C.V.Eng.& Arabic

29
1 1 Start 2 Select preferred name 3 Review documents 4 Review profile 5 Submit changes Select authored documents by Madkour, Loutfy H. Please uncheck the documents not authored by Madkour, Loutfy H. from the list of 19 documents by selecting the red cross-mark. Sort by Document Title Author(s) Date Source Title (1)Inhibition effect of Schiff base compounds on the corrosion of iron in nitric acid and sodium hydroxide solutions View in Scopus | Hide abstract Madkour, L.H., Zinhome, U.A. 2010 Journal of Corrosion Science and Engineering 13 Studies using chemical and electrochemical techniques were carried out on an iron electrode in 2.0 mo I/liter - nitric acid and 2.0 mol/liter sodium hydroxide solutions to evaluate the corrosion behavior. Schiff bases investigated are found to function well as corrosion inhibitors for iron metal in both nitric acid and sodium hydroxide solutions, but a better performance is noticed in nitric acid solution. This is due to the less negative potential of iron in acidic solution, favoring adsorption of the additives. The Schiff bases act as mixed type inhibitors in acidic solution, whereas they cause only inhibition of the cathode process in alkaline medium and the magnitude of the displacement of the Tafel plot is proportional to its concentration. The additives inhibit the corrosion through their ability of getting adsorbed on the iron surface by interaction with π-electrons of the aromatic rings, and the azo methine group. The adsorption process was found to obey Temkin adsorption isotherm. Also, the adsorbed Schiff base molecules interact with iron ions formed on the metal surface leading to neutral and cationic iron-Schiff base complexes. Models for the inhibition corrosion behavior were developed based upon various statistical analyses of the experimental data. © University of Manchester and the authors. (2) SEMICONDUCTIVITY BEHAVIOUR OF EGYPTIAN NATURAL SINTERED ORE FOR THERMOTECHNOLOGICAL APPLICATIONS (3)Inhibition effect of hydantoin compounds on the corrosion of iron in nitric and sulfuric acid solutions View in Scopus | Hide abstract Madkour, Loutfy.H., Madkour, L.H., Hassanein, A.M., Ghoneim, M.M., Eid, S.A. 2010 2001 Journal of the University of Chemical Technology and Metallurgy, 45, 3, 2010, 335-346 Monatshefte fur Chemie 132 (2) , pp. 245

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Transcript of C.V.Eng.& Arabic

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1 Start

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3 Review documents

4 Review profile

5 Submit changes

Select authored documents by Madkour, Loutfy H.

Please uncheck the documents not authored by Madkour, Loutfy H. from the list of 19 documents by selecting the red

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Document Title Author(s) Date Source Title

(1)Inhibition effect of Schiff base

compounds on the corrosion of iron in nitric

acid and sodium hydroxide solutions View in Scopus | Hide abstract

Madkour, L.H., Zinhome, U.A.

2010

Journal of Corrosion

Science and

Engineering 13

Studies using chemical and electrochemical techniques were carried out on an iron electrode in 2.0 mo I/liter -

nitric acid and 2.0 mol/liter sodium hydroxide solutions to evaluate the corrosion behavior. Schiff bases

investigated are found to function well as corrosion inhibitors for iron metal in both nitric acid and sodium

hydroxide solutions, but a better performance is noticed in nitric acid solution. This is due to the less negative

potential of iron in acidic solution, favoring adsorption of the additives. The Schiff bases act as mixed type

inhibitors in acidic solution, whereas they cause only inhibition of the cathode process in alkaline medium and the

magnitude of the displacement of the Tafel plot is proportional to its concentration. The additives inhibit the

corrosion through their ability of getting adsorbed on the iron surface by interaction with π-electrons of the

aromatic rings, and the azo methine group. The adsorption process was found to obey Temkin adsorption isotherm.

Also, the adsorbed Schiff base molecules interact with iron ions formed on the metal surface leading to neutral and

cationic iron-Schiff base complexes. Models for the inhibition corrosion behavior were developed based upon

various statistical analyses of the experimental data. © University of Manchester and the authors.

(2) SEMICONDUCTIVITY BEHAVIOUR OF

EGYPTIAN NATURAL SINTERED ORE

FOR THERMOTECHNOLOGICAL

APPLICATIONS

(3)Inhibition effect of hydantoin compounds on the

corrosion of iron in nitric and sulfuric acid

solutions

View in Scopus | Hide abstract

Madkour, Loutfy.H.,

Madkour, L.H., Hassanein, A.M.,

Ghoneim, M.M., Eid, S.A.

2010

2001

Journal of the University of

Chemical Technology and

Metallurgy, 45, 3, 2010,

335-346

Monatshefte fur

Chemie 132 (2) , pp.

245

Page 2: C.V.Eng.& Arabic

2

The inhibition of corrosion of iron in 2 M nitric acid and 2 M sulfuric acid solutions by substituted

phenylhydantoin, thiohydantoin, and dithiohydantoin compounds was measured using thermometric, weight loss,

and polarization methods. The three methods gave consistent results. The polarization curves indicated that the

hydantoin compounds act as mixed-type inhibitors. The adsorption of the inhibitors were found to obey the

Temkin adsorption isotherm. The higher inhibition efficiency of the additives in nitric with respect to sulfuric acid

solution may be attributed to the reduced formation of soluble quaternary nitrogen salts in nitric acid medium,

favouring adsorption of the parent additive on the metal surface. The obtained results indicate that the corrosion

rate of iron in both acids increases with increasing temperature, both in absence and presence of the tested

inhibitors. Kinetic-thermodynamic model functions and Temkin isotherm data are compared and discussed. The

synergistic effect of halide anions on the inhibition efficiency of the hydantoin compounds was also investigated.

(4)Kinetics of substituted bis- and mono-azo dyes as

corrosion inhibitors for aluminium in hydrochloric

acid and sodium hydroxide solutions

View in Scopus | Hide abstract

Madkour, L.H., Issa, R.M., El-

Ghrabawy, I.M.

1999

Journal of Chemical

Research - Part S (7) ,

pp. 408

This investigation is designed to apply an advanced kinetic-thermodynamic model on the data obtained from

acidic and alkaline corrosion of aluminium using bis- and mono-azo dyes as corrosion inhibitors.

(5)Electrochemical Behaviour of 3-Arylazo-1,2,4-

triazole Compounds in Aqueous Buffered Solutions

View in Scopus | Hide abstract

Madkour, L.H. 1998

Journal of Chemical

Research - Part S (9) ,

pp. 514

A variety of electroanalytical methods, e.g. DC polarography, cyclic voltammetry and controlled potential

coulometry have been employed upon 3-arylazo-1,2,4-triazole derivatives, AAT; substituents affect the reduction

potentials but do not alter the reduction pattern.

(6)Inhibition of the acid corrosion of iron with

haloacetic acids

View in Scopus | Hide abstract

El-Gaber, A.S.,

Madkour, L.H., El-

Asklany, A.H., Fouda, A.S.

1997

Bulletin of

Electrochemistry 13

(2) , pp. 62

The efficiency of chloro, dichloro, trichloro, bromo, and iodoacetic acids as inhibitors for acid corrosion of iron

was studied using polarization technique. A significant retardation of the corrosion rate is observed in the inhibited

HNO3 solution. The rate of corrosion depends on the nature of the inhibitor and its concentration and on the

temperature of the system. It was found that iodoacetic acid has a significant inhibiting effect on the corrosion of

the metal and protection efficiencies approaching 94% were measured. The inhibitor shifts the free corrosion

potential in the cathodic direction and polarizes both the cathodic and anodic half reactions. It was found that the

compounds under consideration are chemisorbed on the iron surface according to the Frumkin isotherm. The Tafel

slope is approximately constant and independent of the concentration of the inhibitor. The thermodynamic

parameters of adsorption obtained reveal a strong interaction of these inhibitors on the iron surface.

(7)Inhibition of the corrosion of 16/14 austenitic

stainless steel by oxygen and nitrogen containing

compounds

Madkour, L.H., Ghoneim, M.M.

1997

Bulletin of

Electrochemistry 13

(1) , pp. 1

Page 3: C.V.Eng.& Arabic

3

View in Scopus | Hide abstract

Corrosion inhibition by methoionine (MET), citrulline (CIT), alanine (AL), glycine (GLY) and hydroxyproline

(HPR) with respect to the dissolution of tungsten stainless steels in hydrochloric acid solution was studied using

potentiodynamic, Tafel extrapolation and polarization resistance methods. Polarization curves indicated that the

primary passivation potential (Epp) and the transpassive region shift towards more positive potentials in presence

of the studied amino acids, i.e. there is more passivation at wide potential range in the presence of amino acid

inhibitors. The corrosion parameters are dependent on the percentage of tungsten in the alloy composition as well

as the nature of the tested amino acids. The intermetallic compound Fe3W2 may form a galvanic cell with the

matrix around the Fe3W2 phase within the matrix that is formed as a dispersed phase.

(8)Thermodynamic behaviour of complex

antimonite ore for electrodeposition of metal value

View in Scopus | Hide abstract Madkour, L.H. 1997

Journal de Chimie

Physique et de

Physico-Chimie

Biologique 94 (3) , pp.

