 0.810 109


Bromoform 25.0 65-125ug/l1.026.8 1.74 100


2-Butanone (MEK) 25.0 15-150ug/l2.536.9 V12.14 139

n-Butylbenzene 25.0 70-130ug/l0.5035.6 5.08 122

sec-Butylbenzene 25.0 70-125ug/l0.5031.2 4.02 109






Chloroform 25.0 70-130ug/l0.5032.4 0.290 129



4-Chlorotoluene 25.0 70-125ug/l0.5032.2 M1ND 129


1,2-Dibromo-3-chloropropane 25.0 50-150ug/l2.538.4 M1ND 154


Dibromomethane 25.0 70-120ug/l0.5029.6 1.11 114













Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers






Ethylbenzene 25.0 70-125ug/l0.5050.3 18.9 125


2-Hexanone 25.0 20-150ug/l2.537.1 0.490 146


Isopropylbenzene 25.0 75-130ug/l0.5034.1 6.17 112

p-Isopropyltoluene 25.0 70-130ug/l0.5033.1 M1ND 132


4-Methyl-2-pentanone (MIBK) 25.0 55-135ug/l2.536.7 V1, M10.550 145


Naphthalene 25.0 40-150ug/l2.550.0 M111.0 156

n-Propylbenzene 25.0 70-130ug/l0.5032.7 3.85 116

Styrene 25.0 55-135ug/l0.5027.8 ND 111




Toluene 25.0 70-125ug/l0.5033.7 7.51 105



1,1,1-Trichloroethane 25.0 70-130ug/l0.5033.3 M1ND 133







Vinyl Acetate 25.0 40-150ug/l0.5030.4 0.230 121


Xylenes, Total 50.0 75-120ug/l1.086.4 29.2 114



25.0 80-125Surrogate: 4-Bromofluorobenzene ug/l32.3 S10129

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1038.9 15.3 94 29

Benzene 25.0 2570-125ug/l0.5029.3 2.81 106 5


Bromochloromethane 25.0 2075-130ug/l0.5027.1 0.810 105 3


Bromoform 25.0 2565-125ug/l1.031.2 1.74 118 15


2-Butanone (MEK) 25.0 3015-150ug/l2.535.0 V12.14 131 5

n-Butylbenzene 25.0 3070-130ug/l0.5033.3 5.08 113 7

sec-Butylbenzene 25.0 3070-125ug/l0.5030.0 4.02 104 4






Chloroform 25.0 2070-130ug/l0.5026.5 0.290 105 20





1,2-Dibromo-3-chloropropane 25.0 3050-150ug/l2.539.1 M1ND 156 2


Dibromomethane 25.0 2070-120ug/l0.5028.8 1.11 111 3




Dichlorodifluoromethane 25.0 3060-150ug/l0.5024.6 R1ND 99 36


1,2-Dichloroethane 25.0 2065-140ug/l0.5027.3 R1ND 109 35


cis-1,2-Dichloroethene 25.0 2070-125ug/l0.5025.5 ND 102 0.7





Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers






Ethylbenzene 25.0 2570-125ug/l0.5046.7 18.9 111 7


2-Hexanone 25.0 3020-150ug/l2.535.9 0.490 142 3


Isopropylbenzene 25.0 2575-130ug/l0.5035.1 6.17 116 3



4-Methyl-2-pentanone (MIBK) 25.0 2555-135ug/l2.534.6 V1, M10.550 136 6


Naphthalene 25.0 3040-150ug/l2.544.6 11.0 134 11

n-Propylbenzene 25.0 3070-130ug/l0.5033.1 3.85 117 1

Styrene 25.0 3555-135ug/l0.5027.3 ND 109 2

1,1,1,2-Tetrachloroethane 25.0 2070-125ug/l0.5026.3 ND 105 0.04

1,1,2,2-Tetrachloroethane 25.0 2570-125ug/l0.5031.8 M1ND 127 8


Toluene 25.0 2070-125ug/l0.5032.0 7.51 98 5






Trichlorofluoromethane 25.0 2565-150ug/l0.5025.2 R1ND 101 33




Vinyl Acetate 25.0 3040-150ug/l0.5027.5 0.230 109 10


Xylenes, Total 50.0 1575-120ug/l1.081.5 29.2 105 6




Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

Batch: 10B0083 Extracted: 02/02/10

Blank Analyzed: 02/02/2010 (10B0083-BLK1)

Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND V1





tert-Butylbenzene ug/l0.50ND V1, N1a









Dibromochloromethane ug/l0.50ND V1
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







Hexachlorobutadiene ug/l1.01.50 B1










Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 02/02/2010 (10B0083-BS1)

Acetone 25.0 10-150ug/l1011.4 45

Benzene 25.0 80-120ug/l0.5023.2 93




Bromoform 25.0 75-130ug/l1.025.6 V1102


2-Butanone (MEK) 25.0 40-150ug/l2.517.7 71



tert-Butylbenzene 25.0 80-120ug/l0.5032.9 V1, L3, N1a132





Chloroform 25.0 75-120ug/l0.5024.8 99




Dibromochloromethane 25.0 80-120ug/l0.5027.5 V1110
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 02/02/2010 (10B0083-BS1)





Hexachlorobutadiene 25.0 40-150ug/l1.028.3 B1113

2-Hexanone 25.0 20-150ug/l2.531.2 125

Iodomethane 25.0 80-130ug/l2.525.8 103






Naphthalene 25.0 40-150ug/l2.526.8 107


Styrene 25.0 80-120ug/l0.5025.8 103




Toluene 25.0 80-120ug/l0.5023.3 93
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Dup Analyzed: 02/02/2010 (10B0083-BSD1)

Acetone 25.0 3510-150ug/l1011.4 46 0.4

Benzene 25.0 1580-120ug/l0.5023.0 92 1



Bromodichloromethane 25.0 1580-120ug/l0.5026.6 106 0.8

Bromoform 25.0 2075-130ug/l1.024.9 V199 3


2-Butanone (MEK) 25.0 3540-150ug/l2.519.4 77 9



tert-Butylbenzene 25.0 1580-120ug/l0.5030.4 V1, L3, N1a122 8

Carbon disulfide 25.0 1570-140ug/l0.5021.3 85 0.6




Chloroform 25.0 1575-120ug/l0.5024.9 100 0.6




Dibromochloromethane 25.0 1580-120ug/l0.5027.6 V1110 0.1


1,2-Dibromoethane (EDB) 25.0 1580-120ug/l0.5023.9 95 0.3














Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







Hexachlorobutadiene 25.0 3540-150ug/l1.027.0 B1108 5

2-Hexanone 25.0 3520-150ug/l2.536.0 144 14

Iodomethane 25.0 1080-130ug/l2.525.9 104 0.4






Naphthalene 25.0 3040-150ug/l2.526.1 105 2


Styrene 25.0 1580-120ug/l0.5025.8 103 0




Toluene 25.0 1580-120ug/l0.5023.0 92 1




1,1,2-Trichloroethane 25.0 1580-120ug/l0.5023.7 95 0.5

Trichloroethene 25.0 1580-120ug/l0.5022.7 91 0.4







Xylenes, Total 75.0 1560-140ug/l1.074.7 100 0.3




Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 02/02/2010 (10B0083-MS1) Source: PTA1400-12

Acetone 25.0 10-150ug/l108.58 ND 34

Benzene 25.0 70-125ug/l0.5022.7 ND 91




Bromoform 25.0 65-125ug/l1.024.1 V1ND 96





tert-Butylbenzene 25.0 70-125ug/l0.5031.3 V1, N1aND 125









Dibromochloromethane 25.0 70-130ug/l0.5026.4 V1ND 105
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 02/02/2010 (10B0083-MS1) Source: PTA1400-12





Hexachlorobutadiene 25.0 40-150ug/l1.026.8 B1ND 107

2-Hexanone 25.0 20-150ug/l2.525.9 ND 104









Styrene 25.0 55-135ug/l0.5025.4 ND 101




Toluene 25.0 70-125ug/l0.5022.9 ND 92
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 02/02/2010 (10B0083-MSD1) Source: PTA1400-12

Acetone 25.0 3510-150ug/l107.45 ND 30 14

Benzene 25.0 2570-125ug/l0.5022.4 ND 90 1


Bromochloromethane 25.0 2075-130ug/l0.5023.6 ND 94 0.04


Bromoform 25.0 2565-125ug/l1.024.6 V1ND 98 2





tert-Butylbenzene 25.0 2570-125ug/l0.5030.9 V1, N1aND 123 1









Dibromochloromethane 25.0 2070-130ug/l0.5026.3 V1ND 105 0.2
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 02/02/2010 (10B0083-MSD1) Source: PTA1400-12


cis-1,3-Dichloropropene 25.0 2075-130ug/l0.5025.1 ND 101 0.9



Hexachlorobutadiene 25.0 3040-150ug/l1.027.4 B1ND 110 2

2-Hexanone 25.0 3020-150ug/l2.525.4 ND 101 2

Iodomethane 25.0 3060-150ug/l2.526.0 ND 104 0.8



Methylene Chloride 25.0 2065-130ug/l1.021.4 ND 85 0.7

4-Methyl-2-pentanone (MIBK) 25.0 2555-135ug/l2.528.5 ND 114 0.1

Methyl-tert-butyl Ether (MTBE) 25.0 2565-140ug/l0.5022.7 ND 91 0.4

Naphthalene 25.0 3040-150ug/l2.525.2 ND 101 0.1


Styrene 25.0 3555-135ug/l0.5024.2 ND 97 4




Toluene 25.0 2070-125ug/l0.5022.4 ND 90 2
















Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Boron mg/l0.20ND

Calcium mg/l2.0ND

Iron mg/l0.050ND

Magnesium mg/l2.0ND


Sodium mg/l2.0ND

LCS Analyzed: 01/22/2010 (10A0609-BS1)

Boron 1.00 85-115mg/l0.200.979 98

Calcium 21.0 85-115mg/l2.021.4 102

Iron 1.00 85-115mg/l0.0501.07 107

Magnesium 21.0 85-115mg/l2.021.9 104

Manganese 1.00 85-115mg/l0.0101.01 101

Sodium 20.0 85-115mg/l2.020.1 101


Boron 1.00 2085-115mg/l0.200.982 98 0.3

Calcium 21.0 2085-115mg/l2.021.5 102 0.5

Iron 1.00 2085-115mg/l0.0501.06 106 0.8

Magnesium 21.0 2085-115mg/l2.022.0 105 0.5

Manganese 1.00 2085-115mg/l0.0101.01 101 0.1

Sodium 20.0 2085-115mg/l2.020.2 101 0.3


Boron 1.00 75-125mg/l0.205.36 4.26 110

Calcium 21.0 75-125mg/l2.0326 307 94

Iron 1.00 75-125mg/l0.0502.45 1.43 103

Magnesium 21.0 75-125mg/l2.0138 115 106

Manganese 1.00 75-125mg/l0.0101.05 0.0902 96

Sodium 20.0 75-125mg/l2.0465 M1434 157

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Boron 1.00 75-125mg/l0.205.28 4.22 106

Calcium 21.0 75-125mg/l2.0390 M1363 129

Iron 1.00 75-125mg/l0.0501.17 0.111 106

Magnesium 21.0 75-125mg/l2.0125 102 111

Manganese 1.00 75-125mg/l0.0100.966 0.0190 95

Sodium 20.0 75-125mg/l2.0453 M1420 164


Boron 1.00 1075-125mg/l0.205.37 4.26 111 0.2

Calcium 21.0 1075-125mg/l2.0337 M1307 143 3

Iron 1.00 1075-125mg/l0.0502.48 1.43 105 1

Magnesium 21.0 1075-125mg/l2.0138 115 111 0.7

Manganese 1.00 1075-125mg/l0.0101.04 0.0902 95 2

Sodium 20.0 1075-125mg/l2.0458 434 118 2


Boron 1.00 1075-125mg/l0.205.36 4.22 114 2

Calcium 21.0 1075-125mg/l2.0396 M1363 154 1

Iron 1.00 1075-125mg/l0.0501.17 0.111 106 0.3

Magnesium 21.0 1075-125mg/l2.0127 102 120 1

Manganese 1.00 1075-125mg/l0.0100.949 0.0190 93 2

Sodium 20.0 1075-125mg/l2.0465 M1420 225 3

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

DISSOLVED METALS


Data

Qualifiers



Iron mg/l0.050ND


Iron mg/l0.050ND

LCS Analyzed: 01/22/2010 (10A0620-BS1)

Iron 1.00 85-115mg/l0.0500.983 98


Iron 1.00 2085-115mg/l0.0500.976 98 0.7


Iron 1.00 75-125mg/l0.0500.966 ND 97


Iron 1.00 75-125mg/l0.0502.83 1.76 107


Iron 1.00 1075-125mg/l0.0500.957 ND 96 0.9


Iron 1.00 1075-125mg/l0.0502.92 1.76 117 3

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Chloride mg/l2.0ND


Sulfate mg/l2.0ND

LCS Analyzed: 01/20/2010 (10A0584-BS1)


Nitrate-N 4.00 90-110mg/lNA4.12 103

Sulfate 20.0 90-110mg/lNA20.9 N1a104


Chloride 20.0 1590-110mg/lNA20.2 N1a101 0.1

Nitrate-N 4.00 1590-110mg/lNA4.14 103 0.2

Sulfate 20.0 1590-110mg/lNA20.9 N1a104 0.1


Nitrate-N 4.00 80-120mg/l0.2014.2 10.4 94


Chloride 100 80-120mg/l10484 397 87

Nitrate-N 20.0 80-120mg/l1.044.7 23.5 106

Sulfate 100 80-120mg/l10164 56.0 108


Nitrate-N 4.00 1580-120mg/l0.2014.1 10.4 92 0.4


Chloride 100 1580-120mg/l10483 397 86 0.3

Nitrate-N 20.0 1580-120mg/l1.044.5 23.5 105 0.4

Sulfate 100 1580-120mg/l10163 56.0 107 0.4

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers




LCS Analyzed: 01/21/2010 (10A0616-BS1)

Ammonia-N 10.0 85-115mg/l0.509.81 98


Ammonia-N 10.0 2085-115mg/l0.509.69 97 1


Ammonia-N 10.0 70-130mg/l0.508.96 0.390 86


Ammonia-N 10.0 2070-130mg/l0.509.08 0.390 87 1








LCS Analyzed: 01/26/2010 (10A0693-BS1)



Alkalinity as CaCO3 250 2090-110mg/l6.0256 102 0.1

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Alkalinity as CaCO3 20mg/l6.0193 192 0.5

Bicarbonate Alkalinity as CaCO3 20mg/l6.0193 192 0.5












Chloride mg/l2.0ND

Sulfate mg/l2.0ND

LCS Analyzed: 01/25/2010 (10A0700-BS1)

Chloride 20.0 90-110mg/lNA19.3 96

Sulfate 20.0 90-110mg/lNA19.7 99


Chloride 20.0 1590-110mg/lNA19.3 96 0.02

Sulfate 20.0 1590-110mg/lNA19.7 99 0.02

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Chloride 20.0 80-120mg/l2.096.5 79.6 84

Sulfate 20.0 80-120mg/l2.037.2 16.9 102


Chloride 20.0 80-120mg/l2.043.5 23.6 100

Sulfate 20.0 80-120mg/l2.072.3 54.3 90


Chloride 20.0 1580-120mg/l2.096.3 79.6 83 0.1

Sulfate 20.0 1580-120mg/l2.036.8 16.9 100 1


Chloride 20.0 1580-120mg/l2.043.7 23.6 100 0.3

Sulfate 20.0 1580-120mg/l2.072.5 54.3 91 0.2




LCS Analyzed: 01/25/2010 (10A0701-BS1)





Perchlorate 15ug/l2.02.72 R93.56 27

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers





Perchlorate 25.0 80-120ug/l2.021.6 0.878 83


Perchlorate 25.0 80-120ug/l2.023.9 2.02 88


Perchlorate 25.0 1580-120ug/l2.021.8 0.878 84 1


Perchlorate 25.0 1580-120ug/l2.023.8 2.02 87 0.3




LCS Analyzed: 01/29/2010 (10A0882-BS1)



Phosphorus,Total - P 0.300 2090-110mg/l0.100.327 109 0.3


Phosphorus,Total - P 0.300 80-120mg/l0.502.34 2.08 87

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers




Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers




LCS Analyzed: 01/26/2010 (10A0725-BS1)


LCS Analyzed: 01/26/2010 (10A0725-BS2)









Total Organic Carbon 20.0 2080-120mg/l1.019.7 0.731 95 2






Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 01/28/2010 (10A0843-BS1)


LCS Analyzed: 01/28/2010 (10A0843-BS2)





Total Organic Carbon 30.0 2080-120mg/l1.029.3 98 0.5


Total Organic Carbon 20.0 80-120mg/l1.018.8 ND 94




Total Organic Carbon 20.0 2080-120mg/l1.018.4 ND 92 3


Total Organic Carbon 20.0 2080-120mg/l1.019.9 1.86 90 0.3

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorate ug/l20ND

Chlorite ug/l20ND



LCS Analyzed: 01/29/2010 (10A2918-BS1)

Chlorate 100 75-125ug/l2097.7 98

Chlorite 100 75-125ug/l2097.8 98




Chlorate 240 75-125ug/l200307 90.0 90

Chlorite 240 75-125ug/l200218 ND 91




Chlorate 240 75-125ug/l200316 93.1 93

Chlorite 240 75-125ug/l200206 ND 86




Chlorate 240 2575-125ug/l200301 90.0 88 2

Chlorite 240 2575-125ug/l200213 ND 89 2



Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorate 240 2575-125ug/l200302 93.1 87 5

Chlorite 240 2575-125ug/l200211 ND 88 3





Chlorite ug/l20ND


LCS Analyzed: 01/31/2010 (10A3035-BS1)

Chlorite 100 75-125ug/l2095.6 96



Chlorite 100 75-125ug/l40101 ND 101



Chlorite 100 2575-125ug/l4095.5 ND 95 5


Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00


B1 Target analyte detected in method blank at or above the method reporting limit.








R9 Sample RPD exceeded the laboratory acceptance limit


S6 Surrogate recovery was below laboratory and method acceptance limits. Reextraction and/or reanalysis confirms low

recovery caused by matrix effect.




Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily




454-9303





Sampled:

Received:

01/20/10


Project ID:

PTA0936

PGA North/103965.00



TestAmerica Phoenix

Water XE200.7

Water XEPA 300.0

Water XEPA 314.0

XWater XEPA 8260B

Water XM2320 B

Water XM4500-P B, E

Water XM5310B

WaterSM 4500-P B, E

Water XSM4500-NH3D






Analysis Performed: HydrogenSamples: PTA0936-01, PTA0936-03, PTA0936-09



Method Performed: EPA 300.1Samples: PTA0936-01, PTA0936-03, PTA0936-07

Project Manager

TestAmerica Phoenix

PTA0936

Kylie Emily



SENDING LABORATORY;

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 189 Phoenix, AZ 85040 Phone: (602) 437 ~3340

Fax: (602) 454~9303 Project Manager: Kylie Emily Client: Environmental Resources Management lnc.-West


PTA0936

RECEIVING LA BORA TORY:

TestAmerica Irvine

17 461 Derian Ave. Suite 1 00 Irvine, CA 92614 Phone :(949) 261~1022

Fax: (949) 261~1228 Project Location: AZ ~ARIZONA Receipt Temperature: \ · ~ oc Ice:

Analysis Units Due Expires lnte'rlab Price Surch Comments

Sample ID; PTA0936-01 (IRZ-IW-02-01202010 ·Water) Sampled: 01120110 OS:30

Chlorate (300.1) mg/1 02/04/10 02/17/10 09:30 $30.00 0%

Chlorite (300.1)- 0 mg/1 02/04/10 02/03/10 09:30 $30.00 0%


500 ml Poly w/EDA (L) 125ml Brown Poly w/ EDA M

Sample ID: PTA0936-03 (IRZ-IW-01-01202010 ·Water) Sampled: 0112011011 :25 Chlorate (300.1) mg/1 02/04/10 02/17/1011:25 $30.00 0%

Chlorite (300.1) - 0 mg/1 02/04/10 02/03/1 0 11 :25 $30.00 0%


500 ml Poly w/EDA (L) 125ml Brown Poly w/ EDA(M

Sample ID: PTA0936-07 (IRZ-IW-04-01202010- Water) Sampled: 01120110 14:35 Chlorate (300.1) mg/1 02/04/10 02117110 14:35 $30.00

Chlorite (300.1) - 0 mg/1 02/04/10 02/03/10 14:35


500 ml Poly w/EDA (L) 125ml Brown Poly w/ EDA M

$30.00

0%

0%

_____,__,.,.?ifb---+----_ 1 £, f, l"f<'D Fe lsv 0 (- l:t -;o / t-:.oZJ Released By Dateffime Received By Dateffime

Released By Daterrime

~ \\1-)-(lo I\~\'" ----~~~------------~ Datem~ Page 1 of 1

. 1\ ~00'\ Received By


TAL-0013-550 (12/08) ,... { 1 Jl fl

Project Manager:Vo..-u-\G. eJ.t\M-j

Sampler:3. ~\'v-..- /11 ...SGh"'N\.'-{_Iu,__


L·\


[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ. 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ. 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Phone Number:

\f ~ -'l 'iS _ztt-o I Fax Numbe~ 17 <7! f 4 ;pi - <: 'f ~ - 1... ~\1

#of Cont.

Sampling Sampling Preservatives Date Time

Analysis Required

I~

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Reli/~ecf)B>j. ~ / ·\I <"J.I~~tel~ime~,( t. ( Received By: Date/Time: Turnaround Time: (Check)

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JL _ _L ( _ ) 1 L 48 hours normal

. lielinquished By: Date/Time: tyceived in)-a~ Daf{=!fime:j Sample Integrity: (Check)

/ ' I~ I /.:Ze /,o rr.;;_; intact V' on ice

Note: By relinquishing samples lei TestAmerica, client agrees to pay for the--servites ';'equ~sted on this chain of custod~ form1 and any additional analyses performed on this project.

Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.


TAL-0013-550 (12/08)


seQ_ t~L :1

Project Manager:

Sampler:~ {)6---..)L l "


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[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798"3620 FAX (702) 798-3621

Project/ PO Number: .T Analysis Required ~ :!;.:t

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Phone Number: ~-- - t .j ~ 5!. ~ g~ ---6 VI l.. lJ 1 :>::. ' Cl 0 ~~ ::L

Fax Number: -'") 0 1 k-'z ~ rl--~ r:_jl_ ~ ·r. -S $. J. rl. og - v-. --1 :--- 0 0 cE ~6 3 -#of Sampling Sampling

Preservatives o<l G8 ;;Jj ~ {) ~ Cont. Date Time N :;f:~

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Date/Time: Turnaround Time: (Check) fJ(i. iv flo~~ e. ty-:z same day 72 hours

R1uishkldlBy: Date/Time: ~vedBy: Date/Time: 24 hours 5 days

/ ("'\ 48 hours normal

Ffelinquished By: Date/Time: { R~bBy: Date/Time~ /,, Sample Integrity: (Check) #(L<l.. 0, :;).

1 Zo /b t 1---~ lfntact 0 on ice ~ _..., _-/

Note: B relin uishing sam les to TestAmerica, client agrees to a for the services le uested on this chain of custod form ahd an ~dditional analyses performed on this pro·ect. y q p py q y y Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

~--~---------------- ---------

TestAmerica THE LEADER IN ENVIRONMENTAL TESTING

TAL-0013-550 (12/08)


.s~ ~L:tJ-L ~ "'<:-

Project Manager:


[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Project/ PO Number:

.......

Phone Number:

Analysis Required

Sampler: ~ ~ , ~ber:

c2 Q

..3 Sample Description

Sample Container #of Sampling Matrix Type Cont. Date

Sampling . r( Time Preservatives o0

DL l- -~ -~4 -o l 7-o ]$;) 1<0 ~ V0A- 3 rh.,,IJ o

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Relinqu#d fN':J//l-- \ . pate/Time: Received By: Date/Time: Turnaround Time: (Check)

!/' I 'iflAJ 11Pl L 0 .e__ r7: ~ ( L ~ same day ---~~~~~------------------L-~--~~~--~--~~~~~------------------~~~--------------4 Relijquishe'd By: Date/Time: R*ived B"y: Date/Time: 24 hours

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72 hours __ _

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normal

Relinquished By: Date /Time: /_ ~ ed v Lab By: - l k:at1', T~me: In I ~::~le ln~y: on ice

Note: By relinqui~hin~ sample_s t_o TestAmerica, client agree~ to ?ay for the s~rv~es ~equested on this chain of custodt form and any additional analyses perf6rmed on this project. Payment for serv1ces IS due w1th1n 30 days from the date of mvo1ce. Sample(s) Will be disposed of after 30 days.

-----------------~ ---~·- ----


P1001276-02

P1 001276-03



Report Date: 02/08/10 Client Proj Name: PTA0936

Client Proj #: PT A0936 Suite 189 Phoenix, AZ 85040

Client Sample ID PTA0936-01

PTA0936-03

PTA0936-09

Laboratory Results Total pages in data package: q

Mlcroseeps test results meet all the requirements of the NELAC standards or provide reasons and/or justification if they do not.

Approved By: (fhf)

Proiect Manager: Debbie Halla

The analytical results reported here are reliable and usable to the precision expressed in this report. As required by some regulating authorities, a full discussion of the uncertainty in our analytical results can be obtained at our web site or through customer service. Unless otherwise specified, all results


Case Narrative:

As a valued client we would appreciate your comments on our service. Please call customer service at (412)826-5245 or email [email protected].





Sam(;!le Descrigtion Matrix Lab Sample#


Report Date: 02/08/1 0 Client Proj Name: PTA0936


Samgled Date/Time Received PTA0936-01 Vapor P1001276-01 20Jan.10 9:30 22 Jan. 10 15:38


Data Qualifiers: 1- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovcry/RPD poor for MS/MSD, SAMP/DuP, B- detected in blank, S - field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N • NELAC certified analysis

By

sl



SamQie DescriRtion Matrix Lab Sample#




SamRied Date/Time Received PTA0936-03 Vapor P1 00 12 76-02 20 Jan. 10 11:25 22 Jan. 10 15:38


Data Qualifiers: J ·estimated value, U ·Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, s'AMP/DUP, B - detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L - Subcontracted Lab used, N- NELAC certified analysis

By

sl



Sam[;!le Descrigtion Matrix Lab Sample#




Samgled Date/Time Received PTA0936-09 Vapor P1 001276-03 20 Jan. 10 15:30 22 Jan. 1 o 15:38


Data Qualifiers: J- estimated value, U ·Non detect, R- Poor surrogate recovery, M - Recovery/RPD poor for MS/M:SD, SAMPfDUP, B- detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L - Subcontracted Lab used, N- NELAC certified analysis

By

sl


Address: 4625 East Cotton Center Blvd. Suite 189 Phoenix, AZ. 85040

Prep Method:

Analysis Method:

M100203011-MB

Result TrueSpikeConc. RDL


M100203011-LCS



M1 00203011-LCSD








~Recove(Y Ctl Limits

- NA

%RecoverY Ctl Limits

101.00 75-125

%Recove(Y Ctl Limits RPD

101.00 75- 125 0.00

RPD Ctl Limits

0-20

.__ ___ ---ll Outlined Results Indicate results outside of Control limits

Data Qualifiers: J- estimated value, U -Non detect, R- Poor surrogate recovery, M - Recovery/RPD poor for MS/MSD, SAMPIDUP, B - detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N · NELAC certified analysis

SUBCONTRACT ORDER TestAmerica Pho1:1nix

SENDING LABORATORY:

TestAmerica Phoenix 4625 East Cotton Center Blvd. Ste 189 Phoenix, AZ. 85040 Phone: (602) 437-3340 Fax: (602) 454-9303 Project Manager: Kylie Emily

PTA0936


Microseeps/Univ of Pittsburgh App Research Center · 220 William Pitt Way

Pittsburgh, PA 15238 Phone :(412)826-5245 Fax: (412)826-3433 Project Location: AZ.- ARIZONA Receipt Temperature: oc Ice: Y I N

Standard TAT is requested unless specific due date is requested. => Due Date: ---- Initials: ___ _

Analysis Units

Sample ID: PTA0936-01 (IRZ-IW-02-01202010- Water)

Hydrogen


NA (N)

%

Sample ID: PTA0936-03 (IRZ-IW-01·01202010 ·Water)

Hydrogen


NA (N)

%

Sample ID: PTA0936·09 {IRZ-IW-04-01202010 ·Water)

Hydrogen


NA (A)

Released By

%

Expires Comments

Sampled: 01/20/10 09:30 02117110 09:30 Microseeps

Sampled: 01/20/1011:25 02/17/10 11:25 Microseeps

Sampled: 01/20/1 o 15:30 02/17/10 15:30 Microseeps

Page 1 of 1

rest America THE LEADER IN ENVIRONMENTAL TESTING

~L-0013·550 {12/08) ~ { 1 h n

Project Manager: v CA.v\c.. eVV'•'-5

Sampler:]. \-h\~/li ..Sch..-.N\.>.(.L

Sample Container


[]Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, /l:Z. 85040 {602) 437-3340 FAX (602) 454-9303 [ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520} 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

rt- Analysis Required

Phone Number:

'{~ -'1.CtJ-llf-o l Fax 4';1l_:~ f f -11 t':l~

A\Pagej__ of J \l

Sample Description Matrix Type #of Cont.

Sampling Sampling Preservatives Date lime Special! nstructions

\ \_

I

\L -1

I

Received By: Date/Time: Turnaround Time: (Check)

/\ same day 72 hours __ _

.Receijed . .ftZ= B : Date/Time: 24 hours 5 days

/ .I ) r 1 48 hours normal

fl~linquished By: Date/Time: ~ceived~· Da~?'ime:j Sample Integrity: (Check)

_/ · I 'l... / j.:Z.c. LLO ( 'f-;z..L intact 0 on ice

Note: By relinquishing samples to TestAmerica, client agrees to pay for th-e-serviles ';equ~sted on this chain of custod; form1 and any additional analyses performed on this project.

Payment lor services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

-- ~------------~--~--- ----~---------

!).).

3 -1.:)(

fest America THE LEADER IN ENVIRONMENTAL TESTING

A~-o0\3·550 (12106)


SE:.Q_ f~L 1,

Project Manager;

Sampler: c;.ee_. ~(}-..s..e... ']_


bL.i:-JI.v -o ~ - o tz.<l2.o 1 o HY-o \1\)f\--\ 9P I""'L

\ II ...


( ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, f!IZ 85040 (602) 437-3340 FAX {602) 454-9303 [ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 ( ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 8~120 (702) 798"3620 FAX (702) 798-3521

Project! PO Number: I Analysis Required 1.,.-f-

~:i ? -~n .Jcl. ~.:- ...t

j. :lc:~~ i __<2. 1 Phone Number: 'j'J ,-

'2 ;:;! ~ ~~ -6 Vl

d 0 lJ 1 l) ~ 3{ Fax Number: ~ Q ~ ~z~ ~~

r::..Y. ~ ·r. ...3 j,J_ ('i,.

~!j • v-.. 0 J

cE jo 3 .,.. .5 -#of Sampling Sampling Preservatives o<J

~2 -{; -5 F-Cont Date lime

3 \1-u- [0 \\ ~£...) 'A-c-~ K --1-- _l\'::lt-fL- )!

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.s\9~1'l"L. BPfr K !tJ \1£"'"'~ lr J?PPr K ero~ p-o\y I V1>A t.{ ~ K 1\IY'\u---. Vol\- I

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Relin;xed 7JfJ- ./ >} Date/Time: ~( L7dBy: Date/Time: Turnaround Time: (Check} ~I

\. 2o { .:> .e. cr:z same day 72 hours

R1uis!WctlBy: Date/Time: ~~dBy: Date/Time: 24 hours 5 days

/ 48 hours normal

Ffe!inquished By: Date/Time: .( Re~bBy: ' Date/Time~ I. Sample Integrity: (Check) ~ ·• r.· . lfntact 0 0, .?-

t ..P.c f¢ t 1--.J.. on ice tt! ·""(. _/ !2'

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services /equested on this chain.of custody form a~d any ~dditional analyses performed on this project. Pa.yment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

r estAmerica CHAIN OF CUSTODY FORM

THE LEADER IN ENVIRONMENTAL TESTING

1\L-0013·550 (12/0S)

[ 1 Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix; AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ 1 Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ 1 Las Vegas - 2520 E. Sunset, Suite 3, las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621 ,1 Page Z of -']

:::nent Name I Address:

.s~ ~U.Jl ~ ...,-

Project Manager:

~ Sampler:

Project/ PO Number:

...._______ Phone Number:

~ber:

Sample Container #of Sampnng

c2 Q

..3 Sampling . rl..

Analysis Required

Sample Description Matrix Type Cont Date Time Preservatives o0 Special Instructions

~'2. -~ -~~:.4 -Ol 7-c"b 10 \\~ V0A- 3 tiP!Jo I ~L j__ \ \

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l\ n~pLa~e/:ime1: -r./l( Received By: Date/Time: Turnaround lime: (Check) LPL -v ..oc:... 1 l-- tb same day 72 hours __ _

Retiz<iuishe'd By: Date/lime: VR~ived By: Date/Time: 24 hours 5 days

/ r \ r 48 hours normal

Relinquished By: Date/lime: /_ ~~~ ed ~Lab By: / Datef!Time: Sample Integrity: (Check)

- - [ .12:, I , 0 I n I intact '\L"_ on ice

Note: By relinqui~hin~ sample_s t_o TestAmerica, client agree~ to pay for the servi~es~equested on this chain_of custod§ form and any additional analyses per!~rmed on this project. Payment tor services IS due WJthm 30 days from the date of mvo1ce. Sample(s) Wlll be d1sposed of after 30 days.

V· ;J. <><

I ' .X: \/ -~./

/


454-9303

LABORATORY REPORT





Received:

Issued:

03/03/10

03/03/10

03/23/10 09:44









CASE NARRATIVE


PTC0221-01 IRZ-MW-D-115-03032010 Water

PTC0221-02 IRZ-MW-D-125-03032010 Water

PTC0221-03 IRZ-MW-C-115-03032010 Water

PTC0221-04 IRZ-MW-C-125-03032010 Water

PTC0221-05 IRZ-IW-5-03032010 Water

PTC0221-06 IRZ-IW-5-03032010 Water

PTC0221-07 IRZ-IW-5-03032010R Water

PTC0221-08 IRZ-IW-4-03032010 Water

PTC0221-09 IRZ-IW-4-03032010 Water

PTC0221-10 Trip Blank Water

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily

<Page 1 of 49>


454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00









N1a-300.0-Results exceeded the linear range in the MS/MSD and therefore are not available for reporting.


N1a-8260- Sample PTC0221-10RE1 was analyzed with headspace for Trichloroethene. The original run of

the sample had TCE carryover from the sample run just before it. The sample is a Trip blank therefore

there were no other vials available to use for the rerun.



