BROOKLYN, NEW YORK Remedial Investigation Report · BROOKLYN, NEW YORK Remedial Investigation...
Transcript of BROOKLYN, NEW YORK Remedial Investigation Report · BROOKLYN, NEW YORK Remedial Investigation...
DOMINO SUGAR SITE E
317-329 KENT AVENUE BROOKLYN, NEW YORK
Remedial Investigation Report
NYC VCP Site Number: 15CVCP002K
Prepared for:
Two Trees Management, LLC
45 Main Street, Suite 602
Brooklyn, NY 11201
Prepared by:
EEBB CC
1808 Middle Country Road
Ridge, NY 11961
September 2014
Environmental Business Consultants
REMEDIAL INVESTIGATION REPORT
TABLE OF CONTENTS
LIST OF ACRONYMS
CERTIFICATION
EXECUTIVE SUMMARY ...................................................................................................... i
REMEDIAL INVESTIGATION REPORT ............................................................................ 1
1.0 SITE BACKGROUND............................................................................................... 1
1.1 Site Location and Current Usage ............................................................................ 1
1.2 Proposed Redevelopment Plan ............................................................................... 1
1.3 Description of Surrounding Property...................................................................... 3
2.0 SITE HISTORY.......................................................................................................... 5
2.1 Past Uses and Ownership........................................................................................ 5
2.1.1 Phase I Environmental Site Assessment Report (EHI, 2004) ......................... 5
2.1.2 Phase I Environmental Site Assessment Report (Emteque LLC, 2012).......... 5
2.2 Previous Investigations ........................................................................................... 7
2.2.1 Phase III Environmental Site Assessment (Nova, 2004) ........................................ 7
2.2.2 Subsurface (Phase II) Investigation (AKRF, 2009) ................................................ 8
2.3 Site Inspection......................................................................................................... 8
2.4 Areas of Concern .................................................................................................... 9
3.0 PROJECT MANAGEMENT.................................................................................... 10
3.1 Project Organization ............................................................................................. 10
3.2 Health and Safety.................................................................................................. 10
3.3 Materials Management.......................................................................................... 10
4.0 REMEDIAL INVESTIGATION ACTIVITIES....................................................... 11
4.1 Geophysical Investigation..................................................................................... 11
4.2 Borings and Monitoring Wells.............................................................................. 11
4.3 Sample Collection and Chemical Analysis........................................................... 12
5.0 ENVIRONMENTAL EVALUATION..................................................................... 17
5.1 Geological and Hydrogeological Conditions........................................................ 17
5.2 Soil Chemistry ...................................................................................................... 17
REMEDIAL INVESTIGATION REPORT
TABLE OF CONTENTS
5.3 Groundwater Chemistry........................................................................................ 18
5.5 Prior Activity ........................................................................................................ 19
5.6 Impediments to Remedial Action ......................................................................... 19
TABLES Table 1 - Construction Details for Soil Borings Table 2 - Soil Analytical Results (VOCs) Table 3 - Soil Analytical Results (SVOCs) Table 4 - Soil Analytical Results (Pesticides/PCBs) Table 5 - Soil Analytical Results (Metals) Table 6 - Groundwater Analytical Results (VOCs) Table 7 - Groundwater Analytical Results (SVOCs) Table 8 - Groundwater Analytical Results (Pesticides/PCBs) Table 9 - Groundwater Analytical Results (Total Metals) Table 10 - Groundwater Analytical Results (Dissolved Metals) Table 11 - Soil Gas Analytical Results (VOCs)
FIGURES Figure 1 - Site Location Map Figure 2 - Site Boundary Map Figure 3 - Redevelopment Plan Figure 4 - Surrounding Land Use Figure 5 - Site Sampling Locations Figure 6 - Soil Exceedences Map Figure 7 - Groundwater Exceedences Map Figure 8 - Soil Vapor Detections
ATTACHMENTS Attachment A - Soil Boring Logs Attachment B - Groundwater Sampling Logs Attachment C - Soil Gas Sampling Logs Attachment D - Laboratory Reports in Digital Format Attachment E - EHI 2004 Phase I Report Attachment F - Emteque 2012 Phase I Report Attachment G - Nova 2004 Phase III Report Attachment H - AKRF 2009 Phase II Report
LIST OF ACRONYMS Acronym Definition
AOC Area of Concern
CAMP Community Air Monitoring Plan
COC Contaminant of Concern
CPP Citizen Participation Plan
CSM Conceptual Site Model
DER-10 New York State Department of Environmental Conservation Technical Guide 10
FID Flame Ionization Detector
GPS Global Positioning System
HASP Health and Safety Plan
HAZWOPER Hazardous Waste Operations and Emergency Response
IRM Interim Remedial Measure
NAPL Non-aqueous Phase Liquid
NYC VCP New York City Voluntary Cleanup Program
NYC DOHMH New York City Department of Health and Mental Hygiene
NYC OER New York City Office of Environmental Remediation
NYS DOH ELAP
New York State Department of Health Environmental Laboratory Accreditation Program
OSHA Occupational Safety and Health Administration
PID Photo-ionization Detector
QEP Qualified Environmental Professional
RI Remedial Investigation
RIR Remedial Investigation Report
SCO Soil Cleanup Objective
SPEED Searchable Property Environmental Electronic Database
CERTIFICATION I, Kevin Brussee, am a Qualified Environmental Professional, as defined in RCNY § 43-1402(ar). I have primary
direct responsibility for implementation of the Remedial Investigation for the Domino Sugar Site E Redevelopment
Project located at 317 to 329 Kent Avenue, Brooklyn, NY, (NYC VCP Site No. 15CVCP002K). I am responsible
for the content of this Remedial Investigation Report (RIR), have reviewed its contents and certify that this RIR is
accurate to the best of my knowledge and contains all available environmental information and data regarding the
property.
Qualified Environmental Professional Date Signature
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
i Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
EXECUTIVE SUMMARY The Remedial Investigation Report (RIR) provides sufficient information for establishment of
remedial action objectives, evaluation of remedial action alternatives, and selection of a remedy
pursuant to RCNY§ 43-1407(f). The remedial investigation (RI) described in this document is
consistent with applicable guidance.
Site Location and Current Usage
Domino Sugar Site E is located at 317 to 329 Kent Avenue in the Williamsburg-South Side
section of Brooklyn, New York, and is currently identified as a portion of Block 2428, Lot 1 on
the New York City Tax Map. Figure 1 shows the Site location. Lot 1 is a 57,600 ft2 lot located
on the east side of Kent Avenue between South 3rd Street to the north and South 4th Street to the
south. Site E has been undeveloped and utilized for parking for employees of the Domino Sugar
Company and other sugar refinery companies since the 1940's. The former parking lot is
currently being utilized as The Brooklyn Bike Park, a recreational bicycle track.
Site A is currently bordered by South 3rd Street to the north, South 4th Street to the south,
several residential apartment buildings and a scrap metal facility to the east and Kent Avenue to
the west. Site A is an rectangular shaped lot consisting of 180 ft of street frontage on Kent
Avenue and 320 ft of street frontage on both South 3rd Street and South 4th Street, for a total of
approximately 57,600 ft2. A map of the site boundary is shown on Figure 2.
Summary of Proposed Redevelopment Plan
Redevelopment of the former Domino Sugar properties (Block 2414, Lot 1 and Block 2428, Lot
1) will include four new mixed-use buildings (Sites A, B, D, E), adaptively reuse the existing
landmarked Refinery building (Site F), create a one acre inland green space to be called Domino
Square (Site C) and develop a new waterfront park.
The proposed future use of Site E will consist of a new 15-story mixed-use building with 5 cellar
levels. The new building will have a total floor area of approximately 774,003 ft2, consisting of
approximately 20,612 ft2 of retail space, a 178,718 ft2 parking facility, and 114,369 ft2 of
community facility uses. This building would rise to a maximum height of approximately 435
feet.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
ii Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
The lowest cellar level (C5) will occupy the majority of the Site E footprint, with the exception
of areas in the northwest and southwest corners. Cellar level C5 will consist of three separate
community facility areas that will be used as a soccer field, gymnasium, and an aquatic center.
Cellar level C5 will also have four elevator pits, and five stairwells. The next lowest cellar level
(C4) will consist of a locker room for the community facilities on C5, and an additional
recreation space for the community facility. Cellar level C3 will consist of a storage room and
office space for the community facilities, and several large mechanical rooms. Cellar levels C2
and C1 will consist of an underground parking garage, but will also contain the the electrical
room, telecom room, plumbing room, gas meter room, water and sewer room, fire protection
room, two compactor rooms, bike storage room, men's and women's lockers and lunch room, the
building supers' office, workshop and storage room.
The building's first floor will consist of three retail spaces on the west end of the building, the
building's residential lobby, and additional parking. The second floor will have apartments along
the west end of the building, additional ground level retail spaces along the eastern end of South
3rd Street and South 4th Street, and additional parking spaces within the middle of the building.
The third floor will consist of residential apartments along Kent Avenue, South 3rd Street and
South 4th Street, and parking within the center of the building. After the 3rd floor, the building
divides into two separate towers. The two residential towers rise from the 4th floor to the 12th
floor before joining again at the 13th floor. The 4th through 15th floors consist solely of
residential apartments.
Assuming an excavation depth of approximately 52 ft for the entire 57,600 ft2 lot for
construction of the new building's five cellar levels, a total of approximately 111,000 cubic yards
(166,400 tons) of soil will require excavation. Layout of the proposed site development is
presented in Figure 3. The current zoning designation is C6-2. The proposed use is consistent
with existing zoning for the property.
Summary of Past Uses of Site and Areas of Concern
Historic Sanborn maps were reviewed to determine the historic use of Site E. The Sanborn maps
indicate Site that prior to 1887, Site was primarily developed with multiple 3-story row houses
along South 3rd Street and South 4th Street. However, the northwest corner of Site E was
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
iii Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
developed with a 9-story industrial building identified as the kiln and filter house for the
Havemeyer & Elder Sugar Refinery located across Kent Avenue. The building contained
numerous coal fired boilers and two large smoke stacks.
By 1904 Sanborn map, the sugar refinery operation had expanded to several of the lots along
South 4th Street. The sugar refinery facility operated under the name American Sugar Refinery.
It consisted of a 7-story industrial building at 29 to 35 South 4th Street that housed 16 electrical
engines, a 2-story building at 38-40 South 3rd Street that was utilized for coal storage, a 2 and 4-
story building at 42-44 South 3rd Street that housed numerous boilers, and a 10-story industrial
building at 317-323 Kent Avenue that consisted of 14 boilers, and was utilized as the kiln and
filter house. Several of the 3-story row houses along South 4th Street were also utilized by
American Sugar Refinery for pattern storage. A small lot at 325 Kent Avenue was developed
with three 3-story buildings identified as the facility's plating room, paints, and saw-dust house.
By 1918, the American Sugar Refining Company of NY utilized nearly the entire footprint of
Site E, with the exception of a 3-story apartment building w/first floor store on the corner of
South 4th Street and Kent Avenue (329 Kent Avenue). The 1918 Sanborn map labels Site E as
several distinct sections with letters according to the use of the buildings by the American Sugar
Refining Company of NY.
Section G - Consists of two buildings and an open space area - 1) 317 - 323 Kent Avenue
- A 9-story building with a basement that was used as the kiln and filter house, 2) 32-36
South 3rd Street - labeled as the old boiler house, and as vacant and partly removed, and
3) 38-40 South 3rd Street - a coal yard.
Section Q - Consists of three buildings 1) 46-54 South 3rth Street - A 68ft high building
consisting of six large syrup tanks, 2) 42-44 South 3rd Street - a 2-story building used for
storage of bone black and 3) 49 South 4th Street - a 1-story building labeled as a filling
house.
Section P - Developed with two adjacent seven story buildings. The building at 37-49
South 4th Street was labeled as the filter house, and the building at 29-35 South 4th Street
was labeled as the filler house.
Section T - Developed with a former 3-story residential building labeled as the pattern
shop, and an open lot likely used for parking.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
iv Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
By 1935, most of the industrial buildings are vacant, and by 1947, the majority of the
buildings on Site E were demolished. The remaining two 3-story buildings on the corner of
South 4th Street and Kent Avenue (327 and 329 Kent Avenue) were demolished by 1977.
The AOCs identified for Site E include:
1. Historic fill layer is present at the Site from grade to depths as great as 15 feet below
grade;
2. The past use of a portion of Site E as a plating facility; and
3. Areas of the Site that were formerly developed with industrial buildings that house large
scale electric generators and boilers for the sugar refinery.
Summary of the Work Performed under the Remedial Investigation
EBC performed the following scope of work within Site E in April of 2014:
1. Conducted a Site inspection to identify AOCs and physical obstructions (i.e. structures,
buildings, etc.);
2. Installed six soil borings within Site E, and collected twelve soil samples for chemical
analysis from the soil borings to evaluate soil quality; and
3. Installed two groundwater monitoring wells within Site E and collected two groundwater
samples from the two monitoring wells, and collected one groundwater sample from an
existing geotechnical monitoring well to evaluate groundwater quality; and
4. Installed five soil vapor probes across the Site and collected five soil vapor samples for
chemical analysis.
Summary of Environmental Findings
1. The elevation of Site E is approximately 34 feet on the eastern end, and approximately 21
feet along Kent Avenue.
2. Depth to groundwater varies across Site E from approximately 34 feet on the eastern end,
to approximately 22 feet along Kent Avenue.
3. Depth to bedrock is at the Site is greater than 100 feet.
4. The stratigraphy of Site E, from the surface down, consists of a layer of historic fill
material that varies from 2 to approximately 15ft, underlain by a medium silty brown
sand with gravel.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
v Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
5. Soil/fill samples collected during the 2014 EBC RI, 2004 Nova Phase III, and 2008
AKRF Phase II showed no VOCs above Unrestricted Use SCOs with the exception of
acetone (68 micrograms per kilogram [µg/Kg]). Naphthalene (maximum [max] of 430
µg/Kg) was detected in multiple soil samples below Unrestricted Use SCOs. Eight
SVOCs including benz(a)anthracene (max of 23,000 μg/Kg), benzo(a)pyrene (max of
20,000 μg/Kg), benzo(b)fluoranthene (max of 20,000 μg/Kg), benzo(k)fluoranthene (max
of 20,000 μg/Kg), chrysene (max of 19,000 μg/Kg), dibenz(a,h)anthracene (max of 8,600
μg/Kg), indeno(1,2,3-cd)pyrene (max of 18,000) and phenanthrene (max of 160,000
μg/Kg) were detected above Unrestricted Use and Restricted Residential Use SCOs
within soil samples retained from the historic fill layer. Several metals including arsenic
(137 mg/Kg), cadmium (8.19 mg/kg), copper (max of 185 mg/Kg), lead (max of 446
mg/Kg), mercury (max of 0.55 mg/Kg), nickel (39.6 mg/Kg), and zinc (max of 1,480
mg/Kg) were detected above Unrestricted Use SCOs. Of these metals, arsenic, cadmium
and lead also exceeded Restricted Residential Use SCOs within soil samples collected
from the historic fill layer. PCB-1254 (210 µg/Kg) was detected within one shallow soil
sample at a concentration above Unrestricted Use SCOs and within one shallow soil
sample and PCB-1260 (maximum of 25 µg/Kg) was detected within two shallow soil
samples at a concentration below Unrestricted Use SCOs. The pesticides 4,4'-DDD (max
of 15 µg/Kg) and 4,4'-DDT (max of 13 µg/Kg) were detected within two shallow soil
samples at a concentration above Unrestricted Use SCOs. Neither the pesticides nor
PCBs were detected within any of the deeper soil samples retained from the same soil
boring locations. Overall, the findings were consistent with observations for historical fill
sites in areas throughout NYC.
6. Groundwater samples collected during the 2014 EBC RI and 2008 AKRF Phase II
showed no detectable concentrations of pesticides or PCBs. The chlorinated VOCs cis-
1,2-dichlorothene (maximum of 5.56 µg/L), tetrachloroethene (maximum of 5.7 µg/L),
and trichloroethene (maximum of 27 µg/L) were detected within the groundwater
samples collected by AKRF in 2008 and EBC in 2014 above GQS. The following VOCs
were detected in one or more of the groundwater samples at concentrations below GQS:
1,1-dichloroethene (1.7 µg/L), acetone (maximum of 2.7 µg/L), carbon disulfide (0.90
µg/L), chloroform (1.5 µg/L), and methylene chloride (0.38 µg/L). SVOCs detected
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
vi Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
above GQS included benzo(a)anthracene (max of 0.49 µg/L), benzo(b)fluoranthene (max
of 0.48 µg/L), benzo(k)fluoranthene (0.08 µg/L), bis(2-ethylhexyl)phthalate (max of 42
µg/L), chrysene (max. of 0.49 µg/L), and indeno(1,2,3-cd)pyrene (3.7 µg/L) in one or
more of the three groundwater samples collected by EBC in 2014 and the groundwater
sample collected by AKRF in 2008. Dissolved metals present in groundwater at levels
above GQS included iron, lead, magnesium, manganese, selenium and sodium. The
presence of some of these metals in groundwater, specifically those that are common
salinity indicators, can be attributed to the proximity to the East River and the intrusion of
road salting.
7. Soil vapor samples collected during the 2014 EBC RI indicated petroleum related VOCs
and chlorinated VOCs were present at low concentrations. Petroleum-related VOCs
(BTEX) were detected at a maximum concentration of 141.43 μg/m3. Overall the highest
reported concentrations was for acetone (maximum of 7693 μg/m3). Trichloroethylene
(TCE) was detected in three of the five soil vapor samples at a concentration ranging
from 241 to 61.2 μg/m3. The New York State Department of Health (NYSDOH) Final
Guidance on Soil Vapor Intrusion (October 2006) notes mitigation is the recommended
action for a TCE concentrations above 250 μg/m3 in soil gas.Tetrachloroethylene (PCE)
was detected in all five soil vapor samples, and ranged in concentration from 2.03 to 28.3
μg/m3. Carbon tetrachloride was detected within three of the five soil vapor samples at a
maximum concentration of 0.566 μg/m3, and 1,1,1-trichloethylene (TCA) was detected in
three of the five soil vapor samples at a maximum concentration of 3.54 μg/m3. The PCE,
carbon tetrachloride and TCA concentrations are below the monitoring level ranges
established within the NYSDOH Final Guidance on Soil Vapor Intrusion.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
1
EEBB CC Environmental Business Consultants 1808 Middle Country Road
Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
REMEDIAL INVESTIGATION REPORT 1.0 SITE BACKGROUND
Two Trees Management LLC has applied to enroll in the New York City Voluntary Cleanup
Program (NYC VCP) to investigate and remediate a 1.32-acre Site located at 317 to 329 Kent
Avenue in the Williamsburg-South Side section of Brooklyn, New York. Site E will be
redeveloped with a 15-story mixed use building that will have 5 cellar levels for community
facility space and parking. The portion of the RI work conducted on Site E was performed
between April 2, 2014, and May 8, 2014. This RIR summarizes the nature and extent of
contamination and provides sufficient information for establishment of remedial action
objectives, evaluation of remedial action alternatives, and selection of a remedy that is protective
of human health and the environment consistent with the use of the property pursuant to RCNY§
43-1407(f).
1.1 Site Location and Current Usage
Domino Sugar Site E is located at 317 to 329 Kent Avenue in the Williamsburg-South Side
section of Brooklyn, New York, and is currently identified as a portion of Block 2428, Lot 1 on
the New York City Tax Map. Figure 1 shows the Site location. Lot 1 is a 57,600 ft2 lot located
on the east side of Kent Avenue between South 3rd Street to the north and South 4th Street to the
south. Site E has been undeveloped and utilized for parking for employees of the Domino Sugar
Company and other sugar refinery companies since the 1940's. The former parking lot is
currently being utilized as The Brooklyn Bike Park, a recreational bicycle track.
Site A is currently bordered by South 3rd Street to the north, South 4th Street to the south,
several residential apartment buildings and a scrap metal facility to the east and Kent Avenue to
the west. Site A is an rectangular shaped lot consisting of 180 ft of street frontage on Kent
Avenue and 320 ft of street frontage on both South 3rd Street and South 4th Street, for a total of
approximately 57,600 ft2.A map of the site boundary is shown on Figure 2.
1.2 Proposed Redevelopment Plan
Redevelopment of the former Domino Sugar properties (Block 2414, Lot 1 and Block 2428, Lot
1) will include four new mixed-use buildings (Sites A, B, D, E), adaptively reuse the existing
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
2 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
landmarked Refinery building (Site F), create a one acre inland green space to be called Domino
Square (Site C) and develop a new waterfront park.
The proposed future use of Site E will consist of a new 15-story mixed-use building with 5 cellar
levels. The new building will have a total floor area of approximately 774,003 ft2, consisting of
approximately 20,612 ft2 of retail space, a 178,718 ft2 parking facility, and 114,369 ft2 of
community facility uses. This building would rise to a maximum height of approximately 435
feet.
The lowest cellar level (C5) will occupy the majority of the Site E footprint, with the exception
of areas in the northwest and southwest corners. Cellar level C5 will consist of three separate
community facility areas that will be used as a soccer field, gymnasium, and an aquatic center.
Cellar level C5 will also have four elevator pits, and five stairwells. The next lowest cellar level
(C4) will consist of a locker room for the community facilities on C5, and an additional
recreation space for the community facility. Cellar level C3 will consist of a storage room and
office space for the community facilities, and several large mechanical rooms. Cellar levels C2
and C1 will consist of an underground parking garage, but will also contain the the electrical
room, telecom room, plumbing room, gas meter room, water and sewer room, fire protection
room, two compactor rooms, bike storage room, men's and women's lockers and lunch room, the
building supers' office, workshop and storage room.
The building's first floor will consist of three retail spaces on the west end of the building, the
building's residential lobby, and additional parking. The second floor will have apartments along
the west end of the building, additional ground level retail spaces along the eastern end of South
3rd Street and South 4th Street, and additional parking spaces within the middle of the building.
The third floor will consist of residential apartments along Kent Avenue, South 3rd Street and
South 4th Street, and parking within the center of the building. After the 3rd floor, the building
divides into two separate towers. The two residential towers rise from the 4th floor to the 12th
floor before joining again at the 13th floor. The 4th through 15th floors consist solely of
residential apartments.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
3 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
Assuming an excavation depth of approximately 52 ft for the entire 57,600 ft2 lot for
construction of the new building's five cellar levels, a total of approximately 111,000 cubic yards
(166,400 tons) of soil will require excavation. Layout of the proposed site development is
presented in Figure 3. The current zoning designation is C6-2. The proposed use is consistent
with existing zoning for the property.
Layout of the proposed site development is presented in Figure 3. The current zoning designation
is C6-2. The proposed use is consistent with existing zoning for the property.
1.3 Description of Surrounding Property
The area immediately surrounding Site E consists of the former Domino Sugar facility buildings
to west, and industrial buildings to the north, south and east. Figure 4 shows the surrounding land
usage of the adjacent properties listed below as well as additional properties located up to 500
feet away from the Site. No hospitals, schools or daycare facilities are located within a 250 ft
radius of the Site.
Surrounding Property Usage
Direction Property Description
North – Opposite side of South 3rd Street
Block 2415, Lot 1 - 315 Kent Avenue Developed with a 1-story industrial/manufacturing building
Block 2415, Lot 7501 - 29 South 3rd Street Developed a new 4-story, 26-unit residential apartment building.
Block 2415, Lot 38 - 37 South 3rd Street Developed a 4-story, 8-unit residential apartment building, with first floor retail space.
Block 2415, Lots 36 and 37 - 41 and 43 South 3rd Street Two small undeveloped lots
South – Opposite side of South 4th Street
Block 2441, Lot 8 - 331 Kent Avenue Developed with a 2-story commercial/office building consisting of 3 commercial spaces and one residential unit.
Block 2441, Lot 12 - 34 South 4th Street Developed with a 1-1/2-story industrial/manufacturing building constructed in 1996.
Block 2441, Lot 15 - 48 South 4th Street Developed with former 2-1/2 story industrial/manufacturing building converted into residential apartments.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
4 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
Block 2441, Lot 21 - 47 South 5th Street Developed with a small one-story industrial/manufacturing building converted into a bar/restaurant.
East – Adjacent Property
Block 2428, Lot 24 - 56 South 3rd Street Developed with a new 4-story residential/apartment building. Block 2428, Lot 30 - 55 South 4th Street Developed with a one industrial/manufacturing building utilized for scrap metal sorting/storage. Block 2428, Lots 36 and 27 - 376 and 378 Wythe Avenue Two thin lots developed with multi-family walk-ups with rear yards.
West –
Block 2414, Lot 1 (SITE C) - 314 Kent Avenue Former industrial buildings associated with the Domino Sugar Factory.
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
5 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
2.0 SITE HISTORY
2.1 Past Uses and Ownership
Two Phase I Environmental Site Assessment (ESA) Reports have been completed for Sites A, B,
C, D, E and F. Both reports are summarized below.
2.1.1 Phase I Environmental Site Assessment Report (EHI, 2004)
A Phase I Environmental Site Assessment Report was completed by Environmental Health
Investigations, Inc. in 2004, for Sites A, B, C, D, E, and F. A copy of the Phase I Report is
attached in Attachment E. The Phase I Environmental Site Assessment Report identified the
vacant lot as parking for Domino Sugar employees, but did not thoroughly investigate the Site E
history prior to use as parking. The Phase I Report did not reveal any on-Site Recognized
Environmental Conditions in connection with Site E.
2.1.2 Phase I Environmental Site Assessment Report (Emteque LLC, 2012)
A Phase I Environmental Site Assessment Report was completed by Emteque LLC in 2012, for
Sites A, B, C, D, E, and F. A copy of the Phase I Report is attached in Attachment F. Historic
Sanborn maps provided within the report were reviewed to determine the following historic use
of Site E:
1887 Sanborn Map - The 1887 Sanborn map indicates Site E formerly consisted of multiple
20 or 25ft wide lots along South 3rd Street and South 4th Street that were developed with 3
story houses. The northwest corner of Site E was developed with a 9-story building used as
the kiln and filter house for the Havemeyer & Elder Sugar Refinery. The building contained
numerous coal fired boilers and two large smoke stacks.
1904 Sanborn Map - The 1904 Sanborn map indicates the sugar refinery operation
expanded to several of the lots along South 4th Street. The facility was now operated under
the name American Sugar Refinery. It consisted of a 7-story building at 29 to 35 South 4th
Street that housed 16 engines, a 2-story building at 38-40 South 3rd Street that was utilized
for coal storage, a 2 and 4-story building at 42-44 South 3rd Street that housed numerous
boilers, and a 10-story building at 317-323 Kent Avenue that consisted of 14 boilers, and was
utilized as the kiln and filter house. Several of the 3-story houses at 37, 39 and 41 South 4th
DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report
6 Environmental Business Consultants
EEBB CC 1808 Middle Country Road Ridge, NY 11961
Phone 631.504.6000 Fax 631.924.2870
Street are labeled as pattern storage. A small lot at 325 Kent Avenue is developed with three
buildings labeled as a plating room, paints, and saw-dust house.
1918 Sanborn Map - The 1918 Sanborn map indicates the American Sugar Refining
Company of NY utilized nearly the entire footprint of Site E, with the exception of a 3-story
apartment building w/first floor store on the corner of South 4th Streetn and Kent Avenue
(329 Kent Avenue). Site E is shown as being developed with the following:
o Section G - Consists of two buildings and an open space area - 1) 317 - 323 Kent
Avenue - A 9-story building with a basement that was used as the kiln and filter
house, 2) 32-36 South 3rd Street - labeled as the old boiler house, and as vacant and
partly removed, and 3) 38-40 South 3rd Street - a coal yard.
o Section Q - Consists of three buildings 1) 46-54 South 3rth Street - A 68ft high
building consisting of six large syrup tanks, 2) 42-44 South 3rd Street - a 2-story
building used for storage of bone black and 3) 49 South 4th Street - a 1-story building
labeled as a filling house.
o Section P - Developed with two adjacent seven story buildings. The building at 37-49
South 4th Street was labeled as the filter house, and the building at 29-35 South 4th
Street was labeled as the filler house.
o Section T - Developed with a former 3-story residential building labeled as the
pattern shop, and an open lot likely used for parking.
1935 Sanborn Map - The 1935 Sanborn map appears to label most buildings as the same as
those depicted on the 1918 Sanborn map, but most buildings are labeled as vacant.
1947, 1950 and 1965 Sanborn Maps - The 1947, 1950 and 1965 Sanborn maps depict the
majority of Site E as being undeveloped with the exception of two 3-story buildings on the
corner of South 4th Street and Kent Avenue (327 and 329 Kent Avenue).
1977-2007 Sanborn Maps - All Sanborn maps from 1977 to 2007 depict the entire footprint
of Site E as undeveloped.
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The Emteque LLC Phase I Environmental Site Assessment Report identified multiple recognized
environmental conditions in connection with Lot 1. However, only one is believed to be
associated with Site E:
Historic / Urban fill (Site A) - Emteque LLC stated previous environmental investigations
have identified soil and groundwater contamination attributed to previous filling of the
property prior to development. Emteque LLC recommended additional sampling of soil and
groundwater to fully characterize the site to aid in the development and implementation both
engineering and institutional controls. Additionally, further characterization of the site soil
will be required prior to its off-site disposal.
2.2 Previous Investigations
EBC was provided digital copies of previous investigations performed at the Site. A summary of
each is provided below.
2.2.1 Phase III Environmental Site Assessment (Nova, 2004)
A Phase III Environmental Site Assessment was performed at Site E, as well as the remainder of
the Domino Sugar property (Sites A, B, C, D and F) by Nova Consulting & Engineering, LLC
(Nova) in June of 2004. The Phase III Environmental Site Assessment included the installation
of five evenly spaced soil borings across Site E. From each of the five soil borings, Nova
retained soil samples in 4 ft intervals from 0-4 feet below grade to 16 to 20 feet below grade or
refusal.
Each of the soil samples were submitted for laboratory analysis of VOCs, and SVOCs, and the
soil samples retained from soil borings B-4 and B-5 were also submitted for laboratory analysis
of RCRA metals. The laboratory results are compared to NYSDEC Unrestricted Use Soil
Cleanup Objectives (UUSCOs) and Restricted Residential Use Soil Cleanup Objectives
(RRSCOs) as presented in 6NYCRR Part 375-6.8 and CP51 on Tables 2a, 3a, and 5. Figure 6
shows the location and posts the values for soil that exceeds UUSCOs and RRSCOs. A copy of
the report is included in Attachment G.
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2.2.2 Subsurface (Phase II) Investigation (AKRF, 2009)
A Subsurface (Phase II) Investigation was performed across Lot 1, and Block 2428, Lot 1 by
AKRF, Inc. (AKRF) in February of 2009. The Subsurface (Phase II) Investigation was
conducted to determine whether current or former on- or off-site activities have adversely
affected the subject property. AKRF’s Subsurface (Phase II) Investigation included the following
work on Site E:
Installation of two soil borings (SB-12 and SB-13) to collect a shallow soil sample (0-2ft)
and a deep soil sample from both soil borings (16-18ft and 27-29ft) for laboratory
analysis.
Conversion of soil boring SB-13 into a monitoring well and the collection of one
groundwater sample from the monitoring well.
Each of the four soil samples were submitted for laboratory analysis of VOCs, SVOCs,
pesticides/PCBs and metals. The laboratory results are compared to 6NYCRR Part 375-6.8 and
CP51 as presented in Tables 2a, 3a, 4, and 5. Figure 6 shows the location and posts the values for
soil that exceeds UUSCOs and RRSCOs.
Groundwater sample SB-13 was submitted for laboratory analysis of VOCs, SVOCs,
pesticides/PCBs, total metals and dissolved metals. The laboratory results are summarized on
Tables 6 through 10, and compared to New York State 6NYCRR Part 703.5 Class GA
Groundwater Quality Standards (GQS). Figure 7 shows the location and posts the values for
groundwater that exceed GQS. A copy of the report is included in Attachment H.
2.3 Site Inspection
Mr. Dominick Mosca of EBC performed a site inspection on Thursday, April 2, 2014, beginning
at approximately 7:00 am. The reconnaissance included a visual inspection of Site E, roadways,
and sidewalks surrounding Site E, and the exterior of adjacent properties. At the time of the
inspection, Site E was undeveloped, but was utilized as a bicycle park. The Site was uncapped,
and the exposed soil cover has shaped to construct roadways/pathways for bicycles. An 8-foot
high chain link fence was constructed around the perimeter of the Site and gates on South 3rd
Street, South 4th Street and Kent Avenue provided access. A small trailer was set up near the
gate on Kent Avenue, which was utilized for bicycle rentals and access to the bicycle park.
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No storm drains, aboveground storage tanks, or any hazardous chemicals were observed in Site E
during the Site inspection.
2.4 Areas of Concern
The AOCs identified for Site E include:
1. Historic fill layer is present at the Site from grade to depths as great as 15 feet below
grade;
2. The past use of a portion of Site E as a plating facility; and
3. Areas of the Site that were formerly developed with industrial buildings that house large
scale electric generators and boilers for the sugar refinery.
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3.0 PROJECT MANAGEMENT
3.1 Project Organization
The Qualified Environmental Profession (QEP) responsible for preparation of this RIR is Kevin
Brussee.
3.2 Health and Safety
All work described in this RIR was performed in full compliance with applicable laws and
regulations, including Site and OSHA worker safety requirements and HAZWOPER
requirements.
3.3 Materials Management
All material encountered during the RI was managed in accordance with applicable laws and
regulations.
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4.0 REMEDIAL INVESTIGATION ACTIVITIES
EBC performed the following scope of work within Site E in April of 2014:
1. Conducted a Site inspection to identify AOCs and physical obstructions (i.e. structures,
buildings, etc.);
2. Installed six soil borings within Site E, and collected twelve soil samples for chemical
analysis from the soil borings to evaluate soil quality; and
3. Installed two groundwater monitoring wells within Site E and collected two groundwater
samples from the two monitoring wells, and collected one groundwater sample from an
existing geotechnical monitoring well to evaluate groundwater quality; and
4. Installed five soil vapor probes across the Site and collected five soil vapor samples for
chemical analysis.
4.1 Geophysical Investigation
A geophysical investigation was not performed as a part of this assessment.
4.2 Borings and Monitoring Wells
Drilling and Soil Logging
On April 2, 2014, and April 8, 2014, six soil borings (SB1, SB2 and SB4 through SB7) were
performed in the approximate locations shown on Figure 5. Refusal was repeatedly encountered
at very shallow depths at soil boring SB3, and was therefore not completed. The location of the
six completed soil borings were chosen to gain representative soil quality information across Site
E. For each of the six soil borings, soil samples were collected continuously from grade to
refusal using a five-foot steel macro-core sampler with acetate liners and Geoprobe direct-push
equipment. Soil recovered from each of the soil borings was field screened for the presence of
VOCs with a photo-ionization detector (PID) and visually inspected for evidence of
contamination. No PID readings above background concentrations were obtained from any of the
soil borings.
One soil sample was retained from each boring representing the interval 0 to 2 feet below grade
and one soil sample was retained from each of the soil borings from the 2ft interval immediately
above the refusal depth. Therefore, soil samples were retained from the interval 15 to 17 feet
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below grade for soil borings SB4, SB6, and SB7, the interval 14 to 16 feet below grade for soil
boring SB5, and 29 to 31 feet below grade for soil borings SB1 and SB2.
Soil boring details are provided in Table 1. Boring logs were prepared by a Qualified
Environmental Professional and are attached in Attachment A.
Groundwater Monitoring Well Construction
A temporary 1-inch diameter PVC monitoring well consisting of 10 feet of 0.010 slot screen was
installed at two locations (E-MW1 and E-MW3), set to intersect the water table. Monitoring well
E-MW1 was installed on the western end of the Site and required installation at a depth of
approximately 40 feet below grade due the higher elevation of the Site on the western end.
Monitoring well E-MW3 was installed on the eastern end of the Site at a depth of approximately
30 feet below grade due to the 13 ft difference elevation between the western and eastern ends of
the Site. Monitoring well E-MW2 was an existing 2-inch diameter monitoring well installed by
the geotechnical company at a depth of approximately 40 feet below grade. Monitoring well
sampling details are provided in Table 1. Monitoring well locations are shown in Figure 5.
Survey
Soil borings and wells were located to the nearest 0.10 foot with respect to two or more
permanent site features.
Water Level Measurement
Approximate groundwater level measurements were collected using a Solinst oil/water interface
meter to ensure the surface of the water table was within the screened section of the monitoring
well. No free product was observed within the three monitoring wells. Water level data is
included in Table 1.
4.3 Sample Collection and Chemical Analysis
Sampling performed as part of the field investigation was conducted for all Areas of Concern
and also considered other means for bias of sampling based on professional judgment, area
history, discolored soil, stressed vegetation, drainage patterns, field instrument measurements,
odor, or other field indicators. All media including soil and soil vapor have been sampled and
evaluated in the RIR. Discrete (grab) samples have been used for final delineation of the nature
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and extent of contamination and to determine the impact of contaminants on public health and
the environment. The sampling performed and presented in this RIR provides sufficient basis for
evaluation of remedial action alternatives, establishment of a qualitative human health exposure
assessment, and selection of a final remedy.
Soil Sampling
Twelve soil samples were collected for chemical analysis during this RI. Data on soil sample
collection for chemical analyses, including dates of collection and sample depths, is reported in
Tables 2, 3, 4 and 5. Figure 5 shows the location of samples collected during this RI, and the soil
boring locations of the 2009 AKRF Phase II. Laboratories and analytical methods for soil
samples collected during the 2014 EBC RI are shown below.
The twelve soil samples were collected in pre-cleaned, laboratory supplied glassware, stored in a
cooler with ice and submitted for analysis to Phoenix Environmental Laboratories (Phoenix) of
587 East Middle Turnpike, Manchester, CT 06040, a New York State ELAP certified
environmental laboratory (ELAP Certification No. 11301). All six soil samples retained from the
interval 0 to 2 feet below grade were analyzed for the presence of volatile organic compounds
(VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method
8270, pesticides/PCBs by EPA Methods 8081/8082 and target analyte list (TAL) metals. IEach
of the six soil samples retained from the deeper interval were analyzed for VOCs by EPA
Method 8260, SVOCs by EPA Method 8270, and TAL metals. Since pesticides and PCBs were
detected above UUSCOs within the 0-2ft soil sample retained from soil boring SB6, the deeper
soil sample from the same soil boring was also analyzed for pesticides/PCBs by EPA Methods
8081/8082.
Groundwater Sampling
Three groundwater samples were collected from Site E. Two of the groundwater samples (MW1
and MW3) were collected from one-inch diameter PVC monitoring wells installed 5-feet below
the water table interface by EBC. The third groundwater sample (MW2) was collected from a 2-
inch diameter monitoring well installed by the geotechnical company. The three groundwater
samples were collected utilizing dedicated polyethylene tubing and a stainless steel check valve.
Groundwater samples were collected in pre-cleaned, laboratory supplied glassware, stored in a
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cooler with ice and submitted to Phoenix for analysis of VOCs by EPA Method 8260, SVOCs by
EPA Method 8270, and both total and dissolved TAL metals. One of the groundwater samples
(MW3) was also analyzed for pesticides/PCBs by EPA Methods 8081/8082. Groundwater
sample collection data is reported in Tables 6 through 10. Sampling logs with information on
purging and sampling of groundwater monitoring wells is included in Attachment B. Figure 5
shows the location of each of the three monitoring wells sampled by EBC and the location in
which groundwater was sampled during the 2008 AKRF Phase II. Laboratories and analytical
methods for groundwater samples collected during the 2014 EBC RI are shown below.
Soil Vapor Sampling
Five soil vapor probes were installed within Site E and five soil vapor samples were collected for
chemical analysis during this RI. Soil vapor sampling locations are shown in Figure 5. Soil vapor
sample collection data is reported in Table 11. Soil vapor sampling logs are included in
Attachment C. Methodologies used for soil vapor assessment conform to the NYS DOH Final
Guidance on Soil Vapor Intrusion, October 2006.
