CERTIFICATE OF ANALYSIS · 2020-08-04 · A2LA Certificate Number 4329.02 Certificate #4329.02...

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CERTIFICATE OF ANALYSIS prepared for: NULEAF NATURALS 1550 LARIMER ST. #964 A0034S DENVER, CO 80202 Type: Unit Test: Potency Batch ID: 188 Test ID: 4202345.0014 Reported: 14-Jul-2020 Method: TM14 CANNABINOID PROFILE Compound LOQ (mg) Result (mg) Result (mg/g) Delta 9-Tetrahydrocannabinolic acid (THCA-A) 0.22 ND ND Delta 9-Tetrahydrocannabinol (Delta 9THC) 0.11 0.50 0.7 Cannabidiolic acid (CBDA) Delta 8-Tetrahydrocannabinol (Delta 8THC) 0.12 ND ND mg CBD Cannabinolic Acid (CBNA) 0.30 ND ND Cannabinol (CBN) 16mg 0.29 ND ND Cannabidiol (CBD) 0.16 16.00 22.2 Cannabigerol (CBG) 0.11 0.40 0.6 Tetrahydrocannabivarinic Acid (THCVA) 0.19 ND ND 0.13 ND ND Cannabigerolic acid (CBGA) 0.19 ND ND Cannabidivarin (CBDV) 0.15 0.30 0.4 Cannabichromenic Acid (CBCA) 0.16 ND ND Tetrahydrocannabivarin (THCV) 0.10 ND ND Cannabidivarinic Acid (CBDVA) 0.27 ND ND Total Potential THC** 0.50 0.70 Total Potential CBD** 16.00 22.25 Cannabichromene (CBC) 0.20 0.60 0.8 Total Cannabinoids 17.80 24.75 NOTES: % = % (w/w) = Percent (Weight of Analyte / Weight of Product) # of Servings = 1, Sample Weight=0.71923g N/A * Total Cannabinoids result reflects the absolute sum of all cannabinoids detected. ** Total Potential THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during decarboxylation step. Total THC = THC + (THCa *(0.877)) and Total CBD = CBD + (CBDa *(0.877)) ND = None Detected (Defined by Dynamic Range of the method) FINAL APPROVAL Testing results are based solely upon the sample submitted to Botanacor Laboratories, LLC, in the condition it was received. Botanacor Laboratories, LLC warrants that all analytical work is conducted professionally in accordance with all applicable standard laboratory practices using validated methods. Data was generated using an unbroken chain of comparison to NIST traceable Reference Standards and Certified Reference Materials. This report may not be reproduced, except in full, without the written approval of Botanacor Laboratories, LLC. ISO/IEC 17025:2005 Accredited A2LA Certificate Number 4329.02 Certificate #4329.02 BoWanacor LaboraWorieV, All RighWV ReVerYed _ 1301 S JaVon SW UniW K, DenYer, CO 80223 _ 888.800.8223 _ ZZZ.boWanacor.com PREPARED BY / DATE APPROVED BY / DATE 0.00% 0.07% 0.00% 2.22% THCa delta 9 THC CBDa CBD Ryan Weems Ben Minton 14-Jul-2020 14-Jul-2020 2:34 PM 5:30 PM

Transcript of CERTIFICATE OF ANALYSIS · 2020-08-04 · A2LA Certificate Number 4329.02 Certificate #4329.02...

