Cocaine Purity Test CPT0110 - Drogas de Abuso · Secondly the reagent was prepared by snapping open...

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COCAINE PURITY LABORATORY TEST RESULTS A laboratory analysis of the Cocaine Purity test. M.M.C. INTERNATIONAL B.V. Frankenthalerstraat 16-18 4816 KA Breda The Netherlands Phone: +31-765711140 Fax: +31-76-5719300 Email: [email protected] www.narcotictests.com

Transcript of Cocaine Purity Test CPT0110 - Drogas de Abuso · Secondly the reagent was prepared by snapping open...

COCAINE PURITY LABORATORY TEST RESULTS

A laboratory analysis of the Cocaine Purity test.

M.M.C. INTERNATIONAL B.V. Frankenthalerstraat 16-18 4816 KA Breda The Netherlands

Phone: +31-765711140 Fax: +31-76-5719300

Email: [email protected] www.narcotictests.com

M.M.C. International B.V. Laboratory and Production Manager Benji Voesenek Page 1 of 6 Phone number: +31-76-5711140

Introduction We at M.M.C. International are producers of presumptive colorimetric ampoule tests for the police

and customs officers. These tests give a presumptive identification of a suspected substance. These

tests in no way substitute the need for further confirmation by for example GC-MS analysis. Always

have your sample confirmed by a laboratory. In order to give you, the customer, the best

identification possible we do tests at our laboratory to ensure the quality of our products and to

expose possible cross reactions with our tests. In this report we tested our Cocaine purity test and

we confirmed our samples with GC-MS.

Chemicals Used In this test we used the following chemicals:

Chemical Manufacturer Purity

Alpha-D(+)-Glucose Across Organics 99,0%

Aspirin Sigma-Aldrich 99,9%

Benzocaine Sigma-Aldrich 99,9%

Boric acid Carl-Roth 99,9%

Caffeine Carl-Roth 99,9%

Creatine Sigma-Aldrich 99,9%

D(+)-Sacharose Carl-Roth 99,7%

D-Mannitol Sigma-Aldrich 98,5%

D-Sorbitol Carl-Roth 99,7%

Ibuprofen Sigma-Aldrich 98,3%

Lactose monohydrate Carl-Roth 99,5%

Levamisole Across Organics 99,9%

Lidocaine Sigma-Aldrich 99,9%

Magnesium sulphate Carl-Roth 99,7%

Paracetamol Sigma-Aldrich 99,8%

Phenacitin Sigma-Aldrich 99,9%

Procaine Sigma-Aldrich 97,0%

Vitamine C Carl-Roth 99,5%

Cocaine Duchefa Farma B.V. 99,8%

Amphetamine Duchefa Farma B.V. 99,9%

Methamphetamine Duchefa Farma B.V. 99,7%

Ephedrine Sigma-Aldrich 99,0%

M.M.C. International B.V. Laboratory and Production Manager Benji Voesenek Page 2 of 6 Phone number: +31-76-5711140

Equipment Used In our analysis we used a Kern ABS 120-4 analytical balance to weigh the chemicals.

Besides the chemicals and electronic equipment we used regular laboratory supplies and our

Cocaine purity test.

Semi-Quantitative Analysis First, the pure Cocaine was cut with benzocaine in 5 different ratios:

Percentage of Cocaine Amount of Benzocaine Amount of Cocaine

10% 18mg 2mg

30% 14mg 6mg

50% 10mg 10mg

70% 6mg 14mg

90% 2mg 18mg

Secondly the reagent was prepared by snapping open the ampoule and adding the entire solution

from the dropper to the ampoule. The top layer of the reagent will colour green at this time.

The weighed samples were added to the ampoules and the following results were obtained:

From left to right the amount of cocaine increases. In the most left ampoule has a slightly brown

bottom layer, but this is not very clear on the photo below due to lighting conditions.

M.M.C. International B.V. Laboratory and Production Manager Benji Voesenek Page 3 of 6 Phone number: +31-76-5711140

The chart we made according to the test done with different ratios of cocaine and benzocaine.

