DEPARTMENT OF ENVIRONMENTAL SERVICES …. i - i i . state of new hampshire . enviroj!mentas ervices...

State of New Hampthire lt-STE MANAGEM ENT COUNCIL

DEPARTMENT OF ENVIRONMENTAL SERVICES G ILDIniiCKAaD5cshy-IT 111411lU n(shy

WASTE MANAGEMENT DIVISI ON

6 Haz en Drive Concord NH 03301-6509

603-271-2900

ROB~~~~~~EY TTYTD0 -800-992middot3312or225-4033

PHIUP JO~~~iN Ph D

MICHAELA SILLS Ph O bull PE ( lllUESGlS(U

March 26 1991

Ms Cheryl Sprague RPM NH Superfund Support Sectton Waste nage~~ent Dfvfsfon USEPA Region I JFX Federal Bldg Boston MA 02203

Ro DOVEl IIJIIICIPAL IAIIlFILL

SWoct SIIIPLING RESUL1S

Dear Ms Sprague

On March 8 1991 a representative of tile New Hlslli re Oepartbullnt of Envfrorental Services Waste Managent Dfvhfon collected ubullples eight wells at four locations betwen the Bell_- Reserwfr and the Dower Munlcfpal Landfill

The s111ples were anlayzed for the presene of volatfle organic COIIIpOunds (YOCs) using GCS (EPA oethod 624) Tile results of tile analyses indicate thlt no volatfle organic c0111p0unds were detected fn stx of ttle eight wells Various VOCs were detected tn saples taken fn wells 8-SWT and 8-BU (seeattached)

Please contact 111e at (603)271-2649 straquould you have art questions

Richard H Pease PE Relllld1al Project nager

RHP j d549 cc Carl W Baxter PE Adlrlfnfstrator NHDES -EB

II

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STATE OF NEW HAMPSHIRE

ENVIROjMENTAL S ERVICES LABORATORY

Chain of Custody Form

DES SAMPLENUMBER (s) SAMPLE LOCATION TESTS REQUESTED bull

1JSoq Jmiddot7-111S~tJ -rtJP~ 20(pound11SJD ~-81l llS MW5_LL- Vou17LSl JmiddotBbullIl 1_~ HW SLL- lfou11lS17- ~-f~l fao ~w ~wr ll~11lSl3 J-8-fl ifaD NWSWT ll-l1lSI4 JmiddotBmiddot tau IUW6WT- llc-1l1t~lS a-ampmiddot~~ (Rz~ MIN~ L)T lQWLZISI~ --1-fllrllbull ~~~ su- llo~tll~rJ l-8 11 Q 6i~ au lAilY- l11lf

-Sampfl lfo MlllDZ~ lliSf1tSl~ N-Jo~u- IIIIU

l1JgQ flloJ 2z-S lllJ--- atSld ~w rtHohamp~ __jMI_l ~ ~lZL~_ NW l(lIA- VDLS7flJ UtJ lOwJmiddot l middotfl tS U VtgtLI171 Spf J-BJ JSao oltJ o wl IAOIJbullbullbull bullu-st

-~middot middotmiddot ~c

~I

~ oate 1 rme R~~by~

J-11-f f()o ~c-hlaquo-j- 7tc4f~lOteJIIIiie Kecc ea cyJJt-~J11lt1

iii~~~t ocne7t rme Rete rvea cy

~---------------------------------------- yA-na_r__se___________

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DEPAR~ftibullo~tE~JRM=i[bullSERVICES VOLATILE ORGANIC REPORT

Extended Hazardous Subbulltance List

SAMPLE NUMBER 171509 DATE SAMPLED bull 03-07-9115 00 LOCATION bull NA

TRIP BLANKPROGRAM IDI - 6 04 SAMPLER bull JBZSITE lOt - 2910 MATRIX bull WATER

ANALYTE Result Detection Limit

Mothrlene chloride p~b BD 2 0001ch orobroaoaethane p b BD 100 ~~y~~~~~ gt BD 100

BD 100

BD 100ggr~~~r~~~g~~~ gt BD 100BDl~5Ic6~~~~thane g~ BD

100

BD 100lf7~-yen~ gsro~~anbull Ct 100

BD 1001 1 2 -Tr chlorQethane p b BD lOO11212-rbulltrachloroethane p b 1l-D ch orltgt9thYlene b 100c -112-Dichlorbethylene b 18 1 00Tr Ch OltOethY101110 BD 100Tetra~bloroethylene BD 1001 2-o1U1oioprlgtnbull BD 2 00c-13-D ch otoptopenet-1 -D ~ ~~opropene

~gr~h~xa0~ bull 8l 00o t 88

lllothr-t-Cuty1 ether 100 1 oobullrmiddotbull g

m~n~nzene b 188 X eneo (Total) b 18 l 00

M~middotr~~nbullonbull ~ 18 88 Dicb rrobonfeneo p bb BDBD 2 bull 00Met~r thy ~atone p 3000 ~=~bbn d~~~rIa~atone gg~ BD 4 00

~~Y~~~m~ cct RB 88 ~=~~i~~~~ylvinyl ether ggt BD 20 00

x~~l~ncetate ggt BD 30 00

Jmm~~~~~~~=~~~__J~L__________JL_____________JJL_____ _ ~ METHOD OF ANALYSIS- EPA 624

~0bullbull 9~~r~6~io~ ~1f~~s fh~~~ ~~rt~f~~~l10~arts per mill n Bla nk space tor result bull analyte was lookea for but ~s below detect~on