Reviewed By:

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-01 (IRZ-MW-D-115-03032010 - Water) Sampled: 03/03/10


Acetone 3/12/20103/12/201010C0480 10 1EPA 8260B 17

Benzene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 4.4

3/12/20103/12/2010EPA 8260BBromobenzene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BBromochloromethane 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BBromodichloromethane 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BBromoform 1.010C0480 1ND

3/12/20103/12/2010EPA 8260BBromomethane 1.010C0480 1ND

3/12/20103/12/2010EPA 8260B2-Butanone (MEK) 2.510C0480 1ND

3/12/20103/12/2010EPA 8260Bn-Butylbenzene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260Bsec-Butylbenzene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260Btert-Butylbenzene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BCarbon disulfide 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BCarbon tetrachloride 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BChlorobenzene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BChloroethane 1.010C0480 1ND

3/12/20103/12/2010EPA 8260BChloroform 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BChloromethane 1.010C0480 1ND

3/12/20103/12/2010EPA 8260B2-Chlorotoluene 0.5010C0480 1ND


3/12/20103/12/2010EPA 8260BDibromochloromethane 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260B1,2-Dibromo-3-chloropropane 2.510C0480 1ND

3/12/20103/12/2010EPA 8260B1,2-Dibromoethane (EDB) 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BDibromomethane 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260B1,2-Dichlorobenzene 0.5010C0480 1ND



3/12/20103/12/2010EPA 8260BDichlorodifluoromethane 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260B1,1-Dichloroethane 0.5010C0480 1ND


3/12/20103/12/2010EPA 8260B1,1-Dichloroethene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260Bcis-1,2-Dichloroethene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260Btrans-1,2-Dichloroethene 0.5010C0480 L31ND

3/12/20103/12/2010EPA 8260B1,2-Dichloropropane 0.5010C0480 1ND



3/12/20103/12/2010EPA 8260B1,1-Dichloropropene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260Bcis-1,3-Dichloropropene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260Btrans-1,3-Dichloropropene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BEthylbenzene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BHexachlorobutadiene 1.010C0480 1ND

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-01 (IRZ-MW-D-115-03032010 - Water) - cont. Sampled: 03/03/10


3/12/20103/12/2010EPA 8260B2-Hexanone 2.510C0480 1ND

3/12/20103/12/2010EPA 8260BIodomethane 2.510C0480 1ND

3/12/20103/12/2010EPA 8260BIsopropylbenzene 0.5010C0480 L31ND

3/12/20103/12/2010EPA 8260Bp-Isopropyltoluene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BMethylene Chloride 1.010C0480 1ND

3/12/20103/12/2010EPA 8260B4-Methyl-2-pentanone (MIBK) 2.510C0480 1ND

3/12/20103/12/2010EPA 8260BMethyl-tert-butyl Ether (MTBE) 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BNaphthalene 2.510C0480 1ND

3/12/20103/12/2010EPA 8260Bn-Propylbenzene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BStyrene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260B1,1,1,2-Tetrachloroethane 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260B1,1,2,2-Tetrachloroethane 0.5010C0480 L31ND

3/12/20103/12/2010EPA 8260BTetrachloroethene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BToluene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260B1,2,3-Trichlorobenzene 1.010C0480 1ND


3/12/20103/12/2010EPA 8260B1,1,1-Trichloroethane 0.5010C0480 1ND


Trichloroethene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 53

3/12/20103/12/2010EPA 8260BTrichlorofluoromethane 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260B1,2,3-Trichloropropane 1.010C0480 1ND

3/12/20103/12/2010EPA 8260B1,2,4-Trimethylbenzene 0.5010C0480 L31ND

3/12/20103/12/2010EPA 8260B1,3,5-Trimethylbenzene 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BVinyl Acetate 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BVinyl chloride 0.5010C0480 1ND

3/12/20103/12/2010EPA 8260BXylenes, Total 1.010C0480 1ND




Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-02 (IRZ-MW-D-125-03032010 - Water) Sampled: 03/03/10


Acetone 3/12/20103/12/201010C0480 10 1EPA 8260B 18

Benzene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 3.7







































Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-02 (IRZ-MW-D-125-03032010 - Water) - cont. Sampled: 03/03/10











3/12/20103/12/2010EPA 8260BStyrene 0.5010C0480 1ND




3/12/20103/12/2010EPA 8260BToluene 0.5010C0480 1ND
















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-03 (IRZ-MW-C-115-03032010 - Water) Sampled: 03/03/10


Acetone 3/12/20103/12/201010C0480 10 1EPA 8260B 22

Benzene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 73







































Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-03 (IRZ-MW-C-115-03032010 - Water) - cont. Sampled: 03/03/10











3/12/20103/12/2010EPA 8260BStyrene 0.5010C0480 1ND




3/12/20103/12/2010EPA 8260BToluene 0.5010C0480 1ND
















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-04 (IRZ-MW-C-125-03032010 - Water) Sampled: 03/03/10


Acetone 3/12/20103/12/201010C0480 10 1EPA 8260B 17

Benzene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 41




Bromoform 3/12/20103/12/201010C0480 1.0 1EPA 8260B 1.0



































Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-04 (IRZ-MW-C-125-03032010 - Water) - cont. Sampled: 03/03/10











3/12/20103/12/2010EPA 8260BStyrene 0.5010C0480 1ND




3/12/20103/12/2010EPA 8260BToluene 0.5010C0480 1ND
















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-05 (IRZ-IW-5-03032010 - Water) Sampled: 03/03/10


3/12/20103/12/2010EPA 8260BAcetone 1010C0480 1ND

Benzene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 0.51










Carbon disulfide 3/12/20103/12/201010C0480 0.50 1EPA 8260B 0.71




Chloroform 3/12/20103/12/201010C0480 0.50 1EPA 8260B 0.82














1,1-Dichloroethene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 1.6

cis-1,2-Dichloroethene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 3.2










Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-05 (IRZ-IW-5-03032010 - Water) - cont. Sampled: 03/03/10











3/12/20103/12/2010EPA 8260BStyrene 0.5010C0480 1ND



Tetrachloroethene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 0.68

3/12/20103/12/2010EPA 8260BToluene 0.5010C0480 1ND















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-05RE1 (IRZ-IW-5-03032010 - Water) - cont. Sampled: 03/03/10


Trichloroethene 3/15/20103/15/201010C0520 50 100EPA 8260B 1800




Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-07 (IRZ-IW-5-03032010R - Water) Sampled: 03/03/10


3/12/20103/12/2010EPA 8260BAcetone 1010C0480 1ND

3/12/20103/12/2010EPA 8260BBenzene 0.5010C0480 1ND



Bromodichloromethane 3/12/20103/12/201010C0480 0.50 1EPA 8260B 1.8















Dibromochloromethane 3/12/20103/12/201010C0480 0.50 1EPA 8260B 0.77





















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-07 (IRZ-IW-5-03032010R - Water) - cont. Sampled: 03/03/10











3/12/20103/12/2010EPA 8260BStyrene 0.5010C0480 1ND




3/12/20103/12/2010EPA 8260BToluene 0.5010C0480 1ND















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-07RE1 (IRZ-IW-5-03032010R - Water) - cont. Sampled: 03/03/10


3/15/20103/15/2010EPA 8260BTrichloroethene 0.5010C0520 1ND




Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



3/12/20103/12/2010EPA 8260BAcetone 1010C0480 1ND

3/12/20103/12/2010EPA 8260BBenzene 0.5010C0480 1ND




























1,1-Dichloroethene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 1.1

cis-1,2-Dichloroethene 3/12/20103/12/201010C0480 0.50 1EPA 8260B 2.3










Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result












3/12/20103/12/2010EPA 8260BStyrene 0.5010C0480 1ND




3/12/20103/12/2010EPA 8260BToluene 0.5010C0480 1ND















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result







Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-10 (Trip Blank - Water) Sampled: 03/03/10


3/12/20103/12/2010EPA 8260BAcetone 1010C0480 1ND

3/12/20103/12/2010EPA 8260BBenzene 0.5010C0480 1ND







































Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-10 (Trip Blank - Water) - cont. Sampled: 03/03/10











3/12/20103/12/2010EPA 8260BStyrene 0.5010C0480 1ND




3/12/20103/12/2010EPA 8260BToluene 0.5010C0480 1ND















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0221-10RE1 (Trip Blank - Water) - cont. Sampled: 03/03/10 N1a


3/15/20103/15/2010EPA 8260BTrichloroethene 0.5010C0520 Q21ND




Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 3/5/20103/4/201010C0190 0.10 2E200.7 500

Manganese 3/5/20103/4/201010C0190 0.010 1E200.7 3.3

Sodium 3/5/20103/4/201010C0190 2.0 1E200.7 420



Iron 3/5/20103/4/201010C0190 0.050 1E200.7 100

Manganese 3/5/20103/4/201010C0190 0.010 1E200.7 0.67

Sodium 3/5/20103/4/201010C0190 2.0 1E200.7 460

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

DISSOLVED METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 3/8/20103/5/201010C0276 0.050 1E200.7 3.3



Iron 3/8/20103/5/201010C0276 0.050 1E200.7 1.6

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Alkalinity as CaCO3 3/4/20103/4/201010C0223 6.0 1M2320 B 190

Bicarbonate Alkalinity as CaCO3 3/4/20103/4/201010C0223 6.0 1M2320 B 190

3/4/20103/4/2010M2320 BCarbonate Alkalinity as CaCO3 6.010C0223 1ND

3/4/20103/4/2010M2320 BHydroxide Alkalinity as CaCO3 6.010C0223 1ND

Nitrate-N 3/4/20103/3/201010C0159 1.0 5EPA 300.0 12

Phosphate 3/10/20103/10/201010C0404 0.30 1SM 4500-P B, E 160

Phosphorus,Total - P 3/9/20103/8/201010C0379 10 100M4500-P B, E 52

3/4/20103/4/2010M2320 BAlkalinity, Phenolphthalein 6.010C0223 1ND



Perchlorate 3/11/20103/10/201010C0354 4.0 2EPA 314.0 7.8

Sample ID: PTC0221-05RE1 (IRZ-IW-5-03032010 - Water) Sampled: 03/03/10


Chloride 3/4/20103/4/201010C0208 40 20EPA 300.0 800

Sulfate 3/4/20103/4/201010C0208 40 20EPA 300.0 1000







Nitrate-N 3/4/20103/3/201010C0159 1.0 5EPA 300.0 7.7


Phosphorus,Total - P 3/9/20103/8/201010C0379 1.0 10M4500-P B, E 5.1




Perchlorate 3/11/20103/10/201010C0354 4.0 2EPA 314.0 14



Chloride 3/4/20103/4/201010C0208 40 20EPA 300.0 810

Sulfate 3/4/20103/4/201010C0208 40 20EPA 300.0 1100

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



Total Organic Carbon 3/9/20103/9/201010C0336 1.0 1M5310B 1.4




Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



3/11/20103/11/2010EPA 300.1Chlorate 4010C1438 D12ND

3/11/20103/11/2010EPA 300.1Chlorite 20010C1438 D110ND




3/11/20103/11/2010EPA 300.1Chlorate 4010C1438 D12ND



Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: IRZ-IW-5-03032010 (PTC0221-05) - Water

2 03/03/2010 12:10 03/03/2010 16:52 03/03/2010 17:30 03/04/2010 04:11EPA 300.0


2 03/03/2010 14:40 03/03/2010 16:52 03/03/2010 17:30 03/04/2010 04:39EPA 300.0

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

Batch: 10C0480 Extracted: 03/12/10

Blank Analyzed: 03/12/2010 (10C0480-BLK1)

Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 03/12/2010 (10C0480-BS1)

Acetone 25.0 10-150ug/l1029.2 117

Benzene 25.0 80-120ug/l0.5026.5 106




Bromoform 25.0 75-130ug/l1.028.4 114


2-Butanone (MEK) 25.0 40-150ug/l2.526.2 105








Chloroform 25.0 75-120ug/l0.5024.9 100




















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 03/12/2010 (10C0480-BS1)






2-Hexanone 25.0 20-150ug/l2.529.5 118

Iodomethane 25.0 80-130ug/l2.524.0 96






Naphthalene 25.0 40-150ug/l2.524.9 100


Styrene 25.0 80-120ug/l0.5023.2 93




Toluene 25.0 80-120ug/l0.5026.5 106
















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Dup Analyzed: 03/12/2010 (10C0480-BSD1)

Acetone 25.0 3510-150ug/l1034.6 138 17

Benzene 25.0 1580-120ug/l0.5027.6 110 4




Bromoform 25.0 2075-130ug/l1.029.9 120 5


2-Butanone (MEK) 25.0 3540-150ug/l2.528.3 113 8








Chloroform 25.0 1575-120ug/l0.5027.8 111 11
















trans-1,2-Dichloroethene 25.0 1580-120ug/l0.5030.5 L3122 12




Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3520-150ug/l2.533.4 134 13

Iodomethane 25.0 1080-130ug/l2.527.3 R6109 13

Isopropylbenzene 25.0 1580-130ug/l0.5033.0 L3132 4





Naphthalene 25.0 3040-150ug/l2.529.2 117 16


Styrene 25.0 1580-120ug/l0.5026.8 107 15


1,1,2,2-Tetrachloroethane 25.0 2080-120ug/l0.5030.5 L3122 9


Toluene 25.0 1580-120ug/l0.5027.5 110 4








1,2,4-Trimethylbenzene 25.0 1580-120ug/l0.5030.1 L3121 5








Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 03/12/2010 (10C0480-MS1) Source: PTC0254-29

Acetone 25.0 10-150ug/l1027.8 3.33 98

Benzene 25.0 70-125ug/l0.5025.9 ND 104




Bromoform 25.0 65-125ug/l1.026.5 ND 106























1,2-Dichloroethane 25.0 65-140ug/l0.5026.9 0.200 107







Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.526.8 ND 107




Methylene Chloride 25.0 65-130ug/l1.025.0 0.170 99





Styrene 25.0 55-135ug/l0.5022.9 ND 91




Toluene 25.0 70-125ug/l0.5026.4 ND 106
















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 03/12/2010 (10C0480-MSD1) Source: PTC0254-29

Acetone 25.0 3510-150ug/l1026.4 3.33 92 5

Benzene 25.0 2570-125ug/l0.5026.0 ND 104 0.4



Bromodichloromethane 25.0 2075-125ug/l0.5027.0 ND 108 0.4

Bromoform 25.0 2565-125ug/l1.027.3 ND 109 3














Dibromochloromethane 25.0 2070-130ug/l0.5026.0 ND 104 0.6


1,2-Dibromoethane (EDB) 25.0 2070-125ug/l0.5026.5 ND 106 0.5






1,1-Dichloroethane 25.0 2070-130ug/l0.5027.8 ND 111 0.04

1,2-Dichloroethane 25.0 2065-140ug/l0.5025.9 0.200 103 4







Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 2565-130ug/l0.5028.4 ND 114 0.5





2-Hexanone 25.0 3020-150ug/l2.527.1 ND 108 1




Methylene Chloride 25.0 2065-130ug/l1.025.4 0.170 101 2





Styrene 25.0 3555-135ug/l0.5023.8 ND 95 4




Toluene 25.0 2070-125ug/l0.5027.0 ND 108 2
















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Blank Analyzed: 03/15/2010-03/23/2010 (10C0520-BLK1)

Acetone ug/l10ND

Benzene ug/l0.50ND







LCS Analyzed: 03/15/2010 (10C0520-BS1)




















Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Iron mg/l0.050ND


Sodium mg/l2.0ND

LCS Analyzed: 03/05/2010 (10C0190-BS1)

Iron 1.00 85-115mg/l0.0500.918 92

Manganese 1.00 85-115mg/l0.0100.963 96

Sodium 20.0 85-115mg/l2.018.3 92


Iron 1.00 2085-115mg/l0.0500.945 94 3

Manganese 1.00 2085-115mg/l0.0100.990 99 3

Sodium 20.0 2085-115mg/l2.019.5 97 6


Iron 1.00 75-125mg/l0.0500.964 ND 96

Manganese 1.00 75-125mg/l0.0100.990 ND 99

Sodium 20.0 75-125mg/l2.041.7 21.2 102


Iron 1.00 1075-125mg/l0.0500.953 ND 95 1

Manganese 1.00 1075-125mg/l0.0100.983 ND 98 0.7

Sodium 20.0 1075-125mg/l2.040.3 21.2 95 3

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

DISSOLVED METALS


Data

Qualifiers



Iron mg/l0.050ND


Iron mg/l0.050ND

LCS Analyzed: 03/08/2010 (10C0276-BS1)

Iron 1.00 85-115mg/l0.0500.963 96


Iron 1.00 2085-115mg/l0.0500.978 98 2


Iron 1.00 75-125mg/l0.0501.49 0.484 100


Iron 1.00 1075-125mg/l0.0501.51 0.484 103 2

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Chloride mg/l2.0ND


Sulfate mg/l2.0ND

LCS Analyzed: 03/04/2010 (10C0159-BS1)


Nitrate-N 4.00 90-110mg/lNA3.84 96

Sulfate 20.0 90-110mg/lNA19.4 N1a97



Nitrate-N 4.00 1590-110mg/lNA3.83 96 0.3

Sulfate 20.0 1590-110mg/lNA19.3 N1a97 0.4


Nitrate-N 4.00 80-120mg/l0.2010.1 6.22 98


Nitrate-N 4.00 1580-120mg/l0.2010.1 6.22 98 0.04



Chloride mg/l2.0ND

Sulfate mg/l2.0ND

LCS Analyzed: 03/04/2010 (10C0208-BS1)


Sulfate 20.0 90-110mg/lNA20.2 N1a101

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers




Sulfate 20.0 1590-110mg/lNA20.1 N1a101 0.3








LCS Analyzed: 03/04/2010 (10C0223-BS2)




Duplicate Analyzed: 03/04/2010 (10C0223-DUP1) Source: PTC0067-01












Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers




LCS Analyzed: 03/10/2010 (10C0354-BS1)



Perchlorate 25.0 1585-115ug/lNA23.9 96 0.6

Duplicate Analyzed: 03/10/2010 (10C0354-DUP1) Source: PTB1552-05

Perchlorate 15ug/l2.0ND ND

Duplicate Analyzed: 03/10/2010 (10C0354-DUP2) Source: PTB1552-14


Matrix Spike Analyzed: 03/10/2010 (10C0354-MS1) Source: PTB1552-06

Perchlorate 25.0 80-120ug/l2.026.3 2.59 95

Matrix Spike Analyzed: 03/10/2010 (10C0354-MS2) Source: PTB1552-17

Perchlorate 25.0 80-120ug/l2.023.2 ND 93

Matrix Spike Dup Analyzed: 03/10/2010 (10C0354-MSD1) Source: PTB1552-06

Perchlorate 25.0 1580-120ug/l2.028.1 2.59 102 6

Matrix Spike Dup Analyzed: 03/10/2010 (10C0354-MSD2) Source: PTB1552-17

Perchlorate 25.0 1580-120ug/l2.024.0 ND 96 3




Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers


LCS Analyzed: 03/09/2010 (10C0379-BS1)







Phosphorus,Total - P 0.300 2080-120mg/l0.502.09 M21.86 78 0.2

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers




LCS Analyzed: 03/09/2010 (10C0336-BS1)








Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorate ug/l20ND

Chlorite ug/l20ND


LCS Analyzed: 03/11/2010 (10C1438-BS1)

Chlorate 100 75-125ug/l20102 102

Chlorite 100 75-125ug/l2096.8 97


Matrix Spike Analyzed: 03/11/2010 (10C1438-MS1) Source: ITC0679-01

Chlorate 100 75-125ug/l20204 103 100

Chlorite 100 75-125ug/l2023.4 M2ND 23


Matrix Spike Dup Analyzed: 03/11/2010 (10C1438-MSD1) Source: ITC0679-01

Chlorate 100 2575-125ug/l20200 103 97 2

Chlorite 100 2575-125ug/l2020.5 M2ND 21 13


Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00










Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily




454-9303





Sampled:

Received:

03/03/10


Project ID:

PTC0221

PGA North/103965.00



TestAmerica Phoenix

Water XE200.7

Water XEPA 300.0

Water XEPA 314.0

XWater XEPA 8260B

Water XM2320 B

Water XM4500-P B, E

Water XM5310B

WaterSM 4500-P B, E






Analysis Performed: HydrogenSamples: PTC0221-05, PTC0221-08



Method Performed: EPA 300.1Samples: PTC0221-05, PTC0221-08

Project Manager

TestAmerica Phoenix

PTC0221

Kylie Emily



SENDING LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvdc. ~S!~t~9 Phoenix, AZ 85040 Phone: (602) 437-3340 Fax: (602) 454-9303 Project Manager: Kylie Emily Client: Environmental Resources Management Inc.-West

Analysis Units Due

Sample iD: PTC0221-05 (IRz-IW-5-03032010- Water)


PTC0221 J:[COG6E; RECEIVING LABORATORY:

TestAmerica Irvine

17 461 Derian Ave. Suite 1 00 Irvine, CA 92614 Phone :(949) 261-1022 Fax: (949) 261-1228 Project Location: AZ - ARIZONA

··Receipt Temperature: · · · ··: °C . ·: Ice: . Y ·I. N .


Sampled: 03/03/10 12:10 Chlorate (300.1)

Chlorite (300.1) - 0

mg/1

mg/1

03/17/10 03/31/10 12:10 $30.00 0% Irvine

0% Irvine . 03/17/10 03/17/10 12:10 $30.00


500 ml Poly w/EDA (L) 125mL Brown Poly w/ EDA M

Sample ID: PTC0221-0B (IRZ-IW-4-03032010.- Water) Sampled: 03/03/10 14:40

Chlorate (300.1)


mg/1

mg/1

03/17/10 03/31/10 14:40 $30.00 0% Irvine

0% Irvine 03/17/10 03/17/10 14:40 $30.00


500 ml Poly w/EDA (L) 125ml Brown Poly w/ EDA(M

Released By DatefTime

~J<j¥ O:S-01....-tQ ;y.oo fC'-\ Received By DaterTime ~ fJ c_

V"1,/?6M/t :?>/do tf;.~ 3 .cfJ -R-ec-'e""'iv'-e-'d"'~B"-'y"""'-''-=~'----=OL...>.!..L,;, Datemme Page 1 of 1


TAL-0013-550 (12/08)

Client Name I Address: G =r~-~-d'~"" -5J,{)c9ts-<;l & R tv1 7 :;;_ 7-:L

~Gl)ff~O.t~ A 2- ~Sd-~f

Project Manager: f' lJ_ lA l C\. c""~·~'~-!J Sampler: ._, { oh(/l /l%o .-h.t-,_ (,

Sample Container


[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

.Pc'liectl PO N"mbe~ Analysis Required ~I 0 . .

f & ...t ;1/o ... --tc, i c) 3 f l5, 0~ ,...--.;: c; ~ ~~ ~ ......

Phone Number·: "'' l.L-:J:: l(fTJ 9~'8 ~..1-i·O I <:1:' ~ ~ ~~ ~

_'-C. 1;;::, a ~ ~ ~ Fax Number: Cef '{) \..,£) ~ ~

q: ~ ~->~- ...._] ,9(? 'J.Ib.f...

~ ~ ~ ~,~ ~~ "' ---..::: C>

--s;:> -s:' 0 #of Sampling Sampling

Page t of

~~ ~ t "\'_~

~ ~~ 't!!.' r-~ ~;;$ ~

~'-E. .-(iS

:;.... ~~

Sample Description Matrix Type Cont. Date Time Preservatives ~· ~ '\'::) ~(2 --~ ~. <:l\._ r Ft'-PJ T - Special Instructions

11_&_;;:.-!YJtv- 0-- N5-03@~olt f1.J {) !loA- 3 5/3/;o f}J>/6 H~/ '>\ ·,

trrLDUl -b) \

LAL:.,~M lr..r--0-J}.! -oso~)otb Ot!/5 ~ ..-.e_-z_

lr~:Z:...-J\11\fr-C..-'/ /5..{)3~ )f)/IJ D d9 ::ws X: -o3 ~ -1\A lv- L-tl..5-o 3 of :Jo/ 0 v '4.1 o d's D 'V ~ -ott Ite2. -1- \tv-<)- OsfJs ~olb .· ~v-lf{ 15 I~ I b Vift-t~_ K x- ~ y ~ <- \- k ;;~ x~ ' 70S'·,'[){o.

'"t-R2 -:I W- 5 -tJsDs}o/D ~ VoA 5 1~ I I i+Gl ~· -/ ·-0+

llRG-I IA/-t1-oso1.) o!V Va."" f_S._ l~ j ft-{Lto ~rit-{ ·~ ).:; ~ y ~ ~ :><'. y .x. >< -D6,o~

Trlr> G4v1J-r ··'lj VoA I '\V " -It> ' ...

~

'

Relinquished By:

~ Date/Time: Received By: Date/Time: Turnaround Time: (Check)

-'~ J./5/to_ !65 ~ ~ ~···

same day 72 hours - )

Re!inquishe~: Date/Time: R~;,e1~e\y: Date/Time: 24 ·hours 5 days

/ 48 hours normal

Relinquished By: Date/Time: .~:.. -Receivedj :r By: flDretTime: LlD'i;;_ Sample Integrity: (Check) )l eC:); _d-.v C . ~· .'3

. 1'~ k7

'""" ,~ ·qt, '·P J.!) intact on ice

/

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requ~sted on this chain of custody form and any additional analyses performed on this project Payment for services is due within 30 days from the date of invoice. Sample(s) wili' be disposed of after 30 days.



Report Date: 03/19/1 0 Client Proj Name: PTC0221

Client Proj #:- PTC0221

Address: 4625 East Cotton Center Blvd. Suite 189 _

;o~-cc ... "*~·.~ .......... ~-=-~· ~~·~=~~~,--~~-· .. _-~~~*-PhOeniX, AZ 85040


P1 003064-02

Client SamQie ID PTC0221-05

PTC0221-08

Laboratory Results Total pages in data package: __ &_· __ _

Microseeps test results meet all the requirements of the NELAC standards or provide reasons and/or justification If they do not.

Approved Bv:

Project Manager: Debbie Halla

The analytical results reported here are reliable and usable to the precision expressed In this report. As required by some regulating authorities, a full discussion of the uncertainty In our analytical results can be obtained at our web site or through customer service. Unless otherwise specified, all results


Case Narrative:

As a valued client we would appreciate your comments on our service. Please call customer service at (412)826-5245 oremaif customersetv/[email protected].

:rw William Pitt Way • Pittsburgh, PA 15238. • Tel 412-826-5245 • Fax 412-826-3433




SamQie Descrigtion Matrix Lab Sample#

Page; Page 2 of 5 Lab Proj #: P1 003064


Client Proj #: PTC0221

Samgled Date/Time Received PTC0221-05 Vapor P1 003064-01 03 Mar. 10 12:10 05 Mar. 10 12:06

Analyte(s) Flae Result PQL Units Method# Analysis Date


Data Qualifiers: J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B- detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N - NELAC certified analysis

By

sl


Suite i89 Phoenix, fl.Z 85040

Samgle Descri12tion Matrix Lab Sample#



Client Proj #: PTC022i

Samgled Date/Time Received PTC0221-08 Vapor P1 003064-02 03 Mar. 10 14:40 05 Mar. 10 12:06


Data Qualifiers: J ·estimated value, U- Non detect, R ·Poor surrogate recovery, M- Recovery!RPD poor for MS!M:SD, SAMPIDUP, B- detected in blank, S - field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N- NELAC certified analysis

By

sl



Prep Method:

Analysis Method:

M100317033wMB

Result TrueSgikeConc. RDL


M100317033-LCS

Result TrueSJ2ikeConc.


M100317033-LCSD

Result TrueSgikeConc.


Page: Page 4 of 5 La!:? Proj #: P1 003064

Report Date: 03/19/10 Client Proj Name: PTC0221




%Recove[Y Ctl Limits

- NA

%Recove,y Ctl Limits

90.00 75-125

%Recove,y Ctl Limits RPD

89.00 75-125 1.14

RPD Ctl Limits

0-20

'-------''Outlined Results indicate results outside of Control limits

Data Qualifiers: J- estimated value, U -Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MSJMSD, SAMP/DUP, B - detected in blank, S - field sample as received did not meet NELAC sample acceptance criteria, L - Subcontracted Lab used, N - NELAC certified analysis



Prep Method:

Analysis Method:

M100317034-MB

Result TrueS11ikeConc. RDL


M100317034-LCS



M 1 00317034-LCSD

Result TrueSnikeConc.








- NA


98.00 75- 125

%Recovery Ctl Limits RPD·

99.00 75 -125 1.04

RPD Ctl Limits

0-20

,__ ____ _,j Outlined Results Indicate results outside of Control limits

Pata Qualifiers: J ~estimated value, U ~Non detect, R- Poor surrogate recovery, M • Recovery/RPD poor for MSIMSD, SAMP/DUP, B ·detected in blank, S ~field sample as received did not meet NELAC sample acceptance criteria, L - Subcontracted Lab used, N • NELAC certified analysis

SENDING LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 189 Phoenix, AZ 85040 Phone: (602) 437-3340 Fax: (602) 454-9303 Project Manager: Kylie Emily

SUBCONTRACT ORDER TestAmeric~ _Phoenix

PTC0221



220 William Pitt Way Pittsburgh, PA 15238 = ·-

Phone :(412)826-5245 Fax: (412)826-3433 Project Location: AZ- ARIZONA Receipt Temperature: oc · Ice: Y I N


Analysis ,Units

Sample ID: PTC0221-05 (IRZ-IW-5-03032010- Water)

Hydrogen


NA(N)

%

Sample ID: PTC0221-08 (IRZ-IW-4-03032010 ·Water)

Hydrogen %


NA (N)

,/·-··"\

J-c;4--=· Released By

Released By Datemme

Expires Comments

Sampled: 03/03/10 12:10 03/31/10 12:10 DO NOT CHILUNO ICE-Microseeps

Sampled: 03/03/10 14:40 03/31/10 14:40 DO NOT CHILUNO ICE-Microseeps

Page 1 of 1


454-9303

LABORATORY REPORT





Received:

Issued:

03/04/10

03/04/10

03/24/10 12:52









CASE NARRATIVE


PTC0324-01 IRZ-MW-C-03042010 Water

PTC0324-02 IRZ-MW-C-03042010 Water

PTC0324-03 IRZ-MW-C-03042010D Water

PTC0324-04 IRZ-IW-2-03042010 Water

PTC0324-05 IRZ-MW-B-03042010 Water

PTC0324-06 IRZ-MW-B-03042010 Water

PTC0324-07 IRZ-MW-D-03042010 Water

PTC0324-08 IRZ-MW-D-03042010 Water

PTC0324-09 IRZ-IW-3-03042010 Water

PTC0324-10 IRZ-IW-3-03042010 Water

PTC0324-11 IRZ-IW-3-03042010R Water

PTC0324-12 IRZ-IW-1-03042010 Water

PTC0324-13 IRZ-IW-1-03042010 Water

PTC0324-14 Trip Blank-1 Water

PTC0324-15 Trip Blank-2 Water

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily

<Page 1 of 75>


454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00


HOLDING TIMES: Not all holding times were met. Results were qualified where the sample analysis did not occur within

method specified holding time requirements.

N1-The holding time for the filtration of this test is immediate. It was filtered in the laboratory as soon as

possible after receipt.



N1a-Results exceeded the linear range in the MS/MSD and therefore are not available for reporting. The

batch was accepted based on acceptable recovery in the Blank Spike (LCS).



Reviewed By:

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-01RE1 (IRZ-MW-C-03042010 - Water) Sampled: 03/04/10 D1


3/16/20103/16/2010EPA 8260BAcetone 5010C0610 5ND

3/16/20103/16/2010EPA 8260BBenzene 2.510C0610 5ND






3/16/20103/16/2010EPA 8260B2-Butanone (MEK) 1210C0610 5ND













3/16/20103/16/2010EPA 8260B1,2-Dibromo-3-chloropropane 1210C0610 5ND











3/16/20103/16/2010EPA 8260Btrans-1,2-Dichloroethene 2.510C0610 5ND








3/16/20103/16/2010EPA 8260BHexachlorobutadiene 5.010C0610 B15ND

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-01RE1 (IRZ-MW-C-03042010 - Water) - cont. Sampled: 03/04/10 D1


3/16/20103/16/2010EPA 8260B2-Hexanone 1210C0610 5ND

3/16/20103/16/2010EPA 8260BIodomethane 1210C0610 5ND

3/16/20103/16/2010EPA 8260BIsopropylbenzene 2.510C0610 5ND



3/16/20103/16/2010EPA 8260B4-Methyl-2-pentanone (MIBK) 1210C0610 5ND


3/16/20103/16/2010EPA 8260BNaphthalene 1210C0610 5ND


3/16/20103/16/2010EPA 8260BStyrene 2.510C0610 5ND




3/16/20103/16/2010EPA 8260BToluene 2.510C0610 5ND
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-03 (IRZ-MW-C-03042010D - Water) Sampled: 03/04/10 D1


3/15/20103/15/2010EPA 8260BAcetone 5010C0494 5ND

3/15/20103/15/2010EPA 8260BBenzene 2.510C0494 5ND







































Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-03 (IRZ-MW-C-03042010D - Water) - cont. Sampled: 03/04/10 D1











3/15/20103/15/2010EPA 8260BStyrene 2.510C0494 5ND




3/15/20103/15/2010EPA 8260BToluene 2.510C0494 5ND















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-03RE1 (IRZ-MW-C-03042010D - Water) - cont. Sampled: 03/04/10






Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-04 (IRZ-IW-2-03042010 - Water) Sampled: 03/04/10 D1


3/15/20103/15/2010EPA 8260BAcetone 5010C0494 5ND

3/15/20103/15/2010EPA 8260BBenzene 2.510C0494 5ND







































Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-04 (IRZ-IW-2-03042010 - Water) - cont. Sampled: 03/04/10 D1











3/15/20103/15/2010EPA 8260BStyrene 2.510C0494 5ND



3/15/20103/15/2010EPA 8260BTetrachloroethene 2.510C0494 M25ND

3/15/20103/15/2010EPA 8260BToluene 2.510C0494 5ND















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result







Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-05 (IRZ-MW-B-03042010 - Water) Sampled: 03/04/10


Acetone 3/15/20103/15/201010C0494 10 1EPA 8260B 30

3/15/20103/15/2010EPA 8260BBenzene 0.5010C0494 1ND






2-Butanone (MEK) 3/15/20103/15/201010C0494 2.5 1EPA 8260B 9.9

































Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-05 (IRZ-MW-B-03042010 - Water) - cont. Sampled: 03/04/10











3/15/20103/15/2010EPA 8260BStyrene 0.5010C0494 1ND




Toluene 3/15/20103/15/201010C0494 0.50 1EPA 8260B 1.7





Trichloroethene 3/15/20103/15/201010C0494 0.50 1EPA 8260B 1.7











Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-07RE1 (IRZ-MW-D-03042010 - Water) Sampled: 03/04/10


3/16/20103/16/2010EPA 8260BAcetone 20010C0586 20ND

3/16/20103/16/2010EPA 8260BBenzene 1010C0586 20ND

3/16/20103/16/2010EPA 8260BBromobenzene 1010C0586 20ND

3/16/20103/16/2010EPA 8260BBromochloromethane 1010C0586 20ND

3/16/20103/16/2010EPA 8260BBromodichloromethane 1010C0586 20ND

3/16/20103/16/2010EPA 8260BBromoform 2010C0586 20ND

3/16/20103/16/2010EPA 8260BBromomethane 2010C0586 20ND


3/16/20103/16/2010EPA 8260Bn-Butylbenzene 1010C0586 20ND

3/16/20103/16/2010EPA 8260Bsec-Butylbenzene 1010C0586 20ND

3/16/20103/16/2010EPA 8260Btert-Butylbenzene 1010C0586 20ND

3/16/20103/16/2010EPA 8260BCarbon disulfide 1010C0586 20ND

3/16/20103/16/2010EPA 8260BCarbon tetrachloride 1010C0586 20ND

3/16/20103/16/2010EPA 8260BChlorobenzene 1010C0586 20ND

3/16/20103/16/2010EPA 8260BChloroethane 2010C0586 20ND

3/16/20103/16/2010EPA 8260BChloroform 1010C0586 20ND

3/16/20103/16/2010EPA 8260BChloromethane 2010C0586 20ND

3/16/20103/16/2010EPA 8260B2-Chlorotoluene 1010C0586 20ND


3/16/20103/16/2010EPA 8260BDibromochloromethane 1010C0586 20ND


3/16/20103/16/2010EPA 8260B1,2-Dibromoethane (EDB) 1010C0586 20ND

3/16/20103/16/2010EPA 8260BDibromomethane 1010C0586 20ND

3/16/20103/16/2010EPA 8260B1,2-Dichlorobenzene 1010C0586 20ND



3/16/20103/16/2010EPA 8260BDichlorodifluoromethane 1010C0586 20ND

3/16/20103/16/2010EPA 8260B1,1-Dichloroethane 1010C0586 20ND


3/16/20103/16/2010EPA 8260B1,1-Dichloroethene 1010C0586 20ND

3/16/20103/16/2010EPA 8260Bcis-1,2-Dichloroethene 1010C0586 20ND

3/16/20103/16/2010EPA 8260Btrans-1,2-Dichloroethene 1010C0586 20ND

3/16/20103/16/2010EPA 8260B1,2-Dichloropropane 1010C0586 20ND



3/16/20103/16/2010EPA 8260B1,1-Dichloropropene 1010C0586 20ND

3/16/20103/16/2010EPA 8260Bcis-1,3-Dichloropropene 1010C0586 20ND

3/16/20103/16/2010EPA 8260Btrans-1,3-Dichloropropene 1010C0586 20ND

3/16/20103/16/2010EPA 8260BEthylbenzene 1010C0586 20ND

3/16/20103/16/2010EPA 8260BHexachlorobutadiene 2010C0586 20ND

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-07RE1 (IRZ-MW-D-03042010 - Water) - cont. Sampled: 03/04/10




3/16/20103/16/2010EPA 8260BIsopropylbenzene 1010C0586 20ND

3/16/20103/16/2010EPA 8260Bp-Isopropyltoluene 1010C0586 20ND

3/16/20103/16/2010EPA 8260BMethylene Chloride 2010C0586 20ND


3/16/20103/16/2010EPA 8260BMethyl-tert-butyl Ether (MTBE) 1010C0586 20ND


3/16/20103/16/2010EPA 8260Bn-Propylbenzene 1010C0586 20ND

3/16/20103/16/2010EPA 8260BStyrene 1010C0586 20ND

3/16/20103/16/2010EPA 8260B1,1,1,2-Tetrachloroethane 1010C0586 20ND


3/16/20103/16/2010EPA 8260BTetrachloroethene 1010C0586 20ND

3/16/20103/16/2010EPA 8260BToluene 1010C0586 20ND

3/16/20103/16/2010EPA 8260B1,2,3-Trichlorobenzene 2010C0586 20ND


3/16/20103/16/2010EPA 8260B1,1,1-Trichloroethane 1010C0586 20ND



3/16/20103/16/2010EPA 8260BTrichlorofluoromethane 1010C0586 20ND

3/16/20103/16/2010EPA 8260B1,2,3-Trichloropropane 2010C0586 20ND

3/16/20103/16/2010EPA 8260B1,2,4-Trimethylbenzene 1010C0586 20ND


3/16/20103/16/2010EPA 8260BVinyl Acetate 1010C0586 20ND

3/16/20103/16/2010EPA 8260BVinyl chloride 1010C0586 20ND

3/16/20103/16/2010EPA 8260BXylenes, Total 2010C0586 20ND




Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-09 (IRZ-IW-3-03042010 - Water) Sampled: 03/04/10 D1


3/15/20103/15/2010EPA 8260BAcetone 100010C0494 100ND

3/15/20103/15/2010EPA 8260BBenzene 5010C0494 100ND






































3/15/20103/15/2010EPA 8260BHexachlorobutadiene 10010C0494 B1100ND

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-09 (IRZ-IW-3-03042010 - Water) - cont. Sampled: 03/04/10 D1











3/15/20103/15/2010EPA 8260BStyrene 5010C0494 100ND




3/15/20103/15/2010EPA 8260BToluene 5010C0494 100ND
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-11 (IRZ-IW-3-03042010R - Water) Sampled: 03/04/10


3/16/20103/16/2010EPA 8260BAcetone 1010C0610 1ND

3/16/20103/16/2010EPA 8260BBenzene 0.5010C0610 1ND



Bromodichloromethane 3/16/20103/16/201010C0610 0.50 1EPA 8260B 1.7















Dibromochloromethane 3/16/20103/16/201010C0610 0.50 1EPA 8260B 0.83





















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-11 (IRZ-IW-3-03042010R - Water) - cont. Sampled: 03/04/10











3/16/20103/16/2010EPA 8260BStyrene 0.5010C0610 1ND




3/16/20103/16/2010EPA 8260BToluene 0.5010C0610 1ND
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



3/16/20103/16/2010EPA 8260BAcetone 100010C0610 100ND

3/16/20103/16/2010EPA 8260BBenzene 5010C0610 100ND






































3/16/20103/16/2010EPA 8260BHexachlorobutadiene 10010C0610 B1100ND

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result












3/16/20103/16/2010EPA 8260BStyrene 5010C0610 100ND




3/16/20103/16/2010EPA 8260BToluene 5010C0610 100ND
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-14 (Trip Blank-1 - Water) Sampled: 03/04/10


3/15/20103/15/2010EPA 8260BAcetone 1010C0494 1ND

3/15/20103/15/2010EPA 8260BBenzene 0.5010C0494 1ND







































Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-14 (Trip Blank-1 - Water) - cont. Sampled: 03/04/10











3/15/20103/15/2010EPA 8260BStyrene 0.5010C0494 1ND




3/15/20103/15/2010EPA 8260BToluene 0.5010C0494 1ND
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-15 (Trip Blank-2 - Water) Sampled: 03/04/10


3/15/20103/15/2010EPA 8260BAcetone 1010C0494 1ND

3/15/20103/15/2010EPA 8260BBenzene 0.5010C0494 1ND







































Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-15 (Trip Blank-2 - Water) - cont. Sampled: 03/04/10











3/15/20103/15/2010EPA 8260BStyrene 0.5010C0494 1ND




3/15/20103/15/2010EPA 8260BToluene 0.5010C0494 1ND
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTC0324-01 (IRZ-MW-C-03042010 - Water) Sampled: 03/04/10


Iron 3/8/20103/5/201010C0261 0.050 1E200.7 11

Manganese 3/8/20103/5/201010C0261 0.010 1E200.7 0.021

Sodium 3/8/20103/5/201010C0261 2.0 1E200.7 450



Iron 3/8/20103/5/201010C0261 0.050 1E200.7 26

Manganese 3/8/20103/5/201010C0261 0.010 1E200.7 0.075

Sodium 3/8/20103/5/201010C0261 10 5E200.7 1700

Sample ID: PTC0324-07 (IRZ-MW-D-03042010 - Water) Sampled: 03/04/10


Iron 3/8/20103/5/201010C0261 0.050 1E200.7 2.3

Manganese 3/8/20103/5/201010C0261 0.010 1E200.7 0.026

Sodium 3/8/20103/5/201010C0261 2.0 1E200.7 470



Iron 3/9/20103/5/201010C0261 500 10000E200.7 91000

Manganese 3/8/20103/5/201010C0261 0.010 1E200.7 11

Sodium 3/8/20103/5/201010C0261 2.0 1E200.7 380



Iron 3/8/20103/5/201010C0261 0.050 1E200.7 14

Manganese 3/8/20103/5/201010C0261 0.010 1E200.7 0.046

Sodium 3/8/20103/5/201010C0261 2.0 1E200.7 430

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

DISSOLVED METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 3/8/20103/5/201010C0276 0.050 1E200.7 0.48



