[CHAIN OF CUSTODY RECORDS, INORGANIC ANALYSIS DATA ... · ENVIRONMENTAL PROTECTION AGENCY Office of...
11
i««»B3ai-fl»KEatga»a^raB^8s«aa««!ffl^^ Co-^ iBs-Si^S^P A^b^cx-^s^ 003632
Transcript of [CHAIN OF CUSTODY RECORDS, INORGANIC ANALYSIS DATA ... · ENVIRONMENTAL PROTECTION AGENCY Office of...
i««»B3ai-fl»KEatga»a raB 8s«aa««!ffl ^
Co-^ iBs-Si S^P
A^b^cx-^s^
003632
ENVIRONMENTAL PROTECTION AGENCYOffice of Enforcement
CHAIN OF CUSTODY RECORD
REGIONSFirst Internatlonat Bidg., 120T Elm St.
Dallas. Texas 75270PROJ. NO. PROJECT NAME
SAMPLERS? fSigtvarure}
STATION LOCATION
CONTAfNEFtS
REMARKS
^ 'T^Cw.L <C. U^ry^J I { I Y-
Relinqflished by; (SijSfiattiref Dale /TEme Received by: {Slynswref Relinquished by: (Signswrs) Date /Time Received by: (Sign»nir»)
Rfrffncjuished by: (Signaturef Date /Time Received by: ^Signature) Relinquished by: {Signatura) Date /Time ReceFved by: (Signature
Relinquished by: cs'ffnwf(w?/ Date /Time Received for Laboratorykby: Dare /Time Remarks
Distribution: Original Accompanies ShEpmen't; Copy to Coo'Srriator Fiard Fires
003633
U.S. EPA Contract Laboratory ProgranSABple Management Office "• -P.O. Box 818 - Mexaodria, VA 22313703/557-2490 .lai 8-557-2490 Date
COVER PAGE . : -mORGANIC ANALYSES DATA 'PACKAGE ' ' ' '
Lab lsalse .JTC^Env-irrmmqr^l Consultants ^S6 ^0- S43 -^^
SOW 2So; 78 4 . ' Qiy^> >>4J rj) 3 ) CP "Q.C. Reporc No. 4^-Sample Hmab ra
ERA ?0. Lab IDMo. EPA Ko. - Lab ID No
Comments:
ICP Interelesent and background corrections applied? Yea -^^ KoIf yes, corrections applied before . \>- or after _, _ generation of tav data.
Footnoces:MR -Form 1:Value -
nor. required by contract at this tine
If the result is a value greater than or equal to the instrumentdetection Ucntc but lefis than the contract, required detection limit,report the value in brackets (i.e.. (10]). Indicate chs analyticalmethod used trieh P (for ICP), A (Flame A A ) , or F (furnace A A )Indicate® alfaent uaa analyzed for but not detected. Report uifch the Instrumentdeiecclon liatt value (e.g.i IOU).Indicacea a value esciciaced or Gor; reported due to the presence ofincerferencee Explanatory nota included on cover page* • ^r: :••••:-a'ff
' Indicates value deterained by Method of Scandard Addition.Indicates iipika asinple recovery is not wiehiQ control litaita,
' Indicates duplicate analysifi ia not within control limits.Indicated Cha correlation coefficient for aethod of Btandard addition isleas than 0.595
003634
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-Initial Calibration Source ^fff &o B
FORM II
Q . C REPORT No. 42
IMITIA) AND CONTINUING CALIBRATION VERIFICATION
Lab Na»e: K?TC FNtHRONMFNTAL CN5LT5.
fiATF 05/07/07Coepound
Metals:
CASE No- sas 2648SOU No. 046UNITS: ug/L
Continuing CalibrationTrue V&l round HR Found HR Method
Initial Calib.Trup k'al Found ^R
PAGE 1
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2
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• ICP, A - FIaBS/ F - Furnace AA
003636
ropM inQ . C REPORT No
0' ANK5
Lab Naae: JTC r:M^IRONhi;NTAL CNSLT^-DATE 05/09W
PAGE 1
CASE N D . sas 2640UNITS: ug/L
Continuing CalibrationClank I'alue Preparation Blank
Matpiy; Matriy:Coapound Dianh '/alii" IsolidI t
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003637
T&RM IVQ C REPORT No. 42
ICP INTERr-CREMCE CHECK SAMPLEJTC FiWRONMCNTAL CN5LT5. W: No 5is 2648Lab Nflae
-f .!:•• JAMF-LE 1 . 0 . ics-85DATE 05/09/07 C^^ SAMPLE SOURCE EPA
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^2'"7.,......<2s$J..530.9
4 6 1 . 1
006.3
505624.0
1078 .7
505. •l
407.3
40467.6
4364.1
525863.0
5 1 5 . 4. J ••••.»..»•«——••. J.I
949.6
009.4
4 5 1 0 . 0 U
11^' i er' I36.0 U
476.1
923.5
84
N
/112
101
91
101
109
105
95
24
104
105
98,—-—•
1 0 4 . 0
90.