State ot DEPARTMENT OF

VOLATILE Extended Haza

SAMPLE NUMBER 171510

DATE SAMPLED - 03-08-910915 LOCATION bull DOVER DOVER LANDFILLPROGRAM IDI - 6 04 SAMPLER bull JBZ

SITE ID I - 2910 MATRIX bull WATER


METHOD OF ANALYSIS- EPA 624

~0-bull g~~r~~=~~io~ ~iTs ih=~~ ~~r~P~~~~1~onarts per mill n Blank space tor result bull analyte was lookeS for but ~s below detect~on

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DEPAR~~Mao~fEJre~RM~yeni[eSERVICES VOLATILE ORGANIC REPORT

Extended Hazardous Substance List


DATE SAMPLED - 03-08-9109 15 LOCATION PROGRAM IDI - 6 04 SAMPLERSITE IDI - 2910 MATRIX

ANALYTE Result

bull DOVER DOVER LANDFILL

bull JBZ bull WATER

Detection Limit Screen ooScreen ooScreen ooScreen ooScreen ooScreen ooScreen ooScreen 00Screen ooScreen oo screen oo ScrHn oo screen oo screen 00Screen ooScreen oo

~LICATE

~0-- g~~r~~=~~io~ 1T~s fh=~~ ~w~pe~~a1~0arts par mill n Blank space or result bull analyte was look=rtor but ~s below datactYon

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VOLATILE Extended Haz

SAMPLE NUMBER 171512 DATE SAMPLED

bull OJ-08-910930 LOCATION bull gg~ LANDFILL PROGRAM IDt bull 6 04 SAMPLER bull JBZSITE IDt bull 2910 MATRIX bull WATER


BD 200BD 100BD 100BD 100BD 100BD 100BD 100BD 100BD 100BD 100 BD 100

BD 100BD 100BD 100BD 1008D 200


~0-bull 9~~r~~=~~io~ 1T fh~~ ~~~~pe~~a1onarts per mill n Blank space tor result - analyte was lookertor but ~s below detect7on

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state of New DEPARTMENT OF ENVIR

VOLATILE ORG Extended Hazardou

SAMPLE NUMBER 171513 DATE SAMPLED bull 03-08-9109 30 LOCATION bull DOVER

DOVER LANDFILLPROGRAM IOt - 6 04 SAMPLER bull JBZSITE IDI - 2910 MATRIX bull WATER ANALYTE Result Detection Limit

Screen oo~t~~r~~~~rg~~~~tgne cc~ Screen 00 screen oo~~~~~~~~ra gg~ screen oo screen oog~r~~~r~~~~fi~ ggg Screen 00

Chloriet~ane Screen ooppbppb1 1-D ch oroethane Screen ooplb12-D ch OJoethane Screen oo111-Tr chloroethane p b Screen oo1 1 2-Tr chlorpt~thane p b Screen oo11212-Tetrachloroethane p b 1 1-o chlorthylene ~ b Screen oocpoundt-112-D1chloroethylene b screen oo Trich oroethvlepe b scrn bulloo Tetrarcloroeth~lene b scrn oo ~f7g-EMfg~ CPne ~ Screen 00

~tl ~-gtfc uoampropane ~ Screen bull00cv~Iohexag e b screen oo Mthil-t-butyl u b Screen oo

zyne b Scrn bull00 Tm~en-nzene ~ ~~~=~ ggX eneo (Total) b Scrn 00

~Po~~~naene t ~g~~ 88 Dichl~robanbullenee b Screen bulloo Me~l fthYl ketone b Screen bulloo ~=rbbn a~YIlketone t Scrn 00

~y~~~~e ggt =g~==~ gg~=~~~~=~hylvinyl ether gg~ Screen oo

X~~l~ncetate cct Screen bull00

Jmm~~~~~~__J~L_______J~~~________________JL______

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DEPAR~~yeneO~fE~~RMmftyeni[bullSERVICES VOLATILE ORGANIC REPORT

Extended Hazardous Subatance List


DATE SAMPLED - 03-08-911025 LOCATION bull DOVER DOVER LANDFILL

PROGRAM IDI 6 04 SAMPLER bull JBZSITE IDf - 2910 MATRIX bull WATER


80 200 80 100 80 100 80 100 80 100 80 100 80 100

150 100 3860 100

100 80 100

100 100 450 100 300 100 80 100 80 200


~o- 9~~ror~~io~ ~iT ih~~ ~~r~P~h~A1onarts per muu n Blank space for result bull analyte was lookeS tor but ~s below detect~on

l

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DEPAR~=yenbullO~fE~~RM=ueSERVICES

ExteX~iaT~~~~g~Ii~~~e List

SAMPLE NUMBER 171515 DATE SAMPLED - 03-08-9110 25 LOCATION bull DOVER

DOVER LANDFILLPROGRAM IDI - 604 SAMPLER bull JBZSITE IDI - 2910 MATRIX bull WATER

ANALYTE Result Detection Limit Screen oo~t~~r~~g~rg~~~~tgne cc~ Screen ooScreen oo~6Y~~~~ cc~ Screen oo

carbon tetrachloride plb screen ooCh orodibrobullobullethane p b Screen ooChloriathana p b Screen oo1 1-D chloroethane p b Screen oo1 2-o chloroathana p b Screen oo111-Tr chloroethane p b screen 00112-Tr chloroathane ppb screen oo1 1 212-Tetrachloroethane ppb 1 1-D chloroathvlene ~ b~ screen 00ci~-11 2-Dtchlorbethylene Screen 00

Screen 00tit~ m~~umiddotrn Screen oo1 2-D~c~lOfODr~na b ScrMn ooc-1 3-D ch oloplopana b ~i~middot~-g ~~Y~~ropene b screen ooCV~fohaxana ~ ScrMn bull00Ktth~l-t-butyl ether ~ Screen 00 aetRzine b screen bulloo ~tKen~nzene zg~ 88 ~l anao (Total) b ~~= bullggChr~efg~nzene b screen oo Dich rrobanfanao ~b Screen 00Methr thy ketone b ScrMn bull00 ~=~~bn ar~Ylreketone Screen bull00