620

This paper outlines the hydrometallurgical processing and the various possible approaches for the recovery of

metallic antimony from its antimonite sulphide ore by electrolysis. Thermodynamic calculations have been made

to find the optimum conditions for roasting and/or sulphate roasting of Wadi Abu Quraiya antimonite ore. The

antimonite ore (Sb2S3) is roasted directly without concentration and large savings in reagent and chemical

processes are expected. A suitable roasting temperature of 1200 K for 4 hours has been determined. Metallic

antimony is cathodically electrodeposited with a high current efficiency at current densities of 350 to 500 A/m2

depending on the composition of leach liquor solutions. The results of the electron microscopy investigation

confirmed by metal value data in the ASTM cards are in good agreement with the chemical analysis.

(9)Electrolytic recovery of antimony from natural

stibnite ore

View in Scopus | Hide abstract

Madkour, L.H., Salem, I.A.

1996 Hydrometallurgy 43

(1-3) , pp. 265

Stibnite ore at Wadi Abu Quraiya, situated in the central Eastern Desert of Egypt has been subjected to

petrographical, mineralogical, infrared, X -ray diffraction, chemical and spectral analyses. Hydrometallurgical

treatment based on leaching with acids, precipitation and electrode-position of metal values from the ore have been

developed. Studies to investigate suitable electrolytic baths for the cathodic deposition of metallic antimony either

directly from the leach liquor or in the presence of complexing agents have been carried out. The influence of

various factors on the electrodeposition process of the element from its electrolyte solutions is discussed.

Advantages of the flowsheet and various approaches depending on convenient electrolytes for the deposition of

antimony from the stibnite ore have been investigated. The results of spectrophotometric and chemical analyses

revealed that the purity of the metal is > 99%.

(10)Thermo-physical studies on ilmenite ore for

mass production of ceramic capacitors

View in Scopus | Hide abstract

Madkour, L.H., Abou-

Sekkina, M.M.,

Hemeda, O.M.

1996

Erzmetall: Journal for

Exploration, Mining

and Metallurgy 49 (5) ,

pp. 309

The ore of the ilmenite deposit in Wadi Abou Ghalaga, Eastern Desert has been subjected to chemical, differential

thermal and X-ray analyses. Thermophysical and chemical treatment of the ore based on sintering at 1000°C upon

which electrical conductivity, dielectric constant and dielectric loss vs. temperature have been developed. Results

Page 4: C.V.Eng.& Arabic

4

obtained led to promising data in forming its very high dielectric constant and very low dielectric loss (tan δ),

which makes it suitable as a good source for mass production of ceramic capacitors. Furthermore, the AC

conduction mechanism and energy gap as well as the extrinsic activation energy were evaluated. - In the present

work, all of the electric and dielectric measurements of the ilmenite ore make it suitable for the production of

ceramic capacitors in the electronic industry.

(11)Electrodeposition of lead and its dioxide from

Egyptial carbonate ore residuum

View in Scopus | Hide abstract

Madkour, L.H. 1996

Bulletin of

Electrochemistry 12

(3-4) , pp. 234

Acid-leach residue resulting from the sulphate roasting of Zn-Pb Egyptial carbonate ore is used for the production

of lead, after hydrometallurgical treatments. Studies to investigate various baths for the deposition of lead and lead

dioxide have been carried out. The results showed a wide variety of electrolysis, either soluble simple salts, or

those containing complex anions and in virtually all cases, very high current efficiencies are obtained. The effects

of various factors on the electrodeposition of Pb and PbO2 are discussed. In commercial practice, the properties

and service requirements dictate the precise electrolyte that should be used since the properties of electrodeposited

lead vary with the baths. Mechanism of the electrolytic production of the element and its dioxide is discussed. The

results spectrophotometric and chemical analyses revealed that the purity of the metal is > 99%.

(12)Electrolytic separation of lead and its dioxide

from carbonate ore residiuum

View in Scopus | Hide abstract

Madkour, L.H. 1995

Indian Journal of

Chemical Technology

2 (6) , pp. 343

The electrolytic separation of lead and lead dioxide from pre-roasted carbonate ore residues was studied using a

variety of acid and alkaline baths. The optimum conditions and the efficiency of the electrolyte extraction was

determined. The effects of current density, temperature, and metal ion concentration on the faradic current

efficiency were investiagated.

(13)Inhibition of copper corrosion by

arylazotriazoles in nitric acid solution

View in Scopus | Hide abstract

Madkour, L.H., Elmorsi, M.A.,

Ghoneim, M.M.

1995

Monatshefte für

Chemie Chemical

Monthly 126 (10) , pp.

1087

A study has been made to investigate the effect of some azoheterocyclic dyes of the type 3-arylazo 1,2,4-triazole

(AT) on the corrosion of copper exposed to 0.5 M nitric acid solution at different temperatures and at different AT

concentrations. Using potentiodynamic polarization and Tafel electrochemical methods, it can be shown that AT

compounds are good inhibitors of copper corrosion in HNO3 solution. The kinetic and thermodynamic parameters

of the inhibited system were determined. The high inhibition efficiency of these compounds may be due to the

adsorption of the additive itself and/or the adsorption of the formed Cu(II)-AT complexes at the polarized

electrode interface. Cathodic polarization measurements showed that AT dyes are predominantly cationic

inhibitors. © 1995 Springer-Verlag.

(14)HYDRO- AND ELECTROMETALLURGY

TREATMENT OF CASSITERITES ( greater than

S%NO//2 CONCENTRATE.

View in Scopus | Hide abstract

Madkour, L.H. 1988 Aufbereitungs-Technik

29 (5) , pp. 273

Electrolytic extraction methods are used to process Igla cassiterite concentrate in the central part of the Eastern

Desert of Egypt. The cassiterite is subjected to alkaline leaching using caustic soda in the presence of sodium

nitrate as an oxidant in a ball-mill autoclave, where grinding and leaching take place simultaneously. The

influences of the amount and concentration of caustic soda and sodium nitrate, and of the digestion temperature

Page 5: C.V.Eng.& Arabic

5

and time on the alkaline leaching efficiency of tin recovery are discussed. The results obtained are found to

coincide well with the corresponding ASTM cards for Na//2SnO//3 multiplied by (times) 3H//2O. Acid leaching

and fusion methods are also applied to cassiterite processing. The effect of leaching efficiency of various baths, the

optimum current density and the temperature on the tin recovery and the current efficiency are tabulated. The

results of electron microscopic investigation, confirmed by the metal values given in the ASTM cards, coincide

well with those given by spectrophotometric and chemical analyses.

(15)THERMODYNAMIC STUDIES ON

SULPHATE ROASTING FOR ZINC

ELECTROWINNING FROM CARBONATE

ORE.

View in Scopus | Hide abstract

Madkour, Loutfy H. 1986

Journal of Chemical

Technology and

Biotechnology 36 (5) ,

pp. 197

The bulk of the work consists of a theoretical study of the possibility of submitting Umm-Gheig carbonate ore to

sulphate roasting. The use of the admixture with pyrites is to enable a carbonate ore to be treated in a similar way

to a sulphide ore, and by doing so, to produce a roasted product capable of being treated by orthodox zinc

electrowinning methods using sulphate solutions. Thermodynamic studies have been made to find the optimum

conditions for sulphate roasting, in either normal air or enriched 36% oxygen air. The results of the electron

microscopic investigation confirmed by metal value data given in the ASTM cards coincide well with results given

by chemical analysis.

(16)HYDROMETALLURGICAL AND

ELECTROMETALLURGICAL TREATMENT

OF CASSITERITE CONCENTRATE.

View in Scopus | Hide abstract

Madkour, Loutfy H. 1986

Erzmetall: Journal for

Exploration, Mining

and Metallurgy 39 (4) ,

pp. 162

Electrowinning is carried out on Igla concentrate in the Eastern Desert of Egypt. The grain size, chemical,

mechanical and x-ray diffraction analyses were investigated. Soluble stannate is produced from after alkaline

treatment. Leaching efficiency from various baths, current density, temperature, tin recovery and current efficiency

were tabulated. Recommended flowsheets are given.

(17)Electrodeposition of titanium and its dioxide

from ilmenite

View in Scopus

Madkour, L.H., Fouda, A.S.

1986

Journal of

Electroanalytical

Chemistry 199 (1) , pp.

207

(18)RECOMMENDED FLOWSHEETS FOR THE

ELECTROLYTIC EXTRACTION OF LEAD

AND ZINC FROM RED SEA POLYMETAL

ORE.

View in Scopus | Hide abstract

Madkour, Loutfy H. 1985

Journal of chemical

technology and

biotechnology.

Chemical technology

35 A (3) , pp. 108

The polymetal complex ore Umm-Gheig considered in Egypt as a rather rich source of lead and zinc is subjected

to mineralogical, chemical, spectral, X-ray and differential thermal analyses. Hydrometallurgical treatments based

on leaching, precipitation and electrodeposition of metal from the ore are established. The influences of current

density, temperature and metal ion concentration on the Faradic current efficiency are discussed. Advantages and

disadvantages of flowsheets and various approaches depending on convenient baths for the electrodeposition of

metals are investigated. The results of electron microscopic investigation confirmed by metal value data given in

the A. S. T. M. cards coincide well with those given by chemical analysis.

