CASE NUMBER 3940 - INORGANIC ANALYSIS DATA PACKAGE

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California Analytical laboratories. Inc. 2544 Industrial Boulevard • West Sacramento, CA QS691 • (916) 372-1393

U.5. EPA Contract Laboratory Program Sample Management Office P.0. Box 818 - Alexandria, VA 22313 703/ 557-2li90 ITS: 8-557-2490

DATE REPORTED: 4/11/eS Date Received: 2/19/ffj

COVER PAGE INORGANIC ANALYSESDATA PACKAGE --- -

Lab Same: California Analytical Labs, Inc. Case No.: 3940 Q.C. Report No.:

Sam12l~ Surnbers

EPA ~o. Lab ID No. EPA No. ---~- P2185- -MFA102 MFA101 MFA103 P2187 MFA104 MFA105 P2189 MFA106 MFA107 P2191 MH108 MF:\109 P2193 MFAllO HFAl 11 P2195 MFA112 MFAil3 P2197 ~WA114 HF AllS P2199 t-WA 116 MFA117 P2201 MFA118 MFA119 P2203 MFA120 :'fFA121 P2205 MFA122 MFA123 P2207 MFA124 MFA125 P2209 MFA126 MFA127 P2211 MFA128 MFA129 P2213 MFA130 MFA131 P2215 MFA132 MFA133 P2217 MFA134 >IF Al 35 P2219 MFA136 MFA137 P2221 MFA138 MFA139 P2223 HFA140 MFA141 P2225 MFA142 MFA143 P2227 MFA144 MFA145 P2229 MFA146

ICP Interelement and background corrections applied? Yes. Footnotes: NR - not required by contract at this time

3940

Lab ID No. P2186~

P2188 P2190 P2192 P2194 P2196 P2198 P2200 P2202 P2204 P2206 P2208 P2210 P2212 P2214 P2216 P27.18 P2220 P2222 P2224 P2226 P2228 P2230

Value - If the result is a \'alu;~ greater than or equal to the instrument detection limit but less than the contract required detection limit, report the value in brackets (i.e. [10] ). Indicate the analytical method used with P (for ICP/Flame AA), F (for furnace), or CV (for cold vapor).

U - Indicates element was analyzed for but not detected. Report with the detection limit value (e.g., <IOU).

E - Indicatea a value estimated or not reported due to the presence of inter-ference. Explanatory note included on cover page.

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Case ~o.: 3940 DATE REPORTED: 4/11/85

s R

- Indicates value determined by Method of Standard Addition. - Indicates spike sample recovery is not within control limits.

* +

- Indicates duplicate analysis is not within control limits. Indicates the correlation coefficient for method of standard addition less than 0.995

Co1l'l:Jents: ~ recoveries for several elements were outside ~ recommended windotos, ~tl:tJ! .. could be caused Er, matrix interferences.

QcJ9a<U~ Mark Masino

LA -~~A !). ~ ~Jh~;y--S. ~vong, PhD d

Director of Inorganic Services Vice President

~ Research and Analytical Services

Inorganics Lab Manager

California Anoli.,tical Loborotories, Inc.

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U.S. EPA CON ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFAl0l :: f c~ 3 DATE: 4/9/85 )5 >' i Lcf 2" 1

INORGANIC ANALYSIS SHEET

LAB NAME: CALIF.ANAL.LAB. CASE NO:3940 SOW NO.: 68-01-6810 QC RPT.13940 LAB.SAMPLE NO.: P2185

ELEMENTS IDENTIFIED ANO MEASURED

CONC.: MATRIX:

LOW~ SOIL:

ELEMENTS,.METHOO l. ALUMINIUM •• , P 2 • ANTIMONY •••• P J, ARSENIC .... ,p 3. ARSENIC •.... F 4. BARIUM •••••• P 5. BERYLLIUM, •• P 6. CADMIUM ••••• P 7. CALCIUM ••••• P a. CHROMIUM ••• &P 9. COBALT ...... P 10. COPPER .••.•• P 11 • IRON ••• , , ••• P 12. LEAD ••••• , •• P 12 • LEAD .••••.•• F 13. MAGNESiill1 ••• P 14.MANGANESE .•. P 15.MERCURY .•.• cv 16. NICKEL •••••• P 17.POTASSIUM ..• P 18. SELENIUM ... , P 18, SELENIUM ••• , F 19.SILVER ..•... P 2 0. SODitJM. , •• , • P 2 l. THALLIUM •••• F 22 • TIN ••••••••• P 2 .3 • VANADIUM ..•. P 24. ZINC ••.• , •• , P 25.CYANIDE ... , .C

% SOLID

COMMENTS:

[ (

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[

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(

MEDIUM: XX xx

MG/KG DRY WEIGHT 3071 <7 u R

"2'fr Iv I,,... JJ <r, <2. 3 U

49) 0.4]

<:2.0 868)

7 * <3.5 u

7] 3928 * N/R

31. 8 s 195] 208 *

0. ff 1,-~ If,..., R <17 u

510) N/R

<2,1 U <l.3 u R

478] <2.1 u

<18 u 9.1]

12 N/R

85

LAS MANAGER:ffe-"'-

,.. ~ .,1..., ,·,.. L .. &,..,

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U.S. EPA COh ACT LABORATORY PROGRAM Si\MPLE MANAGEMENT OFFICE E'FA SAMPLE NO:

MFJ..102 ~ i 01..,t P.O. BOX 818 ALEXANDRIA,VA 22313 103/557-2490 FTS:8-557-2490 DATE:4/'.i/85 G:..r, ~- Le I LJ


LAB NAME: CALIF.ANAL.LAB, CASF. N0:3940 SOW NO.: 68-01~6810 QC RPT.i3S40 LAB.SAMPLE NO.: P2186

ELEMENTS IDENTIFIED AND MEASURED

CONC.: LOW: MEDIUM: XX MATRIX: SOIL: xx

ELEMENTS •. METHOO MG/KG DRY WEIGHT l. ALUMINIUM. , • P 8895 2, ANTIMONY •••• P <7 u R 3. ARSENIC.,, .. P N/R 3 • ARSENIC •...• F C 2,5) 4. BARIUM ••••• , P 151 s. BERYLLIUM, •• P [ 1.0) 6. CADMIUM, •••• P <2.0 7. CALCIUM •• , • , P ( 1003] 8. CHROMIUM,,, .P 12 * 9. COBALT •••• , • P ( 7] 10,COPPER.,,, .. P ( 6] 11.IRON .. , •.... P 6581 * 12, LEAD .••••••. P N/R 12.LEAO ..... , .. F 9.3 s 13.MAGNESIUM .• ,P ( 685) 14.MANGANESE ... P 344 * 15.MERCURY .••• cv <O.l u R 16,NICKEL,,, ... P <17 u 17.POTASSIUM ... P ( 978] 18. SELENIUM •• , , P N/R 18. SELENIUM. , •• F <2,1 u 19 • SILVER • , , • • • P <1.3 u R 20. SODitJM •••••• P [ 1238} 21. THALLIUM. , •• F <2.1 u 22. TIN .••• , •••• P <18 u 2 3 • VANADIUM. , •• P [ 17,3] 24.ZINC ...•.... P 165 25. CYANIDE ••••• C N/R

% SOLID 86

COMMENTS:

LAB MANAGER: rf:?----...

2

0 tr'\

"' 0 0 0 -

I


U.S. EPA COi .ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFA103 :: 'Ii?(/-P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE: 4/9/85 L _ K-'/ 1


LAB NAME: CALIF.ANAL.LAB, CASE NO:3940 SOW NO.: 68-01-6810 QC RPT,#3940 LAB.SAMPLE NO.: P2l87


CONC.: LOW: MATRIX: SOIL:

ELEMENTS. ,METHOD 1. ALUMINIUM., .P 2 • ANTIMONY •• , • P J. ARSENIC ... ,.P J. ARSENIC ...• ,F [ 4. BARIUM ...... P [ 5. BERYLLIUM ... P ( 6 . CADMIUM ..... P 7, CALCIUM ...•. P [ 8, CHROMIUM .. , .P 9, COBALT ..•..• P 10,COPPER •.... ,p [ 11,IRON ••...•. ,P 12. LEAD •••••••• P 12. LEAD •••••••• r' 13.MAGNESIUM ... P 14.MANGANESE .. ,P 15,MERCURY, ... CV 16.NICKEL ..•... P 17,POTASSIUM,.,P 18.SELENIUM .... P 18.SELENIUM .... F 19.SILVER •....• P 20,SODIUM •....• P 21,THALLIUM .•.. F 22,TIN ...•.. , .. P 23,VANADIUM .•.. P 24,ZINC .•••.•• ,p 25,CYAN!DE., ... C

% SOLID

COMMENTS:

(

(

[

(

xx MEDIUM: XX

MG/KG DRY WEIGHT 3082 <7 u R N/R 2.8)

33] 0.4]

<2,0 526]

7 * <3.5 U 7]

4352 * N/R

24.4 s 188]

64 * <0.1 U R <17 U

743] J\J .. ~ tv/R

<2.1 U <l.3 U R

576] <2.1 U

<10 U 1:3.lJ

535 N/R

82

LAB MANAGER: ;!/4~

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3

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U.S. EPA CON ..ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: 1 MFA104 = 'f-Cl) ;; .... ~., ... "'" P,O, BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE: 4/9/85 ti L ,, ,·. L. t- .!_


LAB NAME: CALIF.ANAL.LAB. CASE NO:3940 SOW NO.t 68-01-6810 QC RPT,#3940 LAB.SAMPLE NO.: P2l88


CONC,: LOW: MATRIX: SOIL: xx

ELE:MENTS .. METHOD l. ALUMINIUM •.. P 2. ANTIMONY .... P 3 • ARSENIC., ••. P 3. ARSENIC ••••• F 4 • BARIUM., •••• P ( s. BERYLLIUM ••• P 6, CADMIUM ••••• P 7, CALCIUM ••• I Ip 8. CHROMIUM •• I. p [ 9. COBALT •••••• P 10.COPPER ...... P ( 11. IRON •••••••• P 12. LEAD, ••••••• P 12. LEAD ........ F 13,MAGNESIUM ... P 14,MANGANESE ... P 15,MERCURY .... CV 16,NICKEL ..• , .. P 17.POTASSIUM ... P [ 18.SELENIUM., ,,p 18.SELENIUM .... F 19, SILVER ... , .. P 20.SODIUM .•..•• P [ 21.THALLIUM, ... F 22.TIN ••••••••• P 23,VANADIUM .... P ( 24,ZINC •....... P 25.CYANIDE ..... C

% SOLID

COMMENTS:

MEDIUM: xx

MG/KG DRY' WEIGHT 1553 <7 u R N/R

<2.3 u 11]

<0.3 u <2.0

<214 u 4) * <3.5 u 2]

703 * N/R 4,2 s

<184 u 15 *

<0.1 u R <17 u

493] ""2-4-..AIA /df-,

<2.1 u <1.3 u R

1351] <2.1 u

<18 u 5.2] 342 N/R

91

"/ LAB MANAGER: w,,cy- l.

