Certificate of Analysis · 50MG OTG MUSCLE & JOINT CREAM Harvest/Lot ID: # 0519342324 Batch#:...
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report is an Kaycha Labs certification. The results relate only to the material or product analyzed. Test results are confidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batch material may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter, ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) and Limit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured by an analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholds for human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty of measurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for the pass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310. Jorge Segredo Lab Director State License # CMTL-0002 ISO Accreditation # 97164 ___________________ Signature 08/28/2020 ___________________ Signed On 4131 SW 47th AVENUE SUITE 1408 DAVIE, FL, 33314, USA Kaycha Labs Travel Muscle & Joint 50mg N/A Matrix: Derivative Certificate of Analysis Sample:DA00819007-001 Harvest/Lot ID: 000112019 Seed to Sale #N/A Batch Date :N/A Batch#: 000112019 Sample Size Received: 50 gram Retail Product Size: 10 Ordered : 08/18/20 Sampled : 08/18/20 Completed: 08/28/20 Expires: 08/28/21 Sampling Method: SOP Client Method Aug 28, 2020 | Green Roads 5150 SW 48TH WAY DAVIE, FL, 33314, US PASSED Page 1 of 4 PRODUCT IMAGE SAFETY RESULTS MISC. Pesticides PASSED Heavy Metals PASSED Microbials PASSED Mycotoxins PASSED Residuals Solvents PASSED Filth NOT TESTED Water Activity NOT TESTED Moisture NOT TESTED Terpenes NOT TESTED CANNABINOID RESULTS Total THC 0.000% THC/Container :0.000 mg Total CBD 0.506% CBD/Container :50.600 mg Total Cannabinoids 0.506% Total Cannabinoids/Container :50.600 mg CBC CBD CBDA CBDV CBG CBGA CBN D8-THC D9-THC THCA THCV ND 0.506% ND ND ND ND ND ND ND ND ND ND 5.060 mg/g ND ND ND ND ND ND ND ND ND LOD 0.001 0.0001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.001 0.001 % % % % % % % % % % % Cannabinoid Profile Test Analyzed by Weight Extraction date : Extracted By : 450 3.0795g 08/19/20 12:08:11 965 Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 08/20/20 18:22:56 Analytical Batch -DA014899POT Instrument Used : DA-LC-003 Batch Date : 08/19/20 10:47:27 Reagent Dilution Consums. ID 032320.28 400 280678841 081920.R05 918C4-918J 081920.R04 914C4-914AK 929C6-929H Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Transcript of Certificate of Analysis · 50MG OTG MUSCLE & JOINT CREAM Harvest/Lot ID: # 0519342324 Batch#:...
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # 97164 ___________________
Signature
08/28/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, USA
Kaycha LabsTravel Muscle & Joint 50mg
N/AMatrix: Derivative
Certificateof Analysis
Sample:DA00819007-001Harvest/Lot ID: 000112019
Seed to Sale #N/ABatch Date :N/A
Batch#: 000112019Sample Size Received: 50 gram
Retail Product Size: 10Ordered : 08/18/20Sampled : 08/18/20
Completed: 08/28/20 Expires: 08/28/21Sampling Method: SOP Client Method
Aug 28, 2020 | Green Roads5150 SW 48TH WAYDAVIE, FL, 33314, US
PASSEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthNOT TESTED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesNOT TESTED
CANNABINOID RESULTS
Total THC
0.000%THC/Container :0.000 mg
Total CBD
0.506%CBD/Container :50.600 mg
Total Cannabinoids
0.506%Total Cannabinoids/Container:50.600 mg
CBC CBD CBDA CBDV CBG CBGA CBN D8-THC D9-THC THCA THCV
ND 0.506% ND ND ND ND ND ND ND ND ND
ND5.060mg/g ND ND ND ND ND ND ND ND ND