Iron 3/8/20103/5/201010C0276 0.050 N11E200.7 27



3/8/20103/5/2010E200.7Iron 0.05010C0276 1ND



Iron 3/8/20103/5/201010C0276 0.050 1E200.7 2.4



3/8/20103/5/2010E200.7Iron 0.05010C0276 1ND

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result







3/10/20103/10/2010SM 4500-P B, EPhosphate 0.3010C0404 1ND

3/9/20103/8/2010M4500-P B, EPhosphorus,Total - P 0.1010C0379 1ND





Sample ID: PTC0324-01RE1 (IRZ-MW-C-03042010 - Water) Sampled: 03/04/10


Chloride 3/8/20103/8/201010C0337 40 20EPA 300.0 730

Nitrate-N 3/6/20103/6/201010C0338 1.0 H25EPA 300.0 20

Sulfate 3/8/20103/8/201010C0337 40 20EPA 300.0 940






3/5/20103/5/2010EPA 300.0Nitrate-N 0.2010C0249 1ND

Phosphate 3/10/20103/10/201010C0404 0.30 1SM 4500-P B, E 5.8

Phosphorus,Total - P 3/9/20103/8/201010C0379 0.50 M25M4500-P B, E 1.9



3/15/20103/15/2010EPA 314.0Perchlorate 6.010C0558 D13ND

Sample ID: PTC0324-05RE1 (IRZ-MW-B-03042010 - Water) Sampled: 03/04/10



3/15/20103/15/2010M2320 BBicarbonate Alkalinity as CaCO3 6.010C0550 1ND

Carbonate Alkalinity as CaCO3 3/15/20103/15/201010C0550 6.0 1M2320 B 1000

Chloride 3/8/20103/8/201010C0337 40 20EPA 300.0 1700

Hydroxide Alkalinity as CaCO3 3/15/20103/15/201010C0550 6.0 1M2320 B 450

Sulfate 3/8/20103/8/201010C0337 40 20EPA 300.0 500

Alkalinity, Phenolphthalein 3/15/20103/15/201010C0550 6.0 1M2320 B 960

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result













Sample ID: PTC0324-07RE1 (IRZ-MW-D-03042010 - Water) Sampled: 03/04/10


Chloride 3/8/20103/8/201010C0337 40 20EPA 300.0 730

Nitrate-N 3/6/20103/6/201010C0338 1.0 5EPA 300.0 20

Sulfate 3/8/20103/8/201010C0337 40 20EPA 300.0 940







Nitrate-N 3/5/20103/5/201010C0249 0.20 1EPA 300.0 19


Phosphorus,Total - P 3/9/20103/8/201010C0379 1.0 10M4500-P B, E 6.5







Chloride 3/8/20103/8/201010C0337 40 20EPA 300.0 790

Sulfate 3/8/20103/8/201010C0337 40 20EPA 300.0 1100

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result







Nitrate-N 3/5/20103/5/201010C0249 0.20 1EPA 300.0 16









Chloride 3/8/20103/8/201010C0337 40 20EPA 300.0 810

Sulfate 3/8/20103/8/201010C0337 40 20EPA 300.0 1100

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



3/9/20103/9/2010M5310BTotal Organic Carbon 1.010C0336 1ND



Total Organic Carbon 3/9/20103/9/201010C0336 1.0 1M5310B 10










Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



Chlorate 3/16/20103/16/201010C1985 40 2EPA 300.1 85





Chlorate 3/16/20103/16/201010C1985 100 5EPA 300.1 180





Chlorate 3/16/20103/16/201010C1985 40 2EPA 300.1 85





Chlorate 3/16/20103/16/201010C1985 40 2EPA 300.1 89





Chlorate 3/16/20103/16/201010C1985 40 2EPA 300.1 77

Chlorite 3/16/20103/16/201010C1985 400 20EPA 300.1 900


Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00


Date/Time

Analyzed

Date/Time

Extracted

Date/Time

Sampled

Date/Time

Received

Hold Time

(in days)

Sample ID: IRZ-MW-C-03042010 (PTC0324-01RE1) - Water

2 03/04/2010 08:31 03/04/2010 17:17 03/06/2010 09:00 03/06/2010 11:16EPA 300.0

Sample ID: IRZ-MW-B-03042010 (PTC0324-05) - Water

2 03/04/2010 10:15 03/04/2010 17:17 03/05/2010 13:15 03/05/2010 17:55EPA 300.0

Sample ID: IRZ-MW-D-03042010 (PTC0324-07RE1) - Water

2 03/04/2010 11:10 03/04/2010 17:17 03/06/2010 09:00 03/06/2010 10:49EPA 300.0


2 03/04/2010 13:23 03/04/2010 17:17 03/05/2010 13:15 03/05/2010 18:49EPA 300.0


2 03/04/2010 15:00 03/04/2010 17:17 03/05/2010 13:15 03/05/2010 19:17EPA 300.0

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 03/15/2010 (10C0494-BS1)

Acetone 25.0 10-150ug/l1016.8 67

Benzene 25.0 80-120ug/l0.5022.6 90




Bromoform 25.0 75-130ug/l1.021.2 85


2-Butanone (MEK) 25.0 40-150ug/l2.518.1 72








Chloroform 25.0 75-120ug/l0.5022.8 91




















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 03/15/2010 (10C0494-BS1)






2-Hexanone 25.0 20-150ug/l2.517.6 70

Iodomethane 25.0 80-130ug/l2.523.7 95






Naphthalene 25.0 40-150ug/l2.524.7 99


Styrene 25.0 80-120ug/l0.5023.4 94




Toluene 25.0 80-120ug/l0.5022.0 88
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1017.8 71 6

Benzene 25.0 1580-120ug/l0.5023.6 94 4




Bromoform 25.0 2075-130ug/l1.022.0 88 4

Bromomethane 25.0 2055-150ug/l1.023.0 92 0.3

2-Butanone (MEK) 25.0 3540-150ug/l2.518.2 73 0.7








Chloroform 25.0 1575-120ug/l0.5023.6 94 3




Dibromochloromethane 25.0 1580-120ug/l0.5022.2 89 0.7

1,2-Dibromo-3-chloropropane 25.0 3550-150ug/l2.521.8 87 0.09















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







Hexachlorobutadiene 25.0 3540-150ug/l1.027.9 B1111 0.2

2-Hexanone 25.0 3520-150ug/l2.518.4 74 5

Iodomethane 25.0 1080-130ug/l2.524.8 99 4






Naphthalene 25.0 3040-150ug/l2.525.0 100 1


Styrene 25.0 1580-120ug/l0.5024.5 98 5




Toluene 25.0 1580-120ug/l0.5022.7 91 3
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 125 10-150ug/l5065.0 ND 52

Benzene 125 70-125ug/l2.5131 ND 104

Bromobenzene 125 75-120ug/l2.5132 ND 105

Bromochloromethane 125 75-130ug/l2.5130 ND 104

Bromodichloromethane 125 75-125ug/l2.5140 ND 112

Bromoform 125 65-125ug/l5.0114 ND 91

Bromomethane 125 45-150ug/l5.0142 ND 113

2-Butanone (MEK) 125 15-150ug/l1272.8 ND 58

n-Butylbenzene 125 70-130ug/l2.5137 ND 110

sec-Butylbenzene 125 70-125ug/l2.5136 ND 109

tert-Butylbenzene 125 70-125ug/l2.5152 ND 122

Carbon disulfide 125 65-145ug/l2.5166 ND 133

Carbon tetrachloride 125 65-135ug/l2.5154 ND 123

Chlorobenzene 125 75-120ug/l2.5130 ND 104

Chloroethane 125 65-140ug/l5.0138 ND 111

Chloroform 125 70-130ug/l2.5130 0.550 103

Chloromethane 125 55-145ug/l5.0123 ND 98

2-Chlorotoluene 125 70-125ug/l2.5129 ND 103


Dibromochloromethane 125 70-130ug/l2.5122 ND 98

1,2-Dibromo-3-chloropropane 125 50-150ug/l12106 ND 85

1,2-Dibromoethane (EDB) 125 70-125ug/l2.5131 ND 105

Dibromomethane 125 70-120ug/l2.5129 ND 103

1,2-Dichlorobenzene 125 75-120ug/l2.5130 ND 104



Dichlorodifluoromethane 125 60-150ug/l2.585.3 ND 68

1,1-Dichloroethane 125 70-130ug/l2.5132 ND 106


1,1-Dichloroethene 125 70-130ug/l2.5133 ND 107

cis-1,2-Dichloroethene 125 70-125ug/l2.5139 ND 111

trans-1,2-Dichloroethene 125 75-125ug/l2.5129 ND 103

1,2-Dichloropropane 125 75-125ug/l2.5133 ND 107



Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 125 65-130ug/l2.5131 ND 105

cis-1,3-Dichloropropene 125 75-130ug/l2.5136 ND 109

trans-1,3-Dichloropropene 125 70-130ug/l2.5135 ND 108

Ethylbenzene 125 70-125ug/l2.5133 ND 107

Hexachlorobutadiene 125 40-150ug/l5.0136 B1ND 109

2-Hexanone 125 20-150ug/l1272.1 ND 58

Iodomethane 125 60-150ug/l12139 ND 112

Isopropylbenzene 125 75-130ug/l2.5135 ND 108

p-Isopropyltoluene 125 70-130ug/l2.5137 ND 110

Methylene Chloride 125 65-130ug/l5.0128 ND 103

4-Methyl-2-pentanone (MIBK) 125 55-135ug/l12115 ND 92

Methyl-tert-butyl Ether (MTBE) 125 65-140ug/l2.5118 ND 94

Naphthalene 125 40-150ug/l12124 ND 99

n-Propylbenzene 125 70-130ug/l2.5135 ND 108

Styrene 125 55-135ug/l2.5134 ND 107

1,1,1,2-Tetrachloroethane 125 70-125ug/l2.5135 ND 108


Tetrachloroethene 125 65-130ug/l2.586.0 ND 69

Toluene 125 70-125ug/l2.5133 ND 107

1,2,3-Trichlorobenzene 125 50-150ug/l5.0134 ND 107


1,1,1-Trichloroethane 125 70-130ug/l2.5142 ND 113


Trichloroethene 125 70-125ug/l2.5652 M2742 -72

Trichlorofluoromethane 125 65-150ug/l2.5176 ND 141

1,2,3-Trichloropropane 125 70-130ug/l5.0129 ND 103

1,2,4-Trimethylbenzene 125 70-125ug/l2.5133 ND 106


Vinyl Acetate 125 40-150ug/l2.5130 ND 104

Vinyl chloride 125 60-140ug/l2.5120 ND 96

Xylenes, Total 375 75-120ug/l5.0400 ND 107




Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 125 3510-150ug/l5059.3 ND 47 9

Benzene 125 2570-125ug/l2.5125 ND 100 4

Bromobenzene 125 2075-120ug/l2.5127 ND 101 4

Bromochloromethane 125 2075-130ug/l2.5128 ND 102 2

Bromodichloromethane 125 2075-125ug/l2.5132 ND 106 6

Bromoform 125 2565-125ug/l5.0111 ND 89 2

Bromomethane 125 3545-150ug/l5.0127 ND 102 11

2-Butanone (MEK) 125 3015-150ug/l1274.4 ND 59 2

n-Butylbenzene 125 3070-130ug/l2.5126 ND 101 8

sec-Butylbenzene 125 3070-125ug/l2.5129 ND 103 5

tert-Butylbenzene 125 2570-125ug/l2.5144 ND 115 6

Carbon disulfide 125 2565-145ug/l2.5149 ND 119 11

Carbon tetrachloride 125 2565-135ug/l2.5144 ND 115 7

Chlorobenzene 125 2075-120ug/l2.5123 ND 98 6

Chloroethane 125 2565-140ug/l5.0125 ND 100 10

Chloroform 125 2070-130ug/l2.5124 0.550 99 4

Chloromethane 125 3555-145ug/l5.0116 ND 93 5

2-Chlorotoluene 125 2570-125ug/l2.5123 ND 98 5

4-Chlorotoluene 125 2570-125ug/l2.5123 ND 98 6

Dibromochloromethane 125 2070-130ug/l2.5117 ND 94 5

1,2-Dibromo-3-chloropropane 125 3050-150ug/l12103 ND 83 3

1,2-Dibromoethane (EDB) 125 2070-125ug/l2.5122 ND 98 8

Dibromomethane 125 2070-120ug/l2.5122 ND 98 6

1,2-Dichlorobenzene 125 2075-120ug/l2.5123 ND 99 5



Dichlorodifluoromethane 125 3060-150ug/l2.578.1 ND 62 9

1,1-Dichloroethane 125 2070-130ug/l2.5125 ND 100 6

1,2-Dichloroethane 125 2065-140ug/l2.5122 ND 97 3

1,1-Dichloroethene 125 2570-130ug/l2.5122 ND 98 8

cis-1,2-Dichloroethene 125 2070-125ug/l2.5133 ND 106 4

trans-1,2-Dichloroethene 125 2575-125ug/l2.5121 ND 97 7

1,2-Dichloropropane 125 2075-125ug/l2.5124 ND 99 7



Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 125 2565-130ug/l2.5120 ND 96 8

cis-1,3-Dichloropropene 125 2075-130ug/l2.5126 ND 101 7

trans-1,3-Dichloropropene 125 2070-130ug/l2.5127 ND 102 6

Ethylbenzene 125 2570-125ug/l2.5124 ND 99 8

Hexachlorobutadiene 125 3040-150ug/l5.0132 B1ND 105 3

2-Hexanone 125 3020-150ug/l1268.8 ND 55 5

Iodomethane 125 3060-150ug/l12132 ND 106 6

Isopropylbenzene 125 2575-130ug/l2.5124 ND 100 8

p-Isopropyltoluene 125 3070-130ug/l2.5130 ND 104 5

Methylene Chloride 125 2065-130ug/l5.0123 ND 98 4

4-Methyl-2-pentanone (MIBK) 125 2555-135ug/l12109 ND 87 5

Methyl-tert-butyl Ether (MTBE) 125 2565-140ug/l2.5116 ND 93 1

Naphthalene 125 3040-150ug/l12123 ND 98 0.7

n-Propylbenzene 125 3070-130ug/l2.5127 ND 102 6

Styrene 125 3555-135ug/l2.5124 ND 99 8

1,1,1,2-Tetrachloroethane 125 2070-125ug/l2.5129 ND 103 5

1,1,2,2-Tetrachloroethane 125 2570-125ug/l2.5124 ND 99 0.6

Tetrachloroethene 125 2565-130ug/l2.578.7 M2ND 63 9

Toluene 125 2070-125ug/l2.5121 ND 97 10

1,2,3-Trichlorobenzene 125 3550-150ug/l5.0133 ND 106 0.7

1,2,4-Trichlorobenzene 125 2550-150ug/l5.0134 ND 107 4

1,1,1-Trichloroethane 125 2570-130ug/l2.5132 ND 105 8

1,1,2-Trichloroethane 125 2075-125ug/l2.5119 ND 95 6

Trichloroethene 125 2570-125ug/l2.5593 M2742 -119 9

Trichlorofluoromethane 125 2565-150ug/l2.5155 ND 124 13

1,2,3-Trichloropropane 125 2570-130ug/l5.0131 ND 105 2

1,2,4-Trimethylbenzene 125 3070-125ug/l2.5125 ND 100 6

1,3,5-Trimethylbenzene 125 2575-130ug/l2.5126 ND 100 6

Vinyl Acetate 125 3040-150ug/l2.5128 ND 102 2

Vinyl chloride 125 2560-140ug/l2.5112 ND 90 7

Xylenes, Total 375 1575-120ug/l5.0376 ND 100 6




Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 03/16/2010 (10C0586-BS1)

Acetone 25.0 10-150ug/l1025.2 101

Benzene 25.0 80-120ug/l0.5021.2 85




Bromoform 25.0 75-130ug/l1.027.5 110


2-Butanone (MEK) 25.0 40-150ug/l2.523.7 95








Chloroform 25.0 75-120ug/l0.5022.5 90




















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 03/16/2010 (10C0586-BS1)






2-Hexanone 25.0 20-150ug/l2.525.7 103

Iodomethane 25.0 80-130ug/l2.525.2 101






Naphthalene 25.0 40-150ug/l2.524.6 99


Styrene 25.0 80-120ug/l0.5022.2 89




Toluene 25.0 80-120ug/l0.5022.8 91
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1021.4 86 16

Benzene 25.0 1580-120ug/l0.5020.8 83 2




Bromoform 25.0 2075-130ug/l1.026.6 106 3


2-Butanone (MEK) 25.0 3540-150ug/l2.519.8 79 18







Chloroethane 25.0 1570-130ug/l1.020.0 80 0.3

Chloroform 25.0 1575-120ug/l0.5022.5 90 0




Dibromochloromethane 25.0 1580-120ug/l0.5027.2 109 0.5
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







Hexachlorobutadiene 25.0 3540-150ug/l1.015.7 R663 36

2-Hexanone 25.0 3520-150ug/l2.522.9 91 12

Iodomethane 25.0 1080-130ug/l2.524.7 99 2






Naphthalene 25.0 3040-150ug/l2.520.9 84 16


Styrene 25.0 1580-120ug/l0.5021.8 87 2



Tetrachloroethene 25.0 2070-130ug/l0.5024.4 97 0.2

Toluene 25.0 1580-120ug/l0.5022.3 89 2









1,3,5-Trimethylbenzene 25.0 1580-130ug/l0.5024.8 99 0.2







Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1020.3 ND 81

Benzene 25.0 70-125ug/l0.5022.3 ND 89




Bromoform 25.0 65-125ug/l1.025.5 ND 102







Carbon tetrachloride 25.0 65-135ug/l0.5029.3 0.180 116



Chloroform 25.0 70-130ug/l0.5027.8 4.95 92














1,1-Dichloroethene 25.0 70-130ug/l0.5046.7 21.8 99

cis-1,2-Dichloroethene 25.0 70-125ug/l0.5031.9 9.36 90

trans-1,2-Dichloroethene 25.0 75-125ug/l0.5024.1 0.110 96

1,2-Dichloropropane 25.0 75-125ug/l0.5028.0 5.08 92



Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.521.3 ND 85






Methyl-tert-butyl Ether (MTBE) 25.0 65-140ug/l0.5022.3 0.160 88



Styrene 25.0 55-135ug/l0.5019.8 0.320 78




Toluene 25.0 70-125ug/l0.5024.1 0.270 95



1,1,1-Trichloroethane 25.0 70-130ug/l0.5077.6 52.6 100


Trichloroethene 25.0 70-125ug/l0.50790 M3786 19






Vinyl chloride 25.0 60-140ug/l0.5019.6 0.300 77





Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1020.8 ND 83 2

Benzene 25.0 2570-125ug/l0.5021.2 ND 85 5



Bromodichloromethane 25.0 2075-125ug/l0.5024.0 M27.38 67 8

Bromoform 25.0 2565-125ug/l1.025.5 ND 102 0.3


2-Butanone (MEK) 25.0 3015-150ug/l2.521.2 ND 85 0.4





Carbon tetrachloride 25.0 2565-135ug/l0.5026.9 0.180 107 9



Chloroform 25.0 2070-130ug/l0.5027.0 4.95 88 3














1,1-Dichloroethene 25.0 2570-130ug/l0.5045.7 21.8 96 2

cis-1,2-Dichloroethene 25.0 2070-125ug/l0.5030.4 9.36 84 5

trans-1,2-Dichloroethene 25.0 2575-125ug/l0.5022.7 0.110 90 6

1,2-Dichloropropane 25.0 2075-125ug/l0.5025.6 5.08 82 9

1,3-Dichloropropane 25.0 2070-120ug/l0.5022.7 1.12 86 2


Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3020-150ug/l2.522.6 ND 90 6




Methylene Chloride 25.0 2065-130ug/l1.023.1 1.31 87 0.8


Methyl-tert-butyl Ether (MTBE) 25.0 2565-140ug/l0.5022.1 0.160 88 0.8



Styrene 25.0 3555-135ug/l0.5018.4 0.320 72 8




Toluene 25.0 2070-125ug/l0.5022.6 0.270 89 6



1,1,1-Trichloroethane 25.0 2570-130ug/l0.5075.1 52.6 90 3


Trichloroethene 25.0 2570-125ug/l0.50768 M3786 -68 3






Vinyl chloride 25.0 2560-140ug/l0.5019.8 0.300 78 1





Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 03/16/2010 (10C0610-BS1)

Acetone 25.0 10-150ug/l1013.4 53

Benzene 25.0 80-120ug/l0.5024.4 98




Bromoform 25.0 75-130ug/l1.021.9 88


2-Butanone (MEK) 25.0 40-150ug/l2.515.9 64








Chloroform 25.0 75-120ug/l0.5024.7 99




















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 03/16/2010 (10C0610-BS1)






2-Hexanone 25.0 20-150ug/l2.514.3 57

Iodomethane 25.0 80-130ug/l2.525.4 102






Naphthalene 25.0 40-150ug/l2.523.0 92


Styrene 25.0 80-120ug/l0.5026.2 105




Toluene 25.0 80-120ug/l0.5023.5 94
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1016.6 67 22

Benzene 25.0 1580-120ug/l0.5023.7 95 3




Bromoform 25.0 2075-130ug/l1.022.0 88 0.5


2-Butanone (MEK) 25.0 3540-150ug/l2.517.7 71 11




Carbon disulfide 25.0 1570-140ug/l0.5028.3 113 0.6


Chlorobenzene 25.0 1580-120ug/l0.5024.7 99 0.2

Chloroethane 25.0 1570-130ug/l1.023.3 93 0.9

Chloroform 25.0 1575-120ug/l0.5024.0 96 3


2-Chlorotoluene 25.0 1580-120ug/l0.5024.4 98 0.4




1,2-Dibromoethane (EDB) 25.0 1580-120ug/l0.5023.8 95 0.1














Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers




cis-1,3-Dichloropropene 25.0 1580-120ug/l0.5025.8 103 0.2


Ethylbenzene 25.0 1580-120ug/l0.5024.9 100 0.7

Hexachlorobutadiene 25.0 3540-150ug/l1.027.3 B1109 1

2-Hexanone 25.0 3520-150ug/l2.516.6 66 15

Iodomethane 25.0 1080-130ug/l2.525.1 100 1






Naphthalene 25.0 3040-150ug/l2.523.6 94 2

n-Propylbenzene 25.0 1575-130ug/l0.5025.2 101 0.04

Styrene 25.0 1580-120ug/l0.5025.9 104 1




Toluene 25.0 1580-120ug/l0.5023.6 94 0.2

1,2,3-Trichlorobenzene 25.0 3555-150ug/l1.025.1 100 0.4





Trichlorofluoromethane 25.0 2570-150ug/l0.5032.2 129 0.5


1,2,4-Trimethylbenzene 25.0 1580-120ug/l0.5025.5 102 0.2








Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1010.3 ND 41

Benzene 25.0 70-125ug/l0.5025.6 ND 102




Bromoform 25.0 65-125ug/l1.020.7 ND 83










Chloroform 25.0 70-130ug/l0.5025.4 0.0900 101




















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







Hexachlorobutadiene 25.0 40-150ug/l1.028.1 B1ND 112

2-Hexanone 25.0 20-150ug/l2.513.2 ND 53









Styrene 25.0 55-135ug/l0.5024.6 ND 99




Toluene 25.0 70-125ug/l0.5025.1 ND 101
















Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l109.65 ND 39 7

Benzene 25.0 2570-125ug/l0.5024.8 ND 99 3




Bromoform 25.0 2565-125ug/l1.020.1 ND 80 3










Chloroform 25.0 2070-130ug/l0.5024.9 0.0900 99 2






1,2-Dibromoethane (EDB) 25.0 2070-125ug/l0.5023.8 ND 95 0.4














Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







Hexachlorobutadiene 25.0 3040-150ug/l1.028.2 B1ND 113 0.6

2-Hexanone 25.0 3020-150ug/l2.513.5 ND 54 2









Styrene 25.0 3555-135ug/l0.5024.2 ND 97 2



Tetrachloroethene 25.0 2565-130ug/l0.5016.7 ND 67 0.5

Toluene 25.0 2070-125ug/l0.5024.7 ND 99 2





Trichloroethene 25.0 2570-125ug/l0.5029.6 4.35 101 0.5











Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Iron mg/l0.050ND


Sodium mg/l2.0ND

LCS Analyzed: 03/08/2010 (10C0261-BS1)

Iron 1.00 85-115mg/l0.0500.951 95

Manganese 1.00 85-115mg/l0.0100.996 100

Sodium 20.0 85-115mg/l2.019.1 95


Iron 1.00 2085-115mg/l0.0500.959 96 0.8

Manganese 1.00 2085-115mg/l0.0101.01 101 2

Sodium 20.0 2085-115mg/l2.019.1 95 0.02


Iron 1.00 75-125mg/l0.0501.82 0.799 102

Manganese 1.00 75-125mg/l0.0101.11 0.0991 101

Sodium 20.0 75-125mg/l2.0163 145 90


Iron 1.00 75-125mg/l0.0502.09 1.06 103

Manganese 1.00 75-125mg/l0.0101.12 0.102 102

Sodium 20.0 75-125mg/l2.0141 120 106


Iron 1.00 1075-125mg/l0.0501.86 0.799 106 2

Manganese 1.00 1075-125mg/l0.0101.13 0.0991 103 2

Sodium 20.0 1075-125mg/l2.0165 145 98 0.9

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Iron 1.00 1075-125mg/l0.0502.08 1.06 103 0.4

Manganese 1.00 1075-125mg/l0.0101.12 0.102 102 0.5

Sodium 20.0 1075-125mg/l2.0144 120 118 2

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

DISSOLVED METALS


Data

Qualifiers



Iron mg/l0.050ND


Iron mg/l0.050ND

LCS Analyzed: 03/08/2010 (10C0276-BS1)

Iron 1.00 85-115mg/l0.0500.963 96


Iron 1.00 2085-115mg/l0.0500.978 98 2


Iron 1.00 75-125mg/l0.0501.49 0.484 100


Iron 1.00 1075-125mg/l0.0501.51 0.484 103 2

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers








LCS Analyzed: 03/04/2010 (10C0223-BS2)


















Chloride mg/l2.0ND


Sulfate mg/l2.0ND

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers


LCS Analyzed: 03/05/2010 (10C0249-BS1)


Nitrate-N 4.00 90-110mg/lNA3.84 96

Sulfate 20.0 90-110mg/lNA19.4 N1a97



Nitrate-N 4.00 1590-110mg/lNA3.85 96 0.2

Sulfate 20.0 1590-110mg/lNA19.5 N1a97 0.5


Nitrate-N 4.00 80-120mg/l0.208.06 4.06 100


Chloride 20.0 80-120mg/l2.054.9 35.7 96

Nitrate-N 4.00 80-120mg/l0.204.19 0.363 96

Sulfate 20.0 80-120mg/l2.069.9 52.0 89


Nitrate-N 4.00 1580-120mg/l0.208.01 4.06 99 0.7


Chloride 20.0 1580-120mg/l2.056.3 35.7 103 3

Nitrate-N 4.00 1580-120mg/l0.204.48 0.363 103 7

Sulfate 20.0 1580-120mg/l2.071.3 52.0 96 2



Chloride mg/l2.0ND

Sulfate mg/l2.0ND

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers


LCS Analyzed: 03/08/2010 (10C0337-BS1)

Chloride 20.0 90-110mg/lNA19.3 96

Sulfate 20.0 90-110mg/lNA19.3 96


Chloride 20.0 1590-110mg/lNA19.3 96 0.04

Sulfate 20.0 1590-110mg/lNA19.3 96 0.1


Chloride 20.0 80-120mg/l2.034.5 13.0 107

Sulfate 20.0 80-120mg/l2.020.4 0.340 101


Chloride 20.0 80-120mg/l2.023.0 3.05 100

Sulfate 20.0 80-120mg/l2.031.4 11.7 98


Chloride 20.0 1580-120mg/l2.034.7 13.0 109 0.8

Sulfate 20.0 1580-120mg/l2.020.8 0.340 102 1


Chloride 20.0 1580-120mg/l2.023.6 3.05 103 2

Sulfate 20.0 1580-120mg/l2.032.0 11.7 101 2




Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers


LCS Analyzed: 03/06/2010 (10C0338-BS1)

Nitrate-N 4.00 90-110mg/lNA3.84 96


Nitrate-N 4.00 1590-110mg/lNA3.85 96 0.2

Matrix Spike Analyzed: 03/06/2010 (10C0338-MS1) Source: PTC0324-07RE1

Nitrate-N 20.0 80-120mg/l1.040.0 20.3 99

Matrix Spike Dup Analyzed: 03/06/2010 (10C0338-MSD1) Source: PTC0324-07RE1

Nitrate-N 20.0 1580-120mg/l1.039.6 20.3 96 1




LCS Analyzed: 03/09/2010 (10C0379-BS1)







Phosphorus,Total - P 0.300 2080-120mg/l0.502.09 M21.86 78 0.2

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers








LCS Analyzed: 03/15/2010 (10C0550-BS1)




Duplicate Analyzed: 03/15/2010 (10C0550-DUP1) Source: PTC0324-05RE1


Bicarbonate Alkalinity as CaCO3 20mg/l6.0ND ND

Carbonate Alkalinity as CaCO3 20mg/l6.01020 1020 0

Hydroxide Alkalinity as CaCO3 20mg/l6.0460 450 2

Alkalinity, Phenolphthalein 20mg/l6.0970 960 1




LCS Analyzed: 03/15/2010 (10C0558-BS1)

Perchlorate 25.0 85-115ug/l2.022.8 91

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers



Perchlorate 25.0 1585-115ug/l2.022.8 91 0.4






Perchlorate 25.0 80-120ug/l2.026.0 3.67 89


Perchlorate 25.0 80-120ug/l2.025.8 3.71 88


Perchlorate 25.0 1580-120ug/l2.026.8 3.67 92 3


Perchlorate 25.0 1580-120ug/l2.025.8 3.71 88 0.1

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers




LCS Analyzed: 03/09/2010 (10C0336-BS1)








Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorate ug/l20ND

Chlorite ug/l20ND


LCS Analyzed: 03/16/2010 (10C1985-BS1)

Chlorate 100 75-125ug/l2099.8 100

Chlorite 100 75-125ug/l2098.2 98



Chlorate 100 75-125ug/l40600 M3525 75

Chlorite 100 75-125ug/l4082.9 ND 83



Chlorate 100 75-125ug/l4097.5 ND 98

Chlorite 100 75-125ug/l4094.6 ND 95



Chlorate 100 2575-125ug/l40598 M3525 72 0.4

Chlorite 100 2575-125ug/l4083.8 ND 84 1



Chlorate 100 2575-125ug/l4093.5 ND 93 4

Chlorite 100 2575-125ug/l4092.4 ND 92 2


Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00


B1 Target analyte detected in method blank at or above the method reporting limit.


H2 Initial analysis within holding time. Reanalysis for the required dilution was past holding time.








Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




454-9303





Sampled:

Received:

03/04/10


Project ID:

PTC0324

PGA North/103965.00



TestAmerica Phoenix

Water XE200.7

Water XEPA 300.0

Water XEPA 314.0

XWater XEPA 8260B

Water XM2320 B

Water XM4500-P B, E

Water XM5310B

WaterSM 4500-P B, E






Analysis Performed: HydrogenSamples: PTC0324-01, PTC0324-07, PTC0324-09, PTC0324-12



Method Performed: EPA 300.1Samples: PTC0324-01, PTC0324-05, PTC0324-07, PTC0324-09, PTC0324-12

Project Manager

TestAmerica Phoenix

PTC0324

Kylie Emily




SENDING LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 189 - Phoeriix,·AZ 85040 ·· - ··

Phone: (602) 437-3340

Fax: (602) 454-9303 Project Manager: Kylie Emily ·client: Environmental Resources Management lnc.,West.---

Analysis Units Due

Sample ID: PTC0324-01 (IRZ-MW-C-0~042010- Water)

PTC0324


TestAmerica Irvine

17 461 Derian Ave. Suite 1 00 Irvine, CA 92614

Phone :(949) 261-1022

Fax: (949) 261-1228 Project Location: AZ. - ARIZONA

···Receipt Temperature:· : . · "C


Sampled: 03/04/10 08:31 Chlorate (300.1)


mg/1

mg/1

03/19/10 04/01/10 08:31 $30.00 0% Irvine

0% Irvine 03/19/10 03/18/10 08:31 $30.00


500 ml Poly w/EDA (L) 125mL Brown Poly w/ EDA (M)

Sample ID: PTC0324-05 (IRZ-MW-B-03042010- Water) Sampled: 03104110 10:15 Chlorate (300.1) mg/1 03/19/10 04/01/10 10:15 $30.00 0% Irvine

Chlorite (300.1) - 0 mg/1 03/19/10 03/18/10 10:15 $30.00 0% Irvine


500 ml Poly w/EDA (L) 125mL Brown Poly w/ EDA(M

Sample ID: PTC0324-07 (IRZ-MW-D-0304201 0 -Water) Sampled: 0310411 o 11 :1 o Chlorate (300.1) mg/1 03/19/10 04/01/10 11:10 $30.00 0% Irvine

Chlorite (300.1) - 0 mg/1 0311911 0 03/18/1 0 11:1 0


500 ml Poly w/EDA (L) 125mL Brown Poly w/ EDA M

$30.00 0% Irvine

Sample 10: PTC0324-09 (IRZ-IW-3-03042010- Water) Sam led: 03104110 13: 3 Chlorate (300.1) mg/1 03/19/10 04/01/10 13:23 $30.00 0% Irvine

Chlorite (300.1) - 0 mg/1 03/19/10 03/18/10 13:23


500 ml Poly w/EDA (L) 125mL Brown Poly w/ EDA (M)

_n~"--~ ___ & )!D /1~ D

Rea Date/Time

Released By Date/Time

$30.00 0% Irvine

lee: Y ·I N ·

Analysis Units Due


PTC0324

· Expires lnteriab Price Surch Comments

Sample ID: PTC0324-12 (IRZ-IW-1-03042010- Water) ... Sampled: 03/04/10 15:00

Chlorate (300.1)


mg/1

mg/1

03/19/10 04/01/10 15:00 $30.00 0% Irvine

03/19/10 .. 03/18/10 15:00 $30.00 0% Irvine


50U·m.rPoly w/EDA.(L). 125niL"BroWri Polljw/ EDA (M), . .

Page 2 of2


TAL-0013-550 (12/08)

Client Name/Address: fi 111&16.., S0~oo/ E RM 7)7) ~;., 1TJ1{01

~c...o-t"f'$ Jalf ..A-2. ~ s-..J~ J

Project Manager: p~11 J Q. Cl-to.~j

Sampler:

I. S v~a wtJ.c~ tv-· Sample Container Sample Description Matrix Type


[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

p;:~p~~. Analysis Required

)'-... r . to 3 9 6 S. o b ;;> ---;$

o;;:, ,........,_

t.t~ Phone Number:

=~ 't9<J :):Lft'J/ ~ ""-Leg 0 'I,.. ~ """" ~ :'-~ '-( 0~ .. ~ ~ . Fax Number: ~ +' ..... ...... <:1.. --.s:"

t.f2 D ,9g ~ ro & -o --.:? - ·>. ~Q ~:::: .Q,. ._}

....-) ---s ~ -.::: .,_ .;_ "" <1. "' I( 0

~ #of Sampling Sampling --- ~ '"" ~ Preservatives 99. -S ~· ~~ \2 Cont. Date Time ~ ~..) ~\,.,~ .Q Q.

Page of

I

.... t i- '\-~ -')..' ~ ~ 0 - .t ~...s

:r--W (\ ..... " "- \ ~ --"=- ~

-i?::! )...

~ v.~ ...:: Special Instructions

JRJ.-!r1w-c-o~o'f~o 10 }-P.} u ilti;r,(J) 15 5A~ og;f V'a~,(J< ~ ~ >r X X' ~ ~ ).,-- ~ X -Dl1 o2.

I R~-M w-c..-o.rM ::lDto fJ 1-1 0 VoA 5 ~/rfio D11J }-{ c/ X -o3

J~:?.-Iw-:t- O.JfJ'I ~o 'o· N:.U rll).jr{ tJ 7 s/lf.l!-o U<JlD )(' ;;( -P4 ~?/.AI\) QflVI V '~ .Ir;?2.-l.ii{w_g -o30if .)~ IQ 1-L 0 ~r!Vit?t II-( Y"flti> Mt5 Vl).,..f'J ){ y 2( X y ~ / ~ X ~ ~ -VS o~.n '\. o t~-1 '1 1.0&--M w.:. D-o 3 o'f :.\ rl 'o /-{:, 0 llol""lt"S ~~ 1h,{l> /110 Vtrvlff X' ~ y Y' y ~· '(\" ~ v ~ ),f.c.a.lvr(l PP ~ l!Rz.-2\J- ~-o~o"f<;)r; /o H;b lllll"'1~ 15 Yo/iu n:rr 'Vl~V'tfls >< K y ~ K ;>(' ~ ~ ~ )( ~ lJ. '1 frff r fV(),

•. rJ,.,i>;

Yrt2.-lVV'-s -01 o-f~olo R KiJ Vo~t 5 1/'1/w q~tf t-lv( v I -~,

¥ -ll

iR'2-- .3:\v- ko $ O\.f J om H'lu ~v-lt'<; . J5 v~tl Is ~v lld-Ylf~ X ~ x--- x:- y x- ~ K X X - t z..l 13

Ti:_t& _Bj tf-Ak . .-/ X' .-j~ o8~ I~ If 10 I

t:j/avt h'- -} k - ~~ )~j_~ ~~~OD. lrt,;t:l '

Relinquished By: Datet~~C Received By: Date/Time: Turnaround Time: (Check)

::~~_/2{ --'\.... Y1; 10 '717 , .... ----, same day 72 hours

Relinquished ,asz7 Date/Time: • Rec~~: Date/Time: 24 hours 5 days

I \ } 48 hours normal

Relinquished By: Date/Time: r;flcr:e:_l.._,~y: 7:ter;me: Sample Integrity: {Check) j ·Ob

j ~r-1" -·- 3'lf ro·-t-rr~ intact /) on ice x· .-(

Note: By relinquishing sampies to TestAmerica, client a rees to a for t~~nhces re u/sted on this chain of cu~tody form and an g p y q y additional anal ses y p erformed on this ro·ect. p J oc:.... Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

Client Name: Test America Page: Page 1 of 7 - ------------ ---GGntact;--Kylie-Emily---- --------------------------l:abProj-#:-P-100307-9--- -------------

Lab Sample#

P1 003079-01

P1 003079-02

P1 003079-03

P1 003079-04

Address: 4625 East Cotton Center Blvd. Report Date: 03/19/10 Suite 189 Client Proj Name: PTC0324

· ~-Phoenix, AZ 85040 Client Proj #: PTC0324

Client Sample ID

PTC0324-01

PTC0324-07

PTC0324-09

PTC0324-12

Laboratory Results Total pages in data package:

Microseeps test results meet all the requirements of the NELAC standards or provide reasons andfor justification if they do not.

Approved By: {}fr})

Protect Manager: Debbie Halla



Case Narrative:

As a valued client we would appreciate your comments on our service. Please call customer service at (412)826-5245 or email [email protected] ..