Page 1: CERTIFICATE OF ANALYSIS · 2020-08-04 · A2LA Certificate Number 4329.02 Certificate #4329.02 BoWanacor LaboraWorie, All RighW Reered _ 1301 S Jaon S UniW K, DenYer, CO 80223 _ 888.800.8223

CERTIFICATE OF ANALYSISprepared for: NULEAF NATURALS

1550 LARIMER ST. #964

A0034SDENVER, CO 80202

Type: Unit

Test: Potency

Batch ID: 188 Test ID: 4202345.0014

Reported: 14-Jul-2020 Method: TM14

CANNABINOID PROFILECompound LOQ (mg) Result (mg) Result (mg/g)

Delta 9-Tetrahydrocannabinolic acid (THCA-A) 0.22 ND NDDelta 9-Tetrahydrocannabinol (Delta 9THC) 0.11 0.50 0.7Cannabidiolic acid (CBDA)

Delta 8-Tetrahydrocannabinol (Delta 8THC) 0.12 ND NDmg CBD Cannabinolic Acid (CBNA) 0.30 ND ND

Cannabinol (CBN)

16mg

0.29 ND NDCannabidiol (CBD) 0.16 16.00 22.2

Cannabigerol (CBG) 0.11 0.40 0.6Tetrahydrocannabivarinic Acid (THCVA) 0.19 ND ND

0.13 ND NDCannabigerolic acid (CBGA) 0.19 ND ND

Cannabidivarin (CBDV) 0.15 0.30 0.4Cannabichromenic Acid (CBCA) 0.16 ND ND

Tetrahydrocannabivarin (THCV) 0.10 ND NDCannabidivarinic Acid (CBDVA) 0.27 ND ND

Total Potential THC** 0.50 0.70Total Potential CBD** 16.00 22.25

Cannabichromene (CBC) 0.20 0.60 0.8

Total Cannabinoids 17.80 24.75

NOTES:% = % (w/w) = Percent (Weight of Analyte / Weight of Product) # of Servings = 1, Sample Weight=0.71923g

N/A

* Total Cannabinoids result reflects the absolute sum of all cannabinoids detected.

** Total Potential THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during decarboxylation step. Total THC = THC + (THCa *(0.877)) and Total CBD = CBD + (CBDa *(0.877)) ND = None Detected (Defined by Dynamic Range of the method)

FINAL APPROVAL

Testing results are based solely upon the sample submitted to Botanacor Laboratories, LLC, in the condition it was received. Botanacor Laboratories, LLC warrants that all analytical work is conducted professionally in accordance with all applicable standard laboratory practices using validated methods. Data was generated using an unbroken chain of comparison to NIST traceable Reference Standards and Certified Reference Materials. This report may not be reproduced, except in full, without the written approval of Botanacor Laboratories, LLC. ISO/IEC 17025:2005 Accredited A2LA Certificate Number 4329.02

Certificate #4329.02

Botanacor Laboratories™, All Rights Reserved | 1301 S Jason St Unit K, Denver, CO 80223 | 888.800.8223 | www.botanacor.com

PREPARED BY / DATE APPROVED BY / DATE

0.00%

0.07%

0.00%

2.22%

THCa

delta 9 THC

CBDa

CBD

Ryan Weems Ben Minton14-Jul-2020 14-Jul-20202:34 PM 5:30 PM

Page 2: CERTIFICATE OF ANALYSIS · 2020-08-04 · A2LA Certificate Number 4329.02 Certificate #4329.02 BoWanacor LaboraWorie, All RighW Reered _ 1301 S Jaon S UniW K, DenYer, CO 80223 _ 888.800.8223

Testing results are based solely upon the sample submitted to Botanacor Laboratories, LLC, in the condition it was received. Botanacor Laboratories, LLC warrants that all analytical work is conducted professionally in accordance with all applicable standard laboratory

practices using validated methods. Data was generated using an unbroken chain of comparison to NIST traceable Reference Standards and Certified Reference Materials. This report may not be reproduced, except in full, without the written approval of Botanacor Laboratories,

LLC.