LOD 0.001 0.0001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.001 0.001
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :450 3.0795g 08/19/20 12:08:11 965
Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 08/20/20 18:22:56Analytical Batch -DA014899POT Instrument Used : DA-LC-003 Batch Date : 08/19/20 10:47:27
Reagent Dilution Consums. ID
032320.28 400 280678841081920.R05 918C4-918J081920.R04 914C4-914AK
929C6-929HFull spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # 97164 ___________________
Signature
08/28/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, USA
Kaycha LabsTravel Muscle & Joint 50mg
N/AMatrix : Derivative
Certificate of Analysis PASSEDGreen Roads
5150 SW 48TH WAYDAVIE, FL, 33314, USTelephone: (844) 747-3367Email: [email protected]
Sample : DA00819007-001Harvest/LOT ID: 000112019Batch# : 000112019Sampled : 08/18/20Ordered : 08/18/20
Sample Size Received : 50 gramCompleted : 08/28/20Expires: 08/28/21Sample Method : SOP Client Method
Page 2 of 4
Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.3 NDACEPHATE 0.01 ppm 3 NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDBIFENAZATE 0.01 ppm 3 NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 3 NDCHLORMEQUAT CHLORIDE 0.1 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.5 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZANON 0.01 ppm 0.2 NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDDIMETHOMORPH 0.02 ppm 3 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 1.5 NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 2 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 2 NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 3 NDKRESOXIM-METHYL 0.01 ppm 1 NDMALATHION 0.02 ppm 2 NDMETALAXYL 0.01 ppm 3 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 3 NDNALED 0.025 ppm 0.5 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL BUTOXIDE 0.1 ppm 3 NDPRALLETHRIN 0.01 ppm 0.4 ND
Pesticides LOD Units Action Level ResultPROPICONAZOLE 0.01 ppm 1 NDPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.05 ppm 1 NDPYRIDABEN 0.02 ppm 3 NDSPINETORAM 0.02 PPM 3 NDSPIROMESIFEN 0.01 ppm 3 NDSPIROTETRAMAT 0.01 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0 PPM 20 ND
TOTAL PERMETHRIN 0.01 ppm 1 NDTOTAL SPINOSAD 0.01 ppm 3 NDTRIFLOXYSTROBIN 0.01 ppm 3 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By585 0.9478g 08/19/20 03:08:50 585
Analysis Method - SOP.T.30.065, SOP.T.40.065 , SOP.T.30.065, SOP.T40.070Analytical Batch - DA014873PESInstrument Used : DA-LCMS-001_DER (PES)Batch Date : 08/18/20 12:09:32
Reagent Dilution Consums. ID062220.12 10 280678841081820.R21 76262-590081820.R22081820.R20
Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060 Sample Preparationfor Pesticides Analysis via LCMSMS and SOP.T40.065 Procedure for Pesticide Quantification Using LCMS). *Volatile Pesticide screening is performed using GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # 97164 ___________________
Signature
08/28/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, USA
Kaycha LabsTravel Muscle & Joint 50mg
N/AMatrix : Derivative
Certificate of Analysis PASSEDGreen Roads
5150 SW 48TH WAYDAVIE, FL, 33314, USTelephone: (844) 747-3367Email: [email protected]
Sample : DA00819007-001Harvest/LOT ID: 000112019Batch# : 000112019Sampled : 08/18/20Ordered : 08/18/20
Sample Size Received : 50 gramCompleted : 08/28/20Expires: 08/28/21Sample Method : SOP Client Method
Page 3 of 4
Residual Solvents PASSED
Solvent LOD Units ActionLevel(PPM)
Pass/Fail Result
1,1-DICHLOROETHENE 0.8 ppm 8 PASS ND