(19)POLAROGRAPHIC REDUCTION OF SOME

ARYLIDENE DERIVATIVES OF OXALIC

HYDRAZIDE IN BUFFER SOLUTIONS OF

VARYING pH.

Issa, R.M., Ghoneim, M.M.,

El-Baradie, H.Y.F.,

Madkour, L.H. 1985

Electrochemical

Society Extended

Abstracts 85-1 , pp.

754

Page 6: C.V.Eng.& Arabic

6

View in Scopus | Hide abstract

The polarograms obtained in solutions of pH 2-5 display a single wave with almost identical heights. The value of

the diffusion coefficient was obtained from the Stockes relation; and the molar volume was calculated from the

molecular height and density. The important kinetic parameters of the electrode reaction are determined using the

Koutecky method and its modification. The values confirmed the irreversible kinetic controlled nature of the

waves.

(20)ELECTROCHEMICAL REDUCTION OF

SOME ARYLIDENE DERIVATIVES OF

SALICYLIC, OXALIC, SUCCINIC AND

METHYL ( 2-HYDROXY PHENIDENE )-

BENZOIC HYDRAZIDES IN NONAQUEOUS

MEDIUM AT A MERCURY CATHODE.

View in Scopus | Hide abstract

Ghoneim, M.M., Issa, R.M.,

Madkour, L.H. 1985

Electrochemical

Society Extended

Abstracts 85-1 , pp.

753

Hydrazides of organic acids and their arylidene derivatives became of special interest in recent years since they

readily function as chelating agents. This work deals with the polarographic reduction of arylidene derivatives of

some organic acid hydrazides in DMF containing N (C//4 H//9)//4Clo//4. This is to elucidate their reduction

processes at the DME. The nature of the electrode reaction and its kinetic parameters (k degree //f//,//h, DELTA

G* and alpha ) have been determined and discussed.

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Page 7: C.V.Eng.& Arabic

7

Loutfy Hamid Madkour

Professor of Physical Chemistry, Saudi Arabia

Prof. Loutfy H. Madkour graduated as B. Sc. Chem. in 1972 at Cairo University and

as M.Sc. Electrometallurgy at Menia University in 1979. In 1982 He obtained his Ph.D.in Electro-chemistry at Tanta University. Prof. Dr. Madkour, s special research

interests are : Physical chemistry, Electrochemistry, Electrometallurgy, Electro

analytical chemistry, Analytical chemistry, Polarography, Electrolytic extraction of

heavy metals from natural ores and deposits, Electrochemical thermodynamics,

and Environmental chemistry. Prof. Madkour is serving in different positions in Egypt, Republic of Yemen, Kuwait and KINGDOM OF SAUDI ARABIA. Prof. Loutfy. H.

Madkour joined now again from 18 Sept 2010 as Professor for Physical and Electro

analytical Chemistry. at Chemistry Department, Faculty of Science KING

ABDULAZIZ UNIVERSITY P.O. Box 80203 Jeddah 21589 KINGDOM OF SAUDI ARABIA.

Scholarly Contributions [Data Provided by ]

1. Inhibition effect of Schiff base compounds on the corrosion of iron in nitric acid and sodium hydroxide solutions

Journal of Corrosion Science and Engineering, vol. 13, 2010

2. Inhibition effect of hydantoin compounds on the corrosion of iron in nitric and sulfuric acid solutions

Monatshefte fur Chemie, vol. 132, no. 2, pp. 245–258, 2001

3. Kinetics of substituted bis- and mono-azo dyes as corrosion inhibitors for

aluminium in hydrochloric acid and sodium hydroxide solutions Journal of Chemical Research - Part S, no. 7, pp. 408–409, 1999

4. Electrochemical Behaviour of 3-Arylazo-1,2,4-triazole Compounds in Aqueous

Buffered Solutions

Journal of Chemical Research - Part S, no. 9, pp. 514–515, 1998

5. Inhibition of the acid corrosion of iron with haloacetic acids Bulletin of Electrochemistry, vol. 13, no. 2, pp. 62–66, 1997

6. Inhibition of the corrosion of 16/14 austenitic stainless steel by oxygen and

nitrogen containing compounds

Bulletin of Electrochemistry, vol. 13, no. 1, pp. 1–7, 1997

7. Thermodynamic behaviour of complex antimonite ore for electrodeposition of

metal value

Journal de Chimie Physique et de Physico-Chimie Biologique, vol. 94, no. 3,

pp. 620–634, 1997

8. Electrolytic recovery of antimony from natural stibnite ore

Hydrometallurgy, vol. 43, no. 1-3, pp. 265–275, 1996

Page 8: C.V.Eng.& Arabic

8

9. Thermo-physical studies on ilmenite ore for mass production of ceramic

capacitors

Erzmetall: Journal for Exploration, Mining and Metallurgy, vol. 49, no. 5, pp.

309–313, 1996

10. Electrodeposition of lead and its dioxide from Egyptial carbonate ore

residuum

Bulletin of Electrochemistry, vol. 12, no. 3-4, pp. 234–236, 1996

11. Electrolytic separation of lead and its dioxide from carbonate ore residiuum

Indian Journal of Chemical Technology, vol. 2, no. 6, pp. 343–344, 1995

12. Inhibition of copper corrosion by arylazotriazoles in nitric acid solution

Monatshefte für Chemie Chemical Monthly, vol. 126, no. 10, pp. 1087–1095, 1995

13. HYDRO- AND ELECTROMETALLURGY TREATMENT OF CASSITERITES (

greater than S%NO//2 CONCENTRATE.

Aufbereitungs-Technik, vol. 29, no. 5, pp. 273–281, 1988

14. THERMODYNAMIC STUDIES ON SULPHATE ROASTING FOR ZINC ELECTROWINNING FROM CARBONATE ORE.

Journal of Chemical Technology and Biotechnology, vol. 36, no. 5, pp. 197–

211, 1986

15. HYDROMETALLURGICAL AND ELECTROMETALLURGICAL TREATMENT OF CASSITERITE CONCENTRATE.

Erzmetall: Journal for Exploration, Mining and Metallurgy, vol. 39, no. 4, pp.

162–167, 1986

16. Electrodeposition of titanium and its dioxide from ilmenite Journal of Electroanalytical Chemistry, vol. 199, no. 1, pp. 207–210, 1986

17. RECOMMENDED FLOWSHEETS FOR THE ELECTROLYTIC EXTRACTION OF

LEAD AND ZINC FROM RED SEA POLYMETAL ORE.

Journal of chemical technology and biotechnology. Chemical technology, vol. 35 A, no. 3, pp. 108–114, 1985

18. POLAROGRAPHIC REDUCTION OF SOME ARYLIDENE DERIVATIVES OF

OXALIC HYDRAZIDE IN BUFFER SOLUTIONS OF VARYING pH.

Electrochemical Society Extended Abstracts, vol. 85-1, pp. 754–755, 1985

19. ELECTROCHEMICAL REDUCTION OF SOME ARYLIDENE DERIVATIVES OF SALICYLIC, OXALIC, SUCCINIC AND METHYL ( 2-HYDROXY PHENIDENE )-

BENZOIC HYDRAZIDES IN NONAQUEOUS MEDIUM AT A MERCURY CATHODE.

Electrochemical Society Extended Abstracts, vol. 85-1, pp. 753, 1985

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Copyright © 2010 - 2011 Elsevier B.V. All rights reserved. Scopus ® is a registered trademark of Elsevier B.V.

Prof. Dr. Loutfy Hamid Madkour Chemistry Department, Faculty of Science, King Abdul-Aziz University P.O. Box

80203, Jeddah 21589, Kingdom of Saudi Arabia (KSA).

Scopus Author Identifier: 6701732721

E-mail: [email protected]

[email protected]

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Prof. Dr. Loutfy Hamid Aly MADKOUR

Short Vitae : Scopus Author Identifier : 6701732721

Prof. Loutfy H. Madkour graduated as B. Sc. Chem. in 1972 at Cairo University and as M.Sc.

Electrometallurgy at Menia University in 1979. In 1982 He obtained his Ph.D.in electro-chemistry at Tanta

University. Prof. Dr. Madkour, s special research interests are : physical chemistry, electrochemistry,

electrometallurgy, electro analytical chemistry, analytical chemistry, polarography, electrolytic extraction of

heavy metals from natural ores and deposits, electrochemical thermodynamics, and environmental chemistry.

Prof. Madkour is serving in different positions in Egypt, Kuwait, Sana’a University at Republic of Yemen and

Kingdom of Saudi Arabia. Prof. L. H. Madkour joined now at Chemistry Department, Faculty of Science at

King Abdul-Aziz University P.O .Box 80203 Jeddah 21589 as Professor for Physical and Electro analytical

chemistry.