Botanacor Laboratories™, All Rights Reserved | 1301 S Jason St Unit K, Denver, CO 80223 | 888.800.8223 | www.botanacor.com

PREPARED BY / DATE APPROVED BY / DATE

* ND = None Detected (Defined by Dynamic Range of the method)

FINAL APPROVAL

Mercury 0.062 - 6.23 ND

Lead 0.066 - 6.58 ND

Arsenic 0.065 - 6.54 ND

Cadmium 0.066 - 6.62 ND

Analyte Dynamic Range (ppm) Result (ppm)

Type: Concentrate

Test: Metals

HEAVY METALS

Batch ID: N/A Test ID: T000085074

Reported: 14-Jul-2020 Method: TM19

CERTIFICATE OF ANALYSISprepared for: NULEAF NATURALS

1550 LARIMER ST. #964

A0034SDENVER, CO 80202

14-Jul-202010:34 AM 3:26 PM

Ryan Weems Ben Minton14-Jul-2020

Page 3: CERTIFICATE OF ANALYSIS · 2020-08-04 · A2LA Certificate Number 4329.02 Certificate #4329.02 BoWanacor LaboraWorie, All RighW Reered _ 1301 S Jaon S UniW K, DenYer, CO 80223 _ 888.800.8223

Botanacor Laboratories™, All Rights Reserved | 1301 S Jason St Unit K, Denver, CO 80223 | 888.800.8223 | www.botanacor.com

TYM: None DetectedTotal Aerobic: None Detected

FINAL APPROVAL

PREPARED BY / DATE APPROVED BY / DATE

Testing results are based solely upon the sample submitted to Botanacor Laboratories, LLC, in the condition it was received. Botanacor Laboratories, LLC warrants that all analytical work is conducted professionally in accordance with all applicable standard laboratory

practices using validated methods. Data was generated using an unbroken chain of comparison to NIST traceable Reference Standards and Certified Reference Materials. This report may not be reproduced, except in full, without the written approval of Botanacor Laboratories,

LLC. ISO/IEC 17025:2005 Accredited A2LA Certificate Number 4329.03Certificate #4329.03

Free from visual mold, mildew, and foreign matter

* CFU/g = Colony Forming Unit per Gram** Values recorded in scientific notation, a common microbial practice of expressing numbers that are too large to be conveniently written in decimal form.

Examples: 10^2 = 100 CFU10^3 = 1,000 CFU10^4 = 10,000 CFU10^5 = 100,000 CFU

NOTES:

Salmonella None Detected

Total Coliforms** None Detected

Total Yeast and Molds** None Detected

E. coli None Detected

Contaminant Result (CFU/g)*

Total Aerobic Count** None Detected

Type: Concentrate

Test: Microbial Contaminants

MICROBIAL CONTAMINANTS

Batch ID: N/A Test ID: T000085071

Reported: 12-Jul-2020 Method: Concentrate - Test Methods: TM05, TM06

CERTIFICATE OF ANALYSISprepared for: NULEAF NATURALS

1550 LARIMER ST. #964

A0034SDENVER, CO 80202

Robert Belfon Greg Zimpfer12-Jul-2020 12-Jul-20203:59 PM 7:44 PM

Page 4: CERTIFICATE OF ANALYSIS · 2020-08-04 · A2LA Certificate Number 4329.02 Certificate #4329.02 BoWanacor LaboraWorie, All RighW Reered _ 1301 S Jaon S UniW K, DenYer, CO 80223 _ 888.800.8223

Compound Dynamic Range (ppb) Result (ppb) Compound Dynamic Range (ppb) Result (ppb)

Testing results are based solely upon the sample submitted to Botanacor Laboratories, LLC, in the condition it was received. Botanacor Laboratories, LLC warrants that all analytical work is conducted professionally in accordance with all applicable standard laboratory

practices using validated methods. Data was generated using an unbroken chain of comparison to NIST traceable Reference Standards and Certified Reference Materials. This report may not be reproduced, except in full, without the written approval of Botanacor Laboratories,

LLC.