In the following chapter we will test the cross reactivity of the Cocaine Purity test with several other

substances

M.M.C. International B.V. Laboratory and Production Manager Benji Voesenek Page 4 of 6 Phone number: +31-76-5711140

Cross-Reactivity In the following pictures and tables the cross reactivity of the Cocaine Purity test is demonstrated.

From left to right:

Number Substance Reaction

1 Alpha-D(+)-Glucose None

2 Aspirin None

3 Benzocaine None

4 Boric acid None

5 Caffeine None

6 Creatine None

7 D(+)-Sacharose None

8 D-Mannitol None

9 D-Sorbitol None

10 Ibuprofen Clouded bottom layer

11 Lactose monohydrate None

M.M.C. International B.V. Laboratory and Production Manager Benji Voesenek Page 5 of 6 Phone number: +31-76-5711140

From left to right:

Number Substance Reaction

12 Levamisole Very dark brown top layer

13 Lidocaine Dark Brown specks sinking to the bottom

14 Magnesium sulphate Dark green top layer

15 Paracetamol None

16 Phenacitin None

17 Procaine None

18 Vitamin C Pinkish top and bottom layer

19 Cocaine HCL Brown to dark brown bottom layer depending on purity

From left to right:

Number Substance Reaction

20 Amphetamine None

21 Methamphetamine None

22 Ephedrine None

M.M.C. International B.V. Laboratory and Production Manager Benji Voesenek Page 6 of 6 Phone number: +31-76-5711140

Conclusion: The cross reactivity of the Cocaine Purity test is very good even compared to our standard

Cocaine/Crack test. This test gives less cross reactions and also lets you determine the purity of the

Cocaine samples. With this test you can identify if a substance is Cocaine and you can determine the

purity at the same time.

Creation date: Friday, December 20th, 2013

M.M.C. International B.V. MSDS – Material Safety Data Sheet

Page 1 of 5

1. Identification of the substance/mixture and of the company 1.1 Product identifiers

Product name : Cocaine Purity Test

Product number : CPT0110

Brand : MMC International

1.2 Relevant identified uses of the substance or mixture and uses advised against

Identified uses : Laboratory chemicals, Manufacture of substances

1.3 Details of the supplier of the safety data sheet

Company : M.M.C. International B.V.

Frankenthalerstraat 16-18

4816KA Breda

The Netherlands

Telephone : +31 76-5711140

Fax : +31 76-5719300

E-mail address : [email protected]

1.4 Emergency telephone number

Emergency Phone # : 112

2. Hazards identification 2.1 Classification of the substance or mixture

Classification according to Regulation (EC) No 1272/2008 [EU-GHS/CLP]

Acute toxicity, Oral (Category 4), H302

Acute toxicity, Inhalation (Category 4), H332

Skin irritation (Category 2), H315

Eye irritation (Category 2), H319

Carcinogenicity (Category 2), H351

Reproductive toxicity (Category 2), H361d

Specific target organ toxicity - single exposure (Category 3), Central nervous system, H336

Specific target organ toxicity - repeated exposure (Category 2), H373

For the full text of the H-Statements mentioned in this Section, see Section 16.

Classification according to EU Directives 67/548/EEC or 1999/45/EC

Xn Harmful R22, R48/20/22

Xn Harmful R40

Xi Irritant R38

2.2 Label elements

Hazard statement(s)

H302 + H332 Harmful if swallowed or if inhaled

H315 Causes skin irritation.

Creation date: Friday, December 20th, 2013

M.M.C. International B.V. MSDS – Material Safety Data Sheet

Page 2 of 5

H319 Causes serious eye irritation.

H336 May cause drowsiness or dizziness.

H351 Suspected of causing cancer.

H361d Suspected of damaging the unborn child.

H373 May cause damage to organs through prolonged or repeated exposure.

Precautionary statement(s)

P261 Avoid breathing vapours.

P281 Use personal protective equipment as required.

P305 + P351 + P338 IF IN EYES: Rinse cautiously with water for several minutes. Remove

contact lenses, if present and easy to do. Continue rinsing.