NC
IfNC
101 .
97.
1 . 9
C
0:.5
.1
.9
.3
-5
.8
.7
.5
.8
,8
,7-—
......
'1T.•-4'
3
i& J^q93•'»—/
i4
Mean uaiup hated on n - ..sS^L"True value o F EPA lf:P Int®FTire^5"chefl!i 5» Qiatepaified ....,..,.-.»«„ ' M^an „„ ample or contfactcn1 gt&ndard
003638
T^RM VQ . C - REPORT No. 12
SPIKE ^MPLE RCCOUERYJ-TC f:NVIRONM'-:NTAL CNSLT5. Ca«ie No. aas 2648
-EPA 5&Bp1.e ND. r5472Lab 5a»pls tD No. 2-0157UNITS ug/L
Matrix soil
1-a.b Naye.
DATE 0^/09/87
StscaKs:ass-ssKaw.xwai3:==ssasasss7aasa:ss=ass:atssiasasisssss'WSS!asssasa'siSiae=sssf=atsasaSSSsi£aa'sssassassaiss=sssisax'sCONTROL LIMIT SPIKEII SAMPLE SAMPLE SPIKE
COMPOUND ^R RESULT ( 5 5 R ) RESULT ( 5 R ) AODCD (5AI KR !
MCTAL5:Aluainm 75-1?5 23103.2 C3330.9 N/R
Ant iaany
Arsenic
ftarjua
D^ryHiuti
CadaiUB
Cftlciuft
Chroniufi
Cohsit
Copper
Iron
l-ead
MaQneaiua
Manganepe
Mercury
Nickel
POt55^iUB
5elpftiu»
Giluer
^QdlfJt
Tha31 iua
Tin
iJanatllUB
Zitic
Olh^r:
Cyanide
75 -125
75 125
75 125
7 5 - 1 2 5
75- 1?*5
75-1P5
75-125
75- 125
7F>--125
75--125
75- 125
75-125
7 5 - 1 ? 5
75 125
75--ins75 125
7 5 - 3 2 5
75 1^5
75' 125
75 '125
75' 125
7.t*• 125
7S-325
.. ...-...-.-... 0 .......
60453.0
413 .3
227.7
41550.2
1 5 1 0 . 9
1 0 1 2 . 1
..... ..0..'..^.573.4
n riOc^<J?Uo
QA/ ^^\
140.1
2276,5
47.6
45.4
557.3
3567.9
• r?/ L.. „. ....d.-'ib.:30.3
^764.4
552.4
534.3
044.0
C
02750
1...... .£)•!.(
t720
C
S7
r151
4
4
205
20
14
44335
1020
3046
1555
45
/ ' -7
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36
40
3n6
.0 U
^)u.0 3
.*? U
.7 'J
.5
.1
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.0 U
.6
.4
.7
,0
O.LL.2
4H.1 U
.0
7u -s r.0 U
.6 3
.7
(Oc^ /o-o
t /
500.0
500.0
^S9^ 10-Lrooo.o
50.0
50.0
N/R
200.0
5 G O . O
250.0
N/R
500.0
N/f t
500.0
1 . 0
500.0
N/R
^5^(5-50.0
N/R
500 0
500 .0
20,
106,
95.
91 .
104.
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9 1 .
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9
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003639
T^aRM UIQ . C , REPORT No . 42
DUPLICATESFN'URONMFNTAL CN5LT5. Case No. sas 2640t.ab Narc: JTC
DATE 05/09/87 .EPA Qanple N o . f5472Lab 5a»ple ID No 2-0157UNITS •3/«aMatrix sail
taissssiSAvixiuiittEcaiasssaaascas-sassesaKstamsSa^s^ssaasaasssssssssastSasisat'ssas.ssatesssysisasiBiSis&aaaa»*aa!5==tc;ayia=is.-=tissCoapuundssasxaassas.saaaa.'asaMat»l«:
i • A l u a x n u e
Control Li »lt 5 a M p l e ( S » Duplicated)) RPO•.awSfaa!*au.maiSSsssssssaiKSsss'SSi!SS:aXssi='Stssa3ssssawas3saEStS&sassas.ss:st=sssasaassassssssaSiasi
1 . AlUBlflUB
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4.
5
6.
7.
0
9.
10
1 1 . .
12.
t3,
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16
17 .
10
19
20
21
22.
23.„......S4
Othir:
Cyp
.f!
