INSTRUCTION MANUAL.CSTR SET UP DESCRIPTION SPECIFICATIONS INSTALLATIONREQUIRMENTS INSTALLATION AND CONNECTIONS PRECAUTIONS TROUBLE SHOOTINGEXPREMENTATION THEORY OPERATING PROCEDURE SYSTEM CONSTANTS OBSERVATION TABLE CALCULATIONSCSTR AIM:Tostudythes!o"#$%t#o"o& ethy' %ette#"%o"st"t(o)st#**e*t"+*e%to* "d to dete*,#"e !e*%e"t-e %o".e*s#o" "d theo*et#%' %o".e*s#o"/APPARATUS: A CSTR setu!0 1u*ette0 !#!ette0 %o"#%' (s+s/ Mesu*#"- %y'#"de*s et%/CHEMICALS : Ethy' %ette0 NOH0 o2'#% %#d0 HC'0 !he"o'!hth'e#" #"d#%to*THEORY: S!o"#$%t#o" o& ethy' %ette u"de*-oes s &o''o)s3CH4COOC5H6 7 NOH 8 CH4COON 7 C5H6OHB7 A8 PRe%t#o" #s ,de ho,o-e"eous "d #s $*st o*de* )#th *es!e%t to este* "d'+'#/ The *te o& *e%t#o" %" the*e&o*e 1e )*#tte" s0 9*A : ;CACB; : FAOB : : @CAOA XAB > C ; CAOAD @< E XAB @M9XABF; CAOA : XA> @< 9 XAB @M 9 XAB 9999999 @ CAOA )he" M G A%et#% %#d 9=/=6 NA'' so'ut#o"s *e !*e!*ed &*esh'y "d st"de*d#se NOH )#th o2'#% %#d/Thee2!e*#,e"t #s to 1e %**#ed out t *oo, te,!e*tu*e/ F#'' u! the &eed t"+s)#th 6 '#te*s o& NOH "d ethy' %ette/ F#"d out the .o'u,e o& the *e%to*/AdHust tot' (o) *te #"to the *e%to* #" su%h)y to h.e *es#de"%e t#,e o&I96 ,#"/ Co''e%t the s,!'es &te* 5 t#,e/ At #"te*.' o& 6 ,#" %o''e%t I96s,!'es/T#t*te the s,!'e -#"st HC' #,,ed#te'y @s the *e%t#o" #s .e*y&st e2!e*#,e"t #s %**#ed out )#thout **estt#o"/BFo* stedy stte to 1e !!*o%hed'o) 5 to 4t#,e to 1e e'!sed1e&o*e t+#"- s,!'es &o* t#t*t#o"/Volume of reactor i ! liter.O"erati#$ "roce%ure1. Feed t"+s E o!e" s,'' #* .e"t .'.e "d #"su*e tht 1otto, .'.es*e %'osed/ F#'' u! &eed t"+s s'o)'y/ C'ose '' .'.es o& &eed t"+/2. St*t #* su!!'y to 1oth the t"+s th*ou-h #* *e-u'to*0 ssu*#"- thtthe #* !*essu*e &*o, *e-u'to* to &eed t"+s )#'' "ot e2%eed < to %,D/3. S'o)'y o!e" &eed .'.e sy 56J o!e"/4. AdHust Rot ,ete* .'.es to des#*ed (o)s "d e"su*e stedy9stte (o)*te/5. I"#t#''y +ee! ,#"#,u, (o) *tes !oss#1'e/6. A&te* *e%h#"- to stedy9stte o& !*o%ess %o"d#t#o"s st*t to )#thd*)s,!'es/7. A&te* e2!e*#,e"tt#o" $*st %'ose #* su!!'y .'.e to t"+s/8. D*#" '' t"+s s'o)'y/9. F'ush '' syste, t"+s "d .esse's 1y %#*%u't#"- )te* th*ou-h #t/10. Im"orta#t #ote:du*#"- !"eu,t#% %o".ey#"-0 do"At ''o) #* to !ssth*ou-h Rot ,ete*s &*o, &eed t"+/ It ,y d,-e Rot ,ete* tu1e/So e"su*e suK%#e"t ?u"t#ty o& &eed ,te*#' #" &eed t"+s/ O&SERVATION:Vo'u,e o& *e%to* : VVo'/F'o) *te o& este* : VB Vo'/ (o) *te o& NOH : VANo*,'#ty o& este* : CBONo*,'#ty o& NOH : CAO No*,'#ty o& o2'#% %#d : NOXNo*,'#ty o& HC' : NHC'S*/ No/ T#,e @ ,#"BBu*ette *ed#"- @ VHC'BCALCULATIONS:: V > @VA 7 VBBCA : NHC' VHC' > V s,!'eCAOA : CAOA E CAB > CAOAX CAOA: @CAOA E CAB > CAOA/Theo*et#%' %o".e*s#o" %" 1e %'%u'ted 1y ; CAOA : XA > @< E XAB @M9XAB 999999 @ CAOA )he" M G