Supplemental Hazard Statements

none

2.3 Other hazards - none

3. Composition/information on ingredients 3.1 Mixture:

Component CAS-No. Concentration

Chloroform 67663 50-60%

Water (distilled) 7732185 40-50%

4. First aid measures 4.1 Description of first aid measures

General advice

Consult a physician. Show this safety data sheet to the doctor in attendance.

If inhaled

Remove to fresh air immediately. If not breathing, give artificial respiration. If breathing is

difficult, give oxygen (To be administered by qualified medical personnel only!) Get medical

attention.

In case of skin contact

Flush skin with plenty of soap and water for at least 15 minutes. Remove contaminated clothing.

Seek medical attention.

In case of eye contact

Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower

lids. Do not allow victim to rub or keep eyes closed. Get medical aid immediately.

If swallowed

DO NOT induce vomiting. If victim is conscious and alert, give 2-4 cups of milk or water. (Never

give anything by mouth to an unconscious person!) Get medical attention immediately.

Creation date: Friday, December 20th, 2013

M.M.C. International B.V. MSDS – Material Safety Data Sheet

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4.2 Most important symptoms and effects, both acute and delayed

Inhalation: Headache, dizziness, unconsciousness, coma

Ingestion: Nausea, vomiting, diarrhea

Skin: Burning pain, itching, redness

4.3 Indication of any immediate medical attention and special treatment needed

No data available

5. Firefighting measures 5.1 Extinguishing media

Water spray, dry chemical, foam

5.2 Special hazards arising from the substance or mixture

Carbon oxides

5.3 Advice for firefighters Wear self-contained breathing apparatus and protective clothing.

5.4 Further information

"Empty" containers may contain product residue and may be dangerous. Empty containers

should be completely drained and bunged and then disposed of according to local, state, and

federal regulations

6. Accidental release measures 6.1 Personal precautions, protective equipment and emergency procedures

Wear vapor respirator, safety goggles, and rubber gloves. Remove sources of ignition (i.e. open

flames, sparks). Dike if necessary. Dilute with water and add slight excess of soda ash.

6.2 Environmental precautions

Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge

into the environment must be avoided.

6.3 Methods and materials for containment and cleaning up

Mix and neutralize with 6M HCl. Soak up with inert absorbent material (sand or earth

recommended; do not use flammable substances such as sawdust). Ventilate and wash spill site

after collection. Dispose according to local, state, and federal regulations.

7. Handling and storage 7.1 Precautions to be Taken:

Keep in tightly closed container. Keep cool and dry. Prevent from freezing. Avoid all ignition

sources (heat, open flame, spark). Avoid incompatible materials. Use only in well-ventilated

areas. Do not ingest or inhale. Avoid contact with skin, eyes, and clothing. Avoid prolonged or

repeated exposure. Wash thoroughly after handling.

7.2 Other Precautions:

"Empty" containers may contain product residue and may be dangerous. Empty containers

should be completely drained and bunged and then disposed of according to local, state, and

federal regulations.

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M.M.C. International B.V. MSDS – Material Safety Data Sheet

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8. Exposure controls/personal protection 8.1 Ventilation Requirements:

Use only in well-ventilated areas.

8.2 Personal Protective Equipment:

Safety goggles, gloves, vapor respirator, protective clothing.

9. Physical and chemical properties 9.1 Information on basic physical and chemical properties

Boiling Point: 61 °C

Melting Point: -63 °C

Evaporation Rate (Butyl Acetate = 1): 1.6

Vapor Pressure (mm Hg.): 160

Specific Gravity (H20 = 1): NE

Vapor Density (AIR = 1): 4.12

Solubility In Water: 8 g/l

Other Information:

Liquid with sweet odour

10. Stability and reactivity 10.1 Stability:

Stable at room temperature in closed containers under normal storage and handling conditions .