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0 0 0 -


U.S. EPA COh ~CT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFA105 = 'IL lb P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE: 4/ 9'/85


LAB NAME: CALIF.ANAL.LAB. CASE NO:3940 SOW NO.: 68-01-6810 QC RPT.#3940 LAB.SAMPLE NO.: P2189


CONC.: LOW: MATRIX: SOIL~

ELEMENTS •• METHOD l • ALUMINIUM ••• P 2 • ANTIMONY •••• P 3. ARSENIC ..... P 3. ARSENIC, ..•. F 4. BARIUM •••••• P 5 • BERYLLIUM ••• P 6 • CADMIUM . . . . . P 7. CALCIUM ..... P 8 • CHROMIUM • • • • P 9. COBALT •••••• P 10. COPPER .•••.• P 11. IRON •••••••• P 12. LEAD ........ P 12. LEAD, ••••••• F 13.MAGNESIUM ... P 14.MANGANESE ... P 15 .MERCURY •••• CV 16.NICKEL ...•.. P 17. POTli.SSitJM ••• P 18 • SELENIUM •. , • P 18. SELENIUM •••• F 19,SILVER .....• P 2 0 • SODIUM •• , , , , P 21,THALLIUM .... F 22,TIN,., ..... ,P 2 3 • VANADIUM, ••• P 24,ZINC.,, .•... P 25,CYANIDE •..•. c

% SOLID

COMMENTS:

( [

(

(

[

[

[

(

xx MEDIUM: XX

11:G/KG DRY WEIGHT 3157 <7 U R

-¥]....~{ flt-<2. 3 U

34] 0.3] 4,5 991)

6 * <3.5 U 5)

3557 * N/R

60.l s 200] 125 *

<0.1 U R <17 U

353) "2-0.__.lv/4 tk~

<2.1 U <1.3 U R

534] <2.1 U

<18 U 9,0] 302 N/R

74

5

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0 0 0 --


U.S. EPA COh .{ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SA}1PLE NO: 6 P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA106 = 'lv~l_ DATE: 4/9/85


LAB NAME: CALIF.ANAL.LAB. CASE N0:3940 SOW NO.: 68-01-6810 QC RPr.#3940 LAB.SAMPLE NO.: P2190



ELEMENTS .. METHOD l. ALUMINIUM ••• P 2. ANTIMONY •••• P 3. ARSENIC •..•. P 3, ARSENIC ••••• F 4, BARIUM ...... P 5. BERYLLIUM ..• P 6. CADMIUM ..... P 7, CALCIUM ...•. P 8 • CHROMIUM • • • • P 9. COBALT ....•. P 10.COPPER .•.... P 11.!RON •••••••• P 12.LEAD .•...... P 12. LEAD .......• F 13,MAGNESIUM ... P 14.MANGANESE .•• P 15.MERCURY ..•. cv 16,NICKEL •..... P 17.POTASSIUM .•. P 18.SELENIUM ..•. P 18.SELENIUM .... F 19, SILVER ...... P 20,SODIUM ..•... P 21,THALLIUM .•.. F 2 2 • TIN ••••••••• P 23.VANADIUM .... P 24.ZINC ..•..... P 25.CYANIDE ... , .C

% SOLID

COMMENTS:

xx

( (

(

(

(

(

[

[

MEDIUM: XX

MG/KG DRY WEIGHT 6059 <7 U

1-1/K. ~[<Iv,.., R

<2. 3 U 49)

0.5] <2.0 2253)

11 * <3.5 U

11) 9629 * N/R

89.3 s 453) 180 *

<0.1 U R <17 U

926] ZS-. fVjtt rl~---

<2.1 U <1.3 U R

704] <2.1 U

<18 U 16.7)

164 N/R

70

LAB 11.,\NAGER: /j:&-/

5 •~' t,\ I.' {;

BLl<4, l,--f:_ .z.c

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U.S. EPA CON ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

EPA SAMPLE No: MFAl07 ° 'I(.) 'i 1

DATE: 4/9/85


LAB NAME: CALIF.ANAL.LAB. CASE NO:3940 SOW NO.: 68-01-5810 QC RPT,13940 LAB. SAMPLE NO. : P2 l9 l

E~EMENTS IDENTXFIEO AND.MEASURED CONC.: LOW: MATRIX: SOIL:

ELEMENTS .. METHOD 1. ALUMINIUM .•• P 2. ANTIMONY ..•• p 3. ARSENIC .•... P 3. ARSENIC ••.•• F 4. BARIUM ..•.•• p 5. BERYLLIUM •.. p 6. CADMIUM ..••• p 7. CALCIUM •..•• p 8. CHROMIUM .... p 9. COBALT ••.••• P 10.COPPER .•.••• ? 11. IRON •..••••. P 12. LEAD •••.•.•. P 12. LEAD •••••••• F 13,MAGNES!UM, .• P 14,MANGANESE .•• p 15.MERCURY •..• cv 16.NICKEL •..... P 17.POTASSIUM, •• P 18.SELENIUM .•. ,p 18.SELENIUM •••• F 19.SILVER .•••.• P 20.SODIUM •••••• P 21.THALLIUM •••• F 22.TIN ••••.•••. P 23.VANADIUM ..•• P 24.ZINC ••..••.. P 25.CYANIDE •...• c

% SOLID

COMMENTS:

{

[

(

(

[

xx MEDIUM: XX

MG/KG DRY WEIGHT 1989 <7 U R

N/R 44.0 S

118 0.3)

<2.0 805]

lo * <:'l.S U

16 75120 *

N/R 34.9 S

250J 142 *

<0,1 U R <17 U

1855] N/R

<2.1 U <l. 3 U R

5139 <2,l U

<18 U 15.2]

28 N/R

83

LAB MANAGER: /4~-;,

7 s ~c.., ~.r.....: .... iJL1'.:.. L.:tL

tr. 0 0 0


U.S. EPA COh ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MF Al OS -= 'Io 7 'fl DATE: 4/9/85


LAB NAME~ SOW NO.:

CALIF.ANAL.LAB. CASE NO:3940

LAB. SAMPLE NO. : 68-01-6810 QC RPT,#3940 ·P2-3·1·9 2- p;,,: /',':: SP--

ELEMENTS IDENTIFIED MD MEA~URED

CONC,: LOW: MATRIX: SOIL:

ELEMENTS •. METHOD 1. ALUMINIUM ••• P 2. ANTIMONY, ... P 3, ARSENIC ..••• P 3. ARSENIC •.... F 4. BARIUM, ..... P 5. BERYLLIUM ... P 6, CADMIUM ••••• P 7 • CALCIUM ••••• P 8 • CHROMIUM •••• P 9. COBALT •..... P 10.COPPER ...•.. P 11. IRON •••••••• P 12. LEAD •••••••• P 12. LEAD •••••••• F 13 .MAGNESIUM ••• P 14,MANGANESE •. ,P 15,MERCURY .•.. cv 16.NICKEL .•.•.• P 17. POTASSIUM ••• P 18 • SELENIUM •••• P 18. SELENIUM •••• F 19.SILVER ....•• P 20. SODitJM •• , • , • P 2 l. THALLIUM •••• F 2 2. TIN ••••••••• P 2 3 • VAHADIUM •••• P 24,ZINC ........ P 25.CYANIDE ..... C

% SOLID

COMMENTS:

xx

[

(

(

MEDIUM: XX

MG/KG DRY WEIGHT 2153 <7 u R N/R 3. 3)

44) 0. 4)

11.7 1551]

5) * <3,5 u 11)

2933 * N/R 482.1

<184 u 224 * <0.1 U R

<17 u 468] ·~fa_ µ19--.

<2.1 U <1.3 u R

594) <2.1 U

<18 u 6.9]

2170 li/R

84

LAB MANAGER:ffe7

8 ~ ' r :, .... b~ .... ,·i<..1.....• \~

RLK .). i- .. C ,:l

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U, S, EPA. COl :ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA109 -:: 'f C'} 3 D,\TE: 4/9/8 5


LAB NAME: CALIF.ANAL.LAB. CASE NO:3940 SOW NO,: 68-01-6810 QC RPT.#3940 LAB.SAMPLE NO.: P2193

ELEMENTS IOENTI.FlE-0 ANO MEA$tJREO.


ELEMENTS, ,METHOD 1, ALUMINiuM ..• P 2, ANTIMONY •..• P 3, ARSENIC .•..• P 3, ARSENIC .. , .,F 4, BARIUM .. , ... P S. BERYLLIUM, .. P 6, CADMIUM ...•• P 7, CALCIUM •. , .,P 8, CHROMIUM, ... P 9, COBALT ..• , ,,p 10,COPPER .... , ,P 11.IRON ..... , .. P 12 • LEAD. , . , ..•. P 12. LEAD •••••• , • F 13,MAGNESIUM,, .P 14. MANGANESE, •• P 15,MERCURY .... CV 16,NICKEL .•.... P 17,POTASSIUM .. ,P 18,SELENIUM .... P 18.SELENIUM, ... F 19,SILVER ...... P 20.SOOIUM ..•... P 21.THALLIUM, ,,.F 22,TIN ...•..... P 23,VANADIUM •••• P 24.ZINC ....•.. ,P 25,CYANIDE ...•. c

% SOLID

COMMENTS:

( (

(

(

[

(

(

xx MEDIUM: XX


N/R <2.3 u

41] 0.5]

<2.0 274]

10 * <3,5 U SJ

8512 * H/R 6.6 382)

27 * <0,1 U R <17 U

752J lv/r, ~ Ju-

<2.1 U <1.3 u R

600] <2.1 U

<18 U 18.4]

20 N/R

83

LAB MANAGER: ilp-7

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0 C' 0

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U.S. EPA COl .ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: 10

MFAllO -= 'IO 7.e:, P.O. BOX 818 ALEXANDRIA,VA 223~3 703/557-2490 FTS~S-557-2490

<'. .

OA'"l:" • 4/9/85 _, -~ • 4-Clc1..' • · _,._,. BI ~ .,- : ~ ' 1h...1 ~c~ ,.,.,_


LAB NAME: CALIF.ANAL.LAB. CASE NO:3940 SOW NO.: 68-01-6810 QC RPT,#3940 LAB.SAMPLE NO,: P2194



ELEMENTS .. METHOO 1. ALUMINIUM .•. P 2, ANTIMONY ••.. P J. ARSENIC ..... P 3. ARSENIC ..... F ~. BARIUM ...... P 5. BERYLLIUM .•. P 6, CADMIUM ..... P 7. CALCIUM .•... P 8. CHROMIUM .... P 9. COBALT •... , .P 10.COPPER •..•.• P 11. IRON •••••••• P 12. LEAD •••••••• P 12. LEAD ........ F 13 • MAGNESIUM ••• P 14.MANGANESE., .P 15.MERCURY ..•• CV 16.NICKEL ...••. P 17.POTASSitrn ..• P 18. SELENIUM •••• P lS.SELENIUM ••.. F 19.SILVER .• , .. ,P 20,SODIUM .. , ..• P 21, THALLIUM, , •• F 22. TIN •••• , •••• P 23, VAN:\OIUM •••• P 24.ZINC,.,., ••• P 25.CYANIDE ..... C

% SOLID

COMMENTS:

xx

(

(

(

(

(

MEDIUM: XX

MG/KG DRY WEIGHT 2009 <7 U R N/R

<2.3 U 43)

<O. 3 U 3.0

2091] 8 *

<3.5 U 9]

3883 * N/R

114.0 <184 U

117 * <O,l U R <17 U

753] N/R

<2,l U <1.3 U R

602} <2.1 U

<18 U 6.7) 696 N/R

75

LAB MANAGER: /IP-/

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0 0 0 -

I I I I I I I I I I I I I I I I I

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I

11 EPA SAMPLE NO:

U.S. EPA co~ ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFAlll = L/tYl0 S ._, b!.>~l• fa('~ DATE:4/9/85 nlK4, l.•(1