SamQied DaterTime Received PTC0324-01 Vapor P1 003079-01 04 Mar. 10 8:31 08 Mar. 10 12:35

Analyte(s) Flag Result PQL Units Method# Analysis Date

RiskAnalysis N Hydrogen 5900.000 120.000 nM AM2DGAX 3/16/10

Data Qualifiers: J. estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MSfMSD, SAMP/DUP, B- detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L • Subcontracted Lab used, N - NELAC certified analysis

By

sl

Client Name: Test America Contact Kylie Emily


Sam(;!le DescriQtion Matrix Lab Sample#




SamQied Date/Time Received PTC0324·07 Vapor P1 003079-02 04 Mar. 1 0 11: 1 0 08 Mar. 10 12:35


Data Qualifiers: J- estimated value, U- Non detect, R- Poor surrogate recovery, M • Recovery/RPD poor for MS/MSD, SAMP/DUP, B- detected in blank, S ~field sample as received did not meet NELAC sample acceptance criteria, L- Subcontmoted Lab used, N- NELAC certified analysis

By

sl


Address: 4625 East Cotton Center Blvd.

Sample Description PTC0324-09

Analyte(s) RiskAnalysis N Hydrogen


Matrix Vapor

Flag


Result PQL Units

23.000 0.600 nM




Sampled DatefTime 04 Mar. 1 0 13:23

Received 08 Mar. 10 12:35

Method# Analysis Date By

AM20GAX 3/15/10 sl

Data Qualifiers: J- estimated value, U- Non detec~ R- Poor surrogate recovery, M- Recovery!RPD poor for MS/MSD, SAMP/DUP, B -detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N - NELAC certified analysis


Suite 189 Phoenlx:, AZ 85040

Sam~le Descri~tion Matrix Lab Sample#




Samgled DatefTime Received PTC0324-12 Vapor P1 003079-04 04 Mar. 1 0 15:00 08 Mar. 1 0 12:35

Analyte(s~ Flag Result PQL Units Method# Analysis Date RiskAnalysis N Hydrogen 42.000 0.600 nM AM20GAX 3/15/10

Data Qualifiers: J- estimated value, U ·Non detect, R ·Poor surrogate recovel}', M- Recovel}'/RPD poor for MS/MSD, SAMP/DUP, B -detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L ·Subcontracted Lab used, N- NELAC certified analysis

By

sl



Prep Method:

Analysis Method:

M100317033"MB

Result TrueS:gikeConc. RDL


M100317033"LCS



M100317033-LCSD








%Recover:y Ctl Limits

- NA

%Recover:y Ctr Limits

90.00 75-125

%Recover:y Ctl Limits RPD

89.00 75-125 1.14

RPD Ctl Limits

0. 20

'---------'1 Outlined Results indicate results outside of Control limits

Data Qualifiers: J ·estimated value, U ·Non detect, R ·Poor surrogate recovery, M • Recovery/RPD poor for MS/MSD, SAMP/DUP, B- detected in blank, S - field sample as received did not meet NELAC sample acceptance criteria, L • Subcontracted Lab used, N - NELAC certified analysis



Prep Method:

Analysis Method:

M1 00317034-MB

Result TrueSnikeConc. RDL


M1 00317034-LCS



M100317034-LCSD









- NA


98.00 75- 125

%RecoverY Ctl Limits RPD

99.00 75-125 1.04

RPD Ctl Limits

0-20

~..-. ___ .._.__jl Outlined Results indicate results outside of Control limits

Data Qualifiers: J -estimated value, U -Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSO, SAMP/DUP, B -detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N- NELAC certified analysis


PTC0324

SENDING LABORATORY: RECEIVING LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 189 c) 7l Microseeps/Univ of Pittsburgh App Research Center

Phoenix, /lZ 85040.. · · · ·- · ~ · 0) ·· 220 William Pitt Way - ---- -- - - -- · - - - - -

Phone: (602) 437-3340 \/ 0 Fax: (602) 454-9303

. Pittsburgh,.PA 15238 .. Phone :(412)826-5245 Fax: (412)826-3433

Project Manager: Kylie Emily Project Location: /lZ -ARIZONA · ··· 'Receipt"Temperature: - ·· · oc · Ice: .. Y ·f ·N · ..


Analysis Units Expires

Sample 10: PTC0324-01 (IRZ-MW-C-03042010 ·Water) Sampled: 03104110 oa:31

Hydrogen % 04/01/10 08:31


NA N

Sample ID: PTC0324-07 (IRZ-MW-D-03042010 ·Water)

Hydrogen


"-JA

%

Sample ID: PTC0324-09 (IRZ-lW-3-0304201 0 • Water)

Hydrogen


NA(N)

%

Sample 10: PTC0324-12 (IRZ-IW~1-0304201 0 ·• Water)

Hydrogen


NA(N)

%

Sampled: 03/04/10 11 :10 04/01/10 11:10

Sampled: 03/04/1 0 13:23 04/01/10 13:23

Sampled: 03/04/10 15:00 04/01/10 15:00

Relea~ J/4 /tf?o Daternme

Comments

DO NOT CHlLUNO lCE-Microseeps

DO NOT CHlLUNO lCE-Microseeps

DO NOT CHILUNO ICE-Microseeps

DO NOT CHILUNO ICE~Microseeps

/?:~ o0 Daternme

!DUO n~temme Page 1 of 1


454-9303

LABORATORY REPORT





Received:

Issued:

05/05/10

05/05/10

05/25/10 12:02







Project: PGA North/103965


CASE NARRATIVE


PTE0287-01 IRZ-MW-D-115-05052010 Water

PTE0287-02 IRZ-MW-D-125-05052010 Water

PTE0287-03 IRZ-MW-C-115-05052010 Water

PTE0287-04 IRZ-MW-C-125-05052010 Water

PTE0287-05 IRZ-IW-5-05052010 Water

PTE0287-06 IRZ-IW-4-05052010 Water

PTE0287-07 IRZ-IW-4-05052010R Water

PTE0287-08 IRZ-MW-C-05052010 Water

PTE0287-09 IRZ-MW-C-05052010D Water

PTE0287-10 Trip Blank Water

Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily

<Page 1 of 48>


454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965





N1 = Sample PTE0287-05 did not have a pH < 2 S.U. per method requirements. The sample had black

sediment in the bottom of each vial. Each vial had a pH of 3 S.U.


N1a-The RPD exceeded the acceptance limit due to sample matrix effects.



Reviewed By:

Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-01 (IRZ-MW-D-115-05052010 - Water) Sampled: 05/05/10


5/6/20105/6/2010EPA 8260BAcetone 1010E0200 1ND

Benzene 5/6/20105/6/201010E0200 0.50 1EPA 8260B 3.6

5/6/20105/6/2010EPA 8260BBromobenzene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BBromochloromethane 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BBromodichloromethane 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BBromoform 1.010E0200 1ND

5/6/20105/6/2010EPA 8260BBromomethane 1.010E0200 1ND

5/6/20105/6/2010EPA 8260B2-Butanone (MEK) 2.510E0200 1ND

5/6/20105/6/2010EPA 8260Bn-Butylbenzene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260Bsec-Butylbenzene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260Btert-Butylbenzene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BCarbon disulfide 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BCarbon tetrachloride 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BChlorobenzene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BChloroethane 1.010E0200 1ND

5/6/20105/6/2010EPA 8260BChloroform 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BChloromethane 1.010E0200 1ND

5/6/20105/6/2010EPA 8260B2-Chlorotoluene 0.5010E0200 1ND


5/6/20105/6/2010EPA 8260BDibromochloromethane 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260B1,2-Dibromo-3-chloropropane 2.510E0200 1ND

5/6/20105/6/2010EPA 8260B1,2-Dibromoethane (EDB) 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BDibromomethane 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260B1,2-Dichlorobenzene 0.5010E0200 1ND



5/6/20105/6/2010EPA 8260BDichlorodifluoromethane 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260B1,1-Dichloroethane 0.5010E0200 1ND


5/6/20105/6/2010EPA 8260B1,1-Dichloroethene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260Bcis-1,2-Dichloroethene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260Btrans-1,2-Dichloroethene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260B1,2-Dichloropropane 0.5010E0200 1ND



5/6/20105/6/2010EPA 8260B1,1-Dichloropropene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260Bcis-1,3-Dichloropropene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260Btrans-1,3-Dichloropropene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BEthylbenzene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BHexachlorobutadiene 1.010E0200 1ND

Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-01 (IRZ-MW-D-115-05052010 - Water) - cont. Sampled: 05/05/10


5/6/20105/6/2010EPA 8260B2-Hexanone 2.510E0200 1ND

5/6/20105/6/2010EPA 8260BIodomethane 2.510E0200 1ND

5/6/20105/6/2010EPA 8260BIsopropylbenzene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260Bp-Isopropyltoluene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BMethylene Chloride 1.010E0200 1ND

5/6/20105/6/2010EPA 8260B4-Methyl-2-pentanone (MIBK) 2.510E0200 1ND

5/6/20105/6/2010EPA 8260BMethyl-tert-butyl Ether (MTBE) 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BNaphthalene 2.510E0200 1ND

5/6/20105/6/2010EPA 8260Bn-Propylbenzene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BStyrene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260B1,1,1,2-Tetrachloroethane 0.5010E0200 1ND


5/6/20105/6/2010EPA 8260BTetrachloroethene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BToluene 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260B1,2,3-Trichlorobenzene 1.010E0200 1ND


5/6/20105/6/2010EPA 8260B1,1,1-Trichloroethane 0.5010E0200 1ND


Trichloroethene 5/6/20105/6/201010E0200 0.50 1EPA 8260B 69

5/6/20105/6/2010EPA 8260BTrichlorofluoromethane 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260B1,2,3-Trichloropropane 1.010E0200 1ND

5/6/20105/6/2010EPA 8260B1,2,4-Trimethylbenzene 0.5010E0200 1ND


5/6/20105/6/2010EPA 8260BVinyl Acetate 1.010E0200 1ND

5/6/20105/6/2010EPA 8260BVinyl chloride 0.5010E0200 1ND

5/6/20105/6/2010EPA 8260BXylenes, Total 1.010E0200 1ND




Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-02 (IRZ-MW-D-125-05052010 - Water) Sampled: 05/05/10


5/6/20105/6/2010EPA 8260BAcetone 1010E0200 1ND

Benzene 5/6/20105/6/201010E0200 0.50 1EPA 8260B 3.8






2-Butanone (MEK) 5/6/20105/6/201010E0200 2.5 1EPA 8260B 2.9

































Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-02 (IRZ-MW-D-125-05052010 - Water) - cont. Sampled: 05/05/10











5/6/20105/6/2010EPA 8260BStyrene 0.5010E0200 1ND




5/6/20105/6/2010EPA 8260BToluene 0.5010E0200 1ND
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-03 (IRZ-MW-C-115-05052010 - Water) Sampled: 05/05/10


5/6/20105/6/2010EPA 8260BAcetone 1010E0200 1ND

Benzene 5/6/20105/6/201010E0200 0.50 1EPA 8260B 28







































Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-03 (IRZ-MW-C-115-05052010 - Water) - cont. Sampled: 05/05/10











5/6/20105/6/2010EPA 8260BStyrene 0.5010E0200 1ND




5/6/20105/6/2010EPA 8260BToluene 0.5010E0200 1ND
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-04 (IRZ-MW-C-125-05052010 - Water) Sampled: 05/05/10


5/6/20105/6/2010EPA 8260BAcetone 1010E0200 1ND

Benzene 5/6/20105/6/201010E0200 0.50 1EPA 8260B 29







































Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-04 (IRZ-MW-C-125-05052010 - Water) - cont. Sampled: 05/05/10











5/6/20105/6/2010EPA 8260BStyrene 0.5010E0200 1ND




5/6/20105/6/2010EPA 8260BToluene 0.5010E0200 1ND
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-05 (IRZ-IW-5-05052010 - Water) Sampled: 05/05/10 N1


5/6/20105/6/2010EPA 8260BAcetone 10010E0200 10ND

5/6/20105/6/2010EPA 8260BBenzene 5.010E0200 10ND




5/6/20105/6/2010EPA 8260BBromoform 1010E0200 10ND

5/6/20105/6/2010EPA 8260BBromomethane 1010E0200 10ND

5/6/20105/6/2010EPA 8260B2-Butanone (MEK) 2510E0200 10ND







5/6/20105/6/2010EPA 8260BChloroethane 1010E0200 10ND


5/6/20105/6/2010EPA 8260BChloromethane 1010E0200 10ND




5/6/20105/6/2010EPA 8260B1,2-Dibromo-3-chloropropane 2510E0200 10ND














5/6/20105/6/2010EPA 8260B2,2-Dichloropropane 1010E0200 10ND





5/6/20105/6/2010EPA 8260BHexachlorobutadiene 1010E0200 10ND

Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-05 (IRZ-IW-5-05052010 - Water) - cont. Sampled: 05/05/10 N1


5/6/20105/6/2010EPA 8260B2-Hexanone 2510E0200 10ND

5/6/20105/6/2010EPA 8260BIodomethane 2510E0200 10ND



5/6/20105/6/2010EPA 8260BMethylene Chloride 1010E0200 10ND

5/6/20105/6/2010EPA 8260B4-Methyl-2-pentanone (MIBK) 2510E0200 10ND


5/6/20105/6/2010EPA 8260BNaphthalene 2510E0200 10ND


5/6/20105/6/2010EPA 8260BStyrene 5.010E0200 10ND




5/6/20105/6/2010EPA 8260BToluene 5.010E0200 10ND

5/6/20105/6/2010EPA 8260B1,2,3-Trichlorobenzene 1010E0200 10ND






5/6/20105/6/2010EPA 8260B1,2,3-Trichloropropane 1010E0200 10ND



5/6/20105/6/2010EPA 8260BVinyl Acetate 1010E0200 10ND


5/6/20105/6/2010EPA 8260BXylenes, Total 1010E0200 10ND




Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-06 (IRZ-IW-4-05052010 - Water) Sampled: 05/05/10


5/6/20105/6/2010EPA 8260BAcetone 10010E0200 10ND

5/6/20105/6/2010EPA 8260BBenzene 5.010E0200 10ND







































Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-06 (IRZ-IW-4-05052010 - Water) - cont. Sampled: 05/05/10











5/6/20105/6/2010EPA 8260BStyrene 5.010E0200 10ND




5/6/20105/6/2010EPA 8260BToluene 5.010E0200 10ND
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-07RE1 (IRZ-IW-4-05052010R - Water) Sampled: 05/05/10


5/7/20105/7/2010EPA 8260BAcetone 1010E0257 1ND

5/7/20105/7/2010EPA 8260BBenzene 0.5010E0257 1ND



Bromodichloromethane 5/7/20105/7/201010E0257 0.50 1EPA 8260B 2.3











Chloroform 5/7/20105/7/201010E0257 0.50 1EPA 8260B 5.0




Dibromochloromethane 5/7/20105/7/201010E0257 0.50 1EPA 8260B 0.63





















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-07RE1 (IRZ-IW-4-05052010R - Water) - cont. Sampled: 05/05/10











5/7/20105/7/2010EPA 8260BStyrene 0.5010E0257 1ND




5/7/20105/7/2010EPA 8260BToluene 0.5010E0257 1ND





5/7/20105/7/2010EPA 8260BTrichloroethene 0.5010E0257 1ND











Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-08 (IRZ-MW-C-05052010 - Water) Sampled: 05/05/10


5/6/20105/6/2010EPA 8260BAcetone 5010E0200 5ND

5/6/20105/6/2010EPA 8260BBenzene 2.510E0200 5ND







































Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-08 (IRZ-MW-C-05052010 - Water) - cont. Sampled: 05/05/10











5/6/20105/6/2010EPA 8260BStyrene 2.510E0200 5ND




5/6/20105/6/2010EPA 8260BToluene 2.510E0200 5ND
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-09 (IRZ-MW-C-05052010D - Water) Sampled: 05/05/10


5/6/20105/6/2010EPA 8260BAcetone 10010E0200 10ND

5/6/20105/6/2010EPA 8260BBenzene 5.010E0200 10ND







































Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-09 (IRZ-MW-C-05052010D - Water) - cont. Sampled: 05/05/10











5/6/20105/6/2010EPA 8260BStyrene 5.010E0200 10ND




5/6/20105/6/2010EPA 8260BToluene 5.010E0200 10ND
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-10 (Trip Blank - Water) Sampled: 05/05/10


5/6/20105/6/2010EPA 8260BAcetone 1010E0200 1ND

5/6/20105/6/2010EPA 8260BBenzene 0.5010E0200 1ND







































Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0287-10 (Trip Blank - Water) - cont. Sampled: 05/05/10











5/6/20105/6/2010EPA 8260BStyrene 0.5010E0200 1ND




5/6/20105/6/2010EPA 8260BToluene 0.5010E0200 1ND
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 5/12/20105/6/201010E0212 5.0 100E200.7 1600



Iron 5/12/20105/6/201010E0212 5.0 100E200.7 1000



Iron 5/10/20105/6/201010E0212 0.050 1E200.7 35

Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Perchlorate 5/12/20105/12/201010E0409 10 5EPA 314.0 12



Perchlorate 5/12/20105/12/201010E0409 2.0 1EPA 314.0 12



Perchlorate 5/12/20105/12/201010E0409 2.0 1EPA 314.0 8.7

Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

Batch: 10E0200 Extracted: 05/06/10

Blank Analyzed: 05/06/2010 (10E0200-BLK1)

Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/06/2010 (10E0200-BS1)

Acetone 25.0 10-150ug/l1023.7 95

Benzene 25.0 80-120ug/l0.5025.4 102




Bromoform 25.0 75-130ug/l1.023.8 95


2-Butanone (MEK) 25.0 40-150ug/l2.524.3 97








Chloroform 25.0 75-120ug/l0.5025.2 101




















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/06/2010 (10E0200-BS1)






2-Hexanone 25.0 20-150ug/l2.525.8 103

Iodomethane 25.0 80-130ug/l2.526.8 107






Naphthalene 25.0 40-150ug/l2.525.5 102


Styrene 25.0 80-120ug/l0.5028.5 114




Toluene 25.0 80-120ug/l0.5026.0 104
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Dup Analyzed: 05/06/2010 (10E0200-BSD1)

Acetone 25.0 10-150ug/l1024.0 96 1 35

Benzene 25.0 80-120ug/l0.5023.5 94 8 15

Bromobenzene 25.0 80-120ug/l0.5025.1 100 5 15

Bromochloromethane 25.0 80-125ug/l0.5023.9 96 7 15

Bromodichloromethane 25.0 80-120ug/l0.5024.7 99 6 15

Bromoform 25.0 75-130ug/l1.023.5 94 1 20

Bromomethane 25.0 55-150ug/l1.022.0 88 6 20

2-Butanone (MEK) 25.0 40-150ug/l2.523.4 94 4 35

n-Butylbenzene 25.0 80-130ug/l0.5026.6 106 2 15

sec-Butylbenzene 25.0 80-125ug/l0.5025.2 101 6 15

tert-Butylbenzene 25.0 80-120ug/l0.5026.1 104 3 15

Carbon disulfide 25.0 70-140ug/l0.5025.8 103 3 15

Carbon tetrachloride 25.0 75-130ug/l0.5025.6 102 5 20

Chlorobenzene 25.0 80-120ug/l0.5024.9 100 6 15

Chloroethane 25.0 70-130ug/l1.023.3 93 3 15

Chloroform 25.0 75-120ug/l0.5023.8 95 6 15

Chloromethane 25.0 60-140ug/l1.022.4 90 3 20

2-Chlorotoluene 25.0 80-120ug/l0.5025.0 100 4 15


Dibromochloromethane 25.0 80-120ug/l0.5026.3 105 6 15

1,2-Dibromo-3-chloropropane 25.0 50-150ug/l2.522.6 91 6 35

1,2-Dibromoethane (EDB) 25.0 80-120ug/l0.5025.4 101 7 15

Dibromomethane 25.0 75-120ug/l0.5025.5 102 4 15

1,2-Dichlorobenzene 25.0 80-120ug/l0.5024.7 99 4 15

1,3-Dichlorobenzene 25.0 80-120ug/l0.5025.7 103 0.4 15


Dichlorodifluoromethane 25.0 60-150ug/l0.5024.3 97 4 30

1,1-Dichloroethane 25.0 70-125ug/l0.5023.9 95 4 15


1,1-Dichloroethene 25.0 75-125ug/l0.5023.9 96 8 20

cis-1,2-Dichloroethene 25.0 80-120ug/l0.5023.6 94 8 15

trans-1,2-Dichloroethene 25.0 80-120ug/l0.5024.7 99 3 15

1,2-Dichloropropane 25.0 80-120ug/l0.5024.6 98 5 15



Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 75-120ug/l0.5025.3 101 7 15

cis-1,3-Dichloropropene 25.0 80-120ug/l0.5025.8 103 5 15

trans-1,3-Dichloropropene 25.0 80-125ug/l0.5026.4 105 6 15

Ethylbenzene 25.0 80-120ug/l0.5026.3 105 1 15

Hexachlorobutadiene 25.0 40-150ug/l1.024.3 97 4 35

2-Hexanone 25.0 20-150ug/l2.525.5 102 1 35

Iodomethane 25.0 80-130ug/l2.526.0 104 3 10

Isopropylbenzene 25.0 80-130ug/l0.5029.1 116 5 15

p-Isopropyltoluene 25.0 80-130ug/l0.5026.4 106 4 15

Methylene Chloride 25.0 70-120ug/l1.023.2 93 3 15

4-Methyl-2-pentanone (MIBK) 25.0 60-135ug/l2.524.7 99 5 25

Methyl-tert-butyl Ether (MTBE) 25.0 70-130ug/l0.5024.3 97 3 20

Naphthalene 25.0 40-150ug/l2.525.6 102 0.2 30

n-Propylbenzene 25.0 75-130ug/l0.5027.6 110 3 15

Styrene 25.0 80-120ug/l0.5027.6 110 3 15

1,1,1,2-Tetrachloroethane 25.0 75-125ug/l0.5026.3 105 1 15

1,1,2,2-Tetrachloroethane 25.0 80-120ug/l0.5025.8 103 0.2 20

Tetrachloroethene 25.0 70-130ug/l0.5026.7 107 3 20

Toluene 25.0 80-120ug/l0.5024.5 98 6 15

1,2,3-Trichlorobenzene 25.0 55-150ug/l1.024.5 98 6 35


1,1,1-Trichloroethane 25.0 75-125ug/l0.5023.8 95 5 15


Trichloroethene 25.0 80-120ug/l0.5024.0 96 10 15

Trichlorofluoromethane 25.0 70-150ug/l0.5024.4 98 0.2 25

1,2,3-Trichloropropane 25.0 70-130ug/l1.024.4 97 2 20

1,2,4-Trimethylbenzene 25.0 80-120ug/l0.5027.1 108 0.7 15

1,3,5-Trimethylbenzene 25.0 80-130ug/l0.5026.2 105 8 15

Vinyl Acetate 25.0 40-150ug/l1.020.8 83 16 25

Vinyl chloride 25.0 70-130ug/l0.5023.5 94 2 20

Xylenes, Total 50.0 60-140ug/l1.051.6 103 5 15




Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 05/06/2010 (10E0200-MS1) Source: PTE0288-02

Acetone 25.0 10-150ug/l1025.3 ND 101

Benzene 25.0 70-125ug/l0.5023.3 ND 93




Bromoform 25.0 65-125ug/l1.021.1 ND 84











Chloromethane 25.0 55-145ug/l1.021.4 0.180 85



















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.526.6 ND 106









Styrene 25.0 55-135ug/l0.5022.1 ND 89




Toluene 25.0 70-125ug/l0.5023.1 0.490 91
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 05/06/2010 (10E0200-MSD1) Source: PTE0288-02

Acetone 25.0 10-150ug/l1025.1 ND 101 0.8 35

Benzene 25.0 70-125ug/l0.5025.0 ND 100 7 25

Bromobenzene 25.0 75-120ug/l0.5026.5 ND 106 12 20

Bromochloromethane 25.0 75-130ug/l0.5025.7 ND 103 8 20

Bromodichloromethane 25.0 75-125ug/l0.5026.7 ND 107 12 20

Bromoform 25.0 65-125ug/l1.023.9 ND 95 12 25

Bromomethane 25.0 45-150ug/l1.025.3 ND 101 18 35

2-Butanone (MEK) 25.0 15-150ug/l2.525.3 ND 101 2 30

n-Butylbenzene 25.0 70-130ug/l0.5027.9 ND 112 13 30

sec-Butylbenzene 25.0 70-125ug/l0.5027.4 ND 109 12 30

tert-Butylbenzene 25.0 70-125ug/l0.5027.4 ND 110 10 25

Carbon disulfide 25.0 65-145ug/l0.5028.6 ND 114 12 25

Carbon tetrachloride 25.0 65-135ug/l0.5027.5 ND 110 13 25

Chlorobenzene 25.0 75-120ug/l0.5025.9 ND 104 11 20

Chloroethane 25.0 65-140ug/l1.024.8 ND 99 10 25

Chloroform 25.0 70-130ug/l0.5025.2 ND 101 6 20

Chloromethane 25.0 55-145ug/l1.024.9 0.180 99 15 35

2-Chlorotoluene 25.0 70-125ug/l0.5026.3 ND 105 12 25


Dibromochloromethane 25.0 70-130ug/l0.5027.2 ND 109 14 20

1,2-Dibromo-3-chloropropane 25.0 50-150ug/l2.527.3 ND 109 15 30

1,2-Dibromoethane (EDB) 25.0 70-125ug/l0.5027.0 ND 108 7 20

Dibromomethane 25.0 70-120ug/l0.5027.1 ND 109 6 20

1,2-Dichlorobenzene 25.0 75-120ug/l0.5026.2 ND 105 14 20



Dichlorodifluoromethane 25.0 60-150ug/l0.5027.1 ND 108 14 30

1,1-Dichloroethane 25.0 70-130ug/l0.5026.5 ND 106 12 20


1,1-Dichloroethene 25.0 70-130ug/l0.5026.9 ND 108 14 25

cis-1,2-Dichloroethene 25.0 70-125ug/l0.5025.3 ND 101 8 20

trans-1,2-Dichloroethene 25.0 75-125ug/l0.5025.7 ND 103 8 25

1,2-Dichloropropane 25.0 75-125ug/l0.5026.1 ND 104 7 20

1,3-Dichloropropane 25.0 70-120ug/l0.5025.8 0.700 100 5 20


Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 65-130ug/l0.5025.9 ND 104 7 25

cis-1,3-Dichloropropene 25.0 75-130ug/l0.5026.7 ND 107 12 20

trans-1,3-Dichloropropene 25.0 70-130ug/l0.5028.8 ND 115 10 20

Ethylbenzene 25.0 70-125ug/l0.5027.6 ND 110 16 25

Hexachlorobutadiene 25.0 40-150ug/l1.024.6 ND 98 12 30

2-Hexanone 25.0 20-150ug/l2.527.8 ND 111 4 30

Iodomethane 25.0 60-150ug/l2.527.6 ND 110 10 30

Isopropylbenzene 25.0 75-130ug/l0.5031.5 ND 126 14 25

p-Isopropyltoluene 25.0 70-130ug/l0.5028.0 ND 112 19 30

Methylene Chloride 25.0 65-130ug/l1.025.7 ND 103 11 20

4-Methyl-2-pentanone (MIBK) 25.0 55-135ug/l2.528.0 ND 112 9 25

Methyl-tert-butyl Ether (MTBE) 25.0 65-140ug/l0.5025.0 ND 100 6 25

Naphthalene 25.0 40-150ug/l2.526.3 ND 105 11 30

n-Propylbenzene 25.0 70-130ug/l0.5029.6 ND 118 16 30

Styrene 25.0 55-135ug/l0.5024.1 ND 96 9 35

1,1,1,2-Tetrachloroethane 25.0 70-125ug/l0.5026.0 ND 104 10 20


Tetrachloroethene 25.0 65-130ug/l0.5027.3 0.350 108 15 25

Toluene 25.0 70-125ug/l0.5025.8 0.490 101 11 20

1,2,3-Trichlorobenzene 25.0 50-150ug/l1.026.0 ND 104 13 35


1,1,1-Trichloroethane 25.0 70-130ug/l0.5025.5 ND 102 10 25


Trichloroethene 25.0 70-125ug/l0.5026.7 ND 107 12 25

Trichlorofluoromethane 25.0 65-150ug/l0.5026.8 ND 107 12 25

1,2,3-Trichloropropane 25.0 70-130ug/l1.027.8 ND 111 11 25

1,2,4-Trimethylbenzene 25.0 70-125ug/l0.5026.1 ND 104 11 30


Vinyl Acetate 25.0 40-150ug/l1.026.5 ND 106 7 30

Vinyl chloride 25.0 60-140ug/l0.5025.6 ND 102 17 25

Xylenes, Total 50.0 75-120ug/l1.053.9 N1aND 108 16 15




Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/07/2010 (10E0257-BS1)

Acetone 25.0 10-150ug/l1022.6 90

Benzene 25.0 80-120ug/l0.5022.9 92




Bromoform 25.0 75-130ug/l1.021.2 85


2-Butanone (MEK) 25.0 40-150ug/l2.521.8 87








Chloroform 25.0 75-120ug/l0.5022.4 90




















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/07/2010 (10E0257-BS1)






2-Hexanone 25.0 20-150ug/l2.522.1 89

Iodomethane 25.0 80-130ug/l2.525.5 102






Naphthalene 25.0 40-150ug/l2.524.7 99


Styrene 25.0 80-120ug/l0.5026.5 106




Toluene 25.0 80-120ug/l0.5025.0 100
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1025.2 101 11 35

Benzene 25.0 80-120ug/l0.5023.5 94 3 15


Bromochloromethane 25.0 80-125ug/l0.5023.9 96 0.8 15

Bromodichloromethane 25.0 80-120ug/l0.5024.1 97 0.1 15

Bromoform 25.0 75-130ug/l1.023.0 92 8 20

Bromomethane 25.0 55-150ug/l1.021.0 84 0.9 20

2-Butanone (MEK) 25.0 40-150ug/l2.523.9 96 9 35





Carbon tetrachloride 25.0 75-130ug/l0.5024.9 100 0.3 20



Chloroform 25.0 75-120ug/l0.5022.2 89 0.9 15



4-Chlorotoluene 25.0 80-120ug/l0.5024.3 97 0.2 15









1,1-Dichloroethane 25.0 70-125ug/l0.5021.9 88 0.2 15



cis-1,2-Dichloroethene 25.0 80-120ug/l0.5022.7 91 0.5 15




2,2-Dichloropropane 25.0 75-130ug/l1.021.8 87 0.7 15

Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.527.8 111 23 35

Iodomethane 25.0 80-130ug/l2.524.2 97 5 10






Naphthalene 25.0 40-150ug/l2.525.7 103 4 30

n-Propylbenzene 25.0 75-130ug/l0.5025.7 103 0.8 15

Styrene 25.0 80-120ug/l0.5028.5 114 8 15




Toluene 25.0 80-120ug/l0.5024.5 98 2 15



1,1,1-Trichloroethane 25.0 75-125ug/l0.5022.0 88 0.5 15


Trichloroethene 25.0 80-120ug/l0.5023.9 95 0.04 15

Trichlorofluoromethane 25.0 70-150ug/l0.5022.3 89 2 25




Vinyl Acetate 25.0 40-150ug/l1.022.6 91 0.7 25






Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1025.8 ND 103

Benzene 25.0 70-125ug/l0.5023.5 ND 94




Bromoform 25.0 65-125ug/l1.022.3 ND 89










Chloroform 25.0 70-130ug/l0.5026.3 4.05 89




















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.523.5 ND 94









Styrene 25.0 55-135ug/l0.5026.4 ND 106




Toluene 25.0 70-125ug/l0.5024.8 0.430 98
















Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1026.5 ND 106 3 35

Benzene 25.0 70-125ug/l0.5023.5 ND 94 0.04 25



Bromodichloromethane 25.0 75-125ug/l0.5026.5 1.91 98 4 20

Bromoform 25.0 65-125ug/l1.023.1 ND 92 3 25






Carbon disulfide 25.0 65-145ug/l0.5026.1 ND 104 0.3 25




Chloroform 25.0 70-130ug/l0.5027.5 4.05 94 5 20

Chloromethane 25.0 55-145ug/l1.022.2 ND 89 3 35



Dibromochloromethane 25.0 70-130ug/l0.5026.6 0.560 104 0.2 20



Dibromomethane 25.0 70-120ug/l0.5025.2 ND 101 0.4 20





1,1-Dichloroethane 25.0 70-130ug/l0.5023.0 ND 92 0.4 20

1,2-Dichloroethane 25.0 65-140ug/l0.5023.0 0.170 91 1 20







Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 65-130ug/l0.5023.6 ND 95 0.6 25





2-Hexanone 25.0 20-150ug/l2.524.0 ND 96 2 30

Iodomethane 25.0 60-150ug/l2.526.6 ND 106 0.7 30








Styrene 25.0 55-135ug/l0.5026.0 ND 104 2 35




Toluene 25.0 70-125ug/l0.5024.8 0.430 97 0.4 20





Trichloroethene 25.0 70-125ug/l0.5024.1 0.280 95 4 25

Trichlorofluoromethane 25.0 65-150ug/l0.5022.9 ND 92 0.6 25




Vinyl Acetate 25.0 40-150ug/l1.024.3 ND 97 0.5 30


Xylenes, Total 50.0 75-120ug/l1.049.7 ND 99 0.1 15




Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Iron mg/l0.050ND

LCS Analyzed: 05/10/2010 (10E0212-BS1)

Iron 1.00 85-115mg/l0.0500.944 94


Iron 1.00 85-115mg/l0.0500.957 96 1 20


Iron 1.00 75-125mg/l0.0501.07 0.0930 98


Iron 1.00 75-125mg/l0.0500.968 ND 97


Iron 1.00 75-125mg/l0.0501.08 0.0930 98 0.4 10


Iron 1.00 75-125mg/l0.0500.983 ND 98 1 10

Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers




LCS Analyzed: 05/12/2010 (10E0409-BS1)

Perchlorate 25.0 85-115ug/l2.027.4 110


Perchlorate 25.0 85-115ug/l2.027.3 109 0.5 15

Duplicate Analyzed: 05/12/2010 (10E0409-DUP1) Source: PTE0173-04

Perchlorate ug/l2.02.85 2.88 1 15




Perchlorate 25.0 80-120ug/l2.029.6 1.91 111


Perchlorate 25.0 80-120ug/l2.027.3 1.39 104


Perchlorate 25.0 80-120ug/l2.028.8 1.91 108 3 15


Perchlorate 25.0 80-120ug/l2.027.5 1.39 104 0.7 15

Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965





Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




454-9303





Sampled:

Received:

05/05/10


Project ID:

PTE0287

PGA North/103965



TestAmerica Phoenix

Water XE200.7

Water XEPA 314.0

XWater XEPA 8260B






Analysis Performed: HydrogenSamples: PTE0287-05, PTE0287-06, PTE0287-08

Project Manager

TestAmerica Phoenix

PTE0287

Kylie Emily




TAL-0013-550 (12/08)

Client Name/Address: J; _..,. A S ~ I E"~M 7).. 7}.. - ),:."'" lo\.-1/\ d ~ ~

. · sc;uf.•rvO

~ ++s ~~t(l A--2, Project Manager: PwL11. c.-~<{ Vl_!?

Sampler: /. 5c~~.)~.h...


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I r"1 tP Q ftvd--p V~-~ v

I


[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

Project/ PO Number: Analysis Required

(J ~A- ;V o--y lb-~9bS

~ Phone Num'l{'9 \.) c

9 8 ~ ~!{,.t9 ' :r Q ...r <!-.? :...

""' H '--0 ----s:- ~

Fax Number: 4:& O CJ 9 ¥' ).-{.,-{) b -...£J l) - ~

tt l -6 ~

<f: ·-\-' -+-#of Sampling Sampling Preservatives ~ Cont. Date Time --

~ >/5/ru \)8.d> '><' 1Q$S\J x 0.8'55 )')'.

\}; 0~ '>( ·--h ~ I 0\) ;><' X:: )\ X

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Relinquished By: Date/Time: Received By: Date/Time: Turnaround Time:

Cf,_,_ ./VJ. ~ _If__, s/5/l-;7 -·--:> same day Relinquishe,d/13y: I Date/Time: ~!'(eceived By: Date/Time: 24 hours

/ 48 hours

Relinquished By: Date/Time: (__ Received in Lab!IA___, .5/o;;;i~e: Sample Integrity:

lt,~lS intact / .

Page of


~rEDZ.-f5~ -D 1 ~ ot, -0_)

-(j..f

'-OS

-o(f

-.o--:)-

..._At2.

-dt '-10

(Check)

72 hours

5 days

normal

(Check)

on ice c;t_

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.


Page: Page 1 of 6 Lab Proj#: P1005116

Report Date: 05/24/10 Client Proj Name: PTE0287

Client Proj #: PTE0287

Lab Sample#

P1005116-01

P1 005116-02

P1005116-03


Client Sample ID

PTE0287-05(1RZ-IW-5-05052010)

PTE0287 -OO(IRZ-IW-4-05052010)

PTED287 -DB(IRZ-MWC-0505201 0)

Laboratory Results Total pages in data package: _ _.±t:...._ __

Microseeps test results meet all the requirements of the NELAC standards or provide reasons and/or justification if they do not.

Approved By:


The analytical results reported here are reliable and usable to the precision expressed In this report. As required by some regulating authorities, a full discussion of the uncertainty in our analytical results can be obtained at our web site or through customer seJVIce. Unless otherwise specified, all results


Case Narrative:






Sam12le Descri!;,!tion Matrix Lab Sample#




Sam(;!led Date/Time R.eceived PTE028 7 -05(1 RZ-IW-5-050520 1 Vapor P1005116-01 05 May. 10 11:00 10 May. 10 9:13

Clnalyte(s) Flag Result PQL Units Method# Analysis Date RiskAnalysis N Hydrogen 5600.000 120.000 nM AM20GAX 5/19/10

Data Qualifiers; J- estimated value, U -Non detect, R -Poor surrogate recovery, M- Recovery!RPD poor for MS/MSD, SAMP/DUP, B - detected in blank, S- field sample as received did not meet NELAC sample acceptance criteria, L • Subcontracted Lab used, N- NELAC certified analysis

By

sl




Page: Page 3 of 6 LabProj#: P1005116

Report Date: 05/24/1 0 Client Proj Name: PTE0287


SamQied Date/Time Received PTE0287 -OS{IRZ-IW-4-0505201 Vapor P1005116-02 05 May. 10 12:48 10 May. 10 9:13


Data Qualifiers: J - estimated value, U -Non detect, R -Poor surrogate recovery, M - Recovery/RPD poor for MS/MSD, SAMP/DUP, B - detected in blank, S- field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N- NELAC certified analysis

By

sl



Samgle DescriQtion Matrix Lab Sample#




SamQied Date/Time Received PTE0287 -OB(IRZ-MW-C-050520 Vapor P1 005116-03 05 May. 10 14:19 10 May. 10 9:13

'A91alyte(s) Flag Result PQL Units Method# Analysis Date RiskAnalysls N Hydrogen 24.000 0.600 nM AM20GAX 5/17/10

Data Qualifiers: J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery!RPD poor for MS/MSD, SAMP/DuP, B- detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N - NELAC certified analysis

By

sl



Prep Method:

Analysis Method:

M100518034~MB

Result TrueS!!ikeConc. RDL


M100518034-LCS

Result TrueSgikeConc.


M100518034-LCSD








%Recove~ Ctl Limits

- NA

%Recove~ Ctl Limits

93.00 75- 125

%Recove~ Ctl Limits RPD

93.00 75-125 0.00

RPD Ctl Limits

0-20

1--------ll Outlined Results indicate results outside of Control limits

Data Qualifiers: J -estimated value, U -Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMPmUP, B- detected in blank, S - field sample as received did not meet NELAC sample acceptance criteria, L - Subcontracted Lab used, N - NELAC certified analysis



Prep Method:

Analysis Method:

M100519030-MB

Result TrueS12ikeConc. RDL


M100519030-LCS

Result TrueS2ikeConc.