My website is :

istrationId=HGHCIJPCIIHKPHLHJGICHOIIHPMHLMPGHYJhttp://syndic8.scopus.com/getMessage?reg

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CURRICULUM VITAE:

Professor Dr. Loutfy Hamid Madkour

Scopus Author Identifier: 6701732721

Professor of Physical and Electro analytical Chemistry at Chemistry Department, Faculty of Science, Tanta

University, 31527, Tanta, Egypt .

My address now : **Chemistry Department, Faculty of Science, King Abdul-Aziz University P.O. Box 80203, Jeddah

21589,Kingdom of Saudi Arabia(KSA)

(1)Personal Data

(2)Scientific Qualifications

(3)Scientific Activities

(4)Academic Appointments (Egypt)

(5)Academic Appointments (Abroad)

(6) Scientific Certificates

(7) Conferences and Meetings

(8) Publications

(9) Books and Seminars

(10) How to Contact?

(1) Personal Data:

Name :Prof. Loutfy Hamid Aly Madkour

Page 12: C.V.Eng.& Arabic

12

Nationality : Egyptian

(2) Scientific Qualifications :

(1)B Sc. Chemistry, Cairo University, Egypt, (1972)

(2)Ma Sc. Physical Chemistry, Mania University, Egypt, (1979)

(3)Ph.D. Physical Chemistry (Electro analytical Chemistry), Tanta University, Egypt, (1982)

(3) Scientific Activities :

(1) Reviewer: of Journal Industrial and Engineering Chemistry Research, Published by the American

Chemical Society (A C S)

(2)Member: of American Association for the Advancement of Science (AAAS)

(3)Member: of Egyptian Corrosion Bulletin

(4) Academic Appointments (Egypt) :

Chemistry Department, Faculty of Science, Tanta University, 31527, Tanta, Egypt.

(1) Demonstrator from: (Nov.21, 1974 - Nov.4, 1979)

(2) Assist. Lecturer from: (Nov.5, 1979 - April 26, 1983)

(3) Lecturer of Physical Chemistry from: (April 27, 1983-May 24, 1987)

(4) Associate Prof. of Physical Chemistry from: (May 25, 1987- June 28, 1999)

(5) Professor of Physical Chemistry from: (June 29, 1999 till Now)

(5) Academic Appointments (Abroad) :

(1)Chemistry Department, College of Basic Education P.O.Box:34053, KUWAIT from (1987- 1993), as:

Associate Prof. of Physical Chemistry .

(2)Chemistry Department, Faculty of Science, King Abdul Aziz University Medina Mounwara, P O Box: 344,

Kingdom of Saudi Arabia (KSA) as Professor of Physical Chemistry from: (2001- 2003).

(3)Chemistry Department, Faculty of Science, Sana’a University, P O Box: 13499, Yemen Republic; as

Professor of Physical Chemistry: from: (Sept. 2006 till July 2009).

(4)Chemistry Department, Faculty of Sciences and Arts, King Abdul Aziz University, P.O. Box 80207 Jeddah

21589, Kingdom of Saudi Arabia (KSA) as Professor of Physical Chemistry from Sept.2009 till now.

(6) Scientific Certificates :

(1) Master Degree in “Physical Chemistry”

{Electrochemistry} entitled:

Page 13: C.V.Eng.& Arabic

13

Ma Sc. Thesis: “Extraction of Copper, Lead, and Zinc Metals from Umm-Smoky Deposit Ore, Eastern Desert

by Electro-Metallurgical Methods”.

(2)Doctor Degree in “Physical Chemistry” {Electrochemistry} entitled:

Ph. D. Thesis:” Polar graphic and Electro analytical Studies on Some Organic Compounds Containing the

Reducible Centers C = N, N - N, C -N”.

(7) Conferences and Meetings :

I enclose a list of sharing in [13] “thirteen” International Conferences by submitting (oral and poster) my

research publications, from (1984 till 2008) in Egypt and abroad in the field of Physical Chemistry,

Electrochemistry, Electro analytical Chemistry, and its applications in industry

(8) Publications :

I published more than [50] “fifty” publication in different fields of Physical and Electro analytical

Chemistry in many of International Journals, printed in: (UK, Germany, France, Austria, USA, India,

Hungary, Korea and Egypt).

I enclose the list of my publication.

(9) Books and Seminars :

I- Books:

(1) .Book: “Practical and Applied Chemistry”, published by: The Public Authority for Applied Education

and Training, Kuwait, first edition (1993).

(2).Book: “Introduction of General Chemistry” published by: The Public Authority for Applied Education

and Training, Kuwait, first edition (1988).

II- Seminars:

● Seminar on: “Technology of Extractive Metallurgy of Heavy Metals from Natural Ores and

Deposits" at Chemistry Department, Faculty of Science, King Abdul Aziz University, Medina

Mounwara, Kingdom of Saudi Arabia, date: (Feb. 20, 2002)

● Seminar on: “Types of Corrosion and Methods of Corrosion Protection for Metals and

Alloys” at Chemistry Department, Faculty of Science, Tanta University, date :( March, 13, 2006)

(10) How to Contact ?

(1) Chemistry Department, Faculty of Science, King Abdul Aziz University. P.O. Box 80203, Jeddah 21589,

Kingdom of Saudi Arabia.

(2) Faculty of Science, Chemistry Department, Tanta University, 31527, Tanta, Egypt.

(2).Phone : 002-040/3319895 , 0020104710946, 0020100216135 (Tanta- Egypt)

: 002-03/5362231 (Alex.-Egypt)

: 00966/026400000/64423 , Mobile:0560682579 (Kingdom of Saudi Arabia)

:Fax: 026952292 P.O. Box 80203 Jeddah 21589

Page 14: C.V.Eng.& Arabic

14

(3).E-mail : [email protected]

: [email protected]

(4).Website :

http://syndic8.scopus.com/getMessage?registrationId=HGHCIJPCIIHKPHLHJGICHOIIHPMHLMPGHYJ

QWNNJJJ

http://www.google.com/profiles/117418238982110812610

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essage%3FregistrationId%3DHGHCIJPCIIHKPHLHJGICHOIIHPMHLMPGHYJQWNNJJJ

hared/06171069775297846234?chttp://www.google.com/reader/s

-http://www.scopus.com/results/results.url?sort=plf

-K0ALo0_cR3g98VH4S_FYzR:560&sot=aut&sdt=a&sl=18&s=AUf&src=s&sid=U

ID+(6701732721)&origin=rssreader

hindawi.com/81910424.html-http://www.sage

http://www.hindawi.com/81910424.html

http://www.kau.edu.sa/Default.aspx?Site_ID=0055595&lng=AR

http://www.kau.edu.sa/Files/0055595/Researches/56721_27009.html

http://www.refdoc.fr/Noticeresultat?NoticeresultatnbPageP=1

http://www.refdoc.fr/Noticeresultat?NoticeresultatnbPageP=2

2721http://www.scopus.com/authid/detail.url?authorId=670173

Scopus Author Identifier : 6701732721

List of Publications Presented By:

Prof. Dr. Loutfy Hamid Madkour

* Chemistry Department, Faculty of Science, Tanta University, 31527, Tanta, Egypt.

My address now is :

**Chemistry Department, Faculty of Science, King Abdul-Aziz University P.O. Box 80203, Jeddah 21589,

Kingdom of Saudi Arabia (KSA)

[1] Treatment of Umm - Samiuki Complex. F. Taha, S. E. Afifi and L.H. Madkour.

J.Tabbin Institute for Metallurgical Studies (T.I.M.S.), (1982), No.47, pp. 1-19

Page 15: C.V.Eng.& Arabic

15

[2] Electrolytic Deposition of Metal Values from Umm - Samiuki Poly sulphide Ore.

(I) Flow sheets for the Assessment of Copper, Lead and Zinc S.E. Afifi, F.Taha and L.H. Madkour.

Egypt. J. Chem., (1984), 27, No.3, pp.275 - 282.

[3] Electrolytic Separation of Metal Values from Umm - Smoke Poly sulphide Ore.

(II) On the Optimum Conditions and Efficiency of Separation Processes. S.E. Afifi, F. Taha and L.H.

Madkour, Egypt. J. Chem., (1984), 27, No.3, pp. 283-296.

[4] Electrochemical Reduction of Some Arylidene Derivatives of Salicylic, Oxalic, Succinic and Methyl (2-

Hydroxy Phenidene) - Benzoic Hydrazides in Non-Aqueous Medium at a Mercury Cathode. M. M. Ghoneim

R. M. Issa and L. H. Madkour. 167th The Electrochemical Society Meeting - Toronto, Ontario,

Canada, May 12-17, (1985), p. 753.

[5] The Polargraphic Reduction of Some Arylidene Derivatives of Oxalic Hydrazide in Buffer Solutions of

varying pH. R. M. Issa, M. M. Ghoneim, H.Y.F. El-Brady and L. H. Madkour. 167th The

Electrochemical Society Meeting - Toronto, Ontario, Canada, May 12-17, (1985), pp. 754-755.

[6] Electro reduction of Bis- Benzylidene Succinic Hydrazide Derivatives at the DME in Buffer Solutions.

H. Y. El-Baradie M. M. Ghoneim, R. M.Issa and L. H. Madkour. Bulletin of Electrochemistry 3 (1)

January-February (1987), pp. 23-27.