LAB NAME: CALIF,A.~AL,lAB, CASE NO:3940 SOW NO.: 68-01-6810 QC RPT.#3940 LAB.SAMPLE NO.: P2195

ELEMENTS IDEN: FIED AND MEASURED

CONC, ~ MATRIX:

LOW: SOIL:

ELEMENTS .• METHOD 1. ALUMINIUM ••• P 2. ANTIMONY, ... P 3. ARSENIC .. , •. P 3. ARSENIC ....• F 4. BARIUM ...... P =• BERYLLIUM .. ,P 6. CADMIUM ..... P 7. CALCIUM ... ,,P 8. CHROMIUM .... P 9. COBALT ....•. P 10.COPPER ...... P 11. IRON. , .....• P 12. LEAD •••• , , •• P 12,LEAO •••••••• F 13.MAGNESIUM ... P 14.MANGANESE ... P 15.MERCURY .... cv 16,NICKEL .•...• P 17.POTASSIUM, .. P 18.SELENIUM .... P 18,SELENIUM .... F 19.SILVER •..... P 20,SODIUM ..•... P 21,THALLIUM ... ,F 22. TIN ••••••.•. P 23,VANADIUM., .. P 24.ZINC, ....... P 25.CYANIDE ..... c

% SOLID

COMMENTS:

( [

(

[

(

xx MEDIUM: XX


N/R <.2.3 U

36) 0.4]

<2.0 <214 U

26 * <3.5 U

4] 20129 *

N/R 9.0

<184 U 43 *

<0.1 U R <17 U

435] N/R

<2,1 U <l.3 U R

502) <2.1 U

<18 U 36.3

492 N/R

89

LAB MANAGER•#':"

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I I I I I I I I I I I I

II I I I I I I

U.S. EPA CON ACT LABORATORY PR~RAM SAMPLE MANAGEMENT OFFICE E?A SAMPLE NO: P.O. POX 818 ALEXAJlORiA,VA 22313 703/557-2490 FTS:8-557-2490

M:Al12 ~ 'tv7SDATE: 4/9/85

INORGANIC 1NALYSIS SHEET

LAB NAME: CALIF.ANAL.LAB, CJ~E N0:3340 SOW NO.: uS-01-6810 Q: RPT.#3$40 LAB.SAMPLE NO.: P2196

ELEHiENTS IOEN'I'IF.IED Ali.:) MEASCiU::D

CONC,: LOW: MATRIX: SOIL:

ELEMENTS .. METHOD l. ALUMINitm ... P 2. ANTIMONY, ••. ~ 3, ARSENIC ..•.. P 3. ARSENIC ..... F 4. BARIUM •..... P 5. BERYLLIUM ... P 6 • CADMIUM ••••• P 7. CALCIUM ..•.. P 8, CHROMIUM ..•. P 9. COBALT •...•. P 10,COPPER .•.•.. P 11,IRON .•...... P 12. LEAD,., ••••• P 12. LEAD,., ••.•• F 13,MAGNESIUM .•. P 14. lOJtGANESE ••• P 15.MERCURY .... cv 16. IHCKEL, •••.• P 17,POTASSIUM ... P 18. SELENIUM •••• P 18.SELENIUM .•.. F 19,SILVER ••.... P 20. SODIUM •••••• P 21, THALLIUM •••• F 22. TIN •.••••••. P 23,VANADIUM ..•• P 24. ZINC., •••••• P 25,CY'ANIDE ..... c

% SOLID

COMMEN·rs:

( (

(

(

(

(

xx 111::lIUM: XX

MG/KG ORY WE:GHT 4878 <7 U R

N/R 3. 2 J

44] <O. 3 U

<2.0 2997

11 * <3.5 U

17 6374 * N/R

91. l) s + 502] 122 *

<0.1 U R <17 U 1017]

N/R <2.1 U <1.3 U R

614) <2 .1 U

<18 U 11.9)

569 M/R

72

LAB MANAGER: //157

12 .: ~ \ - ,.._c.: f'

CJ '- K L, ~ ,_ + 15

0 <::::!" I.[\

0 0 0 -


U.S. EPA co~ ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFA113 = '/0<1 o P.O. BOX 818 ALEXANDRIA,VA 22313 703/557~2490 FTS:8-557-2490 DATE: 4/9/85

INORGANIC ANALYSIS SKEET

LAB NAME: CALIF.ANAL.LAB. CASE NO:3940 SOW NO.: 68-01-6810 QC RPT.#3940 LAB,SA.MPLE NO.: P2197

ELEMENTS IDENTIFIED AHO MEASURED


ELEMENTS •• METHOD 1. ALUMINIUM .•. P 2. ANTIMONY .... P 3. ARSENic ..... P 3. ARSENIC ..... F 4. BARIU11 •.•.•• P 5 • BERYLLIUM ••• P 6. CADMIUM ..... P 7, CALCIUM ....• P 8. CHROMIUM, ... P 9. COBALT ...... P 10.COPPER •...•. P 11. IRON .... , , •. p 12. LEAD, ••••••• P 12 . LEAD •••••••• F 13.MAGNESIUM, .. P 14.MANGANESE ... P 15.MERCURY •.•. cv 16.NICKEL .•.... P 17.POTASSIUM, .. P 18.SELENIUM .... P 18.SELENIUM .... F 19.SILVER .....• P 20.SODIUM ...•.. P 21.THALLIUM .... F 22.TIN ..•...... P 23.VANADIUM .•. ,P 24,ZINC ....... ,P 25.CYANIDE ..... C

% SOLID

COMMENTS:

xx

[ [

[

[

(

(

(

MEDIUM: XX


N/R 3. 4]

55] <0, 3 U

<2.0 1036)

16 * <3.5 U 50

12733 * N/R 202.l s

298] 150 * <0.1 U R

<17 U 536) N/R

<2.1 U <1.3 U R

506] <2.1 U

<18 U 13. OJ

163 N/R

73

LAB MANAGER:I/P7

13

~

<:;j"

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0 0 0

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I I I I I I I I I I I I I I I I I I

!I

U.S. EPA COh .ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFA114 ...,,_ 9c4?..._ 1-1 P.O. BOX 818 ALEXANORIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE: 4/9/85 Su.b:.,.,.~, Ja.<.: ~

t;.IK .3, .L.:_t 14 INORGANIC ANALYSIS SHEET


ELEMENTS 101:.NTIFIED AND r!EASURED


ELEMENTS .. METHOD l. ALUMINIUM ••• P 2. ANTIMONY •... P 3. AP~ENIC ..... P 3. A•"JENIC ..... F 4. BARPJM •••••• P 5. BERYLLIUM .•. }? 6. CADMIUM ..... P 7. CALCIUM •.•.. P 8 • CHROMIUM •••• P 9, COBALT •.•.•• P 10.COPPER ..•.•. P 11.IR0N •.•••••. P 12. LEAD •••••••• P 12. LEAD •••••••• F 13.MAGNESIUM ... P 14.MANGANESE .•• P 15.MER~URY ...• cv 16. HICKEL •••••• P 17.POTASSIUM .•. P 18.SELENIUM ..•. P 18.SELENIUM .... F 19.SILVER .•.... P 20. sooruM •..••• P 21.THALL!UM .•.• F 22.TIN ..•...•.. P 23.VANADIUM ...• P 24.ZINC ....•... P 25.CYANIDE .•••• C

% SOLID

COMMENTS:

xx MEDIUM: XX

MG/KG DEY WEIGHT 9800 <7 U R N/R

<2. 3 U ( 56) ( 0.4)

<2.0 ( 1355]

14 * <3.5 U

29 8273 * N/R

119.3 S [ 551)

91 * 0, Jr ~ /dtn R

<17 U [ 756)

(

[

N/R <2.1 U <l. 3 lT

1495J <2.1 U

<18 U 21. 1)

126 N/R

75

R

I I I I

I I

Ii I I I I I I

I I I

I I

I I I

I I

I I I

U.S. EPA CON ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFA115 -- 4 c, 'I 3 15 P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE:4/9/85 _:,. v~ ,, .;a .. ,.1 ('·





ELEMENTS .• METHOD l. ALIDUNIUM ••• P

MG/KG DRY WEIGHT

2. ANTIMONY .... P 3. ARSENIC •.... P 3. ARSENIC ...•. F 4. BARIUM ...... P 5. BERYLLIUM, ,,p 6. CADMIUM •.... P 7. CALCIUM ..•.. P 8. CHROMIUM .... P 9. COBALT .• , ... P 10.COPPER •..... P 11, IRON ..•.•••• P 12, LEAD •••.•... P 12.LEAD ....•... F 13.MAGNESIUM ... P 14,MANGANESE ... P 15.MERCURY, ... CV 16,NICKEL ....•. P 17.POTASSIUM ... P 18. SELENIUM •••• P 18.SELENIUM •.•. F 19.SILVER ••..•. P 20.SODIUM ....•• P 21.THALLIUM .... F 22.TIN .•.•..•.• P 23.VANADIUM •... p 24.ZINc •.•..•.. p 25.CYAN!DE ...•. c

% SOLID

COMMENTS~

[

[

[

(

3413 <7 U R

N/R 104.2 s

45] <O. 3 U

<2.0 18006

99 * <3.5 U

24 8572 * N/R

105.4 739] 136 *

<0.1 U R <17 U

540) N/R

<2.l U <l. 3 U R

472] <2.1 U

<18 U 12.3]

407 N/R

83

/~' LAB MANAGER: [y!f✓' ,,,,"7'

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0

0 0 --


U.S. EPA COh .ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE HO:

MFA116::: 46 l/'1 , f 16

P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE! 4/9 / 8 5 " ,._,_ ( to..<! E_

{' ' ~ I a, 1)\1,.. .J.., '...- t


LAB NAME: CALIF.ANAL.LAB. CASE N0:3940 SOW NO.: 68-01-6810 QC RPT.#3940 LAB.SAMPLE NO.: P2200



ELEMENTS .. METHOD l. ALUMINIUM ••• P

MG/KG DRY WEIGHT

2. ANTIMONY ..•• P 3. ARSENlC ..... P 3. ARSENIC ..... F 4. BARIUM ...... P 5. BERYLLIUM ••• P 6. CADMIUM ..... P 7 • CALCIUM ••••• P 8. CHROMIUM ...• P 9 • COBALT •••••• P 10.COl?PER .••.•. P 11.IRON ........ P 12, LEAD •••••••• P 12. LEAD ••.••.•• F 13.MAGNESIUM ... P 14.MANGANESE ..• P 15.MERCURY ...• CV 16.NICKEL ..•..• P 17.POTASSIUM •.. P 18.SELENIUM .... P 18.SELENlUM ...• F 19.SILVER .•...• P 2 0 • SODIUM •••••• P 21.THALL!UM •••• F 22.TIN ......... P 23.VANADIUM., •. P 24.ZINC •••••••• P 25.CYANIDE ..... C

% SOLID

COMMENTS:

( ( (

[

(

[

[

[

6306 <7 U R

N/R 2.5)

71) 0.4)

<2.0 8854

16 * 4]

13 12462 *

N/R 98.l s

762] 199 *

<0.1 U R <17 {J

801) N/R

<2.l U <l.3 U R

532] <2.1 U

<18 U 17.2]

77 N/R

79

I LAB MANAGER:~:J--7

c:::j"

'-J ..

1.0.