~y~~m~e CCE ~~~~ 88 ~ii2~~~~~ylvinyl ether CCE screen oo X~~l~ncetate CC~ Screen bull00

_m~mf~~~~~~~~--J~L_______J~~~________________JL______

middot)

State of DEPARTMENT OF



DATE SAMPLED - 03-08-9110 30 LOCATION bull DOVER DOVER LANDFILL

PROGRAM IDI - 604 SAMPLER bull J8ZSITE IDI - 2910 MATRIX bull WATER


BD 2 00~~CI~~g~rg~i~gne ggt BD 100BD 100~~~~~~~-111 ggt BD 100BD 100g~r~~~r~~~g~~~~~= ggt BD 100

Chlorothano ppb 5 00 1001 1-o1chloroethane ppb 3 40 100

610 100lf7~-yen~lg~~~~~~ane ~ ~ BD 1001 1 2-TrtchiOr~thane b BD 1001 1 2 1 2-Tetrachloroethane b 1 1-Dbullchlorolt~thvlono b 1 20 1 00 cit-112-Dichlorbethylene b u oo 1 00 Trich oroothvlono p b 11 00 1 00 Tetra~h oroethxlbullnbull p b 2 10 1 oo ~f7~-8~~Fo~~ rone ~ t BD 2 00

~iH-~~i~H~~ampropono gt 7300 bulloo ~~of~~~~C~t1l bullthbullr gt 18 U8 Bonz no b 6 70 100J Bthy bonzono b bullsoo soo TolUene 2200 100 Rlenea (Total) 8700 1 00

~r~middotf~~nzono t a~go l 88 Dich rrobon~o~o tb BD 200Mbulll fthl~ tone b 80 30 oo ~rbbn arurJ bullketone 80 4 00

~y~~-~~~e gg~ 18 88 ~=~~i~~g~ylvinyl ether ggt BD 20 00

x~~lncbulltate ggt 60000 15000

6ti~rd~~6~~middotn gg~ bull1888 2g88 _H~~~~~~~~~___J~~--------------~t~~--------------~L______ ~ METHOD OF ANALYSIS- EPA 624

~Dmiddot 9~~r~fi~~io~ ~1T~s ih~~~- ~~r~~~~a1onarts per mini n Blank space for result a nalyte was lookeS for but ~s below detectYon

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DEPARriiyenbullO~fE~~R~=lleSERVICES

Exte~~~T~~a~~~~Ii~~Wce List



PROGRAM IDI 604 SAMPLER bull JBZSITE IDI - 2910 MATRIX bull WATER

ANALYTE Result Detection Limit Screen oo screen ooScreen oo screen oo screen oo screen oo screen ooScreen ooScreen ooScreen oo screen oo Screen 00Screen ooScreen oo screen oo screen oo

OEPAR~ftieO~tE~RS=i[bullSERVICES

Exte~3~T~~a~~~~~~~~~ List

SAMPLE NUMBER 171518 DATE SAMPLED - 03-08-911330 LOCATION bull DOVER

DOVER lANDFILLPROGRAM IDI 6 04 SAMPLER bull JBZSITE IDI - 2910 MATRIX bull WATER


-~t~cr~~~~g~~~~tg~------cc~--------------ig-----------------igg--------

~ampY~~~~-111 cc~ g 1 gg g~r~~~t~~~~~amp~ cc~ g 1ggChloriothano ppbb BD 1 oo 1 1-0 chloroethane pp 80 100 12-o chloroethane p bb a o0 1 0081 1 1-Tr chloroethane p 1 00 112-Tr chloroethane t 80 100 lbull l~l~hibullra5lfgthane bb 80 100 ct-112-oYcgftlr~thylene BD 100 Trich oroath opo BD 1 00 Tetrachloroe Ylene BD 100 1 2-oicU1o~prlgtJgtanbull ao 2 ooc-1 J-D ~~g~op~opono

~i~middotI-D rrYpropono BD 4 00 cvgyenohexano BD 2 oo ath~l-t-butyl ether 8D 100

mrn~bullbullnbull 018 1880T Uene 100l onoo (Toto) 1 oo

~~~~~~nzene 18 l gg g~~r~ir~~ono ~ 18 J3 88 ~rbpound~ af~uilokotono ~ BD 4 00

~ro=~~e ct g gg~=~~i~~~~ylvinyl ether cct 80 2000

x~~l~ncbulltate cct 80 30 00

Jmmm~~~~~~~__J~L__________JL_____________JJL______ ~ EPA METHOD 624

~0-- 9~~r~fi~io~ ~ir fh~~ ~~rt~pe~~A1~onarts per milli n Blank space tor result bull analyte was lookeSOtor but ~s below detect~on

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DEPAR~i~ieO~fEfreyRg=ubullSERVICES VOLATILE ORGANIC REPORT



DATE SAMPLED - 03-08-911330 LOCATION bull DOVER OOVER LANDFILLPROGRAM IDI 604 SAMPLER bull JBZ

SITE IDI - 2910 MATRIX bull WATER

ANALYTE Result Detection Libullit

~r~~r~~g~rg~~~itgne gg~ ~~y~~~~~ gg~ gcr~~~r~~~~~~~= cct Chloriethane ppb11-D chloroethane ppb 1 2-0 chlorEthane ppb1 1 1-Tr ch oroethane ppb112-Tr cb oroethane ppb1 1 212-Tetrachloroethane ppb1 1-o chloroethvlene ppb~~i~~~~-~~Y~thylene PPE Tetrachforoethvrene gb 1 2-DicgtlOfODropane pc-13-Dtchiotoptopene p b

~1~ ~-~h~rY~~propene I~ cv~yeno~exage bKbulltbl-i- ~o~tyl ether b rtRrn~naene t TolUene b llenea (Total) b