[7] The Electro reduction of Some Arylidene Derivatives of Salicylic Hydrazide in Buffer Solutions. R.M.

Issa, H.Y.F. El-Baradie, Y.A. El-Awady and L. H. Madkour. Pakistan Journal of Scientific and

Industrial Research (1988).

[8] The effect of some -Diketo Compounds on the Corrosion of Zinc in Hydrochloric Acid Solution. A. S.

Fouda, A. H. Elasklany and L. H. Madkour. J. Indian Chem. Soc., (1984), 61, pp. 425-429.

[9] Recommended Flow sheets for the Electrolytic Extraction of Lead and Zinc from Red Sea Poly metal Ore.

Loutfy H. Madkour. J. Chem. Tech. Biotechnology, (1985), 35A, pp. 108-114. 12th Egyptian

Chemical Conference, Cairo, 7-10 April, (1984), pp. 28-29.

http://www3.interscience.wiley.com/journal/114273969/abstract

[10] Thermodynamic Studies on Soleplate Roasting for Zinc Electro winning from the Carbonate Ore.

Loutfy H. Madkour. J. Chem. Tech. Biotechnology, (1985), 36, pp. 197-211.

http://www3.interscience.wiley.com/journal/114217967/abstract

[11] Electrode position of Titanium and Its Dioxide from Ilmenite. L. H. Madkour and A.S. Fouda. J.

Page 16: C.V.Eng.& Arabic

16

Electro anal. Chem., 199 (1986) 207-210.

http://cat.inist.fr/?aModele=afficheN&cpsidt=8717161

[12] Hydrometallurgical and Electrometallurgical Treatment of Cassiterite Concentrate. Loutfy H.

Madkour J. Erzmetall (1986), 39 (4), 162-167.

[13] Correlation between Effectiveness of Aliphatic Amines as Corrosion Inhibitors and Electron Density

Calculations. A.S. Fouda, L. H. Madkour and M.S.Soliman. BULLETIN DE LA SOCIETE

CHIMIQUE DE FRANCE (1986) No3, 358-360.

[14] Electro-deposition of Tin from Tinstone Ore. A. S. Fouda, L. H. Madkour and M.E.Khalifa.

BULLETIN DE LA SOCIETE CHIMIQUE DE FRANCE (1986) No4, 504-506.

[15] Inhibitive Action of some Amines and Hydrazine’s towards Corrosion of Zinc in Tri cholera acetic Acid

Solution. A. S. Fouda and L. H. Madkour. BULLETIN DE LA SOCIETE CHIMIQUE DE FRANCE

(1986) No5, 745-749.

[16] Estimation of Inorganic Phosphate in Tissue Proteins Spectrophoto-metrically. Loutfy H. Madkour

Oriental J. Chem. Vol. 2, (2), (1986). The First Chemical Conference, Alexandria, 28-30 April, (1985), p.4.

[17] Critical Micelle Concentrations of Hexadecyl trim ethyl ammonium Chloride in Water in the

Temperature Range 25-160 oC. A. S. Fouda, L. H. Madkour and D.F.Evans. Indian Journal of

Chemistry, Vol. 25A, December (1986), pp.1102-1104.

[18] The Inhibition of the Dissolution of Aluminum in Hydrochloric Acid by Some Biacetylmonoxime

Hydrazones. A. S. Fouda, A. H., L. H. Madkour and K. M. Ibrahim. Acta Chimica Hungarian

124(3), pp. 377-385 (1987).

[19] Adsorption of Some Aliphatic Carbonyl Compounds on Aluminum from Acidic Chloride Solution. L. H.

Madkour, A.S. Fouda and H.A. Mustafa Oriental J. Chem., Vol. 3, (1), (1987).

[20] Polar graphic Reduction of 4-Arylazo -l-Phenyl Parasol 3, 5 Dionne and Some of Its Derivatives in

Aqueous Ethanol Buffers. M. M. Ghoneim, R. M. Issa, L. H. Madkour and E. Hammam. The First

Chemical Conference, Alexandria, 28-30 April, 1985. p.128. Journal of the Electrochemical Society Vol.

134, No.3, March (1987).

[21] Reuse of Scrap Brass for the Production of Standard Bronze Alloy. M. A.A. Mustafa, A. M. Ramadan,

F.El-Sayed and L. H. Madkour. Proc. 1st Chem. Conf., Fact. Sci., Mans. Univ., Sept. 24-26 (1986),

Page 17: C.V.Eng.& Arabic

17

pp. 63-70.

[22] Electrode position of Indium. A.S. Fouda, L.H. Madkour and A.I. Ahmed BULLETIN DE LA

SOCIETE CHIMIQUE DE FRANCE (1987), No. 2, 270-272.

[23] Electro reduction of 4-arylhydrazono-1-phenyl-pyrazolidin-3,5-diones in

20% ethanolic buffers at mercury electrode.

R. M. Issa, M.M. Ghoneim, M.A. El-Morsi, L.H. Madkour, E. Hammam.

J. Electrochemical Soc., 134 (3), 140C (1987).

[24] Hydro- and Electrometallurgical Treatment of SnO2. Loutfy H. Madkour J.

AUFBEREITUNGS-TECHNIK-Nr. 5 (1988), 273 - 281. http://www.immage.org/abstract.asp?Line=37682

[25] Synthesis and Characterization of 2, 2`-biimidazole Complexes of Oxo-cations of Molybdenum (VI, V)

and Uranium (VI). S. S. Kandil and Loutfy H. Madkour. Journal Spectroscopy Letters, 26 (3),

535-550 (1993).

[26] Electrolytic Spa ration of Lead and Its Dioxide. Loutfy H. Madkour, Indian Journal of Chemical

Technology. Vol. 2, November (1995), 343.

[27] Electrolytic Extraction of Uranium from Egyptian Phosphorus’s. Loutfy H. Madkour. J.

ERZMETALL 48 (1995) Nr. 2, 104-109.

[28] Inhibition of Copper Corrosion by Arylazotriazoles in Nitric Acid Solution. L. H. Madkour, M.A.

Elmorsi and M. M. Ghoneim. J. Monatshefte für Chemie 126: 1087-1095 (1995).

http://www.springerlink.com/content/khw270200422j341/

[29] Inhibitory Effect of Some Carbazides on Corrosion of Aluminum in Hydrochloric Acid and Sodium

Hydroxide Solutions. A. S. Fouda, L.H. Madkour, A. A. Elshafei and A. H. Elasklany. J. Mat.-wiss.u.

Werkstofftech. 26, 342 - 346 (1995).

http://www3.interscience.wiley.com/journal/109622110/abstract?CRETRY=1&SRETRY=0

[30] Corrosion Inhibitors for Zinc in 2 M HCl Solution. A. S. Fouda, L. H. Madkour, A.A. El-Shafei and

S.A. Abd El-Maksoud. Bulletin Korean Chemical Society (1995), Vol. 16, No. 5, pp. 454-458.

Page 18: C.V.Eng.& Arabic

18

[31] Inhibition of the Acid Corrosion of Copper with Some Azoheterocyclic Dyes. L. H. Madkour, M. M.

Gonium and I.H. El-Shamy. 5th Bin Sina International Conference On Pure and Applied Heterocyclic

Chemistry-An-Shams University, Cairo, Egypt, 9-12 December, 202, (1995).

[32] Electrode position of Lead and Its Dioxide from Egyptian Carbonate Ore Residuum. Loutfy H.

Madkour. Bulletin of Electrochemistry 12 (3-4) (1996), pp. 234 - 236.

[33] Electrolytic Recovery of Antimony from Natural Stibnite Ore. Loutfy H. Madkour and Ibrahim A.

Salem. J. Hydrometallurgy 43 (1996) 265 - 275.

http://www.sciencedirect.com/science?_ob=ArticleURL&_udi=B6VBT-3SVJ8N1-

N&_user=10&_coverDate=11%2F30%2F1996&_rdoc=1&_fmt=high&_orig=search&_sort=d&_docanch

or=&view=c&_searchStrId=1224843903&_rerunOrigin=google&_acct=C000050221&_version=1&_urlVe

rsion=0&_userid=10&md5=a3298de7832b161c7f47a49adb7b0c3f

[34] Thermo-physical Studies on Ilmenite Ore for Mass Production of Ceramic Capacitors. L. H.

Madkour, M. M. Abou-Sekkina and O. M. Hemeda. J. ERZMETALL 49 (1996) Nr. 5, 309-313.

http://d.wanfangdata.com.cn/NSTLQK_NSTL_QK11490547.aspx

[35] Thermodynamic Behavior of Complex Antimonite Ore for Electrode position of Metal Value. Loutfy

H. Madkour. Journal de Chime Physique (1997) 94, 620 - 634. © Elsevier, Paris.

[36] Inhibition of the Corrosion of 16/14 Austenitic Stainless Steel by Oxygen and Nitrogen Containing

Compounds. L. H. Madkour and M.M. Ghoneim. Bulletin of Electrochemistry 13 (1) (1997), pp. 1 -

7.

[37] Inhibition of the Acid Corrosion of Iron with Halo acetic Acids. A. S. El-Gaber, L.H. Madkour, A.H.