Botanacor Laboratories™, All Rights Reserved | 1301 S Jason St Unit K, Denver, CO 80223 | 888.800.8223 | www.botanacor.com

PREPARED BY / DATE APPROVED BY / DATE

* ND = None Detected (Defined by Dynamic Range of the method)N/A

FINAL APPROVAL

Kresoxim-methyl 49 - 2499 ND* Trifloxystrobin 44 - 2499 ND*Imidacloprid 47 - 2499 ND* Thiamethoxam 41 - 2499 ND*Imazalil 287 - 2499 ND* Thiacloprid 43 - 2499 ND*Hexythiazox 43 - 2499 ND* Tebuconazole 309 - 2499 ND*Fludioxonil >305 ND* Spiroxamine 2 18 - 2499 N/AFlonicamid 44 - 2499 ND* Spiroxamine 1 15 - 2499 N/AFipronil 58 - 2499 ND* Spirotetramat >303 ND*Fenoxycarb >42 ND* Spiromesifen >294 ND*Etoxazole 298 - 2499 ND* Spinosad D 79 - 2499 ND*Etofenprox 42 - 2499 ND* Spinosad A 30 - 2499 ND*E-Fenpyroximate 27 - 2499 ND* Pyridaben 42 - 2499 ND*Dimethoate 43 - 2499 ND* Propoxur 44 - 2499 ND*Dichlorvos >288 ND* Prophos 299 - 2499 ND*Diazinon 300 - 2499 ND* Phosmet 41 - 2499 ND*Clofentezine 284 - 2499 ND* Permethrin 268 - 2499 ND*Chlorpyrifos 40 - 2499 ND* Paclobutrazol 45 - 2499 ND*Chlorantraniliprole 49 - 2499 ND* Oxamyl 39 - 2499 ND*Carbofuran 44 - 2499 ND* Naled 42 - 2499 ND*Carbaryl 45 - 2499 ND* Myclobutanil 47 - 2499 ND*Boscalid 35 - 2499 ND* MGK 264 2 99 - 2499 ND*Bifenazate 38 - 2499 ND* MGK 264 1 169 - 2499 ND*Azoxystrobin 45 - 2499 ND* Methomyl 41 - 2499 ND*Abamectin >366 ND* Methiocarb 43 - 2499 ND*

ND*Acetamiprid 44 - 2499 ND* Metalaxyl 41 - 2499 ND*

PESTICIDE RESIDUE

Acephate 42 - 2499 ND* Malathion 306 - 2499

Test: Pesticides

Batch ID: Test ID: 6479398.0026

Reported: 13-Jul-2020 Method: TM17

CERTIFICATE OF ANALYSISprepared for: NULEAF NATURALS

1550 LARIMER ST. #964

A0034SDENVER, CO 80202

Type: Concentrate

13-Jul-20205:15 PM 6:59 PM

Tyler Wiese Greg Zimpfer13-Jul-2020

Page 5: CERTIFICATE OF ANALYSIS · 2020-08-04 · A2LA Certificate Number 4329.02 Certificate #4329.02 BoWanacor LaboraWorie, All RighW Reered _ 1301 S Jaon S UniW K, DenYer, CO 80223 _ 888.800.8223

PREPARED BY / DATE APPROVED BY / DATE

Testing results are based solely upon the sample submitted to Botanacor Laboratories, LLC. Botanacor Laboratories, LLC warrants that all analytical work is conducted professionally in accordance with all applicable standard laboratory practices using validated methods. Data was generated using an unbroken chain of comparison to NIST traceable Reference Standards and Certified Reference Materials. This

report may not be reproduced, except in full, without the written approval of Botanacor Laboratories, LLC. ISO/IEC 17025:2005 Accredited A2LA Certificate Number 4329.02

Certificate #4329.02

Botanacor Laboratories™, All Rights Reserved | 1301 S Jason St Unit K, Denver, CO 80223 | 888.800.8223 | www.botanacor.com