Antiaony
Afsenic
Uar)UB
B^ryHiua
CadeiuB
Calciu
Chroaiun
nobalt„...-„.......-.--.-.-—Copper
Iron
L»5ad
Magp<*s'iu»
Manganese
Mercury
Nickel
PatasHiu*
SeVftniua>..-.-—..,...-... ...-. . .5) li/ef*
S O d t U B
ThP.lliu»
Tin
Uanadiut,... .......-.-. ,.i. .,.-.". . .7inc
...,,.•..... ..... .•.^..•-.•.-•-•• •• •nicle 4/^ ,
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20.00 It
6,0
- lo20,0 C
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.5
20.00 K
20,00 X
5.0
2.5
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ft?-^o joTo500.0 C
20 .00 %
'..J.J...-. ..-...-..4 . 0
5&13f \
1 . 0
500 0
I.I...........4.0
5.0 C
20.00 %
S"i .. •vJ
2333.1
5.7 U
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.5 U
.5 U
0275.0
20.5
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1 4 U
^433.6
1^
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155.5
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-. . il...............11 ,,,,,.,
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4 5 1 . 0 U
... „ ., "l L3.6 U
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30.7
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2056.1
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101•? 9 3
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6 1 0 1 . 9
30.3
2 0 U
1 . 4 U
4930.0
W264.6 3
1 1 7 . 9
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....J . ...
tlu.7 U
4 5 1 . 0 U
U-< "1-..-."y^.-l3.6 U
4 . 4 3
57.4
f^ .•——'"M0/$>
12.62
NC
A t^CNC
NC
NC
30.24 »
60.57 «
NC
NC
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rs •NC
27.53 »
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,... ...-..-..-.......-, ....NC
30.99 lit
U (OCRPO a C i Q - D i / K S I- D » / 2 » 3 y 100NC • Non calculnblft RPD due to ua)ue(s ) lass than CROL
003640
}W VII
Q . C . REPORT No
IM*nRUMr.NT orTtXnON LIMITS ANDIrt&OPATORY CONTROL SAMPLE
lab NaBC: JTC WlROMMn:MTfti. CN5LTS. CASE No. sas 2640 DATE 05/0^/87LC5 No,
c.u'sssvt&sssaStsss.ssassvtastassssasastsass.sttcsatss.s'sisa.ssssvaw&tsssStK.stsiisiatssstssstSswssaiXSiie.a.v.Ktcsstsmwis&VKasea's
Required Detection Instrument Detection Lab Control 5a«pleCoapound Liaits (CRDLt-ug/ l Lieits ( IDLl-ug/1 Uni ts- ufl/L
tCP/AA FurnaceID * ID * True FountI %R
aswvaxws»»^^9Kaxsss=ss•as;saassassst•sssclsiss•as:St=xssxs.•sas=xxs.s=s:=tsctUiss===:assasavsssnaSK.statSc<•awatsssclal
Metals:I Alualnun 200 140 1 0 0 0 0 . 0 11003 .6 1 1 0 .
2.
0.
4.
5.
6.
7.
0.
9.
1 0 .
il-iain1 4 ,
15 .
1 6 .
1 7 .
10
1 9 ,
CO
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p.a.R3
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np-riua
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Cadaiua
Calciua
Chrcntiua
Cobalt
Copp«r
Iron
Lead
Magne^iun
Manaaner-ft
Mercury 0.2
Nichel
Patftssiua
OP 1 e n i u 6
Silu®r
'jOdiuB
Th&Sliuii
Tin
liRniLdiun
Zinc;
hgr-:
Rrside
• Not, paqulref
6010
200
5
5
5000
10
50
as100
5
5000
15
40
5000
S
10
SOOO
10
40
50
20
57
100
10
4.9
4.7
950
7.0
20
14
37
60
470
3,0
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25
1?.30
1 1 4
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4136
21
19
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5,4
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2
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400.
400,
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1 0 0 0 .
2000,
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1 1 4 & . 9
1033.1
405.3
369.0
220.14.3
1 1 5 4 . 0
3.070.7
1974.6
334;*. 6
1 0 1 6 . 0
10030 9
2035.C
o?.l41090.0
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44675.9
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003641
Q<C* Report No. .JjiJL
STANDARD AIiDHlON RESULTS
IAB WAKE JTC _En vjron men t a 1 __gj[i _l j^_^
" sllLli3imiBaiii-Ti MT—^-i -rrf'A"'•^ ••—""••^••*-^-ir *if
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2 A»i> J 3 ADO
COK./ABS.1 | COM./ABS,1
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t
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(J-WJ-kW
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1 CON la th< concetteraciLon <s4d'sd» ABS* ia the inscrunent: ceadou£ in abaorbance orconcentration.
^~ Cop.detitracAon as determined by MSA
*"r" is che correlacion coeffi&lanc.
+ " fior^BlaUori coefflclQni; ia oucoide of GOrttrol vindov of 0,995«
003642