El-Asklany and A. S. Fouda. Bulletin of Electrochemistry 13 (2) (1997), pp. 62 - 66.

[38] Electrochemical Behavior of 3-Arylazo-1, 2, 4-triazole (AAT) compounds in Aqueous Buffered Solutions.

Loutfy H. Madkour. Journal of Chemical Research (S), (1998), 514 - 515. Journal of Chemical

Research (M), (1998), Vol. 9 (September), 2301 - 2320.

[39] Electrochemical Behavior of Nickel Dissolution in Acidic Nitrate and Chloride Solutions. Loutfy H.

Page 19: C.V.Eng.& Arabic

19

Madkour. Envoi. & Soc. Journal (Chemistry Administration) Vol. 1, Page 213 - 231 (1998). The First

International Conference on the Role of Chemistry Administration for Attending Environment and

Society, Cairo, 15 - 17 December 1998, Egypt.

http://www.rsc.org/delivery/_ArticleLinking/DisplayArticleForFree.cfm?doi=a800519b&JournalCode=JC

[40] Kinetics of the Substituted Bis- and Mono- Azo dyes as Corrosion Inhibitors for Aluminum in

Hydrochloric Acid and Sodium Hydroxide Solutions. Loutfy H. Madkour, R. M. Issa and I.M. El-

Ghrabawy. Journal of Chemical Research (S), (1999), 408 - 409. Journal of Chemical Research (M),

(1999), 1701 - 1726.

http://www.rsc.org/delivery/_ArticleLinking/DisplayArticleForFree.cfm?doi=a805608k&JournalCode=JC

[41] Inhibition of the Corrosion of Iron by Hydantoin Compounds in Acidic Media Loutfy H.

Madkour, A.M. Hassanein, M.M. Ghoneim and S.A. Eid. 18th Annual Conference CORROSION

PROBLEMS IN INDUSTRY, Ismailia, Egypt - Egyptian Corrosion Society (ECS), November 23 - 25, (1999).

Volume I (12), 1-14.

http://resources.metapress.com/pdf-preview.axd?code=frvmc8v14dn55l98&size=largest

[42] Corrosion Inhibitors for Iron in Sodium Hydroxide Solution. M.M. Ghoneim, Loutfy H.

Madkour, A.M. Hassanein and S.A. Aid. 18 th Annual Conference CORROSION PROBLEMS IN

INDUSTRY, Ismailia, Egypt - Egyptian Corrosion Society (ECS), November. 23 - 25, (1999). Volume II (6), 1-

15.

[43] Inhibition Effect of Hydantoin Compounds on the Corrosion of Iron in Nitric and Sulphuric Acid

Solutions. Loutfy H. Madkour, A. M. Hassanein, M. M. Ghoneim and S. A. Eid. J. Monatschefte

für Chemie, 132, 245-258, (2001).

[44] Inhibition Effect of Schiff Base Compounds on the Corrosion of Iron in Nitric Acid and Sodium

Hydroxide Solutions. Loutfy H. Madkour, R.M. Issa and U.A. Zinhome, The Third International

Page 20: C.V.Eng.& Arabic

21

Conference on Electrochemistry and Its Applications (ICE-3), Luxor, 13-15 February, (2001).

[45] Inhibitory Effect of Some Substituted Mono- and Bis- Azo dyes on Corrosion of Copper in Acidic and

Alkaline Solutions. Loutfy H. Madkour, R. M. Issa and U.A. Zinhome, the Fourth International

Conference on Electrochemistry, 16-19 February, (2004) Aswan, South Valley University, Egypt.

[46] Investigation of the Inhibiting Action of Some Substituted Azo Molecules on the Corrosion of Iron in Nitric

Acid and Sodium Hydroxide Solutions. Loutfy H. Madkour, R. M. Issa and U.A. Zinhome, The Fifth

International Conference on Electrochemistry (ICEV), (2006), Luxor, Egypt. Journal of Applied

Electrochemistry (2010),in press.

[47] Examples of Recent Successful Applications of New Electroplating technology for the Non-Conducting

Materials, Loutfy H. Madkour and R. H.Al-Bendary,

The Fifth International Conference on Electrochemistry (ICEV), (2006), Luxor, Egypt.

[48] Semiconductivity Behaviour of Egyptian Natural Sintered Ore For Thermo technological Applications.

Loutfy H. Madkour. The Second International Conference on Basic Sciences and Advanced Technology

(BSAT-II), Assiut, Egypt, November 5-8, (2000).

Journal of the University of Chemical Technology and Metallurgy (UCTM), 45, 3, 335-346, (2010).

http://www.uctm.edu/journal/j2010-3/14_Madkour_335-345.pdf

[49]INHIBITION EFFECT OF SCHIFF BASE COMPOUNDS ON THE CORROSION OF IRON IN

NITRIC ACID AND SODIUM HYDROXIDE SOLUTIONS

Loutfy H. Madkour and U.A. Zinhome

Journal of Corrosion Science and Engineering, Volume 13 (2010).

Page 21: C.V.Eng.& Arabic

21

انغـــــــــــــشج انزاذــــــــح

نطـــــــف حـــايذ ػه يذكـــــىس/ د . أ :االعى

يصــــــــش : انجغــــــــــح

كــــاء كهشتح ، ذآكم انفهضاخ وانغثائك ، وكاء انرؼذ )أعرار كـــاء فضائح : انىظفح انحانح

تمغى انكــاء ، كهح انؼهىو ، فشع ( انهذسويرانىسجا وانثشويرانىسجا وكاذكح انرفاػالخ وانرحهم انكـــائ ان تاعرخذاو انطشق انكهشتح

.انهكح انؼشتح انغؼىدح 21589جـــذج 80203:ب.هك ػثذ انؼضض ،صشال جذج ، جايؼح ان

انىظفح تجهىسح يصـــش انؼشتح : أعرار انكـــــاء انفضائح وانرحههح – لغى انكـــاء – كهح انؼهـــــــىو – جــايؼــح طـــطــــا –

.يصــــــش –ططــا 31527:سيض تشذ

(جهىسح يصش انؼشتح) 002\0104710946: ، جىال002\0100216135:، جىال 02\040\3319895:ذهفى

(انهكح انؼشتح انغؼىدح) 0560682579 : جىال : 02/6400000/64423 /00966 ،فاكظ:6952292 02 ,

[email protected] : تشذ إنكرشو

[email protected]

Scopus Author Identifier: 6701732721

My website:

http://syndic8.scopus.com/getMessage?registrationId=HGHCIJPCIIHKPHLHJGICHOIIHPMHLMPGHYJQWNNJJ

J

http://www.google.com/profiles/117418238982110812610

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essage%3FregistrationId%3DHGHCIJPCIIHKPHLHJGICHOIIHPMHLMPGHYJQWNNJJJ

hared/06171069775297846234?chttp://www.google.com/reader/s

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-K0ALo0_cR3g98VH4S_FYzR:560&sot=aut&sdt=a&sl=18&s=AUf&src=s&sid=U

ID+(6701732721)&origin=rssreader

hindawi.com/81910424.html-http://www.sage

http://www.hindawi.com/81910424.html

http://www.kau.edu.sa/Default.aspx?Site_ID=0055595&lng=AR

http://www.kau.edu.sa/Files/0055595/Researches/56721_27009.html

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2721http://www.scopus.com/authid/detail.url?authorId=670173

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22

المإهالت العلمـــــة :

".جــد جدا" بتقدر عام كلة العلـــــــوم–من جــامعة القـــاهرة . م1972درجة بكالوروس العــلوم ف تخصص كمـــــاء خاصة دور ونو ( 1) ( .موافقة مجلس جامعة المنـــــا .)م24/7/1979: درجة المـاجســــتر ف العــلوم ف الكماء الفزائة بتارخ( 2) ( .طـــنطــــــا موافقة مجلس جـــامعـــة . )م27/10/1982:درجة الدكتوراه ف العــــــــلوم ف تخصص الكمـــــــاء الفزائة بتارخ( 3)

الخبرة األكـــادمــــة العملـــة التدرســــــة :

.م21/11/1974:جـــامعـــة المنــــا من تارخ –معــــد بقســــــــم الكمــــــــاء بكلــــــة العـــلوم ( 1)

: جــــامعــــة طــنطــــا من تارخ –نقل إل مثل وظفته كمعـــد بقســـــم الكمــــــــاء بكلة العــــــلوم ( 2) .م14/6/1979 م5/11/1979: :جـــامعة طـــنطـــا من تارخ –مدرس مســــــاعـــد بقســــــــم الكمــــــاء بكلة العـــلوم ( 3) .م27/4/1983: جـــامعة طــــنطــــا من تارخ –ور بقســــــم الكمــــــاء بكلة العـــلوم مدرس دكت(4) .م25/5/1987: جــامعة طــنطـــا من تارخ –أســـــــتاذ مســـــاعـــد بقســــــــــم الكماء بكلة العـــلوم (5) بجــــامعــــة " كمـــــــاء كهـــــــربة"تخصص دقق " كمـــــــــــاء فزائة"ـة العـــــــلوم تخصص أســــــــتاذ بقســــــــم الكمـــــاء بكلـــ(6)