0 0 0 -


U.S. EPA CON_ ACT LABORATORY PROGRA.~ SAMPLE MANAGEMENT OFFICE EPA 3Al1PLE NO:

MFAll 7 ~ '/v'I I P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE:4/9/85


LAB NAME: CALIF.ANAL.LAB. CASE N0:3940 SOW NO.: 68-01-6810 QC RPT.#3940 LAB. SAMPLE NO.: P220l

ELEMENTS IDENT!FIEP AND MEASURED


tLEMENTS .. METHOD MG/KG DRY WEIGH'!' l. ALUMINIUM ••• P 4684 2. ANTIMONY .... P <7 u R 3. AP..SENIC ..... P N/R 3. ARSENIC ..•.. F [ 4,1] 4. BARIUM •••••• P ( 52] 5. BERYLLIUM ... P <0.3 u 6. CADMIUM ••••• P <2.0 7. CALCIUM ••••• P [ 1396) 8. CHROMIUM •... P 8 * 9. COBALT •••••• P <J.5 u 10.COPPER ..••.. P 21 11, IRON ••••• , •. P 6494 * 12. LEAD •••••••• P N/R 12. Y.JEAD •••.•••• F 64.2 s 13.MAGNESIUM ... P [ 422] 14,MANGANESE ... P 73 . * 15 .MERCURY •••• CV o. s~ -358.0- /'4;, R 16.NICKEL ....•. P <17 u 17.POTASSIUM ... P [ 657] 18.SELENIUM .... P N/R 18,SELENIUM, , .. F <2.1 u 19.SILVER. ,,,,,P <l.3 u R 20. soonrn: ...... P [ 631] 2 1. TliALLIUM. • •• F <2.1 u 22.TIN,,., ••••• P <18 u 2 3 • VANADIUM •••• P ( 12.2] 24. ZINC •••••••• P 84 25.CYANIDE ..... C N/R

% SOLID 81

COMMENTS:

LAB MANAGER: ~,/

17

u, t";;j'

I.('\

0 0 0 ,-..

I I II I 11 I

I I I

I I I: I

I I I I I I I I I I I

U.S. EPA CON . ..ACT LABvRATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: 18 P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA118-=- '-IV'-17 DATE:4/9/85


LAB NAME: CALIF.ANAL.LAB. CASE N0~3940 SOW NO.: 68-01-6810 QC RPT.#3940 LAB.SAMPLE NO.: P2202



ELEMENTS .. METHOD l. ALUMINIUM .•. P 2. ANTIMONY .... P 3. ARSENIC ••... P 3. ARSENIC ••••• f' 4. BARIUM ...... P 5 • BERYLLIUM ••• P 6 . CADMIUM .•... P 7. CALCIUM ••.•. P 8, CHROMIUM •.•. P 9. COBALT .•.... P 10.COPPER, ..... P 11. IRON •.....•. P 12. LEAD ••.••••• P 12.LEAD ........ F 13. MAGNESIUM ••• P 14.MA.NGANESE ••• P 15.MERCURY •... cv 16.NICKEL ...... P 17.POTASSIUM •.• P 18.SELENIUM •... P 18.SELENIUM •••• F 19.SILVER .•.••• P 20.SODIUM .••••. P 21.THALLIUM .... F 22.TIN ••••...•. P 23.VANADIUM ..•. P 24.ZINC •••...•• P 25.CYANIDE ..••. c

% SOLID

COMMENTS:

( {

(

[

(

[

[

[

xx MEDIUM: XX


N/R <2.3 u

68) 0.6)

<2.0 1004)

7 * <3.5 U

5) 4803 * N/R

38.6 s 2~ 9) 240 *

<O. 1 U R <17 u

301) N/R

<2.1 U <l. 3 u R

589) <2.1 U

<18 u 9.2]

30 N/R

79

LAB MANAGER: jf/p1.-;

5 '""'"' ~:.t:..i \--.

'° c::::t \.(\

0 0 0 --


U.S. EPA COh~~<ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE HO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA119"' 410 }7 DATE:4/9/85


LAB NAME: CALIF.ANAL.LAB. CASE HO:3940 SOW NO.: 68-01-6810 QC RPT.#3940 LAB.SAMPLE NO.: P2203



ELEMENTS .• METHOD 1. ALUMINIUM •.• P 2. A!·lTIMONY .... P 3. ARSENIC .•... P 3. ARSENIC ..•.. F 4. BARIUM ...... P 5. BERYLLIUM •.. P 6, CADMIUM ..... P 7, CALCIUM .•... P 8, CHROMIUM .•.. P 9. COBALT .•.... P IO.COPPER ..•... P 11.IRON .•...... P 12.LEAD •..•.•.. P 12.LEAD ....•.•. F 13. MAGNESIUM, •• P 14.MANGANESE ••. P 15.MERCURY ...• cv 16,N!CKEL ...... P 17.POTASSIUM ... P 18.SELENIUM .... P 18.SELENIUM .... F 19.SILVER .•• , .• P 20.SODIUM ..••.. P 21.THALLIUM .... F 2 2 • TIN ••••••••• P 23.VANADIUM .•.• P 24.ZINC .....•.. P 25,CYANIDE .•.•. C

% SOLID

COMMENTS:

xx

(

(

[

c-. p.r-

[

[

(

MEDIUM: XX


N/R <2.3 U

65] <0. 3 U

<2.0 1588)

7 * <J.5 U

11] 5124 *

N/R 61.6 s

<184 U 313 *

"253. 6 • nc---- R <17 U

319] N/R

<2.1 U <l.3 U R

560] <2.1 U

<18 U 7.8]

60 N/R

69

.fxt1l 17 LAB MANAGER:?f i''

19

r-~

LC\

0 0

0


U.S. EPA CON' ... _.ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: 20 P.O. BOX 8".8 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA120 ::: 'io 3 3 DATE:4/9/85 S '""b:,"" "u' •

(3;K3 -cl 'J... INORGANIC ANALYSIS SHEET




ELEMENTS •• METHOD l . ALUMINIUM ... P 2. ANTIMONY ..•. P 3. ARSENIC •••.. P 3. ARSENIC •••.• F 4. BARIUM ..••.• P 5, BERYLLIUM ... P 6. CADMIUM •..•• P 1 . CALCIUM ...•• P 8. CHROMIUM., .• P 9. COBALT •....• P 10.COPPER ....•. P 11. IRON •••••••• P 12. LEAD •.•••... P 12. LEAD •••••••• F 13.MAGNESIUM •.. P 14.MANGANESE ••. P 15.MERCURY •••• cv 16.NICKEL ..••.. P 17.POTASSIUM •.• P 18.SELENIUM ••.. P 18.SELENIUM ...• F 19.SILVER •••••• P 20,SODIUM ••.••• P 21.THALLiill1., •• F 2 2. TIN ••••••••• P 23.VANADIUM •••• P 24.ZINC ••...••• P 25.CYANIDE ...•• C

% SOLID

COMMENTS:

[

[

[ [

xx MEDIUM: XX


N/R <2,3 U

145 0.8)

<2.0 797]

3) * 5] 2]

4715 * N/R 8.1 367) 262 *

<0.1 U R <17 U

<252 U M/R

<2,l U <l.3 U R

2018) <2.1 U

<18 U 10.6]

6] N/R

87

ro ~

I.(\

0 0 0 -

I I I I I I I I I I I I I I I I

U. S • EPA CON' ... _ .ACT LABO RA TORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SA."1PLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFAl:21-=- '/tYl.5 DATE:4/9/85

INORGANIC ANl1LYSIS SHEET

LAB NAME: CALIF.ANAL.LAB. SOW NO.: (.,,f ✓ C/-t,-fJI) LAB.SAMPLE NO.: P2205

CASE NO~ J 9~! l QC RPT. # _j ~•~f i;



ELEMENTS .. METHOD 1. ALUMINIUM ••• P 2 . ANTIMONY .... P 3. ARSENIC ..•.. P 3. ARSENIC •.... F 4 • BARIUlL ••••• P 5. BERYLLIUM ••• P 6 • CADMIUM ••••• P 7. CALCIUM .•.•. P 8 • CHROMIUM •••• P 9. COBALT •••••• P 10.COPPER ...... P 11. IRON •••••••• P 12. LEAD .•.....• P 12. LEAD ..•....• F 13. MAGNESIUM •• , P 14. MANGANESE ••• P 15.MERCURY .... cv 16.NICKEL ...... P 17. POTASSIUM ... P 18.SELENIUM .... P 18 • SELENIUM •••• F 19.SILVER .....• P 20. SODIUM •••••• P 2 l. THALLIUM .•.. F 22.TIN ••••••••• P 2 3 • VANADIUM •••• P 24.ZINC •.••• , •• P 25. CYANIDE., ••• C

% SOLID

COMMENTS:

xx

[

[

(

MEDIUM: XX


N/R 19.3 s

77] <O. 3 U

<2.0 2906

47 <3.5 U

32 5493 * N/R

59.1 s 387)

88 * <O.l U

<17 U <252 U

N/R <2.1 U R <l.3 U

435) <2.1 U

<18 U 6.6) 4::o N/R

88

1/4'~ -~ LAB MANAGER: U,4;/ !/

21

,.,._ I_.

tj

1.0.

0 0 0 -


U.S. EPA CON'l. .CT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA122 ~ '1 o 'I lo DATE:4/9/85


LAB NAME: CALIF.ANAL.LAB. SOW NO. : f.,., f ~ 0/- /vf !D LAB.SAMPLE NO.: P2206

CASE NO: J''/10 QC RPT. #3CJ1C



ELEMENTS .• METHOD 1. ALUMINIUM ••• P 2. ANTIMONY ..•. P 3. ARSENIC •.... P 3. ARSENIC .•.•• F 4. BARIUM ...•.. P 5. BERYLLIUM •.. P 6. CADMIUM ..••• P 7. CALCIUM ..•.. P 8. CHROMIUM .•.. P 9. COBALT ...... P 10.COPPER ....•. P 11.IRON ..••..•. P l~.LEAD ........ P 12. LEAD •••••••• F 13.MAGNESIUM .•. P 14.MANGANESE •.. P 15.MERCURY .•.. cv 16.NICKEL •...•. P 17.POTASSIUM ..• P 18.SELENIUM •... P 18.SELENIUM .... F 19.SILVER •.•.•. P 20.SODIUM ...•.. P 21.THALLIUM ..•. F 22.TIN ..•...... P 23.VANADIUM .... P 24.ZINC ........ P 25,CYANIDE •..•• C

% SOLID

COMMENTS:

xx

[

[

(

(

(

(

MEDIUM: XX

MG/KG DRY WEIGHT 1757

11] N/R

14.7 26]

<O. 3 U <2.0

784) 15

<3.5 U 9]

4616 * N/R

28.8 s <184 U

37 * <0.1 U

<17 U <252 U

N/R <2.1 U R <l.3 U

396] <2.1 U

<18 U 4. 7 J 620 N/R

92

LAB MANAGER: /ifr,~

22

0

lf\ I.(\

0 0 0 ..-


U.S. EPA CON~_ACT LABORATORY PROGRAM SAMPLE MANAGEMENT Cl-'FICE P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 ¥TS:8-557-2490

EPA SAMPLE NO: 2 J MF.i\123 ~ 'ltJ 70

,'

DATE: 4/9/85 _'., .._..., +•l·-:' (-


LAB NAME: CALIF .J,.1-'AL. LAB. sow NO. : (-,} -CJ- b '?tO LAB.SAMPLB No.: P2207



ELEMENTS •. METHOD 1. ALUMINIUM .•• P 2. ANTIMONY ..•• P 3. ARSENIC ....• P 3. ARSENlC ....• F 4. BARIUM •• , ••• P 5. BERYLLIUM ••• P 6 • CADMIIB-.f ••••• P 7. CALCIUM ..••• !> 8 . CHROMIUM ...• P 9. COBALT .•..•. P 10.COPPER .••.•. P 11. IRON .•..••.. P 12.LEAD •......• P 12.LEAD •••••..• F 13,MAGNESIUM ... P 14,MANGANESE ••. P 15.MERCURY •••• cv 16.NICKEL .•.••• P 17.POTASSIUM ••• P 18,SELENIUM •... P 18, SELENIUM ••• , F 19.SILVER •..••• P 20.SODIUM .••••• P 21,THALLIUM,, ,,F 22.TIN ••••••••. P 23.VANADIUM •••• p 24,ZINC •••••••• P 2 5, CYANIDE. , ••• C

\ SOLID

COMMENTS:

xx

[

[

[

(

[

MEDIUM: XX


N/R <2.3 U

26] <0, 3 U

<2.0 1061)

5 <3.5 U

14 8625 * N/R

35.2 S + 317] 163 *

<0.l U <17 U

280} N/R

<2 .1 U R <1.3 U

451] <2.l U

<18 U 6.3] 181 N/R

88

LAB MANAGER:fo'..,,

0 i K;. L,.·t 2.

lf\

I.(\

0

0 0

I I I


U.S. EPA CON1 • ..A.CT LABORATORY PROGRAM SAM?LE MANAGEMENT OFFICE EPi~ SAMPLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MF A.., ..., 4 :. 'I o 7 ).__ ( DATE:4/9 .,5 ~ u.r t-ClC!. L.