~~~~~~zane t Dichlorobenfenee b Methyl fthY ketone b ~=~~ af~~nlaeketone g~

~y~~~~~e CEt ~=~~i~~~ylvinyl ether ggt X~~t~ncetate ggt

Screen oo screen oo Screen 00Screen oo screen oo Screen 00 Screen oo screen oo screen oo Screen 00 screen oo Screen ooScreen 00 Screen 00Screen 00 ScrMn 00

screen bull00 Screen bull00 Screen oo ~~=~ 88 screen bull00 Screen oo

~~~ 88 screen bulloo Screen bull00 Screen bull00

lg~~ 88 Screen bulloo

Screen bull00

Jm~~m~~~__JIL_______J~~L______________JL______ ~PLICATE

~0-- 9~~r~~~io~ ~1 fh~~ ~~r~Pmiddot~~1onarts per milli n Blank space for result - analyte was lookerfor but ~s below detectYon

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DEPAR~=~eO~fE~~RMm~i[eSERVICES VOLATILE ORGANIC REPORT



DATE SAMPLED bull 03-08-911335 IDCATION bull DOVER DOVER LANDFILL

PROGRAM IOI - 604 SAMPLER bull JBZ SITE IDI - 2910 MATRIX bull WATER


80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624

~Dbull 9~~r~~~io~ ~ir fh=~~ ~~r~P~~~~1~onarts per milli n Blank space for result bull analyte was lookeS for but ~s below detectYon

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state ofDEPARTMENT OF



DATE SAMPLED bull 03-08-911335 LOCATION bull gg~~ LANDFILL PROGRAM IDf 6 04 SAMPLER bull JBZ SITE lOt bull 2910 MATRIX bull WATER


Methylene chlorideOichlorobromobullethane ~6Y~~~~gCafbon tetrachlorideCh orodibrcmoaethane Ch orietbane1 1-0 chloroethane 1 2-D cbloroethane1 1 1-Tr Chloroethane 1 1 2-Tr cb1ortbane1 1 212-Tetrachloroethane ~pound~~1~~AY~t~~~~1ene Tricb oroetbvleneTetrach oroethylene 1 2-oicnlOfOPrllpanbullc-1 3-D cbtoiOplopene ~i~ ~-D rortapropene

~~l~~tyl bulltbbullr z1nemTo ~en~nzenen enebull (Total)

~r~ef~~nbullenbull Dich lrobonfbullnbullbullMethl fthY Jtetone ~=~bn at~~nralbulltone

~Y~~~e ifi~i~=~ylvinyl ether

X~~rncetate

Jn~~~~~~~~~~~____

p~bp b Ct p b p b p b p b p bp b ~ bb

t b b

bbt tg

gtM_________J~~iiL______________JL______

Screen oo screen oo screen oo screen oo screen ooScreen oo Screen oo Screen oo Screen oo screen oo screen oo Screen oo screen oo scrn oo Screen 00 Screen oo

Screen bull00

=~~= ggscreen bulloo ~g~ ggScreen bull00 lg~ ggScreen bullooScrn bulloo scroon oo

~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE

~0-- 9~~r~~~io~ ~1T fh~~~ ~~r~ep~~~1~onarts per mill n Blank space for result bull analyte was lookeS for but ~a below detectYon

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DEPARri~~~a0~EJre~RM=libullSERVICES VOLATILE ORGANIC REPORT

Extended Hazardous Subbulltance Lbt


DATE SAMPLED - 03-08-91 15 25 LOCATION bull DOVER DOVER LANDFILLPROGRAM IDI - 604 SAMPLER bull JBZSITE IDI - 2910 MATRIX bull WATER

ANALYTE Result Detection Liait BD 200 BD 100 BD 1 00 BD 100 BD 100 BD 100 BD 100 BD 100 BD 100 BD 100 BD 100

BD 100 BD lOO BD 1 00 BD lOO BD 200

EPA METHOD 624

~Dbull 9~~r~~~~io~ 1T~s fh~~ ~~~epeh=A1onarts per milli n Blank space or result bull analyte was lookSOor but ~s below detectYon


DATE SAMPLED bull 03-08-911525 LOCATION bull DOVER DOVER LANDFILL

PROGRAM IOI - 604 SAMPLER bull JBZSITE IDI - 2910 MATRIX bull WATER

ANALYTE Rebullult Detection Limit 0

I DO

Methylene chloride p~b Screen oo 0lt Dichlorobromoaethane p b screen oo Screen oo ~zm~~~~~g E~ screen ~3oo

screen oo ltIgt CggJ~~~r~~~g~~6~ cc~ Screen oo --middot z Screen oo ~l~~~fir~~thanbull t Screen oo ~8

12-Dchlorrgthano b Screen oo ~1 1 1-Tr ch oroethane b ScrHn 00 lt D 1 12-Tr ch or~thane b Screen 00 r 1 1 2 2-Tetrachloroethane tb ur1 1~D1chlorthylono Screen 00 Dn zScreen ooi~i~Si~-~~~~~thylene o oScreen ooTotrathforooth~rono Screen 00 0H 1 2-Difilofm no Screen oo r c-1 3-D ch o p openbull r t-1 3-D ch orcproponoVi~l loride Screen bull 00 eve ohexace screen bull oo Ml ~1-t- utyl ethe~ Screen 00 1Rzine screen bull oo yeno1Ken~zene ~~~ 88 Xlanebull (Total) Screen bulloo

~r~ef~~nzene ~~~ 88 Dich rrobonfanao b ampcroon bull00 Meter fthY ketone b screen oo ~=~bampn ar~~lJAeketone g~ ScrHn bull 00

myr=-~e cc~ ~~~=~ ss ~=ix~=~ylvinyl ether gg~ Screen bulloo

x~l~ncetate ggg Screen 00

Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE

~0bullbull 9~~r~fi~io~ ~1T~s fh~~~ ~W~pe~~a1~onarts per milli n Blank space tor result bull analyte was lookartor but ~s below detect~on

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DATE SAMPLED

PROGIWI IDf SITE IDf

ANALYTE

DEPAR~~middotO~fE~~R~=i[bullSERVICES VOLATILE ORGANIC REPORT



bull 03-08-911330 WCATION bull DOVER DOVER LANDFILL

604 SAMPLER bull JBZ bull 2910 MATRIX bull WATER

Reault Detection Limit 80 200 80 100 80 10080 100 80 100 80 100 80 100 80 100 80 100 80 100 80 100

80 100 80 100 80 100 80 100 80 200

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DATE SAMPLED

PROGRAM IDt SITE IDt

State ot Ne DEPARTMENT OF ENV

VOLATILE OR Extended Hazard


- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull

DOVER DOVER LANDFILL JBZ WATER

a~1 middotarl

g- 1 ~bull rmiddotmiddotlabull f

I ANALYTE Result Detection Limit

0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

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GCMS PERFORMANCE STANDARD

Bromofluorobenzene

-l Date ~ - amp ~ I Time 4m 51nitst0rumentYI~5~f~r~lt=~~~~~~~ -2E~~~=Sample Range Ana lyst RRTV

Tune Check middot

me Ion Abundance Criteria Relative Abundance

50 15 - 40 of the base peak q-f

75 30 - 60 of the base peak -fftgt

95 Base peak 100 relat ive abundance iOO96 5 -9 of the base peak

-middot0173 Less than 1 of the base peak

