Destilacion 2015 Final
-
Upload
andrez-valverde-armas -
Category
Documents
-
view
214 -
download
0
Transcript of Destilacion 2015 Final
-
8/18/2019 Destilacion 2015 Final
1/24
Datos de Destilación
t (min) T fondo (°C) T tope (°C) t (min)0 24.7 22.1 11.032 38.4 22.1 11.23
3 40.6 22.1 11.313.1 41.2 22.1 11.46
3.15 43.7 22.1 11.593.23 46.4 22.1 12.063.34 48.3 22.1 12.23.43 50 22.1 13.013.55 52 22.1 14.044.12 55 22.1 14.454.25 57 22.1 14.534.37 58.7 22.1 15.06
4.54 60.8 22.1 15.275.02 62.2 22.1 15.425.15 63.9 22.1 15.55.23 64.7 22.1 16.095.44 67.4 22.2 16.51
6 69.9 22.2 17.056.17 70.4 22.2 17.536.33 72 22.2 18.196.44 72.8 22.2 18.516.57 74 22.2 19.37.05 74.5 22.2 19.467.19 75.7 22.2 20.077.31 76.7 22.2 21.527.42 77.7 22.2 23.597.52 78.5 22.2 24.348.05 79.6 22.2 26.128.16 82 22.2 27.158.27 84.2 22.2 28.258.44 86.6 22.2 29.18.57 87.3 22.2 32.599.16 88.9 22.2 38.11
9.41 90.4 22.2 40.299.57 91 22.3 42.11
10.17 91.7 22.3 47.0810.28 92.2 22.3 51.3
10.4 92.6 22.3 54.310.53 92.9 22.3 57
Al estado estacionaio!
-
8/18/2019 Destilacion 2015 Final
2/24
T fondo (°C) 97.1 T tope (°C) 78.3
MÉTODO DE PONCHON Y SAVARIT
75.1766
Cp C1 C2 CA"#a 75.1766 0.0018015 0.000018015$tanol 102.826 0.34091 0.00230345
Cp !ases C1 C2 CA"#a 32.24 0.001923 0.00001055
$tanol 19.9 0.2096 %0.0001038
Te"p#$C% T #$&% '()*ido #+% Vapo, #-%100 373.15 0 0 5130.34783938295.5 368.65 0.019 0.17 5307.925561748
89 362.15 0.0721 0.3891 6066.62437654586.7 359.85 0.0966 0.4375 6398.03651387785.3 358.45 0.1238 0.4704 6861.64933135684.1 357.25 0.1661 0.5089 7664.42268244482.7 355.85 0.2337 0.5445 8949.01048555282.3 355.45 0.2608 0.558 9471.8972828581.5 354.65 0.3273 0.5826 10755.2974461880.7 353.85 0.3965 0.6122 12050.1946124779.8 352.95 0.5079 0.6564 14150.3400560179.7 352.85 0.5198 0.6599 14368.4320174479.3 352.45 0.5732 0.6841 15350.42480532
78.74 351.89 0.6763 0.7385 17273.0938257478.41 351.56 0.7472 0.7815 18588.6719527278.15 351.3 0.8943 0.8943 21450.49251967
78.4 351.55 1 1 23708.131905
De la !,./caHD 0 Hlo #"ol% 20000H31 #"ol% 59000H4 #"ol% 5500
H'#"ol%
& (
& ((
,1/ .5 -1,
'
-
8/18/2019 Destilacion 2015 Final
3/24
H5 #"ol% 5000
Re6*7o total innito89 innito
, &1(_ −= & + + &
& . & '= & − & +
-
8/18/2019 Destilacion 2015 Final
4/24
-
8/18/2019 Destilacion 2015 Final
5/24
T fondo (°C) T tope (°C) #esta 193.3 22.3 esid#o 193.9 22.3 /estilado 1
94.2 22.394.5 22.3 #esta 294.6 22.3 esid#o 294.8 22.3 /estilado 294.8 49.195.1 80.3 #esta 395.2 79.6 esid#o 395.5 78.9 /estilado 395.5 78.895.5 78.7 #esta 4
95.5 78.6 esid#o 495.5 78.5 /estilado 495.6 78.595.7 78.495.7 78.3 A ("+mol)95.8 78.2 ("+mol)95.7 78.2 /ensidad A ("+ml)95.6 78.2 /ensidad ("+ml)95.6 78.295.6 78.295.6 78.2 esid#o95.6 78.1 /estilado95.6 78.1 Alimentacion95.5 78.1 MÉTODO DE MCCA:E95.5 78.1 (a)95.6 78.2 Temp(°C)95.7 78.2 10095.8 78.2 95.595.9 78.2 8995.9 78.2 86.796.2 78.2 85.3
96.4 78.2 84.196.5 78.2 82.796.6 78.3 82.396.9 78.2 81.5
97 78.2 80.797.1 78.3 79.8
79.779.3
-
8/18/2019 Destilacion 2015 Final
6/24
78.7478.4178.1578.4
H3 #"ol% ; a!*a #!%43972.76827462 ; etanol #!%50934.0035932754468.38466022
54842.45855955089.4709539855461.4954327855678.6409689455792.2368619155963.9730445956204.7507179556634.0075262856656.1403508156909.8981520857584.7711750758146.5748108859842.50621879
61659.175605
H sol*ción #"ol%
)) 1 '2 = +2+3 T(°) cp (*+mol.)