The five soil vapor implants were installed using Geoprobe™ equipment and tooling. The vapor
implants that were installed were the Geoprobe™ Model AT86 series, which are constructed of a
6-inch length of double woven stainless steel wire. The implants were installed to at depths
ranging from 15 to 25 feet below grade. Each implant was attached to ¼ inch polyethylene
tubing which extended approximately 18 inches beyond that needed to reach the surface. The
tubing was capped with a ¼ inch plastic end to prevent the infiltration of foreign particles into
the tube. Coarse sand was placed around the vapor implant to a height of approximately 1 foot
above the bottom of the implant. The remainder of the borehole was sealed with a bentonite
slurry to the surface.
Soil vapor sampling for the five soil vapor implants installed on April 2 and April 8, 2014, was
conducted on April 9 and April 17, 2014. Prior to sampling, each sampling location was tested to
ensure a proper surface seal had been obtained. In accordance with NYSDOH guidance
(NYSDOH Guidance for Evaluating Soil Vapor Intrusion in the State of New York, February
2005), a tracer gas (helium) was used as a quality assurance/quality control device to verify the
integrity of the sampling point seal prior to collecting the samples. Prior to testing and collecting
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samples, the surface immediately surrounding the polyethylene tubing of the vapor implant was
sealed using a 1 foot ft by 1 ft square sheet of 2 mil HDPE plastic firmly adhered to a wetted
layer of granular bentonite. The seal was then tested by enriching the air space above the seal
with a tracer gas (helium) while continuously monitoring air drawn from the implant with a
helium detector (Dielectric Model MGD-2002, Multi-Gas Detector) for a minimum of 15
minutes. The tracer gas test procedure was employed at all five soil vapor sampling locations. No
surface seal leaks were observed at any of the locations.
Following verification that the surface seal was tight, one to three volumes (i.e., the volume of
the sample probe and tube) of air was purged from the implant using a calibrated vacuum pump.
After purging, a 6-liter Summa® canister, fitted with a 2-hour flow regulator, was attached to the
surface tube of each of the five soil vapor implants. Prior to initiating sample collection, sample
identification, canister number, date and start time were recorded on tags attached to each
canister and in a bound field note book. Sampling then proceeded by fully opening the flow
control valve on each canister in turn. Immediately after opening the flow control valve on a
canister, the initial vacuum (inches of mercury) was recorded in the field book and on the sample
tag. When the vacuum level in the canister was between 5 and 8 inches of mercury (approx 2
hours), the flow controller valve was closed, and the final vacuum recorded in the field notebook
and on the sample tag.
The soil gas sample identification, date, start time, start vacuum, end time and end vacuum were
recorded on tags attached to each canister and on a sample log sheet (Attachment C). Samples
were submitted to Phoenix for laboratory analysis of VOCs EPA Method TO-15.
Chemical Analysis
Chemical analytical work presented in this RIR has been performed in the following manner:
Factor Description
Quality Assurance Officer The chemical analytical quality assurance is directed by Phoenix
Environmental Laboratories
Chemical Analytical
Laboratory
Chemical analytical laboratory(s) used in the RI is NYS ELAP
certified and was Phoenix Environmental Laboratories
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Chemical Analytical
Methods
Soil and groundwater analytical methods:
TAL Metals by EPA Method 6010C (rev. 2007);
VOCs by EPA Method 8260C (rev. 2006);
SVOCs by EPA Method 8270D (rev. 2007);
Pesticides by EPA Method 8081B (rev. 2000);
PCBs by EPA Method 8082A (rev. 2000);
Soil vapor analytical methods:
VOCs by TO-15 VOC parameters.
Results of Chemical Analyses
Laboratory data for soil, groundwater, and soil vapor are summarized in Tables 2 through 11.
Laboratory data deliverables for all samples evaluated in this RIR are provided in digital form in
Attachment D.
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5.0 ENVIRONMENTAL EVALUATION
5.1 Geological and Hydrogeological Conditions
Stratigraphy
The stratigraphy of Site E, from the surface down, consists of a layer of historic fill material that
varies from 2 to approximately 15ft below grade, underlain by a brown silty sand.
5.2 Soil Chemistry
Data collected during the RI performed in 2014 when combined with the data collected during
the 2004 Nova Phase III, and 2008 AKRF Phase II is sufficient to delineate the vertical and
horizontal distribution of contaminants in soil/fill at the Site. A summary table of data for
chemical analyses performed on soil samples is included in Tables 2a, 2b, 3a, 3b, 4 and 5.
Laboratory results from the 2014 EBC RI, 2004 Nova Phase III, and 2008 AKRF Phase II were
compared to NYSDEC Part 375 Table 375-6.8(a) and (b) Soil Cleanup Objectives (SCOs) for
Unrestricted Use and Restricted Residential Use. A copy of each of the laboratory reports for the
2014 EBC RI soil samples is provided in Attachment D. Figure 6 shows the location and posts
the values for soil/fill from both the 2014 EBC RI and 2008 AKRF Phase II that exceeds
UUSCOs and RRSCOs.
Soil/fill samples collected during the 2014 EBC RI, 2004 Nova Phase III, and 2008 AKRF Phase
II showed no VOCs above Unrestricted Use SCOs with the exception of acetone (68 micrograms
per kilogram [µg/Kg]). Naphthalene (maximum [max] of 430 µg/Kg) was detected in multiple
soil samples below Unrestricted Use SCOs. Eight SVOCs including benz(a)anthracene (max of
23,000 μg/Kg), benzo(a)pyrene (max of 20,000 μg/Kg), benzo(b)fluoranthene (max of 20,000
μg/Kg), benzo(k)fluoranthene (max of 20,000 μg/Kg), chrysene (max of 19,000 μg/Kg),
dibenz(a,h)anthracene (max of 8,600 μg/Kg), indeno(1,2,3-cd)pyrene (max of 18,000) and
phenanthrene (max of 160,000 μg/Kg) were detected above Unrestricted Use and Restricted
Residential Use SCOs within soil samples retained from the historic fill layer. Several metals
including arsenic (137 mg/Kg), cadmium (8.19 mg/kg), copper (max of 185 mg/Kg), lead (max
of 446 mg/Kg), mercury (max of 0.55 mg/Kg), nickel (39.6 mg/Kg), and zinc (max of 1,480
mg/Kg) were detected above Unrestricted Use SCOs. Of these metals, arsenic, cadmium and lead
also exceeded Restricted Residential Use SCOs within soil samples collected from the historic
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fill layer. PCB-1254 (210 µg/Kg) was detected within one shallow soil sample at a concentration
above Unrestricted Use SCOs and within one shallow soil sample and PCB-1260 (maximum of
25 µg/Kg) was detected within two shallow soil samples at a concentration below Unrestricted
Use SCOs. The pesticides 4,4'-DDD (max of 15 µg/Kg) and 4,4'-DDT (max of 13 µg/Kg) were
detected within two shallow soil samples at a concentration above Unrestricted Use SCOs.
Neither the pesticides nor PCBs were detected within any of the deeper soil samples retained
from the same soil boring locations. Overall, the findings were consistent with observations for
historical fill sites in areas throughout NYC.
5.3 Groundwater Chemistry
Data collected during the RI performed in 2014 when combined with the data collected during
the 2008 AKRF Phase II is sufficient to delineate the distribution of contaminants in
groundwater at the Site. A summary table of data for chemical analyses performed on
groundwater samples collected during the 2014 EBC RI and 2008 AKRF Phase II is included in
Tables 6 through 10. Figure 7 shows the location and posts the values for groundwater that
exceed the New York State 6NYCRR Part 703.5 Class GA Groundwater Quality Standards
(GQS) for the 2014 EBC RI and 2008 AKRF Phase II. A copy of the laboratory report for the
2014 RI groundwater samples is provided in Attachment D.
Groundwater samples collected during the 2014 EBC RI and 2008 AKRF Phase II showed no
detectable concentrations of pesticides or PCBs. The chlorinated VOCs cis-1,2-dichlorothene
(maximum of 5.56 µg/L), tetrachloroethene (maximum of 5.7 µg/L), and trichloroethene
(maximum of 27 µg/L) were detected within the groundwater samples collected by AKRF in
2008 and EBC in 2014 above GQS. The following VOCs were detected in one or more of the
groundwater samples at concentrations below GQS: 1,1-dichloroethene (1.7 µg/L), acetone
(maximum of 2.7 µg/L), carbon disulfide (0.90 µg/L), chloroform (1.5 µg/L), and methylene
chloride (0.38 µg/L). SVOCs detected above GQS included benzo(a)anthracene (max of 0.49
µg/L), benzo(b)fluoranthene (max of 0.48 µg/L), benzo(k)fluoranthene (0.08 µg/L), bis(2-
ethylhexyl)phthalate (max of 42 µg/L), chrysene (max. of 0.49 µg/L), and indeno(1,2,3-
cd)pyrene (3.7 µg/L) in one or more of the three groundwater samples collected by EBC in 2014
and the groundwater sample collected by AKRF in 2008. Dissolved metals present in
groundwater at levels above GQS included iron, lead, magnesium, manganese, selenium and
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sodium. The presence of some of these metals in groundwater, specifically those that are
common salinity indicators, can be attributed to the proximity to the East River and the intrusion
of road salting.
5.4 Soil Vapor Chemistry
Data collected during the 2014 RI is sufficient to delineate the distribution of contaminants in
soil vapor at the Site. A summary table of data for chemical analyses performed on soil vapor
samples is included in Table 11. Soil vapor analytical results were compared to NYSDOH Final
Guidance on Soil Vapor Intrusion (October 2006) Matrix 1 and 2 guidance values. Figure 8
shows the location and posts the values for soil vapor samples with detected concentrations of
NYSDOH Matrix 1 and 2 compounds.
Soil vapor samples collected during the 2014 EBC RI indicated petroleum related VOCs and
chlorinated VOCs were present at low concentrations. Petroleum-related VOCs (BTEX) were
detected at a maximum concentration of 141.43 μg/m3. The highest reported concentration was
for acetone (maximum of 7693 μg/m3). Trichloroethylene (TCE) was detected in three of the five
soil vapor samples at a concentration ranging from 241 to 61.2 μg/m3. The New York State
Department of Health (NYSDOH) Final Guidance on Soil Vapor Intrusion (October 2006) notes
mitigation is the recommended action for a TCE concentrations above 250 μg/m3 in soil gas.
Tetrachloroethylene (PCE) was detected in all five soil vapor samples, and ranged in
concentration from 2.03 to 28.3 μg/m3. Carbon tetrachloride was detected within three of the five
soil vapor samples at a maximum concentration of 0.566 μg/m3, and 1,1,1-trichloethylene (TCA)
was detected in three of the five soil vapor samples at a maximum concentration of 3.54 μg/m3.
The PCE, carbon tetrachloride and TCA concentrations are below the monitoring level ranges
established within the NYSDOH Final Guidance on Soil Vapor Intrusion.
5.5 Prior Activity
Based on an evaluation of the data and information from the RIR, disposal of significant amounts
of hazardous waste is not suspected for Site E.
5.6 Impediments to Remedial Action
There are no known impediments to remedial action at this property.
Table 1Former Domino Sugar Facility
Site E317-329 Kent Avenue, Brooklyn, NY
Soil Boring / Well Information
SB1 4/8/2014 40 2 Geoprobe - -SB2 4/2/2014 31 2 Geoprobe - -SB4 4/2/2014 20 2 Geoprobe - -SB5 4/2/2014 10 2 Geoprobe - -SB6 4/8/2014 20 2 Geoprobe - -SB7 4/8/2014 20 2 Geoprobe - -
MW1 4/8/2014 40 1 PVC 10.00 34.89MW2 Existing 40 1 PVC 10.00 30.43MW3 5/7/2014 30 1 PVC 10.00 22.47
SAMPLE ID Total Depth (ft) Diameter (in)DTW (ft)
Screen Length (ft)
DateConstruction
Materials
TABLE 2aSite E
Former Domino Sugar SiteBrooklyn, New York
Soil Analytical ResultsVolatile Organic Compounds
1,1,1,2-Tetrachloroethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,1,1-Trichloroethane 680 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.82 U 0.78 U 0.83 U 0.87 U
1,1,2,2-Tetrachloroethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.2 U 1.1 U 1.2 U 1.2 U
1,1,2-Trichloroethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.97 U 0.93 U 0.98 U 1 U
1,1-Dichloroethane 270 26,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.73 U 0.7 U 0.73 U 0.77 U
1,1-Dichloroethene 330 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.88 U 0.85 U 0.89 U 0.94 U
1,1-Dichloropropene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,2,3-Trichlorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,2,3-Trichloropropane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,2,4-Trichlorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,2,4-Trimethylbenzene 3,600 52000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,2,4,5-Trimethylbenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,2-Dibromoethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,2-Dichlorobenzene 1,100 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,2-Dichloroethane 20 3,100 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.2 U 1.2 U 1.2 U 1.3 U
1,2-Dichloropropane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.1 U 1 U 1.1 U 1.2 U
1,3,5-Trimethylbenzene 8,400 52000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,3-Dichlorobenzene 2,400 4,900 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,3-Dichloropropane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,4-Dichlorobenzene 1,800 13,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
2,2-Dichloropropane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
2-Chlorotoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
2-Hexanone (Methyl Butyl Ketone) - - - - - - - - - - - - - - - - - - - - 2.9 U 2.8 U 3 U 3.1 U
4-Chlorotoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Acetone 50 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 2.6 U 2.5 U 2.6 U 2.8 U
Benzene 60 4,800 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.79 U 0.76 U 0.8 U 0.84 U
Bromobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Bromochloromethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Bromodichloromethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.73 U 0.7 U 0.73 U 0.77 U
Bromoform BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.9 U 1.9 U 2 U 2.1 U
Bromomethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.7 U 1.6 U 1.7 U 1.8 U
Carbon Disulfide - - - - - - - - - - - - - - - - - - - - 0.59 U 0.57 U 0.6 U 0.63 U
Carbon tetrachloride 760 2,400 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.79 U 0.76 U 0.8 U 0.84 U
Chlorobenzene 1,100 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.98 U 0.94 U 0.99 U 1 U
Chlorodibromomethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Chlorodifluoromethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Chloroethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.4 U 1.4 U 1.4 U 1.5 U
Chloroform 370 49,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.59 U 0.57 U 0.6 U 0.63 U
Chloromethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.1 U 1.1 U 1.1 U 1.2 U
cis-1,2-Dichloroethene 250 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1 U 0.99 U 1 U 1.1 U
cis-1,3-Dichloropropene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.69 U 0.67 U 0.7 U 0.74 U
Dibromochloromethane - - - - - - - - - - - - - - - - - - - - 1.2 U 1.1 U 1.2 U 1.3 U
Dibromochloropropane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Dibromomethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Dichlorodifluoromethane 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Ethylbenzene 1,000 41,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.79 U 0.76 U 0.8 U 0.84 U
Freon 113 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Hexachlorobutadiene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Isopropylbenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
m&p-Xylenes 260 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Methyl Ethyl Ketone (2-Butanone) 120 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 3.8 U 3.6 U 3.8 U 4 U
Methyl Isobutyl Ketone BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 15 U 3.3 U 8 U 16 U
Methylene chloride 50 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 15 U 3.3 U 8 U 16 U
Napthalene 12,000 100,000 BDL BDL BDL BDL BDL BDL BDL 18 BDL BDL BDL BDL BDL 34 BDL 65 74 BDL 21 BDL - - - -
n-Butylbenzene 12,000 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
n-Propylbenzene 3,900 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
o-Xylene 260 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
p-Diethylbenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
p-Ethyltoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
p-Isopropyltoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
sec-Butylbenzene 11,000 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Styrene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.4 U 1.4 U 1.5 U 1.5 U
tert-ButylMethylEther BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
tert-Butylbenzene 5,900 100000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Tetrachloroethene 1,300 19,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.83 U 0.79 U 0.84 U 0.88 U
Toluene 700 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.66 U 0.63 U 0.67 U 0.7 U
Total Xylenes - - - - - - - - - - - - - - - - - - - - 2.7 U 2.6 U 2.8 U 2.9 U
trans-1,2-Dichloroethene 190 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.1 U 1 U 1.1 U 1.1 U
trans-1,3-Dichloropropene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.2 U 1.1 U 1.2 U 1.3 U
Trichloroethene 470 21,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.1 U 1.1 U 1.1 U 1.2 U
Trichlorofluoromethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Vinyl Chloride 20 900 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.5 U 1.4 U 1.5 U 1.5 U
Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives
ND - Not-detected
BDL - Delow Detection Limit
Dash - Not Analyzed
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.
U - The compound was anlayzed for but not detected at or above the MDL.
Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value
Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value
µg/Kg
NOVA Phase III
µg/Kgµg/Kg µg/Kg µg/Kg µg/Kg µg/Kgµg/Kg µg/Kg
6/23/2004 6/23/2004 11/7/2008
(1-3')
11/7/2008
(27-29')
AKRF PhaseII
AKRF PhaseII
6/23/2004
(16-18')
AKRF PhaseII
AKRF PhaseII
11/7/20086/23/2004 6/23/2004 11/7/2008
(12-16')(8-12')
SB-13
(1-3')
NOVA Phase III
NOVA Phase III
B-5
(0-4') (4-8')
NOVA Phase III
NOVA Phase III
SB-12
µg/Kg
6/23/2004 6/23/2004
µg/Kg
6/23/2004
µg/Kg µg/Kgµg/Kg µg/Kg
6/23/2004 6/23/2004 6/23/2004
NOVA Phase III
NOVA Phase III
(4-8')
NOVA Phase III
NOVA Phase III
NOVA Phase III
(0-4')(16-20')
B-3
(12-16')
NOVA Phase III
(8-12')
B-4
NOVA Phase III
(8-12')(0-4')
B-1
6/23/2004
µg/Kg
6/23/2004 6/23/20046/23/2004 6/23/2004 6/23/2004
µg/Kg µg/Kg µg/Kg
COMPOUNDNYSDEC Part 375.6
Unrestricted Use Soil Cleanup Objectives
NYDEC Part 375.6 Restricted Residential
Soil Cleanup Objectives*
(4-8')(12-16')
µg/Kg
NOVA Phase III
NOVA Phase III
(8-12')(4-8')(0-4')
µg/Kg
(8-12') (12-16')(0-4')
NOVA Phase III
NOVA Phase III
NOVA Phase III
NOVA Phase III
NOVA Phase III
NOVA Phase III
B-2
(4-8')
Results
6/23/2004
µg/Kg µg/Kg µg/Kg
6/23/2004 6/23/2004
ResultsResultsResultsResultsResultsResults
Previous Investigations
ResultsResultsResults ResultsResultsResultsResultsResults ResultsResultsResultsResultsResultsResults ResultsResultsResults
TABLE 2bSite E
Former Domino Sugar SiteBrooklyn, New York
Soil Analytical ResultsVolatile Organic Compounds
Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL
1,1,1,2-Tetrachloroethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,1,1-Trichloroethane 680 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,1,2,2-Tetrachloroethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,1,2-Trichloroethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,1-Dichloroethane 270 26,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,1-Dichloroethene 330 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,1-Dichloropropene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,2,3-Trichlorobenzene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
1,2,3-Trichloropropane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
1,2,4-Trichlorobenzene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
1,2,4-Trimethylbenzene 3,600 52000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
1,2,4,5-Trimethylbenzene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
1,2-Dibromoethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,2-Dichlorobenzene 1,100 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
1,2-Dichloroethane 20 3,100 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,2-Dichloropropane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,3,5-Trimethylbenzene 8,400 52000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
1,3-Dichlorobenzene 2,400 4,900 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
1,3-Dichloropropane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
1,4-Dichlorobenzene 1,800 13,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
2,2-Dichloropropane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
2-Chlorotoluene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
2-Hexanone (Methyl Butyl Ketone) < 47 47 < 29 29 < 41 41 < 40 40 < 40 40 < 34 34 < 49 49 < 45 45 < 27 27 < 36 36 < 36 36 < 61 61
2-Isorpropyltoluene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
4-Chlorotoluene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
4-Methyl-2-pentanone < 47 47 < 29 29 < 41 41 < 40 40 < 40 40 < 34 34 < 49 49 < 45 45 < 27 27 < 36 36 < 36 36 < 61 61
Acetone 50 100,000 < 50 50 < 50 50 < 50 50 < 50 50 < 50 50 < 50 50 12 50 49 50 68 54 < 50 50 < 50 50 < 50 50
Acrylonitrile < 19 19 < 11 11 < 16 16 < 16 16 < 16 16 < 14 14 < 20 20 < 18 18 < 11 11 < 15 15 < 14 14 < 24 24
Benzene 60 4,800 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Bromobenzene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
Bromochloromethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Bromodichloromethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Bromoform < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Bromomethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Carbon Disulfide < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Carbon tetrachloride 760 2,400 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Chlorobenzene 1,100 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Chloroethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Chloroform 370 49,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Chloromethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
cis-1,2-Dichloroethene 250 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
cis-1,3-Dichloropropene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Dibromochloromethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Dibromomethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Dichlorodifluoromethane 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Ethylbenzene 1,000 41,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Hexachlorobutadiene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
Isopropylbenzene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
m&p-Xylenes 260 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Methyl Ethyl Ketone (2-Butanone) 120 100,000 < 56 56 < 34 34 < 49 49 < 49 49 < 48 48 < 41 41 < 59 59 < 54 54 < 32 32 < 44 44 < 43 43 < 73 73
Methyl Isobutyl Ketone < 19 19 < 11 11 < 16 16 < 16 16 < 16 16 < 14 14 < 20 20 < 18 18 < 11 11 < 15 15 < 14 14 < 24 24
Methylene chloride 50 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Napthalene 12,000 100,000 < 9.3 9.3 < 5.7 5.7 430 310 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
n-Butylbenzene 12,000 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
n-Propylbenzene 3,900 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
o-Xylene 260 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
p-Isopropyltoluene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
sec-Butylbenzene 11,000 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
Styrene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
tert-Butylbenzene 5,900 100000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12
Tetrachloroethene 1,300 19,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Tetrahydrofuran < 19 19 < 11 11 < 16 16 < 16 16 < 16 16 < 14 14 < 20 20 < 18 18 < 11 11 < 15 15 < 14 14 < 24 24
Toluene 700 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
trans-1,2-Dichloroethene 190 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
trans-1,3-Dichloropropene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
trans-1,4-dichloro-2-butene < 19 19 < 11 11 < 16 16 < 16 16 < 16 16 < 14 14 < 20 20 < 560 560 < 560 560 < 15 15 < 14 14 < 24 24
Trichloroethene 470 21,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Trichlorofluoromethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Trichlorotrifluoroethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Vinyl Chloride 20 900 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12
Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives
ND - Not-detected
BDL - Delow Detection Limit
Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value
Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value
EBC RI EBC RI EBC RI
µg/Kg
4/8/2014
µg/Kg µg/Kg
4/2/2014 4/8/2014
EBC RI EBC RI
4/2/2014
EBC RI
4/2/2014 4/8/20144/2/2014 4/2/2014
µg/Kg
4/8/2014
(0-2')
µg/Kg µg/Kg
4/8/2014
EBC RIEBC RIEBC RI
4/8/2014
µg/Kg
EBC RICOMPOUND
NYSDEC Part 375.6 Unrestricted Use Soil Cleanup Objectives
NYDEC Part 375.6 Restricted Residential
Soil Cleanup Objectives*
4/8/2014
EBC RI
µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg
EBC RI
SB7
(0-2')
2014 Remedial Investigation
SB5 SB6
(12-14') (0-2') (15-17') (15-17')
SB4
(0-2')(29-31')(0-2')
SB1 SB2
(29-31') (0-2') (15-17')
TABLE 3aSite E
Former Domino Sugar SiteBrooklyn, New York
Soil Analytical ResultsSemi-Volatile Organic Compounds
1,2,4-Trichorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 610 U 59 U 620 U 65 U
1,2-Dichlorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 600 U 58 U 610 U 64 U
1,2-Diphenylhydrazine BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
1,3-Dichlorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 500 U 48 U 510 U 53 U
1,4-Dichlorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 640 U 62 U 650 U 69 U
2,2'-Oxybis (1-chloropropane) - - - - - - - - - - - - - - - - - - - - 710 U 69 U 720 U 76 U
2,4,5-Trichlorophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 550 U 53 U 560 U 59 U
2,4,6-Trichlorophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 610 U 58 U 610 U 65 U
2,4-Dichlorophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 620 U 60 U 630 U 66 U
2,4-Dimethylphenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 490 U 47 U 490 U 52 U
2,4-Dinitrophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 4,100 U * 390 U * 4,100 U * 430 U *
2,4-Dinitrotoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 570 U 55 U 580 U 61 U
2,6-Dinitrotoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 500 U 48 U 500 U 53 U
2-Chloronaphthalene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 640 U 62 U 650 U 68 U
2-Chlorophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 670 U 65 U 680 U 72 U
2-Methylnaphthalene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 710 1,500 1,400 BDL BDL BDL BDL 690 U 66 U 1300 J 73 U
2-Methylphenol (o-cresol) 330 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 540 U 52 U 550 U 58 U
2-Nitroaniline BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 590 U 57 U 600 U 63 U
2-Nitrophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 520 U 51 U 530 U 56 U
3&4-Methylphenol (p-cresol) BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
3,3'-Dichlorobenzidine BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 620 U 60 U 630 U 66 U
3-Nitroaniline BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 570 U 55 U 570 U 60 U
4,6-Dinitro-2-methylphenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 270 U 26 U 270 U 29 U
4-Bromophenyl phenyl ether BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 550 U 53 U 560 U 59 U
4-Chloro-3-methylphenol - - - - - - - - - - - - - - - - - - - - 540 U 52 U 550 U 58 U
4-Chloroaniline BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 490 U 47 U 490 U 52 U
4-Chlorophenyl phenyl ether BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 630 U 61 U 640 U 68 U
4-Methylphenol - - - - - - - - - - - - - - - - - - - - 720 U 69 U 730 U 76 U
4-Nitroaniline BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 560 U 54 U 570 U 60 U
4-Nitrophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 670 U 65 U 680 U 72 U
Acenaphthene 20,000 100,000 BDL BDL BDL BDL BDL 330 BDL BDL BDL BDL BDL BDL BDL 2,500 2,900 2,400 BDL BDL BDL BDL 1,800 J 63 U 3,200 69 U
Acenaphthylene 100,000 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 740 J 66 U 700 U 73 U
Anthracene 100,000 100,000 BDL BDL BDL BDL BDL 1,200 BDL BDL BDL BDL 37 BDL BDL 8,300 8,300 13,000 800 BDL 690 BDL 5,700 64 U 7,200 71 U
Benz(a)anthracene 1,000 1,000 BDL BDL BDL BDL BDL 3,600 BDL 510 400 BDL 120 BDL BDL 21,000 16,000 23,000 3,200 490 540 BDL 17,000 54 U 12,000 59 U
Benzo(a)pyrene 1,000 1,000 BDL BDL BDL BDL BDL 3,000 BDL 1,400 430 BDL 140 BDL BDL 17,000 13,000 20,000 3,300 460 390 BDL 15,000 40 U 9,900 45 U
Benzo(b)fluoranthene 1,000 1,000 BDL BDL BDL BDL BDL 3,100 BDL 1,200 380 BDL 120 BDL BDL 16,000 13,000 20,000 3,100 420 360 BDL 18,000 51 U 11,000 57 U
Benzo(ghi)perylene 100,000 100,000 BDL BDL BDL BDL BDL 1,400 BDL 1,200 BDL BDL 86 BDL BDL 6,900 7,400 7,700 1,800 BDL 270 BDL 16,000 41 U 8,000 45 U
Benzo(k)fluoranthene 800 3,900 BDL BDL BDL BDL BDL 3,100 BDL 660 380 BDL 120 BDL BDL 16,000 13,000 20,000 3,100 420 360 BDL 6,200 46 U 3,700 51 U
Benzyl alcohol - - - - - - - - - - - - - - - - - - - - 520 U 50 U 530 U 56 U
Benzyl butyl phthalate BDL BDL BDL BDL BDL BDL BDL 1,200 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 610 U 100 J 620 U 65 U
Bis(2-chloroethoxy)methane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 620 U 60 U 630 U 66 U
Bis(2-chloroethyl)ether BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 850 U 82 U 860 U 90 U
Bis(2-chloroisopropyl)ether BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -
Bis(2-ethylhexyl)phthalate BDL BDL 200 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 57 590 U 200 J 600 U 200 J Carbazole BDL BDL BDL BDL BDL 370 BDL BDL BDL BDL BDL BDL BDL 2,200 3,100 3,500 320 BDL BDL BDL 2,700 J 58 U 3,400 64 U
Chrysene 1,000 3,900 BDL BDL BDL BDL BDL 3,200 BDL 1,400 420 BDL 110 BDL BDL 18,000 15,000 19,000 3,000 480 610 BDL 17,000 61 U 12,000 68 U
Dibenz(a,h)anthracene 330 330 BDL BDL BDL BDL BDL 480 BDL BDL BDL BDL BDL BDL BDL 2,600 1,900 2,500 520 BDL BDL BDL 4,500 36 U 4,100 40 U
Dibenzofuran 7,000 59000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 2,200 3,300 4,500 BDL BDL BDL BDL 1,300 J 63 U 2,800 J 70 U
Diethyl phthalate BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 700 U 67 U 710 U 74 U
Dimethylphthalate BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 630 U 61 U 640 U 68 U
Di-n-butylphthalate BDL BDL 45 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 700 U 68 U 710 U 75 U
Di-n-octylphthalate BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 530 U 51 U 540 U 56 U
Fluoranthene 100,000 100,000 BDL BDL BDL BDL BDL 7,700 550 2,500 520 540 210 BDL 400 53,000 27,000 41,000 6,000 740 1,800 BDL 37,000 64 U 29,000 71 U
Fluorene 30,000 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 3,300 4,200 6,100 BDL BDL BDL BDL 1,600 J 66 U 3,400 73 U
Hexachlorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 720 U 69 U 730 U 77 U
Hexachlorobutadiene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 640 U 61 U 650 U 68 U
Hexachlorocyclopentadiene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 930 U 90 U 940 U 99 U
Hexachloroethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 580 U 56 U 590 U 62 U
Indeno(1,2,3-cd)pyrene 500 500 BDL BDL BDL BDL BDL 1,300 BDL 730 BDL BDL BDL BDL BDL 6,900 7,900 7,700 1,500 300 270 BDL 18,000 40 U 8,900 44 U
Isophorone BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 690 U 66 U 700 U 73 U
Naphthalene 12,000 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,100 2,700 1,800 BDL BDL BDL BDL 820 J 63 U 3,100 70 U
Nitrobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 730 U 70 U 740 U 78 U
N-Nitrosodi-n-propylamine BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 740 U 72 U 750 U 80 U
N-Nitrosodiphenylamine BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 600 U 58 U 610 U 64 U
Pentachlorophenol 800 6,700 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 370 U 36 U 370 U 39 U
Phenanthrene 100,000 100,000 BDL BDL BDL BDL BDL 5,200 440 2,500 610 360 160 BDL BDL 53,000 37,000 35,000 3,100 330 3,100 BDL 29,000 63 U 30,000 70 U
Phenol 330 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 610 U 59 U 620 U 66 U
Pyrene 100,000 100,000 BDL BDL BDL BDL BDL 6,800 410 3,100 890 530 190 BDL 450 46,000 35,000 41,000 5,900 780 1,400 BDL 34,000 71 U 23,000 79 U
Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives
Dash- Not Analyzed
BDL - Delow Detection Limit
ND - Not-detected
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.
U - The compound was anlayzed for but not detected at or above the MDL.
Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value
Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value
Results Results
NOVA Phase III
NOVA Phase III
NOVA Phase III
NOVA Phase III
Results
NOVA Phase III
Results Results Results Results
6/23/2004
(4-8')COMPOUND NYSDEC Part 375.6
Unrestricted Use Soil Cleanup Objectives**
B-1 B-2
6/23/2004 6/23/2004
Results
NYDEC Part 375.6 Restricted
Residential Soil Cleanup
Objectives**
NOVA Phase III
NOVA Phase III
NOVA Phase III
NOVA Phase III
NOVA Phase III
NOVA Phase III
(1-3')
NOVA Phase III
NOVA Phase III
(0-4')(4-8') (8-12') (12-16')
B-5 SB-12
(16-18')
AKRF PhaseII
(8-12')
SB-13
(0-4') (4-8') (8-12') (12-16') (16-20') (0-4') (4-8') (12-16') (27-29')
B-3 B-4
(8-12') (12-16') (0-4') (1-3')(8-12') (0-4') (4-8')
AKRF PhaseII
6/23/2004 6/23/2004 6/23/2004 6/23/2004 6/23/2004 6/23/2004 6/23/2004
NOVA Phase III
NOVA Phase III
6/23/2004 6/23/2004 6/23/2004 6/23/2004
AKRF PhaseII
NOVA Phase III
AKRF PhaseII
NOVA Phase III
NOVA Phase III
6/23/2004 6/23/2004 6/23/2004 11/7/20086/23/2004 6/23/2004
NOVA Phase III
NOVA Phase III
11/7/2008
µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kgµg/Kg
6/23/2004
µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kgµg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg
Results Results Results ResultsResults Results Results Results Results
µg/Kg µg/Kg
11/7/2008
Previous Investigations
µg/Kg
ResultsResults Results Results Results
11/7/2008
Results Results
TABLE 3bSite E
Former Domino Sugar SiteBrooklyn, New York
Soil Analytical ResultsSemi-Volatile Organic Compounds
Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL
1,2,4,5-Tetrachlorobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
1,2,4-Trichorobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
1,2-Dichlorobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
1,2-Diphenylhydrazine < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
1,3-Dichlorobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
1,4-Dichlorobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
2,4,5-Trichlorophenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
2,4,6-Trichlorophenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
2,4-Dichlorophenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
2,4-Dimethylphenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
2,4-Dinitrophenol < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900
2,4-Dinitrotoluene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
2,6-Dinitrotoluene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
2-Chloronaphthalene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
2-Chlorophenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
2-Methylnaphthalene < 250 250 < 240 240 550 540 < 240 240 < 270 270 < 250 250 < 500 500 180 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
2-Methylphenol (o-cresol) 330 100,000 < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 330 330 < 260 260
2-Nitroaniline < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900
2-Nitrophenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
3&4-Methylphenol (p-cresol) < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
3,3'-Dichlorobenzidine < 710 710 < 680 680 < 1600 1,600 < 670 670 < 760 760 < 720 720 < 1400 1,400 < 830 830 < 3600 3,600 < 700 700 < 1400 1,400 < 750 750
3-Nitroaniline < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900
4,6-Dinitro-2-methylphenol < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900
4-Bromophenyl phenyl ether < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
4-Chloro-3-methylphenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
4-Chloroaniline < 710 710 < 680 680 < 1600 1,600 < 670 670 < 760 760 < 720 720 < 1400 1,400 < 830 830 < 3600 3,600 < 700 700 < 1400 1,400 < 750 750
4-Chlorophenyl phenyl ether < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
4-Nitroaniline < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900
4-Nitrophenol < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900
Acenaphthene 20,000 100,000 < 250 250 < 240 240 1,100 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Acenaphthylene 100,000 100,000 < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 820 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Acetophenone < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Aniline < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900
Anthracene 100,000 100,000 < 250 250 < 240 240 2,800 540 < 240 240 < 270 270 < 250 250 240 500 1,200 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Benz(a)anthracene 1,000 1,000 160 250 < 240 240 4,800 540 < 240 240 220 270 < 250 250 1,400 500 9,300 290 1,800 1,300 < 250 250 950 500 < 260 260
Benzidine < 710 710 < 680 680 < 1600 1,600 < 670 670 < 760 760 < 720 720 < 1400 1,400 < 830 830 < 3600 3,600 < 700 700 < 1400 1,400 < 750 750
Benzo(a)pyrene 1,000 1,000 140 250 < 240 240 3,700 540 < 240 240 180 270 < 250 250 1,200 500 8,300 290 1,800 1,300 < 250 250 790 500 < 260 260
Benzo(b)fluoranthene 1,000 1,000 190 250 < 240 240 5,000 540 < 240 240 260 270 < 250 250 1,800 500 11,000 290 2,300 1,300 < 250 250 1,000 500 < 260 260
Benzo(ghi)perylene 100,000 100,000 < 250 250 < 240 240 1,500 540 < 240 240 < 270 270 < 250 250 380 500 3,200 290 640 1,300 < 250 250 510 500 < 260 260
Benzo(k)fluoranthene 800 3,900 < 250 250 < 240 240 1,500 540 < 240 240 < 270 270 < 250 250 480 500 3,700 290 990 1,300 < 250 250 440 500 < 260 260
Benzoic Acid < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900
Benzyl butyl phthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Bis(2-chloroethoxy)methane < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Bis(2-chloroethyl)ether < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Bis(2-chloroisopropyl)ether < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Bis(2-ethylhexyl)phthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Carbazole < 1800 1,800 < 1700 1,700 1,000 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 690 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900
Chrysene 1,000 3,900 160 250 < 240 240 4,200 540 < 240 240 240 270 < 250 250 1,300 500 8,600 290 1,800 1,300 < 250 250 920 500 < 260 260
Dibenz(a,h)anthracene 330 330 < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 330 330 < 260 260
Dibenzofuran 7,000 59000 < 250 250 < 240 240 1,200 540 < 240 240 < 270 270 < 250 250 < 500 500 200 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Diethyl phthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Dimethylphthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Di-n-butylphthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Di-n-octylphthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Fluoranthene 100,000 100,000 240 250 < 240 240 9,900 540 < 240 240 340 270 < 250 250 2,100 500 18,000 290 2,400 1,300 < 250 250 1,900 500 < 260 260
Fluorene 30,000 100,000 < 250 250 < 240 240 1,400 540 < 240 240 < 270 270 < 250 250 < 500 500 230 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Hexachlorobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Hexachlorobutadiene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Hexachlorocyclopentadiene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Hexachloroethane < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Indeno(1,2,3-cd)pyrene 500 500 < 250 250 < 240 240 1,400 540 < 240 240 < 270 270 < 250 250 370 500 3,400 290 < 1300 1,300 < 250 250 460 500 < 260 260
Isophorone < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Naphthalene 12,000 100,000 < 250 250 < 240 240 870 540 < 240 240 < 270 270 < 250 250 < 500 500 590 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Nitrobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
N-Nitrosodimethylamine < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
N-Nitrosodi-n-propylamine < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
N-Nitrosodiphenylamine < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Pentachloronitrobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Pentachlorophenol 800 6,700 < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Phenanthrene 100,000 100,000 160 250 < 240 240 12,000 540 < 240 240 260 270 < 250 250 1,200 500 5,800 290 1,200 1,300 < 250 250 830 500 < 260 260
Phenol 330 100,000 < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 330 330 < 260 260
Pyrene 100,000 100,000 240 250 < 240 240 7,700 540 < 240 240 320 270 < 250 250 1,900 500 16,000 290 2,700 1,300 < 250 250 1,600 500 < 260 260
Pyridine < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260
Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives
Dash- Not Analyzed
BDL - Delow Detection Limit
ND - Not-detected
Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value
Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value
µg/Kg µg/Kg
4/2/2014 4/2/2014 4/8/2014 4/8/2014 4/8/2014
µg/Kg µg/Kg µg/Kg
(0-2') (15-17') (0-2') (15-17')
4/8/2014 4/8/2014
EBC RI EBC RI EBC RI EBC RI
4/2/2014
EBC RI EBC RI EBC RI EBC RI EBC RI
4/2/2014 4/8/2014 4/2/2014
µg/Kgµg/Kg µg/Kg µg/Kg µg/Kg
NYDEC Part 375.6 Restricted
Residential Soil Cleanup Objectives*
COMPOUND NYSDEC Part 375.6 Unrestricted Use SoilCleanup Objectives*
SB1
(0-2') (29-31')
EBC RI EBC RI
4/8/2014
µg/Kg µg/Kg
2014 Remedial InvestigationSB2 SB4 SB5 SB6 SB7
(12-14')
EBC RI
(0-2')(0-2') (29-31') (0-2') (15-17')
TABLE 4Site E
Former Domino Sugar Site Brooklyn, New York
Soil Analytical ResultsPesticides / PCBs
Results RL Results RL Results RL Results RL Results RL Results RL Results RL
PCB-1016 100 1,000 5.1 U 4.9 U 5.2 U 5.5 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36
PCB-1221 100 1,000 1.2 U 1.2 U 1.2 U 1.3 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36
PCB-1232 100 1,000 5.1 U 4.9 U 5.2 U 5.5 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36
PCB-1242 100 1,000 5.1 U 4.9 U 5.2 U 5.5 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36
PCB-1248 100 1,000 5.1 U 4.9 U 5.2 U 5.5 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36
PCB-1254 100 1,000 1.7 U 1.6 U 1.7 U 1.8 U < 35 35 < 38 38 < 38 38 < 36 36 210 36 < 35 35 < 36 36
PCB-1260 100 1,000 25 3.7 U 7.7 J 4.1 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36
PCB-1262 100 1,000 - - - - < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36
PCB-1268 100 1,000 - - - - < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36
4,4-DDD 3.3 13,000 7.3 0.64 15 0.7 < 2.6 2.6 < 2.8 2.8 < 2.7 2.7 < 2.6 2.6 < 2.6 2.6 < 2.5 2.5 < 2.6 2.6
4,4-DDE 3.3 8,900 0.75 U 0.72 0.76 0.79 < 2.6 2.6 < 2.8 2.8 < 2.7 2.7 < 2.6 2.6 < 2.6 2.6 < 2.5 2.5 < 2.6 2.6
4,4-DDT 3.3 7,900 13 0.87 9.3 0.96 U < 2.6 2.6 < 2.8 2.8 < 2.7 2.7 < 2.6 2.6 24 2.6 < 2.5 2.5 < 2.6 2.6
a-BHC 20 480 0.27 U 0.26 0.28 0.29 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
a-Chlordane 0.31 U 0.29 0.31 0.33 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6
Aldrin 5 97 0.20 U 0.19 0.2 0.21 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
b-BHC 36 360 0.42 U 0.4 0.61 0.44 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
Chlordane - - - - < 21 21 < 23 23 < 23 23 < 22 22 < 22 22 < 21 21 < 22 22
d-BHC 40 100,000 0.41 U 0.39 0.41 0.43 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
Dieldrin 5 200 0.64 U 0.61 0.64 U 0.68 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
Endosulfan I 2,400 24,000 0.33 U 0.31 0.33 U 0.35 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6
Endosulfan II 2,400 24,000 0.69 U 0.67 2.9 J 0.74 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6
Endosulfan Sulfate 2,400 24,000 0.66 U 0.64 0.67 U 0.70 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6
Endrin 14 11,000 0.69 U 0.66 5.1 0.73 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
Endrin aldehyde 10 0.44 14 0.48 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6
Endrin ketone 0.68 U 0.65 0.68 U 0.72 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
gamma-BHC 100 280 0.32 U 0.31 0.32 U 0.34 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
g-Chlordane 0.70 J 0.57 2 0.63 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6
Heptachlor 42 2,100 0.36 U 0.34 U 0.36 U 0.38 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
Heptachlor epoxide 0.34 U 0.32 U 0.34 U 0.36 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8
Methoxychlor 4.1 U 3.9 U 14 J 4.3 U < 7.1 7.1 < 92 92 < 7.6 7.6 < 22 22 < 7.3 7.3 < 7.0 7 < 18 18
Toxaphene 13 U 12 U 13 U 13 U < 180 180 < 190 190 < 190 190 < 180 180 < 180 180 < 180 180 < 180 180
Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives
ND - Not-detected
Dash - Not analyzed
N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.
Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value
Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value
(1-3')(16-18')
AKRF Phase IIAKRF Phase II
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
AKRF Phase II AKRF Phase IICOMPOUNDNYSDEC Part 375.6
Unrestricted Use Soil Cleanup Objectives
NYDEC Part 375.6 Restricted Residential
Soil Cleanup Objectives*
(1-3')
Results
(27-29')
ResultsResultsResults
µg/Kg
11/7/2008
µg/Kg µg/Kgµg/Kg
11/7/2008 11/7/2008 11/7/2008
Previous Investigations 2014 Remedial Investigation
SB1 SB2 SB4 SB5 SB6 SB7SB-12 SB-13
EBC RI EBC RI
(0-2') (15-17')
EBC RI EBC RI
(0-2') (0-2')
µg/Kgµg/Kg µg/Kg
(0-2')(0-2') (0-2')
4/8/2014
EBC RIEBC RI EBC RI
µg/Kg µg/Kg
4/8/2014 4/8/20144/2/2014 4/2/2014
µg/Kg µg/Kg
4/8/2014 4/2/2014
TABLE 5Site E
Former Domino Sugar SiteBrooklyn, New York
Soil Analytical ResultsMetals
Aluminum - - - - - - - - 2,880 2,720 5,590 2,860Antimony - - - - - - - - 1.3 U 1.2 U 1.3 U 1.7 U
Arsenic 13 16 BDL 1.9 1.4 0.82 BDL BDL BDL BDL 5 J 1.8 J 10.2 0.87 U
Barium 350 400 49 74 36 47 87 110 26 45 53.7 25.3 95.6 18.7Beryllium 7.2 72 - - - - - - - - 0.24 J 0.22 U 0.39 J 0.31 U
Cadmium 2.5 c 4.3 1.2 0.8 BDL 0.77 1.1 1.7 BDL BDL 1.7 J 0.51 U 1.8 J 0.73 U
Calcium - - - - - - - - 122,000 874 59,100 6,400Chromium 30 c 180 - trivalent 10 20 11 14 6.8 9.4 8.8 11 6.3 6.1 12.6 6.3Cobalt - - - - - - - - 4 3.4 5.4 3.3Copper 50 270 - - - - - - - - 71.7 9.5 79.7 7.9Iron - - - - - - - - 9,740 7,090 25,000 6,990Lead 63 c 400 140 11 5.3 40 91 84 7.1 7.3 192 4.1 J 446 2.8 JMagnesium - - - - - - - - 81,200 1,390 3,900 3,280Manganese 1600 c 2,000 - - - - - - - - 215 283 242 211Mercury 0.18 c 0.81 0.12 0.022 0.032 0.076 0.11 0.052 0.0073 0.011 0.22 0.015 U 0.27 0.017 U
Nickel 30 310 - - - - - - - 19.1 11.1 13.2 6.4 JPotassium - - - - - - - 676 386 768 497Selenium 3.9c 180 BDL BDL BDL BDL BDL BDL BDL BDL 1 U 0.88 U 0.95 U 1.3 U
Silver 2 180 BDL BDL BDL BDL BDL BDL BDL BDL 0.31 U 0.27 U 0.3 U 0.39 U
Sodium - - - - - - - - 377 77.5 J 980 125 JThallium - - - - - - - - 3.4 U 3 U 3.3 U 4.3 U
Vanadium - - - - - - - - 31.5 8.9 23.2 8Zinc 109 c 10,000 - - - - - - - - 96.9 46.9 695 14.3 J
Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL
Aluminum 6,940 37 3,240 36 7,520 39 3,250 34 6,520 35 4,440 36 6,340 35 6,000 42 5,240 34 6,770 32 10,500 39 8,370 38
Antimony < 1.9 1.9 < 1.8 1.8 < 1.9 1.9 < 1.7 1.7 < 1.7 1.7 < 1.8 1.8 < 1.7 1.7 < 2.1 2.1 < 3.0 3 < 1.6 1.6 < 1.9 1.9 < 1.9 1.9
Arsenic 13 16 2.7 0.7 0.7 0.7 5.7 0.8 1.5 0.7 7.1 0.7 1.5 0.7 7.2 0.7 137 0.8 4.8 0.7 1.4 0.6 12.2 0.8 1.1 0.8
Barium 350 400 97.5 0.7 20.3 0.7 84.4 0.8 22.1 0.7 56 0.7 38.8 0.7 80.8 0.7 126 0.8 82.3 0.7 45.4 0.6 75.4 0.8 61.5 0.8
Beryllium 7.2 72 0.3 0.3 < 0.29 0.29 0.35 0.31 < 0.27 0.27 0.28 0.28 0.31 0.29 0.32 0.28 0.74 0.33 < 0.27 0.27 0.35 0.26 0.38 0.31 0.54 0.31
Cadmium 2.5 c 4.3 < 0.37 0.37 < 0.36 0.36 < 0.39 0.39 < 0.34 0.34 < 0.35 0.35 < 0.36 0.36 < 0.35 0.35 8.19 0.42 0.44 0.34 < 0.32 0.32 < 0.39 0.39 < 0.38 0.38
Calcium 18,100 37 2,030 3.6 36,500 39 11,100 34 44,300 35 15,200 36 37,400 35 21,400 42 50,400 34 2,730 3.2 62,000 39 2,050 3.8
Chromium 30 c 180 - trivalent 16.4 0.37 6.68 0.36 13.3 0.39 7.08 0.34 10.7 0.35 8.23 0.36 12.6 0.35 18.9 0.42 13.1 0.34 27.4 0.32 10.6 0.39 18.1 0.38
Cobalt 5.3 0.37 2.67 0.36 4.01 0.39 2.75 0.34 2.51 0.35 2.97 0.36 4.14 0.35 18.1 0.42 3.71 0.34 5.18 0.32 3.03 0.39 7.71 0.38
Copper 50 270 32 0.37 8.42 0.36 153 3.9 7.68 0.34 34.8 0.35 12.6 0.36 57 0.35 185 4.2 42.3 0.34 18.9 0.32 25.8 0.39 18.5 0.38
Iron 18,500 37 8,230 3.6 14,000 39 8,800 34 12,200 35 8,940 3.6 16,200 35 78,600 42 14,800 34 15,300 32 15,100 39 23,900 38
Lead 63 c 400 98.7 0.7 2.3 0.7 167 7.7 12.1 0.7 108 0.7 39 0.7 166 7 308 8.3 156 6.7 6.6 0.6 174 7.7 6.4 0.8
Magnesium 9,810 37 1,960 3.6 3,460 3.9 3,390 3.4 4,740 3.5 2,150 3.6 11,200 35 2,600 4.2 12,000 34 2,950 32 6,150 39 3,410 38
Manganese 1600 c 2,000 330 3.7 185 3.6 173 3.9 176 3.4 227 3.5 254 3.6 255 3.5 435 4.2 209 3.4 357 3.2 328 3.9 480 3.8
Mercury 0.18 c 0.81 0.55 0.06 < 0.08 0.08 0.14 0.09 < 0.06 0.06 0.09 0.07 < 0.08 0.08 0.28 0.06 0.23 0.1 0.34 0.06 < 0.06 0.06 0.14 0.07 < 0.09 0.09
Nickel 30 310 13.5 0.37 6.9 0.36 15.2 0.39 7.56 0.34 10.2 0.35 8.6 0.36 15.1 0.35 39.6 0.42 14 0.34 12.3 0.32 8.69 0.39 18.1 0.38
Potassium 2,070 7 756 7 1,140 8 767 7 905 7 997 7 938 7 1,330 8 966 7 1,480 6 1,230 8 2,490 8
Selenium 3.9c 180 < 1.5 1.5 < 1.4 1.4 < 1.5 1.5 < 1.4 1.4 < 1.4 1.4 < 1.5 1.5 < 1.4 1.4 < 1.7 1.7 < 1.3 1.3 < 1.3 1.3 < 1.5 1.5 < 1.5 1.5
Silver 2 180 < 0.37 0.37 < 0.36 0.36 < 0.39 0.39 < 0.34 0.34 < 0.35 0.35 < 0.36 0.36 < 0.35 0.35 < 0.42 0.42 < 0.34 0.34 < 0.32 0.32 < 0.39 0.39 < 0.38 0.38
Sodium 282 7 95 7 543 8 137 7 672 7 128 7 338 7 326 8 251 7 194 6 1,280 8 180 8
Thallium < 1.5 1.5 < 1.4 1.4 < 1.5 1.5 < 1.4 1.4 < 1.4 1.4 < 1.5 1.5 < 1.4 1.4 < 1.7 1.7 < 1.3 1.3 < 1.3 1.3 < 1.5 1.5 < 1.5 1.5
Vanadium 29.7 0.4 13.8 0.4 28.3 0.4 15.6 0.3 25.3 0.3 15.5 0.4 25.8 0.3 59 0.4 28.7 0.3 30.3 0.3 23.2 0.4 29.4 0.4
Zinc 109 c 10,000 77.7 0.7 14 0.7 87.1 0.8 13.5 0.7 116 0.7 22.2 0.7 121 0.7 1,480 8.3 130 0.7 25 0.6 104 0.8 32.2 0.8
Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives
ND - Not-detected
Dash - Not analyzed
BDL - Below Detection Limit
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
N - The concentration is based on the response for the nearest internal. This flag is used on the TIC form for all compounds identified.
U - The compound was anlayzed for but not detected at or above the MDL.
Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value
Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value
6/23/2004 6/23/2004 6/23/2004 6/23/2004
SB-12
NOVA Phase III
B-5
(0-4') (4-8') (8-12') (12-16')
NOVA Phase III
(1-3') (16-18')
ResultsResultsResultsResults
SB-13
6/23/2004 6/23/2004
mg/Kg
11/7/2008 11/7/2008
mg/Kg mg/Kg
(1-3')
mg/Kg
(27-29')
11/7/2008
AKRF Phase II
11/7/2008
AKRF Phase II
ResultsResults
6/23/2004
mg/Kg mg/Kg
6/23/2004
mg/Kg mg/Kg
AKRF Phase II
COMPOUND
NYSDEC Part 375.6 Unrestricted Use
Soil Cleanup Objectives
NYDEC Part 375.6 Restricted
Residential Soil Cleanup
Objectives*
EBC RI(0-2')
mg/Kg
EBC RI EBC RI EBC RI EBC RI EBC RI
COMPOUND
NYSDEC Part 375.6 Unrestricted Use
Soil Cleanup Objectives
NYDEC Part 375.6 Restricted
Residential Soil Cleanup
Objectives*
mg/Kg
B-3
(0-4') (4-8') (8-12') (12-16')
NOVA Phase III
mg/Kg
NOVA Phase III
mg/Kg mg/Kg
NOVA Phase III NOVA Phase IIINOVA Phase III NOVA Phase III
Previous Investigations
2014 Remedial InvestigationSB1 SB2 SB4 SB5 SB6 SB7
Results
AKRF Phase II
(12-14') (0-2')(29-31') (0-2') (29-31') (0-2') (15-17')
ResultsResultsResults ResultsResults
(15-17') (0-2')(15-17') (0-2')
4/2/2014 4/2/2014 4/2/2014 4/2/20144/8/2014 4/8/2014 4/2/2014 4/8/2014
mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kgmg/Kg mg/Kgmg/Kg
EBC RI EBC RI
mg/Kg mg/Kg
4/8/2014 4/8/2014 4/8/20144/8/2014
EBC RI EBC RI EBC RI EBC RI
TABLE 6Site E
Former Domino Sugar SiteBrooklyn, New York
Groundwater Analytical ResultsVolatile Organic Compounds
SB-13
AKRF Phase II
11/7/2008
µg/L
Results
1,1,1,2-Tetrachlorothane 5 - < 1.0 1 < 1.0 1 < 1.0 1
1,1,1-Trichloroethane 5 0.69 U < 5.0 5 < 5.0 5 < 5.0 5
1,1,2,2-Tetrachloroethane 5 0.81 U < 1.0 1 < 1.0 1 < 1.0 1
1,1,2-Trichloroethane 1 0.65 U < 1.0 1 < 1.0 1 < 1.0 1
1,1-Dichloroethane 5 1.0 U < 5.0 5 < 5.0 5 < 5.0 5
1,1-Dichloroethene 5 1.7 J < 1.0 1 < 1.0 1 < 1.0 1
1,1-Dichloropropene - < 1.0 1 < 1.0 1 < 1.0 1
1,2,3-Trichlorobenzene - < 1.0 1 < 1.0 1 < 1.0 1
1,2,3-Trichloropropane 0.04 - < 1.0 1 < 1.0 1 < 1.0 1
1,2,4-Trichlorobenzene - < 1.0 1 < 1.0 1 < 1.0 1
1,2,4-Trimethylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1
1,2-Dibromo-3-chloropropane 0.04 - < 1.0 1 < 1.0 1 < 1.0 1
1,2-Dibromoethane - < 1.0 1 < 1.0 1 < 1.0 1
1,2-Dichlorobenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1
1,2-Dichloroethane 0.6 0.72 U < 2.0 2 < 2.0 2 < 2.0 2
1,2-Dichloropropane 0.94 0.71 U < 1.0 1 < 1.0 1 < 1.0 1
1,3,5-Trimethylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1
1,3-Dichlorobenzene 5 - < 5.0 5 < 5.0 5 < 5.0 5
1,3-Dichloropropane 5 - < 1.0 1 < 1.0 1 < 1.0 1
1,4-Dichlorobenzene 5 - < 5.0 5 < 5.0 5 < 5.0 5
2,2-Dichloropropane 5 - < 1.0 1 < 1.0 1 < 1.0 1
2-Chlorotoluene 5 - < 1.0 1 < 1.0 1 < 1.0 1
2-Hexanone (Methyl Butyl Ketone) 1.1 U < 1.0 1 < 1.0 1 < 1.0 1
2-Isopropyltoluene 5 - < 1.0 1 < 1.0 1 < 1.0 1
4-Chlorotoluene 5 - < 1.0 1 < 1.0 1 < 1.0 1
4-Methyl-2-Pentanone 0.38 U < 1.0 1 < 1.0 1 < 1.0 1
Acetone 2.4 J < 5.0 5 < 5.0 5 2.7 5
Acrolein - < 5.0 5 < 5.0 5 < 5.0 5
Acrylonitrile 5 - < 5.0 5 < 5.0 5 < 5.0 5
Benzene 1 0.74 U < 0.70 1 < 0.70 1 < 0.70 1
Bromobenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1
Bromochloromethane 5 - < 1.0 1 < 1.0 1 < 1.0 1
Bromodichloromethane 0.48 U < 1.0 1 < 1.0 1 < 1.0 1
Bromoform 0.46 U < 5.0 5 < 5.0 5 < 5.0 5
Bromomethane 5 2.1 U < 5.0 5 < 5.0 5 < 5.0 5
Carbon Disulfide 60 0.90 J < 1.0 1 < 1.0 1 < 1.0 1
Carbon tetrachloride 5 1.1 U < 1.0 1 < 1.0 1 < 1.0 1
Chlorobenzene 5 0.72 U < 5.0 5 < 5.0 5 < 5.0 5
Chloroethane 5 1.1 U < 5.0 5 < 5.0 5 < 5.0 5
Chloroform 7 1.5 J < 5.0 5 < 5.0 5 < 5.0 5
Chloromethane 60 1.1 U < 5.0 5 < 5.0 5 < 5.0 5
cis-1,2-Dichloroethene 5 5.5 4.7 1 3.6 1 < 1.0 1
cis-1,3-Dichloropropene 0.28 U < 0.40 0 < 0.40 0 < 0.40 0
Dibromochloromethane 0.55 U < 1.0 1 < 1.0 1 < 1.0 1
Dibromomethane 5 - < 1.0 1 < 1.0 1 < 1.0 1
Dichlorodifluoromethane 5 - < 1.0 1 < 1.0 1 < 1.0 1
Ethylbenzene 5 0.87 U < 1.0 1 < 1.0 1 < 1.0 1
Hexachlorobutadiene 0.5 - < 1.0 1 < 1.0 1 < 1.0 1
Isopropylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1
m&p-Xylenes 5 - < 1.0 1 < 1.0 1 < 1.0 1
Methyl Ethyl Ketone (2-Butanone) 50 1.1 U < 1.0 1 < 1.0 1 < 1.0 1
Methyl t-butyl ether (MTBE) 10 - < 1.0 1 < 1.0 1 < 1.0 1
Methylene chloride 5 0.78 U < 3.0 3 < 3.0 3 0.38 3
Naphthalene 10 - < 1.0 1 < 1.0 1 < 1.0 1
n-Butylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1
n-Propylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1
o-Xylene 5 - < 1.0 1 < 1.0 1 < 1.0 1
p-Isopropyltoluene - < 1.0 1 < 1.0 1 < 1.0 1
sec-Butylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1
Styrene 5 0.64 U < 1.0 1 < 1.0 1 < 1.0 1
tert-Butylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1
Tetrachloroethene 5 5.7 4.7 1 3.6 1 < 1.0 1
Tetrahydrofuran (THF) - < 5.0 5 < 5.0 5 < 5.0 5
Toluene 5 0.72 U < 1.0 1 < 1.0 1 < 1.0 1
Total Xylenes 2.3 U - - -
trans-1,2-Dichloroethene 5 0.76 U < 5.0 5 < 5.0 5 < 5.0 5
trans-1,3-Dichloropropene 0.4 0.57 U < 0.40 0 < 0.40 0 < 0.40 0
trans-1,4-dichloro-2-butene 5 - < 1.0 1 < 1.0 1 < 1.0 1
Trichloroethene 5 27 24 1 20 1 0.32 1
Trichlorofluoromethane 5 - < 1.0 1 < 1.0 1 < 1.0 1
Trichlorotrifluoroethane - < 1.0 1 < 1.0 1 < 1.0 1
Vinyl Chloride 2 0.99 U < 1.0 1 < 1.0 1 < 1.0 1
Notes:Dash - Not Analyzed
U - The compound was anlayzed for but not detected at or above the MDL.
N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.
Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
5/8/2014
µg/L µg/L µg/L
Results Results Results
4/9/2014 4/9/2014
COMPOUNDNYSDEC Groundwater
Quality Standards
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
E-MW1 E-MW2 E-MW3
EBC RI EBC RI EBC RI
TABLE 7Site E
Former Domino Sugar SiteBrooklyn, New York
Groundwater Analytical ResultsSemi-Volatile Organic Compounds
SB-13
AKRF Phase II
11/7/2008
µg/Lµg/L Results Result RL Result RL Result RL
1,2,4,5-Tetrachlorobenzene - < 1.5 1.5 < 1.9 1.9 < 0.50 0.5
1,2,4-Trichlorobenzene 0.65 U < 5.0 5 < 6.3 6.3 < 5.0 5
1,2-Dichlorobenzene 0.48 U < 1.0 1 < 1.3 1.3 < 1.0 1
1,2-Diphenylhdrazine - < 5.0 5 < 6.3 6.3 < 5.0 5
1,3-Dichlorobenzene 0.43 U < 1.0 1 < 1.3 1.3 < 1.0 1
1,4-Dichlorobenzene 0.51 U < 1.0 1 < 1.3 1.3 < 1.0 1
2,2'-Oxybis (1-chloropropane) 5 0.71 U - - -
2,4,5-Trichlorophenol 3 0.54 U < 1.0 1 < 1.3 1.3 < 1.0 1
2,4,6-Trichlorophenol 3 0.49 U < 1.0 1 < 1.3 1.3 < 1.0 1
2,4-Dichlorophenol 0.55 U < 1.0 1 < 1.3 1.3 < 1.0 1
2,4-Dimethylphenol 0.50 U < 1.0 1 < 1.3 1.3 < 1.0 1
2,4-Dinitrophenol 1.1 U < 1.0 1 < 1.3 1.3 < 1.0 1
2,4-Dinitrotoluene 5 0.30 U < 5.0 5 < 6.3 6.3 < 5.0 5
2,6-Dinitrotoluene 5 0.42 U < 5.0 5 < 6.3 6.3 < 5.0 5
2-Chloronaphthalene 10 0.49 U < 5.0 5 < 6.3 6.3 < 5.0 5
2-Chlorophenol 0.61 U < 1.0 1 < 1.3 1.3 < 1.0 1
2-Methylnaphthalene 0.47 U < 5.0 5 < 6.3 6.3 < 5.0 5
2-Methylphenol (o-cresol) 0.60 U < 1.0 1 < 1.3 1.3 < 1.0 1
2-Nitroaniline 5 0.53 U < 5.0 5 < 6.3 6.3 < 5.0 5
2-Nitrophenol 0.51 U < 1.0 1 < 1.3 1.3 < 1.0 1
3&4-Methylphenol (m&p-cresol) 0.39 U < 1.0 1 < 1.3 1.3 < 1.0 1
3,3'-Dichlorobenzidine 5 0.66 U < 5.0 5 < 6.3 6.3 < 5.0 5
3-Nitroaniline 5 0.37 U < 5.0 5 < 6.3 6.3 < 5.0 5
4,6-Dinitro-2-methylphenol 0.37 U < 1.0 1 < 1.3 1.3 < 1.0 1
4-Bromophenyl phenyl ether 0.49 U < 5.0 5 < 6.3 6.3 < 5.0 5
4-Chloro-3-methylphenol 1.3 U < 1.0 1 < 1.3 1.3 < 1.0 1
4-Chloroaniline 5 0.67 U < 3.5 3.5 < 4.4 4.4 < 3.5 3.5
4-Chlorophenyl phenyl ether 0.49 U < 5.0 5 < 6.3 6.3 < 5.0 5
4-Nitroaniline 5 0.28 U < 5.0 5 < 6.3 6.3 < 5.0 5
4-Nitrophenol 0.38 U < 1.0 1 < 1.3 1.3 < 1.0 1
Acenaphthene 20 0.38 U < 5.0 5 < 6.3 6.3 < 5.0 5
Acenaphthylene 0.47 U < 0.10 0.1 < 0.13 0.1 < 0.10 0.1
Acetophenone - < 5.0 5 < 6.3 6.3 < 5.0 5
Aniline - < 3.5 3.5 < 4.4 4.4 < 3.5 3.5
Anthracene 50 0.42 U < 5.0 5 < 6.3 6.3 < 5.0 5
Benzo(a)anthracene 0.002 0.49 J 0.03 0 0.19 0 0.06 0
Benzidine 5 < 10 10 < 5.6 5.6 < 4.5 4.5
Benzo(a)pyrene 0.38 J < 0.02 0 < 0.03 0 0.02 0
Benzo(b)fluoranthene 0.002 0.48 J < 0.02 0 0.29 0 0.04 0
Benzo(g,h,i)perylene 1.8 J < 0.02 0 < 0.03 0 0.02 0
Benzo(k)fluoranthene 0.002 0.43 U < 0.02 0 0.08 0 < 0.020 0
Benzoic Acid 0.39 U < 25 25 < 31 31 < 25 25
Benzyl Butyl phthalate 0.48 U < 5.0 5 < 6.3 6.3 < 5.0 5
Bis(2-chloroethoxy)methane 5 1.1 U < 5.0 5 < 6.3 6.3 < 5.0 5
Bis(2-chloroethyl)ether 1 1.0 U < 1.0 1 < 1.3 1.3 < 1.0 1
Bis(2-chloroisopropyl)ether - < 5.0 5 < 6.3 6.3 < 5.0 5
Bis(2-ethylhexyl)phthalate 5 42 < 1.6 1.6 4.1 2 < 1.0 1
Carbazole 0.35 U < 25 25 < 31 31 < 25 25
Chrysene 0.002 0.49 J 0.03 0 0.29 0 0.05 0
Dibenzo(a,h)anthracene 0.32 U < 0.02 0 0.04 0 < 0.020 0
Dibenzofuran 0.39 U < 5.0 5 < 6.3 6.3 < 5.0 5
Diethylphthalate 50 0.42 U < 5.0 5 < 6.3 6.3 < 5.0 5
Dimethylphthalate 50 0.33 U < 5.0 5 < 6.3 6.3 < 5.0 5
Di-n-butylphthalate 50 0.49 U < 5.0 5 < 6.3 6.3 < 5.0 5
Di-n-octylphthalate 50 0.45 U < 5.0 5 < 6.3 6.3 < 5.0 5
Fluoranthene 50 1.3 J < 5.0 5 < 6.3 6.3 < 5.0 5
Fluorene 50 0.48 U < 5.0 5 < 6.3 6.3 < 5.0 5
Hexachlorobenzene 0.04 0.48 U < 0.02 0 < 0.03 0 < 0.020 0
Hexachlorobutadiene 0.5 0.86 U - < 0 0 < 0.40 0.4
Hexachlorocyclopentadiene 5 0.75 U < 5.0 5 < 6.3 6.3 < 5.0 5
Hexachloroethane 5 0.52 U < 2.4 2.4 < 3.0 3 < 0.50 0.5
Indeno(1,2,3-cd)pyrene 0.002 3.7 J < 0.02 0 0.05 0 < 0.020 0
Isophorone 0.38 U < 5.0 5 < 6.3 6.3 < 5.0 5
Naphthalene 0.42 U < 5.0 5 < 6.3 6.3 < 5.0 5
Nitrobenzene 0.4 0.73 U - < 0.04 0 < 0.10 0.1
N-Nitrosodimethylamine - < 1.0 1 < 1.3 1.3 < 1.0 1
N-Nitrosodi-n-propylamine 0.41 U < 5.0 5 < 6.3 6.3 < 5.0 5
N-Nitrosodiphenylamine 50 0.35 U < 5.0 5 < 6.3 6.3 < 5.0 5
Pentachloronitrobenzene - < 0.10 0.1 < 0.13 0.1 < 0.10 0.1
Pentachlorophenol 1.2 U < 0.80 0.8 < 1.0 1 < 0.80 0.8
Phenanthrene 50 1.2 J < 0.10 0.1 0.49 0.1 0.23 0.1
Phenol 0.29 U < 1.0 1 < 1.3 1.3 < 1.0 1
Pyrene 50 1.0 J < 5.0 5 < 6.3 6.3 < 5.0 5
Pyridine - < 10 10 < 13 13 < 10 10
Notes:Dash - Not Analyzed
U - The compound was anlayzed for but not detected at or above the MDL.
N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.
Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard
S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
4/9/2014 4/9/2014 5/8/2014
µg/L µg/L µg/L
Compound NYSDEC Groundwater Quality Standards
E-MW1 E-MW2 E-MW3
EBC RI EBC RI EBC RI
TABLE 8Site E
Former Domino Sugar SiteBrooklyn, New York
Groundwater Analytical ResultsPesticides / PCBs
SB-13
AKRF Phase II
11/7/2008
µg/L
Results Result RL
PCB-1016 0.09 0.084 U < 0.069 0.069
PCB-1221 0.09 0.36 U < 0.069 0.069
PCB-1232 0.09 0.084 U < 0.069 0.069
PCB-1242 0.09 0.084 U < 0.069 0.069
PCB-1248 0.09 0.084 U < 0.069 0.069
PCB-1254 0.09 0.051 U < 0.069 0.069
PCB-1260 0.09 0.053 U < 0.069 0.069
PCB-1262 0.09 - < 0.069 0.069
PCB-1268 0.09 - < 0.069 0.069
4,4-DDD 0.3 0.012 U < 0.14 0.14
4,4-DDE 0.2 0.011 U < 0.14 0.14
4,4-DDT 0.11 0.016 U < 0.14 0.14
a-BHC 0.94 - < 0.069 0.069
a-Chlordane 1.94 0.0089 U < 0.14 0.14
Alachlor 0.0054 U < 1.0 1
Aldrin 0.0092 U < 0.021 0.021
b-BHC 0.04 0.0084 U < 0.069 0.069
Chlordane 0.05 - < 1.4 1.4
d-BHC 0.04 0.0064 U < 0.069 0.069
Dieldrin 0.004 0.011 U < 0.021 0.021
Endosulfan I 0.0052 U < 0.14 0.14
Endosulfan II 0.011 U < 0.14 0.14
Endosulfan Sulfate 0.015 U < 0.14 0.14
Endrin 0.016 U < 0.14 0.14
Endrin aldehyde 5 0.010 U < 0.14 0.14
Endrin ketone 0.012 U < 0.14 0.14
gamma-BHC 0.05 0.0060 U < 0.069 0.069
g-Chlordane 0.0054 U < 0.14 0.14
Heptachlor 0.04 0.0084 U < 0.14 0.14
Heptachlor epoxide 0.03 0.0065 U < 0.14 0.14
Methoxychlor 35 0.10 U < 1.4 1.4
Toxaphene 0.24 U < 3.5 3.5
Notes:U - The compound was anlayzed for but not detected at or above the MDL.
DASH - Not analyzed
Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard
COMPOUNDNYSDEC Groundwater
Quality Standards
E-MW3
EBC RI
5/8/2014
µg/L
TABLE 9Site E
Former Domino Sugar SiteBrooklyn, New York
Groundwater Analytical ResultsMetals
SB-13
AKRF Phase II
11/7/2008
mg/L
Results Result RL Result RL
Aluminum NS 61 2.43 0.01 3.68 0.01
Antimony 0.003 0.0088 U < 0.003 0.003 < 0.003 0.003
Arsenic 0.025 0.04 < 0.004 0.004 < 0.004 0.004
Barium 1 0.59 0.126 0.01 0.128 0.01
Beryllium 0.003 0.0052 J < 0.001 0.001 < 0.001 0.001
Cadmium 0.005 0.0028 U < 0.004 0.004 < 0.004 0.004
Calcium NS 141 110 0.01 124 0.01
Chromium 0.05 0.5 0.004 0.001 0.008 0.001
Cobalt NS 0.099 < 0.005 0.005 < 0.005 0.005
Copper 0.2 0.58 0.007 0.005 0.014 0.005
Iron 0.5 178 2.89 0.01 3.89 0.01
Lead 0.025 0.16 < 0.002 0.002 0.031 0.002
Magnesium 35 65 31.2 0.01 30.9 0.01
Manganese 0.3 3 2.65 0.05 0.229 0.005
Mercury 7.00E-04 0.00009 U < 0.0002 2.00E-04 < 0.0002 2.00E-04
Nickel 0.1 0.39 0.014 0.004 0.005 0.004
Potassium NS 23 12.9 0.1 11.8 0.1
Selenium 0.01 0.0053 J 0.009 0.004 0.007 0.004
Silver 0.05 0.0013 U < 0.005 0.005 < 0.005 0.005
Sodium 2 213 237 1 249 1
Thallium 0.0005 0.008 U < 0.002 0.002 < 0.002 0.002
Vanadium NS 0.21 < 0.010 0.01 < 0.010 0.01
Zinc 2 8 < 0.010 0.01 0.031 0.01
Notes:Dash - Not Analyzed
U - The compound was anlayzed for but not detected at or above the MDL. NS - No Standard
Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard
mg/L
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
E-MW1 E-MW2
EBC RI EBC RI
4/9/2014 4/9/2014
COMPOUNDNYSDEC Groundwater
Quality Standards
mg/L
TABLE 10Site E
Former Domino Sugar SiteBrooklyn, New York
Groundwater Analytical ResultsDissolved Metals
SB-13
AKRF Phase II
11/7/2008
mg/L
Results Result RL Result RL Result RL
Aluminum NS 0.047 U 0.9 0.01 0.39 0.01 0.39 0.01
Antimony 0.003 0.0088 U < 0.003 0.003 < 0.003 0.003 < 0.003 0.003
Arsenic 0.025 0.0044 U < 0.003 0.003 < 0.003 0.003 0.003 0.003
Barium 1 0.082 0.12 0.011 0.1 0.011 0.1 0.011
Beryllium 0.003 0.0011 U < 0.001 0.001 < 0.001 0.001 < 0.001 0.001
Cadmium 0.005 0.0028 U < 0.004 0.004 < 0.004 0.004 0.001 0.004
Calcium NS 131 112 0.01 124 0.01 39.6 0.01
Chromium 0.05 0.001 U 0.001 0.001 < 0.001 0.001 0.005 0.001
Cobalt NS 0.014 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005
Copper 0.2 0.0014 U < 0.005 0.005 < 0.005 0.005 0.003 0.005
Iron 0.5 1.8 0.88 0.01 0.18 0.01 0.38 0.01
Lead 0.025 0.003 U < 0.002 0.002 < 0.002 0.002 0.001 0.002
Magnesium 35 38.5 31.6 0.01 30.9 0.01 8.03 0.01
Manganese 0.3 0.63 2.89 0.053 0.137 0.005 0.019 0.005
Mercury 0.0007 0.00009 U < 0.0002 0.0002 < 0.0002 0.0002 < 0.0004 0.0004
Nickel 0.1 0.019 0.012 0.004 < 0.004 0.004 < 0.004 0.004
Potassium NS 9 13.6 0.1 13.1 0.1 12.5 0.1
Selenium 0.01 0.0058 J < 0.004 0.004 0.006 0.004 0.068 0.004
Silver 0.05 0.0013 U < 0.005 0.005 < 0.005 0.005 0.001 0.005
Sodium 2 211 255 1.1 247 1.1 87.5 1.1
Thallium 0.0005 0.008 U < 0.001 0.001 < 0.001 0.001 < 0.001 0.001
Vanadium NS 0.0012 U < 0.01 0.01 < 0.01 0.01 0.007 0.011
Zinc 2 0.25 < 0.011 0.011 < 0.011 0.011 0.008 0.011
Notes:Dash - Not AnalyzedNS - No Standard
U - The compound was anlayzed for but not detected at or above the MDL.
Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard
J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.