M1 00519030-LCSD

Result TrueS2ikeConc.








- NA


102.00 75- 125

%Recovery Ctl Limits RPD

102.00 75-125 0.00

RPD Ctl Limits

0-20

L---------'1 Outlined Results indicate results outside of Control limits

Data Qualifiers: J ·estimated value, U- Non detect, R -Poor surrogate recovery, M - Recovery/RPD poor for MS/MSD, SAMP/DUP, B - detected in blwtk, S - field sample as received did not meet NELAC sample acceptance criteria, L - Subcontracted Lab used, N - NELAC certified wtalysis

SENDING LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 189 Phoenix,,AZ 85040 . Phone: (602) 437-3340 Fax: (602) 454-9303 Project Manager: Kylie Emily


PTE0287



220 William Pitt Way Pittsburgh, PA 15238 Phone :(412)826-5245 Fax: (412}826-3433 Project Location: AZ- ARIZONA ·

· ·· · ReceiprTempetature: · · oc.. .. ... "ICe: · Y · ·t N ·

Standard ~AT is requested unless specific due date is requested. ==> Due Date: ---- Initials: --..,...--

l,,ni~

Sample ID: PTE0287-05 (IRZ-IW-5-05052010- Water}

Hydrogen

containem ·sui)f>i;9Ci: NA(F)

%

Sample ID: PTE0287-06 (IRZ-IW-4-05052010- Water}

Hydrogen


NA (F)

%

Sample ID: PTE0287 -08 (IRZ-MW-C-0505201 0 -Water)

Hydrogen


NA(F)

%

E?CP.ires. . . . ...

Sampled: 05105/1 o 11:00 06/02/1 0 11:00

Sampled: 05/05/10 12:48 06/02/10 12:48

Samgled: 05/05/10 14:19 06/02/1 0 14:1 9

-.,-----;.,.-~-'? ____ 4 ~~ ( ~0 Released By Datemme

. . Cqrt:Jme-:t.ts ..




Page 1 of 1


454-9303

LABORATORY REPORT





Received:

Issued:

05/06/10

05/06/10

05/25/10 13:26







Project: PGA North/103965


CASE NARRATIVE


PTE0370-01 IRZ-MW-D-05062010 Water

PTE0370-02 IRZ-MW-B-05062010 Water

PTE0370-03 IRZ-IW-3-05062010 Water

PTE0370-04 IRZ-IW-1-05062010 Water

PTE0370-05 IRZ-IW-1-05062010R Water

PTE0370-06 Trip Blank Water








Reviewed By:

Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily

<Page 1 of 61>


454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-01 (IRZ-MW-D-05062010 - Water) Sampled: 05/06/10


5/7/20105/7/2010EPA 8260BAcetone 10010E0257 10ND

5/7/20105/7/2010EPA 8260BBenzene 5.010E0257 10ND







































Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-01 (IRZ-MW-D-05062010 - Water) - cont. Sampled: 05/06/10











5/7/20105/7/2010EPA 8260BStyrene 5.010E0257 10ND




5/7/20105/7/2010EPA 8260BToluene 5.010E0257 10ND
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-02 (IRZ-MW-B-05062010 - Water) Sampled: 05/06/10


Acetone 5/7/20105/7/201010E0257 10 1EPA 8260B 38

Benzene 5/7/20105/7/201010E0257 0.50 1EPA 8260B 1.8






2-Butanone (MEK) 5/7/20105/7/201010E0257 2.5 1EPA 8260B 7.7






Chlorobenzene 5/7/20105/7/201010E0257 0.50 1EPA 8260B 7.0
















1,1-Dichloroethene 5/7/20105/7/201010E0257 0.50 1EPA 8260B 0.68

cis-1,2-Dichloroethene 5/7/20105/7/201010E0257 0.50 1EPA 8260B 1.7










Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-02 (IRZ-MW-B-05062010 - Water) - cont. Sampled: 05/06/10







4-Methyl-2-pentanone (MIBK) 5/7/20105/7/201010E0257 2.5 1EPA 8260B 3.4




5/7/20105/7/2010EPA 8260BStyrene 0.5010E0257 1ND




Toluene 5/7/20105/7/201010E0257 0.50 1EPA 8260B 1.9















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-02RE1 (IRZ-MW-B-05062010 - Water) - cont. Sampled: 05/06/10






Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



Trichloroethene 5/7/20105/7/201010E0257 25 50EPA 8260B 1200




Sample ID: PTE0370-03RE1 (IRZ-IW-3-05062010 - Water) Sampled: 05/06/10


5/11/20105/11/2010EPA 8260BAcetone 5010E0352 V15ND

5/11/20105/11/2010EPA 8260BBenzene 2.510E0352 5ND

































Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-03RE1 (IRZ-IW-3-05062010 - Water) - cont. Sampled: 05/06/10

















5/11/20105/11/2010EPA 8260BStyrene 2.510E0352 5ND




5/11/20105/11/2010EPA 8260BToluene 2.510E0352 5ND









5/11/20105/11/2010EPA 8260BVinyl Acetate 5.010E0352 V15ND






Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



5/7/20105/7/2010EPA 8260BAcetone 50010E0257 50ND

5/7/20105/7/2010EPA 8260BBenzene 2510E0257 50ND

5/7/20105/7/2010EPA 8260BBromobenzene 2510E0257 50ND

5/7/20105/7/2010EPA 8260BBromochloromethane 2510E0257 50ND

5/7/20105/7/2010EPA 8260BBromodichloromethane 2510E0257 50ND




5/7/20105/7/2010EPA 8260Bn-Butylbenzene 2510E0257 50ND

5/7/20105/7/2010EPA 8260Bsec-Butylbenzene 2510E0257 50ND

5/7/20105/7/2010EPA 8260Btert-Butylbenzene 2510E0257 50ND

5/7/20105/7/2010EPA 8260BCarbon disulfide 2510E0257 50ND

5/7/20105/7/2010EPA 8260BCarbon tetrachloride 2510E0257 50ND

5/7/20105/7/2010EPA 8260BChlorobenzene 2510E0257 50ND


5/7/20105/7/2010EPA 8260BChloroform 2510E0257 50ND


5/7/20105/7/2010EPA 8260B2-Chlorotoluene 2510E0257 50ND

5/7/20105/7/2010EPA 8260B4-Chlorotoluene 2510E0257 50ND

5/7/20105/7/2010EPA 8260BDibromochloromethane 2510E0257 50ND


5/7/20105/7/2010EPA 8260B1,2-Dibromoethane (EDB) 2510E0257 50ND

5/7/20105/7/2010EPA 8260BDibromomethane 2510E0257 50ND

5/7/20105/7/2010EPA 8260B1,2-Dichlorobenzene 2510E0257 50ND



5/7/20105/7/2010EPA 8260BDichlorodifluoromethane 2510E0257 50ND

5/7/20105/7/2010EPA 8260B1,1-Dichloroethane 2510E0257 50ND

5/7/20105/7/2010EPA 8260B1,2-Dichloroethane 2510E0257 50ND

5/7/20105/7/2010EPA 8260B1,1-Dichloroethene 2510E0257 50ND

5/7/20105/7/2010EPA 8260Bcis-1,2-Dichloroethene 2510E0257 50ND

5/7/20105/7/2010EPA 8260Btrans-1,2-Dichloroethene 2510E0257 50ND




5/7/20105/7/2010EPA 8260B1,1-Dichloropropene 2510E0257 50ND

5/7/20105/7/2010EPA 8260Bcis-1,3-Dichloropropene 2510E0257 50ND

5/7/20105/7/2010EPA 8260Btrans-1,3-Dichloropropene 2510E0257 50ND

5/7/20105/7/2010EPA 8260BEthylbenzene 2510E0257 50ND


Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-04 (IRZ-IW-1-05062010 - Water) - cont. Sampled: 05/06/10




5/7/20105/7/2010EPA 8260BIsopropylbenzene 2510E0257 50ND

5/7/20105/7/2010EPA 8260Bp-Isopropyltoluene 2510E0257 50ND



5/7/20105/7/2010EPA 8260BMethyl-tert-butyl Ether (MTBE) 2510E0257 50ND


5/7/20105/7/2010EPA 8260Bn-Propylbenzene 2510E0257 50ND

5/7/20105/7/2010EPA 8260BStyrene 2510E0257 50ND

5/7/20105/7/2010EPA 8260B1,1,1,2-Tetrachloroethane 2510E0257 50ND

5/7/20105/7/2010EPA 8260B1,1,2,2-Tetrachloroethane 2510E0257 50ND

5/7/20105/7/2010EPA 8260BTetrachloroethene 2510E0257 50ND



5/7/20105/7/2010EPA 8260B1,1,1-Trichloroethane 2510E0257 50ND

5/7/20105/7/2010EPA 8260B1,1,2-Trichloroethane 2510E0257 50ND

Trichloroethene 5/7/20105/7/201010E0257 25 50EPA 8260B 6700

5/7/20105/7/2010EPA 8260BTrichlorofluoromethane 2510E0257 50ND


5/7/20105/7/2010EPA 8260B1,2,4-Trimethylbenzene 2510E0257 50ND

5/7/20105/7/2010EPA 8260B1,3,5-Trimethylbenzene 2510E0257 50ND


5/7/20105/7/2010EPA 8260BVinyl chloride 2510E0257 50ND





Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-04RE2 (IRZ-IW-1-05062010 - Water) - cont. Sampled: 05/06/10


5/11/20105/11/2010EPA 8260BToluene 2510E0372 50ND




Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-05 (IRZ-IW-1-05062010R - Water) Sampled: 05/06/10


5/7/20105/7/2010EPA 8260BAcetone 1010E0257 1ND

5/7/20105/7/2010EPA 8260BBenzene 0.5010E0257 1ND



Bromodichloromethane 5/7/20105/7/201010E0257 0.50 1EPA 8260B 1.9











Chloroform 5/7/20105/7/201010E0257 0.50 1EPA 8260B 4.0




Dibromochloromethane 5/7/20105/7/201010E0257 0.50 1EPA 8260B 0.56





















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-05 (IRZ-IW-1-05062010R - Water) - cont. Sampled: 05/06/10











5/7/20105/7/2010EPA 8260BStyrene 0.5010E0257 1ND




5/7/20105/7/2010EPA 8260BToluene 0.5010E0257 1ND
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-06 (Trip Blank - Water) Sampled: 05/06/10


5/7/20105/7/2010EPA 8260BAcetone 1010E0257 1ND

5/7/20105/7/2010EPA 8260BBenzene 0.5010E0257 1ND







































Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTE0370-06 (Trip Blank - Water) - cont. Sampled: 05/06/10











5/7/20105/7/2010EPA 8260BStyrene 0.5010E0257 1ND




5/7/20105/7/2010EPA 8260BToluene 0.5010E0257 1ND
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 5/11/20105/7/201010E0240 0.050 1E200.7 0.50



Iron 5/11/20105/7/201010E0240 0.050 1E200.7 3.3



Iron 5/11/20105/7/201010E0240 0.050 1E200.7 49



Iron 5/11/20105/7/201010E0240 0.050 1E200.7 0.58

Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result






5/12/20105/12/2010EPA 314.0Perchlorate 1010E0409 D15ND






Perchlorate 5/12/20105/12/201010E0409 10 5EPA 314.0 27

Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/07/2010 (10E0257-BS1)

Acetone 25.0 10-150ug/l1022.6 90

Benzene 25.0 80-120ug/l0.5022.9 92




Bromoform 25.0 75-130ug/l1.021.2 85


2-Butanone (MEK) 25.0 40-150ug/l2.521.8 87








Chloroform 25.0 75-120ug/l0.5022.4 90




















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/07/2010 (10E0257-BS1)






2-Hexanone 25.0 20-150ug/l2.522.1 89

Iodomethane 25.0 80-130ug/l2.525.5 102






Naphthalene 25.0 40-150ug/l2.524.7 99


Styrene 25.0 80-120ug/l0.5026.5 106




Toluene 25.0 80-120ug/l0.5025.0 100
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1025.2 101 11 35

Benzene 25.0 80-120ug/l0.5023.5 94 3 15




Bromoform 25.0 75-130ug/l1.023.0 92 8 20


2-Butanone (MEK) 25.0 40-150ug/l2.523.9 96 9 35








Chloroform 25.0 75-120ug/l0.5022.2 89 0.9 15




















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.527.8 111 23 35

Iodomethane 25.0 80-130ug/l2.524.2 97 5 10






Naphthalene 25.0 40-150ug/l2.525.7 103 4 30


Styrene 25.0 80-120ug/l0.5028.5 114 8 15




Toluene 25.0 80-120ug/l0.5024.5 98 2 15
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1025.8 ND 103

Benzene 25.0 70-125ug/l0.5023.5 ND 94




Bromoform 25.0 65-125ug/l1.022.3 ND 89










Chloroform 25.0 70-130ug/l0.5026.3 4.05 89




















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.523.5 ND 94









Styrene 25.0 55-135ug/l0.5026.4 ND 106




Toluene 25.0 70-125ug/l0.5024.8 0.430 98
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1026.5 ND 106 3 35

Benzene 25.0 70-125ug/l0.5023.5 ND 94 0.04 25




Bromoform 25.0 65-125ug/l1.023.1 ND 92 3 25






Carbon disulfide 25.0 65-145ug/l0.5026.1 ND 104 0.3 25




Chloroform 25.0 70-130ug/l0.5027.5 4.05 94 5 20




Dibromochloromethane 25.0 70-130ug/l0.5026.6 0.560 104 0.2 20








1,1-Dichloroethane 25.0 70-130ug/l0.5023.0 ND 92 0.4 20








Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.524.0 ND 96 2 30

Iodomethane 25.0 60-150ug/l2.526.6 ND 106 0.7 30








Styrene 25.0 55-135ug/l0.5026.0 ND 104 2 35




Toluene 25.0 70-125ug/l0.5024.8 0.430 97 0.4 20












Xylenes, Total 50.0 75-120ug/l1.049.7 ND 99 0.1 15




Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/07/2010 (10E0270-BS1)

Acetone 25.0 10-150ug/l1023.7 95

Benzene 25.0 80-120ug/l0.5022.8 91




Bromoform 25.0 75-130ug/l1.023.8 95


2-Butanone (MEK) 25.0 40-150ug/l2.523.7 95








Chloroform 25.0 75-120ug/l0.5022.7 91




















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/07/2010 (10E0270-BS1)






2-Hexanone 25.0 20-150ug/l2.523.0 92

Iodomethane 25.0 80-130ug/l2.522.8 91






Naphthalene 25.0 40-150ug/l2.523.9 96


Styrene 25.0 80-120ug/l0.5023.0 92




Toluene 25.0 80-120ug/l0.5022.9 91
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1020.3 81 15 35

Benzene 25.0 80-120ug/l0.5023.6 94 3 15




Bromoform 25.0 75-130ug/l1.025.2 101 6 20


2-Butanone (MEK) 25.0 40-150ug/l2.521.7 87 9 35








Chloroform 25.0 75-120ug/l0.5023.2 93 2 15




















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.522.9 92 0.4 35

Iodomethane 25.0 80-130ug/l2.523.5 94 3 10






Naphthalene 25.0 40-150ug/l2.523.9 95 0.3 30


Styrene 25.0 80-120ug/l0.5023.6 94 3 15




Toluene 25.0 80-120ug/l0.5023.8 95 4 15











Vinyl chloride 25.0 70-130ug/l0.5022.1 89 0.05 20





Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1025.9 3.51 90

Benzene 25.0 70-125ug/l0.5024.0 ND 96




Bromoform 25.0 65-125ug/l1.022.8 ND 91










Chloroform 25.0 70-130ug/l0.5033.4 9.40 96




















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.521.4 ND 85









Styrene 25.0 55-135ug/l0.5020.1 ND 80




Toluene 25.0 70-125ug/l0.5025.0 0.760 97
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1030.3 3.51 107 16 35

Benzene 25.0 70-125ug/l0.5025.5 ND 102 6 25




Bromoform 25.0 65-125ug/l1.027.3 ND 109 18 25










Chloroform 25.0 70-130ug/l0.5034.9 9.40 102 5 20




















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.523.1 ND 92 8 30






Methyl-tert-butyl Ether (MTBE) 25.0 65-140ug/l0.5024.4 0.120 97 6 25



Styrene 25.0 55-135ug/l0.5018.9 ND 76 6 35




Toluene 25.0 70-125ug/l0.5026.0 0.760 101 4 20












Xylenes, Total 50.0 75-120ug/l1.051.4 ND 103 8 15




Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND V1

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND










Vinyl Acetate ug/l1.0ND V1






Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/11/2010 (10E0352-BS1)

Acetone 25.0 10-150ug/l1029.3 V1117

Benzene 25.0 80-120ug/l0.5024.0 96




Bromoform 25.0 75-130ug/l1.022.2 89


2-Butanone (MEK) 25.0 40-150ug/l2.525.4 102








Chloroform 25.0 75-120ug/l0.5025.1 100




















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/11/2010 (10E0352-BS1)






2-Hexanone 25.0 20-150ug/l2.521.7 87

Iodomethane 25.0 80-130ug/l2.524.8 99






Naphthalene 25.0 40-150ug/l2.524.0 96


Styrene 25.0 80-120ug/l0.5024.5 98




Toluene 25.0 80-120ug/l0.5025.3 101










Vinyl Acetate 25.0 40-150ug/l1.028.6 V1114






Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1026.1 V1104 12 35

Benzene 25.0 80-120ug/l0.5024.2 97 1 15




Bromoform 25.0 75-130ug/l1.021.0 84 6 20


2-Butanone (MEK) 25.0 40-150ug/l2.524.2 97 5 35

n-Butylbenzene 25.0 80-130ug/l0.5023.3 93 0.8 15


tert-Butylbenzene 25.0 80-120ug/l0.5023.8 95 0.1 15

Carbon disulfide 25.0 70-140ug/l0.5023.6 94 0.8 15




Chloroform 25.0 75-120ug/l0.5025.2 101 0.4 15

Chloromethane 25.0 60-140ug/l1.021.2 85 0.8 20



Dibromochloromethane 25.0 80-120ug/l0.5023.2 93 0.5 15
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 75-120ug/l0.5024.3 97 0.8 15

cis-1,3-Dichloropropene 25.0 80-120ug/l0.5025.4 102 0.08 15




2-Hexanone 25.0 20-150ug/l2.519.3 77 11 35

Iodomethane 25.0 80-130ug/l2.524.9 100 0.3 10

Isopropylbenzene 25.0 80-130ug/l0.5027.6 110 0.4 15





Naphthalene 25.0 40-150ug/l2.523.7 95 2 30


Styrene 25.0 80-120ug/l0.5024.0 96 2 15




Toluene 25.0 80-120ug/l0.5024.9 100 1 15


1,2,4-Trichlorobenzene 25.0 50-150ug/l1.024.6 98 0.9 30





1,2,3-Trichloropropane 25.0 70-130ug/l1.026.6 106 0.5 20



Vinyl Acetate 25.0 40-150ug/l1.025.7 V1103 11 25

Vinyl chloride 25.0 70-130ug/l0.5021.3 85 0.7 20





Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1023.0 V16.02 68

Benzene 25.0 70-125ug/l0.5025.8 ND 103




Bromoform 25.0 65-125ug/l1.022.2 ND 89

Bromomethane 25.0 45-150ug/l1.024.8 0.370 98










Chloromethane 25.0 55-145ug/l1.022.0 0.170 87




1,2-Dibromo-3-chloropropane 25.0 50-150ug/l2.521.7 0.900 83















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.517.4 2.22 61









Styrene 25.0 55-135ug/l0.5024.3 ND 97




Toluene 25.0 70-125ug/l0.5025.9 0.200 103










Vinyl Acetate 25.0 40-150ug/l1.026.2 V1ND 105






Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1021.6 V16.02 62 6 35

Benzene 25.0 70-125ug/l0.5023.6 ND 94 9 25




Bromoform 25.0 65-125ug/l1.019.8 ND 79 12 25

Bromomethane 25.0 45-150ug/l1.022.2 0.370 87 11 35









Chloroform 25.0 70-130ug/l0.5024.1 ND 97 7 20

Chloromethane 25.0 55-145ug/l1.020.0 0.170 80 9 35




1,2-Dibromo-3-chloropropane 25.0 50-150ug/l2.516.1 0.900 61 30 30










cis-1,2-Dichloroethene 25.0 70-125ug/l0.5022.6 0.130 90 10 20





Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.516.0 2.22 55 9 30









Styrene 25.0 55-135ug/l0.5022.0 ND 88 10 35



Tetrachloroethene 25.0 65-130ug/l0.5023.2 ND 93 12 25

Toluene 25.0 70-125ug/l0.5023.0 0.200 91 12 20










Vinyl Acetate 25.0 40-150ug/l1.022.2 V1ND 89 16 30






Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/11/2010 (10E0372-BS1)

Acetone 25.0 10-150ug/l1026.5 106

Benzene 25.0 80-120ug/l0.5023.2 93




Bromoform 25.0 75-130ug/l1.020.8 83


2-Butanone (MEK) 25.0 40-150ug/l2.523.7 95








Chloroform 25.0 75-120ug/l0.5022.8 91




















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 05/11/2010 (10E0372-BS1)






2-Hexanone 25.0 20-150ug/l2.525.2 101

Iodomethane 25.0 80-130ug/l2.523.9 96






Naphthalene 25.0 40-150ug/l2.524.2 97


Styrene 25.0 80-120ug/l0.5025.5 102




Toluene 25.0 80-120ug/l0.5024.1 96
















Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1025.3 101 5 35

Benzene 25.0 80-120ug/l0.5022.6 90 2 15

Bromobenzene 25.0 80-120ug/l0.5023.0 92 0.5 15



Bromoform 25.0 75-130ug/l1.020.6 82 0.8 20


2-Butanone (MEK) 25.0 40-150ug/l2.522.5 90 5 35








Chloroform 25.0 75-120ug/l0.5024.2 97 6 15














1,1-Dichloroethene 25.0 75-125ug/l0.5023.9 96 0.5 20






Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers




cis-1,3-Dichloropropene 25.0 80-120ug/l0.5024.0 96 0.04 15



Hexachlorobutadiene 25.0 40-150ug/l1.022.8 91 0.4 35

2-Hexanone 25.0 20-150ug/l2.525.2 101 0.04 35

Iodomethane 25.0 80-130ug/l2.524.2 97 1 10


p-Isopropyltoluene 25.0 80-130ug/l0.5024.3 97 0.9 15




Naphthalene 25.0 40-150ug/l2.523.6 94 3 30


Styrene 25.0 80-120ug/l0.5027.2 109 7 15




Toluene 25.0 80-120ug/l0.5023.9 96 0.5 15







1,2,3-Trichloropropane 25.0 70-130ug/l1.023.7 95 0.8 20









Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1029.1 ND 116

Benzene 25.0 70-125ug/l0.5024.8 ND 99




Bromoform 25.0 65-125ug/l1.021.4 ND 85






























Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.526.4 ND 106









Styrene 25.0 55-135ug/l0.5028.2 ND 113




Toluene 25.0 70-125ug/l0.5024.7 0.190 98




1,1,2-Trichloroethane 25.0 75-125ug/l0.5025.6 3.05 90












Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1029.7 ND 119 2 35

Benzene 25.0 70-125ug/l0.5025.0 ND 100 1 25



Bromodichloromethane 25.0 75-125ug/l0.5025.4 ND 102 0.4 20

Bromoform 25.0 65-125ug/l1.021.1 ND 84 1 25







Carbon tetrachloride 25.0 65-135ug/l0.5025.2 ND 101 0.4 25


Chloroethane 25.0 65-140ug/l1.025.2 ND 101 0.1 25

Chloroform 25.0 70-130ug/l0.5026.4 ND 106 0.7 20
















trans-1,2-Dichloroethene 25.0 75-125ug/l0.5026.1 ND 104 0.08 25




Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers





trans-1,3-Dichloropropene 25.0 70-130ug/l0.5026.7 ND 107 0.7 20



2-Hexanone 25.0 20-150ug/l2.525.1 ND 101 5 30



p-Isopropyltoluene 25.0 70-130ug/l0.5025.2 ND 101 0.7 30






Styrene 25.0 55-135ug/l0.5026.1 ND 104 8 35




Toluene 25.0 70-125ug/l0.5025.3 0.190 100 2 20




1,1,2-Trichloroethane 25.0 75-125ug/l0.5024.1 3.05 84 6 20












Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Iron mg/l0.050ND

LCS Analyzed: 05/11/2010 (10E0240-BS1)

Iron 1.00 85-115mg/l0.0500.936 94


Iron 1.00 85-115mg/l0.0500.934 93 0.2 20


Iron 1.00 75-125mg/l0.0501.01 0.0681 94


Iron 1.00 75-125mg/l0.0501.01 0.0681 94 0.4 10

Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers




LCS Analyzed: 05/12/2010 (10E0409-BS1)

Perchlorate 25.0 85-115ug/l2.027.4 110


Perchlorate 25.0 85-115ug/l2.027.3 109 0.5 15






Perchlorate 25.0 80-120ug/l2.029.6 1.91 111


Perchlorate 25.0 80-120ug/l2.027.3 1.39 104


Perchlorate 25.0 80-120ug/l2.028.8 1.91 108 3 15


Perchlorate 25.0 80-120ug/l2.027.5 1.39 104 0.7 15

Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965






Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




454-9303





Sampled:

Received:

05/06/10


Project ID:

PTE0370

PGA North/103965



TestAmerica Phoenix

Water XE200.7

Water XEPA 314.0

XWater XEPA 8260B






Analysis Performed: HydrogenSamples: PTE0370-01, PTE0370-03, PTE0370-04

Project Manager

TestAmerica Phoenix

PTE0370

Kylie Emily




TAL·0013-550 (12/08)

Client Name I Address: 5 th_o~ J t .,, -r.., Jo 6,ZN1 7 ;r 7 j_ [; .I,.,J,I\iA

c;c..;/--t~ ~Jrt 4.L Project Manager:

f"'-.,._/,. zr-..~"'t:J Sample~ (

- c~ t<YV<i.P/;!rL-


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it~~ ~ltv .... S~(DbJ0/\1 I~2--J.w-~r -fJS & 6 ~era IR2-lVr-/-osoG.JOlO rc_


[ ] Phoenix 7 4625 E. Cotton Center Blvd.; Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621


PC A-. .fl/·zj 9-6< ---, )'-

~ \' -Phone Number: -/ .a ~

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Fax Numb~rp D 0 '·

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...,.., ... ~ ::r_"- ¥ #of Sampling Sampling

Preservatives \)Ct -f.::'::: ~

' v

Cont. Date lime

b S/hfto 0\~~ \._--v- ~ )I ~ ~{)· 3-:::f-D~ ::,1

$ )~/io O'f~O ~ :x-- ~ -.o?..

c; 516/{() D'JS ( ~ v \( v - .93

6 s/6/io ll ,)1 x-- K >s"' )r-- -.0~

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( bo-ff/p~ ,..,{l;l~&pi"J 4.$ fi1 u---3 )

--r;.tP fJ /,VI A ~ -i'!{n , , .. ,

D. Date/Time: Turnaround Time: (Check) Relinquished Bb"~UJ ~atet~/c/ru Jv~ T

''")By: same day 72 hours

Relinquished By: Date/Time: ~dBy: Date/lime: 24 hours 5 days

/ 48 hours normal

Relinquished By: Date/Time: ( Received in LTi~- ~tt7~~ Sample Integrity; (Check)

Ill-:- .31 intact of.. on ice "

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. ·Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

~

Lab Sample#

P1 005115-01

P1 005115-02

P1005115-03




Client Proj #: PTE0370 Suite 189 Phoenix, AZ 85040

Client Sample ID

PTE03 70-01 (IRZ-MWD-05062010)

PTE0370-03(1RZ-IW-3-(05062010)

PTE0370-04(1RZ-IW-1-05062010)

Laboratory Results Total pages in data package: _j-_._ __

Microseeps test results meet all the requirements of the NElAC standards or provide reasons and/or justification if they do not.

Approved By: --lfJ2u:......t:lo.~~~'-"'""'~Jill..:......==O:,.______,_,("'--~=-.!_..:.. ..:;.J_ Date: I




Case Narrative:




Client Name: Test America Contact Kylie Emily Address: 4625 East Cotton Center Blvd.


SamQie Descrigtion Matrix Lab Sample#



Client Proj #: -pTE0370

Samgled Date/Time Received PTE0370-01 (IRZ-MW-D-050620 Vapor P1 005115-01 06 May. 10 8:24 10 May. 10 8:47

~alyte(s) Flag Result PQL Units Method# Analysis Date RiskAnalysis N Hydrogen 22.000 0.600 nM AM20GAX 5/17/10

Data Qualifiers: J - estimated value, U- Non detect, R- Poor surrogate recovecy, M - Recovery/RPD poor for MSIMSD, SAMP/DUP, B • detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N - NELAC certified analysis

By

sl




Page: Page 3 of 6 Lab Proj#: P1005115



SamQied Datemme Received PTE0370-03(1RZ-IW-3- Vapor P1 005115-02 06 May. 10 9:51 10 May. 10 8:47

~~fQJ Flag Result PQL Units Method# Analysis Date By RiskAnalysis N Hydrogen 5300.000 120.000 nM AM20GAX 5/19/10 sl

4"~ Data Qualifiers: J ·estimated value, U ·Non detect, R ·Poor surrogate recovery, M • Recovery/RPD poor for MS/MSD, SAMP/DUP, B ·detected f~1 in blank, S ·field sample as received did not meet NELAC sample acceptance criteria, L ·Subcontracted Lab used, N • NELAC certified analysis


Address: 4625 East Cotton Center Blvd. Suite 189 Phoenix, p.z 85040

Sam!;)le DescriQtion Matrix Lab Sample#




Sam!;)led Date/Time Received PTE0370-04(1 RZ-IW-1-0506201 Vapor P1005115-03 06 May. 10 11:22 10 May. 10 8:47


1~·~ Data Qualifiers: J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery!RPD poor for MSIMSD, SAMP/DUP, B- detected ~-t in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N - NELAC certified analysis

By

sl



Prep Method:

Analysis Method:

M1 00518034-MB



M100518034-LCS



M100518034-LCSD









- NA


93.00 75-125

%Recove!Y Ctl Limits RPD

93.00 75- 125 0.00

RPD Ctl Limits

0-20 ·'

.__ ___ ___.I Outlined Results indicate results outside of Control limits

Data Qualifiers: J- estimated value, U -Non detect, R -Poor surrogate recovery, M - Recovery/RPD poor for MSIMSD, SAMP/DUP, B • detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N • NELAC certified analysis



Prep Method:

Analysis Meth.od:

M100519030-MB



M1 00519030-LCS



M1 00519030-LCSD









- NA


102.00 75-125

%Becove[Y Ctl Limits RPD

102.00 75-125 0.00

RPD Ctl Limits

0-20

,_ ___ ____.!Outlined Results indicate results outside of Control limits

Data Qualifiers: J- estimated value, U -Non detect, R - Poor surrogate recovery, M - Recovery/RPD poor for MS/MSD, SAMP/DUP, B -detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N - NELAC certified analysis

SENDING LABORATORY:

SUBCONTRACT ORDER TestAmerica Pho~nix

PTE0370


TestAmerica Phoenix Microseeps/Univ of Pittsburgh App Research Center 4625 East Cotton Center Blvd. Ste 189 220 William Pitt Way

---- P.hoenix,-AZ.85040--····- ········-··· ~- .. . ....... - ..... - .. --Pittsburgh,-P.A 15238 ............... H .................. __ ................ .

Phone: (602) 437-3340 Phone :(412)826-5245 Fax: (602) 454-9303 Fax: (412)826-3433 Project Manager: Kylie Emily Project Location:-AZ·-. ARIZONA~

-----·-·-:-··-~.--:----~ :------ ·-----· --::": ··- .... ---.~:·:·:-·-:·:···. ·:··--· ----·-·-- · ··• ·· ... ·---. ··Re<:reipl Te"i.npe"ratute:·· ............ ···oc- ...... .,._ ... '"Ice:· ·--:-y· -t ·'"N·:· ·: ...... _~;-- ·: -- ..... .

Standard TAT is requested unless specific due date is requested. => Due Date: ___ _ Initials: ___ _

.. __ _An~IY~!s_.. ........ .. .. . IJ!)_i~~L . _ ............ .... ... ... ~xpjres ................ ..

Sample ID: PTE0370-01 (IRZ-MW-D-0506201 0 -Water) Sampled: 05/06/10 08:24

Hydrogen % 06/03/10 08:24 . . · -------- caniainers. s·uppiie£ · NA(A)

, ........... , ... -~· .......... · .......... ~--...... - ....... _ ~-- ..................... ~·- ... -· -~ ....... ·~

Sample ID: PTE0370·03 (IRZftiW·3-05062010- Water)

Hydrogen


NA(A)

%

Sample ID: PTE0370-04 (IRZ-IW-1-05062010- Wat~r)

Hydrogen


NA (A)

Released By

Released By

%

Datemme

Sampled: 05/06/10 09:51 06/03/10 09:51

·Sampled: 05/06/10 11 :22 06/03/10 11:22

. ___ C()mm_ef!ts_ .




Page 1 of 1

4625 East Cotton Center Blvd. Ste 189 Phoenix, AZ 85040 (602) 437-3340 Fax:(602) 454-9303

INVOICE

Invoice To:

PO Number:

Client:

Invoice Date: 08/19/10

Project:

Qty Analysis/Description Matrix Cost Cost

NA

For Billing Inquiries please contact:

Remit Payment To:

Client Contact:

TAT Charge

Rush RushWorkorder:

Lab Contact:

98846

Unit Extended

PGA North / PGA North 103965.02

55013296

Environmental Resources Management

Inc-Invoicing

ERM -Walnut Creek (invoicing)

1277 Tret Blvd, Suite 500

Walnut Creek, CA 94597

TestAmerica Laboratories, Inc.

Dept 2314

P.O. Box 122314

Dallas, TX 75312-2314

TestAmerica EIN: 23-2919996

Paula Chang

PTH0241

Invoice Number:

Terms:

(602) 437-3340

Kylie Emily

[email protected] Received: 08/04/10 Samples Reported: 08/18/10

See BelowEnvironmental Resources Management Inc.-West

NoneNAChlorate (EPA 300.1) $90.00 3 $30.00 Water

NoneNAChloride (EPA 300.0) $47.25 3 $15.75 Water

NoneNAChlorite - O $90.00 3 $30.00 Water

NoneNADis Iron (200.7) $45.00 3 $15.00 Water

NoneNAHydrogen $360.00 3 $120.00 Water

NoneNAICP Iron (200.7) $22.50 3 $7.50 Water

NoneNAICP Sodium (200.7) $22.50 3 $7.50 Water

NoneNAPerchlorate (314.0) $210.00 3 $70.00 Water

NoneNASulfate (EPA 300.0) $47.25 3 $15.75 Water

NoneNAVolatile Organics (EPA 8260B) $340.00 4 $85.00 Water

NoneNAVolatile Organics (EPA 8260B) $0.00 1 $0.00 Water

Additional Items

$114.00 Passive Diffusion Bag $28.50 4

$36.18 Shipping Charge $36.18 1

Invoice Total: $1,424.68

Any applicable rush charges are based on the actual turn-around-time met.

Page 1 of 1

55013296Invoice:Prices shown include all applicable discounts.TestAmerica’s Standard Terms & Conditions (Net 30 Days) apply to all

work performed and invoiced unless superseded by a specific executed contract vehicle.

PTH0241

SENDING LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 189

Phoenix, AZ 85040

Phone: (602) 437-3340

Fax: (602) 454-9303Project Manager: Kylie EmilyClient: Environmental Resources Management Inc.-West

SUBCONTRACT ORDERTestAmerica Phoenix

n H 00Qt()RECEIVING LABORATORY:

TestAmerica Irvine

17461 Derian Ave. Suite 100

Irvine, CA 92614

Phone :(949) 261-1022

Fax: (949) 261-1228Project Location: AZ - ARIZONAReceiptTemperature: l.-.l( °C Ice: YIN

Analysis Units Due Expires Interlab Price Surch Comments

Sample ID: PTH0241.01 (IRZ-IW-5-08042010 - Water)

Chlorate (300.1) mg/l 08/18/10

Chlorite (300.1) - 0 mg/l 08/18/10


500 ml Poly w/EDA (F) 125mL Brown Poly wIEDA (G)

Sample 10: PTH0241-03 (IRZ-IW-4-08042010 - Water)

Chlorate (300.1) mg/l 08/18/10

Chlorite (300.1) - 0 mg/l 08/18/10




Chlorate (300.1) mg/l 08/18/10

Chlorite (300.1) - 0 mg/l 08/18/10



Sampled: 08/04/10 11:0209/01/10 11:02 $30.00 0%

08/18/10 11:02 $30.00 0%

Sampled: 08/04/1013:2109/01/1013:21 $30.00 0%

08/18/1013:21 $30.00 0%

Sampled: 08/04/1014:5509/01/1014:55 $30.00 0%

08/18/1014:55 $30.00 0%

Re,easedf1ReleasedBy

8&/0DatelTime

DatelTime

Rece~

Received By

DatelTime

~\ o~ l....\,")'<DatelTime Page 1 of 1

~ll p..@"6

Environmental Resources Management CHAIN OF CUSTODY-RECORD

SAMPLE I.D.

X X

0 BOTTLE INTACT 0 CUSTODY SEALS 0 CHILLED

0 PRESERVED 0 SEALS INTACT 0 SEE REMARKS

WHITE- LABORATORY COPY CANARY- FIELD COPY PINK- DATABASE

'~'·I 1928

X

/. 0 t;e.

GOLD - PROJECT FILE


454-9303

LABORATORY REPORT





Received:

Issued:

08/04/10

08/04/10

08/18/10 16:48









CASE NARRATIVE


PTH0241-01 IRZ-IW-5-08042010 Water

PTH0241-02 IRZ-IW-5-08042010 Water

PTH0241-03 IRZ-IW-4-08042010 Water

PTH0241-04 IRZ-IW-4-08042010 Water

PTH0241-05 IRZ-IW-4-08042010R Water

PTH0241-06 IRZ-IW-3-08042010 Water

PTH0241-07 IRZ-IW-3-08042010 Water

PTH0241-08 Trip Blank Water

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily

<Page 1 of 45>


454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02






N1c-pH = 3


N1a-The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).

N1b-8260-The Laboratory Control Sample and Matrix Spike / Matrix Spike Duplicate recovered high and

outside of acceptance limits for 1,1-Dichloroethene. All associated samples are non-detect for this

compound and therefore are not impacted.

N1b-Cl-Results exceeded the linear range in the MS/MSD and therefore are not available for reporting.


N1d-The RPD exceeded the acceptance limit due to sample matrix effects.