LAD NAME: CALIF.ANAL.LAB. sow NO.: {;J-~01- /;;YI() LAB.SAMPLE NO.: P2208

CASE NO: S940 QC RPT. #J1/-1()


MEDIUM: XX CONC.: LOW: MATRIX: SOIL:

ELEMENTS .. METHOD 1. ALUMINIUM. ..• P 2. ANTIMONY ..•. P 3. ARSENIC .•... P 3. ARSENIC ..... F 4. BARIUM ...... P [ 5. BERYLLIUM ... P 6. CADMIUM ..... P 7. CALCIUM •...• P [ S • CHROMIUM •.•• P 9. COBALT ...... P 10.COPPER •....• P 11. IRON ••••••.. P 12. LEAD •••••••• P 12.TZAD •••••••• F

xx

13.MAGNESIUM ... P ( 14.MANGANESE ..• P 15. MERCURY •••• CV 16.NICKEL ...... P 17.POTASSIUM ... P 18.SELENIUM .. , .P 18.SELENIUM •..• F 19.SILVER ..•••. P 20.soorm! ...... P c 21,THALLIUM ..• F 22 TIN •....••.• P 2J.VANADIUM ..•• P [ 24.ZINC •...•.•• P 25.CYANIOE ••.•• C

% SOLID

COMMENTS:

MG/KG DRY WEIGHT 1593 <7 u

N/R 7.1

61] <0.3 u

<::-:. 0 15t4]

23 <3.5 u

189 4295 * N/R

25.3 241] 100 *

<O.: U <17 u

<252 u N/R

<2.l U R <1.3 u

511] <2.1 U

<18 u 3.9) 363 N/R

85

- ' I- -nlK:? ... , _ _.L J ·- r

(' I ,, I.('\

I.(\

0 0 0 --


u . s . EPA CON'i HACT LABORATORY PROGRAM. SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFA125 -::. re "7 / 25

P.O. BOX 818 ALEXANORIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE: 4/9/85 5 ._, t;!:. _,,_,·- .,..._._, •-


LAB NAME: CALIF.ANAL.LAB. SOW NO.: (:.,f'-(/-J,5"·10 LAB. SAMPLE NO. ~ 1?2209

CASE NO: 1._?l/40 QC RPT, # .J<.:..-JD



ELEMENTS .. METHOD MG/KG ORY WEIGHT 1. ALUMINIUM .•. P 1760 2, ANTIMONY., .. P <7 u 3. ARSENIC .••.. P N/R 3. ARSEHIC ••... F <2.3 u 4. BARIUM •••••• P 265 s. BERYLLIUM ••• P <0.3 u 6. CADMIUM ••••• l? <2.0 ,. CALCIUM ••••• P ( 432] 8. CHROMIUM ..•• P [ 5] 9. COBALT •••••• P <3.5 u 10.COPPER •••••• P [ 7] 11. IRON •..•••.• P 4823 * 12. LEAD •••••••• P N/R 12. LEAD ••••••.• F 26.7 $ 13.MAGNESIUM •.. P <184 u 14,MANGANESE ••. P 1074 * 15,MERCURY •••• cv <O.l u 16,NICKEL •.••.• P <17 u 17.POTASSIUM ••• P <252 u 18.SELENIUM •.•. P N/R 18. SELENIUM •••• F <2.1 u R 19.SILVER •••••. P <l.3 u 20.SOOIUM .•••.. P [ 420] 21 • THALLIUM • • • • F <2.1 u 22.TIN, ........ P <18 u 23,VANADIUM, ... P [ 8. l] 24,ZINC •••.•••• P 495 25.CYANIDE ••... C N/R

.% SOLID 86

COMMENTS:

/2 I LAB MANAGER:~~

r-"\

Ln If\

0 0 0

I I I I I I

! I I I I I I I I I I I I I

U.S. EPA CONTLu~CT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 MFA126 ::. '1075. 26 703/557-2490 FTS: 8-557-2490 DATE: 4/9/85 _s,uj ~ ·--..Y f-a...c.,

INORGANIC ANALYSIS SHEET CI K 2_ , ,,_,_ :~- 1;

LAB NAME: CALIF.ANAL.LAB. sow No.: br-01-1:i00 LAB. SAMPLE NO. : P2 210



ELEMENTS •• METHOD MG/KG DRY WEIGHT L ALUMINIUM ••• P 2819 q 2 • ANTIMONY •••• P <7 u !.(\ 3 • ARSENIC •.••• P N/R t{\ 3. ARSENIC •••.• F [ 2,8) 4. BA.RIUM, ••••• P ( 33) 0 5. BERYLLIUM ••• P <0.3 u 0 6. CADMIUM ••••• P <2.0 0 7. CALCIUM ••••• P [ 1076] --a. CHROMIUM ••.. P 6 9. COBALT .•.••. P <3.5 u 10.COPPER •.... ,P 13 ll. IRON •••••••• P 4678 * 12. LEAD ••••••• , P N/R 12. LEAD •••.••.. F 30,5 s 13 .MAGNESIUM ••• P <184 u 14. MAN'GAi.'lESE ••• P 96 * 15,MERCURY .••• cv <0.1 u 16 .NICKEL •••••. P <17 u 17. POTASSIUM ••• P <252 u 18.SELENIUM ..•• P N/R 18. SELENIUM •••• F <2.l u R 19,SILVER ••••.. P <l. 3 u 20. SODIUM •••• , • P r 447) 2 l. THALLIUM •••• F <2.l u 22.TIN ••••••••• P <18 u 23. VANADIUM •••• P [ 7.7] 2 4. ZINC •••••••• P 198 25,CYANIDE ••••• C N/R

% SOLID 82

COMMENTS:

LAB MANAGER: ;ft;,;/ 1


U.S. EPA CON'J. .. ~CT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFA12 7 =. L/ CbCf ~

27 P.O. BOX 818 ALEXANDRIA,VA 22313 103/557-2490 FTS:8-557-2490 DATE: 4/9/85 -•,, iJ,~ ·-• 1 • ""-r .a.

13 J ,.,- .:: , L ,, "."" ,, INORGANIC ANALYSIS SHEET

LAB NAME: CALIF.AHAL.LAB. sow NO. : l· f'-01- /of I() . LAB. SAMPLE NO. : P2 211

1CASE HO :,31'9li oc RPT. #S'i+o



ELEMENTS .• METHOD 1. ALUMINIUM .•. P 2 • ANTIMONY. , •• P 3. ARSENIC .••.. P 3. ARSENIC .•..• F 4. BARIUM ••••.. P 5. BERYLLIUM •.. P 6. CADMIUM .•..• P 7. CALCIUM •••.• P 8. CHROMIUM •••. P 9. COBALT •.•... P lO. COPPER •.•. , . P 11. IRON ••.•.••. P 12. LEAD ..••.•.. P 12. LEAD •••••••• F 13. MAGNESIUM ••• P 14 • MANGANESE ••• P 15. MERCURY •••• CV 16. NICKEL •••••• P 17. POTASSIUM, •• P 18 • SELENIUM •••• P 18. SELENIUM •••• F 19. SILVER •••••• P 20. SODIUM •••••• P 21. THALLIUM •••• F 22. TIN ••••••••• P 2 3 • VAltAOIUM •••• P 24.ZINC •••••••• P 25.CYANIDE ..•.• c

% SOLID

COMMENTS:

[ [

[

[

(

[

xx MEDIUM: XX


H/R 4.5)

31] <0.3 U

<2.0 338]

10 <3.5 U

105 3133 *

N/R 35.5 S

<184 U 36 *

<0.1 U <17 U

689] N/R

<2.1 U R <1.J U

446] <2.l U

<18 U 3.5] 107 N/R

83

/,. . ;;-1~·-,Y

LAB MANAGER Z't~1.,¥ ,

L,I"\

""' 0 0 0 --


11 I

I I

U.S. EPA CONT~CT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490


LAB NAME: CALIF.ANAL.LAB. SOW NO.: 0.f-01-l, "s'IO LAB.SAMPLE NO.: P2212

CASE No:/?10 QC RPT. # .301{;,



ELEMENTS •• METHOD 1. ALUMINIUM ••. P 2. ANTIMONY .... P 3. ARSENIC ..... P 3. ARSENIC ..•.. F 4. BARIUM ...... P 5 • BERYLLIUM ••• P 6. CADMIUM ..•.• P 7. CALCIUM ..... P 8. CHROMIUM •••• P 9. COBALT .....• P 10. COPPER. , .••• P ll.IRON ••.•••• ,P 12.LEAD ........ P 12. LEAD •••••••• F l~. MAGNESIUM ••• P 14.MANGANESE •.• P 15.MERCURY .... cv 16. NICKEL. , •... P 17.POTASSIUM .•. P 18 • SELENIUM, ••• P 18. SELENIUM ••• , F 19. SILVER •••••• P 20.SODIUM .....• P 2 l. THALLIUM •••• F 22.TIN ••••••••• P 2 3 • VANADitn.f. ••. P 24,ZINC •.... , .• P 25, CYANIDE ••• , • C

% SOLID

COMMENTS:

xx

[

(

(

(

(

MEDIUM: XX

MG/KG DRY WEIGHT 4355 <7 U N/R

<2. 3 U 15)

<0. 3 U <2.0

<214 U 5

<3.5 U 2)

3599 * N/R 2,5

<184 U 9 *

<0.1 U <17 U

716] N/R

<2. 1 U R <l.3 U

409] <2.1 U

<18 U 7.5]

<l.6 U N/R

85

LAB MANAGER: 1~ fff)l /

28

'° I.{\

I.(\

0 0 0

I I I I I I

I I I

I I

I I I I I I I I I I I

EPA SAMPLE NO: U.S. EPA CONTMCT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE

MFA129 ~ l/ Ot 5' DATE:4/9/85

P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490


LAB NAME: CALIF.ANAL.LAB. CASE NO: ;391D sow NO.: by-{.,:- u y'/[' QC RPT. #J<:1 o LAB.SAMPLE NO.: P22l3



ELEMENTS .• METHOD 1 • ALUMINIUM ... P 2. ANTIMONY .... P 3, ARSENIC ..... P 3, ARSENIC ..•.. F 4 • BARIUM •••••• P 5. BERYLLiln1 ••• P 6. CADMIUM ....• P 7. CALCIUM .. , •. P 8 • CHROMIUM •••• P 9. COBALT •••••• P 10.COPPER .•..•. P 11. IRON •••••••• P 12 • LEAD ••••.••• P 12. LEAD ..••..•. F 13. MAGNESIUM ••• P 14,MANGANESE ... P 15,MERCURY., .• CV 16. HICKEL .••••• P 17.POTASSIUM, .. P 18,SELENIUM.,,.P 18 . SELENIUM •.•• F 19.SILVER ...... P 20. SOOitJM ..• , •• P 21,THALLIUM .••. F 22. TIN •••••.••• P 23.VANADIUM .. ,.P 24,ZINC ••...... P 25.CYANIDE ..... C

% SOLID

COMMENTS:

xx

(

( [

(

[

(

(

MEDIUM: XX


N/R <2.3 U

34) <0.3 U

<2.0 1836)

3) <3.S TJ

6] 3390 * N/R

33.l <184 U

61 * <0.l U

<17 U 264) N/R

<2. l U R <l.3 U

465] <2.1 U

<18 U 4,0J

80 N/R

74

LAB MANAGER: ~

29 C ' ~ LA., t- I} '~~ ~

t:31 J< ; , L L' t {/

r-

I.(\

0

0 0


U.S. EPA CONT~ ... ,.CT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE 30 P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

EPA SAMPLE NO: l1FA13 0 ::: '/t.J6 7 S I...'-. 1 1- &.. -,._ ~

DATE: 4/9/85 C: . v /


LAB NAME: CALIF.ANAL.LAB. SOW NO.: 05-C/-- u.,-~/0 LAB.SAMPLE NO.: P2214


CONC.: LOW: MATRIX~ SOIL:

ELEMENTS .. METHOO 1. ALUMINIUM ... P 2. ANTIMONY .... P 3. ARSENIC ..... P 3. ARSENIC ...•. F 4. BARIUM .•.... P 5. BERYLLIUM .•. P 6. CADMIUM ..... P 7. CALCIUM ••••• P 8. CHROMIUM .... P 9. COBALT ...... P 10,COPPER ...... P 11.IRON .•.• , ... P 12.LEAD •••••••• P 12 • LEAD ••.••••• F 13.MAGNESIUM ... P 14.MANGANESE •.. P 15.MERCURY ..•. cv 16.NICKEL ....•. P 17.POTASSIUM ... P 18. SELENIUM •••• P 18. SELENIUM •••• F 19.SILVER .••... P 20.SODIUM ...•.. P 21.THALLIUM ••.. F 22.TIN .•....... P 23.VANADIUM •••• P 24.ZINC ........ P 25.CYANIDE ..•.. C

% SOLID

COMMENTS:

xx

(

[

(

[

[

[

MEDIUM: XX


15.2 S 39]

<O.J U <2.0 1118)

16 <3.5 U

22 4634 * N/R

98.7 S 255)

94 * <O.l U

<17 U 765) N/R

<2 .1 U R <1.3 U

506) <2.1 U

<18 U 5.4]

79 N/R

79

£1 LAB MANAGER:l,,~-4

, cLC. c ~ ,r -'l, C.

cc, L(\

11'

0 0 0


U.S. EPA CON~ • .ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE HO:

MFA131-:-.. 'IOt.J.. P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE:4/9/85


LAB NAME: Cfi,.LIF.ANAL.LAB. sow NO.: l,:s·-01- 6/fJb LAB. SAMPLE NO. : P2 21.5



ELEMENTS •• METHOD 1. ALUMINIUM ..• P 2. ANTIMONY .•.• P 3. ARSENIC •.... P 3. ARSENIC ..•.• F 4. BARIUM ...••• P 5. BERYLLIUM ... P 6 • CADMIUM • • • • • P 7 • CALCIUM .•••• P 8 • CHROMIUM ..•• P 9. COBALT ...... P 10.COPPER .••..• P 11. IRON •.••...• P 12. LEAD ..•...•• P 12.LEAD .•..•.•• F 13.MAGNESIUM ... P 14.MANGANESE ••. P 15.MERCURY .... cv 16.NICI<EL .•.••• P 17.POTASSIUM ..• P 18.SELENIUM ..•. P 18.SELENIUM ...• F 19.SILVER .••..• P 20.SODIUM .•...• P 21.THALLIUM ••.. F 22.TIN .....•.•. P 23.VANAOIUM ••.• P 24.ZINC •.•..••• P 25.CYANIDE .•••• C

% SOLID

COMMEN'rs:

xx MEDIUM: XX


15.9 S [ 32]

<0.3 0 <2.0

( 1927) 25

<3.5 U 16

6137 * N/R

61.5 S [ 189)

44 * <O.l U

<17 U <252 U

4-9--fi/,z tie--, <2 .1 U R <1.3 U

( 414] <2.1 U

<18 U [ J.9J

278 N/R

91

LAB MANAGER:~>'

31

r._~ Lr\

t{\

0 0

0

I I I I I I I I I I I I I I I I ii

I I

U.S. EPA CON1.i:J\CT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

EPA SAMPLE HO: 3· 2 MFA132::,YclS- .

DATE: 4/9/85 -':._,,!a...~ •c


LAB NAME: CALIF. ANAL. LAB. CASE NO: J {j 1 C SOW NO.: / fr-(-'-/ v;(_'l QC RPT. # J'-}1-C; LAB.SAMPLE- NO.; ~ J , P2216



ELEMENTS .. METHOD 1. ALUMINIUM •.. P 2. ANTIMONY .... P 3. ARSENIC ..... P 3. ARSENIC ..... F 4. BARIUM •••••• P 5. BERYLLIUM •.. P 6. CADMIUM ..•.. P 7 • CALCIUM ..... P 8 • CHROMIUM •••• P 9. COBALT •••••• P 10.COPPER •...•• P 11. IRON ••• , •••• P 12.LEAD ........ P 12. LEAD •••••••• F 13. MAG~lESIUM ••• P 14. MANGA..'-IESE .•• P 15,MERCURY .•.. cv 16.NICKEL ...... P 17.POTASSIUM., .P 18.SELENIUM •••• P 18.SELENIUM, .•. F 19.SILVER ...••. P 20. SODitJM ..•••• P 21. THALLIUM •• , • F 22.TIN ••.•••••• P 2 3 • VANADIUM •••• P 24.ZINC •.•...•• P 25,CYANIDE ..... C

% SOLID

COMMENTS:

xx

(

(

MEDIUM: XX


N/R <2.3 U

29] <0.3 U

2.2) 565]

4] <3.5 U

1] 4045 *

N/R 31.2

<184 U 68 *

<0.l U <17 U

<252 U '4-1--~·k. fJI·-,

<2.1 U R <1.3 U

964] <2.1 U

<18 U 5.6] 569 N/R

85

/;' , LAB MANAGER: v~

t3 I I\ 7-. ~ L ( :;·

0 0 0

I I I I I I I I I I I I I I I I I

II

ii I

!

U.S. EPA CON~nACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFA133-=- 'flJb3/ 33 P.O. BOX 818 ALEXANDRIA,VA 22313 703/55?-2490 FTS:8-557-2490 DATE:4/9/85 .":;-.,tJ.:.,<A 1 r~-,~


LAB NAJ1E: CALIF. ANAL. LAB. sow NO.: l,f-{};- /;.'5'10 LAB. SAMPLE NO.: P2217

CASE NO: JJ-10 QC RPT. # j '1-tO

ELEMENTS IDENTIFIED AND MEASOREO


ELEMENTS •. METHOD 1. ALUMINIUM ••• P 2. ANTIMONY .... P 3. ARSENIC ...•• P 3. ARSENIC ••.•• F 4. BART.UM •••••• P 5. BERYLLIUM ... P 6. CADMIUM .. , •. P 7. CALCIUM ....• P 8. CHROMIUM,, ,,p 9. COBALT ...... P 10. COPPER ••• , •• P 11.IRON ......•• P 12. LEAD •••••••• P 12. LEAD ........ F 13. MAGNESIUM .•• P 14.MANGANESE ... P 15. MERCURY •••• CV 16,NICKEL •••••• P 17. POTASSIUM ••• P 18. SELENIUM •.•• P 18. SELENIUM'. •••• F 19. SILVER •••.•• P 20.SODIUM ••.... P 21.THALLIUM .... F 2 2 • TIN ••••••••• P 23.VANAOIUM •.•• P 24.ZINC, ••••••• P 25.CYANIDE .••.• C

% SOLID

COMMENTS:

[

[

( [

xx MEDIUM: XX


N/R 8.8 S

19) <0. 3 U

7.6 256]

<l.l U <3.5 U

157 3938 *

N/R 124.4

<184 U 18 *

<O.l U <17 U

<252 U Ufr"9 'c9,..lv/f... r~ ,

<2.1 U R <1.3 U

407] 3]

<18 U <1.8 U

1576 N/R

80

LAB MANAGER! #p-0

; ' -bl k J..' Lt· t ,

l!"'.

0 0 0 -

I I


U.S. EPA CONT.KA.CT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA134-== '/063 DATE: 4/9/85 .,.~" b~ ~, ~,1. , P

'31K:i.,:_cl:. b INORGANIC ANALYSIS SHEET

LAB NAME: CALIF. ANAL •. LAB. SOW NO.: (;,f-t)/ -ft/;,,/0 LAB.SAMPLE NO.~ ~ P2218


CONC. : LOW: MATRIX: SOIL:

ELEME!;·rs •• METHOD 1 . ALUMINIUM ... P 2. ANTIMONY .... P 3. ARSENIC ..... P 3. ARSENIC ..... F 4. BARIUM ••• , •• P 5. BERYLLIUM, .. P 6. CADMIUM .• , .. P 7 • CALCIUM ••••• P 8 • CHROMIUM •••• P 9. COBALT ••..•. P 10. COPPER •••••• P 11.IRON •••••••• P 1 ~.LEAD •••••••• P J.2. LEAD •••••••• F 13.MAGNESIUM ... P 14.MANGANESE ... P 15.MERCURY .... cv 16. NICKEL •••••. P 17.POTASSIUM ... P 18,SELENIUM ... ,P 18. SELENIUM •••• F 19,SILVER ...... P 20. SODIUM •••••• P 2 l. THALLIUM •••• F 22.TIN ......••. P 2 3. VANADIUM •••• P 24,ZINC, ••• , ••• P 25,CYANIDE ..... C

% SOLID

COMMENTS:

[ (

(

(

xx

[ (

(

MEDIUM: XX ..


N/R 4. 9 J

77] <0. 3 U

<2.0 2823

14 <3.5 U

8] 6169 * N/R

44.8 378) 101 *

-~a--c .!tj. <17 U lltJ--:-.

<252 U N/R

<2. l U R <l. 3 t:

614] 3]

<18 U 6.9] 406 N/R

77

/1 f"'/2;) /y

LAB MANAGER: C:f/-"

C' '-.['

1.0

0 0 0

I I I I I I I I I I I I I I I I I I ii I

' !