--+esshy17lt Greater than 50 of the base peak q 2175 5-9 of mass 174

tf 1-11176 Greater than 95 but less than

1011 of 174 qz 2 (q

1)] 5 - 9 of IIISS 176 middot2 (~r-

1 Value in parenthesis 1s of mass 1742 Value in parenthesis is of mass 176

Conments Internal standard lot I

Internal standard abundance of ion mass 96 bull

Tuning standard abundance of ion mass 95 bull

middot)

GCIMS PER FORMANCE STANO fiRD

Bromofluorobcnzcne

Site ])~

Instrumcnt 105middotS=~o~t~e=3=t~lr=-===1~Time lfll1Sample Range_ O middot1 Analyst ~a

Tune Checkmiddot

me Ion Abundance Criteri l Relative Abundance

50 15 - 40 of the base pe ak

75 30 - amp0 of the base peak 9 I lt4bull-f

95 Base peak 100 re lative abundance

96 iOO

S -9 of the ba~e pe3 1t l 2

11 3 Less than 1X of the base peilk

174 Greater than SO of the bilSe peak middot-=---shyqshy115 S - 9 of mass 114

( ) 116 Gr eater than 95 but less than --~101 of 174 qltj ltqJltj 117 S - 9 of mass 176

1middot3 (~ i 1 Value in parenthesis is of mass 1742 Value in parenthesis is of mass 176

Conments Internal standard lot 1



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~tl

rrl I =i

f-= gil afbullfl I

--

rshy

~

~ t-

middotlt( -

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middot-0

laquo

middot-r-

~0

()

gt0 ---

middotgt O

lt

XI

3tl

J ~o

g

9o C

z Vgt

C~middot

~z

o~

~ ~~

a ~~

- ~middot w

o

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ltr ---

lt-lt (()_

-pound)

~

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~

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~ ~

rO

J ~~~ ~

~

shy

amp ~

-~ -

-~

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gbull ~

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-~ ~

~

~

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middot-) 0

~ 0

4 ct

01

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1--+

---t-+----+

-----+----+

---+---t---t--shy

~il

--j

I

-middot II

I

Oate______________-i~~--------~-----------i+-----------Ana 1yst____________-f+---==L--~--=------f+---=cccL__

Samp 1e --------------+-------l---+f-------------tl-------- shyPARAH(T[R

chloroform1 2-dichloroet~ane

111-trlchloroethanebromod 1ch 1(J romethanetr1chlorocthenebenzene middotbullod1bromoch loromethanebromoformtetrachloroethylenetoluene bullsJ)chlorobenzene 3ethyl benzene11-xylenea-xylene middotbull -to p-xylene 0cis-1 2~ 1chloroethlne1 l-d1chloroethane ~p-f luorobromobenzene1 4-dichlorobenzene

~ T-12-d1chloroethenecarbon tetrachloride12-d1chloropropanelJ-ltf1chloropropenel12-tr1chloroethanem-d1ch lorobenzeneo-d1ch 1orobenzenechloromtthanebromomethaned1ch 1orod1 f 1uoromethanevinyl chloride chloroethanemethylene chloridetr1 ch 1orof 1uoromethane1 1-d1chloroethene1 3-c 1s-d1 ch 1orop r opene2-chloroethyl vinyl ethe11 22 -tetrachloroethanTHF oacetone2-butanonecarbon disulfide2-hcxanonc ~-mcthyl-2-pcntanonestyrenevinyl 1((lr J =J j -+d1~~middot~-- _____i tJ~-~-v ~~~1 1 ~j~ ~

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Oatbull---------------t~~~~-~i ~g --~~~--~-----------++------------shyAna l yH-------------tf---~-------ft-----------tt-------------Sito_________ft--~0lt0-~cltgtIN__-tl-------H------shysample ------+f-----ll i_u_lt--__13----+l------++------shy

PARAM HR V I OUP t 0 LfV 1 OUP t 0 v 1 OUP t 0

(~ ~~lthl cr~b1 2-dtchloroethane

bromodtch 1t1 romethanetr1chlorocthene It lbenzene -11 1 ~dtbNIIIIOth loromethanebrOCDOfomtetrach1oroethy 1ene ltoluene -lbq )fch lorobenzene 2 _q ethylbenzenea-xylene a-xylenep-xylenech-1 2-dtchloroethane1 1-dtch loroethanep-f Iuorobromobenzene I Ob I I 1bull-dtchlorobenzeneT-12-dtchloroethenecarbon tetrachloride12-ltlichloropropane13-dtchloropropene 112-tr-tcllloroethanem-dtch lorobenzeneo-d1ch lorobenzenechloromethanebronIOIIIetllanedtch lorodt f luorocaethuevinyl chloridechloroethanemethylene chloridetrlchlorofluorOITitthane1 1-lt11 ch loroethene1 3-ch-d1chloropropene2-chloroethyl v1nyl ethe11 22-tetrathloroethanTHFacetone2-butanone

O a t e u3- l ~ -i l

i 1 te DOVER LF

I COMPOUND TRUE NEW I 7 DIFF

Methyl ene Chlor 1de 53 1 I 552 I 4 u

0~ 0

I 1 1- Dlchloroethene 390 I 409 I 4 8 Olt~Hz11 1 1- Dichloroethane 376 I 34 0 I -9 5 H ~ltJgtC-ltz

I 1 2- Di ch lor oethene 302 I 343 I 13 7 H~8Hl)I ChloroforM 35 6 I 33 0 I -7 4 lt~r1r

ld4-1 2 Dichloro e thane 3 0 2 I 252 I - 165 r~n z

11 2-Dichloroethane 296 I 257 I -132 00

IMethyl-T-Butyl Ether 474 I 492 I 3 8

OH

rr

11 I 1-Trichloroethbullne 321 I 306 I -4 6

ICycloheune 249 I 230 I -7 6

I Br DMOd ichl or oMet hbullne 317 I 29 I I -a 1

I Tr ich 1or oethene 351 I 340 I - 3 0

I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3

I Dibr OMOCh 1 or OMet hane 392 I 333 I - 15 0

IBroMofo r 34 7 I 303 I - 1 26

I Tetrach 1 or oe 1 h y lene 389 I 4 1 5 I 6 7

I Toluene 34 7 I 322 I - l 3

I Ch 1 or oben zene 354 I 343 I - 3 2

IEthylben zene 3 4 7 I 348 1 4

l p-BFB 3 3 5 I 309 I - 7 6

I S tyr ene 0 0 I 0 0 I XmiddotXgtICmiddotIImiddotIImiddotXmiddot

lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470

barcodetext SDMS Doc ID 558470

II

- II

STATE OF NEW HAMPSHIRE

ENVIROjMENTAL S ERVICES LABORATORY

Chain of Custody Form

DES SAMPLENUMBER (s) SAMPLE LOCATION TESTS REQUESTED bull

1JSoq Jmiddot7-111S~tJ -rtJP~ 20(pound11SJD ~-81l llS MW5_LL- Vou17LSl JmiddotBbullIl 1_~ HW SLL- lfou11lS17- ~-f~l fao ~w ~wr ll~11lSl3 J-8-fl ifaD NWSWT ll-l1lSI4 JmiddotBmiddot tau IUW6WT- llc-1l1t~lS a-ampmiddot~~ (Rz~ MIN~ L)T lQWLZISI~ --1-fllrllbull ~~~ su- llo~tll~rJ l-8 11 Q 6i~ au lAilY- l11lf