10.2 Incompatibility (Materials to Avoid):

Light, ignition sources (heat, open flame, spark), acetone, alkalies, aluminum, disilane, lithium,

magnesium, nitrogen oxides, acids, phosphorus pentoxide, potassium, hydroxides, alcohols,

potassium tert-butoxide, sodium, sodium methylate, sodium-potassium alloy,

triisopropylphosphine, fluorine, strong oxidizers, acetic anhydride + sodium hydrogensulfate,

acetyl bromide, ammonia, silver nitrate, dichloromethane, disulfuryl difluoride, magnesium

perchlorate, silver, oxides, platinum, potassium, tetrachlorosilane, steroids, ketones

10.3 Decomposition/By Products: Hydrogen chloride, carbon dioxide, chlorine, phosgene gas

10.4 Hazardous Polymerization:

Has not been reported

11. Toxicological information 11.1 Information on toxicological effects Harmful or fatal if swallowed. May cause central nervous system depression. May cause cardiac disturbances. May cause adverse reproductive and fetal effects. Carcinogenicity

Chloroform

ACGIH--A3: Animal carcinogen California--Carcinogen

Creation date: Friday, December 20th, 2013

M.M.C. International B.V. MSDS – Material Safety Data Sheet

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NIOSH--Occupational carcinogen NTP--Suspect carcinogen OSHA--Possible select carcinogen

IARC--Group 2B: Possibly carcinogenic to humans

12. Ecological information 12.1 Adverse effects

Prevent from entering sewers or waterways. May be toxic to some aquatic life.

13. Disposal considerations 13.1 Information on disposal

Dispose according to local, state, and federal regulations.

14. Transport information 14.1 Information on transport

Keep in tightly closed container. Keep cool and dry. Prevent from freezing. Avoid all ignition

sources (heat, open flame, spark). Avoid incompatible materials. Do not ingest or inhale. Avoid

contact with skin, eyes, and clothing. Avoid prolonged or repeated exposure. Wash thoroughly

after handling.

15. Regulatory information 15.1 Safety, health and environmental regulations/legislation specific for the substance or

mixture

No data available

16. Other information 16.1 Risks

Using this product under normal, properly instructed procedures should not be hazardous.

16.2 Further Information

The information above is believed to be accurate and represents the best information currently

available to us but does not purport to be all inclusive and shall be used only as a guide. We

make no warranty of merchantability or any other warranty, expressed or implied, with respect

to such information, and we assume no liability resulting from its use. Users should make their

own investigation to determine the suitability of the information for their particular purposes.

Cocaine Purity Test The MMC Cocaine Purity test is a quick presumptive test for cocaine that will give you an idea about its purity.

With this test you are able to find out whether and how much the cocaine has been cut.

Dealers cut cocaine to increase their profit margins. The substances used for cutting are generally harmless

but it sometimes happens that possibly dangerous substances are added. As a general guideline you can

say that when there is a high percentage of cocaine present in the sample, you are close to the top source

and the cut of dangerous adulterants are diminished. This test does not tell you anything about the

adulterants that were used to cut the sample with.

Contents kit: * 10 Cocaine Purity ampoule tests + 10 buffer solution tubes

* 10 Spatulas

* 1 Instruction Sheet

Instructions: * Prepare a line of the sample on the test field on the lower right corner of this instruction sheet so that it is

covered with powder (approx. 20mg); OR use a supplied spatula and cover the spatula scoop with the

powder (approx. 20mg)

* Make sure the powder does not contain any lumps “rocks”, as this might influent the results of the test; * Open the ampoule with the ampoule-breaker that is on top of each test ampoule;

* Open one (1) buffer solution tube and insert all the liquid into the test ampoule;

* Add the powder (approx. 20mg) to the test ampoule;

* Slowly shake the test ampoule for 5 seconds;

* Look at the colorization of the bottom layer and compare the color to this instruction sheet.

* After use: dispose the test neatly.

Disclaimer: Use of this test is at your own risk. This is a presumptive test. No rights or claims can be derived from (the use of) this test. The manufacturer/supplier cannot be held liable for damages and/or incidents as a result of this test.

Warning: Do not ingest. Do not inhale fumes. Do not bring in contact with eyes, skin and clothing. Possibly irreversible

effects. Keep locked up and out of reach from children. In case of eye contact: rinse with a lot of water and

seek medical advice immediately. Wear protective clothing and gloves. In case of an incident or when feeling

unwell: seek medical advice immediately. Use only in well-ventilated areas.

MMC INTERNATIONAL B.V.

www.narcotictests.com

[email protected]

Phone: +31-76-5711140