U.S. EPA CON .ACT LABORATORY PROGRJL~ SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFA135= ~oqg ~

35 P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE: 4/9/85 S L-.1,.s~~· lC\.Q (-

INORGANIC ANALYSIS SHEET B I K ~' L, i.- 'J

LAB NAME: Cl}.LIF.ANAL.LAB. sow NO.: 65---o;--t,,(ilu LAB.SAMPLE NO.: P2219

CASE NO: 3?10 QC RPT. # ..:.1'1-()

ELEMENTS IDENTIFIED AND MEASGRED


ELEMENTS •• METHOD 1. ALUMINIUM ... P 2. ANTIMONY .••. P 3. ARSENIC •.... P 3. ARSENIC •.•.• F 4. BARIUM •....• P 5. BGRYLLIUM ..• P 6. CADMIUM ...•• P 7. CALCIUM ..•.. P 8. CHROMIUM ...• P 9 • COBALT •••••• P 10.COPPER •....• P 11. IRON •••••••• P 12.LEAO ..•..... P 12. LEAD ..••..•. F 13.MAGNESIUM ••• P 14.MANGANESE .•. P 15.MERCURY •... CV 16.NICKEL •....• P 17,POTASSIUM .•• P 18.SELENIUM .... P 18.SELENIUM •... F 19.SILVER ....•. P 20.SODIUM .•.••• P 21.THALLIUM .•.. F 22.TIN ...•...•• P 23.VANAOIUM ..•. P 24.ZINC .....••. P 25.CYANIDE .••.• C

% SOLID

COMMENTS:

( [

(

(

[

xx MEDIUM: XX


N/R 17.8

84) 0.3)

<2.0 3467

22 <3.5 U

27 6057 *

N/R 26.4

522] 127 *

..&-!;'~,-,-2- 0 • J-1-- A<--,.. <17 U

<252 U /. u,._ '};-5--i\'. K. .,,,

<2.1 U R <l. 3 U

598) <2.1 U

<18 U 7.8] 380 N/R

87

LAB MANAGER: ~/~:1 "

'.[',

I.('\

0 0 0


U.S. EPA CON ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

36

P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA13 6 :::- 1/ C3'7 ,· DATE: 4/9/85 :, ...... \...s ,. , ~ ,H' r~


LAB NAME: CALIF.ANAL.LAB. sow NO.: bf'--01-(o'i;"JD LAB.SAMPLE NO.: P2220

CASE NO: JCJ-1 () QC RPT. #'3q4()



ELEMENTS •. METHOO MG/KG DRY WEIGHT 1. ALUMINlUM ... P 6106 2 • ANTIMONY ..•. P <7 u 3 • ARSENIC •...• P N/R 3. ARSENIC ..... F <2.3 u 4 • BARIUM •••••• P [ 33] 5. BERYLLIUM ... P <0.3 u 6. CADMIUM ••••• P <2.0 7. CALCIUM ••• , • P [ 227] 8. CHROMIUM •••• P 6 9 • COBALT ....• Ip <3.5 u 10,COPPER .... ,.P <0.65 u 11.IRON •••••• , .P 3025 * 12. LEAD •••••••• P N/R 12. LEAD •••••••• F 10.0 s 13,MAGNESIUM,,.P ( 272] 14.MANGANESE ... P 15 * 15.MERCURY ...• cv <O.l u 16.NICKEL .•.•. ,P <17 u 17.POTASSIUM ... P <252 U 18.SELENIUM .... P '2¼-- fl /,z tk ➔ 18.SELENIUM .... F <2.1 U R 19.SILVER ...... P <l.3 u 20.SODIUM •...•. P ( 955] 21.THALLIUM .... F <2.l u 22.TIN •......•. P <18 u 23,VANADIUM .... P [ 6.2] 24.ZINC .•...... P [ 6) 25.CYANIDE •... ,C N/R

% SOLID 85

COMMENTS:

LAB MANAGER:(~

{3 11, 3 L.. l' t- t 3

tj

'-C IS'\

0

0 0 ,.-..


U. S, EPA COl lACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFAl37 ::. l/C 5 C/ P.O. BOX 818 ALEXJI.NDRIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE: 4/9/85 B lK. b


LAB NAME: fALIF, ANAL. LAB. SOW NO. : r,;;f-O/ - {y (,,,/{) LAB.SAMPLE NO.: P2221

CASE NO: Jy10 QC RPT. #.J9i-0

ELEMENTS IDENTIFIED ANO MEA~URED


ELEMENTS .. METHOD MG/KG DRY WEIGHT l. ALUMINIUM •• , P 1866 2. ANTIMONY ..•. P <7 u 3. ARSENIC ..... P N/R 3 • ARSENIC, .•.. F <2.3 tJ 4. BARIUM •••••• P ( 43] 5. BERYLLIUM ••• P <0.3 u 6. CADMIUM .•..• P <2,0 7. CALCIUM ...•. P ( 717] 8. CHROMIUM,,., P 6 9. COBALT ....•• P <3.5 tr 10,COPPER ...... P <0.65 u 11.IRON ......•• P 4273 * 12.LEAD ........ P N/R 12. LEAD •••.•••• F 25.6 s 13.MAGNESIUM .•• P <184 u 14,MANGANESE ... P 94 * 15,MERCURY •... cv <O,l u 16.NICKEL., .... P <J.7 u 17. POTASSIUM, •• P [ 638] 1 ~-~ 18. SELENIUM •••• P -2--9--'°".'K 18.SELENIUM .... F <2.1 u R 19. SILVER •••••. P <1.J u 20.SODIUM ...... P [ 498] 21. THALLIUM •••• F <2.1 u 22.TIN, •••••••• P <18 u 23.VANAD!UM ..•. P ( 9.8] 24.ZINC ..•.•... P 270 25.CYANIOE ..... C N/R

% SOLID 88

COMMENTS:

37

Lot t :2..

1.n

'° U'i

0 0 0 -


U.S. EPA COh ..ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: P.O. BOX 818 ALEXANDRIA, VA 22313 MFA138::: 'IC57 703/557-2490 FTS:8-557-2490 DATE:4/9/85 f3LJ< b, Lot 'f

INORGANIC ANALYSIS SHEET .5~-.r{ o..Q E

LAB NAME: CALIF.ANAL.LAB, sow NO•! {,f-{1/ ~ L~ q / t' LAB.SAMPLE NO.: P2222

CASE NO: (3y10 QC RPT. # J lj-'f 6



ELEMENTS .. MEtHOD 1. ALUMINIUM ... P 2. ANTIMONY, ... P 3 • ARSENIC ••••. P 3. ARSENIC •.. ,.F 4. BARIUM ...... P 5, BERYLLIUM ... P 6. CADMIUM ••••• P 7. CALCIUM., ... P 8. CHROMIUM,, .. P 9. COBALT ...... P 10,COPPER ..•... P 11.IRON ........ P 12. LEAD •••••••• P 12, LEAD. , .••••• f 13. MAGNESIUM ••• P 14 • MANGANESE •• , P 15,Mf.RCURY, .•• CV 16.NICKEL •... ,.P 11.POTASSIUM. ,.P 18.SELENIUM ..•• P 18.SELENIUM .... F 19,SILVER ...... P 20,SODIUM,., ..• P 21.THALLIUM .... F 22.TIN ..•...... P 23.VANADIUM •••. P 24,ZINC ..•..... P 25.CYANIOE ...•. c

.% SOLID

COMMENTS:

[

[

(

[ [

[

xx MEDIUM: XX


<2.3 U 31]

<0,3 U <2.0

573] 6

<3.5 U 2)

4414 * N/R

29,8 S <184 U

83 * <0.1 U

<17 U <252 U

N/R <.2.1 U R <l. 3 U

483) 3)

<18 U 8.6)

<1.6 U N/R

84

38

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~

l.(\

0 0 0 -

I

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U.S. EPA COh .ACT LABORATORY pr ·GRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: 3 ~

MFA139 s: 1/-o.,s 5 4jtFi+.:E.. P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490 OATE:4/9/85 (!;,Lk£, Lot 3


LAB NAME: CALIF.ANAL.LAB. sow ~ro. : l,S,,-o 1-- t, g 10 LAB.SAMPLE NO.: P2223

CASE NO: .,3C/-10 QC RPT. # JcJ1D


CONC.: LOW: MATRIX: SOIL: xx

ELEMENTS •. METHOD 1, ALUMINIUM ..• P 2. ANTIMONY •••• P 3 . ARSENIC., ... P 3 . ARSENIC,, ... F 4. BARIUM •••••• P ( 5. BERYLLIUM ••• P 6. CADMIUM .•... P 7, CALCIUM ••••• P ( s. CHROMIUM .••. P 9, COBALT ...... P 10.COPPER ...... P 11.IRON, •• , •••• P 12. LEAD .•...••• P 12. LEAD •••••••• F 13.MAGNESIUM ... P 14.MANGANESE •.. P 15.MERCURY ..•. cv 16,NICKEL ....•. P 17.POTASSIUM ... P 18. SELENIUM .... P 18.SELENivM., •. F 19. SILV:ER •••••• P 20.SODitJM •••• , .P [ 2 L THALLIUM ••• , F ( 22,TIN ........ ,P 23.VANADIUM .... P [ 24.ZINC •..•.• , ,p 25.CYANIDE •.•.. C

% SOLID

COMMENTS:

MEDIUM: XX

MG/KG DRY WEIGHT 1941 <7 u

N/R <2.3 u

31) <0.3 u

<2.0 577]

6 <3,5 u

17 3803 *

N/R 51.3 s

<184 u 45 *

<0,1 u <17 u

<252 u N/R

<2.l u R <l.3 u

1127) 4]

<18 u 6.3]

24 N/R

75

/1 //"iz;r.,/'"'-·

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U.S. EPA CON ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA140 := Ljc,SI ( DA':E: 4/9/85 S ,.1.,J \--0.-Q. E'


LAB NAME: CALIF.ANAL.LAB. CASE NO:L7f 4 C'; SOW NO.: ;J-6!-6J?U QC RPT. #.J3/1) LAB.SAMPLE NO.: P2224



ELEMENTS,.METHOD l, ALUMINIUM .•• P 2. ANTIMONY .... P 3. ARSENIC ...•. P 3. ARSENIC .. , .• F 4, BARIUM ...... P 5. BERYLLIUM ... P 6. CADMIUM, .. , • P 7. CALCIUM ... ,,P 8. CHROMIUM .... P 9. COBALT ....•. P IO.COPPER ...... P 11.IRON ....... ,P 12. LI:AD ..... , .. P 12. LEAD •••••• , • F 13.MAGNESIUM •.. P 14,MANGANESE .•. P 15.MERCURY .... CV 16.NICKEL ...... P 17.POTASSIUM .•• P 18.SELENIUM .... P 18.SELENIUM .... F 19.SILVER ...•.. P 20,SODIUM,,, ... P 21. THALLIUM •••• F 2 2. TIN •••• , •••• P 23,VANADIUM ...• P 24.ZINC ....•••. P 25,CYANIDE •..•. C

% SOLID

COMMENTS:

[ [

[

(

(

[ [

(

xx MEDIUM: XX

MG/KG DRY WEIGHT 2052 <7 U N/R 2.7)

50) <0.3 U

<2.0 429]

17 <3. 5 U

5] 3522 * N/R

66.3 <184 U

174 * <0.1 U

<17 U 338) N/R

<2.1 U R <1.3 U

507] 4]

<18 U 7.3)

60 N/R

83

{3Lk.. i, /. o t 1 0

LAB MA!IAGER:/1,.,,.._,,

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U.S. EPA COl .ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE No:

MFA14 l !:. t/OSl.