4/9/2014 4/9/2014 5/8/2014
mg/L mg/L mg/L
COMPOUNDNYSDEC Groundwater
Quality Standards
E-MW1 E-MW2 E-MW3
EBC RI EBC RI EBC RI
TABLE 11Site E
Former Domino Sugar SiteBrooklyn, New York
Soil Gas Analytical ResultsVolatile Organic Compounds
NYSDOH Soil OutdoorBackground Levels
(µg/m3) (a) (µg/m3) (b) Result RL Result RL Result RL Result RL Result RL
1,1,1,2-Tetrachloroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,1,1-Trichloroethane 100 <2.0 - 2.8 3.16 1 < 1.00 1 3.54 1 < 1.00 1 1.25 1
1,1,2,2-Tetrachloroethane <1.5 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,1,2-Trichloroethane <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,1-Dichloroethane <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,1-Dichloroethene <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,2,4-Trichlorobenzene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,2,4-Trimethylbenzene <1.0 < 1.00 1 34.5 1 24.5 1 24.3 1 17.8 1
1,2-Dibromoethane <1.5 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,2-Dichlorobenzene <2.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,2-Dichloroethane <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,2-Dichloropropane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,2-Dichlorotetrafluoroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,3,5-Trimethylbenzene <1.0 < 1.00 1 9.28 1 6.78 1 6.58 1 6.29 1
1,3-Butadiene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,3-Dichlorobenzene <2.0 < 1.00 1 5.53 1 1.8 1 2.76 1 6.01 1
1,4-Dichlorobenzene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
1,4-Dioxane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
2-Hexanone 5.28 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
4-Ethyltoluene NA < 1.00 1 6.88 1 5.45 1 5.99 1 4.72 1
4-Isopropyltoluene < 1.00 1 < 1.00 1 1.26 1 < 1.00 1 < 1.00 1
4-Methyl-2-pentanone < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Acetone NA 254 1 387 1 769 1 268 1 610 1
Acrylonitrile < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Benzene <1.6 - 4.7 < 1.00 1 3.32 1 7.02 1 3.48 1 6.13 1
Benzyl Chloride NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Bromodichloromethane <5.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Bromoform <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Bromomethane <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Carbon Disulfide NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 5.63 1
Carbon Tetrachloride 5 <3.1 0.377 0.25 0.503 0.25 < 0.25 0.25 0.566 0.25 < 0.25 0.25
Chlorobenzene <2.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Chloroethane NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Chloroform <2.4 3.81 1 < 1.00 1 8.64 1 < 1.00 1 1.85 1
Chloromethane <1.0 - 1.4 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
cis-1,2-Dichloroethene <1.0 2.65 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
cis-1,3-Dichloropropene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Cyclohexane NA < 1.00 1 3.34 1 4.71 1 3.47 1 5.64 1
Dibromochloromethane <5.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Dichlorodifluromethane NA 1.63 1 2.57 1 2.37 1 2.92 1 2.47 1
Ethanol 9.4 1 52.3 1 58 1 49.3 1 56.9 1
Ethyl Acetate NA < 1.00 1 12.3 1 22.1 1 9 1 14.8 1
Ethylbenzene <4.3 < 1.00 1 15.6 1 11.8 1 13.4 1 14.1 1
Heptane NA 1.15 1 9.26 1 17.3 1 7.21 1 19.2 1
Hexachlorobutadiene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Hexane <1.5 < 1.00 1 5.88 1 13.4 1 5.11 1 18.5 1
Isopropylalcohol NA 4.86 1 2.97 1 4.52 1 4.84 1 3.86 1
Isopropylbenzene < 1.00 1 1.82 1 1.28 1 1.33 1 1.28 1
Xylene (m&p) <4.3 1.04 1 55.5 1 42.5 1 46.9 1 48.2 1
Methyl Ethyl Ketone 19.9 1 23.9 1 41.8 1 18.4 1 31.2 1
MTBE NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Methylene Chloride <3.4 1.6 1 1.25 1 < 1.00 1 1.42 1 1.14 1
n-Butylbenzene < 1.00 1 2.74 1 2.69 1 2.14 1 2.58 1
Xylene (o) <4.3 < 1.00 1 23.1 1 15.4 1 18.4 1 16.9 1
Propylene NA 5.21 1 2.24 1 23.7 1 2.03 1 50.9 1
sec-Butylbenzene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Styrene <1.0 < 1.00 1 1.02 1 1.4 1 1.02 1 1.53 1
Tetrachloroethene 100 2.03 0.25 2.85 0.25 6.57 0.25 3.25 0.25 28.3 0.25
Tetrahydrofuran NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Toluene 1.0 - 6.1 1.81 1 41.8 1 50.1 1 36.8 1 56.1 1
trans-1,2-Dichloroethene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
trans-1,3-Dichloropropene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Trichloroethene 5 <1.7 24.1 0.25 < 0.25 0.25 61.2 0.25 < 0.25 0.25 54.8 0.25
Trichlorofluoromethane NA 1.35 1 1.24 1 1.29 1 1.52 1 1.35 1
Trichlorotrifluoroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1
Vinyl Chloride <1.0 < 0.25 0.25 < 0.25 0.25 < 0.25 0.25 < 0.25 0.25 < 0.25 0.25
BTEX 2.85 139.32 126.82 118.98 141.43
Notes:NA No guidance value or standard available(a) Final Guidance for Evaluating Soil Vapor Intrusion in the State of New York. October 2006. New York State Department of Health.(b) NYSDOH Guidance for Evaluating Soil Vapor Intrusion in the State of New York, February 2005, Summary of Background Levels for Selected Compounds (NYSDOH Database, Outdoor values)Value detected above NYSDOH Air Guidance Value of 5 µg/m3, which according to Soil Vapor/Indoor Air Matrix 1 would require at a minimum, mitigation. Value detected above NYSDOH Air Guidance Value of 100 µg/m3, which according to Soil Vapor/Indoor Air Matrix 2 would require at a minimum, mitigation.
E-SG4(µg/m³)
E-SG5(µg/m³) COMPOUNDS
NYSDOH Maximum Sub-Slab Value
E-SG1(µg/m³)
E-SG2(µg/m³)
E-SG3(µg/m³)
EEBBCCEnvironmental Business Consultants Phone 631.504.6000
Fax1808 Middle Country Road. Ridge. NY 11961 631.924.2780
FORMER DOMINO SUGAR SITE E
FIGURE 1 Site Location Map
USGS Brooklyn Quadrangle 1995, Contour Interval = 10 feet
317-329 Kent Avenue, Brooklyn, NY
SITE LOCATION
EEBBCCEnvironmental Business Consultants
Phone 631.504.6000Fax 631. 924 .2870
Site Name:
Site Address:
Drawing Title:
Figure No.2 317-329 Kent Avenue, Brooklyn, NY 11249
Domino Sugar Site - Site E
Site Boundary Map
1 Inch = 50 Feet
7525 50
Site Boundary
KEY:
0
SCALE:
KENT AVENUE
SO
UT
H 4
TH
ST
RE
ET
SID
EW
ALK
SO
UT
H 3
RD
ST
RE
ET
LOT 30
LOT 1
LOT 24
LO
T 26
LO
T 27
32
0'
180'
E
EEBB CC ENVIRONMENTAL BUSINESSS CONSULTANTS 1808 Middle Country Road, Ridge, New York 11961 Phone: (631) 504-6000 Fax: (631) 924-2870
FIGURE 4 SURROUNDING LAND USE MAP
SITE D 317-329 KENT AVENUE, BROOKLYN, NY
Source: http://www.oasisnyc.net/map.aspx
Site D
Site CSite E
Site F
Site B
EEBBCCEnvironmental Business Consultants
Phone 631.504.6000Fax 631. 924 .2870
Site Name:
Site Address:
Drawing Title:
Figure No.5 317-329 Kent Avenue, Brooklyn, NY 11249
Domino Sugar Site - Site E
Site Sampling Locations
1 Inch = 50 Feet
7525 50
New Building Area
KEY:
0
SCALE:
KENT AVENUE
SO
UT
H 4
TH
ST
RE
ET
Existing Building
SB-13
SIDEWALK
SO
UT
H 3
RD
ST
RE
ET
LOT 30
LOT 1
LOT 24
LO
T 26
LO
T 27
E-MW1E-SB1
E-SB6
E-SB7
E-SB3
Soil Boring Location
GW Sampling Location
Soil Boring Location (AKRF Phase II 2008)
E-SB4 E-SB5
E-SG1
E-SG3
E-SG5
E-SG4
E-MW3
E-MW2
E-SB2
E-SG2
SG Sampling Location
REFUSALS 3-14'
NO SAMPLESALL C&D DEBRIS
RECOVERED
SB-12
E
Soil Boring Location (NOVA Phase III 2004)
B-5
B-3
B-4
B-1
B-2
EEBBCCEnvironmental Business Consultants
Phone 631.504.6000Fax 631. 924 .2870
Site Name:
Site Address:
Drawing Title:
Figure No.6 317-329 Kent Avenue, Brooklyn, NY 11249
Domino Sugar Site - Site E
Soil Exceedences Map
1 Inch = 50 Feet
7525 50New Building Area
KEY:
0
SCALE:
KENT AVENUE
Existing Building
SIDEWALK
SO
UT
H 3
RD
ST
RE
ET
LOT 30 LOT 24
LO
T 26
LO
T 27
E-MW1
E-SB1
E-SB6
E-SB7
E-SB3
Soil Boring Location
GW Sampling Location
Soil Boring Location (AKRF Phase II 2008)
E-SB5
E-SG1
E-SG3
E-SG5
E-SG4
E-MW3
E-MW2E-SB2
E-SG2
SG Sampling Location
REFUSALS 3-14'
NO SAMPLESALL C&D DEBRIS
RECOVERED
VOCs, SVOCs, Pesticides, PCBs ppb
Concentration above Unrestricted Use SCO
Concentration above Restricted Res SCO
Metals ppm
E-SB1 (0-2')
Lead 98.7
Mercury 0.55
E-SB2 (0-2')
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Chrysene
Indeno(1,2,3-cd)pyrene
Copper
Lead
Benzo(k)fluoranthene
3,700
5,000
4,800
1,400
4,200
153
167
1,500
E-SB4 (0-2')
Lead 108
Zinc 116
E-SB5 (0-2')
Benzo(a)anthracene
Benzo(a)pyrene 1,200
Benzo(b)fluoranthene 1,800
1,400
Indeno(1,2,3-cd)pyrene 3,400
Benzo(k)fluoranthene 3,700
Chrysene 8,600
Benzo(a)pyrene 8,300
Chrysene
Copper 57
1,300
Lead 166
Mercury 0.28
Zinc 121
E-SB5 (12-14')
Benzo(a)anthracene 9,300
Benzo(b)fluoranthene 11,000
Nickel 39.6
Lead 308
Mercury 0.23
Cadmium 8.19
Arsenic
Copper 185
Zinc 1,480
137
E-SB6 (0-2')
Acetone 68
Benzo(a)anthracene
Benzo(a)pyrene 1,800
Benzo(b)fluoranthene 2,300
1,800
Zinc 130
Chrysene
PCB-1254 210
1,800
4,4-DDT 24
Lead 156
Mercury 0.34
Benzo(k)fluoranthene 990
E-SB7 (0-2')
Lead 174
Indeno(1,2,3-cd)pyrene
Benzo(k)fluoranthene 6,200
Chrysene 17,000
Benzo(a)pyrene 15,000
AKRF - SB-12 (1-3')
Benzo(a)anthracene 17,000
Benzo(b)fluoranthene 18,000
Copper
0.22
Lead71.7
Mercury
192
4,4'-DDD 7.33
Dibenz(a,h)anthracene
4,4'-DDT 13
18,000
4,500
Indeno(1,2,3-cd)pyrene
Benzo(k)fluoranthene 3,700
Chrysene 12,000
Benzo(a)pyrene 9,900
AKRF - SB-13 (1-3')
Benzo(a)anthracene 12,000
Benzo(b)fluoranthene 11,000
Copper
0.27
Lead79.7
Mercury
446
4,4'-DDD 15
Dibenz(a,h)anthracene
4,4'-DDT 9.3
8,900
4,100
695Zinc
E-SB4
BSoil Boring Location (NOVA Phase III 2004)
SB-13
SB-12
B-5
B-3
B-4
B-1
B-2
Indeno(1,2,3-cd)pyrene
480
Benzo(k)fluoranthene 3,100
Chrysene 3,200
Benzo(a)pyrene 3,000
NOVA B-2 (0-4)
Benzo(a)anthracene 3,600
Benzo(b)fluoranthene 3,100
1,300
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
Chrysene 1,400
Benzo(a)pyrene 1,400
NOVA B-2 (8-12)
Benzo(b)fluoranthene 1,200
730
NOVA B-3 (0-4')
Lead 140
Indeno(1,2,3-cd)pyrene
2,600
Benzo(k)fluoranthene 16,000
Chrysene 18,000
Benzo(a)pyrene 17,000
NOVA B-4 (0-4')
Benzo(a)anthracene 21,000
Benzo(b)fluoranthene 16,000
6,900
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
1,900
Benzo(k)fluoranthene 13,000
Chrysene 15,000
Benzo(a)pyrene 13,000
NOVA B-4 (4-8')
Benzo(a)anthracene 16,000
Benzo(b)fluoranthene 13,000
7,900
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
2,500
Benzo(k)fluoranthene 20,000
Chrysene 19,000
Benzo(a)pyrene 20,000
NOVA B-4 (8-12')
Benzo(a)anthracene 23,000
Benzo(b)fluoranthene 20,000
7,700
Dibenz(a,h)anthracene
Indeno(1,2,3-cd)pyrene
520
Benzo(k)fluoranthene 3,100
Chrysene 3,000
Benzo(a)pyrene 3,300
NOVA B-5 (0-4')
Benzo(a)anthracene 3,200
3,100
1,500
Dibenz(a,h)anthracene
Benzo(b)fluoranthene
Lead 91
Lead 84
NOVA B-5 (4-8')
EEBBCCEnvironmental Business Consultants
Phone 631.504.6000Fax 631. 924 .2870
Site Name:
Site Address:
Drawing Title:
Figure No.7 317-329 Kent Avenue, Brooklyn, NY 11249
Domino Sugar Site - Site E
Groundwater Exceedences Map
1 Inch = 50 Feet
7525 50
New Building Area
KEY:
0
SCALE:
KENT AVENUE
SO
UT
H 4
TH
ST
RE
ET
Existing Building
SB-13
SIDEWALK
SO
UT
H 3
RD
ST
RE
ET
LOT 30
LOT 1
LOT 24
LO
T 26
LO
T 27
E-MW1E-SB1
E-SB6
E-SB7
E-SB3
Soil Boring Location
GW Sampling Location
Soil Boring Location (AKRF Phase II 2008)
E-SB4
E-SB5
E-SG1
E-SG3
E-SG5
E-SG4
E-MW3
E-MW2E-SB2
E-SG2
SG Sampling Location
REFUSALS 3-14'
NO SAMPLESALL C&D DEBRIS
RECOVERED
SB-12
E
E-MW1
Trichloroethylene 24
Chrysene 0.03
VOCs (ug/L)
SVOCs (ug/L)
Iron 0.88
Manganese 2.89
Dissolved Metals (mg/L)
Benzo(a)anthracene 0.03
E-MW2
Trichloroethylene 20
Benzo(b)fluoranthene 0.29
Benzo(k)fluoranthene 0.08
VOCs (ug/L)
SVOCs (ug/L)
Chrysene 0.29
Indeno(1,2,3-cd)pyrene 0.05
Benzo(a)anthracene 0.19
Sodium 255
Sodium 247
Dissolved Metals (mg/L)
E-MW3
Benzo(b)fluoranthene 0.04
Chrysene 0.05
SVOCs (ug/L)
Selenium 0.068
Sodium 87.5
Benzo(a)anthracene 0.06
Dissolved Metals (mg/L)
Iron 0.38
AKRF - SB-13
cis-1,2-Dichloroethene 5.5
Benzo(b)fluoranthene 0.48
Bis(2-ethylexyl)phthalate 42
VOCs (ug/L)
SVOCs (ug/L)
Chrysene 0.49
Indeno(1,2,3-cd)pyrene 3.7
Benzo(a)anthracene 0.49
Iron 1.8
Dissolved Metals (mg/L)
Tetrachloroethene 5.7
Trichloroethene 27
Magnesium 38.5
Manganese 0.63
Sodium 211
EEBBCCEnvironmental Business Consultants
Phone 631.504.6000Fax 631. 924 .2870
Site Name:
Site Address:
Drawing Title:
Figure No.8 317-329 Kent Avenue, Brooklyn, NY 11249
Domino Sugar Site - Site E
Soil Vapor Detections
1 Inch = 50 Feet
7525 50
New Building Area
KEY:
0
SCALE:
KENT AVENUE
SO
UT
H 4
TH
ST
RE
ET
Existing Building
SB-13
SIDEWALK
SO
UT
H 3
RD
ST
RE
ET
LOT 30
LOT 1
LOT 24
LOT
26
LOT
27
E-MW1E-SB1
E-SB6
E-SB7
E-SB3
Soil Boring Location
GW Sampling Location
Soil Boring Location (AKRF Phase II 2008)
E-SB4 E-SB5
E-SG1
E-SG3
E-SG5
E-SG4
E-MW3
E-MW2
E-SB2
E-SG2
SG Sampling LocationREFUSALS 3-14'
NO SAMPLESALL C&D DEBRIS
RECOVERED
SB-12
EE-SG5
Compound µg/m³
1,1,1-Trichloroethane
Carbon Tetrachloride
1.25
PCE 28.3
TCE 54.8
ND
E-SG4
Compound µg/m³
1,1,1-Trichloroethane
Carbon Tetrachloride
ND
PCE 3.25
TCE ND
0.566
E-SG2
Compound µg/m³
1,1,1-Trichloroethane
Carbon Tetrachloride
ND
PCE 2.85
TCE ND
0.503
E-SG1
Compound µg/m³
1,1,1-Trichloroethane
Carbon Tetrachloride
3.16
PCE 2.03
TCE 24.1
0.377
Value Detected Above NYSDOHAir Guidance Value
E-SG3
Compound µg/m³
1,1,1-Trichloroethane
Carbon Tetrachloride
3.54
PCE 6.57
TCE 61.2
ND
Geologic Boring Log Details
Site Elevation Datum
Site Name: TTM1401 DTW Ground Elevation
Drilling Company: Method:Eastern Environmental Solutions Geoprobe Well SpecificationsDate Started:
Installed E-MW1Completion Depth:40 feet D Mosca
DEPTH SAMPLES(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID
(in.) 6 in. (ppm)
0
5
10
15
20
25
30
35
36 0.0
26" - Tan coarse sand.
10" - Saturated fine brown sand.
*Retained soil sample E-SB1(29-31')
30 0.0
30" - Medium brown sand and fine gravel.
32 0.0
32" - Medium brown sand and fine gravel.
to
22 0.0
22" - Medium brown sand and fine gravel.
to
21 0.0
21" - Medium brown sand.
to
25 0.0
7" - Top soil and gravel.
to18" - Medium brown sand.
*Retained soil sample E-SB1(0-2')
4/8/2014 4/8/2014Geologist
E-SB1
(NTS)
Brooklyn, NY Groundwater depth
Date Completed:
30" - Saturated brown sand.
to
E-SB1Location: Performed at the northeast corner of the Site. Depth to Water
(ft. from grade.)Address: Date
1" PVC Set at 40' with 15' screen
to
to
30 0.0
EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS
Geologic Boring Log Details
Site Elevation Datum
Site Name: TTM1401 DTW Ground Elevation
Drilling Company: Method:Eastern Environmental Solutions Geoprobe Well SpecificationsDate Started:
NoneCompletion Depth:31 feet D Mosca
DEPTH SAMPLES(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID
(in.) 6 in. (ppm)
0
5
10
15
20
25
31
E-SB2Location: Performed at the southeast corner of the Site. Depth to Water
(ft. from grade.)Address: Date
Brooklyn, NY Groundwater depth
Date Completed:4/8/2014 4/8/2014
Geologist
E-SB2
(NTS)
13 0.0
13" - Topsoil followed by concrete and brick.
to
*Retained soil sample E-SB1(0-2')
12 0.0
12" - Concrete and brick.
to
8 0.0
8" - Concrete and brick.
to
0 0.0
No recovery, rock in shoe.
to
19 0.0
2" - Historic fill composed of coal and brick.
to
20" - Medium tan sand.
17" - Medium tan sand.
20 0.0to
*Retained soil sample E-SB1(28-30')
EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS
Geologic Boring Log Details
Site Elevation Datum
Site Name: TTM1401 DTW Ground Elevation
Drilling Company: Method:C² Environmental Geoprobe Well SpecificationsDate Started:
NoneCompletion Depth:20 feet D Mosca
DEPTH SAMPLES(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID
(in.) 6 in. (ppm)
0
5
10
15
20
32 0.0
2" - Brick.
to30" - Medium sand and fine gravel.
*Retained soil sample E-SB4(15-17')
28 0.0
18" - Brick and concrete.
to4" - Medium sand and broken brick.
6" - Brick and concrete.
0
No recovery.
to
30 0.0
6" - Topsoil and gravel.
to24" - Brick and concrete.
*Retained soil sample E-SB4(0-2')
4/2/2014 4/2/2014Geologist
E-SB4
(NTS)
Brooklyn, NY Groundwater depth
Date Completed:
E-SB4Location: Performed along South 4th Street approximately 140'
from the east property line.Depth to Water(ft. from grade.)
Address: Date
EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS
Geologic Boring Log Details
Site Elevation Datum
Site Name: TTM1401 DTW Ground Elevation
Drilling Company: Method:Eastern Environmental Solutions Geoprobe Well SpecificationsDate Started:
NoneCompletion Depth:10 feet D Mosca
DEPTH SAMPLES(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID
(in.) 6 in. (ppm)
0
5
10
14
3" - Red brick.
10" - Dark moist historic fill composed of coal, brick, and gravel.
4" - Moist brown silty sand.
*Retained soil sample A-SB5(11-14')
Refusal at 14'.
19 0.0
19" - Brick and concrete.
to
27 0.0
11" - Topsoil
to7" - Concrete.
9" - Red brick.
*Retained soil sample E-SB5(0-2')
4/2/2014 4/2/2014Geologist
E-SB5
(NTS)
Brooklyn, NY Groundwater depth
Date Completed:
to17 0.0
E-SB5Location: Performed along South 3rd Street approximately over
140' from the east property line.Depth to Water(ft. from grade.)
Address: Date
EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS
Geologic Boring Log Details
Site Elevation Datum
Site Name: TTM1401 DTW Ground Elevation
Drilling Company: Method:Eastern Environmental Solutions Geoprobe Well SpecificationsDate Started:
NoneCompletion Depth:20 feet D Mosca
DEPTH SAMPLES(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID
(in.) 6 in. (ppm)
0
5
10
15
20
E-SB6Location: Performed in the southwest corner within the bike park. Depth to Water
(ft. from grade.)Address: Date
Brooklyn, NY Groundwater depth
Date Completed:4/8/2014 4/8/2014
Geologist
E-SB6
(NTS)
to
20 0.0
4" - Top soil.
to
*Retained soil sample E-SB6(0-2')
5" - Brown silty sand.
12 0.0
6" - Concrete and brick.
to
*Retained soil sample E-SB6(15-17')
14 0.0
2" - Red brick.
to7" - Historic fill.
22 0.0
22" - Medium brown sand and gravel. Moist at the bottom 6".
22" - Historic fill composed of coal, brick, etc in a sandy matrix.
6" - Historic fill.
EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS
Geologic Boring Log Details
Site Elevation Datum
Site Name: TTM1401 DTW Ground Elevation
Drilling Company: Method:Eastern Environmental Solutions Geoprobe Well SpecificationsDate Started:
E-MW3Completion Depth:20 feet D Mosca
DEPTH SAMPLES(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID
(in.) 6 in. (ppm)
0
5
10
15
20
1" PVC Set at 25' with 10' screen
E-SB7Location: Performed in the northeast corner of the Site. Depth to Water
(ft. from grade.)Address: Date
Brooklyn, NY Groundwater depth
Date Completed:4/8/2014 4/8/2014
Geologist
E-SB7
(NTS)
20 0.0
4" - Top soil.
to16" - Concrete and brick.
*Retained soil sample E-SB7(0-2')
18 0.0
18" - Concrete and brick.
to
23 0.0
23" - Medium brown sand.
to
45 0.0
45" - Firm, moist brown sandy loam.
to
*Retained soil sample E-SB7(15-17')
EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS
Well I.D.: E-MW1 Date: 4/9/2014
Well Depth (from TOC): 40 Equipment: Check Valve
Static Water Level (from TOC): 34.89 Field Personnel: Dominick Mosca
Height of Water in Well: 5.11
Gallons of Water per Well Volume: 0.2044
Approximate Flow Rate: 400ml/min.
Time Time (24Hr) ~ Flow RateGal.
RemovedpH Cond. (µS/cm) Temp. (ºF) DO (mg/L) Comments
0.00 8:11 400ml/min 0 turbid2.00 8:13 400ml/min 0.22 turbid4.00 8:15 400ml/min 0.44 clear6.00 8:17 400ml/min 0.66 clear8.00 8:19 400ml/min 0.88 clear
8:25 Collected Samples
Note 400 ml = 0.11 gallons
GROUNDWATER PURGE / SAMPLE LOGS
EBCEB C ENVIRONMENTAL BUSINESS CONSULTANTS
Well I.D.: E-MW2 Date: 4/9/2014
Well Depth (from TOC): 40 Equipment: Check Valve
Static Water Level (from TOC): 30.73 Field Personnel: Dominick Mosca
Height of Water in Well: 9.27
Gallons of Water per Well Volume: 1.4832
Approximate Flow Rate: 400ml/min.
Time Time (24Hr) ~Flow RateGal.
RemovedpH Cond. (µS/cm) Temp. (ºF) DO (mg/L) Comments
0.00 8:34 400ml/min 0 turbid2.00 8:36 400ml/min 0.22 turbid4.00 8:38 400ml/min 0.44 turbid6.00 8:40 400ml/min 0.66 turbid8.00 8:42 400ml/min 0.88 clear10.00 8:44 400ml/min 1.1 clear12.00 8:46 400ml/min 1.32 clear14.00 8:48 400ml/min 1.54 clear16.00 8:50 400ml/min 1.76 clear
8:55 Collected Samples
Note 400 ml = 0.11 gallons
GROUNDWATER PURGE / SAMPLE LOGS
EBCEB C ENVIRONMENTAL BUSINESS CONSULTANTS
Well I.D.: E-MW3 Date: 5/8/2014
Well Depth (from TOC): 30 Equipment: Check Valve
Static Water Level (from TOC): 22.47 Field Personnel: Dominick Mosca
Height of Water in Well: 7.53
Gallons of Water per Well Volume: 0.3012
Approximate Flow Rate: 400ml/min.
Time Time (24Hr) ~ Flow RateGal.
RemovedpH Cond. (µS/cm) Temp. (ºF) DO (mg/L) Comments
0.00 8:39 400ml/min 0 turbid2.00 8:41 400ml/min 0.22 turbid4.00 8:43 400ml/min 0.44 clear6.00 8:45 400ml/min 0.66 clear8.00 8:49 400ml/min 0.88 clear
8:55 Collected Samples
Note 400 ml = 0.11 gallons
GROUNDWATER PURGE / SAMPLE LOGS
EBCEB C ENVIRONMENTAL BUSINESS CONSULTANTS
BG30367
Wednesday, May 07, 2014
Sample ID#s:
Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Project ID: DOMINO SUGAR SITE E
Sincerely yours,
Laboratory DirectorPhyllis Shiller
Enclosed are revised Analysis Report pages. Please replace and discard the original pages. If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.
NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B
NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823
SDG CommentsMay 07, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG30363
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB6 15-17
Phoenix ID: BG30367
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportMay 07, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.32Silver 0.32 04/11/14 LK SW6010mg/Kg0.196770Aluminum 32 04/11/14 LK SW6010mg/Kg6.51.4Arsenic 0.6 04/11/14 LK SW6010mg/Kg0.65
45.4Barium 0.6 04/11/14 LK SW6010mg/Kg0.130.35Beryllium 0.26 04/11/14 LK SW6010mg/Kg0.132730Calcium 3.2 04/11/14 LK SW6010mg/Kg3.0
< 0.32Cadmium 0.32 04/11/14 LK SW6010mg/Kg0.135.18Cobalt 0.32 04/11/14 LK SW6010mg/Kg0.1327.4Chromium 0.32 04/11/14 LK SW6010mg/Kg0.1318.9Copper 0.32 04/11/14 LK SW6010mg/kg0.26
15300Iron 32 04/11/14 LK SW6010mg/Kg B32< 0.06Mercury 0.06 04/10/14 RS SW-7471mg/Kg0.041480Potassium 6 04/11/14 LK SW6010mg/Kg2.52950Magnesium 32 04/11/14 LK SW6010mg/Kg1.9357Manganese 3.2 04/11/14 LK SW6010mg/Kg1.3194Sodium 6 04/11/14 LK SW6010mg/Kg2.812.3Nickel 0.32 04/11/14 LK SW6010mg/Kg0.136.6Lead 0.6 04/11/14 LK SW6010mg/Kg0.19
< 1.6Antimony 1.6 04/11/14 LK SW6010mg/Kg0.65< 1.3Selenium 1.3 04/11/14 LK SW6010mg/Kg1.1< 1.3Thallium 1.3 04/11/14 LK SW6010mg/Kg1.330.3Vanadium 0.3 04/11/14 LK SW6010mg/Kg0.1325.0Zinc 0.6 04/11/14 LK SW6010mg/Kg0.3292Percent Solid 04/09/14 I E160.3%
CompletedSoil Extraction for PCB 05/01/14 JB SW3545CompletedSoil Extraction for Pesticide 05/01/14 JB/V SW3545CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471
Page 1 of 6 Ver 2
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
CompletedTotal Metals Digest 04/09/14 CB/AG/WSW846 - 3050
CompletedField Extraction 04/08/14 SW5035
Polychlorinated BiphenylsNDPCB-1016 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1221 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1232 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1242 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1248 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1254 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1260 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1262 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1268 35 05/02/14 AW SW 8082ug/Kg35
QA/QC Surrogates97% DCBP 05/02/14 AW 30 - 150 %%82% TCMX 05/02/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.5 05/05/14 CE SW8081ug/Kg2.5ND4,4' -DDE 2.5 05/05/14 CE SW8081ug/Kg2.5ND4,4' -DDT 2.5 05/05/14 CE SW8081ug/Kg2.5NDa-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.5 05/05/14 CE SW8081ug/Kg3.5NDAldrin 1.8 05/05/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDChlordane 21 05/05/14 CE SW8081ug/Kg21NDd-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 05/05/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndosulfan II 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndosulfan sulfate 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndrin 1.8 05/05/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndrin ketone 1.8 05/05/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.5 05/05/14 CE SW8081ug/Kg3.5NDHeptachlor 1.8 05/05/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 05/05/14 CE SW8081ug/Kg1.8NDMethoxychlor 7.0 05/05/14 CE SW8081ug/Kg7.0NDToxaphene 180 05/05/14 CE SW8081ug/Kg180
QA/QC Surrogates101% DCBP 05/05/14 CE 30 - 150 %%90% TCMX 05/05/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 7.3 04/11/14 U SW8260ug/Kg1.2ND1,1,1-Trichloroethane 7.3 04/11/14 U SW8260ug/Kg1.5ND1,1,2,2-Tetrachloroethane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,1,2-Trichloroethane 7.3 04/11/14 U SW8260ug/Kg0.71ND1,1-Dichloroethane 7.3 04/11/14 U SW8260ug/Kg1.4
Page 2 of 6 Ver 2
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.6ND1,1-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg1.4ND1,2,3-Trichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.5ND1,2,3-Trichloropropane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,2,4-Trichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.5ND1,2,4-Trimethylbenzene 7.3 04/11/14 U SW8260ug/Kg1.0ND1,2-Dibromo-3-chloropropane 7.3 04/11/14 U SW8260ug/Kg2.0ND1,2-Dibromoethane 7.3 04/11/14 U SW8260ug/Kg1.9ND1,2-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg0.80ND1,2-Dichloroethane 7.3 04/11/14 U SW8260ug/Kg0.64ND1,2-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,3,5-Trimethylbenzene 7.3 04/11/14 U SW8260ug/Kg0.96ND1,3-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg0.77ND1,4-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.2ND2,2-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg1.2ND2-Chlorotoluene 7.3 04/11/14 U SW8260ug/Kg1.2ND2-Hexanone 36 04/11/14 U SW8260ug/Kg3.3ND2-Isopropyltoluene 7.3 04/11/14 U SW8260ug/Kg 11.0ND4-Chlorotoluene 7.3 04/11/14 U SW8260ug/Kg0.84ND4-Methyl-2-pentanone 36 04/11/14 U SW8260ug/Kg1.7NDAcetone 50 04/11/14 U SW8260ug/Kg7.2NDAcrylonitrile 15 04/11/14 U SW8260ug/Kg4.1NDBenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDBromobenzene 7.3 04/11/14 U SW8260ug/Kg0.95NDBromochloromethane 7.3 04/11/14 U SW8260ug/Kg1.1NDBromodichloromethane 7.3 04/11/14 U SW8260ug/Kg0.90NDBromoform 7.3 04/11/14 U SW8260ug/Kg1.0NDBromomethane 7.3 04/11/14 U SW8260ug/Kg5.6NDCarbon Disulfide 7.3 04/11/14 U SW8260ug/Kg1.2NDCarbon tetrachloride 7.3 04/11/14 U SW8260ug/Kg0.84NDChlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.1NDChloroethane 7.3 04/11/14 U SW8260ug/Kg1.7NDChloroform 7.3 04/11/14 U SW8260ug/Kg1.3NDChloromethane 7.3 04/11/14 U SW8260ug/Kg3.8NDcis-1,2-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.6NDcis-1,3-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg0.79NDDibromochloromethane 7.3 04/11/14 U SW8260ug/Kg0.82NDDibromomethane 7.3 04/11/14 U SW8260ug/Kg0.92NDDichlorodifluoromethane 7.3 04/11/14 U SW8260ug/Kg1.9NDEthylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDHexachlorobutadiene 7.3 04/11/14 U SW8260ug/Kg1.5NDIsopropylbenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDm&p-Xylene 7.3 04/11/14 U SW8260ug/Kg2.9NDMethyl Ethyl Ketone 44 04/11/14 U SW8260ug/Kg6.3NDMethyl t-butyl ether (MTBE) 15 04/11/14 U SW8260ug/Kg2.0NDMethylene chloride 7.3 04/11/14 U SW8260ug/Kg1.2NDNaphthalene 7.3 04/11/14 U SW8260ug/Kg2.0NDn-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3
Page 3 of 6 Ver 2
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDo-Xylene 7.3 04/11/14 U SW8260ug/Kg2.8NDp-Isopropyltoluene 7.3 04/11/14 U SW8260ug/Kg1.0NDsec-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDStyrene 7.3 04/11/14 U SW8260ug/Kg2.1NDtert-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.2NDTetrachloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDTetrahydrofuran (THF) 15 04/11/14 U SW8260ug/Kg 16.6NDToluene 7.3 04/11/14 U SW8260ug/Kg1.2NDtrans-1,2-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,3-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,4-dichloro-2-butene 15 04/11/14 U SW8260ug/Kg14NDTrichloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDTrichlorofluoromethane 7.3 04/11/14 U SW8260ug/Kg1.6NDTrichlorotrifluoroethane 7.3 04/11/14 U SW8260ug/Kg1.1NDVinyl chloride 7.3 04/11/14 U SW8260ug/Kg2.4
QA/QC Surrogates105% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%100% Bromofluorobenzene 04/11/14 U 70 - 130 %%114% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 250 04/10/14 DD SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 250 04/10/14 DD SW 8270ug/Kg110ND1,2-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg99ND1,2-Diphenylhydrazine 250 04/10/14 DD SW 8270ug/Kg110ND1,3-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg100ND1,4-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg100ND2,4,5-Trichlorophenol 250 04/10/14 DD SW 8270ug/Kg190ND2,4,6-Trichlorophenol 250 04/10/14 DD SW 8270ug/Kg110ND2,4-Dichlorophenol 250 04/10/14 DD SW 8270ug/Kg120ND2,4-Dimethylphenol 250 04/10/14 DD SW 8270ug/Kg87ND2,4-Dinitrophenol 1800 04/10/14 DD SW 8270ug/Kg250ND2,4-Dinitrotoluene 250 04/10/14 DD SW 8270ug/Kg140ND2,6-Dinitrotoluene 250 04/10/14 DD SW 8270ug/Kg110ND2-Chloronaphthalene 250 04/10/14 DD SW 8270ug/Kg100ND2-Chlorophenol 250 04/10/14 DD SW 8270ug/Kg100ND2-Methylnaphthalene 250 04/10/14 DD SW 8270ug/Kg100ND2-Methylphenol (o-cresol) 250 04/10/14 DD SW 8270ug/Kg170ND2-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg360ND2-Nitrophenol 250 04/10/14 DD SW 8270ug/Kg220ND3&4-Methylphenol (m&p-cresol) 250 04/10/14 DD SW 8270ug/Kg 1140ND3,3'-Dichlorobenzidine 700 04/10/14 DD SW 8270ug/Kg170ND3-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg760ND4,6-Dinitro-2-methylphenol 1800 04/10/14 DD SW 8270ug/Kg380ND4-Bromophenyl phenyl ether 250 04/10/14 DD SW 8270ug/Kg100ND4-Chloro-3-methylphenol 250 04/10/14 DD SW 8270ug/Kg120ND4-Chloroaniline 700 04/10/14 DD SW 8270ug/Kg160ND4-Chlorophenyl phenyl ether 250 04/10/14 DD SW 8270ug/Kg120
Page 4 of 6 Ver 2
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg120ND4-Nitrophenol 1800 04/10/14 DD SW 8270ug/Kg160NDAcenaphthene 250 04/10/14 DD SW 8270ug/Kg110NDAcenaphthylene 250 04/10/14 DD SW 8270ug/Kg98NDAcetophenone 250 04/10/14 DD SW 8270ug/Kg110NDAniline 1800 04/10/14 DD SW 8270ug/Kg710NDAnthracene 250 04/10/14 DD SW 8270ug/Kg120NDBenz(a)anthracene 250 04/10/14 DD SW 8270ug/Kg120NDBenzidine 700 04/10/14 DD SW 8270ug/Kg210NDBenzo(a)pyrene 250 04/10/14 DD SW 8270ug/Kg110NDBenzo(b)fluoranthene 250 04/10/14 DD SW 8270ug/Kg120NDBenzo(ghi)perylene 250 04/10/14 DD SW 8270ug/Kg110NDBenzo(k)fluoranthene 250 04/10/14 DD SW 8270ug/Kg120NDBenzoic acid 1800 04/10/14 DD SW 8270ug/Kg 1700NDBenzyl butyl phthalate 250 04/10/14 DD SW 8270ug/Kg91NDBis(2-chloroethoxy)methane 250 04/10/14 DD SW 8270ug/Kg97NDBis(2-chloroethyl)ether 250 04/10/14 DD SW 8270ug/Kg95NDBis(2-chloroisopropyl)ether 250 04/10/14 DD SW 8270ug/Kg 198NDBis(2-ethylhexyl)phthalate 250 04/10/14 DD SW 8270ug/Kg100NDCarbazole 1800 04/10/14 DD SW 8270ug/Kg270NDChrysene 250 04/10/14 DD SW 8270ug/Kg120NDDibenz(a,h)anthracene 250 04/10/14 DD SW 8270ug/Kg110NDDibenzofuran 250 04/10/14 DD SW 8270ug/Kg100NDDiethyl phthalate 250 04/10/14 DD SW 8270ug/Kg110NDDimethylphthalate 250 04/10/14 DD SW 8270ug/Kg110NDDi-n-butylphthalate 250 04/10/14 DD SW 8270ug/Kg94NDDi-n-octylphthalate 250 04/10/14 DD SW 8270ug/Kg91NDFluoranthene 250 04/10/14 DD SW 8270ug/Kg110NDFluorene 250 04/10/14 DD SW 8270ug/Kg120NDHexachlorobenzene 250 04/10/14 DD SW 8270ug/Kg100NDHexachlorobutadiene 250 04/10/14 DD SW 8270ug/Kg130NDHexachlorocyclopentadiene 250 04/10/14 DD SW 8270ug/Kg110NDHexachloroethane 250 04/10/14 DD SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 250 04/10/14 DD SW 8270ug/Kg120NDIsophorone 250 04/10/14 DD SW 8270ug/Kg98NDNaphthalene 250 04/10/14 DD SW 8270ug/Kg100NDNitrobenzene 250 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodimethylamine 250 04/10/14 DD SW 8270ug/Kg99NDN-Nitrosodi-n-propylamine 250 04/10/14 DD SW 8270ug/Kg110NDN-Nitrosodiphenylamine 250 04/10/14 DD SW 8270ug/Kg130NDPentachloronitrobenzene 250 04/10/14 DD SW 8270ug/Kg130NDPentachlorophenol 250 04/10/14 DD SW 8270ug/Kg130NDPhenanthrene 250 04/10/14 DD SW 8270ug/Kg100NDPhenol 250 04/10/14 DD SW 8270ug/Kg110NDPyrene 250 04/10/14 DD SW 8270ug/Kg120NDPyridine 250 04/10/14 DD SW 8270ug/Kg86
QA/QC Surrogates80% 2,4,6-Tribromophenol 04/10/14 DD 30 - 130 %%55% 2-Fluorobiphenyl 04/10/14 DD 30 - 130 %%
Page 5 of 6 Ver 2
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
77% 2-Fluorophenol 04/10/14 DD 30 - 130 %%51% Nitrobenzene-d5 04/10/14 DD 30 - 130 %%82% Phenol-d5 04/10/14 DD 30 - 130 %%56% Terphenyl-d14 04/10/14 DD 30 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorMay 07, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 6 of 6 Ver 2
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
QA/QC ReportMay 07, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG30363
LCS%
DupRPD
LCSD%
LCSRPD
%Rec
Limits
%RPD
LimitsSampleResult
DupResult
QA/QC Batch 271080, QC Sample No: BG30143 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369)
ICP Metals - SoilNC NCAluminum BRL NC11314.7 105 7.3 75 - 125 306310 7310
87.2 88.8Antimony BRL 1.884.5NC 80.6 4.7 75 - 125 301.1 <4.3
89.5 93.2Arsenic BRL 4.198.9NC 94.4 4.7 75 - 125 301.4 1.59
104 109Barium BRL 4.710310.5 97.4 5.6 75 - 125 3017.1 19.0
95.3 98.6Beryllium BRL 3.4103NC 98.6 4.4 75 - 125 300.22 0.22 B
87.8 90.5Cadmium BRL 3.095.1NC 90.2 5.3 75 - 125 30<0.39 <0.43
NC NCCalcium BRL NC1017.30 99.9 1.1 75 - 125 30798 742
97.6 102Chromium BRL 4.41067.50 100 5.8 75 - 125 309.16 9.87
94.4 97.9Cobalt BRL 3.61031.30 97.3 5.7 75 - 125 303.00 2.96
99.7 104Copper BRL 4.21042.10 100 3.9 75 - 125 306.36 6.23
NC NCIron 9.3 NC1212.70 113 6.8 75 - 125 3011100 10800
92.4 95.9Lead BRL 3.798.6NC 95.8 2.9 75 - 125 303.8 4.68
NC NCMagnesium BRL NC1091.50 102 6.6 75 - 125 301310 1330
104 107Manganese BRL 2.810712.1 102 4.8 75 - 125 3065.8 58.3
95.2 98.9Nickel BRL 3.81033.70 98.3 4.7 75 - 125 306.99 7.25
>130 >130Potassium BRL NC1211.70 112 7.7 m75 - 125 30474 466
79.1 83.0Selenium BRL 4.885.8NC 80.9 5.9 75 - 125 30<1.6 <1.7
93.9 97.3Silver BRL 3.6103NC 94.0 9.1 75 - 125 30<0.39 <0.43
NC NCSodium BRL NC1221.70 114 6.8 75 - 125 301140 1160
88.7 92.1Thallium BRL 3.898.1NC 91.1 7.4 75 - 125 30<3.5 <3.8
98.8 104Vanadium BRL 5.11061.80 102 3.8 75 - 125 3016.5 16.2
101 100Zinc BRL 1.098.65.00 93.3 5.5 75 - 125 3018.3 17.4
QA/QC Batch 271124, QC Sample No: BG30354 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369)107 92.5Mercury - Soil BRL 14.598.5NC 97.2 1.3 70 - 130 300.13 0.10
Additional Mercury criteria: LCS acceptance range for waters is 80-120% and for soils is 70-130%.