.وحتى اآلن . م29/6/1999: طــــنطــــا من تارخ

اإلعارة والسفرات للتدرس خارج جمهورة مصر العربة:

.م15/9/1990إل .م1/10/1987: بكلة التربة بدولة الكوت من تارخ( أســـــتاذ مســـــــاعـــــد )للتدرس إعارة(1) .م15/9/1993إل . م16/9/1991: بكلة التربة بدولة الكوت من تارخ( أســتاذ مســـــاعــــد )استكمال اإلعارة (2) : المملكة العربة الســــــعودة من تارخ, فرع المدنة المنورة -كلة العلــــــوم -لملك عبد العززبجامعة ا( أســـــــتاذ )إعارة للتدرس (3).م6/9/2003إل . م1/9/2001 الجمهورة المنـــــة من, كلة العلــــــــــوم –بجــــامعة صنعــــــــاء ( أســـــــــتاذ )إعــــــارة للتدرس (4)

.م28/7/2009إل . م20/9/2006: تارخ المملكة العربة السعـــــــــــودة من , فرع شمال جدة –كلة العلـــــــــوم –بجــــــامعة الملك عبد العزز ( أســــــــــتاذ )إعــــــــارة للتدرس (5)

.وحتى اآلن . م26/9/2009هـ الموافق 7/10/1430: تارخ

االهتمامات البحثة والنشاطات العلمة:

عة ف مجال نشاط العلم البحث تركز ف العمل األكادم ونشر األبحاث العلمة ف فروع الكماء الفزائة المختلفة وتطبقاتهـا الصنا

الكهرب والبوالروجرافا وكماء البئة والكماء التحللة وكماء التحلل , الكماء الكهربة والكهرومتالورجا والكماء الكناتكة.واالستخالص والترسب الكهرب للفلزات الثقلة من خاماتها ورواسبها الطبعة

:التحكم وعضـــــــــوة الجمعات العلمة الدولة .الجمعة الكمائة األمركة -الناشر –محكم ف مجلة الصناعة وهندسة بحوث الكمـــــــاء ( 1) . معة األمركة لشركاء تقدم العلومعضو ف الج( 2) .عضو ف الجمعة الكمائة المصــــــرة ( 3) .عضو ف جمعــــــــة التآكل المصــــــــــرة ( 4)

األبحـــــــــاث المنشــــــــورة ف المجالت والدورات العلمة الكمائة العالمة :

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23

بحثــــا تخصصا ف مجال فروع تخصصات الكمـــاء الفزائة وتطبقاتها وذلك ف الكماء الكهربة والكماء تم نشـــــــر أكثر من خمســــــون

كبات الحرارة والكماء الكناتكة ومجال استخالص الفلزات وترسبها كهربا من الخامات الطبعة ودراسة تآكل الفلزات والسبائك والمترا, أمركا, فرنســـا, إنجلترا -الناشر –وذلك ف المجالت والدورات العلمة الكمائة التخصصة العالمة , والبوالروجراف والتوصلة الكهربة

.البرتغال ، مصـــــــر , الصن, ألمــــانا, الهند, المجر, كورا, كندا نشـــاطات المإتمرات العلمة الدولة :

لم المشاركة بإلقـــــاء عشــــــــرون بحثــــا تخصصا ف فروع الكماء الفزائة وتطبقاتها وذلك من خالل حضور ثالثة عشر مإتمر ع تم

.عالم

تؤلف الكتب ف الكمــــــــــاء :

"الكمـــــــــــاء العملــــــــة والتطبقـــــــة : " كتاب

.صفحة من الحجم الكبر وحتوي عل خمسة أبواب باإلضافة إل مقدمــــة 565قع الكتاب ف

.م1993الطبعة األول , الهئة العــــامة للتعلم التطبق والتدرب، الكوت, دولة الكوت: الناشــــر

الدورات والبرامج التدربــــــة:

موزعة بن الجامعـــات المصـــرة وجامعات صنعـــــاء وعمران والحددة وذمار بالجمهورة تم اجتاز ثالثة وعشــــرون دورة وبرنامج تدرب . ش العمل الالحقة ألسبوع البحث العلم بجامعة الملك عبد العزز، وحضور ور المنة بالتعـــــاون مع جامعة مست رخت الهولندة

اإلشـــــــراف عل الرســــائل العلمــــــة وعضــوة لجــــان التحكم :

آسا /للطالبة. م2006وكنت ممتحنا لرسالة الدكتوراه عـــام , قمت باإلشــــــراف عل عشـــــــرة رســـــائل مـاجستــــر و أربعــــة رسائل دكتوراه.كة بقسم الكمـــاء بكلة العـــلوم بجامعة صنعــــــاء بالجمهورة المنــــــــة الضب ف تخصص الكماء الكنات عبد هللا

.باإلضــــافة إل أنن أشــــــارك ف فحص وتحكم اإلنتاج العلم المقدم من أعضـــاء هئة التدرس للجان الدائمة للترقــــــة

بإلقاء أبحاث كمائه حامد على مدكور لطف/ الدكتور األستاذالت شارك فها العالمة المإتمرات العالمة

اآلل بالطرق والتحلل وتآكل الفلزات وكماء التعدن الفزائةفروع الكماء فمجال تخصصه فتخصصه

. المختلفةالصناعات فوتطبقـــــات الكمــــــاء الكهربة

.و2006فثشاش 16-13األلصــــش -انؤذش انذون انخــــايــظ ف انكـــــاء انكهــشتح ( 1)

[1] The Fifth International Conference on Electrochemistry (ICE V), 13-16 February, 2006,

Luxor, Egypt. Organized by South Valley University.

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24

(i) Examples of Recent Successful Applications of New Electroplating Technology for the Non-

Conducting Materials

(ii) Investigation of the Inhibiting Action of Some Substituted Azo Molecules on the

Corrosion of Iron in Nitric Acid and Sodium Hydroxide Solutions.

.و2004فثشاش 19-16أعىا -انكاء انكهشتح ف شاتغأن انذونانؤذش (2)

[2] The Fourth International Conference on Electrochemistry, 16-19 February, 2004, Aswan, Egypt.

''Inhibitory Effect of Some Substituted Mono- and Bis- Azo dyes on Corrosion of Copper in Acidic and

Alkaline Solutions''.

م2002فبرار 4-2ـ كلة العلوم ببن سوف " االتجاهات الحدثة ف الكماء وتطبقاتها"المإتمر الدول األول عن ( 3)

[3] The First International Conference on "New Trends in Chemistry and their Applications"

(NTCA 1) Cairo University, Beni-Suef, Egypt, February 2- 4, 2002. ''Inhibition of Copper Corrosion

by Mono-and Bis-Azo dyes in Nitric Acid and Sodium Hydroxide Solutions''

2001فثشاش 15ـ 13انكاء انكهشتح وذطثماذها ـ األلصش فانثانس انذونانؤذش (4)

[4] The Third International Conference on Electrochemistry and Its Applications (ICE-3), Laxer, 13 - 15

February, 2001.

"Effect of Schiff Base Compounds on the Corrosion of Iron in Acidic and Alkaline Solutions”

.و2000ىفثش 8ـ 5ـ أعىط . انؼهىو األعاعح وانركىنىجا انرمذيح ف انثا انذونانؤذش (5)

[5] The Second International Conference on Basic Sciences and Advanced Technology (BSAT - II), Assuit,

Egypt, November 5 - 8, 2000.

“Electro thermal and Semi conductivity Behavior of Sintered Red Sea Poly metallic Complex Ore”

ذظه انجؼح انز" انصاػح فيشاكم انرآكم "انثاي ػشش ػ انؼه انذون انغىانؤذش (6)

.انصشح نرآكم انفهضاخ وحارها

[6] 18th Annual Conference CORROSION PRJBLEMS IN INDUSTRY, November. 23 - 25, 1999.

Ismailia, Egypt - Egyptian Corrosion Society (ECS).

i) “Inhibition of the Corrosion of Iron by Hydantoin Compounds in Acidic Media”.

ii) “Corrosion Inhibitors for Iron in Sodium Hydroxide Solution”.

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25

.انكاء ـ يصهحح انكاء ـ وصاسج انصاػح وانثشوج انؼذح فاألول انؼه انذونانؤذش ( 7)

[7] The First International Conference on The Role of Chemistry Administration for Attending

Environment and Society, Cairo, 15-17 December, 1998, Egypt.

"Electro chemical Behavior of Nickel Dissolution in Acidic Nitrate and Chloride Solutions.

.انؼهىو األعاعح وانركىنىجا انرمذيح فاألول انذون المؤتمر (8)

[8]The First International Conference on Basic Sciences and Advanced Technology, Assuit, 9-12

November, 1996, Egypt. "

''Thermo-physical Studies on Ilmenite Ore for Mass Production of Ceramic Capacitors".