41 P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490 DATE: 4/9/85 13 ll<. 1, L() f: I 0

t!H c: \ r INORGANIC ANALYSIS .:i EET ._,,'-'--OS.,.._,· 1-o_o o



CONC.: LOW: MEDitn1: xx MATRIX: SOIL: xx

ELEMENTS •• METHOD MG/KG DRY WEIGHT 1. ALUMINIUM ••• P 3978 * 0" 2. ANTIMONY ..•. P <7 u R '° 3. ARSENIC ...•. P N/R L(\ 3 • ARSENIC ....• F <2.3 u

0 4 • BARIUM •••••• P ( 43] 5. BERYLLIUM •.• P ( o.3J 0 6. CADMIUM ..... P <2.0 0 7. CALCIUM .•••. P ( 339) -8. CHROMIUM •••. P 7 9. COBALT ...... P [ 7] 10,COPPER .....• P <0.65 u 11.IRON •••••••• P 4948 12,LEAD .......• P N/R 12. LEAD •••••••• F 16.9 s R 13.MAGNESIUM., .P <184 u 14,MANGANESE •.• P 755 R 15.MERCURY •••• cv <0.1 u R 16.NICKEL .... , .p <17 u 17.POTASSIUM ... P <252 u 18. SELENIUM ••.• P N/R 18.SELENIUM .... F <2.1 u R 19.SILVER ....•. P <l.3 u R 20.SODIUM •...• ,P [ 514) 21. THALLIUM. , .• F ( 4) 22,TIN ••••..... P <16 u 23.VANADIUM .... P [ 12,9] 24.ZINC ........ P <1.6 u 25.CYANIDE ••..• C N/R

% SOLID 86

COMMENTS:


U.S. EPA CO! !ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

MFA142 ~ '106-8

42 P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:B-557-2490 DATE:4/9/85

INORGANIC ANALYSIS SHEET BU< G Let 1

s .... b~·..._1f:LCE..


ELEMENTS IDENTIFIED AND MEASUR!°'D

CONC.: LOW: MEDIUM: xx MATRIX: SOIL: xx

ELEMENTS .. METHOD MG/KG DRY WEIGHT l. ALUMINIUM .•. P 1394 * 2. ANTIMONY •... P <7 u R 3. ARSENIC ..... P N/R 3. ARSENIC ....• F <2.3 u 4. BARIUM •••••• P [ 84] 5. BERYLLIUM ••• P <0.3 u 6. CADMIUM ..... P <2.0 7. CALCIUM ••••• P ( 1538) 8. CHROMIUM ..•. P <1.1 U 9. COBALT •..... P <3.5 U lOgCOPPER ...••. P <0.65 u 11. IRON •.•••••• P 1739 12. LEAD •••••••• P N/R 12.LEAD ...•.... F 10.s s R 13.MAGNESIUM ... P <184 u 14.M.ANGANESE .•. P 110 R 15.MERCURY ..•. cv <0.1 U R 16.NICKEL •..•.• P <17 u 17.POTASSIUM ... P <252 u 18. SELENIUM .... P N/R 18,SELENIUM ...• F <2.1 U R 19.SILVER .•••.. P <1.3 u R 20.SODIUM •....• P [ 495] 21.THALLIUM ...• F <2,1 u 22,TIN .•.....•• P <18 u 23.VANADIUM., .. P [ 2.7] 24,ZINC ........ p <1.6 U 25,CYANIDE ....• c N/R

% SOLID 81

COMMENTS:

LAB MANAGER: l/z.~/1-

0

r-11"1

0 0 0 -

I I

I :

I I I I I I I I I I

I I

I

, I I

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U.S. EPA COh ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA143 ~ '-/ o'/1 DA'l'E:4/9/85

43

INORGANIC ANALYSIS SHEET BU<L, Lot 18

LAB NAME! CALIF.ANAL.LAB. CASE N0:3940 SOW NO.: 68-01-6810 QC RPT,#3940 LAB. SAMPLE NO.: P2227

ELEMENTS IDENTIFIED A.ND MEASURED

CONC.: LOW: MEDIUM: xx MATRIX: SOIL: xx

ELEMENTS •. METHOD MG/KG DRY WEIGHT 1. ALUMINIUM ••• P 1771 * 2. ANTIMONY •••• P <7 u R 3. ARSENIC ••••• P N/R 3 • ARSENIC ...•. F <2.3 u 4. BARIUM •••••• P [ 29] 5. BERYLLIUM ••• P <0.3 u 6. CADMIUM ...•. P <2.0 7. CALCIUM ..••. P [ 671] 8. CHROMIUM •••• P [ 3] 9. COBALT ...••. P <3.5 u 10.COPPER ...... P <0.65 u 11.IRON ••••••• • P 3722 12. LEAD ......•. P N/R 12.LEAD ....•... F 91.3 s R 13.MAGNESIUM ... P <184 u 14.MANGANESE ••• P 56 R 15.MERCURY •.•• cv <0.1 U R 16.NICKEL •.•••• P <17 u 17.POTASSIUM .•. P <252 u 18.SELENIUM ...• P N/R 18. SELENIUM •• , • F <2,1 u R 19.SILVER ....•. P <l.3 u R 20. SODIUM •••••• P [ 001) 2 1. THALLIUM •.•• F <2.1 u 22.TIN ••••.•••• P <18 u 2 3 • VANADIUM •••• P [ 4.7) 24.ZINC ..•..••• P ( 10) 25.CYANIDE ...•• c N/R

% SOLID 75

COMMENTS:

LAB MANAGER:~,,,

~

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0 0 0 -


u.s. EPA cot ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EJ?A SAMPLE NO:

MFA144-:. l/-OS"l/

44 P.O. BOX 818 AI,EXANDRIA, VA 22313 703/557-2490 FTS:8-557-2490 DATE:4/9/85 Blk 1 L -I:

-, I) ..zo INORGANIC ANALYSIS SHEET S ""'- °\) s ...., -r ~ ,l,.Cl ~-

LAB NAME: CALIF.ANAL.LAB, CASE NO:3940 SOW NO,: 68-01-6810 QC RPT,#3940 LAB.SAMPLE NO.: P2228


CONC,: LOW: MEDIUM: xx MATRIX: SOIL: xx

ELEMENTS •• METHOD MG/KG DRY WEIGHT l. ALUMINIUM, •. P 1675 * ('1

2. ANTIMONY •.•. P <7 u R r-3 • ARSENIC ••••• P 1'1'/R I.(\ 3. ARSENIC ...•• F <2.3 u

0 4. BARIUM.,, •• , P [ 26) 5. BERYLLIUM ••• P <0.3 u 0 6. CADMIUM •••.• P <2.0 0 7. CALCIUM ••••. P [ 379] -s. CHROMIUM •••• P [ 3) 9. COBALT ••.•.• P <J.5 u 10.COPPER, ••••. P <0.65 u 11. IRON. , •••••• P 2458 12. LEAD •••••••• P N/R 12, LEAD. , ••.••• F 14.1 s R 13.MAGNESIUM ••. P <184 u 14.MANGANFSE ... P 61 R 15. MERCURY •••• CV <0.1 u R 16.NICKEL, .•.•• P <17 u 17,POTASSIUM .•• P <252 u 18,SELENIUM •.•. P N/R 18.SELENIUM •••. F <2.1 u R 19. SILVER •• ,.,. P <l.3 u R 20,SODIUM •••••• P [ 4 71] 2 l. THALLIUM •••• F <2.1 u 22,TIN ••••••••• P <l8 u 23,VANAOIUM •..• P [ 5.1] 24.ZINC, •• , •••• P 36 25.CYANIDE .•••• C N/R

% SOLID 85

COMMENTS:

LAB MANAGE~-,'


U.S. EPA co~ ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO: P.O. BOX 818 ALEXANDRIA,VA 22313 703/557-2490 FTS:8-557-2490

MFA145::. lf-t,SO DATE:4/9/85


LAB NAME: CALIF.ANAL.LAB. CASE NO:3940 SOW NO.: 68-01-6810 QC HPT.#3940 LAB.SAMPLE NO.: P2229



ELEMENTS. , METHOD 1 • ALUMINIUM ••• P 2 • ANTIMONY •••• P 3. ARSENIC ••••• P 3. ARSENIC ..... F 4. BARIUM ...... P 5 • BERYLLIUM .•• P 6. CAOMIUM ..... P 7. CALCIUM ...•• P 8. CHROMIUM .... P 9. COBALT •••• , • P 10.COPPER ...... P 11.IRON ........ P 12. LEAD •••••••• P 12. LEAD ........ F 13 .MAGNESIUM •• , P l 1L MANGANESE ••• P 15.MERCURY .... cv 16.NICKEL ...... P 17,POTASSitJM ... P 18.SELENitJM .... P 18.SELENIUM .... F 19.SILVER •.•... P 20. SODIUM •••••• P 21. THALLIUM •••• F 22.TIN •.•••.••• P 23.VANADIUM .... P 24.ZINC •••••••• P 25.CYANIDE ••••• c

% SOLID

COMMENTS:

MEDIUM: XX xx

MG/KG DRY WEIGHT 2704 * <7 U R N/R

[ 2.6] [ 61] [ 0.4)

<2.0 [ 1050]

15 <3.5 U

15 11045

N/R 61. 5 S R

<184 U 158 R

o, z_J'- -2--B--r..-O~/I&-, R <17 U

<252 U N/R

<2.1 U R <1.3 U R

( 545) <2.1 U

<18 U ( 15.4]

60 N/R

78

LAD MANAGER: t!-t,;,,";::'

45

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0 0 0


U.S. EPA CO? .ACT LABORATORY PROGRAM SAMPLE MANAGEMENT OFFICE EPA SAMPLE NO:

46 P.O. BOX 818 ALEXANORIA,VA 22313 MFA146~ ~O.Sfu ( 703/557-2490 FTS: 8-557-2490 DATE: 4/9/85 SuJ,ls -•-•-h1.~ ~-

INORGANIC ANALYSIS SHEET BLK {;,, LtJT 3




ELEMENTS •. METH0D 1. ALUMINIUM ••• P 2 . ANTIMONY • . . . P 3. ARSENIC .•••. P 3. ARSENIC .•... F 4. BARIUM ....•. P 5 . BERYLLIUM ... P 6 • CADMIUM • • • • • P 7 • CALCIUM ••••• P 8. CHROMIUM .••• P 9. COBALT •••••• P 10.COPPER .•...• P 11. IRON .••••••• P 12. LEAD •••••••• P 12 . LEAD ...•..•• F 13.MAGNESIUM .•• P 14.MANGANESE .•. P 15.MERCURY .•.. cv 16.NICKEt ••••.• P ~7.POTASSIUM .•• P 18.SELENIUM •••. P 18.SELENIUM ..•• F 19.SILVER ••.••• P 20.SOD!UM ..•••• P 21.THALLlUM ..•. F 22.TIN •.•..•.•. P 23.VANADIUM .... P 24.ZINC ••..•.•. P 25.CYANIDE ..•.• C

% SOLID

COMMENTS:

xx

(

(

(

(

MEDIUM: XX

MG/KG DRY WEIGHT 994 * <7 U R N/R

<2.3 u 10]

<0.3 u <2.0

<214 U 2]

<3.5 U <0.65 U

933 N/R 3.2 s R

<184 u 13 R

<0. l U R <17 U

<252 U N/R

<2.1 U R <1.3 U R

435] <2.1 U

<18 U 4.6]

<1.6 U N/R

86

LAB MANAGER:~,-,..,,

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CASE NUMBER 3940 - INORGANIC ANALYSIS DATA PACKAGE

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