Comment:
QA/QC Batch 271068, QC Sample No: BG30370 (BG30370)
ICP Metals - SoilNC NCAluminum BRL NC1049.80 103 1.0 75 - 125 303800 4190
91.9 93.3Antimony BRL 1.5113NC 113 0.0 75 - 125 30<1.7 <1.7
88.4 89.6Arsenic BRL 1.394.2NC 92.8 1.5 75 - 125 30<0.7 0.76
101 102Barium BRL 1.010310.2 100 3.0 75 - 125 3021.4 23.7
94.8 95.2Beryllium BRL 0.4101NC 100 1.0 75 - 125 30<0.27 <0.26
87.8 88.1Cadmium BRL 0.395.9NC 94.8 1.2 75 - 125 30<0.33 <0.33
NC NCCalcium BRL NC1097.80 97.3 11.3 75 - 125 303100 3350
96.2 96.8Chromium BRL 0.61045.50 100 3.9 75 - 125 307.78 8.22
93.3 93.9Cobalt BRL 0.699.313.1 98.4 0.9 75 - 125 302.92 3.33
99.0 99.1Copper BRL 0.11051.70 102 2.9 75 - 125 309.10 9.26
NC NCIron 8.4 NC1123.60 110 1.8 75 - 125 309380 9720
90.6 91.6Lead BRL 1.194.9NC 92.6 2.5 75 - 125 302.2 2.94
Page 1 of 8
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
DupRPD
LCSD%
LCSRPD
%Rec
Limits
%RPD
LimitsSampleResult
DupResult
NC NCMagnesium BRL NC10327.0 99.6 3.4 75 - 125 302270 2980
109 94.9Manganese BRL 13.810327.1 101 2.0 75 - 125 30201 264
92.8 93.6Nickel BRL 0.999.84.70 98.2 1.6 75 - 125 307.62 7.27
>130 >130Potassium BRL NC11511.4 112 2.6 m75 - 125 30688 771
77.4 77.7Selenium BRL 0.482.8NC 81.4 1.7 75 - 125 30<1.3 <1.3
92.9 93.3Silver BRL 0.496.4NC 95.1 1.4 75 - 125 30<0.33 <0.33
129 129Sodium BRL 0.0117NC 115 1.7 m75 - 125 30124 117
88.7 89.3Thallium BRL 0.794.6NC 94.9 0.3 75 - 125 30<1.3 <1.3
100 98.0Vanadium BRL 2.010320.8 103 0.0 75 - 125 3012.5 15.4
87.9 89.8Zinc BRL 2.194.817.4 92.8 2.1 75 - 125 3014.7 17.5
QA/QC Batch 271125, QC Sample No: BG30370 (BG30370)104 101Mercury - Soil BRL 2.996.6NC 92.1 4.8 70 - 130 30<0.07 <0.08
Additional Mercury criteria: LCS acceptance range for waters is 80-120% and for soils is 70-130%.
Comment:
m = This parameter is outside laboratory ms/msd specified recovery limits.
Page 2 of 8
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
QA/QC ReportMay 07, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
QA/QC Batch 271077, QC Sample No: BG30355 (BG30363, BG30366, BG30368)
Pesticides - Solid107 834,4' -DDD ND 25.395 108 12.8 40 - 140 30
90 714,4' -DDE ND 23.689 90 1.1 40 - 140 30
82 644,4' -DDT ND 24.784 84 0.0 40 - 140 30
92 87a-BHC ND 5.681 93 13.8 40 - 140 30
93 80a-Chlordane ND 15.092 93 1.1 40 - 140 30
86 69Aldrin ND 21.981 73 10.4 40 - 140 30
98 91b-BHC ND 7.497 94 3.1 40 - 140 30
NA NAChlordane ND NCNA NA NC 40 - 140 30
77 71d-BHC ND 8.181 77 5.1 40 - 140 30
93 82Dieldrin ND 12.686 87 1.2 40 - 140 30
94 86Endosulfan I ND 8.983 91 9.2 40 - 140 30
93 80Endosulfan II ND 15.043 65 40.7 r40 - 140 30
88 79Endosulfan sulfate ND 10.860 65 8.0 40 - 140 30
96 85Endrin ND 12.294 93 1.1 40 - 140 30
85 78Endrin aldehyde ND 8.647 70 39.3 r40 - 140 30
103 95Endrin ketone ND 8.187 86 1.2 40 - 140 30
111 103g-BHC ND 7.594 93 1.1 40 - 140 30
99 82g-Chlordane ND 18.899 97 2.0 40 - 140 30
101 82Heptachlor ND 20.8103 99 4.0 40 - 140 30
103 93Heptachlor epoxide ND 10.292 93 1.1 40 - 140 30
121 102Methoxychlor ND 17.088 89 1.1 40 - 140 30
NA NAToxaphene ND NCNA NA NC 40 - 140 30
83 88% DCBP 93 5.886 95 9.9 30 - 150 30
83 81% TCMX 88 2.486 90 4.5 30 - 150 30
Alpha and gamma chlordane were spiked and analyzed instead of technical chlordane. Gamma chlordane recovery is reported in theLCS, LCSD, MS and MSD.
Comment:
QA/QC Batch 271075, QC Sample No: BG30355 (BG30363, BG30366, BG30368)
Polychlorinated Biphenyls - Solid92 98PCB-1016 ND 6.375 95 23.5 40 - 140 30
PCB-1221 ND 40 - 140 30
PCB-1232 ND 40 - 140 30
PCB-1242 ND 40 - 140 30
PCB-1248 ND 40 - 140 30
PCB-1254 ND 40 - 140 30
92 101PCB-1260 ND 9.399 91 8.4 40 - 140 30
PCB-1262 ND 40 - 140 30
PCB-1268 ND 40 - 140 30
89 87% DCBP (Surrogate Rec) 87 2.3100 90 10.5 30 - 150 30
92 90% TCMX (Surrogate Rec) 81 2.299 92 7.3 30 - 150 30
Page 3 of 8
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
QA/QC Batch 271323, QC Sample No: BG30364 (BG30363, BG30364 (91, 1X) , BG30365, BG30366, BG30367, BG30368, BG30369, BG30370, BG30371 (50X) , BG30372)
Volatiles - Solid101 1041,1,1,2-Tetrachloroethane ND 2.999 101 2.0 70 - 130 30
101 1001,1,1-Trichloroethane ND 1.092 94 2.2 70 - 130 30
92 931,1,2,2-Tetrachloroethane ND 1.190 92 2.2 70 - 130 30
102 951,1,2-Trichloroethane ND 7.195 102 7.1 70 - 130 30
95 971,1-Dichloroethane ND 2.190 97 7.5 70 - 130 30
94 951,1-Dichloroethene ND 1.185 92 7.9 70 - 130 30
100 971,1-Dichloropropene ND 3.092 95 3.2 70 - 130 30
98 981,2,3-Trichlorobenzene ND 0.090 95 5.4 70 - 130 30
95 951,2,3-Trichloropropane ND 0.095 97 2.1 70 - 130 30
96 961,2,4-Trichlorobenzene ND 0.090 94 4.3 70 - 130 30
102 1011,2,4-Trimethylbenzene ND 1.099 102 3.0 70 - 130 30
93 891,2-Dibromo-3-chloropropane ND 4.497 96 1.0 70 - 130 30
101 1011,2-Dibromoethane ND 0.0100 105 4.9 70 - 130 30
99 1001,2-Dichlorobenzene ND 1.092 94 2.2 70 - 130 30
111 1061,2-Dichloroethane ND 4.696 100 4.1 70 - 130 30
95 981,2-Dichloropropane ND 3.193 98 5.2 70 - 130 30
101 1011,3,5-Trimethylbenzene ND 0.096 98 2.1 70 - 130 30
97 981,3-Dichlorobenzene ND 1.093 95 2.1 70 - 130 30
98 1001,3-Dichloropropane ND 2.097 99 2.0 70 - 130 30
99 981,4-Dichlorobenzene ND 1.093 95 2.1 70 - 130 30
94 912,2-Dichloropropane ND 3.289 96 7.6 70 - 130 30
97 972-Chlorotoluene ND 0.090 97 7.5 70 - 130 30
84 892-Hexanone ND 5.8121 127 4.8 70 - 130 30
102 1022-Isopropyltoluene ND 0.096 99 3.1 70 - 130 30
98 1004-Chlorotoluene ND 2.092 98 6.3 70 - 130 30
101 1044-Methyl-2-pentanone ND 2.9127 133 4.6 l70 - 130 30
67 66Acetone ND 1.575 84 11.3 m70 - 130 30
93 93Acrylonitrile ND 0.091 102 11.4 70 - 130 30
97 98Benzene ND 1.094 97 3.1 70 - 130 30
98 99Bromobenzene ND 1.093 94 1.1 70 - 130 30
96 95Bromochloromethane ND 1.095 96 1.0 70 - 130 30
104 102Bromodichloromethane ND 1.994 95 1.1 70 - 130 30
100 101Bromoform ND 1.097 102 5.0 70 - 130 30
80 81Bromomethane ND 1.294 100 6.2 70 - 130 30
87 89Carbon Disulfide ND 2.387 92 5.6 70 - 130 30
100 102Carbon tetrachloride ND 2.094 94 0.0 70 - 130 30
99 99Chlorobenzene ND 0.097 96 1.0 70 - 130 30
82 83Chloroethane ND 1.290 93 3.3 70 - 130 30
102 102Chloroform ND 0.093 98 5.2 70 - 130 30
77 80Chloromethane ND 3.890 95 5.4 70 - 130 30
96 101cis-1,2-Dichloroethene ND 5.189 99 10.6 70 - 130 30
101 101cis-1,3-Dichloropropene ND 0.096 101 5.1 70 - 130 30
101 101Dibromochloromethane ND 0.0100 101 1.0 70 - 130 30
100 103Dibromomethane ND 3.097 99 2.0 70 - 130 30
72 70Dichlorodifluoromethane ND 2.888 92 4.4 70 - 130 30
99 98Ethylbenzene ND 1.097 95 2.1 70 - 130 30
97 101Hexachlorobutadiene ND 4.088 93 5.5 70 - 130 30
99 101Isopropylbenzene ND 2.092 98 6.3 70 - 130 30
100 99m&p-Xylene ND 1.097 98 1.0 70 - 130 30
Page 4 of 8
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
85 88Methyl ethyl ketone ND 3.5105 112 6.5 70 - 130 30
108 106Methyl t-butyl ether (MTBE) ND 1.993 96 3.2 70 - 130 30
90 89Methylene chloride ND 1.186 91 5.6 70 - 130 30
96 99Naphthalene ND 3.198 100 2.0 70 - 130 30
102 101n-Butylbenzene ND 1.098 101 3.0 70 - 130 30
94 95n-Propylbenzene ND 1.196 98 2.1 70 - 130 30
100 105o-Xylene ND 4.995 96 1.0 70 - 130 30
100 101p-Isopropyltoluene ND 1.097 97 0.0 70 - 130 30
97 98sec-Butylbenzene ND 1.091 92 1.1 70 - 130 30
103 104Styrene ND 1.095 97 2.1 70 - 130 30
98 99tert-Butylbenzene ND 1.094 96 2.1 70 - 130 30
98 95Tetrachloroethene ND 3.192 98 6.3 70 - 130 30
97 96Tetrahydrofuran (THF) ND 1.094 101 7.2 70 - 130 30
98 98Toluene ND 0.094 96 2.1 70 - 130 30
94 97trans-1,2-Dichloroethene ND 3.186 92 6.7 70 - 130 30
107 103trans-1,3-Dichloropropene ND 3.894 100 6.2 70 - 130 30
91 92trans-1,4-dichloro-2-butene ND 1.198 100 2.0 70 - 130 30
96 100Trichloroethene ND 4.195 98 3.1 70 - 130 30
62 63Trichlorofluoromethane ND 1.689 95 6.5 m70 - 130 30
99 101Trichlorotrifluoroethane ND 2.093 95 2.1 70 - 130 30
74 76Vinyl chloride ND 2.785 94 10.1 70 - 130 30
102 100% 1,2-dichlorobenzene-d4 102 2.099 97 2.0 70 - 130 30
103 102% Bromofluorobenzene 98 1.0102 100 2.0 70 - 130 30
103 103% Dibromofluoromethane 104 0.099 103 4.0 70 - 130 30
99 98% Toluene-d8 100 1.0101 101 0.0 70 - 130 30
Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.
Comment:
QA/QC Batch 271082, QC Sample No: BG30364 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369, BG30370)
Semivolatiles - Solid84 881,2,4,5-Tetrachlorobenzene ND 4.770 78 10.8 30 - 130 30
80 841,2,4-Trichlorobenzene ND 4.968 76 11.1 30 - 130 30
82 861,2-Dichlorobenzene ND 4.871 79 10.7 30 - 130 30
92 981,2-Diphenylhydrazine ND 6.376 85 11.2 30 - 130 30
80 861,3-Dichlorobenzene ND 7.270 78 10.8 30 - 130 30
81 851,4-Dichlorobenzene ND 4.869 78 12.2 30 - 130 30
100 1022,4,5-Trichlorophenol ND 2.081 91 11.6 30 - 130 30
96 982,4,6-Trichlorophenol ND 2.180 88 9.5 30 - 130 30
77 942,4-Dichlorophenol ND 19.975 84 11.3 30 - 130 30
45 552,4-Dimethylphenol ND 20.045 50 10.5 30 - 130 30
36 272,4-Dinitrophenol ND 28.618 33 58.8 l,m,r30 - 130 30
93 992,4-Dinitrotoluene ND 6.376 87 13.5 30 - 130 30
94 972,6-Dinitrotoluene ND 3.178 87 10.9 30 - 130 30
91 942-Chloronaphthalene ND 3.277 84 8.7 30 - 130 30
86 902-Chlorophenol ND 4.573 82 11.6 30 - 130 30
85 892-Methylnaphthalene ND 4.672 80 10.5 30 - 130 30
80 792-Methylphenol (o-cresol) ND 1.369 77 11.0 30 - 130 30
114 1192-Nitroaniline ND 4.385 103 19.1 30 - 130 30
75 892-Nitrophenol ND 17.169 79 13.5 30 - 130 30
85 903&4-Methylphenol (m&p-cresol) ND 5.772 81 11.8 30 - 130 30
116 1173,3'-Dichlorobenzidine ND 0.9108 115 6.3 30 - 130 30
93 893-Nitroaniline ND 4.480 91 12.9 30 - 130 30
Page 5 of 8
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
96 994,6-Dinitro-2-methylphenol ND 3.152 76 37.5 r30 - 130 30
92 964-Bromophenyl phenyl ether ND 4.379 87 9.6 30 - 130 30
91 984-Chloro-3-methylphenol ND 7.477 87 12.2 30 - 130 30
55 524-Chloroaniline ND 5.654 57 5.4 30 - 130 30
92 944-Chlorophenyl phenyl ether ND 2.275 83 10.1 30 - 130 30
97 994-Nitroaniline ND 2.079 89 11.9 30 - 130 30
103 1034-Nitrophenol ND 0.083 101 19.6 30 - 130 30
86 90Acenaphthene ND 4.572 81 11.8 30 - 130 30
90 92Acenaphthylene ND 2.274 83 11.5 30 - 130 30
88 93Acetophenone ND 5.573 83 12.8 30 - 130 30
81 80Aniline ND 1.273 77 5.3 30 - 130 30
92 96Anthracene ND 4.376 87 13.5 30 - 130 30
93 97Benz(a)anthracene ND 4.278 86 9.8 30 - 130 30
142 135Benzidine ND 5.1174 >200 NC l,m30 - 130 30
81 86Benzo(a)pyrene ND 6.069 77 11.0 30 - 130 30
88 93Benzo(b)fluoranthene ND 5.576 85 11.2 30 - 130 30
93 103Benzo(ghi)perylene ND 10.277 87 12.2 30 - 130 30
92 97Benzo(k)fluoranthene ND 5.374 83 11.5 30 - 130 30
89 98Benzyl butyl phthalate ND 9.683 86 3.6 30 - 130 30
72 87Bis(2-chloroethoxy)methane ND 18.970 76 8.2 30 - 130 30
81 85Bis(2-chloroethyl)ether ND 4.867 76 12.6 30 - 130 30
86 88Bis(2-chloroisopropyl)ether ND 2.370 78 10.8 30 - 130 30
91 99Bis(2-ethylhexyl)phthalate ND 8.483 85 2.4 30 - 130 30
96 99Carbazole ND 3.176 90 16.9 30 - 130 30
92 97Chrysene ND 5.378 87 10.9 30 - 130 30
95 103Dibenz(a,h)anthracene ND 8.178 89 13.2 30 - 130 30
90 95Dibenzofuran ND 5.474 84 12.7 30 - 130 30
92 97Diethyl phthalate ND 5.377 84 8.7 30 - 130 30
90 92Dimethylphthalate ND 2.276 83 8.8 30 - 130 30
89 94Di-n-butylphthalate ND 5.581 86 6.0 30 - 130 30
91 99Di-n-octylphthalate ND 8.481 88 8.3 30 - 130 30
93 96Fluoranthene ND 3.278 87 10.9 30 - 130 30
94 97Fluorene ND 3.176 85 11.2 30 - 130 30
86 93Hexachlorobenzene ND 7.878 84 7.4 30 - 130 30
79 83Hexachlorobutadiene ND 4.969 75 8.3 30 - 130 30
71 70Hexachlorocyclopentadiene ND 1.454 64 16.9 30 - 130 30
80 83Hexachloroethane ND 3.768 76 11.1 30 - 130 30
94 102Indeno(1,2,3-cd)pyrene ND 8.278 87 10.9 30 - 130 30
77 92Isophorone ND 17.874 82 10.3 30 - 130 30
82 87Naphthalene ND 5.970 78 10.8 30 - 130 30
85 88Nitrobenzene ND 3.570 79 12.1 30 - 130 30
83 86N-Nitrosodimethylamine ND 3.669 76 9.7 30 - 130 30
88 92N-Nitrosodi-n-propylamine ND 4.472 81 11.8 30 - 130 30
98 101N-Nitrosodiphenylamine ND 3.080 90 11.8 30 - 130 30
93 96Pentachloronitrobenzene ND 3.280 86 7.2 30 - 130 30
92 93Pentachlorophenol ND 1.160 75 22.2 30 - 130 30
92 97Phenanthrene ND 5.378 87 10.9 30 - 130 30
89 92Phenol ND 3.374 83 11.5 30 - 130 30
94 97Pyrene ND 3.177 89 14.5 30 - 130 30
70 69Pyridine ND 1.462 65 4.7 30 - 130 30
84 92% 2,4,6-Tribromophenol 80 9.175 77 2.6 30 - 130 30
56 57% 2-Fluorobiphenyl 55 1.847 50 6.2 30 - 130 30
78 82% 2-Fluorophenol 81 5.066 71 7.3 30 - 130 30
Page 6 of 8
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
54 55% Nitrobenzene-d5 52 1.844 49 10.8 30 - 130 30
82 85% Phenol-d5 81 3.669 75 8.3 30 - 130 30
64 65% Terphenyl-d14 62 1.653 59 10.7 30 - 130 30
Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)
Comment:
QA/QC Batch 273140, QC Sample No: BG30367 (BG30367)
Pesticides - Solid92 954,4' -DDD ND 3.256 40 - 140 30
96 994,4' -DDE ND 3.189 40 - 140 30
94 984,4' -DDT ND 4.287 40 - 140 30
95 94a-BHC ND 1.182 40 - 140 30
97 97a-Chlordane ND 0.083 40 - 140 30
84 87Aldrin ND 3.579 40 - 140 30
100 98b-BHC ND 2.085 40 - 140 30
92 94Chlordane ND 2.283 40 - 140 30
79 78d-BHC ND 1.367 40 - 140 30
96 97Dieldrin ND 1.086 40 - 140 30
92 94Endosulfan I ND 2.282 40 - 140 30
103 106Endosulfan II ND 2.994 40 - 140 30
73 75Endosulfan sulfate ND 2.759 40 - 140 30
97 97Endrin ND 0.086 40 - 140 30
80 82Endrin aldehyde ND 2.548 40 - 140 30
92 93Endrin ketone ND 1.179 40 - 140 30
94 93g-BHC ND 1.180 40 - 140 30
92 94g-Chlordane ND 2.283 40 - 140 30
88 92Heptachlor ND 4.479 40 - 140 30
96 96Heptachlor epoxide ND 0.085 40 - 140 30
102 106Methoxychlor ND 3.891 40 - 140 30
NA NAToxaphene ND NCNA 40 - 140 30
97 94% DCBP 95 3.194 30 - 150 30
89 86% TCMX 86 3.487 30 - 150 30
Alpha and gamma chlordane were spiked and analyzed instead of technical chlordane. Gamma chlordane recovery is reported in theLCS, MS and MSD.
Comment:
QA/QC Batch 273139, QC Sample No: BG30367 (BG30367)
Polychlorinated Biphenyls - Solid98 82PCB-1016 ND 17.892 85 7.9 40 - 140 30
PCB-1221 ND 40 - 140 30
PCB-1232 ND 40 - 140 30
PCB-1242 ND 40 - 140 30
PCB-1248 ND 40 - 140 30
PCB-1254 ND 40 - 140 30
94 79PCB-1260 ND 17.388 81 8.3 40 - 140 30
PCB-1262 ND 40 - 140 30
PCB-1268 ND 40 - 140 30
101 93% DCBP (Surrogate Rec) 92 8.299 91 8.4 30 - 150 30
100 82% TCMX (Surrogate Rec) 75 19.893 86 7.8 30 - 150 30
QA/QC Batch 271482, QC Sample No: BG30788 (BG30366 (71X) )
Volatiles - Solid99 971,2,3-Trichlorobenzene ND 2.0100 106 5.8 70 - 130 30
Page 7 of 8
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
91 891,2,3-Trichloropropane ND 2.295 98 3.1 70 - 130 30
105 1031,2,4-Trichlorobenzene ND 1.9106 109 2.8 70 - 130 30
100 991,2,4-Trimethylbenzene ND 1.0114 116 1.7 70 - 130 30
94 891,2-Dibromo-3-chloropropane ND 5.594 97 3.1 70 - 130 30
96 971,2-Dichlorobenzene ND 1.0100 103 3.0 70 - 130 30
100 981,3,5-Trimethylbenzene ND 2.0111 111 0.0 70 - 130 30
100 991,3-Dichlorobenzene ND 1.0104 107 2.8 70 - 130 30
98 981,4-Dichlorobenzene ND 0.0103 106 2.9 70 - 130 30
101 1032-Chlorotoluene ND 2.0103 106 2.9 70 - 130 30
104 1022-Isopropyltoluene ND 1.9111 113 1.8 70 - 130 30
100 1004-Chlorotoluene ND 0.0107 108 0.9 70 - 130 30
99 98Bromobenzene ND 1.0100 102 2.0 70 - 130 30
95 96Hexachlorobutadiene ND 1.0103 105 1.9 70 - 130 30
102 101Isopropylbenzene ND 1.0111 111 0.0 70 - 130 30
105 102Naphthalene ND 2.9100 105 4.9 70 - 130 30
103 101n-Butylbenzene ND 2.0118 118 0.0 70 - 130 30
97 97n-Propylbenzene ND 0.0112 116 3.5 70 - 130 30
102 101p-Isopropyltoluene ND 1.0116 114 1.7 70 - 130 30
100 99sec-Butylbenzene ND 1.0107 107 0.0 70 - 130 30
98 98tert-Butylbenzene ND 0.0109 111 1.8 70 - 130 30
100 97trans-1,4-dichloro-2-butene ND 3.0105 108 2.8 70 - 130 30
101 100% 1,2-dichlorobenzene-d4 100 1.098 99 1.0 70 - 130 30
97 97% Bromofluorobenzene 100 0.0106 102 3.8 70 - 130 30
Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.
Comment:
l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.
MS - Matrix SpikePhyllis Shiller, Laboratory Director
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.
May 07, 2014MS Dup - Matrix Spike Duplicate
RPD - Relative Percent Difference
LCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate
NC - No Criteria
Intf - Interference
Page 8 of 8
Sample Criteria Exceedences ReportWednesday, May 07, 2014 Page 1 of 2
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG30363 - EBCCriteria: NY: 375, 375RRS, 375RS
RLCriteria
State: NY
HG-SM Mercury 0.180.55 0.06 mg/KgBG30363 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 6398.7 0.7 mg/KgBG30363 NY / 375-6.8 Metals / Unrestricted Use Soil 63
$8260MADPR Acetone 5068 54 ug/KgBG30366 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8270SMRDP Phenol 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Pentachlorophenol 800ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 800990 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$PCB_SMRDP PCB-1254 100210 36 ug/KgBG30366 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PESTSMDPR 4,4' -DDT 3.324 2.6 ug/KgBG30366 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3HG-SM Mercury 0.180.34 0.06 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 63156 6.7 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SMDP Zinc 109130 0.7 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 109
PB-SMDP Lead 63174 7.7 mg/KgBG30368 NY / 375-6.8 Metals / Unrestricted Use Soil 63
$8260-SMDPR Vinyl chloride 210ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Residential 210$8260-SMDPR trans-1,2-Dichloroethene 190ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 190$8260-SMDPR Methylene chloride 50ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR Methyl Ethyl Ketone 120ND 1500 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260-SMDPR Benzene 60ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260-SMDPR 1,2-Dichloroethane 20ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Vinyl chloride 20ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Acetone 50ND 2500 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50
Sample Criteria Exceedences ReportWednesday, May 07, 2014 Page 2 of 2
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG30363 - EBCCriteria: NY: 375, 375RRS, 375RS
RLCriteria
State: NY
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
NY Temperature NarrationMay 07, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG30363
The samples in this delivery group were received at 4°C.(Note acceptance criteria is above freezing up to 6°C)
Page 1 of 1
1
Sarah - Phoenixlabs
From: Sarah - Phoenixlabs [[email protected]]Sent: Wednesday, April 30, 2014 11:10 AMTo: 'Shannon - Phoenixlabs'Subject: Can you take off hold BG30367Attachments: GBG30363-ChainofCustody-1.pdf
Importance: High
Please run per Dominick BG30367 for PCB and Pest. I will scan to COC
BG31851 - BG31853
Monday, April 21, 2014
Sample ID#s:
Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Project ID: DOMINO SUGAR SITE E
Sincerely yours,
Laboratory DirectorPhyllis Shiller
If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.
NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B
NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
GROUND WATEREBC72 Hour
04/09/14SWsee "By" below
Laboratory Data
E-MW1
Phoenix ID: BG31851
04/11/140:00
17:36
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 21, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG31851
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.005Silver 0.005 04/12/14 LK SW6010mg/L0.00062.43Aluminum 0.010 04/12/14 LK SW6010mg/L0.0024
< 0.004Arsenic - LDL 0.004 04/12/14 LK SW6010mg/L0.0010.126Barium 0.010 04/12/14 LK SW6010mg/L0.0003
< 0.001Beryllium 0.001 04/12/14 LK SW6010mg/L0.001110Calcium 0.010 04/12/14 LK SW6010mg/L0.003
< 0.004Cadmium 0.004 04/12/14 LK SW6010mg/L0.0002< 0.005Cobalt 0.005 04/12/14 LK SW6010mg/L0.00030.004Chromium 0.001 04/12/14 LK SW6010mg/L0.00090.007Copper 0.005 04/12/14 LK SW6010mg/L0.001
< 0.005Silver (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.00060.90Aluminum (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.0026
< 0.003Arsenic, (Dissolved) 0.003 04/12/14 LK SW6010mg/L0.0010.120Barium (Dissolved) 0.011 04/12/14 LK SW6010mg/L0.0003
< 0.001Beryllium (Dissolved) 0.001 04/12/14 LK SW6010mg/L0.001112Calcium (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.003
< 0.004Cadmium (Dissolved) 0.004 04/12/14 LK SW6010mg/L0.0002< 0.005Cobalt, (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.00030.001Chromium (Dissolved) 0.001 04/12/14 LK SW6010mg/L0.0010
< 0.005Copper, (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.0010.88Iron, (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.005
< 0.0002Mercury (Dissolved) 0.0002 04/14/14 RS SW7470mg/L0.0001513.6Potassium (Dissolved) 0.1 04/12/14 LK SW6010mg/L0.131.6Magnesium (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.0012.89Manganese, (Dissolved) 0.053 04/12/14 LK SW6010mg/L0.011255Sodium (Dissolved) 1.1 04/12/14 LK SW6010mg/L1.1
0.012Nickel, (Dissolved) 0.004 04/12/14 LK SW6010mg/L0.0005< 0.002Lead (Dissolved) 0.002 04/12/14 LK SW6010mg/L0.001
Page 1 of 15 Ver 1
E-MW1Phoenix I.D.: BG31851
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
< 0.003Antimony, (Dissolved) 0.003 04/15/14 RS 7010mg/L0.003< 0.004Selenium, (Dissolved) 0.004 04/14/14 E/R 7010mg/L0.002< 0.001Thallium , (Dissolved) 0.001 04/12/14 TH 7010mg/L0.001< 0.01Vanadium, (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.001< 0.011Zinc, (Dissolved) 0.011 04/12/14 LK SW6010mg/L0.001
2.89Iron 0.01 04/12/14 LK SW6010mg/L0.005< 0.0002Mercury 0.0002 04/14/14 RS SW7470mg/L0.00015
12.9Potassium 0.1 04/12/14 LK SW6010mg/L0.131.2Magnesium 0.01 04/12/14 LK SW6010mg/L0.0012.65Manganese 0.050 04/12/14 LK SW6010mg/L0.010237Sodium 1.0 04/12/14 LK SW6010mg/L1.0
0.014Nickel 0.004 04/12/14 LK SW6010mg/L0.0005< 0.002Lead 0.002 04/12/14 LK SW6010mg/L0.001< 0.003Antimony 0.003 04/15/14 RS 7010mg/L0.0020.009Selenium 0.004 04/16/14 RS 7010mg/L0.002
< 0.002Thallium - LDL 0.002 04/16/14 RS 7010mg/L0.001< 0.010Vanadium 0.010 04/12/14 LK SW6010mg/L0.001< 0.010Zinc 0.010 04/12/14 LK SW6010mg/L0.001
CompletedFiltration 04/11/14 AG 0.45um Filter
CompletedDissolved Mercury Digestion 04/14/14 I/I SW7470CompletedMercury Digestion 04/14/14 I/I SW7470CompletedSemi-Volatile Extraction 04/11/14 e/D/D SW3520CompletedDissolved Metals Preparation 04/11/14 AG SW846-3005CompletedTotal Metals Digestion 04/11/14 AG SW846 - 3050
VolatilesND1,1,1,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.19ND1,1,1-Trichloroethane 5.0 04/12/14 RM SW8260ug/L0.19ND1,1,2,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.15ND1,1,2-Trichloroethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,1-Dichloroethane 5.0 04/12/14 RM SW8260ug/L0.23ND1,1-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.24ND1,1-Dichloropropene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichloropropane 1.0 04/12/14 RM SW8260ug/L0.21ND1,2,4-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2,4-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2-Dibromo-3-chloropropane 1.0 04/12/14 RM SW8260ug/L0.36ND1,2-Dibromoethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.16ND1,2-Dichloroethane 2.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.18ND1,3,5-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.21ND1,3-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND1,3-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.22ND1,4-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND2,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.16ND2-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.23ND2-Hexanone 1.0 04/12/14 RM SW8260ug/L0.27ND2-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L 10.21
Page 2 of 15 Ver 1
E-MW1Phoenix I.D.: BG31851
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.16ND4-Methyl-2-pentanone 1.0 04/12/14 RM SW8260ug/L0.19NDAcetone 5.0 04/12/14 RM SW8260ug/L0.31NDAcrolein 5.0 04/12/14 RM SW8260ug/L0.95NDAcrylonitrile 5.0 04/12/14 RM SW8260ug/L0.17NDBenzene 0.70 04/12/14 RM SW8260ug/L0.19NDBromobenzene 1.0 04/12/14 RM SW8260ug/L0.20NDBromochloromethane 1.0 04/12/14 RM SW8260ug/L0.22NDBromodichloromethane 1.0 04/12/14 RM SW8260ug/L0.16NDBromoform 5.0 04/12/14 RM SW8260ug/L0.10NDBromomethane 5.0 04/12/14 RM SW8260ug/L0.25NDCarbon Disulfide 1.0 04/12/14 RM SW8260ug/L0.24NDCarbon tetrachloride 1.0 04/12/14 RM SW8260ug/L0.23NDChlorobenzene 5.0 04/12/14 RM SW8260ug/L0.20NDChloroethane 5.0 04/12/14 RM SW8260ug/L0.24NDChloroform 5.0 04/12/14 RM SW8260ug/L0.22NDChloromethane 5.0 04/12/14 RM SW8260ug/L0.214.7cis-1,2-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.23NDcis-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.15NDDibromochloromethane 1.0 04/12/14 RM SW8260ug/L0.15NDDibromomethane 1.0 04/12/14 RM SW8260ug/L0.23NDDichlorodifluoromethane 1.0 04/12/14 RM SW8260ug/L0.26NDEthylbenzene 1.0 04/12/14 RM SW8260ug/L0.19NDHexachlorobutadiene 1.0 04/12/14 RM SW8260ug/L0.13NDIsopropylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDm&p-Xylene 1.0 04/12/14 RM SW8260ug/L0.42NDMethyl ethyl ketone 1.0 04/12/14 RM SW8260ug/L0.50NDMethyl t-butyl ether (MTBE) 1.0 04/12/14 RM SW8260ug/L0.19NDMethylene chloride 3.0 04/12/14 RM SW8260ug/L0.16NDNaphthalene 1.0 04/12/14 RM SW8260ug/L0.19NDn-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDn-Propylbenzene 1.0 04/12/14 RM SW8260ug/L0.20NDo-Xylene 1.0 04/12/14 RM SW8260ug/L0.45NDp-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L0.21NDsec-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDStyrene 1.0 04/12/14 RM SW8260ug/L0.41NDtert-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.234.7Tetrachloroethene 1.0 04/12/14 RM SW8260ug/L0.24NDTetrahydrofuran (THF) 5.0 04/12/14 RM SW8260ug/L 10.51NDToluene 1.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,2-Dichloroethene 5.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.14NDtrans-1,4-dichloro-2-butene 1.0 04/12/14 RM SW8260ug/L0.4524Trichloroethene 1.0 04/12/14 RM SW8260ug/L0.18NDTrichlorofluoromethane 1.0 04/12/14 RM SW8260ug/L0.23NDTrichlorotrifluoroethane 1.0 04/12/14 RM SW8260ug/L0.23NDVinyl chloride 1.0 04/12/14 RM SW8260ug/L0.14
QA/QC Surrogates98% 1,2-dichlorobenzene-d4 04/12/14 RM 70 - 130 %%
Page 3 of 15 Ver 1
E-MW1Phoenix I.D.: BG31851
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
102% Bromofluorobenzene 04/12/14 RM 70 - 130 %%95% Dibromofluoromethane 04/12/14 RM 70 - 130 %%98% Toluene-d8 04/12/14 RM 70 - 130 %%
SemivolatilesND1,2,4-Trichlorobenzene 5.0 04/16/14 DD SW 8270ug/L1.5ND1,2-Dichlorobenzene 1.0 04/16/14 DD SW 8270ug/L1.4ND1,2-Diphenylhydrazine 5.0 04/16/14 DD SW 8270ug/L1.6ND1,3-Dichlorobenzene 1.0 04/16/14 DD SW 8270ug/L1.5ND1,4-Dichlorobenzene 1.0 04/16/14 DD SW 8270ug/L1.5ND2,4,5-Trichlorophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2,4,6-Trichlorophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2,4-Dichlorophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2,4-Dimethylphenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2,4-Dinitrophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2,4-Dinitrotoluene 5.0 04/16/14 DD SW 8270ug/L2.0ND2,6-Dinitrotoluene 5.0 04/16/14 DD SW 8270ug/L1.6ND2-Chloronaphthalene 5.0 04/16/14 DD SW 8270ug/L1.4ND2-Chlorophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2-Methylnaphthalene 5.0 04/16/14 DD SW 8270ug/L1.5ND2-Methylphenol (o-cresol) 1.0 04/16/14 DD SW 8270ug/L1.0ND2-Nitroaniline 5.0 04/16/14 DD SW 8270ug/L5.0ND2-Nitrophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND3&4-Methylphenol (m&p-cresol) 1.0 04/16/14 DD SW 8270ug/L1.0ND3,3'-Dichlorobenzidine 5.0 04/16/14 DD SW 8270ug/L2.4ND3-Nitroaniline 5.0 04/16/14 DD SW 8270ug/L5.0ND4,6-Dinitro-2-methylphenol 1.0 04/16/14 DD SW 8270ug/L1.0ND4-Bromophenyl phenyl ether 5.0 04/16/14 DD SW 8270ug/L1.5ND4-Chloro-3-methylphenol 1.0 04/16/14 DD SW 8270ug/L1.0ND4-Chloroaniline 3.5 04/16/14 DD SW 8270ug/L2.3ND4-Chlorophenyl phenyl ether 5.0 04/16/14 DD SW 8270ug/L1.7ND4-Nitroaniline 5.0 04/16/14 DD SW 8270ug/L1.7ND4-Nitrophenol 1.0 04/16/14 DD SW 8270ug/L1.0NDAcenaphthene 5.0 04/16/14 DD SW 8270ug/L1.5NDAcetophenone 5.0 04/16/14 DD SW 8270ug/L1.6NDAniline 3.5 04/16/14 DD SW 8270ug/L5.0NDAnthracene 5.0 04/16/14 DD SW 8270ug/L1.6NDBenzidine 10 04/16/14 DD SW 8270ug/L2.9NDBenzoic acid 25 04/16/14 DD SW 8270ug/L10NDBenzyl butyl phthalate 5.0 04/16/14 DD SW 8270ug/L1.3NDBis(2-chloroethoxy)methane 5.0 04/16/14 DD SW 8270ug/L1.4NDBis(2-chloroethyl)ether 1.0 04/16/14 DD SW 8270ug/L1.0NDBis(2-chloroisopropyl)ether 5.0 04/16/14 DD SW 8270ug/L1.4NDCarbazole 25 04/16/14 DD SW 8270ug/L3.8NDDibenzofuran 5.0 04/16/14 DD SW 8270ug/L1.5NDDiethyl phthalate 5.0 04/16/14 DD SW 8270ug/L1.6NDDimethylphthalate 5.0 04/16/14 DD SW 8270ug/L1.6NDDi-n-butylphthalate 5.0 04/16/14 DD SW 8270ug/L1.3NDDi-n-octylphthalate 5.0 04/16/14 DD SW 8270ug/L1.3NDFluoranthene 5.0 04/16/14 DD SW 8270ug/L1.6
Page 4 of 15 Ver 1
E-MW1Phoenix I.D.: BG31851
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDFluorene 5.0 04/16/14 DD SW 8270ug/L1.7NDHexachlorobutadiene 1.0 04/16/14 DD SW 8270ug/L1.8NDHexachlorocyclopentadiene 5.0 04/16/14 DD SW 8270ug/L1.5NDIsophorone 5.0 04/16/14 DD SW 8270ug/L1.4NDNaphthalene 5.0 04/16/14 DD SW 8270ug/L1.4NDNitrobenzene 1.0 04/16/14 DD SW 8270ug/L1.8NDN-Nitrosodimethylamine 1.0 04/16/14 DD SW 8270ug/L1.0NDN-Nitrosodi-n-propylamine 5.0 04/16/14 DD SW 8270ug/L1.6NDN-Nitrosodiphenylamine 5.0 04/16/14 DD SW 8270ug/L1.9NDPhenol 1.0 04/16/14 DD SW 8270ug/L1.6NDPyrene 5.0 04/16/14 DD SW 8270ug/L1.7NDPyridine 10 04/16/14 DD SW 8270ug/L1.2
QA/QC Surrogates90% 2,4,6-Tribromophenol 04/16/14 DD 15 - 110 %%78% 2-Fluorobiphenyl 04/16/14 DD 30 - 130 %%48% 2-Fluorophenol 04/16/14 DD 15 - 110 %%82% Nitrobenzene-d5 04/16/14 DD 30 - 130 %%47% Phenol-d5 04/16/14 DD 15 - 110 %%64% Terphenyl-d14 04/16/14 DD 30 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 1.5 04/15/14 DD SW8270 (SIM)ug/L1.5NDAcenaphthylene 0.10 04/15/14 DD SW8270 (SIM)ug/L0.100.03Benz(a)anthracene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDBenzo(a)pyrene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDBenzo(b)fluoranthene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDBenzo(ghi)perylene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDBenzo(k)fluoranthene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDBis(2-ethylhexyl)phthalate 1.6 04/15/14 DD SW8270 (SIM)ug/L1.40.03Chrysene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDDibenz(a,h)anthracene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDHexachlorobenzene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDHexachloroethane 2.4 04/15/14 DD SW8270 (SIM)ug/L1.5NDIndeno(1,2,3-cd)pyrene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDPentachloronitrobenzene 0.10 04/15/14 DD SW8270 (SIM)ug/L0.10NDPentachlorophenol 0.80 04/15/14 DD SW8270 (SIM)ug/L0.80NDPhenanthrene 0.10 04/15/14 DD SW8270 (SIM)ug/L0.10
QA/QC Surrogates104% 2,4,6-Tribromophenol 04/15/14 DD 15 - 110 %%73% 2-Fluorobiphenyl 04/15/14 DD 30 - 130 %%57% 2-Fluorophenol 04/15/14 DD 15 - 110 %%82% Nitrobenzene-d5 04/15/14 DD 30 - 130 %%58% Phenol-d5 04/15/14 DD 15 - 110 %%63% Terphenyl-d14 04/15/14 DD 30 - 130 %%
Page 5 of 15 Ver 1
E-MW1Phoenix I.D.: BG31851
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Phyllis Shiller, Laboratory DirectorApril 21, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Bobbi Aloisa, Vice President
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 6 of 15 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
GROUND WATEREBC72 Hour
04/09/14SWsee "By" below
Laboratory Data
E-MW2
Phoenix ID: BG31852
04/11/140:00
17:36
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 21, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG31851
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.005Silver 0.005 04/12/14 LK SW6010mg/L0.00063.68Aluminum 0.010 04/12/14 LK SW6010mg/L0.0024
< 0.004Arsenic - LDL 0.004 04/12/14 LK SW6010mg/L0.0010.128Barium 0.010 04/12/14 LK SW6010mg/L0.0003
< 0.001Beryllium 0.001 04/12/14 LK SW6010mg/L0.001124Calcium 0.010 04/12/14 LK SW6010mg/L0.003
< 0.004Cadmium 0.004 04/12/14 LK SW6010mg/L0.0002< 0.005Cobalt 0.005 04/12/14 LK SW6010mg/L0.00030.008Chromium 0.001 04/12/14 LK SW6010mg/L0.00090.014Copper 0.005 04/12/14 LK SW6010mg/L0.001
< 0.005Silver (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.00060.39Aluminum (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.0026
< 0.003Arsenic, (Dissolved) 0.003 04/12/14 LK SW6010mg/L0.0010.100Barium (Dissolved) 0.011 04/12/14 LK SW6010mg/L0.0003
< 0.001Beryllium (Dissolved) 0.001 04/12/14 LK SW6010mg/L0.001124Calcium (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.003
< 0.004Cadmium (Dissolved) 0.004 04/12/14 LK SW6010mg/L0.0002< 0.005Cobalt, (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.0003< 0.001Chromium (Dissolved) 0.001 04/12/14 LK SW6010mg/L0.0010< 0.005Copper, (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.001
0.18Iron, (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.005< 0.0002Mercury (Dissolved) 0.0002 04/14/14 RS SW7470mg/L0.00015
13.1Potassium (Dissolved) 0.1 04/12/14 LK SW6010mg/L0.130.9Magnesium (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.0010.137Manganese, (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.001247Sodium (Dissolved) 1.1 04/12/14 LK SW6010mg/L1.1
< 0.004Nickel, (Dissolved) 0.004 04/12/14 LK SW6010mg/L0.0005< 0.002Lead (Dissolved) 0.002 04/12/14 LK SW6010mg/L0.001
Page 7 of 15 Ver 1
E-MW2Phoenix I.D.: BG31852
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
< 0.003Antimony, (Dissolved) 0.003 04/15/14 RS 7010mg/L0.0030.006Selenium, (Dissolved) 0.004 04/14/14 E/R 7010mg/L0.002
< 0.001Thallium , (Dissolved) 0.001 04/12/14 TH 7010mg/L0.001< 0.01Vanadium, (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.001< 0.011Zinc, (Dissolved) 0.011 04/12/14 LK SW6010mg/L0.001
3.89Iron 0.01 04/12/14 LK SW6010mg/L0.005< 0.0002Mercury 0.0002 04/14/14 RS SW7470mg/L0.00015
11.8Potassium 0.1 04/12/14 LK SW6010mg/L0.130.9Magnesium 0.01 04/12/14 LK SW6010mg/L0.0010.229Manganese 0.005 04/12/14 LK SW6010mg/L0.001249Sodium 1.0 04/12/14 LK SW6010mg/L1.0
0.005Nickel 0.004 04/12/14 LK SW6010mg/L0.00050.031Lead 0.002 04/12/14 LK SW6010mg/L0.001
< 0.003Antimony 0.003 04/15/14 RS 7010mg/L0.0020.007Selenium 0.004 04/15/14 E/R 7010mg/L0.001
< 0.002Thallium - LDL 0.002 04/16/14 RS 7010mg/L0.001< 0.010Vanadium 0.010 04/12/14 LK SW6010mg/L0.0010.031Zinc 0.010 04/12/14 LK SW6010mg/L0.001
CompletedFiltration 04/11/14 AG 0.45um Filter
CompletedDissolved Mercury Digestion 04/14/14 I/I SW7470CompletedMercury Digestion 04/14/14 I/I SW7470CompletedSemi-Volatile Extraction 04/16/14 E/K SW3520CompletedDissolved Metals Preparation 04/11/14 AG SW846-3005CompletedTotal Metals Digestion 04/11/14 AG SW846 - 3050
VolatilesND1,1,1,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.19ND1,1,1-Trichloroethane 5.0 04/12/14 RM SW8260ug/L0.19ND1,1,2,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.15ND1,1,2-Trichloroethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,1-Dichloroethane 5.0 04/12/14 RM SW8260ug/L0.23ND1,1-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.24ND1,1-Dichloropropene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichloropropane 1.0 04/12/14 RM SW8260ug/L0.21ND1,2,4-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2,4-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2-Dibromo-3-chloropropane 1.0 04/12/14 RM SW8260ug/L0.36ND1,2-Dibromoethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.16ND1,2-Dichloroethane 2.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.18ND1,3,5-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.21ND1,3-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND1,3-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.22ND1,4-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND2,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.16ND2-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.23ND2-Hexanone 1.0 04/12/14 RM SW8260ug/L0.27ND2-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L 10.21
Page 8 of 15 Ver 1
E-MW2Phoenix I.D.: BG31852
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.16ND4-Methyl-2-pentanone 1.0 04/12/14 RM SW8260ug/L0.19NDAcetone 5.0 04/12/14 RM SW8260ug/L0.31NDAcrolein 5.0 04/12/14 RM SW8260ug/L0.95NDAcrylonitrile 5.0 04/12/14 RM SW8260ug/L0.17NDBenzene 0.70 04/12/14 RM SW8260ug/L0.19NDBromobenzene 1.0 04/12/14 RM SW8260ug/L0.20NDBromochloromethane 1.0 04/12/14 RM SW8260ug/L0.22NDBromodichloromethane 1.0 04/12/14 RM SW8260ug/L0.16NDBromoform 5.0 04/12/14 RM SW8260ug/L0.10NDBromomethane 5.0 04/12/14 RM SW8260ug/L0.25NDCarbon Disulfide 1.0 04/12/14 RM SW8260ug/L0.24NDCarbon tetrachloride 1.0 04/12/14 RM SW8260ug/L0.23NDChlorobenzene 5.0 04/12/14 RM SW8260ug/L0.20NDChloroethane 5.0 04/12/14 RM SW8260ug/L0.24NDChloroform 5.0 04/12/14 RM SW8260ug/L0.22NDChloromethane 5.0 04/12/14 RM SW8260ug/L0.213.6cis-1,2-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.23NDcis-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.15NDDibromochloromethane 1.0 04/12/14 RM SW8260ug/L0.15NDDibromomethane 1.0 04/12/14 RM SW8260ug/L0.23NDDichlorodifluoromethane 1.0 04/12/14 RM SW8260ug/L0.26NDEthylbenzene 1.0 04/12/14 RM SW8260ug/L0.19NDHexachlorobutadiene 1.0 04/12/14 RM SW8260ug/L0.13NDIsopropylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDm&p-Xylene 1.0 04/12/14 RM SW8260ug/L0.42NDMethyl ethyl ketone 1.0 04/12/14 RM SW8260ug/L0.50NDMethyl t-butyl ether (MTBE) 1.0 04/12/14 RM SW8260ug/L0.19NDMethylene chloride 3.0 04/12/14 RM SW8260ug/L0.16NDNaphthalene 1.0 04/12/14 RM SW8260ug/L0.19NDn-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDn-Propylbenzene 1.0 04/12/14 RM SW8260ug/L0.20NDo-Xylene 1.0 04/12/14 RM SW8260ug/L0.45NDp-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L0.21NDsec-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDStyrene 1.0 04/12/14 RM SW8260ug/L0.41NDtert-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.233.6Tetrachloroethene 1.0 04/12/14 RM SW8260ug/L0.24NDTetrahydrofuran (THF) 5.0 04/12/14 RM SW8260ug/L 10.51NDToluene 1.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,2-Dichloroethene 5.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.14NDtrans-1,4-dichloro-2-butene 1.0 04/12/14 RM SW8260ug/L0.4520Trichloroethene 1.0 04/12/14 RM SW8260ug/L0.18NDTrichlorofluoromethane 1.0 04/12/14 RM SW8260ug/L0.23NDTrichlorotrifluoroethane 1.0 04/12/14 RM SW8260ug/L0.23NDVinyl chloride 1.0 04/12/14 RM SW8260ug/L0.14
QA/QC Surrogates99% 1,2-dichlorobenzene-d4 04/12/14 RM 70 - 130 %%
Page 9 of 15 Ver 1
E-MW2Phoenix I.D.: BG31852
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
98% Bromofluorobenzene 04/12/14 RM 70 - 130 %%96% Dibromofluoromethane 04/12/14 RM 70 - 130 %%101% Toluene-d8 04/12/14 RM 70 - 130 %%
SemivolatilesND1,2,4-Trichlorobenzene 6.3 04/17/14 DD SW 8270ug/L1.9ND1,2-Dichlorobenzene 1.3 04/17/14 DD SW 8270ug/L1.8ND1,2-Diphenylhydrazine 6.3 04/17/14 DD SW 8270ug/L2.0ND1,3-Dichlorobenzene 1.3 04/17/14 DD SW 8270ug/L1.9ND1,4-Dichlorobenzene 1.3 04/17/14 DD SW 8270ug/L1.9ND2,4,5-Trichlorophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2,4,6-Trichlorophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2,4-Dichlorophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2,4-Dimethylphenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2,4-Dinitrophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2,4-Dinitrotoluene 6.3 04/17/14 DD SW 8270ug/L2.5ND2,6-Dinitrotoluene 6.3 04/17/14 DD SW 8270ug/L2.0ND2-Chloronaphthalene 6.3 04/17/14 DD SW 8270ug/L1.8ND2-Chlorophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2-Methylnaphthalene 6.3 04/17/14 DD SW 8270ug/L1.9ND2-Methylphenol (o-cresol) 1.3 04/17/14 DD SW 8270ug/L1.3ND2-Nitroaniline 6.3 04/17/14 DD SW 8270ug/L6.3ND2-Nitrophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND3&4-Methylphenol (m&p-cresol) 1.3 04/17/14 DD SW 8270ug/L1.3ND3,3'-Dichlorobenzidine 6.3 04/17/14 DD SW 8270ug/L3.0ND3-Nitroaniline 6.3 04/17/14 DD SW 8270ug/L6.3ND4,6-Dinitro-2-methylphenol 1.3 04/17/14 DD SW 8270ug/L1.3ND4-Bromophenyl phenyl ether 6.3 04/17/14 DD SW 8270ug/L1.8ND4-Chloro-3-methylphenol 1.3 04/17/14 DD SW 8270ug/L1.3ND4-Chloroaniline 4.4 04/17/14 DD SW 8270ug/L2.9ND4-Chlorophenyl phenyl ether 6.3 04/17/14 DD SW 8270ug/L2.1ND4-Nitroaniline 6.3 04/17/14 DD SW 8270ug/L2.1ND4-Nitrophenol 1.3 04/17/14 DD SW 8270ug/L1.3NDAcenaphthene 6.3 04/17/14 DD SW 8270ug/L1.9NDAcetophenone 6.3 04/17/14 DD SW 8270ug/L2.0NDAniline 4.4 04/17/14 DD SW 8270ug/L6.3NDAnthracene 6.3 04/17/14 DD SW 8270ug/L2.1NDBenzidine 5.6 04/17/14 DD SW 8270ug/L3.7NDBenzoic acid 31 04/17/14 DD SW 8270ug/L13NDBenzyl butyl phthalate 6.3 04/17/14 DD SW 8270ug/L1.6NDBis(2-chloroethoxy)methane 6.3 04/17/14 DD SW 8270ug/L1.7NDBis(2-chloroethyl)ether 1.3 04/17/14 DD SW 8270ug/L1.3NDBis(2-chloroisopropyl)ether 6.3 04/17/14 DD SW 8270ug/L1.7NDCarbazole 31 04/17/14 DD SW 8270ug/L4.7NDDibenzofuran 6.3 04/17/14 DD SW 8270ug/L1.8NDDiethyl phthalate 6.3 04/17/14 DD SW 8270ug/L2.0NDDimethylphthalate 6.3 04/17/14 DD SW 8270ug/L1.9NDDi-n-butylphthalate 6.3 04/17/14 DD SW 8270ug/L1.7NDDi-n-octylphthalate 6.3 04/17/14 DD SW 8270ug/L1.6NDFluoranthene 6.3 04/17/14 DD SW 8270ug/L2.0
Page 10 of 15 Ver 1
E-MW2Phoenix I.D.: BG31852
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDFluorene 6.3 04/17/14 DD SW 8270ug/L2.1NDHexachlorocyclopentadiene 6.3 04/17/14 DD SW 8270ug/L1.9NDIsophorone 6.3 04/17/14 DD SW 8270ug/L1.8NDNaphthalene 6.3 04/17/14 DD SW 8270ug/L1.8NDN-Nitrosodimethylamine 1.3 04/17/14 DD SW 8270ug/L1.3NDN-Nitrosodi-n-propylamine 6.3 04/17/14 DD SW 8270ug/L2.0NDN-Nitrosodiphenylamine 6.3 04/17/14 DD SW 8270ug/L2.4NDPhenol 1.3 04/17/14 DD SW 8270ug/L2.0NDPyrene 6.3 04/17/14 DD SW 8270ug/L2.2NDPyridine 13 04/17/14 DD SW 8270ug/L1.5
QA/QC Surrogates86% 2,4,6-Tribromophenol 04/17/14 DD 15 - 110 %%88% 2-Fluorobiphenyl 04/17/14 DD 30 - 130 %%33% 2-Fluorophenol 04/17/14 DD 15 - 110 %%89% Nitrobenzene-d5 04/17/14 DD 30 - 130 %%33% Phenol-d5 04/17/14 DD 15 - 110 %%91% Terphenyl-d14 04/17/14 DD 30 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 1.9 04/17/14 DD SW8270 (SIM)ug/LNDAcenaphthylene 0.13 04/17/14 DD SW8270 (SIM)ug/L0.19Benz(a)anthracene 0.03 04/17/14 DD SW8270 (SIM)ug/LNDBenzo(a)pyrene 0.03 04/17/14 DD SW8270 (SIM)ug/L0.29Benzo(b)fluoranthene 0.03 04/17/14 DD SW8270 (SIM)ug/LNDBenzo(ghi)perylene 0.03 04/17/14 DD SW8270 (SIM)ug/L0.08Benzo(k)fluoranthene 0.03 04/17/14 DD SW8270 (SIM)ug/L4.1Bis(2-ethylhexyl)phthalate 2.0 04/17/14 DD SW8270 (SIM)ug/L
0.29Chrysene 0.03 04/17/14 DD SW8270 (SIM)ug/L0.04Dibenz(a,h)anthracene 0.03 04/17/14 DD SW8270 (SIM)ug/LNDHexachlorobenzene 0.03 04/17/14 DD SW8270 (SIM)ug/LNDHexachlorobutadiene 0 04/17/14 DD SW8270 (SIM)ug/LNDHexachloroethane 3.0 04/17/14 DD SW8270 (SIM)ug/L0.05Indeno(1,2,3-cd)pyrene 0 04/17/14 DD SW8270 (SIM)ug/LNDNitrobenzene 0.04 04/17/14 DD SW8270 (SIM)ug/LNDPentachloronitrobenzene 0.13 04/17/14 DD SW8270 (SIM)ug/LNDPentachlorophenol 1.0 04/17/14 DD SW8270 (SIM)ug/L0.49Phenanthrene 0.13 04/17/14 DD SW8270 (SIM)ug/L
QA/QC Surrogates108% 2,4,6-Tribromophenol 04/17/14 DD 15 - 110 %%77% 2-Fluorobiphenyl 04/17/14 DD 30 - 130 %%40% 2-Fluorophenol 04/17/14 DD 15 - 110 %%97% Nitrobenzene-d5 04/17/14 DD 30 - 130 %%43% Phenol-d5 04/17/14 DD 15 - 110 %%76% Terphenyl-d14 04/17/14 DD 30 - 130 %%
Page 11 of 15 Ver 1
E-MW2Phoenix I.D.: BG31852
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Phyllis Shiller, Laboratory DirectorApril 21, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Bobbi Aloisa, Vice President
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 12 of 15 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
GROUND WATEREBC72 Hour
04/09/14SWsee "By" below
Laboratory Data
TRIP BLANK
Phoenix ID: BG31853
04/11/140:00
17:36
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 21, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG31851
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.19ND1,1,1-Trichloroethane 5.0 04/12/14 RM SW8260ug/L0.19ND1,1,2,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.15ND1,1,2-Trichloroethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,1-Dichloroethane 5.0 04/12/14 RM SW8260ug/L0.23ND1,1-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.24ND1,1-Dichloropropene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichloropropane 1.0 04/12/14 RM SW8260ug/L0.21ND1,2,4-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2,4-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2-Dibromo-3-chloropropane 1.0 04/12/14 RM SW8260ug/L0.36ND1,2-Dibromoethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.16ND1,2-Dichloroethane 2.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.18ND1,3,5-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.21ND1,3-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND1,3-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.22ND1,4-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND2,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.16ND2-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.23ND2-Hexanone 1.0 04/12/14 RM SW8260ug/L0.27ND2-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L 10.21ND4-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.16ND4-Methyl-2-pentanone 1.0 04/12/14 RM SW8260ug/L0.19
Page 13 of 15 Ver 1
TRIP BLANKPhoenix I.D.: BG31853
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDAcetone 5.0 04/12/14 RM SW8260ug/L0.31NDAcrolein 5.0 04/12/14 RM SW8260ug/L0.95NDAcrylonitrile 5.0 04/12/14 RM SW8260ug/L0.17NDBenzene 0.70 04/12/14 RM SW8260ug/L0.19NDBromobenzene 1.0 04/12/14 RM SW8260ug/L0.20NDBromochloromethane 1.0 04/12/14 RM SW8260ug/L0.22NDBromodichloromethane 1.0 04/12/14 RM SW8260ug/L0.16NDBromoform 5.0 04/12/14 RM SW8260ug/L0.10NDBromomethane 5.0 04/12/14 RM SW8260ug/L0.25NDCarbon Disulfide 1.0 04/12/14 RM SW8260ug/L0.24NDCarbon tetrachloride 1.0 04/12/14 RM SW8260ug/L0.23NDChlorobenzene 5.0 04/12/14 RM SW8260ug/L0.20NDChloroethane 5.0 04/12/14 RM SW8260ug/L0.24NDChloroform 5.0 04/12/14 RM SW8260ug/L0.22NDChloromethane 5.0 04/12/14 RM SW8260ug/L0.21NDcis-1,2-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.23NDcis-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.15NDDibromochloromethane 1.0 04/12/14 RM SW8260ug/L0.15NDDibromomethane 1.0 04/12/14 RM SW8260ug/L0.23NDDichlorodifluoromethane 1.0 04/12/14 RM SW8260ug/L0.26NDEthylbenzene 1.0 04/12/14 RM SW8260ug/L0.19NDHexachlorobutadiene 1.0 04/12/14 RM SW8260ug/L0.13NDIsopropylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDm&p-Xylene 1.0 04/12/14 RM SW8260ug/L0.42NDMethyl ethyl ketone 1.0 04/12/14 RM SW8260ug/L0.50NDMethyl t-butyl ether (MTBE) 1.0 04/12/14 RM SW8260ug/L0.19NDMethylene chloride 3.0 04/12/14 RM SW8260ug/L0.16NDNaphthalene 1.0 04/12/14 RM SW8260ug/L0.19NDn-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDn-Propylbenzene 1.0 04/12/14 RM SW8260ug/L0.20NDo-Xylene 1.0 04/12/14 RM SW8260ug/L0.45NDp-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L0.21NDsec-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDStyrene 1.0 04/12/14 RM SW8260ug/L0.41NDtert-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.23NDTetrachloroethene 1.0 04/12/14 RM SW8260ug/L0.24NDTetrahydrofuran (THF) 5.0 04/12/14 RM SW8260ug/L 10.51NDToluene 1.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,2-Dichloroethene 5.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.14NDtrans-1,4-dichloro-2-butene 1.0 04/12/14 RM SW8260ug/L0.45NDTrichloroethene 1.0 04/12/14 RM SW8260ug/L0.18NDTrichlorofluoromethane 1.0 04/12/14 RM SW8260ug/L0.23NDTrichlorotrifluoroethane 1.0 04/12/14 RM SW8260ug/L0.23NDVinyl chloride 1.0 04/12/14 RM SW8260ug/L0.14
QA/QC Surrogates98% 1,2-dichlorobenzene-d4 04/12/14 RM 70 - 130 %%96% Bromofluorobenzene 04/12/14 RM 70 - 130 %%94% Dibromofluoromethane 04/12/14 RM 70 - 130 %%
Page 14 of 15 Ver 1
TRIP BLANKPhoenix I.D.: BG31853
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
99% Toluene-d8 04/12/14 RM 70 - 130 %%
Comments:
TRIP BLANK INCLUDED.
Phyllis Shiller, Laboratory DirectorApril 21, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Bobbi Aloisa, Vice President
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 15 of 15 Ver 1
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
QA/QC ReportApril 21, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG31851
LCS%
DupRPD
LCSD%
LCSRPD
%Rec
Limits
%RPD
LimitsSampleResult
DupResult
QA/QC Batch 271115, QC Sample No: BG29684 (BG31851, BG31852)113 114Antimony (Dissolved) BRL 0.9109NC 107 1.9<0.003 <0.003
99.6 104Selenium (Dissolved) BRL 4.3101NC 103 2.0<0.004 <0.004
79.6 78.0Thallium (Dissolved) BRL 2.096.0NC 98.2 2.3 75 - 125 20<0.002 <0.002
QA/QC Batch 270936, QC Sample No: BG29684 (BG31851, BG31852)32.2 <30Antimony - Water BRL NC109NC 111 1.8 m75 - 125 20<0.003 <0.003
52.9 52.2Selenium - Water BRL 1.3110NC 107 2.8 m75 - 125 20<0.004 <0.010
78.1 75.0Thallium - Water BRL 4.0108NC 108 0.0 75 - 125 20<0.002 <0.002
QA/QC Batch 271425, QC Sample No: BG31458 (BG31851, BG31852)
ICP Metals - Aqueous93.5 91.9Aluminum BRL 1.799.2NC 98.9 0.3 75 - 125 200.081 0.049
103 104Arsenic BRL 1.0103NC 104 1.0 75 - 125 20<0.004 <0.004
100 101Barium BRL 1.01033.90 102 1.0 75 - 125 200.026 0.025
104 104Beryllium BRL 0.0105NC 104 1.0 75 - 125 20<0.001 <0.001
101 102Cadmium BRL 1.0104NC 104 0.0 75 - 125 20<0.004 <0.001
NC NCCalcium BRL NC1040.80 105 1.0 75 - 125 2012.1 12.0
99.1 100Chromium BRL 0.9101NC 102 1.0 75 - 125 20<0.001 <0.001
104 105Cobalt BRL 1.0107NC 107 0.0 75 - 125 20<0.002 <0.002
100 101Copper BRL 1.0102NC 102 0.0 75 - 125 200.001 <0.005
100 101Iron BRL 1.0104NC 103 1.0 75 - 125 200.024 0.022
100 101Lead BRL 1.0103NC 103 0.0 75 - 125 20<0.002 <0.002
NC NCMagnesium BRL NC1041.50 104 0.0 75 - 125 207.60 7.49
89.7 90.8Manganese BRL 1.21041.30 103 1.0 75 - 125 201.56 1.54
102 103Nickel BRL 1.0105NC 105 0.0 75 - 125 200.001 0.001 B
100 99.9Potassium BRL 0.11010 100 1.0 75 - 125 204.3 4.3
99.2 99.2Silver BRL 0.0100NC 101 1.0 75 - 125 20<0.001 <0.001
NC NCSodium BRL NC1030.20 103 0.0 75 - 125 2060.2 60.3
101 101Vanadium BRL 0.0102NC 103 1.0 75 - 125 20<0.002 <0.002
102 103Zinc BRL 1.0104NC 103 1.0 75 - 125 200.005 0.005
QA/QC Batch 271471, QC Sample No: BG31486 (BG31851, BG31852)105 103Mercury - Water BRL 1.998.3NC 100 1.7 70 - 130 20<0.0002 <0.0002
Additional Mercury criteria: LCS acceptance range for waters is 80-120% and for soils is 70-130%.
Comment:
QA/QC Batch 271417, QC Sample No: BG31860 (BG31851, BG31852)
ICP Metals - Dissolved99.3 96.6Aluminum BRL 2.898.753.3 99.4 0.7 r75 - 125 200.11 0.19
105 102Arsenic BRL 2.9102NC 102 0.0 75 - 125 20<0.003 <0.003
100 96.9Barium BRL 3.11061.10 107 0.9 75 - 125 200.092 0.091
103 100Beryllium BRL 3.0103NC 103 0.0 75 - 125 20<0.001 <0.001
99.4 96.0Cadmium BRL 3.5104NC 104 0.0 75 - 125 20<0.004 <0.004
NC NCCalcium BRL NC1051.50 105 0.0 75 - 125 2061.4 60.5
100 96.7Chromium BRL 3.4102NC 102 0.0 75 - 125 20<0.001 <0.001
Page 1 of 6
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG31851
LCS%
DupRPD
LCSD%
LCSRPD
%Rec
Limits
%RPD
LimitsSampleResult
DupResult
104 101Cobalt BRL 2.91079.50 107 0.0 75 - 125 200.011 0.010
103 100Copper BRL 3.0103NC 103 0.0 75 - 125 200.009 0.011
101 97.4Iron BRL 3.61062.90 106 0.0 75 - 125 200.276 0.284
100 96.5Lead BRL 3.6103NC 103 0.0 75 - 125 20<0.002 <0.002
NC NCMagnesium BRL NC1062.00 106 0.0 75 - 125 2015.4 15.1
96.4 93.0Manganese BRL 3.61042.20 104 0.0 75 - 125 201.41 1.38
101 98.4Nickel BRL 2.61050 105 0.0 75 - 125 200.028 0.028
106 102Potassium BRL 3.899.81.80 101 1.2 75 - 125 205.5 5.4
89.3 86.2Silver BRL 3.599.9NC 100 0.1 75 - 125 20<0.005 <0.005
NC NCSodium BRL NC10112.5 102 1.0 75 - 125 20119 105
102 99.6Vanadium BRL 2.4104NC 104 0.0 75 - 125 20<0.002 <0.002
102 98.7Zinc BRL 3.31013.10 102 1.0 75 - 125 200.033 0.032
m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.
Page 2 of 6
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
QA/QC ReportApril 21, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG31851
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
QA/QC Batch 271375, QC Sample No: BG31851 (BG31851, BG31852)
Semivolatiles - Ground Water1,2,4,5-Tetrachlorobenzene ND 106 98 7.8 30 - 130 20
1,2,4-Trichlorobenzene ND 102 95 7.1 30 - 130 20
1,2-Dichlorobenzene ND 92 86 6.7 30 - 130 20
1,2-Diphenylhydrazine ND 105 97 7.9 30 - 130 20
1,3-Dichlorobenzene ND 92 86 6.7 30 - 130 20
1,4-Dichlorobenzene ND 92 85 7.9 30 - 130 20
2,4,5-Trichlorophenol ND 115 110 4.4 30 - 130 20
2,4,6-Trichlorophenol ND 116 110 5.3 30 - 130 20
2,4-Dichlorophenol ND 110 103 6.6 30 - 130 20
2,4-Dimethylphenol ND 66 62 6.3 30 - 130 20
2,4-Dinitrophenol ND 115 122 5.9 30 - 130 20
2,4-Dinitrotoluene ND 109 101 7.6 30 - 130 20
2,6-Dinitrotoluene ND 108 101 6.7 30 - 130 20
2-Chloronaphthalene ND 104 99 4.9 30 - 130 20
2-Chlorophenol ND 94 89 5.5 30 - 130 20
2-Methylnaphthalene ND 98 93 5.2 30 - 130 20
2-Methylphenol (o-cresol) ND 87 82 5.9 30 - 130 20
2-Nitroaniline ND 159 158 0.6 l30 - 130 20
2-Nitrophenol ND 108 101 6.7 30 - 130 20
3&4-Methylphenol (m&p-cresol) ND 93 88 5.5 30 - 130 20
3,3'-Dichlorobenzidine ND >200 191 NC l30 - 130 20
3-Nitroaniline ND 186 184 1.1 l30 - 130 20
4,6-Dinitro-2-methylphenol ND 122 123 0.8 30 - 130 20
4-Bromophenyl phenyl ether ND 108 100 7.7 30 - 130 20
4-Chloro-3-methylphenol ND 114 108 5.4 30 - 130 20
4-Chloroaniline ND 81 76 6.4 30 - 130 20
4-Chlorophenyl phenyl ether ND 111 103 7.5 30 - 130 20
4-Nitroaniline ND 113 108 4.5 30 - 130 20
4-Nitrophenol ND 120 119 0.8 15 - 130 20
Acenaphthene ND 101 94 7.2 30 - 130 20
Acenaphthylene ND 100 96 4.1 30 - 130 20
Acetophenone ND 100 95 5.1 30 - 130 20
Aniline ND 74 70 5.6 30 - 130 20
Anthracene ND 104 100 3.9 30 - 130 20
Benz(a)anthracene ND 105 100 4.9 30 - 130 20
Benzidine ND >200 >200 NC l30 - 130 20
Benzo(a)pyrene ND 96 91 5.3 30 - 130 20
Benzo(b)fluoranthene ND 112 104 7.4 30 - 130 20
Benzo(ghi)perylene ND 102 103 1.0 30 - 130 20
Benzo(k)fluoranthene ND 107 102 4.8 30 - 130 20
Benzoic acid ND 59 66 11.2 30 - 130 20
Page 3 of 6
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG31851
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
Benzyl butyl phthalate ND 102 95 7.1 30 - 130 20
Bis(2-chloroethoxy)methane ND 101 94 7.2 30 - 130 20
Bis(2-chloroethyl)ether ND 84 79 6.1 30 - 130 20
Bis(2-chloroisopropyl)ether ND 96 89 7.6 30 - 130 20
Bis(2-ethylhexyl)phthalate ND 113 104 8.3 30 - 130 20
Carbazole ND 153 149 2.6 l30 - 130 20
Chrysene ND 102 97 5.0 30 - 130 20
Dibenz(a,h)anthracene ND 109 108 0.9 30 - 130 20
Dibenzofuran ND 104 98 5.9 30 - 130 20
Diethyl phthalate ND 109 100 8.6 30 - 130 20
Dimethylphthalate ND 106 99 6.8 30 - 130 20
Di-n-butylphthalate ND 112 105 6.5 30 - 130 20
Di-n-octylphthalate ND 110 98 11.5 30 - 130 20
Fluoranthene ND 106 103 2.9 30 - 130 20
Fluorene ND 109 104 4.7 30 - 130 20
Hexachlorobenzene ND 104 95 9.0 30 - 130 20
Hexachlorobutadiene ND 99 91 8.4 30 - 130 20
Hexachlorocyclopentadiene ND 72 68 5.7 30 - 130 20
Hexachloroethane ND 92 86 6.7 30 - 130 20
Indeno(1,2,3-cd)pyrene ND 107 105 1.9 30 - 130 20
Isophorone ND 109 101 7.6 30 - 130 20
Naphthalene ND 99 92 7.3 30 - 130 20
Nitrobenzene ND 96 90 6.5 30 - 130 20
N-Nitrosodimethylamine ND 71 72 1.4 30 - 130 20
N-Nitrosodi-n-propylamine ND 96 94 2.1 30 - 130 20
N-Nitrosodiphenylamine ND 121 113 6.8 30 - 130 20
Pentachloronitrobenzene ND 111 101 9.4 30 - 130 20
Pentachlorophenol ND 150 146 2.7 l30 - 130 20
Phenanthrene ND 107 101 5.8 30 - 130 20
Phenol ND 78 74 5.3 15 - 130 20
Pyrene ND 105 104 1.0 30 - 130 20
Pyridine ND 43 42 2.4 30 - 130 20
% 2,4,6-Tribromophenol 96 110 101 8.5 15 - 110 20
% 2-Fluorobiphenyl 70 97 91 6.4 30 - 130 20
% 2-Fluorophenol 81 71 66 7.3 15 - 110 20
% Nitrobenzene-d5 82 94 89 5.5 30 - 130 20
% Phenol-d5 85 72 69 4.3 15 - 110 20
% Terphenyl-d14 81 110 108 1.8 30 - 130 20
Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)
Comment:
QA/QC Batch 271497, QC Sample No: BG31853 (BG31851, BG31852, BG31853)
Volatiles - Ground Water1,1,1,2-Tetrachloroethane ND 94 96 2.1 70 - 130 30
1,1,1-Trichloroethane ND 90 93 3.3 70 - 130 30
1,1,2,2-Tetrachloroethane ND 87 92 5.6 70 - 130 30
1,1,2-Trichloroethane ND 90 103 13.5 70 - 130 30
1,1-Dichloroethane ND 95 98 3.1 70 - 130 30
1,1-Dichloroethene ND 96 97 1.0 70 - 130 30
1,1-Dichloropropene ND 93 95 2.1 70 - 130 30
1,2,3-Trichlorobenzene ND 99 112 12.3 70 - 130 30
1,2,3-Trichloropropane ND 93 98 5.2 70 - 130 30
Page 4 of 6
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG31851
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
1,2,4-Trichlorobenzene ND 100 110 9.5 70 - 130 30
1,2,4-Trimethylbenzene ND 103 106 2.9 70 - 130 30
1,2-Dibromo-3-chloropropane ND 83 93 11.4 70 - 130 30
1,2-Dibromoethane ND 89 95 6.5 70 - 130 30
1,2-Dichlorobenzene ND 93 98 5.2 70 - 130 30
1,2-Dichloroethane ND 86 92 6.7 70 - 130 30
1,2-Dichloropropane ND 93 96 3.2 70 - 130 30
1,3,5-Trimethylbenzene ND 100 100 0.0 70 - 130 30
1,3-Dichlorobenzene ND 96 99 3.1 70 - 130 30
1,3-Dichloropropane ND 90 98 8.5 70 - 130 30
1,4-Dichlorobenzene ND 97 97 0.0 70 - 130 30
2,2-Dichloropropane ND 80 82 2.5 70 - 130 30
2-Chlorotoluene ND 101 101 0.0 70 - 130 30
2-Hexanone ND 80 93 15.0 70 - 130 30
2-Isopropyltoluene ND 100 103 3.0 70 - 130 30
4-Chlorotoluene ND 103 102 1.0 70 - 130 30
4-Methyl-2-pentanone ND 74 84 12.7 70 - 130 30
Acetone ND 84 81 3.6 70 - 130 30
Acrolein ND 113 124 9.3 70 - 130 30
Acrylonitrile ND 87 98 11.9 70 - 130 30
Benzene ND 95 99 4.1 70 - 130 30
Bromobenzene ND 98 99 1.0 70 - 130 30
Bromochloromethane ND 91 95 4.3 70 - 130 30
Bromodichloromethane ND 90 93 3.3 70 - 130 30
Bromoform ND 88 97 9.7 70 - 130 30
Bromomethane ND 109 113 3.6 70 - 130 30
Carbon Disulfide ND 98 99 1.0 70 - 130 30
Carbon tetrachloride ND 88 88 0.0 70 - 130 30
Chlorobenzene ND 97 100 3.0 70 - 130 30
Chloroethane ND 105 110 4.7 70 - 130 30
Chloroform ND 90 94 4.3 70 - 130 30
Chloromethane ND 110 118 7.0 70 - 130 30
cis-1,2-Dichloroethene ND 94 100 6.2 70 - 130 30
cis-1,3-Dichloropropene ND 88 91 3.4 70 - 130 30
Dibromochloromethane ND 89 99 10.6 70 - 130 30
Dibromomethane ND 92 96 4.3 70 - 130 30
Dichlorodifluoromethane ND 116 119 2.6 70 - 130 30
Ethylbenzene ND 99 100 1.0 70 - 130 30
Hexachlorobutadiene ND 86 89 3.4 70 - 130 30
Isopropylbenzene ND 103 105 1.9 70 - 130 30
m&p-Xylene ND 99 101 2.0 70 - 130 30
Methyl ethyl ketone ND 71 84 16.8 70 - 130 30
Methyl t-butyl ether (MTBE) ND 86 97 12.0 70 - 130 30
Methylene chloride ND 80 82 2.5 70 - 130 30
Naphthalene ND 104 119 13.5 70 - 130 30
n-Butylbenzene ND 95 98 3.1 70 - 130 30
n-Propylbenzene ND 108 109 0.9 70 - 130 30
o-Xylene ND 99 102 3.0 70 - 130 30
p-Isopropyltoluene ND 94 99 5.2 70 - 130 30
sec-Butylbenzene ND 90 95 5.4 70 - 130 30
Styrene ND 100 102 2.0 70 - 130 30
tert-Butylbenzene ND 98 98 0.0 70 - 130 30
Tetrachloroethene ND 98 100 2.0 70 - 130 30
Page 5 of 6
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG31851
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
Tetrahydrofuran (THF) ND 86 99 14.1 70 - 130 30
Toluene ND 98 98 0.0 70 - 130 30
trans-1,2-Dichloroethene ND 95 96 1.0 70 - 130 30
trans-1,3-Dichloropropene ND 88 91 3.4 70 - 130 30
trans-1,4-dichloro-2-butene ND 94 101 7.2 70 - 130 30
Trichloroethene ND 98 99 1.0 70 - 130 30
Trichlorofluoromethane ND 91 92 1.1 70 - 130 30
Trichlorotrifluoroethane ND 91 89 2.2 70 - 130 30
Vinyl chloride ND 109 113 3.6 70 - 130 30
% 1,2-dichlorobenzene-d4 98 98 99 1.0 70 - 130 30
% Bromofluorobenzene 94 97 101 4.0 70 - 130 30
% Dibromofluoromethane 96 92 94 2.2 70 - 130 30
% Toluene-d8 101 100 98 2.0 70 - 130 30
A blank MS/MSD was analyzed with this batch.
Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.
Comment:
l = This parameter is outside laboratory lcs/lcsd specified recovery limits.
MS - Matrix SpikePhyllis Shiller, Laboratory Director
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.
April 21, 2014MS Dup - Matrix Spike Duplicate
RPD - Relative Percent DifferenceLCS - Laboratory Control Sample
LCSD - Laboratory Control Sample Duplicate
NC - No CriteriaIntf - Interference
Page 6 of 6
Sample Criteria Exceedences ReportMonday, April 21, 2014 Page 1 of 3
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG31851 - EBCCriteria: NY: GW
RLCriteria
State: NY
$8260DP25R Trichloroethene 524 1.0 ug/LBG31851 NY / TAGM - Volatile Organics / Groundwater Standards 5$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R Hexachlorobutadiene 0.5ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.5$8260DP25R Trichloroethene 524 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 5$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.04$DP8270-SIMF Nitrobenzene 0.4ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.4$DP8270-SIMF Hexachlorobutadiene 0.5ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.5$DP8270-SIMF Benzidine 5ND 10 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMR Benz(a)anthracene 0.0020.03 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.03 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.03 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.0020.03 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(a)pyrene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002AL-WM Aluminum 0.12.43 0.010 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.1D-AL Aluminum (Dissolved) 0.10.90 0.01 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.1DFE-WMDP Iron, (Dissolved) 0.30.88 0.01 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3DMN-WMDP Manganese, (Dissolved) 0.32.89 0.053 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3D-NA Sodium (Dissolved) 20255 1.1 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 20DTL-WMDP Thallium , (Dissolved) 0.0005BRL 0.001 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.0005FE-WMDP Iron 0.32.89 0.01 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3MN-WMDP Manganese 0.32.65 0.050 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 20237 1.0 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 20TL-WMDP Thallium - LDL 0.0005BRL 0.002 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.0005
$8260DP25R Trichloroethene 520 1.0 ug/LBG31852 NY / TAGM - Volatile Organics / Groundwater Standards 5$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R Trichloroethene 520 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF Phenol 1ND 1.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 1$DP8270-SIMF Phenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Bis(2-chloroethyl)ether 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2-Chlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1
Sample Criteria Exceedences ReportMonday, April 21, 2014 Page 2 of 3
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG31851 - EBCCriteria: NY: GW
RLCriteria
State: NY
$DP8270-SIMF 2-Methylphenol (o-cresol) 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2-Nitrophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2,4-Dimethylphenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Bis(2-chloroethoxy)methane 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,4-Dichlorophenol 1ND 1.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 1$DP8270-SIMF 2,4-Dichlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 4-Chloro-3-methylphenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Hexachlorocyclopentadiene 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,4,6-Trichlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2,4,5-Trichlorophenol 1ND 1.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 1$DP8270-SIMF 2,4,5-Trichlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 4-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,6-Dinitrotoluene 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 2,6-Dinitrotoluene 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 3-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 3-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,4-Dinitrophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Dibenzofuran 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 2,4-Dinitrotoluene 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 4-Nitrophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 2-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 4,6-Dinitro-2-methylphenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Benzidine 5ND 5.6 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 3,3'-Dichlorobenzidine 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMR Benz(a)anthracene 0.0020.19 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.19 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.29 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.0020.29 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.29 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.29 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.0020.08 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.0020.08 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(a)pyrene 0.002ND 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.0020.05 0 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.0020.05 0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002AL-WM Aluminum 0.13.68 0.010 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.1D-AL Aluminum (Dissolved) 0.10.39 0.01 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.1D-NA Sodium (Dissolved) 20247 1.1 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 20DTL-WMDP Thallium , (Dissolved) 0.0005BRL 0.001 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.0005FE-WMDP Iron 0.33.89 0.01 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 20249 1.0 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 20
Sample Criteria Exceedences ReportMonday, April 21, 2014 Page 3 of 3
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG31851 - EBCCriteria: NY: GW
RLCriteria
State: NY
PB-WM Lead 0.0250.031 0.002 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.025TL-WMDP Thallium - LDL 0.0005BRL 0.002 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.0005
$8260DP25R Hexachlorobutadiene 0.5ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.5$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R 1,3-Dichlorobenzene 3ND 5.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 3
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
NY Temperature NarrationApril 21, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG31851
The samples in this delivery group were received at 4°C.(Note acceptance criteria is above freezing up to 6°C)
Page 1 of 1
BG30363 - BG30372
Wednesday, April 16, 2014
Sample ID#s:
Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Project ID: DOMINO SUGAR SITE E
Sincerely yours,
Laboratory DirectorPhyllis Shiller
If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.
NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B
NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823
SDG CommentsApril 16, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG30363
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB1 0-2
Phoenix ID: BG30363
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.37Silver 0.37 04/11/14 LK SW6010mg/Kg0.226940Aluminum 37 04/11/14 LK SW6010mg/Kg7.42.7Arsenic 0.7 04/11/14 LK SW6010mg/Kg0.74
97.5Barium 0.7 04/11/14 LK SW6010mg/Kg0.150.30Beryllium 0.30 04/11/14 LK SW6010mg/Kg0.15
18100Calcium 37 04/11/14 LK SW6010mg/Kg34< 0.37Cadmium 0.37 04/11/14 LK SW6010mg/Kg0.155.30Cobalt 0.37 04/11/14 LK SW6010mg/Kg0.1516.4Chromium 0.37 04/11/14 LK SW6010mg/Kg0.1532.0Copper 0.37 04/11/14 LK SW6010mg/kg0.30
18500Iron 37 04/11/14 LK SW6010mg/Kg B370.55Mercury 0.06 04/10/14 RS SW-7471mg/Kg0.042070Potassium 7 04/11/14 LK SW6010mg/Kg2.99810Magnesium 37 04/11/14 LK SW6010mg/Kg2.2330Manganese 3.7 04/11/14 LK SW6010mg/Kg1.5282Sodium 7 04/11/14 LK SW6010mg/Kg3.213.5Nickel 0.37 04/11/14 LK SW6010mg/Kg0.1598.7Lead 0.7 04/11/14 LK SW6010mg/Kg0.22< 1.9Antimony 1.9 04/11/14 LK SW6010mg/Kg0.74< 1.5Selenium 1.5 04/11/14 LK SW6010mg/Kg1.3< 1.5Thallium 1.5 04/11/14 LK SW6010mg/Kg1.529.7Vanadium 0.4 04/11/14 LK SW6010mg/Kg0.1577.7Zinc 0.7 04/11/14 LK SW6010mg/Kg0.3792Percent Solid 04/09/14 I E160.3%
CompletedSoil Extraction for PCB 04/09/14 BB/V SW3545CompletedSoil Extraction for Pesticide 04/09/14 BB SW3545CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471
Page 1 of 49 Ver 1
E-SB1 0-2Phoenix I.D.: BG30363
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
CompletedTotal Metals Digest 04/09/14 CB/AG/W SW846 - 3050
CompletedField Extraction 04/08/14 SW5035
Polychlorinated BiphenylsNDPCB-1016 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1221 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1232 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1242 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1248 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1254 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1260 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1262 35 04/10/14 AW SW 8082ug/Kg35NDPCB-1268 35 04/10/14 AW SW 8082ug/Kg35
QA/QC Surrogates38% DCBP 04/10/14 AW 30 - 150 %%41% TCMX 04/10/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDT 2.6 04/14/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.5 04/14/14 CE SW8081ug/Kg3.5NDAldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDChlordane 21 04/14/14 CE SW8081ug/Kg21NDd-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.5 04/14/14 CE SW8081ug/Kg3.5NDEndosulfan II 3.5 04/14/14 CE SW8081ug/Kg3.5NDEndosulfan sulfate 3.5 04/14/14 CE SW8081ug/Kg3.5NDEndrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.5 04/14/14 CE SW8081ug/Kg3.5NDEndrin ketone 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.5 04/14/14 CE SW8081ug/Kg3.5NDHeptachlor 1.8 04/14/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 04/14/14 CE SW8081ug/Kg1.8NDMethoxychlor 7.1 04/14/14 CE SW8081ug/Kg7.1NDToxaphene 180 04/14/14 CE SW8081ug/Kg180
QA/QC Surrogates40% DCBP 04/14/14 CE 30 - 150 %%47% TCMX 04/14/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 9.3 04/11/14 U SW8260ug/Kg1.5ND1,1,1-Trichloroethane 9.3 04/11/14 U SW8260ug/Kg1.9ND1,1,2,2-Tetrachloroethane 9.3 04/11/14 U SW8260ug/Kg1.3ND1,1,2-Trichloroethane 9.3 04/11/14 U SW8260ug/Kg0.92ND1,1-Dichloroethane 9.3 04/11/14 U SW8260ug/Kg1.9
Page 2 of 49 Ver 1
E-SB1 0-2Phoenix I.D.: BG30363
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 9.3 04/11/14 U SW8260ug/Kg2.0ND1,1-Dichloropropene 9.3 04/11/14 U SW8260ug/Kg1.8ND1,2,3-Trichlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.9ND1,2,3-Trichloropropane 9.3 04/11/14 U SW8260ug/Kg1.3ND1,2,4-Trichlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.9ND1,2,4-Trimethylbenzene 9.3 04/11/14 U SW8260ug/Kg1.3ND1,2-Dibromo-3-chloropropane 9.3 04/11/14 U SW8260ug/Kg2.5ND1,2-Dibromoethane 9.3 04/11/14 U SW8260ug/Kg2.5ND1,2-Dichlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.0ND1,2-Dichloroethane 9.3 04/11/14 U SW8260ug/Kg0.82ND1,2-Dichloropropane 9.3 04/11/14 U SW8260ug/Kg1.3ND1,3,5-Trimethylbenzene 9.3 04/11/14 U SW8260ug/Kg1.2ND1,3-Dichlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.4ND1,3-Dichloropropane 9.3 04/11/14 U SW8260ug/Kg0.99ND1,4-Dichlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.5ND2,2-Dichloropropane 9.3 04/11/14 U SW8260ug/Kg1.6ND2-Chlorotoluene 9.3 04/11/14 U SW8260ug/Kg1.5ND2-Hexanone 47 04/11/14 U SW8260ug/Kg4.2ND2-Isopropyltoluene 9.3 04/11/14 U SW8260ug/Kg 11.3ND4-Chlorotoluene 9.3 04/11/14 U SW8260ug/Kg1.1ND4-Methyl-2-pentanone 47 04/11/14 U SW8260ug/Kg2.2NDAcetone 50 04/11/14 U SW8260ug/Kg9.3NDAcrylonitrile 19 04/11/14 U SW8260ug/Kg5.3NDBenzene 9.3 04/11/14 U SW8260ug/Kg1.9NDBromobenzene 9.3 04/11/14 U SW8260ug/Kg1.2NDBromochloromethane 9.3 04/11/14 U SW8260ug/Kg1.4NDBromodichloromethane 9.3 04/11/14 U SW8260ug/Kg1.2NDBromoform 9.3 04/11/14 U SW8260ug/Kg1.3NDBromomethane 9.3 04/11/14 U SW8260ug/Kg7.2NDCarbon Disulfide 9.3 04/11/14 U SW8260ug/Kg1.5NDCarbon tetrachloride 9.3 04/11/14 U SW8260ug/Kg1.1NDChlorobenzene 9.3 04/11/14 U SW8260ug/Kg1.4NDChloroethane 9.3 04/11/14 U SW8260ug/Kg2.2NDChloroform 9.3 04/11/14 U SW8260ug/Kg1.7NDChloromethane 9.3 04/11/14 U SW8260ug/Kg4.9NDcis-1,2-Dichloroethene 9.3 04/11/14 U SW8260ug/Kg2.0NDcis-1,3-Dichloropropene 9.3 04/11/14 U SW8260ug/Kg1.0NDDibromochloromethane 9.3 04/11/14 U SW8260ug/Kg1.0NDDibromomethane 9.3 04/11/14 U SW8260ug/Kg1.2NDDichlorodifluoromethane 9.3 04/11/14 U SW8260ug/Kg2.5NDEthylbenzene 9.3 04/11/14 U SW8260ug/Kg1.7NDHexachlorobutadiene 9.3 04/11/14 U SW8260ug/Kg2.0NDIsopropylbenzene 9.3 04/11/14 U SW8260ug/Kg1.8NDm&p-Xylene 9.3 04/11/14 U SW8260ug/Kg3.7NDMethyl Ethyl Ketone 56 04/11/14 U SW8260ug/Kg8.1NDMethyl t-butyl ether (MTBE) 19 04/11/14 U SW8260ug/Kg2.6NDMethylene chloride 9.3 04/11/14 U SW8260ug/Kg1.5NDNaphthalene 9.3 04/11/14 U SW8260ug/Kg2.5NDn-Butylbenzene 9.3 04/11/14 U SW8260ug/Kg1.7
Page 3 of 49 Ver 1
E-SB1 0-2Phoenix I.D.: BG30363
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 9.3 04/11/14 U SW8260ug/Kg1.7NDo-Xylene 9.3 04/11/14 U SW8260ug/Kg3.6NDp-Isopropyltoluene 9.3 04/11/14 U SW8260ug/Kg1.3NDsec-Butylbenzene 9.3 04/11/14 U SW8260ug/Kg1.8NDStyrene 9.3 04/11/14 U SW8260ug/Kg2.7NDtert-Butylbenzene 9.3 04/11/14 U SW8260ug/Kg1.5NDTetrachloroethene 9.3 04/11/14 U SW8260ug/Kg2.0NDTetrahydrofuran (THF) 19 04/11/14 U SW8260ug/Kg 18.4NDToluene 9.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,2-Dichloroethene 9.3 04/11/14 U SW8260ug/Kg1.9NDtrans-1,3-Dichloropropene 9.3 04/11/14 U SW8260ug/Kg1.9NDtrans-1,4-dichloro-2-butene 19 04/11/14 U SW8260ug/Kg17NDTrichloroethene 9.3 04/11/14 U SW8260ug/Kg2.0NDTrichlorofluoromethane 9.3 04/11/14 U SW8260ug/Kg2.1NDTrichlorotrifluoroethane 9.3 04/11/14 U SW8260ug/Kg1.5NDVinyl chloride 9.3 04/11/14 U SW8260ug/Kg3.0
QA/QC Surrogates107% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%92% Bromofluorobenzene 04/11/14 U 70 - 130 %%104% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 250 04/10/14 DD SW 8270ug/Kg130ND1,2,4-Trichlorobenzene 250 04/10/14 DD SW 8270ug/Kg110ND1,2-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg100ND1,2-Diphenylhydrazine 250 04/10/14 DD SW 8270ug/Kg120ND1,3-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg110ND1,4-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg110ND2,4,5-Trichlorophenol 250 04/10/14 DD SW 8270ug/Kg190ND2,4,6-Trichlorophenol 250 04/10/14 DD SW 8270ug/Kg110ND2,4-Dichlorophenol 250 04/10/14 DD SW 8270ug/Kg130ND2,4-Dimethylphenol 250 04/10/14 DD SW 8270ug/Kg88ND2,4-Dinitrophenol 1800 04/10/14 DD SW 8270ug/Kg250ND2,4-Dinitrotoluene 250 04/10/14 DD SW 8270ug/Kg140ND2,6-Dinitrotoluene 250 04/10/14 DD SW 8270ug/Kg110ND2-Chloronaphthalene 250 04/10/14 DD SW 8270ug/Kg100ND2-Chlorophenol 250 04/10/14 DD SW 8270ug/Kg100ND2-Methylnaphthalene 250 04/10/14 DD SW 8270ug/Kg110ND2-Methylphenol (o-cresol) 250 04/10/14 DD SW 8270ug/Kg170ND2-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg360ND2-Nitrophenol 250 04/10/14 DD SW 8270ug/Kg230ND3&4-Methylphenol (m&p-cresol) 250 04/10/14 DD SW 8270ug/Kg 1140ND3,3'-Dichlorobenzidine 710 04/10/14 DD SW 8270ug/Kg170ND3-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg770ND4,6-Dinitro-2-methylphenol 1800 04/10/14 DD SW 8270ug/Kg380ND4-Bromophenyl phenyl ether 250 04/10/14 DD SW 8270ug/Kg100ND4-Chloro-3-methylphenol 250 04/10/14 DD SW 8270ug/Kg130ND4-Chloroaniline 710 04/10/14 DD SW 8270ug/Kg170ND4-Chlorophenyl phenyl ether 250 04/10/14 DD SW 8270ug/Kg120
Page 4 of 49 Ver 1
E-SB1 0-2Phoenix I.D.: BG30363
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg120ND4-Nitrophenol 1800 04/10/14 DD SW 8270ug/Kg160NDAcenaphthene 250 04/10/14 DD SW 8270ug/Kg110NDAcenaphthylene 250 04/10/14 DD SW 8270ug/Kg100NDAcetophenone 250 04/10/14 DD SW 8270ug/Kg110NDAniline 1800 04/10/14 DD SW 8270ug/Kg720NDAnthracene 250 04/10/14 DD SW 8270ug/Kg120160Benz(a)anthracene 250 04/10/14 DD SW 8270ug/Kg120JNDBenzidine 710 04/10/14 DD SW 8270ug/Kg210140Benzo(a)pyrene 250 04/10/14 DD SW 8270ug/Kg120J190Benzo(b)fluoranthene 250 04/10/14 DD SW 8270ug/Kg120JNDBenzo(ghi)perylene 250 04/10/14 DD SW 8270ug/Kg120NDBenzo(k)fluoranthene 250 04/10/14 DD SW 8270ug/Kg120NDBenzoic acid 1800 04/10/14 DD SW 8270ug/Kg 1710NDBenzyl butyl phthalate 250 04/10/14 DD SW 8270ug/Kg92NDBis(2-chloroethoxy)methane 250 04/10/14 DD SW 8270ug/Kg98NDBis(2-chloroethyl)ether 250 04/10/14 DD SW 8270ug/Kg96NDBis(2-chloroisopropyl)ether 250 04/10/14 DD SW 8270ug/Kg 199NDBis(2-ethylhexyl)phthalate 250 04/10/14 DD SW 8270ug/Kg100NDCarbazole 1800 04/10/14 DD SW 8270ug/Kg270160Chrysene 250 04/10/14 DD SW 8270ug/Kg120JNDDibenz(a,h)anthracene 250 04/10/14 DD SW 8270ug/Kg120NDDibenzofuran 250 04/10/14 DD SW 8270ug/Kg100NDDiethyl phthalate 250 04/10/14 DD SW 8270ug/Kg110NDDimethylphthalate 250 04/10/14 DD SW 8270ug/Kg110NDDi-n-butylphthalate 250 04/10/14 DD SW 8270ug/Kg95NDDi-n-octylphthalate 250 04/10/14 DD SW 8270ug/Kg92240Fluoranthene 250 04/10/14 DD SW 8270ug/Kg120JNDFluorene 250 04/10/14 DD SW 8270ug/Kg120NDHexachlorobenzene 250 04/10/14 DD SW 8270ug/Kg100NDHexachlorobutadiene 250 04/10/14 DD SW 8270ug/Kg130NDHexachlorocyclopentadiene 250 04/10/14 DD SW 8270ug/Kg110NDHexachloroethane 250 04/10/14 DD SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 250 04/10/14 DD SW 8270ug/Kg120NDIsophorone 250 04/10/14 DD SW 8270ug/Kg100NDNaphthalene 250 04/10/14 DD SW 8270ug/Kg100NDNitrobenzene 250 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodimethylamine 250 04/10/14 DD SW 8270ug/Kg100NDN-Nitrosodi-n-propylamine 250 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodiphenylamine 250 04/10/14 DD SW 8270ug/Kg140NDPentachloronitrobenzene 250 04/10/14 DD SW 8270ug/Kg130NDPentachlorophenol 250 04/10/14 DD SW 8270ug/Kg130160Phenanthrene 250 04/10/14 DD SW 8270ug/Kg100JNDPhenol 250 04/10/14 DD SW 8270ug/Kg110240Pyrene 250 04/10/14 DD SW 8270ug/Kg120JNDPyridine 250 04/10/14 DD SW 8270ug/Kg87
QA/QC Surrogates94% 2,4,6-Tribromophenol 04/10/14 DD 30 - 130 %%55% 2-Fluorobiphenyl 04/10/14 DD 30 - 130 %%
Page 5 of 49 Ver 1
E-SB1 0-2Phoenix I.D.: BG30363
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
77% 2-Fluorophenol 04/10/14 DD 30 - 130 %%55% Nitrobenzene-d5 04/10/14 DD 30 - 130 %%83% Phenol-d5 04/10/14 DD 30 - 130 %%58% Terphenyl-d14 04/10/14 DD 30 - 130 %%
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 6 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB1 29-31
Phoenix ID: BG30364
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.36Silver 0.36 04/11/14 LK SW6010mg/Kg0.213240Aluminum 36 04/11/14 LK SW6010mg/Kg7.20.7Arsenic 0.7 04/11/14 LK SW6010mg/Kg0.72
20.3Barium 0.7 04/11/14 LK SW6010mg/Kg0.14< 0.29Beryllium 0.29 04/11/14 LK SW6010mg/Kg0.142030Calcium 3.6 04/11/14 LK SW6010mg/Kg3.3
< 0.36Cadmium 0.36 04/11/14 LK SW6010mg/Kg0.142.67Cobalt 0.36 04/11/14 LK SW6010mg/Kg0.146.68Chromium 0.36 04/11/14 LK SW6010mg/Kg0.148.42Copper 0.36 04/11/14 LK SW6010mg/kg0.298230Iron 3.6 04/11/14 LK SW6010mg/Kg B3.6
< 0.08Mercury 0.08 04/10/14 RS SW-7471mg/Kg0.05756Potassium 7 04/11/14 LK SW6010mg/Kg2.8
1960Magnesium 3.6 04/11/14 LK SW6010mg/Kg0.21185Manganese 3.6 04/11/14 LK SW6010mg/Kg1.495Sodium 7 04/11/14 LK SW6010mg/Kg3.1
6.90Nickel 0.36 04/11/14 LK SW6010mg/Kg0.142.3Lead 0.7 04/11/14 LK SW6010mg/Kg0.21
< 1.8Antimony 1.8 04/11/14 LK SW6010mg/Kg0.72< 1.4Selenium 1.4 04/11/14 LK SW6010mg/Kg1.2< 1.4Thallium 1.4 04/11/14 LK SW6010mg/Kg1.413.8Vanadium 0.4 04/11/14 LK SW6010mg/Kg0.1414.0Zinc 0.7 04/11/14 LK SW6010mg/Kg0.3697Percent Solid 04/09/14 I E160.3%
CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471CompletedTotal Metals Digest 04/09/14 CB/AG/W SW846 - 3050
CompletedField Extraction 04/08/14 SW5035
Page 7 of 49 Ver 1
E-SB1 29-31Phoenix I.D.: BG30364
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 5.7 04/11/14 U SW8260ug/Kg0.94ND1,1,1-Trichloroethane 5.7 04/11/14 U SW8260ug/Kg1.1ND1,1,2,2-Tetrachloroethane 5.7 04/11/14 U SW8260ug/Kg0.81ND1,1,2-Trichloroethane 5.7 04/11/14 U SW8260ug/Kg0.56ND1,1-Dichloroethane 5.7 04/11/14 U SW8260ug/Kg1.1ND1,1-Dichloroethene 5.7 04/11/14 U SW8260ug/Kg1.2ND1,1-Dichloropropene 5.7 04/11/14 U SW8260ug/Kg1.1ND1,2,3-Trichlorobenzene 5.7 04/11/14 U SW8260ug/Kg1.1ND1,2,3-Trichloropropane 5.7 04/11/14 U SW8260ug/Kg0.81ND1,2,4-Trichlorobenzene 5.7 04/11/14 U SW8260ug/Kg1.1ND1,2,4-Trimethylbenzene 5.7 04/11/14 U SW8260ug/Kg0.82ND1,2-Dibromo-3-chloropropane 5.7 04/11/14 U SW8260ug/Kg1.5ND1,2-Dibromoethane 5.7 04/11/14 U SW8260ug/Kg1.5ND1,2-Dichlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.63ND1,2-Dichloroethane 5.7 04/11/14 U SW8260ug/Kg0.50ND1,2-Dichloropropane 5.7 04/11/14 U SW8260ug/Kg0.81ND1,3,5-Trimethylbenzene 5.7 04/11/14 U SW8260ug/Kg0.76ND1,3-Dichlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.85ND1,3-Dichloropropane 5.7 04/11/14 U SW8260ug/Kg0.61ND1,4-Dichlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.90ND2,2-Dichloropropane 5.7 04/11/14 U SW8260ug/Kg0.96ND2-Chlorotoluene 5.7 04/11/14 U SW8260ug/Kg0.92ND2-Hexanone 29 04/11/14 U SW8260ug/Kg2.6ND2-Isopropyltoluene 5.7 04/11/14 U SW8260ug/Kg 10.79ND4-Chlorotoluene 5.7 04/11/14 U SW8260ug/Kg0.66ND4-Methyl-2-pentanone 29 04/11/14 U SW8260ug/Kg1.4NDAcetone 50 04/11/14 U SW8260ug/Kg5.7NDAcrylonitrile 11 04/11/14 U SW8260ug/Kg3.2NDBenzene 5.7 04/11/14 U SW8260ug/Kg1.1NDBromobenzene 5.7 04/11/14 U SW8260ug/Kg0.74NDBromochloromethane 5.7 04/11/14 U SW8260ug/Kg0.84NDBromodichloromethane 5.7 04/11/14 U SW8260ug/Kg0.71NDBromoform 5.7 04/11/14 U SW8260ug/Kg0.80NDBromomethane 5.7 04/11/14 U SW8260ug/Kg4.4NDCarbon Disulfide 5.7 04/11/14 U SW8260ug/Kg0.93NDCarbon tetrachloride 5.7 04/11/14 U SW8260ug/Kg0.66NDChlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.85NDChloroethane 5.7 04/11/14 U SW8260ug/Kg1.3NDChloroform 5.7 04/11/14 U SW8260ug/Kg1.0NDChloromethane 5.7 04/11/14 U SW8260ug/Kg3.0NDcis-1,2-Dichloroethene 5.7 04/11/14 U SW8260ug/Kg1.2NDcis-1,3-Dichloropropene 5.7 04/11/14 U SW8260ug/Kg0.62NDDibromochloromethane 5.7 04/11/14 U SW8260ug/Kg0.64NDDibromomethane 5.7 04/11/14 U SW8260ug/Kg0.72NDDichlorodifluoromethane 5.7 04/11/14 U SW8260ug/Kg1.5NDEthylbenzene 5.7 04/11/14 U SW8260ug/Kg1.0NDHexachlorobutadiene 5.7 04/11/14 U SW8260ug/Kg1.2NDIsopropylbenzene 5.7 04/11/14 U SW8260ug/Kg1.1
Page 8 of 49 Ver 1
E-SB1 29-31Phoenix I.D.: BG30364
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 5.7 04/11/14 U SW8260ug/Kg2.3NDMethyl Ethyl Ketone 34 04/11/14 U SW8260ug/Kg5.0NDMethyl t-butyl ether (MTBE) 11 04/11/14 U SW8260ug/Kg1.6NDMethylene chloride 5.7 04/11/14 U SW8260ug/Kg0.94NDNaphthalene 5.7 04/11/14 U SW8260ug/Kg1.5NDn-Butylbenzene 5.7 04/11/14 U SW8260ug/Kg1.0NDn-Propylbenzene 5.7 04/11/14 U SW8260ug/Kg1.0NDo-Xylene 5.7 04/11/14 U SW8260ug/Kg2.2NDp-Isopropyltoluene 5.7 04/11/14 U SW8260ug/Kg0.82NDsec-Butylbenzene 5.7 04/11/14 U SW8260ug/Kg1.1NDStyrene 5.7 04/11/14 U SW8260ug/Kg1.6NDtert-Butylbenzene 5.7 04/11/14 U SW8260ug/Kg0.92NDTetrachloroethene 5.7 04/11/14 U SW8260ug/Kg1.2NDTetrahydrofuran (THF) 11 04/11/14 U SW8260ug/Kg 15.1NDToluene 5.7 04/11/14 U SW8260ug/Kg0.90NDtrans-1,2-Dichloroethene 5.7 04/11/14 U SW8260ug/Kg1.1NDtrans-1,3-Dichloropropene 5.7 04/11/14 U SW8260ug/Kg1.2NDtrans-1,4-dichloro-2-butene 11 04/11/14 U SW8260ug/Kg11NDTrichloroethene 5.7 04/11/14 U SW8260ug/Kg1.2NDTrichlorofluoromethane 5.7 04/11/14 U SW8260ug/Kg1.3NDTrichlorotrifluoroethane 5.7 04/11/14 U SW8260ug/Kg0.89NDVinyl chloride 5.7 04/11/14 U SW8260ug/Kg1.9
QA/QC Surrogates107% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%94% Bromofluorobenzene 04/11/14 U 70 - 130 %%104% Dibromofluoromethane 04/11/14 U 70 - 130 %%101% Toluene-d8 04/11/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 240 04/10/14 DD SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 240 04/10/14 DD SW 8270ug/Kg100ND1,2-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg96ND1,2-Diphenylhydrazine 240 04/10/14 DD SW 8270ug/Kg110ND1,3-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg100ND1,4-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg100ND2,4,5-Trichlorophenol 240 04/10/14 DD SW 8270ug/Kg190ND2,4,6-Trichlorophenol 240 04/10/14 DD SW 8270ug/Kg110ND2,4-Dichlorophenol 240 04/10/14 DD SW 8270ug/Kg120ND2,4-Dimethylphenol 240 04/10/14 DD SW 8270ug/Kg84ND2,4-Dinitrophenol 1700 04/10/14 DD SW 8270ug/Kg240ND2,4-Dinitrotoluene 240 04/10/14 DD SW 8270ug/Kg130ND2,6-Dinitrotoluene 240 04/10/14 DD SW 8270ug/Kg110ND2-Chloronaphthalene 240 04/10/14 DD SW 8270ug/Kg97ND2-Chlorophenol 240 04/10/14 DD SW 8270ug/Kg97ND2-Methylnaphthalene 240 04/10/14 DD SW 8270ug/Kg100ND2-Methylphenol (o-cresol) 240 04/10/14 DD SW 8270ug/Kg160ND2-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg340ND2-Nitrophenol 240 04/10/14 DD SW 8270ug/Kg220ND3&4-Methylphenol (m&p-cresol) 240 04/10/14 DD SW 8270ug/Kg 1130ND3,3'-Dichlorobenzidine 680 04/10/14 DD SW 8270ug/Kg160
Page 9 of 49 Ver 1
E-SB1 29-31Phoenix I.D.: BG30364
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND3-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg740ND4,6-Dinitro-2-methylphenol 1700 04/10/14 DD SW 8270ug/Kg370ND4-Bromophenyl phenyl ether 240 04/10/14 DD SW 8270ug/Kg100ND4-Chloro-3-methylphenol 240 04/10/14 DD SW 8270ug/Kg120ND4-Chloroaniline 680 04/10/14 DD SW 8270ug/Kg160ND4-Chlorophenyl phenyl ether 240 04/10/14 DD SW 8270ug/Kg110ND4-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg110ND4-Nitrophenol 1700 04/10/14 DD SW 8270ug/Kg150NDAcenaphthene 240 04/10/14 DD SW 8270ug/Kg100NDAcenaphthylene 240 04/10/14 DD SW 8270ug/Kg95NDAcetophenone 240 04/10/14 DD SW 8270ug/Kg110NDAniline 1700 04/10/14 DD SW 8270ug/Kg690NDAnthracene 240 04/10/14 DD SW 8270ug/Kg110NDBenz(a)anthracene 240 04/10/14 DD SW 8270ug/Kg110NDBenzidine 680 04/10/14 DD SW 8270ug/Kg200NDBenzo(a)pyrene 240 04/10/14 DD SW 8270ug/Kg110NDBenzo(b)fluoranthene 240 04/10/14 DD SW 8270ug/Kg120NDBenzo(ghi)perylene 240 04/10/14 DD SW 8270ug/Kg110NDBenzo(k)fluoranthene 240 04/10/14 DD SW 8270ug/Kg110NDBenzoic acid 1700 04/10/14 DD SW 8270ug/Kg 1680NDBenzyl butyl phthalate 240 04/10/14 DD SW 8270ug/Kg88NDBis(2-chloroethoxy)methane 240 04/10/14 DD SW 8270ug/Kg94NDBis(2-chloroethyl)ether 240 04/10/14 DD SW 8270ug/Kg92NDBis(2-chloroisopropyl)ether 240 04/10/14 DD SW 8270ug/Kg 195NDBis(2-ethylhexyl)phthalate 240 04/10/14 DD SW 8270ug/Kg98NDCarbazole 1700 04/10/14 DD SW 8270ug/Kg260NDChrysene 240 04/10/14 DD SW 8270ug/Kg110NDDibenz(a,h)anthracene 240 04/10/14 DD SW 8270ug/Kg110NDDibenzofuran 240 04/10/14 DD SW 8270ug/Kg99NDDiethyl phthalate 240 04/10/14 DD SW 8270ug/Kg110NDDimethylphthalate 240 04/10/14 DD SW 8270ug/Kg110NDDi-n-butylphthalate 240 04/10/14 DD SW 8270ug/Kg91NDDi-n-octylphthalate 240 04/10/14 DD SW 8270ug/Kg88NDFluoranthene 240 04/10/14 DD SW 8270ug/Kg110NDFluorene 240 04/10/14 DD SW 8270ug/Kg110NDHexachlorobenzene 240 04/10/14 DD SW 8270ug/Kg99NDHexachlorobutadiene 240 04/10/14 DD SW 8270ug/Kg120NDHexachlorocyclopentadiene 240 04/10/14 DD SW 8270ug/Kg100NDHexachloroethane 240 04/10/14 DD SW 8270ug/Kg100NDIndeno(1,2,3-cd)pyrene 240 04/10/14 DD SW 8270ug/Kg110NDIsophorone 240 04/10/14 DD SW 8270ug/Kg95NDNaphthalene 240 04/10/14 DD SW 8270ug/Kg98NDNitrobenzene 240 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodimethylamine 240 04/10/14 DD SW 8270ug/Kg96NDN-Nitrosodi-n-propylamine 240 04/10/14 DD SW 8270ug/Kg110NDN-Nitrosodiphenylamine 240 04/10/14 DD SW 8270ug/Kg130NDPentachloronitrobenzene 240 04/10/14 DD SW 8270ug/Kg130NDPentachlorophenol 240 04/10/14 DD SW 8270ug/Kg130NDPhenanthrene 240 04/10/14 DD SW 8270ug/Kg97
Page 10 of 49 Ver 1
E-SB1 29-31Phoenix I.D.: BG30364
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDPhenol 240 04/10/14 DD SW 8270ug/Kg110NDPyrene 240 04/10/14 DD SW 8270ug/Kg120NDPyridine 240 04/10/14 DD SW 8270ug/Kg84
QA/QC Surrogates84% 2,4,6-Tribromophenol 04/10/14 DD 30 - 130 %%57% 2-Fluorobiphenyl 04/10/14 DD 30 - 130 %%80% 2-Fluorophenol 04/10/14 DD 30 - 130 %%53% Nitrobenzene-d5 04/10/14 DD 30 - 130 %%81% Phenol-d5 04/10/14 DD 30 - 130 %%63% Terphenyl-d14 04/10/14 DD 30 - 130 %%
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 11 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB2 29-31
Phoenix ID: BG30365
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.34Silver 0.34 04/11/14 LK SW6010mg/Kg0.203250Aluminum 34 04/11/14 LK SW6010mg/Kg6.81.5Arsenic 0.7 04/11/14 LK SW6010mg/Kg0.68