)) 1 '2 = +2+3 T(°) cp (*+mol.)
_,2.5/
-
8/18/2019 Destilacion 2015 Final
7/24
0.6
0.7
0.8
0.9
1
E
)_
. & +. & &
$=TA>?A
'
-
8/18/2019 Destilacion 2015 Final
8/24
0
0.1
0.2
0.3
0.4
0.5
-
8/18/2019 Destilacion 2015 Final
9/24
F5
92
F6
93.5
F5
93.5
F
593.5
46.06918.015
0.7955870.997770
=,acción Vol> +i0.0525 0.02
0.93125 0.810.1 0.03
HIE'E101.3
>G#ido (D) Hapo (E)0 0
0.019 0.170.0721 0.38910.0966 0.43750.1238 0.4704
0.1661 0.50890.2337 0.54450.2608 0.5580.3273 0.58260.3965 0.61220.5079 0.65640.5198 0.65990.5732 0.6841
E
FHi, acci:n en Hol#men del etanol.D, acci:n mola del etanol, eso molec#la ("+mol) (s#Indice epaa etanol s#Indice a paa el a"#a)Je,densidad del etanol a 22° C ("+ml).Ja, densidad del a"#a a 22 °C("+ml)
[
[ ] [e
ie
ie
M
V
V
x)(%
(%
+
=
ρ
ρ
-
8/18/2019 Destilacion 2015 Final
10/24
0.6763 0.73850.7472 0.78150.8943 0.8943
1 1
2299.02 ; a!*a #"ol% 41416.8453808.46 ; etanol #"ol% 37244.9437
%706.1
/ia"ama $n
MÉTODO DE PONC
-
8/18/2019 Destilacion 2015 Final
11/24
/@A-AA
0 0.1 0.2 0.3 0.40
10000
20000
30000
40000
50000
60000
70000
KL
Kf
MEZCLA ETA
7 ETAPAS T
?
<
3?
3<
'?
'@
-
8/18/2019 Destilacion 2015 Final
12/24
0.1 0.2 0.3 0.4
-
8/18/2019 Destilacion 2015 Final
13/24
0 0.1 0.2 0.3 0.40
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1
/@A-AA C
MÉTODO DE M
MEZCLA ETANOL - AGUA
7 ETAPAS TEÓRICAS
?
<
]
]a
ia
e
M
V
M
)%1(
)
−
-
8/18/2019 Destilacion 2015 Final
14/24
talpa s Composici:n
HON Y SAVARIT
-
8/18/2019 Destilacion 2015 Final
15/24
CB@C@= D s E
0.5 0.6 0.7 0.8
;<
K>o
K-
OL - AGUA
ÓRICAS
12
@
3132
333
@
'' '2
'1
-
8/18/2019 Destilacion 2015 Final
16/24
0.5 0.6 0.7 0.8
D
-
8/18/2019 Destilacion 2015 Final
17/24
0.5 0.6 0.7 0.8 0.9
B@C@= D s E
D
CCABE THIELE
12
@
-
8/18/2019 Destilacion 2015 Final
18/24
-
8/18/2019 Destilacion 2015 Final
19/24
0.9 1
1
-
8/18/2019 Destilacion 2015 Final
20/24
0.9 1
-
8/18/2019 Destilacion 2015 Final
21/24
1
-
8/18/2019 Destilacion 2015 Final
22/24
-
8/18/2019 Destilacion 2015 Final
23/24
-
8/18/2019 Destilacion 2015 Final
24/24