.انخايظ نهكاء غش يرجاغح انحهمح وذطثماذها انذونعا اتيؤذش ( 9)

[9] 5th IBN Sinai International Conference on Pure and Applied Heterocyclic Chemistry, Ain Shams

University, Cairo, 9 - 12 December, 1995, Egypt.

i ) Inhibition of the Acid Corrosion of Copper with Some Azoth heterocyclic

Dyes

ii) "Inhibition of the Corrosion of 16/14 Austenitic Stainless Steel by Oxygen and

Nitrogen Containing Compounds".

.انرح انؤذش األول نؼهىو انصىسج ػ انكاء ودوسها ف خطح( 10)

[10] Proceeding First Chemical Conference, Faculty of Science, Mansoura University, 24 - 26

September, 1986, and Egypt. "

''Reuse o f Scrap Brass for the Production of Standard Bronze Alloy".

.يؤذش انكاء األول نؼهىو اإلعكذسح( 11)

The First Chemical Conference, Alexandria, 28 - 30 April, 1985, Egypt. [11]

i) "Estimation of Inorganic Phosphate in Tissue Proteins Spectrophotometer-

metrically".

ii) "Paleographic Reduction of 4-Arylazo-1-Phenyl Parasol 3, 5 Dionne and Some

of Its Derivatives in Aqueous Ethanol Buffers".

.ـ ذىسرى ـ كذا 167يؤذش انجؼح انكهشوكائح سلى ( 12)

[12] 167th the Electrochemical Society Meeting - Toronto, Ontario, Canada, 12-17 May, 1985,

Canada.

i) "Electrochemical Reduction of Some Arylidene Derivatives of Salicylic, Oxalic,

Succinic and Methyl (2-Hydroxy Phenidene) - Benzoic Hydracids in Non-

Aqueous Medium at a Mercury Cathode".

ii) "The Polar graphic Reduction of Some Arylidene Derivatives of Oxalic

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26

Hydrazine in Buffer Solutions of Varying pH".

صش انكائانؤذش ( 13) نهثحىز ـ انماهشج انمىيػشش، انجؼح انكائح انصشح ـ انشكض انثا ان

[13] 12th Egyptian Chemical Conference, Cairo, 7-10 April, 1984, Egypt.

i) "Electrochemical Production of Zinc and Lead from Natural Occurring Poly metal

Complex Ore."

ii) "Recommended Flow sheets for the Electrolytic Extraction of Lead and Zinc

from Red Sea poly metal Ore".

إطار مشروع تنمة قدرات ف حامد على مدكور لطف/ أألستاذ الدكتور اجتازهاالدورات والبرامج التدربة الت

التدرس والقادات هئات أعضاء

Faculty and Leadership Development Project (FLDP)

العالوزارة التعلم ,العالوحدة إدارة مشـــروعات تطور التعلم :جهة اإلشــــراف

(.الجمهورة المنـــة -جمهورة مصر العربة )

.و18/4/2004إن 10/4/2004انفرشج ي ف" WINDOWS"انذوسج انرذسثح نثشايج (1)

.و29/4/2004 إن 20/4/2004ي ف انفرشج ”MS WORD”انذوسج انرذسثح نثشايج( 2)

.و15/5/2004إنــ . و7/5/2004ف انفرشج ي ”INTERNET”انذوسج انرذسثح نثشايج (3)

.و2/6/2004إ ن 26/5/2004ف انفرشج ي ”MS EXCEL”انذوسج انرذسثح نثشايج(4)

: يف انفرشج Training program (L4) "انجىاة انماىح" انذوسج انرذسثح نثشايج(5)

.و 18/4/2005إنـــــ 16/4/2005

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27

: ف انفرشج ي Training program (L5)" انجىاة انـانح" انذوسج انرذسثح نثشايج ( 6)

.و 21/4/2005إنــــ 19/4/2005

:ف انفرشج ي Training program (I4) "إداسج انثشـــش" انذوسج انرذسثح نثشايج( 7)

.و9/6/2005إنــــ 6/6/2005

: ف انفرشج ي Training program ( P4 )" داب انهحأخاللاخ وآ"انذوسج انرذسثح نثشايج ( 8)

.و27/6/2005إن 2005/ 25/6

Training program ( L(3 ) "اذخار انمشاساخ وحم انشكـالخ "انذوسج انرذسثح نثشايج ( 9)

.و10/7/2005إنـــ 6/7/2005: ي

:ف انفرشج ي Training program ( P 2 ) "انهــاساخ اإلداســـح " انذوسج انرذسثح نثشايج ( 10)

.و 25/7/2005إنـــ 20/7/2005

:ف انفرشج ي Training program(P3)"إداسج انىلد وضغــىط انؼم" انذوسج انرذسثح نثشايج ( 11)

. و2005/ 8/ 14إنـــــ 8/2005/ 10

Training program (S3) " انرؼهــى تانركـــىنىجـــا" انذوسج انرذسثح نثشــايج ( 12)

. 15/9/2005إنـــــ 12/9/2005: انفرشج ي ف

:يف انفرشج Training program (S1) "ذصى اناهج وانمشساخ"انذوسج انرذسثح نثشايج (13)

.و20/9/2005إن . و17/9/2005

"Training program (S5 ))ذمى انرذسظ "انذوسج انرذسثح نثشايج (14)

“Teaching Evaluating Practice" 30/1/2006إن 28/1/2006: انفرشج ي ف .

Training program (T12))"ذىكذ انجىدج واالػراد"انذوسج انرذسثح نثشايج ( 15)

.و 6/4/2006. إن 5/4/2006: ف انفرشج ي

(6 )(R) ( Training program)" إعرــــشاذجــــح انثحس انؼه"انذوسج انرذسثح نثشايج ( 16)

.و 17/8/2006إن 15/8/2006: ف انفرشج ي

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28

: حىل انرذسظ انجايؼ"انجهىسح انح , جايؼح صؼــاء, انذوسج انرذسثح انر ألايها يشكض ذطىش انرؼهى انجايؼ( 17)

.و2007ياى 6 –أتشم 15: خالل انفرشج ي -"وانرمىى, وذماخ انرؼهى, انطشائك واألعانة

انؼمذج تشكض انحاعة ان تجايؼح صؼاء خالل " ايراص"دوسج سخصح جايؼح صؼــــاء نمادج انحاعىب ترمذش ػاو ( 18)

.و30/1/2008إن . و17/11/2007: انفرشج ي

انمشساخ انهىنذ نرىصف ويالشــح إصالح (MASTERY )انشاسكح ف وسشـح انؼم نشــشوع ياط ذشي ( 19)

, انحذذج ف انجهىسح انـــح –ريـاس –صؼــاء : انذساعح ف انؼهـــىو وانشاضــاخ نثشايج كهاخ انرشتح ف جايؼاخ

. و2008فثشاش 29 – 22: وانر ألد ف يذح ذــؼـض خالل انفرشج ي

انؼمذج تشكض انحاعة ان تجايؼح صؼـــاء انغرىي األول – SPSS) )دوسج انرحهم اإلحصائ تاعرخذاو تشايج ( 20)

.و29/3/2008إن . و5/3/2008: تانجهىسح انح خالل انفرشج ي

, " يحرىاها وإيكااذها انثحثح, (TIMSS)لاػذج تااخ انذساعح انذونح نهشاضاخ وانؼهــىو "انشاسكح ف وسشــح ( 21)

.و2008ياى 6 – 4: انؼمذج تكهح انرشتح تجايؼح صؼــاء خالل انفرشج ي

انؼمذج تكهح انؼــهىو تجايؼح , " ذطىش انذساعاخ انؼهـــا تكهح انؼــهىو تجايؼــح صؼـــاء" انشاسكح ف وسشح ( 22)

.و2008ياى 29 – 28: صؼـــاء خالل انفرشج ي

انر ألايهـا يششوع ذطىش انرؼهــى –" يهــاساخ انثحىز واإلداسج األكادـــح" انشــاسكح ف انذوسج انرذسثح ف ( 23)

:يجايؼــح ػشا خالل انفرشج –جـايؼـح صــؼـاء ,انهىنذحانؼان تانجهىسح انـح تانرؼــاو يغ جــايؼح يغد سخد

. و2008ىــى 9 – 3

ف انهرم انه انثانس انؼمذ تجايؼح " ذح يهاساخ االذصال انفؼال ويؼىلاذه" انشاسكح انفؼانح تئنماء يحاضشج ( 24)

.هـ1432جاد األون إن جاد انثاح 29انهك ػثذ انؼضض خالل انفرشج ي

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انؼمذج تؼادج انثحس انؼه تجايؼح " تاعرخذاو انحاعة ان ISIاالعرفادج ي لىاػذ تااخ " انشاسكح ف وسشح ( 25)

.و7/5/2011انهك ػثذ انؼضض ف

انؼمذج تؼادج انثحس انؼه تجايؼح انهك ػثذ " انجىػاخ انثحثح وانرماخ اإلعرشاذجح" انشاسكح ف وسشح( 26)

.و10/5/2011انؼضض ف

ف دػى انثحىز ويراتؼرها " وسشح ػم نهرؼشف تا ذمذيه يذح انهك ػثذ انؼضض نهؼهىو وانرمح"ف انشاسكح ( 27)

.تجايؼح انهك ػثذ انؼضض .و23/5/2011إنكرشوا انؼمذج ف