Reviewed By:

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0241-01 (IRZ-IW-5-08042010 - Water) Sampled: 08/04/10


8/10/20108/10/2010EPA 8260BAcetone 1010H0366 1ND

8/10/20108/10/2010EPA 8260BBenzene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BBromobenzene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BBromochloromethane 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BBromodichloromethane 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BBromoform 1.010H0366 1ND

8/10/20108/10/2010EPA 8260BBromomethane 1.010H0366 1ND

8/10/20108/10/2010EPA 8260B2-Butanone (MEK) 2.510H0366 1ND

8/10/20108/10/2010EPA 8260Bn-Butylbenzene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260Bsec-Butylbenzene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260Btert-Butylbenzene 0.5010H0366 1ND

Carbon disulfide 8/10/20108/10/201010H0366 0.50 1EPA 8260B 1.5

8/10/20108/10/2010EPA 8260BCarbon tetrachloride 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BChlorobenzene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BChloroethane 1.010H0366 1ND

8/10/20108/10/2010EPA 8260BChloroform 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BChloromethane 1.010H0366 1ND

8/10/20108/10/2010EPA 8260B2-Chlorotoluene 0.5010H0366 1ND


8/10/20108/10/2010EPA 8260BDibromochloromethane 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260B1,2-Dibromo-3-chloropropane 2.510H0366 1ND

8/10/20108/10/2010EPA 8260B1,2-Dibromoethane (EDB) 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BDibromomethane 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260B1,2-Dichlorobenzene 0.5010H0366 1ND



8/10/20108/10/2010EPA 8260BDichlorodifluoromethane 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260B1,1-Dichloroethane 0.5010H0366 1ND


8/10/20108/10/2010EPA 8260B1,1-Dichloroethene 0.5010H0366 L31ND

cis-1,2-Dichloroethene 8/10/20108/10/201010H0366 0.50 1EPA 8260B 3.3

8/10/20108/10/2010EPA 8260Btrans-1,2-Dichloroethene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260B1,2-Dichloropropane 0.5010H0366 1ND



8/10/20108/10/2010EPA 8260B1,1-Dichloropropene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260Bcis-1,3-Dichloropropene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260Btrans-1,3-Dichloropropene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BEthylbenzene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BHexachlorobutadiene 1.010H0366 1ND

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0241-01 (IRZ-IW-5-08042010 - Water) - cont. Sampled: 08/04/10


8/10/20108/10/2010EPA 8260B2-Hexanone 2.510H0366 1ND

8/10/20108/10/2010EPA 8260BIodomethane 2.510H0366 1ND

8/10/20108/10/2010EPA 8260BIsopropylbenzene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260Bp-Isopropyltoluene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BMethylene Chloride 1.010H0366 1ND

8/10/20108/10/2010EPA 8260B4-Methyl-2-pentanone (MIBK) 2.510H0366 1ND

8/10/20108/10/2010EPA 8260BMethyl-tert-butyl Ether (MTBE) 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BNaphthalene 2.510H0366 1ND

8/10/20108/10/2010EPA 8260Bn-Propylbenzene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260B1,1,1,2-Tetrachloroethane 0.5010H0366 1ND


8/10/20108/10/2010EPA 8260BTetrachloroethene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260B1,2,3-Trichlorobenzene 1.010H0366 1ND


8/10/20108/10/2010EPA 8260B1,1,1-Trichloroethane 0.5010H0366 1ND


Trichloroethene 8/10/20108/10/201010H0366 0.50 1EPA 8260B 150

8/10/20108/10/2010EPA 8260BTrichlorofluoromethane 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260B1,2,3-Trichloropropane 1.010H0366 1ND

8/10/20108/10/2010EPA 8260B1,2,4-Trimethylbenzene 0.5010H0366 1ND


8/10/20108/10/2010EPA 8260BVinyl Acetate 1.010H0366 1ND

8/10/20108/10/2010EPA 8260BVinyl chloride 0.5010H0366 1ND

8/10/20108/10/2010EPA 8260BXylenes, Total 1.010H0366 1ND




Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



8/10/20108/10/2010EPA 8260BAcetone 1010H0366 1ND

8/10/20108/10/2010EPA 8260BBenzene 0.5010H0366 1ND




























8/10/20108/10/2010EPA 8260Bcis-1,2-Dichloroethene 0.5010H0366 1ND











Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0241-03 (IRZ-IW-4-08042010 - Water) - cont. Sampled: 08/04/10










8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND















Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0241-03RE1 (IRZ-IW-4-08042010 - Water) - cont. Sampled: 08/04/10


8/10/20108/10/2010EPA 8260B1,1-Dichloroethene 5.010H0400 10ND





Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0241-05 (IRZ-IW-4-08042010R - Water) Sampled: 08/04/10


8/10/20108/10/2010EPA 8260BAcetone 1010H0366 1ND

8/10/20108/10/2010EPA 8260BBenzene 0.5010H0366 1ND



Bromodichloromethane 8/10/20108/10/201010H0366 0.50 1EPA 8260B 1.0











Chloroform 8/10/20108/10/201010H0366 0.50 1EPA 8260B 2.0

























Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0241-05 (IRZ-IW-4-08042010R - Water) - cont. Sampled: 08/04/10











8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND





8/10/20108/10/2010EPA 8260BTrichloroethene 0.5010H0366 1ND











Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0241-06 (IRZ-IW-3-08042010 - Water) Sampled: 08/04/10 Q3, N1c


8/10/20108/10/2010EPA 8260BAcetone 1010H0366 1ND

8/10/20108/10/2010EPA 8260BBenzene 0.5010H0366 1ND










8/10/20108/10/2010EPA 8260BCarbon disulfide 0.5010H0366 1ND





























Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0241-06 (IRZ-IW-3-08042010 - Water) - cont. Sampled: 08/04/10 Q3, N1c











8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND















Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result







Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0241-08 (Trip Blank - Water) Sampled: 08/04/10


8/10/20108/10/2010EPA 8260BAcetone 1010H0366 1ND

8/10/20108/10/2010EPA 8260BBenzene 0.5010H0366 1ND







































Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0241-08 (Trip Blank - Water) - cont. Sampled: 08/04/10











8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND
















Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 8/9/20108/6/201010H0230 0.050 1E200.7 170

Sodium 8/9/20108/6/201010H0230 2.0 1E200.7 380



Iron 8/9/20108/6/201010H0230 0.050 1E200.7 720

Sodium 8/9/20108/6/201010H0230 2.0 1E200.7 390



Iron 8/9/20108/6/201010H0230 0.050 1E200.7 210

Sodium 8/9/20108/6/201010H0230 2.0 1E200.7 470

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

DISSOLVED METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 8/9/20108/6/201010H0224 0.050 1E200.7 2.0



Iron 8/9/20108/6/201010H0224 0.050 1E200.7 9.2



8/9/20108/6/2010E200.7Iron 0.05010H0224 1ND

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Chloride 8/6/20108/6/201010H0255 40 20EPA 300.0 770

Sulfate 8/6/20108/6/201010H0255 40 20EPA 300.0 1000



8/6/20108/6/2010EPA 314.0Perchlorate 4.010H0245 D12ND



Chloride 8/6/20108/6/201010H0255 40 20EPA 300.0 750

Sulfate 8/6/20108/6/201010H0255 40 20EPA 300.0 970



Perchlorate 8/6/20108/6/201010H0245 2.0 1EPA 314.0 6.1



Chloride 8/6/20108/6/201010H0255 40 20EPA 300.0 700

Sulfate 8/6/20108/6/201010H0255 40 20EPA 300.0 810



8/6/20108/6/2010EPA 314.0Perchlorate 2.010H0245 1ND

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



8/12/20108/12/2010EPA 300.1Chlorate 40010H1381 D120ND

8/12/20108/12/2010EPA 300.1Chlorite 4010H1381 D12ND












Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

Batch: 10H0366 Extracted: 08/10/10

Blank Analyzed: 08/10/2010 (10H0366-BLK1)

Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 08/10/2010 (10H0366-BS1)

Acetone 25.0 10-150ug/l1028.6 114

Benzene 25.0 80-120ug/l0.5027.3 109




Bromoform 25.0 75-130ug/l1.027.3 109


2-Butanone (MEK) 25.0 40-150ug/l2.523.8 95








Chloroform 25.0 75-120ug/l0.5027.5 110














1,1-Dichloroethene 25.0 75-125ug/l0.5031.4 L3126






Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 08/10/2010 (10H0366-BS1)






2-Hexanone 25.0 20-150ug/l2.523.7 95

Iodomethane 25.0 80-130ug/l2.528.2 113






Naphthalene 25.0 40-150ug/l2.527.2 109


Styrene 25.0 80-120ug/l0.5029.2 117




Toluene 25.0 80-120ug/l0.5028.0 112
















Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Dup Analyzed: 08/10/2010 (10H0366-BSD1)

Acetone 25.0 10-150ug/l1027.5 110 4 35

Benzene 25.0 80-120ug/l0.5025.9 104 5 15




Bromoform 25.0 75-130ug/l1.024.6 99 10 20


2-Butanone (MEK) 25.0 40-150ug/l2.525.3 101 6 35

n-Butylbenzene 25.0 80-130ug/l0.5024.4 R697 17 15

sec-Butylbenzene 25.0 80-125ug/l0.5023.7 R695 16 15






Chloroform 25.0 75-120ug/l0.5027.4 110 0.3 15




















Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers





trans-1,3-Dichloropropene 25.0 80-125ug/l0.5028.7 115 0.2 15



2-Hexanone 25.0 20-150ug/l2.523.9 96 0.8 35

Iodomethane 25.0 80-130ug/l2.526.7 107 5 10






Naphthalene 25.0 40-150ug/l2.524.6 98 10 30


Styrene 25.0 80-120ug/l0.5027.3 109 7 15




Toluene 25.0 80-120ug/l0.5026.2 105 7 15








1,2,4-Trimethylbenzene 25.0 80-120ug/l0.5024.4 R697 16 15








Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 08/10/2010 (10H0366-MS1) Source: PTH0352-12

Acetone 25.0 10-150ug/l1034.8 ND 139

Benzene 25.0 70-125ug/l0.5029.2 0.860 113




Bromoform 25.0 65-125ug/l1.030.2 ND 121









Chloroethane 25.0 65-140ug/l1.030.2 0.110 120

Chloroform 25.0 70-130ug/l0.5031.3 2.03 117






1,2-Dibromoethane (EDB) 25.0 70-125ug/l0.5031.6 M1ND 126

Dibromomethane 25.0 70-120ug/l0.5030.3 M1ND 121







1,1-Dichloroethene 25.0 70-130ug/l0.5041.9 N1b8.94 132




1,3-Dichloropropane 25.0 70-120ug/l0.5030.4 M10.120 121


Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.529.2 1.96 109

Iodomethane 25.0 60-150ug/l2.59.99 M20.640 37






Naphthalene 25.0 40-150ug/l2.532.9 0.920 128


Styrene 25.0 55-135ug/l0.5021.2 ND 85


1,1,2,2-Tetrachloroethane 25.0 70-125ug/l0.5030.2 0.100 120


Toluene 25.0 70-125ug/l0.5027.4 0.120 109
















Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 08/10/2010 (10H0366-MSD1) Source: PTH0352-12

Acetone 25.0 10-150ug/l1035.6 ND 143 2 35

Benzene 25.0 70-125ug/l0.5031.3 0.860 122 7 25

Bromobenzene 25.0 75-120ug/l0.5030.3 N1aND 121 7 20



Bromoform 25.0 65-125ug/l1.033.1 N1aND 132 9 25







Carbon tetrachloride 25.0 65-135ug/l0.5031.0 0.290 123 6 25


Chloroethane 25.0 65-140ug/l1.031.1 0.110 124 3 25

Chloroform 25.0 70-130ug/l0.5033.4 2.03 126 7 20




Dibromochloromethane 25.0 70-130ug/l0.5035.2 N1aND 141 9 20


1,2-Dibromoethane (EDB) 25.0 70-125ug/l0.5034.0 M1ND 136 7 20

Dibromomethane 25.0 70-120ug/l0.5033.2 M1ND 133 9 20

1,2-Dichlorobenzene 25.0 75-120ug/l0.5030.2 N1aND 121 6 20




1,1-Dichloroethane 25.0 70-130ug/l0.5032.8 N1a0.160 131 8 20


1,1-Dichloroethene 25.0 70-130ug/l0.5043.5 N1b8.94 138 4 25


trans-1,2-Dichloroethene 25.0 75-125ug/l0.5031.3 0.0900 125 4 25

1,2-Dichloropropane 25.0 75-125ug/l0.5032.5 N1aND 130 8 20

1,3-Dichloropropane 25.0 70-120ug/l0.5034.0 M10.120 135 11 20


Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.533.4 1.96 126 13 30

Iodomethane 25.0 60-150ug/l2.54.72 M2, N1d0.640 16 72 30



Methylene Chloride 25.0 65-130ug/l1.033.1 N1a0.190 132 6 20

4-Methyl-2-pentanone (MIBK) 25.0 55-135ug/l2.535.8 N1aND 143 15 25


Naphthalene 25.0 40-150ug/l2.534.7 0.920 135 5 30


Styrene 25.0 55-135ug/l0.5024.3 ND 97 14 35


1,1,2,2-Tetrachloroethane 25.0 70-125ug/l0.5032.3 N1a0.100 129 7 25


Toluene 25.0 70-125ug/l0.5029.2 0.120 116 6 20




1,1,2-Trichloroethane 25.0 75-125ug/l0.5032.3 N1aND 129 12 20

Trichloroethene 25.0 70-125ug/l0.505090 M3, R13040 8190 48 25


1,2,3-Trichloropropane 25.0 70-130ug/l1.032.9 N1aND 131 14 25









Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 08/10/2010 (10H0400-BS1)

Acetone 25.0 10-150ug/l1027.0 108

Benzene 25.0 80-120ug/l0.5025.3 101




Bromoform 25.0 75-130ug/l1.025.6 103


2-Butanone (MEK) 25.0 40-150ug/l2.528.8 115








Chloroform 25.0 75-120ug/l0.5029.0 116




















Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 08/10/2010 (10H0400-BS1)






2-Hexanone 25.0 20-150ug/l2.526.0 104

Iodomethane 25.0 80-130ug/l2.528.6 114






Naphthalene 25.0 40-150ug/l2.529.8 119


Styrene 25.0 80-120ug/l0.5027.0 108




Toluene 25.0 80-120ug/l0.5025.8 103













25.0 80-120Surrogate: Dibromofluoromethane ug/l30.4 S10121



Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1026.6 106 1 35

Benzene 25.0 80-120ug/l0.5026.6 106 5 15




Bromoform 25.0 75-130ug/l1.026.0 104 1 20


2-Butanone (MEK) 25.0 40-150ug/l2.526.6 106 8 35








Chloroform 25.0 75-120ug/l0.5028.6 114 1 15






1,2-Dibromoethane (EDB) 25.0 80-120ug/l0.5026.8 107 0.7 15














Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.524.6 98 5 35

Iodomethane 25.0 80-130ug/l2.529.1 116 2 10






Naphthalene 25.0 40-150ug/l2.528.3 113 5 30


Styrene 25.0 80-120ug/l0.5027.1 108 0.4 15




Toluene 25.0 80-120ug/l0.5026.8 107 4 15
















Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 08/11/2010 (10H0400-MS1) Source: PTH0352-07RE1

Acetone 125 10-150ug/l50139 ND 111

Benzene 125 70-125ug/l2.5141 ND 113



Bromodichloromethane 125 75-125ug/l2.5149 2.60 117

Bromoform 125 65-125ug/l5.0118 ND 94


2-Butanone (MEK) 125 15-150ug/l12139 ND 112








Chloroform 125 70-130ug/l2.5148 ND 119











Dichlorodifluoromethane 125 60-150ug/l2.5141 ND 113



1,1-Dichloroethene 125 70-130ug/l2.5140 1.05 111



1,2-Dichloropropane 125 75-125ug/l2.5145 1.15 115



Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







Hexachlorobutadiene 125 40-150ug/l5.0131 ND 105

2-Hexanone 125 20-150ug/l12136 ND 109




Methylene Chloride 125 65-130ug/l5.0139 0.800 111





Styrene 125 55-135ug/l2.5142 ND 114



Tetrachloroethene 125 65-130ug/l2.5131 ND 105

Toluene 125 70-125ug/l2.5134 ND 108




1,1,2-Trichloroethane 125 75-125ug/l2.5138 12.2 101

Trichloroethene 125 70-125ug/l2.5353 225 103











Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 08/11/2010 (10H0400-MSD1) Source: PTH0352-07RE1

Acetone 125 10-150ug/l50142 ND 114 2 35

Benzene 125 70-125ug/l2.5136 ND 109 4 25

Bromobenzene 125 75-120ug/l2.5140 ND 112 8 20

Bromochloromethane 125 75-130ug/l2.5135 ND 108 3 20

Bromodichloromethane 125 75-125ug/l2.5145 2.60 114 3 20

Bromoform 125 65-125ug/l5.0131 ND 105 11 25

Bromomethane 125 45-150ug/l5.0130 ND 104 0.9 35

2-Butanone (MEK) 125 15-150ug/l12147 ND 118 5 30

n-Butylbenzene 125 70-130ug/l2.5142 ND 114 5 30

sec-Butylbenzene 125 70-125ug/l2.5146 ND 117 8 30

tert-Butylbenzene 125 70-125ug/l2.5141 ND 113 4 25

Carbon disulfide 125 65-145ug/l2.5145 ND 116 3 25

Carbon tetrachloride 125 65-135ug/l2.5141 ND 113 2 25

Chlorobenzene 125 75-120ug/l2.5138 ND 110 1 20

Chloroethane 125 65-140ug/l5.0144 ND 115 4 25

Chloroform 125 70-130ug/l2.5145 ND 116 2 20

Chloromethane 125 55-145ug/l5.0138 ND 110 8 35

2-Chlorotoluene 125 70-125ug/l2.5142 ND 113 6 25


Dibromochloromethane 125 70-130ug/l2.5142 ND 113 0.1 20

1,2-Dibromo-3-chloropropane 125 50-150ug/l12140 ND 112 8 30

1,2-Dibromoethane (EDB) 125 70-125ug/l2.5144 ND 115 4 20

Dibromomethane 125 70-120ug/l2.5148 ND 119 0.3 20

1,2-Dichlorobenzene 125 75-120ug/l2.5145 ND 116 5 20



Dichlorodifluoromethane 125 60-150ug/l2.5140 ND 112 1 30

1,1-Dichloroethane 125 70-130ug/l2.5149 ND 119 2 20


1,1-Dichloroethene 125 70-130ug/l2.5147 1.05 117 5 25

cis-1,2-Dichloroethene 125 70-125ug/l2.5141 ND 113 3 20

trans-1,2-Dichloroethene 125 75-125ug/l2.5147 ND 118 4 25

1,2-Dichloropropane 125 75-125ug/l2.5144 1.15 114 0.9 20

1,3-Dichloropropane 125 70-120ug/l2.5147 4.95 113 3 20

2,2-Dichloropropane 125 65-140ug/l5.0121 ND 97 4 25

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 125 65-130ug/l2.5141 ND 113 1 25

cis-1,3-Dichloropropene 125 75-130ug/l2.5132 ND 105 0.6 20

trans-1,3-Dichloropropene 125 70-130ug/l2.5142 ND 114 3 20

Ethylbenzene 125 70-125ug/l2.5141 ND 112 2 25

Hexachlorobutadiene 125 40-150ug/l5.0142 ND 114 8 30

2-Hexanone 125 20-150ug/l12134 ND 108 1 30

Iodomethane 125 60-150ug/l12147 ND 118 8 30

Isopropylbenzene 125 75-130ug/l2.5155 ND 124 4 25

p-Isopropyltoluene 125 70-130ug/l2.5146 ND 117 5 30

Methylene Chloride 125 65-130ug/l5.0144 0.800 114 3 20

4-Methyl-2-pentanone (MIBK) 125 55-135ug/l12135 ND 108 0.6 25

Methyl-tert-butyl Ether (MTBE) 125 65-140ug/l2.5138 ND 110 2 25

Naphthalene 125 40-150ug/l12148 ND 119 8 30

n-Propylbenzene 125 70-130ug/l2.5147 ND 118 4 30

Styrene 125 55-135ug/l2.5144 ND 115 1 35

1,1,1,2-Tetrachloroethane 125 70-125ug/l2.5138 ND 111 1 20


Tetrachloroethene 125 65-130ug/l2.5129 ND 104 1 25

Toluene 125 70-125ug/l2.5134 ND 107 0.6 20

1,2,3-Trichlorobenzene 125 50-150ug/l5.0150 ND 120 7 35


1,1,1-Trichloroethane 125 70-130ug/l2.5143 ND 114 0.03 25

1,1,2-Trichloroethane 125 75-125ug/l2.5134 12.2 97 3 20

Trichloroethene 125 70-125ug/l2.5344 225 96 3 25

Trichlorofluoromethane 125 65-150ug/l2.5159 ND 128 4 25

1,2,3-Trichloropropane 125 70-130ug/l5.0141 ND 113 8 25

1,2,4-Trimethylbenzene 125 70-125ug/l2.5148 ND 118 6 30


Vinyl Acetate 125 40-150ug/l5.0124 ND 99 2 30

Vinyl chloride 125 60-140ug/l2.5140 ND 112 0.8 25

Xylenes, Total 250 75-120ug/l5.0277 ND 111 3 15




Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Iron mg/l0.050ND

Sodium mg/l2.0ND

LCS Analyzed: 08/09/2010 (10H0230-BS1)

Iron 1.00 85-115mg/l0.0500.939 94

Sodium 20.0 85-115mg/l2.019.0 95


Iron 1.00 85-115mg/l0.0500.925 93 1 20

Sodium 20.0 85-115mg/l2.019.1 95 0.3 20


Iron 1.00 75-125mg/l0.0500.960 ND 96

Sodium 20.0 75-125mg/l2.056.2 36.4 99


Iron 1.00 75-125mg/l0.0501.30 0.319 98

Sodium 20.0 75-125mg/l2.0124 103 105


Iron 1.00 75-125mg/l0.0501.03 ND 103 7 10

Sodium 20.0 75-125mg/l2.054.9 36.4 92 2 10


Iron 1.00 75-125mg/l0.0501.37 0.319 106 5 10

Sodium 20.0 75-125mg/l2.0119 103 78 4 10

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

DISSOLVED METALS


Data

Qualifiers



Iron mg/l0.050ND


Iron mg/l0.050ND

LCS Analyzed: 08/09/2010 (10H0224-BS1)

Iron 1.00 85-115mg/l0.0501.04 104


Iron 1.00 85-115mg/l0.0501.05 105 0.7 20


Iron 1.00 75-125mg/l0.0501.16 0.113 105


Iron 1.00 75-125mg/l0.0501.16 ND 116


Iron 1.00 75-125mg/l0.0501.17 0.113 106 1 10


Iron 1.00 75-125mg/l0.0501.04 R2ND 104 11 10

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers




LCS Analyzed: 08/06/2010 (10H0245-BS1)



Perchlorate 25.0 85-115ug/lNA24.8 99 2 15

Duplicate Analyzed: 08/06/2010 (10H0245-DUP1) Source: PTH0226-02



Perchlorate ug/l2.02.13 R91.61 28 15


Perchlorate 25.0 80-120ug/l2.030.8 7.81 92


Perchlorate 25.0 80-120ug/l2.025.0 2.18 91


Perchlorate 25.0 80-120ug/l2.031.1 7.81 93 1 15


Perchlorate 25.0 80-120ug/l2.024.3 2.18 89 3 15



Chloride mg/l2.0ND

Sulfate mg/l2.0ND

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers


LCS Analyzed: 08/06/2010 (10H0255-BS1)

Chloride 20.0 90-110mg/l2.019.9 N1b99

Sulfate 20.0 90-110mg/l2.019.5 98


Chloride 20.0 90-110mg/l2.019.9 N1b100 0.07 15

Sulfate 20.0 90-110mg/l2.019.6 98 0.5 15


Sulfate 20.0 80-120mg/l2.047.0 27.0 100


Sulfate 20.0 80-120mg/l2.049.6 29.7 100


Sulfate 20.0 80-120mg/l2.047.6 27.0 103 1 15


Sulfate 20.0 80-120mg/l2.049.7 29.7 100 0.06 15

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorate ug/l20ND

Chlorite ug/l20ND


LCS Analyzed: 08/12/2010 (10H1381-BS1)

Chlorate 100 75-125ug/l2092.9 93

Chlorite 100 75-125ug/l2099.9 100


Matrix Spike Analyzed: 08/12/2010 (10H1381-MS1) Source: ITH0228-01

Chlorate 100 75-125ug/l2096.2 16.1 80

Chlorite 100 75-125ug/l2095.8 ND 96


Matrix Spike Dup Analyzed: 08/12/2010 (10H1381-MSD1) Source: ITH0228-01

Chlorate 100 75-125ug/l2097.8 16.1 82 2 25

Chlorite 100 75-125ug/l2097.5 ND 97 2 25


Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02









Q3 Sample received with improper chemical preservation.


R2 The RPD exceeded the acceptance limit.






Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily




454-9303





Sampled:

Received:

08/04/10


Project ID:

PTH0241

PGA North 103965.02



TestAmerica Phoenix

Water XE200.7

Water XEPA 300.0

Water XEPA 314.0

XWater XEPA 8260B






Analysis Performed: HydrogenSamples: PTH0241-01, PTH0241-03, PTH0241-06



Method Performed: EPA 300.1Samples: PTH0241-01, PTH0241-03, PTH0241-06

Project Manager

TestAmerica Phoenix

PTH0241

Kylie Emily



PTH0241

SENDING LABORATORY:

TestAmerica Phoenix


Phoenix, AZ 85040

Phone: (602) 437-3340




TestAmerica Irvine


Irvine, CA 92614

Phone :(949) 261-1022




Chlorate (300.1) mg/l 08/18/10

Chlorite (300.1) - 0 mg/l 08/18/10




Chlorate (300.1) mg/l 08/18/10

Chlorite (300.1) - 0 mg/l 08/18/10




Chlorate (300.1) mg/l 08/18/10

Chlorite (300.1) - 0 mg/l 08/18/10



Sampled: 08/04/10 11:0209/01/10 11:02 $30.00 0%

08/18/10 11:02 $30.00 0%

Sampled: 08/04/1013:2109/01/1013:21 $30.00 0%

08/18/1013:21 $30.00 0%

Sampled: 08/04/1014:5509/01/1014:55 $30.00 0%

08/18/1014:55 $30.00 0%


8&/0DatelTime

DatelTime

Rece~

Received By

DatelTime


~ll p..@"6

Environmental Resources Management CHAIN OF CUSTODY-RECORD

SAMPLE I.D.

X X

0 BOTTLE INTACT 0 CUSTODY SEALS 0 CHILLED

0 PRESERVED 0 SEALS INTACT 0 SEE REMARKS

WHITE- LABORATORY COPY CANARY- FIELD COPY PINK- DATABASE

'~'·I 1928

X

/. 0 t;e.

GOLD - PROJECT FILE



Report Date: 08/13/10 Client Proj Name: PTH0241

Client Proj #: PTH0241

Lab Sample#

P1 008085··01

P1 008085-02

p 1 008085-03


Client Sample ID

PTH0241-01

PTH0241-03

PTH0241-06

Laboratory Results Total pages in data package:

Microseeps test results meet all

Approved Bv:





Case Narrative:

220 William Pitt Way Pittsburgh, PA 15238 Tel 412-826-5245 Fax 412-826-3433

website email @






Received Sample Descriptio.D. PTH0241-01

Matrix Vapor


Sampled Daten·ime 04Aug. 10 11:02 06 Aug. 10 13:51

Res kAna lysis N Hydrogen 930.000 30.000 nM AM20GAX 8/12/1 0

Data Qualifiers: J- estimated value, U -Non detect, R -Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B -detected in blank, S - field sample as received did not meet NELAC sample acceptance criteria, L - Subcontracted Lab used, N - NELAC certified analysis

sl






Received Sample Description PTH0241-03

Matrix Vapor


Sampled Date/Time 04 Aug. 10 13:21 06 Aug. 10 13:51


Data Qualifiers J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, Si\MP/DUP, B- detected

in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N - NELAC certified analysis

sl




Report Date: 08/13/1 0 Client Proj Name: PTH0241


Received Sample Description PTH0241-06

Matrix Vapor

Lab Sample# p 1 008085-03

Sampled Date/Time 04 Aug. 10 14:55 06 Aug. 10 13:51

RiskAna!ysis N Hydrogen 8800.000 120.000 nM AM20GAX 8/12/10

Data Qualifiers J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B- detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N .. NELAC certified analysis

sl



Prep Method:

Analysis Method:

M1 00812003-MB

Result T rueSpikeConc. RDL

Hydrogen < 0.600 nJ\1 0.600

M 1 00812003-LCS



M1 00812003-LCSD



Page: Page 5 of 5 Lab Proj #: P 1 008085





%Recov~ Ctl Limits

- NA

%Recoy~ Ctl Limits

91.00 75- 125


90.00 75- 125 1.13

RP.Q Ctl Li.mjt§

0-20

.___ ____ __.!Outlined Results indicate results outside of Control limits

Data Qualifiers: J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B -detected

in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N - NELAC certified analysis

SENDING LABORATORY:

TestAmerica Phoenix



PTH0241



220 William Pitt Way Pittsburgh, PA 15238 Phone :(412)826-5245 Fax: ( 412 )826-3433 Project Location: AZ - ARIZONA

oc Ice: Y I N

Standard TAT is requested unless specific due date is requested. => Due Date: ----- Initials: ----Analysis Units

Sample ID: PTH0241-01 (IRZ-IW-5-08042010- Water)

Hydrogen


NA

%


Hydrogen


NA

%

Sample ID: PTH0241-06 (IRZ-iW-3-08042010- Water)

Hydrogen


NA

%

·~------------

Released By

-------------------------Released By

gk£ Daterrime

Daterrime

ExpiJres Comments

Sampled: 08/04/10 11 :02 09/01/10 11:02 DO NOT CHILL/NO ICE

Sampled: 08/04/10 13:21 09/01/10 13:21 DO NOT CHILL/NO ICE


Page 1 of 1

PTH0241

SENDING LABORATORY:

TestAmerica Phoenix


Phoenix, AZ 85040

Phone: (602) 437-3340




TestAmerica Irvine


Irvine, CA 92614

Phone :(949) 261-1022




Chlorate (300.1) mg/l 08/18/10

Chlorite (300.1) - 0 mg/l 08/18/10




Chlorate (300.1) mg/l 08/18/10

Chlorite (300.1) - 0 mg/l 08/18/10




Chlorate (300.1) mg/l 08/18/10

Chlorite (300.1) - 0 mg/l 08/18/10



Sampled: 08/04/10 11:0209/01/10 11:02 $30.00 0%

08/18/10 11:02 $30.00 0%

Sampled: 08/04/1013:2109/01/1013:21 $30.00 0%

08/18/1013:21 $30.00 0%

Sampled: 08/04/1014:5509/01/1014:55 $30.00 0%

08/18/1014:55 $30.00 0%


8&/0DatelTime

DatelTime

Rece~

Received By

DatelTime


~ll p..@"6


454-9303

LABORATORY REPORT





Received:

Issued:

08/05/10

08/05/10

08/19/10 13:34









CASE NARRATIVE


PTH0352-01 IRZ-MW-B-08052010 Water

PTH0352-02 IRZ-MW-B-08052010 Water

PTH0352-03 IRZ-MW-D-115-08052010 Water

PTH0352-04 IRZ-MW-D-125-08052010 Water

PTH0352-05 IRZ-MW-D-08052010 Water

PTH0352-06 IRZ-MW-D-08052010 Water

PTH0352-07 IRZ-MW-D-08052010D Water

PTH0352-08 IRZ-MW-C-115-08052010 Water

PTH0352-09 IRZ-MW-C-125-08052010 Water

PTH0352-10 IRZ-MW-C-08052010 Water

PTH0352-11 IRZ-MW-C-08052010 Water

PTH0352-12 IRZ-IW-1-08052010 Water

PTH0352-13 IRZ-IW-1-08052010 Water

PTH0352-14 IRZ-IW-1-08052010R Water

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily

<Page 1 of 72>


454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02






N1a-The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).

N1b-8260-The Laboratory Control Sample and Matrix Spike / Matrix Spike Duplicate recovered high and

outside of acceptance limits for 1,1-Dichloroethene. All associated samples are non-detect for this

compound and therefore are not impacted.

N1b-300.0-Results exceeded the linear range in the MS/MSD and therefore are not available for reporting.


N1c-The RPD exceeded the acceptance limit due to sample matrix effects.







Reviewed By:

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-01 (IRZ-MW-B-08052010 - Water) Sampled: 08/05/10


Acetone 8/10/20108/10/201010H0366 10 1EPA 8260B 34

Benzene 8/10/20108/10/201010H0366 0.50 1EPA 8260B 1.6



























1,2-Dichloroethane 8/10/20108/10/201010H0366 0.50 1EPA 8260B 0.50

cis-1,2-Dichloroethene 8/10/20108/10/201010H0366 0.50 1EPA 8260B 6.4



1,3-Dichloropropane 8/10/20108/10/201010H0366 0.50 1EPA 8260B 0.65







2-Hexanone 8/10/20108/10/201010H0366 2.5 1EPA 8260B 3.4

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-01 (IRZ-MW-B-08052010 - Water) - cont. Sampled: 08/05/10






4-Methyl-2-pentanone (MIBK) 8/10/20108/10/201010H0366 2.5 1EPA 8260B 5.1

Methyl-tert-butyl Ether (MTBE) 8/10/20108/10/201010H0366 0.50 1EPA 8260B 0.68



8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




Toluene 8/10/20108/10/201010H0366 0.50 1EPA 8260B 2.0






1,2,3-Trichloropropane 8/10/20108/10/201010H0366 1.0 1EPA 8260B 1.1









Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-01RE1 (IRZ-MW-B-08052010 - Water) - cont. Sampled: 08/05/10


8/11/20108/10/2010EPA 8260B1,1-Dichloroethene 2510H0400 50ND

Trichloroethene 8/11/20108/10/201010H0400 25 50EPA 8260B 1100




Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-03 (IRZ-MW-D-115-08052010 - Water) Sampled: 08/05/10


Acetone 8/10/20108/10/201010H0366 10 1EPA 8260B 14

Benzene 8/10/20108/10/201010H0366 0.50 1EPA 8260B 5.2



























1,2-Dichloroethane 8/10/20108/10/201010H0366 0.50 1EPA 8260B 0.53





1,3-Dichloropropane 8/10/20108/10/201010H0366 0.50 1EPA 8260B 0.67







Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-03 (IRZ-MW-D-115-08052010 - Water) - cont. Sampled: 08/05/10








Methyl-tert-butyl Ether (MTBE) 8/10/20108/10/201010H0366 0.50 1EPA 8260B 0.93



8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND


1,1,2,2-Tetrachloroethane 8/10/20108/10/201010H0366 0.50 1EPA 8260B 0.74


8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND




1,1,2-Trichloroethane 8/10/20108/10/201010H0366 0.50 1EPA 8260B 0.66



1,2,3-Trichloropropane 8/10/20108/10/201010H0366 1.0 1EPA 8260B 1.3









Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-04 (IRZ-MW-D-125-08052010 - Water) Sampled: 08/05/10


Acetone 8/10/20108/10/201010H0366 10 1EPA 8260B 11

Benzene 8/10/20108/10/201010H0366 0.50 1EPA 8260B 0.81







































Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-04 (IRZ-MW-D-125-08052010 - Water) - cont. Sampled: 08/05/10










8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-04RE1 (IRZ-MW-D-125-08052010 - Water) - cont. Sampled: 08/05/10







Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-05 (IRZ-MW-D-08052010 - Water) Sampled: 08/05/10


8/10/20108/10/2010EPA 8260BAcetone 1010H0366 1ND

8/10/20108/10/2010EPA 8260BBenzene 0.5010H0366 1ND







































Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-05 (IRZ-MW-D-08052010 - Water) - cont. Sampled: 08/05/10











8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-05RE1 (IRZ-MW-D-08052010 - Water) - cont. Sampled: 08/05/10






Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-07 (IRZ-MW-D-08052010D - Water) Sampled: 08/05/10


8/10/20108/10/2010EPA 8260BAcetone 1010H0366 1ND

8/10/20108/10/2010EPA 8260BBenzene 0.5010H0366 1ND







































Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-07 (IRZ-MW-D-08052010D - Water) - cont. Sampled: 08/05/10











8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-07RE1 (IRZ-MW-D-08052010D - Water) - cont. Sampled: 08/05/10






Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-08 (IRZ-MW-C-115-08052010 - Water) Sampled: 08/05/10


Acetone 8/10/20108/10/201010H0366 10 1EPA 8260B 10

Benzene 8/10/20108/10/201010H0366 0.50 1EPA 8260B 7.0







































Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-08 (IRZ-MW-C-115-08052010 - Water) - cont. Sampled: 08/05/10










8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-08RE1 (IRZ-MW-C-115-08052010 - Water) - cont. Sampled: 08/05/10







Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-09 (IRZ-MW-C-125-08052010 - Water) Sampled: 08/05/10


Acetone 8/10/20108/10/201010H0366 10 1EPA 8260B 12

Benzene 8/10/20108/10/201010H0366 0.50 1EPA 8260B 4.7







































Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-09 (IRZ-MW-C-125-08052010 - Water) - cont. Sampled: 08/05/10










8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-09RE1 (IRZ-MW-C-125-08052010 - Water) - cont. Sampled: 08/05/10







Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-10 (IRZ-MW-C-08052010 - Water) Sampled: 08/05/10


8/10/20108/10/2010EPA 8260BAcetone 1010H0366 1ND

8/10/20108/10/2010EPA 8260BBenzene 0.5010H0366 1ND







































Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-10 (IRZ-MW-C-08052010 - Water) - cont. Sampled: 08/05/10











8/10/20108/10/2010EPA 8260BStyrene 0.5010H0366 1ND




8/10/20108/10/2010EPA 8260BToluene 0.5010H0366 1ND















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-10RE1 (IRZ-MW-C-08052010 - Water) - cont. Sampled: 08/05/10






Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-12RE1 (IRZ-IW-1-08052010 - Water) Sampled: 08/05/10


Trichloroethene 8/11/20108/11/201010H0403 50 M2100EPA 8260B 7800




Sample ID: PTH0352-12RE2 (IRZ-IW-1-08052010 - Water) Sampled: 08/05/10


8/12/20108/12/2010EPA 8260BAcetone 50010H0475 50ND

8/12/20108/12/2010EPA 8260BBenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BBromobenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BBromochloromethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260BBromodichloromethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260BBromoform 5010H0475 50ND

8/12/20108/12/2010EPA 8260BBromomethane 5010H0475 50ND

8/12/20108/12/2010EPA 8260B2-Butanone (MEK) 12010H0475 50ND

8/12/20108/12/2010EPA 8260Bn-Butylbenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260Bsec-Butylbenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260Btert-Butylbenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BCarbon disulfide 2510H0475 50ND

8/12/20108/12/2010EPA 8260BCarbon tetrachloride 2510H0475 50ND

8/12/20108/12/2010EPA 8260BChlorobenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BChloroethane 5010H0475 50ND

8/12/20108/12/2010EPA 8260BChloroform 2510H0475 50ND

8/12/20108/12/2010EPA 8260BChloromethane 5010H0475 50ND

8/12/20108/12/2010EPA 8260B2-Chlorotoluene 2510H0475 50ND

8/12/20108/12/2010EPA 8260B4-Chlorotoluene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BDibromochloromethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,2-Dibromo-3-chloropropane 12010H0475 50ND

8/12/20108/12/2010EPA 8260B1,2-Dibromoethane (EDB) 2510H0475 50ND

8/12/20108/12/2010EPA 8260BDibromomethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,2-Dichlorobenzene 2510H0475 50ND



8/12/20108/12/2010EPA 8260BDichlorodifluoromethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,1-Dichloroethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,2-Dichloroethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,1-Dichloroethene 2510H0475 50ND