-Sampfl lfo MlllDZ~ lliSf1tSl~ N-Jo~u- IIIIU

l1JgQ flloJ 2z-S lllJ--- atSld ~w rtHohamp~ __jMI_l ~ ~lZL~_ NW l(lIA- VDLS7flJ UtJ lOwJmiddot l middotfl tS U VtgtLI171 Spf J-BJ JSao oltJ o wl IAOIJbullbullbull bullu-st

-~middot middotmiddot ~c

~I

~ oate 1 rme R~~by~

J-11-f f()o ~c-hlaquo-j- 7tc4f~lOteJIIIiie Kecc ea cyJJt-~J11lt1

iii~~~t ocne7t rme Rete rvea cy

~---------------------------------------- yA-na_r__se___________

---------------------------------------------------------------------------







BD 100


100



















---------------------------------------------------------------------------





ANALYTE Result


bull JBZ bull WATER


~LICATE


---------------------------------------------------------------------------







BD 100BD 100BD 100BD 1008D 200



---------------------------------------------------------------------------












Jmm~~~~~~__J~L_______J~~~________________JL______

I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100

150 100 3860 100

100 80 100

100 100 450 100 300 100 80 100 80 200



l

I 8

---------------------------------------------------------------------------

I I

~ I I









_m~mf~~~~~~~~--J~L_______J~~~________________JL______

middot)
















---------------------------------------------------------------------------

I I

~ I I












-~t~cr~~~~g~~~~tg~------cc~--------------ig-----------------igg--------









---------------------------------------------------------------------------















Screen bull00



I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

--

rshy

~

~ t-

middotlt( -

N

(J

middot-0

laquo

middot-r-

~0

()

gt0 ---

middotgt O

lt

XI

3tl

J ~o

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9o C

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C~middot

~z

o~

~ ~~

a ~~

- ~middot w

o

lt~

~ ~I

cltl tlr

gto

~~ ~

ltr ---

lt-lt (()_

-pound)

~

iJ 9

~ (fl

cV

-D

-r

~

~

clt c-lt

~ ~

rO

J ~~~ ~

~

shy

amp ~

-~ -

-~

- -~ - ggt

~

gbull ~

~

-~ ~

~

~

~

~-lt ~

~

0

~

~

~

I

iil~ I

w

~

~ ~

i f

~

~ ~ 1

middot-) 0

~ 0

4 ct

01

-shy0

1--+

---t-+----+

-----+----+

---+---t---t--shy

~il

--j

I

-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


---------------------------------------------------------------------------







BD 100


100



















---------------------------------------------------------------------------





ANALYTE Result


bull JBZ bull WATER


~LICATE


---------------------------------------------------------------------------







BD 100BD 100BD 100BD 1008D 200



---------------------------------------------------------------------------












Jmm~~~~~~__J~L_______J~~~________________JL______

I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100

150 100 3860 100

100 80 100

100 100 450 100 300 100 80 100 80 200



l

I 8

---------------------------------------------------------------------------

I I

~ I I









_m~mf~~~~~~~~--J~L_______J~~~________________JL______

middot)
















---------------------------------------------------------------------------

I I

~ I I












-~t~cr~~~~g~~~~tg~------cc~--------------ig-----------------igg--------









---------------------------------------------------------------------------















Screen bull00



I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

--

rshy

~

~ t-

middotlt( -

N

(J

middot-0

laquo

middot-r-

~0

()

gt0 ---

middotgt O

lt

XI

3tl

J ~o

g

9o C

z Vgt

C~middot

~z

o~

~ ~~

a ~~

- ~middot w

o

lt~

~ ~I

cltl tlr

gto

~~ ~

ltr ---

lt-lt (()_

-pound)

~

iJ 9

~ (fl

cV

-D

-r

~

~

clt c-lt

~ ~

rO

J ~~~ ~

~

shy

amp ~

-~ -

-~

- -~ - ggt

~

gbull ~

~

-~ ~

~

~

~

~-lt ~

~

0

~

~

~

I

iil~ I

w

~

~ ~

i f

~

~ ~ 1

middot-) 0

~ 0

4 ct

01

-shy0

1--+

---t-+----+

-----+----+

---+---t---t--shy

~il

--j

I

-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470










---------------------------------------------------------------------------





ANALYTE Result


bull JBZ bull WATER


~LICATE


---------------------------------------------------------------------------







BD 100BD 100BD 100BD 1008D 200



---------------------------------------------------------------------------












Jmm~~~~~~__J~L_______J~~~________________JL______

I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100

150 100 3860 100

100 80 100

100 100 450 100 300 100 80 100 80 200



l

I 8

---------------------------------------------------------------------------

I I

~ I I









_m~mf~~~~~~~~--J~L_______J~~~________________JL______

middot)
















---------------------------------------------------------------------------

I I

~ I I












-~t~cr~~~~g~~~~tg~------cc~--------------ig-----------------igg--------









---------------------------------------------------------------------------















Screen bull00



I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

--

rshy

~

~ t-

middotlt( -

N

(J

middot-0

laquo

middot-r-

~0

()

gt0 ---

middotgt O

lt

XI

3tl

J ~o

g

9o C

z Vgt

C~middot

~z

o~

~ ~~

a ~~

- ~middot w

o

lt~

~ ~I

cltl tlr

gto

~~ ~

ltr ---

lt-lt (()_

-pound)

~

iJ 9

~ (fl

cV

-D

-r

~

~