1,2-DICHLOROETHANE 0.2 ppm 2 PASS ND
2-PROPANOL 50 ppm 500 PASS ND
ACETONE 75 ppm 750 PASS ND
ACETONITRILE 6 ppm 60 PASS ND
BENZENE 0.1 ppm 1 PASS ND
BUTANES (N-BUTANE) 500 ppm 5000 PASS ND
CHLOROFORM 0.2 ppm 2 PASS ND
DICHLOROMETHANE 12.5 ppm 125 PASS ND
ETHANOL 500 ppm 5000 PASS ND
ETHYL ACETATE 40 ppm 400 PASS ND
ETHYL ETHER 50 ppm 500 PASS ND
ETHYLENE OXIDE 0.5 ppm 5 PASS ND
HEPTANE 500 ppm 5000 PASS ND
METHANOL 25 ppm 250 PASS ND
N-HEXANE 25 ppm 250 PASS ND
PENTANES (N-PENTANE) 75 ppm 750 PASS ND
PROPANE 500 ppm 5000 PASS ND
TOLUENE 15 ppm 150 PASS ND
TOTAL XYLENES 15 ppm 150 PASS ND
TRICHLOROETHYLENE 2.5 ppm 25 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By850 0.0236g 08/21/20 02:08:26 850
Analysis Method -SOP.T.40.032Analytical Batch -DA014981SOL Reviewed On - 08/24/20 16:13:12Instrument Used : DA-GCMS-002Batch Date : 08/21/20 11:19:30
Reagent Dilution Consums. ID
1 H2017.07700279984161291-111328402
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.40.032 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # 97164 ___________________
Signature
08/28/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, USA
Kaycha LabsTravel Muscle & Joint 50mg
N/AMatrix : Derivative
Certificate of Analysis PASSEDGreen Roads
5150 SW 48TH WAYDAVIE, FL, 33314, USTelephone: (844) 747-3367Email: [email protected]
Sample : DA00819007-001Harvest/LOT ID: 000112019Batch# : 000112019Sampled : 08/18/20Ordered : 08/18/20
Sample Size Received : 50 gramCompleted : 08/28/20Expires: 08/28/21Sample Method : SOP Client Method
Page 4 of 4
Microbials PASSED
Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.STAPHYLOCOCCUS_AUREUS not present in 1 gram.TOTAL_AEROBIC_COUNT 14000PSEUDOMONAS_AERUGINOSA not present in 1 gram.TOTAL YEAST AND MOLD 740 CFU
Analysis Method -SOP.T.40.043 / SOP.T.40.044Analytical Batch -DA014891MIC , DA014893TYM Batch Date : 08/19/20, 08/19/20Instrument Used : PathogenDX PCR_Array Scanner DA-111,PathogenDX PCR_DA-010,DA-111 PathogenDx Scanner,DA-089 Mini-amp Thermocycler
Analyzed by Weight Extraction date Extracted By513, 513 1.0313g 08/19/20 1082, 513
Reagent Consums. ID Consums. ID Consums. ID Consums. ID071020.15101619.03
SG298A918C4-918J914C4-914AK50AX3081919423080717
850C6-850H181019-27411989-024CC-024181207119C28020192803029
A07280700728090052810014D0292804026
28080062811017
Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) methodconsisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoidspurification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus,Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails themicrobiological-impurity testing.
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A+ 0.002 ppm ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA014874MYC | Reviewed On - 08/20/20 16:41:05Instrument Used : DA-LCMS-001_DER (MYC)Batch Date : 08/18/20 12:10:04
Analyzed by Weight Extraction date Extracted By585 1g 08/19/20 04:08:18 585
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.
Heavy Metals PASSED
Reagent Reagent Dilution Consums. ID081320.R13081920.R03071320.08081720.R03081820.R15081820.R14
081720.R24081720.R16081820.R01022520.03030420.06070120.01
100 89401-566
Metal LOD Unit Result Action Level (PPM)
ARSENIC 0.02 PPM ND 3CADMIUM 0.02 PPM NDLEAD 0.05 PPM 0.708 10MERCURY 0.02 PPM ND 55
Analyzed by Weight Extraction date Extracted By53 0.2522g 08/19/20 04:08:22 1022
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA014919HEA | Reviewed On - 08/21/20 09:55:21Instrument Used : DA-ICPMS-001Batch Date : 08/19/20 14:59:55
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.