8/12/20108/12/2010EPA 8260Bcis-1,2-Dichloroethene 2510H0475 50ND

8/12/20108/12/2010EPA 8260Btrans-1,2-Dichloroethene 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,2-Dichloropropane 2510H0475 50ND


Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result




8/12/20108/12/2010EPA 8260B1,1-Dichloropropene 2510H0475 50ND

8/12/20108/12/2010EPA 8260Bcis-1,3-Dichloropropene 2510H0475 50ND

8/12/20108/12/2010EPA 8260Btrans-1,3-Dichloropropene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BEthylbenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BHexachlorobutadiene 5010H0475 50ND

8/12/20108/12/2010EPA 8260B2-Hexanone 12010H0475 50ND

8/12/20108/12/2010EPA 8260BIodomethane 12010H0475 50ND

8/12/20108/12/2010EPA 8260BIsopropylbenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260Bp-Isopropyltoluene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BMethylene Chloride 5010H0475 50ND

8/12/20108/12/2010EPA 8260B4-Methyl-2-pentanone (MIBK) 12010H0475 50ND

8/12/20108/12/2010EPA 8260BMethyl-tert-butyl Ether (MTBE) 2510H0475 50ND

8/12/20108/12/2010EPA 8260BNaphthalene 12010H0475 50ND

8/12/20108/12/2010EPA 8260Bn-Propylbenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BStyrene 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,1,1,2-Tetrachloroethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,1,2,2-Tetrachloroethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260BTetrachloroethene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BToluene 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,2,3-Trichlorobenzene 5010H0475 50ND

8/12/20108/12/2010EPA 8260B1,2,4-Trichlorobenzene 5010H0475 50ND

8/12/20108/12/2010EPA 8260B1,1,1-Trichloroethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,1,2-Trichloroethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260BTrichlorofluoromethane 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,2,3-Trichloropropane 5010H0475 50ND

8/12/20108/12/2010EPA 8260B1,2,4-Trimethylbenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260B1,3,5-Trimethylbenzene 2510H0475 50ND

8/12/20108/12/2010EPA 8260BVinyl Acetate 5010H0475 50ND

8/12/20108/12/2010EPA 8260BVinyl chloride 2510H0475 50ND

8/12/20108/12/2010EPA 8260BXylenes, Total 5010H0475 50ND




Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-14RE1 (IRZ-IW-1-08052010R - Water) Sampled: 08/05/10


8/12/20108/12/2010EPA 8260BAcetone 1010H0475 1ND

8/12/20108/12/2010EPA 8260BBenzene 0.5010H0475 1ND



Bromodichloromethane 8/12/20108/12/201010H0475 0.50 1EPA 8260B 0.84




































Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTH0352-14RE1 (IRZ-IW-1-08052010R - Water) - cont. Sampled: 08/05/10











8/12/20108/12/2010EPA 8260BStyrene 0.5010H0475 1ND




8/12/20108/12/2010EPA 8260BToluene 0.5010H0475 1ND
















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 8/10/20108/9/201010H0290 0.050 1E200.7 490

Sodium 8/11/20108/9/201010H0290 20 10E200.7 1300



Iron 8/10/20108/9/201010H0290 0.050 1E200.7 2.1

Sodium 8/10/20108/9/201010H0290 2.0 1E200.7 470



Iron 8/10/20108/9/201010H0290 0.050 1E200.7 57

Sodium 8/10/20108/9/201010H0290 2.0 1E200.7 430



Iron 8/10/20108/9/201010H0290 0.050 1E200.7 0.62

Sodium 8/10/20108/9/201010H0290 2.0 M21E200.7 430

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

DISSOLVED METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



8/9/20108/6/2010E200.7Iron 0.05010H0224 1ND



8/9/20108/6/2010E200.7Iron 0.05010H0224 1ND



Iron 8/9/20108/6/201010H0224 0.050 1E200.7 0.15



8/9/20108/6/2010E200.7Iron 0.05010H0224 1ND

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Chloride 8/6/20108/6/201010H0255 40 20EPA 300.0 1400

Sulfate 8/6/20108/6/201010H0255 40 20EPA 300.0 390






Chloride 8/6/20108/6/201010H0255 40 20EPA 300.0 730

Sulfate 8/6/20108/6/201010H0255 40 20EPA 300.0 930






Chloride 8/6/20108/6/201010H0255 40 20EPA 300.0 730

Sulfate 8/6/20108/6/201010H0255 40 20EPA 300.0 930






Chloride 8/6/20108/6/201010H0255 40 20EPA 300.0 800

Sulfate 8/6/20108/6/201010H0255 40 20EPA 300.0 1100



Perchlorate 8/6/20108/6/201010H0245 2.0 1EPA 314.0 25

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



Chlorate 8/19/20108/18/201010H2175 0.040 2EPA 300.1 0.069

8/16/20108/16/2010EPA 300.1Chlorite 1.010H1815 D150ND





Chlorate 8/19/20108/18/201010H2175 0.040 2EPA 300.1 0.080






Chlorate 8/19/20108/18/201010H2175 0.040 2EPA 300.1 0.092






Chlorate 8/19/20108/18/201010H2175 0.10 5EPA 300.1 0.13

Chlorite 8/16/20108/16/201010H1815 0.40 20EPA 300.1 1.0



Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 08/10/2010 (10H0366-BS1)

Acetone 25.0 10-150ug/l1028.6 114

Benzene 25.0 80-120ug/l0.5027.3 109




Bromoform 25.0 75-130ug/l1.027.3 109


2-Butanone (MEK) 25.0 40-150ug/l2.523.8 95








Chloroform 25.0 75-120ug/l0.5027.5 110














1,1-Dichloroethene 25.0 75-125ug/l0.5031.4 L3126






Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 08/10/2010 (10H0366-BS1)






2-Hexanone 25.0 20-150ug/l2.523.7 95

Iodomethane 25.0 80-130ug/l2.528.2 113






Naphthalene 25.0 40-150ug/l2.527.2 109


Styrene 25.0 80-120ug/l0.5029.2 117




Toluene 25.0 80-120ug/l0.5028.0 112
















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1027.5 110 4 35

Benzene 25.0 80-120ug/l0.5025.9 104 5 15




Bromoform 25.0 75-130ug/l1.024.6 99 10 20


2-Butanone (MEK) 25.0 40-150ug/l2.525.3 101 6 35

n-Butylbenzene 25.0 80-130ug/l0.5024.4 R697 17 15

sec-Butylbenzene 25.0 80-125ug/l0.5023.7 R695 16 15






Chloroform 25.0 75-120ug/l0.5027.4 110 0.3 15




















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.523.9 96 0.8 35

Iodomethane 25.0 80-130ug/l2.526.7 107 5 10






Naphthalene 25.0 40-150ug/l2.524.6 98 10 30


Styrene 25.0 80-120ug/l0.5027.3 109 7 15




Toluene 25.0 80-120ug/l0.5026.2 105 7 15








1,2,4-Trimethylbenzene 25.0 80-120ug/l0.5024.4 R697 16 15








Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1034.8 ND 139

Benzene 25.0 70-125ug/l0.5029.2 0.860 113




Bromoform 25.0 65-125ug/l1.030.2 ND 121









Chloroethane 25.0 65-140ug/l1.030.2 0.110 120

Chloroform 25.0 70-130ug/l0.5031.3 2.03 117






1,2-Dibromoethane (EDB) 25.0 70-125ug/l0.5031.6 M1ND 126

Dibromomethane 25.0 70-120ug/l0.5030.3 M1ND 121







1,1-Dichloroethene 25.0 70-130ug/l0.5041.9 N1b8.94 132




1,3-Dichloropropane 25.0 70-120ug/l0.5030.4 M10.120 121


Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.529.2 1.96 109

Iodomethane 25.0 60-150ug/l2.59.99 M20.640 37






Naphthalene 25.0 40-150ug/l2.532.9 0.920 128


Styrene 25.0 55-135ug/l0.5021.2 ND 85




Toluene 25.0 70-125ug/l0.5027.4 0.120 109
















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1035.6 ND 143 2 35

Benzene 25.0 70-125ug/l0.5031.3 0.860 122 7 25

Bromobenzene 25.0 75-120ug/l0.5030.3 N1aND 121 7 20



Bromoform 25.0 65-125ug/l1.033.1 N1aND 132 9 25







Carbon tetrachloride 25.0 65-135ug/l0.5031.0 0.290 123 6 25


Chloroethane 25.0 65-140ug/l1.031.1 0.110 124 3 25

Chloroform 25.0 70-130ug/l0.5033.4 2.03 126 7 20




Dibromochloromethane 25.0 70-130ug/l0.5035.2 N1aND 141 9 20


1,2-Dibromoethane (EDB) 25.0 70-125ug/l0.5034.0 M1ND 136 7 20

Dibromomethane 25.0 70-120ug/l0.5033.2 M1ND 133 9 20

1,2-Dichlorobenzene 25.0 75-120ug/l0.5030.2 N1aND 121 6 20




1,1-Dichloroethane 25.0 70-130ug/l0.5032.8 N1a0.160 131 8 20


1,1-Dichloroethene 25.0 70-130ug/l0.5043.5 N1b8.94 138 4 25


trans-1,2-Dichloroethene 25.0 75-125ug/l0.5031.3 0.0900 125 4 25

1,2-Dichloropropane 25.0 75-125ug/l0.5032.5 N1aND 130 8 20

1,3-Dichloropropane 25.0 70-120ug/l0.5034.0 M10.120 135 11 20


Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.533.4 1.96 126 13 30

Iodomethane 25.0 60-150ug/l2.54.72 M2, N1c0.640 16 72 30



Methylene Chloride 25.0 65-130ug/l1.033.1 N1a0.190 132 6 20

4-Methyl-2-pentanone (MIBK) 25.0 55-135ug/l2.535.8 N1aND 143 15 25


Naphthalene 25.0 40-150ug/l2.534.7 0.920 135 5 30


Styrene 25.0 55-135ug/l0.5024.3 ND 97 14 35


1,1,2,2-Tetrachloroethane 25.0 70-125ug/l0.5032.3 N1a0.100 129 7 25


Toluene 25.0 70-125ug/l0.5029.2 0.120 116 6 20




1,1,2-Trichloroethane 25.0 75-125ug/l0.5032.3 N1aND 129 12 20

Trichloroethene 25.0 70-125ug/l0.505090 M3, R13040 8190 48 25


1,2,3-Trichloropropane 25.0 70-130ug/l1.032.9 N1aND 131 14 25









Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 08/10/2010 (10H0400-BS1)

Acetone 25.0 10-150ug/l1027.0 108

Benzene 25.0 80-120ug/l0.5025.3 101




Bromoform 25.0 75-130ug/l1.025.6 103


2-Butanone (MEK) 25.0 40-150ug/l2.528.8 115








Chloroform 25.0 75-120ug/l0.5029.0 116




















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 08/10/2010 (10H0400-BS1)






2-Hexanone 25.0 20-150ug/l2.526.0 104

Iodomethane 25.0 80-130ug/l2.528.6 114






Naphthalene 25.0 40-150ug/l2.529.8 119


Styrene 25.0 80-120ug/l0.5027.0 108




Toluene 25.0 80-120ug/l0.5025.8 103













25.0 80-120Surrogate: Dibromofluoromethane ug/l30.4 S10121



Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1026.6 106 1 35

Benzene 25.0 80-120ug/l0.5026.6 106 5 15




Bromoform 25.0 75-130ug/l1.026.0 104 1 20


2-Butanone (MEK) 25.0 40-150ug/l2.526.6 106 8 35








Chloroform 25.0 75-120ug/l0.5028.6 114 1 15




















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.524.6 98 5 35

Iodomethane 25.0 80-130ug/l2.529.1 116 2 10






Naphthalene 25.0 40-150ug/l2.528.3 113 5 30


Styrene 25.0 80-120ug/l0.5027.1 108 0.4 15




Toluene 25.0 80-120ug/l0.5026.8 107 4 15
















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 125 10-150ug/l50139 ND 111

Benzene 125 70-125ug/l2.5141 ND 113



Bromodichloromethane 125 75-125ug/l2.5149 2.60 117

Bromoform 125 65-125ug/l5.0118 ND 94


2-Butanone (MEK) 125 15-150ug/l12139 ND 112








Chloroform 125 70-130ug/l2.5148 ND 119











Dichlorodifluoromethane 125 60-150ug/l2.5141 ND 113



1,1-Dichloroethene 125 70-130ug/l2.5140 1.05 111






Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







Hexachlorobutadiene 125 40-150ug/l5.0131 ND 105

2-Hexanone 125 20-150ug/l12136 ND 109




Methylene Chloride 125 65-130ug/l5.0139 0.800 111





Styrene 125 55-135ug/l2.5142 ND 114



Tetrachloroethene 125 65-130ug/l2.5131 ND 105

Toluene 125 70-125ug/l2.5134 ND 108




1,1,2-Trichloroethane 125 75-125ug/l2.5138 12.2 101

Trichloroethene 125 70-125ug/l2.5353 225 103











Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 125 10-150ug/l50142 ND 114 2 35

Benzene 125 70-125ug/l2.5136 ND 109 4 25

Bromobenzene 125 75-120ug/l2.5140 ND 112 8 20

Bromochloromethane 125 75-130ug/l2.5135 ND 108 3 20

Bromodichloromethane 125 75-125ug/l2.5145 2.60 114 3 20

Bromoform 125 65-125ug/l5.0131 ND 105 11 25

Bromomethane 125 45-150ug/l5.0130 ND 104 0.9 35

2-Butanone (MEK) 125 15-150ug/l12147 ND 118 5 30

n-Butylbenzene 125 70-130ug/l2.5142 ND 114 5 30

sec-Butylbenzene 125 70-125ug/l2.5146 ND 117 8 30

tert-Butylbenzene 125 70-125ug/l2.5141 ND 113 4 25

Carbon disulfide 125 65-145ug/l2.5145 ND 116 3 25

Carbon tetrachloride 125 65-135ug/l2.5141 ND 113 2 25

Chlorobenzene 125 75-120ug/l2.5138 ND 110 1 20

Chloroethane 125 65-140ug/l5.0144 ND 115 4 25

Chloroform 125 70-130ug/l2.5145 ND 116 2 20

Chloromethane 125 55-145ug/l5.0138 ND 110 8 35



Dibromochloromethane 125 70-130ug/l2.5142 ND 113 0.1 20

1,2-Dibromo-3-chloropropane 125 50-150ug/l12140 ND 112 8 30

1,2-Dibromoethane (EDB) 125 70-125ug/l2.5144 ND 115 4 20

Dibromomethane 125 70-120ug/l2.5148 ND 119 0.3 20




Dichlorodifluoromethane 125 60-150ug/l2.5140 ND 112 1 30



1,1-Dichloroethene 125 70-130ug/l2.5147 1.05 117 5 25

cis-1,2-Dichloroethene 125 70-125ug/l2.5141 ND 113 3 20

trans-1,2-Dichloroethene 125 75-125ug/l2.5147 ND 118 4 25

1,2-Dichloropropane 125 75-125ug/l2.5144 1.15 114 0.9 20

1,3-Dichloropropane 125 70-120ug/l2.5147 4.95 113 3 20

2,2-Dichloropropane 125 65-140ug/l5.0121 ND 97 4 25

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 125 65-130ug/l2.5141 ND 113 1 25

cis-1,3-Dichloropropene 125 75-130ug/l2.5132 ND 105 0.6 20

trans-1,3-Dichloropropene 125 70-130ug/l2.5142 ND 114 3 20

Ethylbenzene 125 70-125ug/l2.5141 ND 112 2 25

Hexachlorobutadiene 125 40-150ug/l5.0142 ND 114 8 30

2-Hexanone 125 20-150ug/l12134 ND 108 1 30

Iodomethane 125 60-150ug/l12147 ND 118 8 30

Isopropylbenzene 125 75-130ug/l2.5155 ND 124 4 25

p-Isopropyltoluene 125 70-130ug/l2.5146 ND 117 5 30

Methylene Chloride 125 65-130ug/l5.0144 0.800 114 3 20

4-Methyl-2-pentanone (MIBK) 125 55-135ug/l12135 ND 108 0.6 25

Methyl-tert-butyl Ether (MTBE) 125 65-140ug/l2.5138 ND 110 2 25

Naphthalene 125 40-150ug/l12148 ND 119 8 30

n-Propylbenzene 125 70-130ug/l2.5147 ND 118 4 30

Styrene 125 55-135ug/l2.5144 ND 115 1 35



Tetrachloroethene 125 65-130ug/l2.5129 ND 104 1 25

Toluene 125 70-125ug/l2.5134 ND 107 0.6 20



1,1,1-Trichloroethane 125 70-130ug/l2.5143 ND 114 0.03 25

1,1,2-Trichloroethane 125 75-125ug/l2.5134 12.2 97 3 20

Trichloroethene 125 70-125ug/l2.5344 225 96 3 25

Trichlorofluoromethane 125 65-150ug/l2.5159 ND 128 4 25

1,2,3-Trichloropropane 125 70-130ug/l5.0141 ND 113 8 25



Vinyl Acetate 125 40-150ug/l5.0124 ND 99 2 30

Vinyl chloride 125 60-140ug/l2.5140 ND 112 0.8 25

Xylenes, Total 250 75-120ug/l5.0277 ND 111 3 15




Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








LCS Analyzed: 08/11/2010 (10H0403-BS1)







1,1-Dichloroethene 25.0 75-125ug/l0.5026.8 107 0.04 20






1,1-Dichloroethene 2500 70-130ug/l502630 25.0 104

Trichloroethene 2500 70-125ug/l508900 M27780 45





1,1-Dichloroethene 2500 70-130ug/l502690 25.0 107 2 25

Trichloroethene 2500 70-125ug/l509240 M27780 59 4 25




Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 08/12/2010 (10H0475-BS1)

Acetone 25.0 10-150ug/l1025.2 101

Benzene 25.0 80-120ug/l0.5024.2 97




Bromoform 25.0 75-130ug/l1.027.8 111


2-Butanone (MEK) 25.0 40-150ug/l2.528.0 112








Chloroform 25.0 75-120ug/l0.5024.7 99




















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 08/12/2010 (10H0475-BS1)






2-Hexanone 25.0 20-150ug/l2.528.9 116

Iodomethane 25.0 80-130ug/l2.529.0 116






Naphthalene 25.0 40-150ug/l2.527.4 110


Styrene 25.0 80-120ug/l0.5028.0 112




Toluene 25.0 80-120ug/l0.5024.6 99
















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1027.4 110 9 35

Benzene 25.0 80-120ug/l0.5025.1 101 4 15




Bromoform 25.0 75-130ug/l1.029.2 117 5 20


2-Butanone (MEK) 25.0 40-150ug/l2.531.9 128 13 35


sec-Butylbenzene 25.0 80-125ug/l0.5025.8 103 0.2 15






Chloroform 25.0 75-120ug/l0.5024.7 99 0.04 15




















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 75-120ug/l0.5025.4 102 0.4 15




Hexachlorobutadiene 25.0 40-150ug/l1.028.6 114 0.6 35

2-Hexanone 25.0 20-150ug/l2.529.1 117 0.9 35

Iodomethane 25.0 80-130ug/l2.531.2 125 7 10


p-Isopropyltoluene 25.0 80-130ug/l0.5026.7 107 0.8 15




Naphthalene 25.0 40-150ug/l2.528.4 113 3 30


Styrene 25.0 80-120ug/l0.5027.6 110 1 15




Toluene 25.0 80-120ug/l0.5025.5 102 3 15






Trichlorofluoromethane 25.0 70-150ug/l0.5028.7 115 0.1 25






Xylenes, Total 50.0 60-140ug/l1.053.4 107 0.9 15




Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1035.0 10.1 100

Benzene 25.0 70-125ug/l0.5022.9 ND 92




Bromoform 25.0 65-125ug/l1.025.5 ND 102










Chloroform 25.0 70-130ug/l0.5022.1 0.340 87




















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.532.5 1.37 125







Naphthalene 25.0 40-150ug/l2.528.1 0.500 111


Styrene 25.0 55-135ug/l0.5025.4 ND 101




Toluene 25.0 70-125ug/l0.5023.5 ND 94
















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1031.3 10.1 85 11 35

Benzene 25.0 70-125ug/l0.5023.6 ND 94 3 25




Bromoform 25.0 65-125ug/l1.026.3 ND 105 3 25



n-Butylbenzene 25.0 70-130ug/l0.5024.7 ND 99 0.4 30




Carbon tetrachloride 25.0 65-135ug/l0.5026.5 ND 106 0.5 25



Chloroform 25.0 70-130ug/l0.5023.1 0.340 91 5 20






1,2-Dibromoethane (EDB) 25.0 70-125ug/l0.5024.2 ND 97 0.9 20


1,2-Dichlorobenzene 25.0 75-120ug/l0.5025.1 ND 101 0.4 20







cis-1,2-Dichloroethene 25.0 70-125ug/l0.5021.5 ND 86 0.8 20





Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers






Ethylbenzene 25.0 70-125ug/l0.5024.3 ND 97 0.2 25


2-Hexanone 25.0 20-150ug/l2.526.4 1.37 100 21 30




Methylene Chloride 25.0 65-130ug/l1.021.8 ND 87 0.9 20



Naphthalene 25.0 40-150ug/l2.526.1 0.500 102 8 30


Styrene 25.0 55-135ug/l0.5025.4 ND 102 0.1 35

1,1,1,2-Tetrachloroethane 25.0 70-125ug/l0.5024.9 ND 100 0.1 20

1,1,2,2-Tetrachloroethane 25.0 70-125ug/l0.5023.6 0.130 94 2 25


Toluene 25.0 70-125ug/l0.5024.7 ND 99 5 20
















Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Iron mg/l0.050ND

Sodium mg/l2.0ND

LCS Analyzed: 08/10/2010 (10H0290-BS1)

Iron 1.00 85-115mg/l0.0500.946 95

Sodium 20.0 85-115mg/l2.018.6 93


Iron 1.00 85-115mg/l0.0500.933 93 1 20

Sodium 20.0 85-115mg/l2.018.6 93 0.03 20


Iron 1.00 75-125mg/l0.0501.56 0.620 94

Sodium 20.0 75-125mg/l2.0433 M2428 28


Iron 1.00 75-125mg/l0.05019.7 M219.9 -22

Sodium 20.0 75-125mg/l2.0129 111 90


Iron 1.00 75-125mg/l0.0501.55 0.620 93 0.7 10

Sodium 20.0 75-125mg/l2.0430 M2428 9 0.9 10


Iron 1.00 75-125mg/l0.05020.0 M219.9 9 2 10

Sodium 20.0 75-125mg/l2.0129 111 93 0.4 10

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

DISSOLVED METALS


Data

Qualifiers



Iron mg/l0.050ND


Iron mg/l0.050ND

LCS Analyzed: 08/09/2010 (10H0224-BS1)

Iron 1.00 85-115mg/l0.0501.04 104


Iron 1.00 85-115mg/l0.0501.05 105 0.7 20


Iron 1.00 75-125mg/l0.0501.16 0.113 105


Iron 1.00 75-125mg/l0.0501.16 ND 116


Iron 1.00 75-125mg/l0.0501.17 0.113 106 1 10


Iron 1.00 75-125mg/l0.0501.04 R2ND 104 11 10

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers




LCS Analyzed: 08/06/2010 (10H0245-BS1)



Perchlorate 25.0 85-115ug/lNA24.8 99 2 15




Perchlorate ug/l2.02.13 R91.61 28 15


Perchlorate 25.0 80-120ug/l2.030.8 7.81 92


Perchlorate 25.0 80-120ug/l2.025.0 2.18 91


Perchlorate 25.0 80-120ug/l2.031.1 7.81 93 1 15


Perchlorate 25.0 80-120ug/l2.024.3 2.18 89 3 15



Chloride mg/l2.0ND

Sulfate mg/l2.0ND

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers


LCS Analyzed: 08/06/2010 (10H0255-BS1)

Chloride 20.0 90-110mg/l2.019.9 N1b99

Sulfate 20.0 90-110mg/l2.019.5 98


Chloride 20.0 90-110mg/l2.019.9 N1b100 0.07 15

Sulfate 20.0 90-110mg/l2.019.6 98 0.5 15


Sulfate 20.0 80-120mg/l2.047.0 27.0 100


Sulfate 20.0 80-120mg/l2.049.6 29.7 100


Sulfate 20.0 80-120mg/l2.047.6 27.0 103 1 15


Sulfate 20.0 80-120mg/l2.049.7 29.7 100 0.06 15

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorite mg/l0.020ND

0.00100 90-115Surrogate: Dichloroacetate (DCA) mg/l0.000980 98

LCS Analyzed: 08/16/2010 (10H1815-BS1)

Chlorite 0.100 75-125mg/l0.0200.0977 98



Chlorite 0.100 75-125mg/l0.0400.0978 ND 98



Chlorite 0.100 75-125mg/l0.0400.100 ND 100 3 25




Chlorate mg/l0.020ND


LCS Analyzed: 08/18/2010 (10H2175-BS1)

Chlorate 0.100 75-125mg/l0.0200.0932 93



Chlorate 0.100 75-125mg/l0.0200.0918 ND 92


Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorate 0.100 75-125mg/l0.0200.0957 ND 96 4 25


Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02










R2 The RPD exceeded the acceptance limit.






Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




454-9303





Sampled:

Received:

08/05/10


Project ID:

PTH0352

PGA North 103965.02



TestAmerica Phoenix

Water XE200.7

Water XEPA 300.0

Water XEPA 314.0

XWater XEPA 8260B






Analysis Performed: HydrogenSamples: PTH0352-05, PTH0352-10, PTH0352-12



Method Performed: EPA 300.1Samples: PTH0352-01, PTH0352-05, PTH0352-10, PTH0352-12

Project Manager

TestAmerica Phoenix

PTH0352

Kylie Emily




PTH0352

SENDING LABORATORY:

TestAmerica Phoenix


Phoenix, AZ 85040

Phone: (602) 437-3340

Fax: (602) 454-9303Project Manager: Kylie EmilyClient: Environmental Resources Management InC.-West


TestAmerica Irvine


Irvine, CA 92614

Phone :(949) 261-1022

Fax: (949) 261-1228Project Location: AZ - ARIZONAReceipt Temperature: DC Ice: Y / N


Sample ID: PTH0352-01 (IRZ-MW-B-OS052010- Water) Sampled: OS10511007:40

Chlorate (300.1) mg/I 08/19/10 09/02/1007:40 $30.00 0%

Chlorite (300.1) - 0 mg/I 08/19/10 08/19/1007:40 $30.00 0%


500 ml Poly w/EDA (F) 125mL Brown Poly w/EDA (G)

Sample ID: PTH0352-05 (IRZ-MW-D-OS052010- Water) Sampled: OS105110OS:55

Chlorate (300.1) mg/I 08/19/10 09/02/1008:55 $30.00 0%

Chlorite (300.1) - 0 mg/l 08/19/10 08/19/1008:55 $30.00 0%



Sample ID: PTH0352-10 (IRZ-MW-C-OS052010- Water) Sampled: OS10511011:05

Chlorate (300.1) mg/I 08/19/1009/02/1011:05 $30.00 0%

Chlorite (300.1)-0 mg/I 08/19/1008/19/1011:05 $30.00 0%



_DL gld\l) jlU-vReleased By DatelTime

Sample ID: PTH0352-12 (IRZ-IW-1-0S052010 - Water)

Chlorate (300.1) mg/I 08/19/10

Chlorite (300.1) - 0 mg/I 08/19/10



Released By DatelTime

Sampled: OS10511013:1309/02/1013:13 $30.00 0%

08/19/1013:13 $30.00 0%

fEDReceived By?ii[~Recei\IeY

1200DatelTime Page 1 of 1

Environmental Resources Management CHAIN OF CUSTODY RECORD

PTl-1 03 ZJ :L ··~~ , .... ,~,:-:::9:-::2--=-9--1

7272E.IndianSchooiRoad,Su~e100•Scottsd~e,AZ•85251•~8~998~4~0~1~•~~~(~48=0~)~99=8~~~1~06~~~~~~~P~a~ge~~~~~~o~f~~~~~

SAMPLE I.D. SAMPLING METHOD

Add i 1"t~pBico ~ r Vf) c , ~~~~~~~~~A+~:;::-b,.-,;r:--f--c----7-r;;::r::;[::-;\/Cnt=)\,-------J--n--;rr;::-b...--;,cj LQ,h .}i c, 1 d ~I\ 14" '1R l:. ~ f\'\ w .. s ·- o a-osO.<Jl Q;

%r ch:>-;ol "c J 'fe.. 11

/. 2.t_ :' TO:

0 PRESERVED 0 SEALS INTACT 0 SEE REMARKS tl)...,,v·l c·~,tl,.;f\ r '"· t\.

[J BOTTLE INTACT 0 CUSTODY SEALS 0 CHILLED ··'

WHITE- LABORATORY COPY CANARY- FIELD COPY PINK- DATABASE GOLD - PROJECT FILE





Lab Sample#

P1 008112-01

P1 008112-02

P1 008112-03

Approved By:

Project Manager:


Client Sample ID

PTH0352-05

PTH0352-1 0

PTH0352-12

Debbie Hallo

Total pages in data package:




Case Narrative:

220 William Pitt Way Pittsburgh, PA 15238 Tel 412-826-5245 Fax 412-826-3433

website email






Received Sample DescrjQtion PTH0352-05

Matrix Vapor


Sar:npled Date/Time 05 Aug. 10 8:55 10 Aug. 10 12:50


Data Qualifiers: .l- estimated value, U- Non detect, R -Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B- detected

in blank, S - field sample as received did not meet NELAC sample acceptance criteria, L - Subcontracted Lab used, N - NELAC certified analysis

sl


Sample Description PTH0352-1 0

RiskAnalysns N Hydrogen


Matrix Vapor


170.000 6.000 nM




Sampled Date/Time 05Aug.10 11:05

AM20GAX 8/12/1 0

Received 10Aug. 10 12:50

sl

Data Qualifiers: .1- estimated value, U- Non detect, R Poor surrogate recovery, M Recovery/RPD poor for MS/MSD, SAMP/DUP, B- detected

in blank, S ··field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N- NELAC certified analysis



Sample Description PTH0352-12

RiskAnalysis N Hydrogen


!VIatrix Vapor

Lab Sample# P1008112-03

100.000 2.400 nM




Sampled Date/Time 05 Aug. 10 13:13

AM20GAX 8/12/10

Received 10Aug. 10 12:50

sl

Data Qualifiers J- estimated value, U -Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B -detected

in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L Subcontracted Lab used, N - NELAC certified analysis





Client Proj #: PTH0352 Suite 189 Phoenix, AZ 85040

Prep Method: Hydrogen by Bubble Strip

Analysis Method: Hydrogen by Bubble Strip

M1 00812003-MB

Result TrueSQikeConc. RDL %Recover:y Ctl Limits

Hydrogen < 0.600 nM 0.600 NA

M1 00812003-LCS

Result TrueSQikeConc. %Recover:y Ctl Limits

Hydrogen 8.900 nM 9.78 91.00 75- 125

M1 00812003-lCSD

Result TrueSQikeConc. %Recover:y Ctl Limits RPD RPD Ctl Limits

Hydrogen 8.800 nM 9.78 90.00 75- 125 1.13 0-20

...._ ____ __,!Outlined Results indicate results outside of Control limits

Data Qualifiers: 1 -estimated value, U -Non detect, R -Poor surrogate recovery, M - Recovery/RPD poor for MS/MSD, SAMP/D1JP, B - detected in blank, S - field sample as received did not meet NELAC sample acceptance criteria, L - Subcontracted Lab used, N - NELAC certified analysis

SUBCONTRACT ORDER

SENDING LABORATORY:

TestAmerica Phoenix


TestAmerica Phoennx



220 William Pitt Way Pittsburgh, PA 15238 Phone :( 412)826-5245 Fax: (412)826-3433 Project Location: AZ- ARIZONA Receipt Temperature: oc Ice: Y I N

Sta)[][dard TAT is re<:p.l!ested U)[][less specific due date is requested. => Due Date: ----- ][][][fttials:

Analysis Units

Sample ID: PTH0352-05 (IRZ-MW-D-0805201 0- Water)

Hydrogen


NA

%

Sample 10: PTH0352-10 (IRZ-MW-C-08052010- Water)

Hydrogen


NA

%


Hydrogen


NA

Released By

r=;eleased By

%

Date/Time

------Date/Time

Expires Comments

Sampled: 08/05/10 08:55 09/02/1 0 08:55 DO NOT CHILL/NO ICE

Sampled: 08/05/10 11:05 09/02/10 11 :05 DO NOT CHILL/NO ICE


\

;i.~,,~ __ .. ..:) Page 1 of 1


PTH0352

SENDING LABORATORY:

TestAmerica Phoenix


Phoenix, AZ 85040

Phone: (602) 437-3340

Fax: (602) 454-9303Project Manager: Kylie EmilyClient: Environmental Resources Management InC.-West


TestAmerica Irvine


Irvine, CA 92614

Phone :(949) 261-1022

Fax: (949) 261-1228Project Location: AZ - ARIZONAReceipt Temperature: DC Ice: Y / N


Sample ID: PTH0352-01 (IRZ-MW-B-OS052010- Water) Sampled: OS10511007:40

Chlorate (300.1) mg/I 08/19/10 09/02/1007:40 $30.00 0%

Chlorite (300.1) - 0 mg/I 08/19/10 08/19/1007:40 $30.00 0%



Sample ID: PTH0352-05 (IRZ-MW-D-OS052010- Water) Sampled: OS105110OS:55

Chlorate (300.1) mg/I 08/19/10 09/02/1008:55 $30.00 0%

Chlorite (300.1) - 0 mg/l 08/19/10 08/19/1008:55 $30.00 0%



Sample ID: PTH0352-10 (IRZ-MW-C-OS052010- Water) Sampled: OS10511011:05

Chlorate (300.1) mg/I 08/19/1009/02/1011:05 $30.00 0%

Chlorite (300.1)-0 mg/I 08/19/1008/19/1011:05 $30.00 0%



_DL gld\l) jlU-vReleased By DatelTime

Sample ID: PTH0352-12 (IRZ-IW-1-0S052010 - Water)

Chlorate (300.1) mg/I 08/19/10

Chlorite (300.1) - 0 mg/I 08/19/10



Released By DatelTime

Sampled: OS10511013:1309/02/1013:13 $30.00 0%

08/19/1013:13 $30.00 0%

fEDReceived By?ii[~Recei\IeY

1200DatelTime Page 1 of 1


454-9303

LABORATORY REPORT





Received:

Issued:

02/10/10

02/10/10

02/26/10 10:54









CASE NARRATIVE


PTB0691-01 IRZ-MW-B-2102010 Water

PTB0691-02 IRZ-MW-B-2102010 Water

PTB0691-03 IRZ-IW-5-2102010 Water

PTB0691-04 IRZ-IW-5-2102010 Water

PTB0691-05 IRZ-MW-C-2102010 Water

PTB0691-06 IRZ-MW-C-2102010 Water

PTB0691-07 Trip Blank Water

PTB0691-08 IRZ-MW-C-2102010R Water

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily

<Page 1 of 56>


454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00







N1-Concentration exceeds the calibration range and therefore result is semi-quantitative.

N1a-pH = 7



Reviewed By:

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-01 (IRZ-MW-B-2102010 - Water) Q3, N1a, D1


2/21/20102/21/2010EPA 8260BAcetone 10010B0809 10ND

2/21/20102/21/2010EPA 8260BBenzene 5.010B0809 10ND




2/21/20102/21/2010EPA 8260BBromoform 1010B0809 10ND





2/21/20102/21/2010EPA 8260Btert-Butylbenzene 5.010B0809 10ND









2/21/20102/21/2010EPA 8260BDibromochloromethane 5.010B0809 10ND




















2/21/20102/21/2010EPA 8260BHexachlorobutadiene 1010B0809 10ND

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-01 (IRZ-MW-B-2102010 - Water) - cont. Q3, N1a, D1











2/21/20102/21/2010EPA 8260BStyrene 5.010B0809 10ND




2/21/20102/21/2010EPA 8260BToluene 5.010B0809 10ND





2/21/20102/21/2010EPA 8260BTrichloroethene 5.010B0809 10ND











Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-03 (IRZ-IW-5-2102010 - Water)


2/23/20102/23/2010EPA 8260BAcetone 10010B0865 10ND

2/23/20102/23/2010EPA 8260BBenzene 5.010B0865 10ND





























cis-1,2-Dichloroethene 2/23/20102/23/201010B0865 5.0 10EPA 8260B 6.3










Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-03 (IRZ-IW-5-2102010 - Water) - cont.











2/23/20102/23/2010EPA 8260BStyrene 5.010B0865 10ND




2/23/20102/23/2010EPA 8260BToluene 5.010B0865 10ND





Trichloroethene 2/23/20102/23/201010B0865 5.0 10EPA 8260B 250











Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-05 (IRZ-MW-C-2102010 - Water)


2/21/20102/21/2010EPA 8260BAcetone 1010B0809 1ND

2/21/20102/21/2010EPA 8260BBenzene 0.5010B0809 1ND




2/21/20102/21/2010EPA 8260BBromoform 1.010B0809 1ND

2/21/20102/21/2010EPA 8260BBromomethane 1.010B0809 1ND

2/21/20102/21/2010EPA 8260B2-Butanone (MEK) 2.510B0809 1ND







2/21/20102/21/2010EPA 8260BChloroethane 1.010B0809 1ND


2/21/20102/21/2010EPA 8260BChloromethane 1.010B0809 1ND




2/21/20102/21/2010EPA 8260B1,2-Dibromo-3-chloropropane 2.510B0809 1ND



















2/21/20102/21/2010EPA 8260BHexachlorobutadiene 1.010B0809 1ND

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-05 (IRZ-MW-C-2102010 - Water) - cont.


2/21/20102/21/2010EPA 8260B2-Hexanone 2.510B0809 1ND

2/21/20102/21/2010EPA 8260BIodomethane 2.510B0809 1ND



2/21/20102/21/2010EPA 8260BMethylene Chloride 1.010B0809 1ND

2/21/20102/21/2010EPA 8260B4-Methyl-2-pentanone (MIBK) 2.510B0809 1ND


2/21/20102/21/2010EPA 8260BNaphthalene 2.510B0809 1ND


2/21/20102/21/2010EPA 8260BStyrene 0.5010B0809 1ND




2/21/20102/21/2010EPA 8260BToluene 0.5010B0809 1ND

2/21/20102/21/2010EPA 8260B1,2,3-Trichlorobenzene 1.010B0809 1ND





2/21/20102/21/2010EPA 8260B1,2,3-Trichloropropane 1.010B0809 1ND





2/21/20102/21/2010EPA 8260BXylenes, Total 1.010B0809 1ND




Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-05RE1 (IRZ-MW-C-2102010 - Water) - cont.






Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-07 (Trip Blank - Water)


2/21/20102/21/2010EPA 8260BAcetone 1010B0809 1ND

2/21/20102/21/2010EPA 8260BBenzene 0.5010B0809 1ND







































Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-07 (Trip Blank - Water) - cont.











2/21/20102/21/2010EPA 8260BStyrene 0.5010B0809 1ND




2/21/20102/21/2010EPA 8260BToluene 0.5010B0809 1ND















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-07RE1 (Trip Blank - Water) - cont.






Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-08 (IRZ-MW-C-2102010R - Water)


2/22/20102/22/2010EPA 8260BAcetone 1010B0821 1ND

2/22/20102/22/2010EPA 8260BBenzene 0.5010B0821 1ND



Bromodichloromethane 2/22/20102/22/201010B0821 0.50 1EPA 8260B 4.0











Chloroform 2/22/20102/22/201010B0821 0.50 1EPA 8260B 5.3




Dibromochloromethane 2/22/20102/22/201010B0821 0.50 1EPA 8260B 2.4





















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-08 (IRZ-MW-C-2102010R - Water) - cont.











2/22/20102/22/2010EPA 8260BStyrene 0.5010B0821 1ND




2/22/20102/22/2010EPA 8260BToluene 0.5010B0821 1ND
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0691-01 (IRZ-MW-B-2102010 - Water)


Iron 2/12/20102/11/201010B0466 50 1000E200.7 4000

Manganese 2/12/20102/11/201010B0466 0.010 1E200.7 9.7

Sodium 2/12/20102/11/201010B0466 2.0 1E200.7 390



Iron 2/12/20102/11/201010B0466 50 1000E200.7 6900

Manganese 2/12/20102/11/201010B0466 10 1000E200.7 32

Sodium 2/12/20102/11/201010B0466 2.0 1E200.7 460



Iron 2/12/20102/11/201010B0466 0.050 1E200.7 30

Manganese 2/12/20102/11/201010B0466 0.010 1E200.7 0.058

Sodium 2/12/20102/11/201010B0466 2.0 1E200.7 460

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

DISSOLVED METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 2/15/20102/12/201010B0515 0.050 1E200.7 150



Iron 2/16/20102/12/201010B0515 50 1000E200.7 4200



2/16/20102/12/2010E200.7Iron 0.05010B0515 1ND

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



2/17/20102/17/2010EPA 314.0Perchlorate 2.010B0670 1ND



2/17/20102/17/2010EPA 314.0Perchlorate 4.010B0670 D12ND



Perchlorate 2/17/20102/17/201010B0670 4.0 2EPA 314.0 10

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



2/18/20102/18/2010EPA 300.1Chlorate 10010B2243 D15ND

2/18/20102/18/2010EPA 300.1Chlorite 10010B2243 D15ND




Chlorate 2/18/20102/18/201010B2243 20 1EPA 300.1 22





Chlorate 2/19/20102/18/201010B2243 40 2EPA 300.1 86



Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 02/21/2010 (10B0809-BS1)

Acetone 25.0 10-150ug/l1022.1 89

Benzene 25.0 80-120ug/l0.5024.2 97




Bromoform 25.0 75-130ug/l1.021.8 87


2-Butanone (MEK) 25.0 40-150ug/l2.524.0 96








Chloroform 25.0 75-120ug/l0.5022.6 90




















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 02/21/2010 (10B0809-BS1)






2-Hexanone 25.0 20-150ug/l2.524.4 98

Iodomethane 25.0 80-130ug/l2.522.1 89






Naphthalene 25.0 40-150ug/l2.524.0 96


Styrene 25.0 80-120ug/l0.5023.7 95




Toluene 25.0 80-120ug/l0.5022.6 91
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1027.1 109 20

Benzene 25.0 1580-120ug/l0.5023.6 94 2




Bromoform 25.0 2075-130ug/l1.024.6 98 12


2-Butanone (MEK) 25.0 3540-150ug/l2.527.1 108 12

n-Butylbenzene 25.0 1580-130ug/l0.5025.9 104 0.8







Chloroform 25.0 1575-120ug/l0.5023.4 94 3







Dibromomethane 25.0 1575-120ug/l0.5024.5 98 0.8













Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3520-150ug/l2.527.4 110 12

Iodomethane 25.0 1080-130ug/l2.522.5 90 2






Naphthalene 25.0 3040-150ug/l2.525.5 102 6


Styrene 25.0 1580-120ug/l0.5023.7 95 0.08




Toluene 25.0 1580-120ug/l0.5022.6 90 0.2











Vinyl chloride 25.0 2070-130ug/l0.5021.5 86 0.4





Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Analyzed: 02/21/2010 (10B0809-MS1) Source: PTB0691-05

Acetone 25.0 10-150ug/l1021.6 ND 87

Benzene 25.0 70-125ug/l0.5023.9 ND 95




Bromoform 25.0 65-125ug/l1.024.8 ND 99










Chloroform 25.0 70-130ug/l0.5021.5 0.190 85




















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.526.5 ND 106









Styrene 25.0 55-135ug/l0.5021.1 ND 84




Toluene 25.0 70-125ug/l0.5023.3 0.170 92





Trichloroethene 25.0 70-125ug/l0.50490 N1, M3453 147











Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


Matrix Spike Dup Analyzed: 02/21/2010 (10B0809-MSD1) Source: PTB0691-05

Acetone 25.0 3510-150ug/l1021.2 ND 85 2

Benzene 25.0 2570-125ug/l0.5022.7 ND 91 5




Bromoform 25.0 2565-125ug/l1.023.3 ND 93 6


2-Butanone (MEK) 25.0 3015-150ug/l2.524.7 ND 99 0.2








Chloroform 25.0 2070-130ug/l0.5021.0 0.190 83 2




















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3020-150ug/l2.524.0 ND 96 10









Styrene 25.0 3555-135ug/l0.5019.8 ND 79 7




Toluene 25.0 2070-125ug/l0.5022.1 0.170 88 5



1,1,1-Trichloroethane 25.0 2570-130ug/l0.5021.2 ND 85 0.9


Trichloroethene 25.0 2570-125ug/l0.50452 N1, M3453 -2 8











Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 02/22/2010 (10B0821-BS1)

Acetone 25.0 10-150ug/l1022.3 89

Benzene 25.0 80-120ug/l0.5023.8 95




Bromoform 25.0 75-130ug/l1.022.9 92


2-Butanone (MEK) 25.0 40-150ug/l2.524.7 99








Chloroform 25.0 75-120ug/l0.5021.1 84




















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 02/22/2010 (10B0821-BS1)






2-Hexanone 25.0 20-150ug/l2.523.3 93

Iodomethane 25.0 80-130ug/l2.522.3 89






Naphthalene 25.0 40-150ug/l2.523.2 93


Styrene 25.0 80-120ug/l0.5023.7 95




Toluene 25.0 80-120ug/l0.5023.6 94
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1019.9 80 11

Benzene 25.0 1580-120ug/l0.5023.2 93 3

Bromobenzene 25.0 1580-120ug/l0.5025.4 102 0.1



Bromoform 25.0 2075-130ug/l1.022.2 89 3


2-Butanone (MEK) 25.0 3540-150ug/l2.521.5 86 14








Chloroform 25.0 1575-120ug/l0.5021.0 84 0.7




















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3520-150ug/l2.522.7 91 3

Iodomethane 25.0 1080-130ug/l2.521.8 87 2






Naphthalene 25.0 3040-150ug/l2.523.0 92 0.9


Styrene 25.0 1580-120ug/l0.5023.2 93 2




Toluene 25.0 1580-120ug/l0.5022.4 90 5
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1027.1 ND 108

Benzene 25.0 70-125ug/l0.5024.9 ND 99




Bromoform 25.0 65-125ug/l1.024.0 ND 96










Chloroform 25.0 70-130ug/l0.5025.6 0.290 101




















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.525.2 ND 101









Styrene 25.0 55-135ug/l0.5021.8 ND 87




Toluene 25.0 70-125ug/l0.5024.3 0.540 95





Trichloroethene 25.0 70-125ug/l0.50740 M2, M3728 47











Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1026.8 ND 107 0.9

Benzene 25.0 2570-125ug/l0.5026.6 ND 106 7




Bromoform 25.0 2565-125ug/l1.023.4 ND 93 3










Chloroform 25.0 2070-130ug/l0.5026.8 0.290 106 5




















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3020-150ug/l2.527.1 ND 108 7









Styrene 25.0 3555-135ug/l0.5023.3 ND 93 7




Toluene 25.0 2070-125ug/l0.5027.3 0.540 107 12





Trichloroethene 25.0 2570-125ug/l0.50757 M3728 115 2











Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers







LCS Analyzed: 02/22/2010 (10B0834-BS1)




















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 02/23/2010 (10B0865-BS1)

Acetone 25.0 10-150ug/l1018.5 74

Benzene 25.0 80-120ug/l0.5023.0 92




Bromoform 25.0 75-130ug/l1.021.4 85


2-Butanone (MEK) 25.0 40-150ug/l2.519.5 78








Chloroform 25.0 75-120ug/l0.5019.7 79




















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 02/23/2010 (10B0865-BS1)






2-Hexanone 25.0 20-150ug/l2.520.2 81

Iodomethane 25.0 80-130ug/l2.523.1 92






Naphthalene 25.0 40-150ug/l2.522.6 90


Styrene 25.0 80-120ug/l0.5023.8 95




Toluene 25.0 80-120ug/l0.5023.9 96
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1018.4 74 0.6

Benzene 25.0 1580-120ug/l0.5023.5 94 2




Bromoform 25.0 2075-130ug/l1.022.1 88 3


2-Butanone (MEK) 25.0 3540-150ug/l2.519.5 78 0.2

n-Butylbenzene 25.0 1580-130ug/l0.5023.3 93 0.04




Carbon tetrachloride 25.0 2075-130ug/l0.5024.0 96 0.7



Chloroform 25.0 1575-120ug/l0.5019.1 76 3














1,1-Dichloroethene 25.0 2075-125ug/l0.5021.8 87 0.1






Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



1,1-Dichloropropene 25.0 1575-120ug/l0.5023.6 94 0.6





2-Hexanone 25.0 3520-150ug/l2.520.3 81 0.6

Iodomethane 25.0 1080-130ug/l2.522.7 91 2




4-Methyl-2-pentanone (MIBK) 25.0 2560-135ug/l2.521.9 88 0.5


Naphthalene 25.0 3040-150ug/l2.524.4 98 8


Styrene 25.0 1580-120ug/l0.5022.9 92 4




Toluene 25.0 1580-120ug/l0.5023.4 94 2
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1051.0 26.1 99

Benzene 25.0 70-125ug/l0.5023.7 ND 95




Bromoform 25.0 65-125ug/l1.023.4 ND 94


2-Butanone (MEK) 25.0 15-150ug/l2.539.6 14.8 99






Chlorobenzene 25.0 75-120ug/l0.5025.1 2.03 92


Chloroform 25.0 70-130ug/l0.5026.7 6.35 81










1,4-Dichlorobenzene 25.0 70-125ug/l0.5025.7 1.20 98










Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 20-150ug/l2.524.2 ND 97









Styrene 25.0 55-135ug/l0.5022.8 0.410 89




Toluene 25.0 70-125ug/l0.5027.4 5.16 89
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1045.7 26.1 78 11

Benzene 25.0 2570-125ug/l0.5024.9 ND 100 5




Bromoform 25.0 2565-125ug/l1.024.4 ND 98 4


2-Butanone (MEK) 25.0 3015-150ug/l2.538.4 14.8 94 3






Chlorobenzene 25.0 2075-120ug/l0.5029.5 2.03 110 16


Chloroform 25.0 2070-130ug/l0.5029.1 6.35 91 9










1,4-Dichlorobenzene 25.0 2070-125ug/l0.5028.4 1.20 109 10










Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3020-150ug/l2.524.6 ND 99 2









Styrene 25.0 3555-135ug/l0.5026.0 0.410 102 13




Toluene 25.0 2070-125ug/l0.5029.9 5.16 99 9
















Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Iron mg/l0.050ND


Sodium mg/l2.0ND

LCS Analyzed: 02/12/2010 (10B0466-BS1)

Iron 1.00 85-115mg/l0.0500.964 96

Manganese 1.00 85-115mg/l0.0101.00 100

Sodium 20.0 85-115mg/l2.019.8 99


Iron 1.00 2085-115mg/l0.0500.962 96 0.2

Manganese 1.00 2085-115mg/l0.0100.997 100 0.7

Sodium 20.0 2085-115mg/l2.020.3 101 2


Iron 1.00 75-125mg/l0.0500.971 ND 97

Manganese 1.00 75-125mg/l0.0100.989 ND 99

Sodium 20.0 75-125mg/l2.0381 361 104


Iron 1.00 75-125mg/l0.0500.953 ND 95

Manganese 1.00 75-125mg/l0.0100.992 ND 99

Sodium 20.0 75-125mg/l2.025.2 5.50 98


Iron 1.00 1075-125mg/l0.0500.978 ND 98 0.7

Manganese 1.00 1075-125mg/l0.0100.993 ND 99 0.5

Sodium 20.0 1075-125mg/l2.0380 361 95 0.4

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

TOTAL METALS


Data

Qualifiers



Iron 1.00 1075-125mg/l0.0501.00 ND 100 5

Manganese 1.00 1075-125mg/l0.0101.01 ND 101 2

Sodium 20.0 1075-125mg/l2.025.8 5.50 101 2

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

DISSOLVED METALS


Data

Qualifiers



Iron mg/l0.050ND

LCS Analyzed: 02/15/2010 (10B0515-BS1)

Iron 1.00 85-115mg/l0.0501.01 101


Iron 1.00 2085-115mg/l0.0501.01 101 0.5


Iron 1.00 75-125mg/l0.0501.11 0.103 101


Iron 1.00 75-125mg/l0.0501.05 ND 105


Iron 1.00 1075-125mg/l0.0501.14 0.103 104 2


Iron 1.00 1075-125mg/l0.0501.06 ND 106 1

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte

INORGANICS


Data

Qualifiers




LCS Analyzed: 02/17/2010 (10B0670-BS1)

Perchlorate 25.0 85-115ug/l2.025.3 101


Perchlorate 25.0 1585-115ug/l2.024.3 97 4

Duplicate Analyzed: 02/17/2010 (10B0670-DUP1) Source: PTB0683-10


Duplicate Analyzed: 02/17/2010 (10B0670-DUP2) Source: PTB0691-01

Perchlorate 15ug/l2.01.79 R91.52 17


Perchlorate 25.0 80-120ug/l2.022.0 2.07 80


Perchlorate 25.0 80-120ug/l2.025.0 ND 100


Perchlorate 25.0 1580-120ug/l2.022.3 2.07 81 2


Perchlorate 25.0 1580-120ug/l2.024.7 ND 99 1

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Chlorate ug/l20ND

Chlorite ug/l20ND


LCS Analyzed: 02/18/2010 (10B2243-BS1)

Chlorate 100 75-125ug/l2098.6 99

Chlorite 100 75-125ug/l2096.0 96


Matrix Spike Analyzed: 02/18/2010 (10B2243-MS1) Source: ITB1760-01

Chlorate 100 75-125ug/l4093.4 ND 93

Chlorite 100 75-125ug/l4093.4 ND 93


Matrix Spike Analyzed: 02/19/2010 (10B2243-MS2) Source: ITB1593-01

Chlorate 100 75-125ug/l20117 32.8 84

Chlorite 100 75-125ug/l2075.9 ND 76


Matrix Spike Dup Analyzed: 02/18/2010 (10B2243-MSD1) Source: ITB1760-01

Chlorate 100 2575-125ug/l4094.6 ND 95 1

Chlorite 100 2575-125ug/l4092.5 ND 93 1


Matrix Spike Dup Analyzed: 02/19/2010 (10B2243-MSD2) Source: ITB1593-01

Chlorate 100 2575-125ug/l20117 32.8 85 0.3

Chlorite 100 2575-125ug/l2078.9 ND 79 4


Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00







Q3 Sample received with improper chemical preservation.




Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily




454-9303





Sampled:

Received:

02/10/10


Project ID:

PTB0691

PGA North/103965.00



TestAmerica Phoenix

Water XE200.7

Water XEPA 314.0

XWater XEPA 8260B






Analysis Performed: HydrogenSamples: PTB0691-01, PTB0691-03, PTB0691-05



Method Performed: EPA 300.1Samples: PTB0691-01, PTB0691-03, PTB0691-05

Project Manager

TestAmerica Phoenix

PTB0691

Kylie Emily



SENDING .LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 1 69 Phoenix, AZ B5040 Phone: (602) 437-3340

Fax: (602) 454-9303 Project Manager: Kylie Emily

SUBCONTRACT OR.DER TestAmerica Phoenix

PTB0691


TestAmerica Irvine

17461 Derian Ave. Suite 100 Irvine, CA 92614 Phone:(949)261-1022

Fax: (949) 261-1226 Project Location: AZ -ARIZONA

Client: Environmental Resources Management: Inc.-West: "Receipt Temperature: ·: . : · oc . ··. . Ice: -.Y N::-···

Analysis Units Due Expires .lnterlab Price Surch. Comments

. sim1ple 10: PTB0691-t»1 (IRZ-MW-B-2102010- Water) Sampled: 02/10/10 09:52

Chlorate (300.1) ·mg/1 02/25/10 03/10/10 09:52 $30.00 0%

Chlorite (300.1)- 0 _mg/1· 02125/10 02124/10 09:52 $30.00 . 0%


500 ml Poly w/EDA (F) 1,25ml Brown Poly w/ .EDA (G)

Sample ID: PTB0691-t»3 (IRZ-IW-5-2102010- Water) Sampled: 02110110 12:49 ·

Chlorate (300.1) mg/1 02125/10 03/10/10 12:49 $30.00 0%

Chlorite (300.1)- 0 mg/1 02125/10 02124/10 12:49 $30.00 0%


500 ml poly w/EDA (F) 125ml Brown Poly w/ EDA G

Sample ID: PTB0691-05 (IRZ-MW-C-2102010- Water) Sampled: 0211011015:37 Chlorate (300.1) mg/1 02125/10 03/10/10 15:37 $30.00 o% Chlorite (300.1) - 0 mg/1 02125/10 02124/10 15:37 $30.00 0%


. 500 ml Poly w/EDA (F). 125ml Brown Poly w/ EDA (G)

.\f[ J- f\ -t, I I 0

10 0

-~-..~~_D_l-_-_/1_--_ID __ if ·00

Released By Datemme

Re:~d:? . , ~mme ' d( ./ ~ &

\~~ ~)~ t/~o.r/ --R~ece.&-iv_e_d"-B-f.y~-"-"-"'-------':...:;.... Datemme Page 1 of 1

Relea!:Jed By

TestAmerica THE LEADER IN ENVIRONMENTAL TESTING

TAL-0013-550 (12/08)


[ ] Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ ] Tucson- 1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ ] Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621

P/LfAmi'~l_~Lf?L ~~S~oLLf ~ojectl PO Num~ · Analysis Required CtJA--tvw-' .

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Proj~t Mtag~ Phone Number: ~ Q....\1 ~a

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d. ~ct dt -£' Sample Description Preservatives ~ cs:.-Matrix Type Cont. Date Time

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<]_ 1-' of\ l (., ~ .41 \f,~l Relin/1h~~v Date/7,e: Received By: Date/Time: Turnaround Time:

2-to-Lo l7:lf3 .c.h same day

Reli,1'uished By: Date/time: 7~ved By: Date/Time: 24 hours

I 48 hours

Relinquished By: Date/Time: (_ ~Lab By: :2--~o ,.ate/Time: Sample Integrity:

{l> 1~6 intact >c

Page l of 'Z.....

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(Check)

72 hours

5 days

normal

(Check) 8"""""' on ice I'C o.

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days irom the date of invoice. Sample(s) will be disposed of after 30 days.

.,


TAL-0013·550 (12/08)

Client Name/Address:

SeL p QJ-e.- 'L Project Manager:

Sampler: '~--'


~2-N\w -C ~L!O£..D~o \-\~ V{)A--\)o ty ~p\'y

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[ I Phoenix~ 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602) 437-3340 FAX (602) 454-9303 [ 1 Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ I Las Vegas - 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621


:L <U

~p(j.__~ ~

i-./6 ·s

~ (,)"2 jt~ Phone Number:

~t_ t \L/ ~ _j ~ -lr

Fax Number: ?, ~ f 1~ ..j =6 0 3 ~ + ~ C)t

~ __. 9. ~

#of Sampling Sampling Preservatives ~ ~ {J t~ 6t

,_. Cont. Date Time :::::t

3 l:i'D'ID rs:·s+ \!-cL (G -:}__ "I Q. ~ I El)(\ ~

co().. )(" )t{'Ji)3 <' \J- (\J-€>]

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Received By: Date/Time: Turnaround Time: R/As~ Date/T7e: ·

2-JO-[D n:l.[:J ~ ~ same day

J~~finqoi€lhed By: Date/time: l/i::7By:

Date/Time: 24 hours

48 hours

Relinquished By: Date/Time: (_ ~~By: ~?te!Tz: Sample Integrity:

- .:J... /1> tO /~3 intact lr.

Page '2- of ~

?fEO~ot \


·- DS""

-es--es

- os-~os

·,_€)lJ2

-os

-0-:J-

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(Check)

72 hours

5 days

normal

(Check) {)_ 8- ~

on ice _..f..--

Note: By relinquishing samples to TestAmerica, client agrees to pay for the se~vices re~ested on this chain of custody fo--:m and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

r-.



Report Date: 02/26/1 o Client Proj Name: PTB0691

Client Proj #: PTB0691

Lab Sample#

?1002145-01

P1 002145-02

P1 002145-03


Client Sample ID

PTB0691-01

PTB0691-03

PTBD691-05

Laboratory Results Total pages in data package: __ (p-=---

Microseeps test results meet all the requirements of the NElAC standards or provide reasons and/or justification If they do not.

Approved Bv: 6J ·fXr;·IO




Case Narrative:

As a valued client we would appreciate your comments on our service. Please cafl customer service at (412)826-5245 or email [email protected].

220 William Pitt Way • Pittsburgh, PA 15238 • Tel 412-826-5245. Fax 412-826-3433



Address: 4625 East Cotton Center Blvd. Suite 189 Phoenix, Al. 85040

Sam(;!le Descrigtion Matrix Lab Sample#


Report Date: 02/26/1 0 Client Proj Name: PTB0691


SamQied Date/Time Received PTB0691-01 Vapor P1 002145-01 10 Feb. 10 9:52 12 Feb. 10 12:41

Analyte(s) Flag Result PQL Units Method# Analysis Date

RiskAnalysis N Hydrogen 38000.000 1200.0001M AM20GAX 2/22/10

Data Qualifiers: J -estimated value, U -Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B - detected in blank, S -field sample as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N - NELAC certified analysis

By

sl

Client Name: Test America Contact: Kylie Emily Apdress: 4625 East Cotton Center Blvd.





. Client Proj #: PTB0691

Sam~led Date/Time Received PTB0691~03 Vapor P1 002145-02 10 Feb. 10 12:49 12 Feb. 10 12:41


Data Qualifiers: J - estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B -detected in blank, S -field san1ple as received did not meet NELAC sample acceptance criteria, L- Subcontracted Lab used, N- NELAC certified analysis

By

sl



Samgle Descri(2tion Matrix Lab Sample#




Samgled Daterrime Received PTB0691-05 Vapor P1002145-03 10 Feb. 10 15:37 12 Feb. 10 12:41

Analyte(s) Ftae Result PQL Units -Method# Analysis Date

RiskAnalysls N Hydrogen 30.000 1.200 nM AM20GAX 2/22/10

Data Qualifiers: J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B- detected in blank, S • field sample as received did not meet NELAC sample acceptance criteria, L - Subcontracted Lab used, N - NELAC certified analysis

By

sl



Prep Method:

Analysis Method:

M 1 00222036~MB



M 1 00222036~LCS



M 1 00222036~LCSD









~ NA


101.00 75- 125


102.00 75- 125 1.01

RPD Ctl Limits

0-20

'-----___jl Outlined Results indicate results outside of Control limits

Data Qualifiers: J- estimated value, U- Non detect, R- Poor surrogate recovery, M- Recovery/RPD poor for MS/MSD, SAMP/DUP, B- detected in blank, S -field sample !IS received did not meet NELAC sample acceptance criteria, L- Subcontrncted Lab used, N - NELAC certified analysis

SENDING LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 189 Phoenix, AZ 85040 Phone: (602) 437-3340

Fax: (602) 454-9303 Project Manager: Kylie Emily


PTB0691



220 William Pitt Way Pittsburgh, PA 15238 Phone :(412)826-5245 Fax: (412)826-3433 Project Location: AZ- ARIZONA Receipt Temperature: °C Ice: Y I N

Standard TAT is requested unless specific due date is requested. ==> Due Date: ---- Initials: ___ _

Analysis Units

Sample 10: PT80691-01 (JRZ-MW-B-2102010- Water)

Hydrogen

Containers Supplied:·

NA (H)

%

Sample ID: PTB0691-03 (IRZ-IW·5·2102010 ·Water)

Hydrogen


NA (H)

%

Sample ID: PTB0691-05 (IRZ-MW-C-2102010 ·Water)

Hydrogen


NA (H)

Released By

Released By

%

Datemme

Expires Comments

Sampled: 02110110 09:52 03/10/10 09:52 Microseeps

Sampled: 02110/10 12:49 03/10/1 0 12:49 Mlcroseeps

Samgled: 02110/10 15:37 03/1 0/1 0 15:37 Microseeps

r:eJ?(,f:' o z.-1 ;.., ro l1: ~ Redeived 8'/---..._~ ~e

Rece~ Datemme Page 1 of 1


454-9303

LABORATORY REPORT





Received:

Issued:

02/11/10

02/11/10

03/01/10 08:46









CASE NARRATIVE


PTB0794-01 IRZ-MW-D-2112010 Water

PTB0794-02 IRZ-MW-D-2112010 Water

PTB0794-03 IRZ-MW-D-2112010-R Water


PTB0794-05 IRZ-IW-4-2112010 Water

PTB0794-06 IRZ-IW-4-2112010 Water

PTB0794-07 IRZ-IW-3-2112010 Water

PTB0794-08 IRZ-IW-3-2112010 Water

PTB0794-09 IRZ-IW-3-2112010-D Water

PTB0794-10 IRZ-IW-2-2112010 Water

PTB0794-11 IRZ-IW-1-2112010 Water

PTB0794-12 IRZ-IW-1-2112010 Water


Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily

<Page 1 of 55>


454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00








Reviewed By:

Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0794-01 (IRZ-MW-D-2112010 - Water)


2/22/20102/22/2010EPA 8260BAcetone 1010B0821 1ND

2/22/20102/22/2010EPA 8260BBenzene 0.5010B0821 1ND




























1,1-Dichloroethene 2/22/20102/22/201010B0821 0.50 1EPA 8260B 0.96











Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0794-01 (IRZ-MW-D-2112010 - Water) - cont.











2/22/20102/22/2010EPA 8260BStyrene 0.5010B0821 1ND




Toluene 2/22/20102/22/201010B0821 0.50 1EPA 8260B 0.54















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0794-01RE1 (IRZ-MW-D-2112010 - Water) - cont.






Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0794-03 (IRZ-MW-D-2112010-R - Water)


Acetone 2/22/20102/22/201010B0821 10 1EPA 8260B 12

2/22/20102/22/2010EPA 8260BBenzene 0.5010B0821 1ND


















Dibromochloromethane 2/22/20102/22/201010B0821 0.50 1EPA 8260B 3.0





















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0794-03 (IRZ-MW-D-2112010-R - Water) - cont.











2/22/20102/22/2010EPA 8260BStyrene 0.5010B0821 1ND




2/22/20102/22/2010EPA 8260BToluene 0.5010B0821 1ND















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0794-03RE1 (IRZ-MW-D-2112010-R - Water) - cont.






Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



2/22/20102/22/2010EPA 8260BAcetone 1010B0821 1ND

2/22/20102/22/2010EPA 8260BBenzene 0.5010B0821 1ND







































Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result












2/22/20102/22/2010EPA 8260BStyrene 0.5010B0821 1ND




2/22/20102/22/2010EPA 8260BToluene 0.5010B0821 1ND
















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



2/23/20102/23/2010EPA 8260BAcetone 10010B0865 10ND

2/23/20102/23/2010EPA 8260BBenzene 5.010B0865 10ND







































Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result












2/23/20102/23/2010EPA 8260BStyrene 5.010B0865 10ND




2/23/20102/23/2010EPA 8260BToluene 5.010B0865 10ND
















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



2/23/20102/23/2010EPA 8260BAcetone 100010B0865 100ND

2/23/20102/23/2010EPA 8260BBenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BBromobenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BBromochloromethane 5010B0865 100ND

2/23/20102/23/2010EPA 8260BBromodichloromethane 5010B0865 100ND




2/23/20102/23/2010EPA 8260Bn-Butylbenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Bsec-Butylbenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Btert-Butylbenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BCarbon disulfide 5010B0865 100ND

2/23/20102/23/2010EPA 8260BCarbon tetrachloride 5010B0865 100ND

2/23/20102/23/2010EPA 8260BChlorobenzene 5010B0865 100ND


2/23/20102/23/2010EPA 8260BChloroform 5010B0865 100ND


2/23/20102/23/2010EPA 8260B2-Chlorotoluene 5010B0865 100ND


2/23/20102/23/2010EPA 8260BDibromochloromethane 5010B0865 100ND


2/23/20102/23/2010EPA 8260B1,2-Dibromoethane (EDB) 5010B0865 100ND

2/23/20102/23/2010EPA 8260BDibromomethane 5010B0865 100ND

2/23/20102/23/2010EPA 8260B1,2-Dichlorobenzene 5010B0865 100ND



2/23/20102/23/2010EPA 8260BDichlorodifluoromethane 5010B0865 100ND

2/23/20102/23/2010EPA 8260B1,1-Dichloroethane 5010B0865 100ND


2/23/20102/23/2010EPA 8260B1,1-Dichloroethene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Bcis-1,2-Dichloroethene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Btrans-1,2-Dichloroethene 5010B0865 100ND




2/23/20102/23/2010EPA 8260B1,1-Dichloropropene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Bcis-1,3-Dichloropropene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Btrans-1,3-Dichloropropene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BEthylbenzene 5010B0865 100ND


Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result





2/23/20102/23/2010EPA 8260BIsopropylbenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Bp-Isopropyltoluene 5010B0865 100ND



2/23/20102/23/2010EPA 8260BMethyl-tert-butyl Ether (MTBE) 5010B0865 100ND


2/23/20102/23/2010EPA 8260Bn-Propylbenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BStyrene 5010B0865 100ND

2/23/20102/23/2010EPA 8260B1,1,1,2-Tetrachloroethane 5010B0865 100ND


2/23/20102/23/2010EPA 8260BTetrachloroethene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BToluene 5010B0865 100ND



2/23/20102/23/2010EPA 8260B1,1,1-Trichloroethane 5010B0865 100ND


Trichloroethene 2/23/20102/23/201010B0865 50 100EPA 8260B 3600

2/23/20102/23/2010EPA 8260BTrichlorofluoromethane 5010B0865 100ND


2/23/20102/23/2010EPA 8260B1,2,4-Trimethylbenzene 5010B0865 100ND


2/23/20102/23/2010EPA 8260BVinyl Acetate 5010B0865 100ND

2/23/20102/23/2010EPA 8260BVinyl chloride 5010B0865 100ND





Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0794-09 (IRZ-IW-3-2112010-D - Water)


2/23/20102/23/2010EPA 8260BAcetone 100010B0865 100ND

2/23/20102/23/2010EPA 8260BBenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BBromobenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BBromochloromethane 5010B0865 100ND

2/23/20102/23/2010EPA 8260BBromodichloromethane 5010B0865 100ND




2/23/20102/23/2010EPA 8260Bn-Butylbenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Bsec-Butylbenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Btert-Butylbenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BCarbon disulfide 5010B0865 100ND

2/23/20102/23/2010EPA 8260BCarbon tetrachloride 5010B0865 100ND

2/23/20102/23/2010EPA 8260BChlorobenzene 5010B0865 100ND


2/23/20102/23/2010EPA 8260BChloroform 5010B0865 100ND




2/23/20102/23/2010EPA 8260BDibromochloromethane 5010B0865 100ND


2/23/20102/23/2010EPA 8260B1,2-Dibromoethane (EDB) 5010B0865 100ND

2/23/20102/23/2010EPA 8260BDibromomethane 5010B0865 100ND




2/23/20102/23/2010EPA 8260BDichlorodifluoromethane 5010B0865 100ND



2/23/20102/23/2010EPA 8260B1,1-Dichloroethene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Bcis-1,2-Dichloroethene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Btrans-1,2-Dichloroethene 5010B0865 100ND




2/23/20102/23/2010EPA 8260B1,1-Dichloropropene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Bcis-1,3-Dichloropropene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Btrans-1,3-Dichloropropene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BEthylbenzene 5010B0865 100ND


Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0794-09 (IRZ-IW-3-2112010-D - Water) - cont.




2/23/20102/23/2010EPA 8260BIsopropylbenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260Bp-Isopropyltoluene 5010B0865 100ND



2/23/20102/23/2010EPA 8260BMethyl-tert-butyl Ether (MTBE) 5010B0865 100ND


2/23/20102/23/2010EPA 8260Bn-Propylbenzene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BStyrene 5010B0865 100ND



2/23/20102/23/2010EPA 8260BTetrachloroethene 5010B0865 100ND

2/23/20102/23/2010EPA 8260BToluene 5010B0865 100ND






2/23/20102/23/2010EPA 8260BTrichlorofluoromethane 5010B0865 100ND




2/23/20102/23/2010EPA 8260BVinyl Acetate 5010B0865 100ND

2/23/20102/23/2010EPA 8260BVinyl chloride 5010B0865 100ND





Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



Acetone 2/22/20102/22/201010B0821 10 1EPA 8260B 57

Benzene 2/22/20102/22/201010B0821 0.50 1EPA 8260B 0.72






2-Butanone (MEK) 2/22/20102/22/201010B0821 2.5 1EPA 8260B 9.4






Chlorobenzene 2/22/20102/22/201010B0821 0.50 1EPA 8260B 2.0



























Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result







Methylene Chloride 2/22/20102/22/201010B0821 1.0 1EPA 8260B 1.8





2/22/20102/22/2010EPA 8260BStyrene 0.5010B0821 1ND




Toluene 2/22/20102/22/201010B0821 0.50 1EPA 8260B 1.8
















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



2/22/20102/22/2010EPA 8260BAcetone 1010B0821 1ND

Benzene 2/22/20102/22/201010B0821 0.50 1EPA 8260B 0.82







































Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result












2/22/20102/22/2010EPA 8260BStyrene 0.5010B0821 1ND



Tetrachloroethene 2/22/20102/22/201010B0821 0.50 1EPA 8260B 1.9

2/22/20102/22/2010EPA 8260BToluene 0.5010B0821 1ND















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PTB0794-11RE1 (IRZ-IW-1-2112010 - Water) - cont.






Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



2/22/20102/22/2010EPA 8260BAcetone 1010B0821 1ND

2/22/20102/22/2010EPA 8260BBenzene 0.5010B0821 1ND







































Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result












2/22/20102/22/2010EPA 8260BStyrene 0.5010B0821 1ND




2/22/20102/22/2010EPA 8260BToluene 0.5010B0821 1ND
















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

TOTAL METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



Iron 2/15/20102/12/201010B0511 0.050 1E200.7 2.8

Manganese 2/15/20102/12/201010B0511 0.010 1E200.7 0.031

Sodium 2/15/20102/12/201010B0511 2.0 1E200.7 480



Iron 2/15/20102/12/201010B0511 50 1000E200.7 6200

Manganese 2/15/20102/12/201010B0511 10 1000E200.7 25

Sodium 2/16/20102/12/201010B0511 200 100E200.7 1300



Iron 2/15/20102/12/201010B0511 5.0 100E200.7 910

Manganese 2/15/20102/12/201010B0511 1.0 100E200.7 9.5

Sodium 2/15/20102/12/201010B0511 200 100E200.7 470



Iron 2/15/20102/12/201010B0511 0.050 1E200.7 79

Manganese 2/15/20102/12/201010B0511 0.010 1E200.7 0.22

Sodium 2/16/20102/12/201010B0511 200 100E200.7 1900



Iron 2/15/20102/12/201010B0511 0.050 1E200.7 0.15

Manganese 2/15/20102/12/201010B0511 0.010 1E200.7 0.018

Sodium 2/15/20102/12/201010B0511 2.0 1E200.7 450

Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

DISSOLVED METALS

Data

QualifiersBatch

Reporting

Limit

Sample

Result



2/15/20102/12/2010E200.7Iron 0.05010B0515 1ND



Iron 2/15/20102/12/201010B0515 50 1000E200.7 2100



Iron 2/15/20102/12/201010B0515 0.050 1E200.7 100



2/15/20102/12/2010E200.7Iron 0.05010B0515 1ND

Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

INORGANICS

Data

QualifiersBatch

Reporting

Limit

Sample

Result










Sample ID: PTB0794-09 (IRZ-IW-3-2112010-D - Water)





2/19/20102/19/2010EPA 314.0Perchlorate 4.010B0741 D12ND




Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor


Data

QualifiersBatch

Reporting

Limit

Sample

Result



Chlorate 2/19/20102/18/201010B2243 40 2EPA 300.1 89










Chlorate 2/19/20102/18/201010B2243 40 2EPA 300.1 84











Chlorite 2/19/20102/18/201010B2243 400 20EPA 300.1 930


Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone ug/l10ND

Benzene ug/l0.50ND




Bromoform ug/l1.0ND






























Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers

















Styrene ug/l0.50ND




Toluene ug/l0.50ND
















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 02/22/2010 (10B0821-BS1)

Acetone 25.0 10-150ug/l1022.3 89

Benzene 25.0 80-120ug/l0.5023.8 95




Bromoform 25.0 75-130ug/l1.022.9 92


2-Butanone (MEK) 25.0 40-150ug/l2.524.7 99








Chloroform 25.0 75-120ug/l0.5021.1 84




















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers


LCS Analyzed: 02/22/2010 (10B0821-BS1)






2-Hexanone 25.0 20-150ug/l2.523.3 93

Iodomethane 25.0 80-130ug/l2.522.3 89






Naphthalene 25.0 40-150ug/l2.523.2 93


Styrene 25.0 80-120ug/l0.5023.7 95




Toluene 25.0 80-120ug/l0.5023.6 94
















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 3510-150ug/l1019.9 80 11

Benzene 25.0 1580-120ug/l0.5023.2 93 3

Bromobenzene 25.0 1580-120ug/l0.5025.4 102 0.1



Bromoform 25.0 2075-130ug/l1.022.2 89 3


2-Butanone (MEK) 25.0 3540-150ug/l2.521.5 86 14








Chloroform 25.0 1575-120ug/l0.5021.0 84 0.7




















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers








2-Hexanone 25.0 3520-150ug/l2.522.7 91 3

Iodomethane 25.0 1080-130ug/l2.521.8 87 2






Naphthalene 25.0 3040-150ug/l2.523.0 92 0.9


Styrene 25.0 1580-120ug/l0.5023.2 93 2




Toluene 25.0 1580-120ug/l0.5022.4 90 5
















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily




454-9303





Sampled:

Received:

02/11/10


Project ID:

PTB0794

PGA North/103965.00

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Analyte



Data

Qualifiers



Acetone 25.0 10-150ug/l1027.1 ND 108

Benzene 25.0 70-125ug/l0.5024.9 ND 99




Bromoform 25.0 65-125ug/l1.024.0 ND 96










Chloroform 25.0 70-130ug/l0.5025.6 0.290 101




















Project Manager

TestAmerica Phoenix

PTB0794

Kylie Emily



DRAFT PHASE III NANO- SCALE ZERO-VALENT IRON PILOT TEST … · 2020. 11. 17. · i EXECUTIVE...

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Transcript of DRAFT PHASE III NANO- SCALE ZERO-VALENT IRON PILOT TEST … · 2020. 11. 17. · i EXECUTIVE...