clt c-lt

~ ~

rO

J ~~~ ~

~

shy

amp ~

-~ -

-~

- -~ - ggt

~

gbull ~

~

-~ ~

~

~

~

~-lt ~

~

0

~

~

~

I

iil~ I

w

~

~ ~

i f

~

~ ~ 1

middot-) 0

~ 0

4 ct

01

-shy0

1--+

---t-+----+

-----+----+

---+---t---t--shy

~il

--j

I

-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


---------------------------------------------------------------------------







BD 100BD 100BD 100BD 1008D 200



---------------------------------------------------------------------------












Jmm~~~~~~__J~L_______J~~~________________JL______

I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100

150 100 3860 100

100 80 100

100 100 450 100 300 100 80 100 80 200



l

I 8

---------------------------------------------------------------------------

I I

~ I I









_m~mf~~~~~~~~--J~L_______J~~~________________JL______

middot)
















---------------------------------------------------------------------------

I I

~ I I












-~t~cr~~~~g~~~~tg~------cc~--------------ig-----------------igg--------









---------------------------------------------------------------------------















Screen bull00



I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

--

rshy

~

~ t-

middotlt( -

N

(J

middot-0

laquo

middot-r-

~0

()

gt0 ---

middotgt O

lt

XI

3tl

J ~o

g

9o C

z Vgt

C~middot

~z

o~

~ ~~

a ~~

- ~middot w

o

lt~

~ ~I

cltl tlr

gto

~~ ~

ltr ---

lt-lt (()_

-pound)

~

iJ 9

~ (fl

cV

-D

-r

~

~

clt c-lt

~ ~

rO

J ~~~ ~

~

shy

amp ~

-~ -

-~

- -~ - ggt

~

gbull ~

~

-~ ~

~

~

~

~-lt ~

~

0

~

~

~

I

iil~ I

w

~

~ ~

i f

~

~ ~ 1

middot-) 0

~ 0

4 ct

01

-shy0

1--+

---t-+----+

-----+----+

---+---t---t--shy

~il

--j

I

-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


---------------------------------------------------------------------------












Jmm~~~~~~__J~L_______J~~~________________JL______

I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100

150 100 3860 100

100 80 100

100 100 450 100 300 100 80 100 80 200



l

I 8

---------------------------------------------------------------------------

I I

~ I I









_m~mf~~~~~~~~--J~L_______J~~~________________JL______

middot)
















---------------------------------------------------------------------------

I I

~ I I












-~t~cr~~~~g~~~~tg~------cc~--------------ig-----------------igg--------









---------------------------------------------------------------------------















Screen bull00



I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

--

rshy

~

~ t-

middotlt( -

N

(J

middot-0

laquo

middot-r-

~0

()

gt0 ---

middotgt O

lt

XI

3tl

J ~o

g

9o C

z Vgt

C~middot

~z

o~

~ ~~

a ~~

- ~middot w

o

lt~

~ ~I

cltl tlr

gto

~~ ~

ltr ---

lt-lt (()_

-pound)

~

iJ 9

~ (fl

cV

-D

-r

~

~

clt c-lt

~ ~

rO

J ~~~ ~

~

shy

amp ~

-~ -

-~

- -~ - ggt

~

gbull ~

~

-~ ~

~

~

~

~-lt ~

~

0

~

~

~

I

iil~ I

w

~

~ ~

i f

~

~ ~ 1

middot-) 0

~ 0

4 ct

01

-shy0

1--+

---t-+----+

-----+----+

---+---t---t--shy

~il

--j

I

-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100

150 100 3860 100

100 80 100

100 100 450 100 300 100 80 100 80 200



l

I 8

---------------------------------------------------------------------------

I I

~ I I









_m~mf~~~~~~~~--J~L_______J~~~________________JL______

middot)
















---------------------------------------------------------------------------

I I

~ I I












-~t~cr~~~~g~~~~tg~------cc~--------------ig-----------------igg--------









---------------------------------------------------------------------------















Screen bull00



I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

--

rshy

~

~ t-

middotlt( -

N

(J

middot-0

laquo

middot-r-

~0

()

gt0 ---

middotgt O

lt

XI

3tl

J ~o

g

9o C

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C~middot

~z

o~

~ ~~

a ~~

- ~middot w

o

lt~

~ ~I

cltl tlr

gto

~~ ~

ltr ---

lt-lt (()_

-pound)

~

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cV

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-r

~

~

clt c-lt

~ ~

rO

J ~~~ ~

~

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amp ~

-~ -

-~

- -~ - ggt

~

gbull ~

~

-~ ~

~

~

~

~-lt ~

~

0

~

~

~

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I






I

-

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OH

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I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


---------------------------------------------------------------------------

I I

~ I I









_m~mf~~~~~~~~--J~L_______J~~~________________JL______

middot)
















---------------------------------------------------------------------------

I I

~ I I












-~t~cr~~~~g~~~~tg~------cc~--------------ig-----------------igg--------









---------------------------------------------------------------------------















Screen bull00



I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

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f-= gil afbullfl I

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I

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I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470

















---------------------------------------------------------------------------