FINAL APPROVAL

0.136% 1.36

NOTES:0

gamma-Terpinene 0.000 0Terpinolene 0.000 0

(-)-beta-Pinene 0.000 0alpha-Terpinene 0.000 0

beta-Ocimene 0.000 0alpha-Pinene 0.000 0

trans-Nerolidol 0.005 0.05Ocimene 0.000 0

beta-Myrcene 0.000 0cis-Nerolidol 0.000 0

d-Limonene 0.000 0PREDOMINANT TERPENES Linalool 0.002 0.02

alpha-Humulene 0.022 0.22(-)-Isopulegol 0.000 0

Eucalyptol 0.000 0Geraniol 0.000 0

beta-Caryophyllene 0.045 0.45

Total Terpenes

(-)-Caryophyllene Oxide 0.000 0p-Cymene 0.000 0

0.062 0.62Camphene 0.000 0delta-3-Carene 0.000 0

TERPENE PROFILE

0.136%

Compound %(w/w) mg/g(-)-alpha-Bisabolol

Type: Concentrate

Test: Terpenes

Batch ID: Test ID: 6090757.001

Reported: 14-Jul-2020 Method: TM10

CERTIFICATE OF ANALYSISprepared for: NULEAF NATURALS

1550 LARIMER ST. #964

A0034SDENVER, CO 80202

0.000%

0.000%

0.000%

0.000%

0.000%

0.000%

0.002%

0.045%

0.022%

0.062%

alpha-Pinene

(-)-beta-Pinene

beta-Myrcene

delta-3-Carene

alpha-Terpinene

d-Limonene

Linalool

beta-Caryophyllene

alpha-Humulene

(-)-alpha-Bisabolol

Ryan Weems14-Jul-20205:46 PM

Ben Minton14-Jul-20206:32 PM

Page 6: CERTIFICATE OF ANALYSIS · 2020-08-04 · A2LA Certificate Number 4329.02 Certificate #4329.02 BoWanacor LaboraWorie, All RighW Reered _ 1301 S Jaon S UniW K, DenYer, CO 80223 _ 888.800.8223

* ND = None Detected (Defined by Dynamic Range of the method)

Botanacor Laboratories™, All Rights Reserved | 1301 S Jason St Unit K, Denver, CO 80223 | 888.800.8223 | www.botanacor.com

PREPARED BY / DATE APPROVED BY / DATE

Testing results are based solely upon the sample submitted to Botanacor Laboratories, LLC, in the condition it was received. Botanacor Laboratories, LLC warrants that all analytical work is conducted professionally in accordance with all applicable standard laboratory

practices using validated methods. Data was generated using an unbroken chain of comparison to NIST traceable Reference Standards and Certified Reference Materials. This report may not be reproduced, except in full, without the written approval of Botanacor Laboratories,

LLC. ISO/IEC 17025:2005 Accredited A2LA Certificate Number 4329.02Certificate #4329.02

NOTES:N/A

FINAL APPROVAL

Toluene 19 - 386 *NDXylenes

(m,p,o-Xylenes) 139 - 2786 *ND

Benzene 0.2 - 4.3 *NDHeptanes 101 - 2010 *ND

Hexane 6 - 130 *NDEthyl Acetate 107 - 2134 *ND

Acetone 105 - 2103 *NDIsopropyl Alcohol 109 - 2175 *ND

Pentane 95 - 1908 *NDEthanol 91 - 1828 *ND

Butanes (Isobutane, n-Butane) 155 - 3105 *ND

Methanol 65 - 1295 *ND

RESIDUAL SOLVENTS

Solvent Dynamic Range (ppm) Result (ppm)Propane 80 - 1591 *ND

Type: Concentrate

Test: Residual Solvents

Batch ID: Test ID: t000075208

Reported: 14-May-2020 Method: TM04

CERTIFICATE OF ANALYSISprepared for: NULEAF NATURALS

1550 LARIMER ST. #964

A0034SDENVER, CO 80202

Ryan Weems14-May-20207:38 PM

Ben Minton14-May-20208:38 PM