I I

~ I I












-~t~cr~~~~g~~~~tg~------cc~--------------ig-----------------igg--------









---------------------------------------------------------------------------















Screen bull00



I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

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f-= gil afbullfl I

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I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470







-~t~cr~~~~g~~~~tg~------cc~--------------ig-----------------igg--------









---------------------------------------------------------------------------















Screen bull00



I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

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I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


---------------------------------------------------------------------------















Screen bull00



I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

--

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--j

I

-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


I I

~ I I







80 200 80 100 80 100 80 100 80 100 80 100 80 100 80 100

100RB 100 80 100

80 100 80 100 80 1 00 80 100 80 2 00

EPA METHOD 624


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

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~

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4 ct

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I

-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


---------------------------------------------------------------------------










X~~rncetate

Jn~~~~~~~~~~~____


t b b

bbt tg

gtM_________J~~iiL______________JL______


Screen bull00


~g~==~ ggScreen oo

Screen bull 00

~DUPLICATE


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

--

rshy

~

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--j

I

-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


---------------------------------------------------------------------------

I I

~ I I







EPA METHOD 624






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

--

rshy

~

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--j

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-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470






I DO







Jm~~~~~~~~~~__J~L_______J~~~________________JL_____ _ ~PLICATE


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

Jil I 1 I

~tl

rrl I =i

f-= gil afbullfl I

--

rshy

~

~ t-

middotlt( -

N

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--j

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-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


I I

~ I I

DATE SAMPLED


ANALYTE







80 100 80 100 80 100 80 100 80 200

I I

~ I I

ilH l

DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

bull bull


a~1 middotarl



0 ~ 0Olt 3 ~ z ~ 3 ltIgt C ~ z

~ ~~ ~ ~

lt ~

r r middot ~ n z

l o o op

r

II

~ II


Bromofluorobenzene


Tune Check middot








1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

Site ])~


Tune Checkmiddot





96 iOO









I I ~ I I

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I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


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DATE SAMPLED





- 03-08-91 13 30 LOCATION

- 6 04 - 2910

SAMPLER MATRIX

bull

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I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


II

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Bromofluorobenzene


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1011 of 174 qz 2 (q






middot)


Bromofluorobcnzcne

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96 iOO









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0~ 0






OH

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I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470



Bromofluorobcnzcne

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96 iOO









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OH

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I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


I I ~ I I

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f-= gil afbullfl I

--

rshy

~

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middotlt( -

N

(J

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laquo

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I






I

-

I

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i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


1--+

---t-+----+

-----+----+

---+---t---t--shy

~il

--j

I

-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


I

-middot II

I






I

-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


-

I

II

I






i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470



i 1 te DOVER LF



0~ 0






OH

rr





I db-Benzene 2 1 3 I 21 3 I - 1

I Benzene 35 1 I 33 6 I --4 3


IBroMofo r 34 7 I 303 I - 1 26


I Toluene 34 7 I 322 I - l 3



l p-BFB 3 3 5 I 309 I - 7 6


lt - Xylene 346 I 30 0 I 9

I p - Xylene 34 C I 30 8 I 11 6

barcode 558470


DEPARTMENT OF ENVIRONMENTAL SERVICES …. i - i i . state of new hampshire . enviroj!mentas ervices...

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Transcript of DEPARTMENT OF ENVIRONMENTAL SERVICES …. i - i i . state of new hampshire . enviroj!mentas ervices...