22.1Barium 0.7 04/11/14 LK SW6010mg/Kg0.14< 0.27Beryllium 0.27 04/11/14 LK SW6010mg/Kg0.1411100Calcium 34 04/11/14 LK SW6010mg/Kg31< 0.34Cadmium 0.34 04/11/14 LK SW6010mg/Kg0.142.75Cobalt 0.34 04/11/14 LK SW6010mg/Kg0.147.08Chromium 0.34 04/11/14 LK SW6010mg/Kg0.147.68Copper 0.34 04/11/14 LK SW6010mg/kg0.278800Iron 34 04/11/14 LK SW6010mg/Kg B34
< 0.06Mercury 0.06 04/10/14 RS SW-7471mg/Kg0.04767Potassium 7 04/11/14 LK SW6010mg/Kg2.6
3390Magnesium 3.4 04/11/14 LK SW6010mg/Kg0.20176Manganese 3.4 04/11/14 LK SW6010mg/Kg1.4137Sodium 7 04/11/14 LK SW6010mg/Kg2.97.56Nickel 0.34 04/11/14 LK SW6010mg/Kg0.1412.1Lead 0.7 04/11/14 LK SW6010mg/Kg0.20< 1.7Antimony 1.7 04/11/14 LK SW6010mg/Kg0.68< 1.4Selenium 1.4 04/11/14 LK SW6010mg/Kg1.2< 1.4Thallium 1.4 04/11/14 LK SW6010mg/Kg1.415.6Vanadium 0.3 04/11/14 LK SW6010mg/Kg0.1413.5Zinc 0.7 04/11/14 LK SW6010mg/Kg0.3497Percent Solid 04/09/14 I E160.3%
CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471CompletedTotal Metals Digest 04/09/14 CB/AG/W SW846 - 3050
CompletedField Extraction 04/08/14 SW5035
Page 12 of 49 Ver 1
E-SB2 29-31Phoenix I.D.: BG30365
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 8.1 04/11/14 U SW8260ug/Kg1.3ND1,1,1-Trichloroethane 8.1 04/11/14 U SW8260ug/Kg1.6ND1,1,2,2-Tetrachloroethane 8.1 04/11/14 U SW8260ug/Kg1.1ND1,1,2-Trichloroethane 8.1 04/11/14 U SW8260ug/Kg0.79ND1,1-Dichloroethane 8.1 04/11/14 U SW8260ug/Kg1.6ND1,1-Dichloroethene 8.1 04/11/14 U SW8260ug/Kg1.8ND1,1-Dichloropropene 8.1 04/11/14 U SW8260ug/Kg1.6ND1,2,3-Trichlorobenzene 8.1 04/11/14 U SW8260ug/Kg1.6ND1,2,3-Trichloropropane 8.1 04/11/14 U SW8260ug/Kg1.1ND1,2,4-Trichlorobenzene 8.1 04/11/14 U SW8260ug/Kg1.6ND1,2,4-Trimethylbenzene 8.1 04/11/14 U SW8260ug/Kg1.2ND1,2-Dibromo-3-chloropropane 8.1 04/11/14 U SW8260ug/Kg2.2ND1,2-Dibromoethane 8.1 04/11/14 U SW8260ug/Kg2.2ND1,2-Dichlorobenzene 8.1 04/11/14 U SW8260ug/Kg0.89ND1,2-Dichloroethane 8.1 04/11/14 U SW8260ug/Kg0.71ND1,2-Dichloropropane 8.1 04/11/14 U SW8260ug/Kg1.1ND1,3,5-Trimethylbenzene 8.1 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichlorobenzene 8.1 04/11/14 U SW8260ug/Kg1.2ND1,3-Dichloropropane 8.1 04/11/14 U SW8260ug/Kg0.86ND1,4-Dichlorobenzene 8.1 04/11/14 U SW8260ug/Kg1.3ND2,2-Dichloropropane 8.1 04/11/14 U SW8260ug/Kg1.4ND2-Chlorotoluene 8.1 04/11/14 U SW8260ug/Kg1.3ND2-Hexanone 40 04/11/14 U SW8260ug/Kg3.6ND2-Isopropyltoluene 8.1 04/11/14 U SW8260ug/Kg 11.1ND4-Chlorotoluene 8.1 04/11/14 U SW8260ug/Kg0.94ND4-Methyl-2-pentanone 40 04/11/14 U SW8260ug/Kg1.9NDAcetone 50 04/11/14 U SW8260ug/Kg8.0NDAcrylonitrile 16 04/11/14 U SW8260ug/Kg4.5NDBenzene 8.1 04/11/14 U SW8260ug/Kg1.6NDBromobenzene 8.1 04/11/14 U SW8260ug/Kg1.1NDBromochloromethane 8.1 04/11/14 U SW8260ug/Kg1.2NDBromodichloromethane 8.1 04/11/14 U SW8260ug/Kg1.0NDBromoform 8.1 04/11/14 U SW8260ug/Kg1.1NDBromomethane 8.1 04/11/14 U SW8260ug/Kg6.2NDCarbon Disulfide 8.1 04/11/14 U SW8260ug/Kg1.3NDCarbon tetrachloride 8.1 04/11/14 U SW8260ug/Kg0.94NDChlorobenzene 8.1 04/11/14 U SW8260ug/Kg1.2NDChloroethane 8.1 04/11/14 U SW8260ug/Kg1.9NDChloroform 8.1 04/11/14 U SW8260ug/Kg1.5NDChloromethane 8.1 04/11/14 U SW8260ug/Kg4.2NDcis-1,2-Dichloroethene 8.1 04/11/14 U SW8260ug/Kg1.8NDcis-1,3-Dichloropropene 8.1 04/11/14 U SW8260ug/Kg0.87NDDibromochloromethane 8.1 04/11/14 U SW8260ug/Kg0.91NDDibromomethane 8.1 04/11/14 U SW8260ug/Kg1.0NDDichlorodifluoromethane 8.1 04/11/14 U SW8260ug/Kg2.2NDEthylbenzene 8.1 04/11/14 U SW8260ug/Kg1.5NDHexachlorobutadiene 8.1 04/11/14 U SW8260ug/Kg1.7NDIsopropylbenzene 8.1 04/11/14 U SW8260ug/Kg1.6
Page 13 of 49 Ver 1
E-SB2 29-31Phoenix I.D.: BG30365
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 8.1 04/11/14 U SW8260ug/Kg3.2NDMethyl Ethyl Ketone 49 04/11/14 U SW8260ug/Kg7.0NDMethyl t-butyl ether (MTBE) 16 04/11/14 U SW8260ug/Kg2.2NDMethylene chloride 8.1 04/11/14 U SW8260ug/Kg1.3NDNaphthalene 8.1 04/11/14 U SW8260ug/Kg2.2NDn-Butylbenzene 8.1 04/11/14 U SW8260ug/Kg1.5NDn-Propylbenzene 8.1 04/11/14 U SW8260ug/Kg1.5NDo-Xylene 8.1 04/11/14 U SW8260ug/Kg3.1NDp-Isopropyltoluene 8.1 04/11/14 U SW8260ug/Kg1.2NDsec-Butylbenzene 8.1 04/11/14 U SW8260ug/Kg1.5NDStyrene 8.1 04/11/14 U SW8260ug/Kg2.3NDtert-Butylbenzene 8.1 04/11/14 U SW8260ug/Kg1.3NDTetrachloroethene 8.1 04/11/14 U SW8260ug/Kg1.7NDTetrahydrofuran (THF) 16 04/11/14 U SW8260ug/Kg 17.3NDToluene 8.1 04/11/14 U SW8260ug/Kg1.3NDtrans-1,2-Dichloroethene 8.1 04/11/14 U SW8260ug/Kg1.6NDtrans-1,3-Dichloropropene 8.1 04/11/14 U SW8260ug/Kg1.7NDtrans-1,4-dichloro-2-butene 16 04/11/14 U SW8260ug/Kg15NDTrichloroethene 8.1 04/11/14 U SW8260ug/Kg1.7NDTrichlorofluoromethane 8.1 04/11/14 U SW8260ug/Kg1.8NDTrichlorotrifluoroethane 8.1 04/11/14 U SW8260ug/Kg1.3NDVinyl chloride 8.1 04/11/14 U SW8260ug/Kg2.6
QA/QC Surrogates103% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%95% Bromofluorobenzene 04/11/14 U 70 - 130 %%106% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 240 04/10/14 DD SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 240 04/10/14 DD SW 8270ug/Kg100ND1,2-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg95ND1,2-Diphenylhydrazine 240 04/10/14 DD SW 8270ug/Kg110ND1,3-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg99ND1,4-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg99ND2,4,5-Trichlorophenol 240 04/10/14 DD SW 8270ug/Kg180ND2,4,6-Trichlorophenol 240 04/10/14 DD SW 8270ug/Kg110ND2,4-Dichlorophenol 240 04/10/14 DD SW 8270ug/Kg120ND2,4-Dimethylphenol 240 04/10/14 DD SW 8270ug/Kg83ND2,4-Dinitrophenol 1700 04/10/14 DD SW 8270ug/Kg240ND2,4-Dinitrotoluene 240 04/10/14 DD SW 8270ug/Kg130ND2,6-Dinitrotoluene 240 04/10/14 DD SW 8270ug/Kg110ND2-Chloronaphthalene 240 04/10/14 DD SW 8270ug/Kg95ND2-Chlorophenol 240 04/10/14 DD SW 8270ug/Kg95ND2-Methylnaphthalene 240 04/10/14 DD SW 8270ug/Kg100ND2-Methylphenol (o-cresol) 240 04/10/14 DD SW 8270ug/Kg160ND2-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg340ND2-Nitrophenol 240 04/10/14 DD SW 8270ug/Kg210ND3&4-Methylphenol (m&p-cresol) 240 04/10/14 DD SW 8270ug/Kg 1130ND3,3'-Dichlorobenzidine 670 04/10/14 DD SW 8270ug/Kg160
Page 14 of 49 Ver 1
E-SB2 29-31Phoenix I.D.: BG30365
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND3-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg730ND4,6-Dinitro-2-methylphenol 1700 04/10/14 DD SW 8270ug/Kg360ND4-Bromophenyl phenyl ether 240 04/10/14 DD SW 8270ug/Kg99ND4-Chloro-3-methylphenol 240 04/10/14 DD SW 8270ug/Kg120ND4-Chloroaniline 670 04/10/14 DD SW 8270ug/Kg160ND4-Chlorophenyl phenyl ether 240 04/10/14 DD SW 8270ug/Kg110ND4-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg110ND4-Nitrophenol 1700 04/10/14 DD SW 8270ug/Kg150NDAcenaphthene 240 04/10/14 DD SW 8270ug/Kg100NDAcenaphthylene 240 04/10/14 DD SW 8270ug/Kg94NDAcetophenone 240 04/10/14 DD SW 8270ug/Kg100NDAniline 1700 04/10/14 DD SW 8270ug/Kg680NDAnthracene 240 04/10/14 DD SW 8270ug/Kg110NDBenz(a)anthracene 240 04/10/14 DD SW 8270ug/Kg110NDBenzidine 670 04/10/14 DD SW 8270ug/Kg200NDBenzo(a)pyrene 240 04/10/14 DD SW 8270ug/Kg110NDBenzo(b)fluoranthene 240 04/10/14 DD SW 8270ug/Kg110NDBenzo(ghi)perylene 240 04/10/14 DD SW 8270ug/Kg110NDBenzo(k)fluoranthene 240 04/10/14 DD SW 8270ug/Kg110NDBenzoic acid 1700 04/10/14 DD SW 8270ug/Kg 1670NDBenzyl butyl phthalate 240 04/10/14 DD SW 8270ug/Kg87NDBis(2-chloroethoxy)methane 240 04/10/14 DD SW 8270ug/Kg93NDBis(2-chloroethyl)ether 240 04/10/14 DD SW 8270ug/Kg91NDBis(2-chloroisopropyl)ether 240 04/10/14 DD SW 8270ug/Kg 193NDBis(2-ethylhexyl)phthalate 240 04/10/14 DD SW 8270ug/Kg97NDCarbazole 1700 04/10/14 DD SW 8270ug/Kg250NDChrysene 240 04/10/14 DD SW 8270ug/Kg110NDDibenz(a,h)anthracene 240 04/10/14 DD SW 8270ug/Kg110NDDibenzofuran 240 04/10/14 DD SW 8270ug/Kg98NDDiethyl phthalate 240 04/10/14 DD SW 8270ug/Kg110NDDimethylphthalate 240 04/10/14 DD SW 8270ug/Kg100NDDi-n-butylphthalate 240 04/10/14 DD SW 8270ug/Kg89NDDi-n-octylphthalate 240 04/10/14 DD SW 8270ug/Kg87NDFluoranthene 240 04/10/14 DD SW 8270ug/Kg110NDFluorene 240 04/10/14 DD SW 8270ug/Kg110NDHexachlorobenzene 240 04/10/14 DD SW 8270ug/Kg98NDHexachlorobutadiene 240 04/10/14 DD SW 8270ug/Kg120NDHexachlorocyclopentadiene 240 04/10/14 DD SW 8270ug/Kg100NDHexachloroethane 240 04/10/14 DD SW 8270ug/Kg100NDIndeno(1,2,3-cd)pyrene 240 04/10/14 DD SW 8270ug/Kg110NDIsophorone 240 04/10/14 DD SW 8270ug/Kg94NDNaphthalene 240 04/10/14 DD SW 8270ug/Kg97NDNitrobenzene 240 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodimethylamine 240 04/10/14 DD SW 8270ug/Kg95NDN-Nitrosodi-n-propylamine 240 04/10/14 DD SW 8270ug/Kg110NDN-Nitrosodiphenylamine 240 04/10/14 DD SW 8270ug/Kg130NDPentachloronitrobenzene 240 04/10/14 DD SW 8270ug/Kg120NDPentachlorophenol 240 04/10/14 DD SW 8270ug/Kg130NDPhenanthrene 240 04/10/14 DD SW 8270ug/Kg96
Page 15 of 49 Ver 1
E-SB2 29-31Phoenix I.D.: BG30365
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDPhenol 240 04/10/14 DD SW 8270ug/Kg110NDPyrene 240 04/10/14 DD SW 8270ug/Kg120NDPyridine 240 04/10/14 DD SW 8270ug/Kg83
QA/QC Surrogates92% 2,4,6-Tribromophenol 04/10/14 DD 30 - 130 %%59% 2-Fluorobiphenyl 04/10/14 DD 30 - 130 %%85% 2-Fluorophenol 04/10/14 DD 30 - 130 %%56% Nitrobenzene-d5 04/10/14 DD 30 - 130 %%86% Phenol-d5 04/10/14 DD 30 - 130 %%58% Terphenyl-d14 04/10/14 DD 30 - 130 %%
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 16 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB6 0-2
Phoenix ID: BG30366
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.34Silver 0.34 04/11/14 LK SW6010mg/Kg0.205240Aluminum 34 04/11/14 LK SW6010mg/Kg6.74.8Arsenic 0.7 04/11/14 LK SW6010mg/Kg0.67
82.3Barium 0.7 04/11/14 LK SW6010mg/Kg0.13< 0.27Beryllium 0.27 04/11/14 LK SW6010mg/Kg0.1350400Calcium 34 04/11/14 LK SW6010mg/Kg310.44Cadmium 0.34 04/11/14 LK SW6010mg/Kg0.133.71Cobalt 0.34 04/11/14 LK SW6010mg/Kg0.1313.1Chromium 0.34 04/11/14 LK SW6010mg/Kg0.1342.3Copper 0.34 04/11/14 LK SW6010mg/kg0.27
14800Iron 34 04/11/14 LK SW6010mg/Kg B340.34Mercury 0.06 04/10/14 RS SW-7471mg/Kg0.04966Potassium 7 04/11/14 LK SW6010mg/Kg2.6
12000Magnesium 34 04/11/14 LK SW6010mg/Kg2.0209Manganese 3.4 04/11/14 LK SW6010mg/Kg1.3251Sodium 7 04/11/14 LK SW6010mg/Kg2.914.0Nickel 0.34 04/11/14 LK SW6010mg/Kg0.13156Lead 6.7 04/11/14 LK SW6010mg/Kg2.0
< 3.0Antimony 3.0 04/11/14 LK SW6010mg/Kg3.0< 1.3Selenium 1.3 04/11/14 LK SW6010mg/Kg1.1< 1.3Thallium 1.3 04/11/14 LK SW6010mg/Kg1.328.7Vanadium 0.3 04/11/14 LK SW6010mg/Kg0.13130Zinc 0.7 04/11/14 LK SW6010mg/Kg0.3491Percent Solid 04/09/14 I E160.3%
CompletedSoil Extraction for PCB 04/09/14 BB/V SW3545CompletedSoil Extraction for Pesticide 04/09/14 BB SW3545CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471
Page 17 of 49 Ver 1
E-SB6 0-2Phoenix I.D.: BG30366
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
CompletedTotal Metals Digest 04/09/14 CB/AG/W SW846 - 3050
CompletedField Extraction 04/08/14 SW5035
Polychlorinated BiphenylsNDPCB-1016 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1221 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1232 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1242 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1248 36 04/10/14 AW SW 8082ug/Kg36210PCB-1254 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1260 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1262 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1268 36 04/10/14 AW SW 8082ug/Kg36
QA/QC Surrogates86% DCBP 04/10/14 AW 30 - 150 %%76% TCMX 04/10/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 04/14/14 CE SW8081ug/Kg2.6244,4' -DDT 2.6 04/14/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDAldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDChlordane 22 04/14/14 CE SW8081ug/Kg22NDd-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan II 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan sulfate 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin ketone 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDHeptachlor 1.8 04/14/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 04/14/14 CE SW8081ug/Kg1.8NDMethoxychlor 7.3 04/14/14 CE SW8081ug/Kg7.3NDToxaphene 180 04/14/14 CE SW8081ug/Kg180
QA/QC Surrogates140% DCBP 04/14/14 CE 30 - 150 %%83% TCMX 04/14/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 5.4 04/11/14 JLI SW8260ug/Kg0.88ND1,1,1-Trichloroethane 5.4 04/11/14 JLI SW8260ug/Kg1.1ND1,1,2,2-Tetrachloroethane 5.4 04/11/14 JLI SW8260ug/Kg0.76ND1,1,2-Trichloroethane 5.4 04/11/14 JLI SW8260ug/Kg0.53ND1,1-Dichloroethane 5.4 04/11/14 JLI SW8260ug/Kg1.1
Page 18 of 49 Ver 1
E-SB6 0-2Phoenix I.D.: BG30366
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 5.4 04/11/14 JLI SW8260ug/Kg1.2ND1,1-Dichloropropene 5.4 04/11/14 JLI SW8260ug/Kg1.0ND1,2,3-Trichlorobenzene 280 04/11/14 JLI SW8260ug/Kg56ND1,2,3-Trichloropropane 280 04/11/14 JLI SW8260ug/Kg40ND1,2,4-Trichlorobenzene 280 04/11/14 JLI SW8260ug/Kg56ND1,2,4-Trimethylbenzene 280 04/11/14 JLI SW8260ug/Kg41ND1,2-Dibromo-3-chloropropane 280 04/11/14 JLI SW8260ug/Kg76ND1,2-Dibromoethane 5.4 04/11/14 JLI SW8260ug/Kg1.4ND1,2-Dichlorobenzene 280 04/11/14 JLI SW8260ug/Kg31ND1,2-Dichloroethane 5.4 04/11/14 JLI SW8260ug/Kg0.47ND1,2-Dichloropropane 5.4 04/11/14 JLI SW8260ug/Kg0.76ND1,3,5-Trimethylbenzene 280 04/11/14 JLI SW8260ug/Kg37ND1,3-Dichlorobenzene 280 04/11/14 JLI SW8260ug/Kg42ND1,3-Dichloropropane 5.4 04/11/14 JLI SW8260ug/Kg0.57ND1,4-Dichlorobenzene 280 04/11/14 JLI SW8260ug/Kg45ND2,2-Dichloropropane 5.4 04/11/14 JLI SW8260ug/Kg0.90ND2-Chlorotoluene 280 04/11/14 JLI SW8260ug/Kg45ND2-Hexanone 27 04/11/14 JLI SW8260ug/Kg2.4ND2-Isopropyltoluene 280 04/11/14 JLI SW8260ug/Kg 139ND4-Chlorotoluene 280 04/11/14 JLI SW8260ug/Kg33ND4-Methyl-2-pentanone 27 04/11/14 JLI SW8260ug/Kg1.368Acetone 54 04/11/14 JLI SW8260ug/Kg5.4NDAcrylonitrile 11 04/11/14 JLI SW8260ug/Kg3.0NDBenzene 5.4 04/11/14 JLI SW8260ug/Kg1.1NDBromobenzene 280 04/11/14 JLI SW8260ug/Kg37NDBromochloromethane 5.4 04/11/14 JLI SW8260ug/Kg0.79NDBromodichloromethane 5.4 04/11/14 JLI SW8260ug/Kg0.67NDBromoform 5.4 04/11/14 JLI SW8260ug/Kg0.75NDBromomethane 5.4 04/11/14 JLI SW8260ug/Kg4.1NDCarbon Disulfide 5.4 04/11/14 JLI SW8260ug/Kg0.87NDCarbon tetrachloride 5.4 04/11/14 JLI SW8260ug/Kg0.62NDChlorobenzene 5.4 04/11/14 JLI SW8260ug/Kg0.80NDChloroethane 5.4 04/11/14 JLI SW8260ug/Kg1.3NDChloroform 5.4 04/11/14 JLI SW8260ug/Kg0.98NDChloromethane 5.4 04/11/14 JLI SW8260ug/Kg2.8NDcis-1,2-Dichloroethene 5.4 04/11/14 JLI SW8260ug/Kg1.2NDcis-1,3-Dichloropropene 5.4 04/11/14 JLI SW8260ug/Kg0.58NDDibromochloromethane 5.4 04/11/14 JLI SW8260ug/Kg0.60NDDibromomethane 5.4 04/11/14 JLI SW8260ug/Kg0.68NDDichlorodifluoromethane 5.4 04/11/14 JLI SW8260ug/Kg1.4NDEthylbenzene 5.4 04/11/14 JLI SW8260ug/Kg0.98NDHexachlorobutadiene 280 04/11/14 JLI SW8260ug/Kg59NDIsopropylbenzene 280 04/11/14 JLI SW8260ug/Kg54NDm&p-Xylene 5.4 04/11/14 JLI SW8260ug/Kg2.1NDMethyl Ethyl Ketone 32 04/11/14 JLI SW8260ug/Kg4.7NDMethyl t-butyl ether (MTBE) 11 04/11/14 JLI SW8260ug/Kg1.5NDMethylene chloride 5.4 04/11/14 JLI SW8260ug/Kg0.88NDNaphthalene 280 04/11/14 JLI SW8260ug/Kg76NDn-Butylbenzene 280 04/11/14 JLI SW8260ug/Kg51
Page 19 of 49 Ver 1
E-SB6 0-2Phoenix I.D.: BG30366
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 280 04/11/14 JLI SW8260ug/Kg51NDo-Xylene 5.4 04/11/14 JLI SW8260ug/Kg2.1NDp-Isopropyltoluene 280 04/11/14 JLI SW8260ug/Kg41NDsec-Butylbenzene 280 04/11/14 JLI SW8260ug/Kg53NDStyrene 5.4 04/11/14 JLI SW8260ug/Kg1.6NDtert-Butylbenzene 280 04/11/14 JLI SW8260ug/Kg45NDTetrachloroethene 5.4 04/11/14 JLI SW8260ug/Kg1.1NDTetrahydrofuran (THF) 11 04/11/14 JLI SW8260ug/Kg 14.8NDToluene 5.4 04/11/14 JLI SW8260ug/Kg0.85NDtrans-1,2-Dichloroethene 5.4 04/11/14 JLI SW8260ug/Kg1.1NDtrans-1,3-Dichloropropene 5.4 04/11/14 JLI SW8260ug/Kg1.1NDtrans-1,4-dichloro-2-butene 560 04/11/14 JLI SW8260ug/Kg520NDTrichloroethene 5.4 04/11/14 JLI SW8260ug/Kg1.1NDTrichlorofluoromethane 5.4 04/11/14 JLI SW8260ug/Kg1.2NDTrichlorotrifluoroethane 5.4 04/11/14 JLI SW8260ug/Kg0.84NDVinyl chloride 5.4 04/11/14 JLI SW8260ug/Kg1.7
QA/QC Surrogates101% 1,2-dichlorobenzene-d4 04/11/14 JLI 70 - 130 %%97% Bromofluorobenzene 04/11/14 JLI 70 - 130 %%102% Dibromofluoromethane 04/11/14 JLI 70 - 130 %%96% Toluene-d8 04/11/14 JLI 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 1300 04/11/14 DD SW 8270ug/Kg630ND1,2,4-Trichlorobenzene 1300 04/11/14 DD SW 8270ug/Kg540ND1,2-Dichlorobenzene 1300 04/11/14 DD SW 8270ug/Kg500ND1,2-Diphenylhydrazine 1300 04/11/14 DD SW 8270ug/Kg580ND1,3-Dichlorobenzene 1300 04/11/14 DD SW 8270ug/Kg530ND1,4-Dichlorobenzene 1300 04/11/14 DD SW 8270ug/Kg530ND2,4,5-Trichlorophenol 1300 04/11/14 DD SW 8270ug/Kg980ND2,4,6-Trichlorophenol 1300 04/11/14 DD SW 8270ug/Kg570ND2,4-Dichlorophenol 1300 04/11/14 DD SW 8270ug/Kg630ND2,4-Dimethylphenol 1300 04/11/14 DD SW 8270ug/Kg440ND2,4-Dinitrophenol 8900 04/11/14 DD SW 8270ug/Kg1300ND2,4-Dinitrotoluene 1300 04/11/14 DD SW 8270ug/Kg700ND2,6-Dinitrotoluene 1300 04/11/14 DD SW 8270ug/Kg560ND2-Chloronaphthalene 1300 04/11/14 DD SW 8270ug/Kg510ND2-Chlorophenol 1300 04/11/14 DD SW 8270ug/Kg510ND2-Methylnaphthalene 1300 04/11/14 DD SW 8270ug/Kg530ND2-Methylphenol (o-cresol) 1300 04/11/14 DD SW 8270ug/Kg840ND2-Nitroaniline 8900 04/11/14 DD SW 8270ug/Kg1800ND2-Nitrophenol 1300 04/11/14 DD SW 8270ug/Kg1100ND3&4-Methylphenol (m&p-cresol) 1300 04/11/14 DD SW 8270ug/Kg 1700ND3,3'-Dichlorobenzidine 3600 04/11/14 DD SW 8270ug/Kg840ND3-Nitroaniline 8900 04/11/14 DD SW 8270ug/Kg3900ND4,6-Dinitro-2-methylphenol 8900 04/11/14 DD SW 8270ug/Kg1900ND4-Bromophenyl phenyl ether 1300 04/11/14 DD SW 8270ug/Kg530ND4-Chloro-3-methylphenol 1300 04/11/14 DD SW 8270ug/Kg630ND4-Chloroaniline 3600 04/11/14 DD SW 8270ug/Kg830ND4-Chlorophenyl phenyl ether 1300 04/11/14 DD SW 8270ug/Kg600
Page 20 of 49 Ver 1
E-SB6 0-2Phoenix I.D.: BG30366
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Nitroaniline 8900 04/11/14 DD SW 8270ug/Kg600ND4-Nitrophenol 8900 04/11/14 DD SW 8270ug/Kg810NDAcenaphthene 1300 04/11/14 DD SW 8270ug/Kg540NDAcenaphthylene 1300 04/11/14 DD SW 8270ug/Kg500NDAcetophenone 1300 04/11/14 DD SW 8270ug/Kg560NDAniline 8900 04/11/14 DD SW 8270ug/Kg3600NDAnthracene 1300 04/11/14 DD SW 8270ug/Kg590
1800Benz(a)anthracene 1300 04/11/14 DD SW 8270ug/Kg600NDBenzidine 3600 04/11/14 DD SW 8270ug/Kg1100
1800Benzo(a)pyrene 1300 04/11/14 DD SW 8270ug/Kg5802300Benzo(b)fluoranthene 1300 04/11/14 DD SW 8270ug/Kg610640Benzo(ghi)perylene 1300 04/11/14 DD SW 8270ug/Kg580J990Benzo(k)fluoranthene 1300 04/11/14 DD SW 8270ug/Kg590JNDBenzoic acid 8900 04/11/14 DD SW 8270ug/Kg 13600NDBenzyl butyl phthalate 1300 04/11/14 DD SW 8270ug/Kg460NDBis(2-chloroethoxy)methane 1300 04/11/14 DD SW 8270ug/Kg490NDBis(2-chloroethyl)ether 1300 04/11/14 DD SW 8270ug/Kg480NDBis(2-chloroisopropyl)ether 1300 04/11/14 DD SW 8270ug/Kg 1500NDBis(2-ethylhexyl)phthalate 1300 04/11/14 DD SW 8270ug/Kg510NDCarbazole 8900 04/11/14 DD SW 8270ug/Kg1400
1800Chrysene 1300 04/11/14 DD SW 8270ug/Kg600NDDibenz(a,h)anthracene 1300 04/11/14 DD SW 8270ug/Kg580NDDibenzofuran 1300 04/11/14 DD SW 8270ug/Kg520NDDiethyl phthalate 1300 04/11/14 DD SW 8270ug/Kg560NDDimethylphthalate 1300 04/11/14 DD SW 8270ug/Kg550NDDi-n-butylphthalate 1300 04/11/14 DD SW 8270ug/Kg480NDDi-n-octylphthalate 1300 04/11/14 DD SW 8270ug/Kg460
2400Fluoranthene 1300 04/11/14 DD SW 8270ug/Kg580NDFluorene 1300 04/11/14 DD SW 8270ug/Kg590NDHexachlorobenzene 1300 04/11/14 DD SW 8270ug/Kg520NDHexachlorobutadiene 1300 04/11/14 DD SW 8270ug/Kg650NDHexachlorocyclopentadiene 1300 04/11/14 DD SW 8270ug/Kg550NDHexachloroethane 1300 04/11/14 DD SW 8270ug/Kg540NDIndeno(1,2,3-cd)pyrene 1300 04/11/14 DD SW 8270ug/Kg590NDIsophorone 1300 04/11/14 DD SW 8270ug/Kg500NDNaphthalene 1300 04/11/14 DD SW 8270ug/Kg510NDNitrobenzene 1300 04/11/14 DD SW 8270ug/Kg630NDN-Nitrosodimethylamine 1300 04/11/14 DD SW 8270ug/Kg500NDN-Nitrosodi-n-propylamine 1300 04/11/14 DD SW 8270ug/Kg580NDN-Nitrosodiphenylamine 1300 04/11/14 DD SW 8270ug/Kg690NDPentachloronitrobenzene 1300 04/11/14 DD SW 8270ug/Kg660NDPentachlorophenol 1300 04/11/14 DD SW 8270ug/Kg680
1200Phenanthrene 1300 04/11/14 DD SW 8270ug/Kg510JNDPhenol 1300 04/11/14 DD SW 8270ug/Kg570
2700Pyrene 1300 04/11/14 DD SW 8270ug/Kg610NDPyridine 1300 04/11/14 DD SW 8270ug/Kg440
QA/QC Surrogates79% 2,4,6-Tribromophenol 04/11/14 DD 30 - 130 %%53% 2-Fluorobiphenyl 04/11/14 DD 30 - 130 %%
Page 21 of 49 Ver 1
E-SB6 0-2Phoenix I.D.: BG30366
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
68% 2-Fluorophenol 04/11/14 DD 30 - 130 %%54% Nitrobenzene-d5 04/11/14 DD 30 - 130 %%77% Phenol-d5 04/11/14 DD 30 - 130 %%60% Terphenyl-d14 04/11/14 DD 30 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Semi-Volatile Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, a dilution was required resulting in an elevated RL for the semivolatile analysis.
Volatile Comment:There was a suppression of the last internal standard in the low level analysis, all affected compounds are reported from the methanol preserved high level analysis which did not exhibit this interference.
For Pesticides, due to matrix interference caused by the presence of PCBs in the samples an elevated MDL was reported.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 22 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB6 15-17
Phoenix ID: BG30367
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.32Silver 0.32 04/11/14 LK SW6010mg/Kg0.196770Aluminum 32 04/11/14 LK SW6010mg/Kg6.51.4Arsenic 0.6 04/11/14 LK SW6010mg/Kg0.65
45.4Barium 0.6 04/11/14 LK SW6010mg/Kg0.130.35Beryllium 0.26 04/11/14 LK SW6010mg/Kg0.132730Calcium 3.2 04/11/14 LK SW6010mg/Kg3.0
< 0.32Cadmium 0.32 04/11/14 LK SW6010mg/Kg0.135.18Cobalt 0.32 04/11/14 LK SW6010mg/Kg0.1327.4Chromium 0.32 04/11/14 LK SW6010mg/Kg0.1318.9Copper 0.32 04/11/14 LK SW6010mg/kg0.26
15300Iron 32 04/11/14 LK SW6010mg/Kg B32< 0.06Mercury 0.06 04/10/14 RS SW-7471mg/Kg0.041480Potassium 6 04/11/14 LK SW6010mg/Kg2.52950Magnesium 32 04/11/14 LK SW6010mg/Kg1.9357Manganese 3.2 04/11/14 LK SW6010mg/Kg1.3194Sodium 6 04/11/14 LK SW6010mg/Kg2.812.3Nickel 0.32 04/11/14 LK SW6010mg/Kg0.136.6Lead 0.6 04/11/14 LK SW6010mg/Kg0.19
< 1.6Antimony 1.6 04/11/14 LK SW6010mg/Kg0.65< 1.3Selenium 1.3 04/11/14 LK SW6010mg/Kg1.1< 1.3Thallium 1.3 04/11/14 LK SW6010mg/Kg1.330.3Vanadium 0.3 04/11/14 LK SW6010mg/Kg0.1325.0Zinc 0.6 04/11/14 LK SW6010mg/Kg0.3292Percent Solid 04/09/14 I E160.3%
CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471CompletedTotal Metals Digest 04/09/14 CB/AG/W SW846 - 3050
CompletedField Extraction 04/08/14 SW5035
Page 23 of 49 Ver 1
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 7.3 04/11/14 U SW8260ug/Kg1.2ND1,1,1-Trichloroethane 7.3 04/11/14 U SW8260ug/Kg1.5ND1,1,2,2-Tetrachloroethane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,1,2-Trichloroethane 7.3 04/11/14 U SW8260ug/Kg0.71ND1,1-Dichloroethane 7.3 04/11/14 U SW8260ug/Kg1.4ND1,1-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.6ND1,1-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg1.4ND1,2,3-Trichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.5ND1,2,3-Trichloropropane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,2,4-Trichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.5ND1,2,4-Trimethylbenzene 7.3 04/11/14 U SW8260ug/Kg1.0ND1,2-Dibromo-3-chloropropane 7.3 04/11/14 U SW8260ug/Kg2.0ND1,2-Dibromoethane 7.3 04/11/14 U SW8260ug/Kg1.9ND1,2-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg0.80ND1,2-Dichloroethane 7.3 04/11/14 U SW8260ug/Kg0.64ND1,2-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,3,5-Trimethylbenzene 7.3 04/11/14 U SW8260ug/Kg0.96ND1,3-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg0.77ND1,4-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.2ND2,2-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg1.2ND2-Chlorotoluene 7.3 04/11/14 U SW8260ug/Kg1.2ND2-Hexanone 36 04/11/14 U SW8260ug/Kg3.3ND2-Isopropyltoluene 7.3 04/11/14 U SW8260ug/Kg 11.0ND4-Chlorotoluene 7.3 04/11/14 U SW8260ug/Kg0.84ND4-Methyl-2-pentanone 36 04/11/14 U SW8260ug/Kg1.7NDAcetone 50 04/11/14 U SW8260ug/Kg7.2NDAcrylonitrile 15 04/11/14 U SW8260ug/Kg4.1NDBenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDBromobenzene 7.3 04/11/14 U SW8260ug/Kg0.95NDBromochloromethane 7.3 04/11/14 U SW8260ug/Kg1.1NDBromodichloromethane 7.3 04/11/14 U SW8260ug/Kg0.90NDBromoform 7.3 04/11/14 U SW8260ug/Kg1.0NDBromomethane 7.3 04/11/14 U SW8260ug/Kg5.6NDCarbon Disulfide 7.3 04/11/14 U SW8260ug/Kg1.2NDCarbon tetrachloride 7.3 04/11/14 U SW8260ug/Kg0.84NDChlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.1NDChloroethane 7.3 04/11/14 U SW8260ug/Kg1.7NDChloroform 7.3 04/11/14 U SW8260ug/Kg1.3NDChloromethane 7.3 04/11/14 U SW8260ug/Kg3.8NDcis-1,2-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.6NDcis-1,3-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg0.79NDDibromochloromethane 7.3 04/11/14 U SW8260ug/Kg0.82NDDibromomethane 7.3 04/11/14 U SW8260ug/Kg0.92NDDichlorodifluoromethane 7.3 04/11/14 U SW8260ug/Kg1.9NDEthylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDHexachlorobutadiene 7.3 04/11/14 U SW8260ug/Kg1.5NDIsopropylbenzene 7.3 04/11/14 U SW8260ug/Kg1.4
Page 24 of 49 Ver 1
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 7.3 04/11/14 U SW8260ug/Kg2.9NDMethyl Ethyl Ketone 44 04/11/14 U SW8260ug/Kg6.3NDMethyl t-butyl ether (MTBE) 15 04/11/14 U SW8260ug/Kg2.0NDMethylene chloride 7.3 04/11/14 U SW8260ug/Kg1.2NDNaphthalene 7.3 04/11/14 U SW8260ug/Kg2.0NDn-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDn-Propylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDo-Xylene 7.3 04/11/14 U SW8260ug/Kg2.8NDp-Isopropyltoluene 7.3 04/11/14 U SW8260ug/Kg1.0NDsec-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDStyrene 7.3 04/11/14 U SW8260ug/Kg2.1NDtert-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.2NDTetrachloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDTetrahydrofuran (THF) 15 04/11/14 U SW8260ug/Kg 16.6NDToluene 7.3 04/11/14 U SW8260ug/Kg1.2NDtrans-1,2-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,3-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,4-dichloro-2-butene 15 04/11/14 U SW8260ug/Kg14NDTrichloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDTrichlorofluoromethane 7.3 04/11/14 U SW8260ug/Kg1.6NDTrichlorotrifluoroethane 7.3 04/11/14 U SW8260ug/Kg1.1NDVinyl chloride 7.3 04/11/14 U SW8260ug/Kg2.4
QA/QC Surrogates105% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%100% Bromofluorobenzene 04/11/14 U 70 - 130 %%114% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 250 04/10/14 DD SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 250 04/10/14 DD SW 8270ug/Kg110ND1,2-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg99ND1,2-Diphenylhydrazine 250 04/10/14 DD SW 8270ug/Kg110ND1,3-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg100ND1,4-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg100ND2,4,5-Trichlorophenol 250 04/10/14 DD SW 8270ug/Kg190ND2,4,6-Trichlorophenol 250 04/10/14 DD SW 8270ug/Kg110ND2,4-Dichlorophenol 250 04/10/14 DD SW 8270ug/Kg120ND2,4-Dimethylphenol 250 04/10/14 DD SW 8270ug/Kg87ND2,4-Dinitrophenol 1800 04/10/14 DD SW 8270ug/Kg250ND2,4-Dinitrotoluene 250 04/10/14 DD SW 8270ug/Kg140ND2,6-Dinitrotoluene 250 04/10/14 DD SW 8270ug/Kg110ND2-Chloronaphthalene 250 04/10/14 DD SW 8270ug/Kg100ND2-Chlorophenol 250 04/10/14 DD SW 8270ug/Kg100ND2-Methylnaphthalene 250 04/10/14 DD SW 8270ug/Kg100ND2-Methylphenol (o-cresol) 250 04/10/14 DD SW 8270ug/Kg170ND2-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg360ND2-Nitrophenol 250 04/10/14 DD SW 8270ug/Kg220ND3&4-Methylphenol (m&p-cresol) 250 04/10/14 DD SW 8270ug/Kg 1140ND3,3'-Dichlorobenzidine 700 04/10/14 DD SW 8270ug/Kg170
Page 25 of 49 Ver 1
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND3-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg760ND4,6-Dinitro-2-methylphenol 1800 04/10/14 DD SW 8270ug/Kg380ND4-Bromophenyl phenyl ether 250 04/10/14 DD SW 8270ug/Kg100ND4-Chloro-3-methylphenol 250 04/10/14 DD SW 8270ug/Kg120ND4-Chloroaniline 700 04/10/14 DD SW 8270ug/Kg160ND4-Chlorophenyl phenyl ether 250 04/10/14 DD SW 8270ug/Kg120ND4-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg120ND4-Nitrophenol 1800 04/10/14 DD SW 8270ug/Kg160NDAcenaphthene 250 04/10/14 DD SW 8270ug/Kg110NDAcenaphthylene 250 04/10/14 DD SW 8270ug/Kg98NDAcetophenone 250 04/10/14 DD SW 8270ug/Kg110NDAniline 1800 04/10/14 DD SW 8270ug/Kg710NDAnthracene 250 04/10/14 DD SW 8270ug/Kg120NDBenz(a)anthracene 250 04/10/14 DD SW 8270ug/Kg120NDBenzidine 700 04/10/14 DD SW 8270ug/Kg210NDBenzo(a)pyrene 250 04/10/14 DD SW 8270ug/Kg110NDBenzo(b)fluoranthene 250 04/10/14 DD SW 8270ug/Kg120NDBenzo(ghi)perylene 250 04/10/14 DD SW 8270ug/Kg110NDBenzo(k)fluoranthene 250 04/10/14 DD SW 8270ug/Kg120NDBenzoic acid 1800 04/10/14 DD SW 8270ug/Kg 1700NDBenzyl butyl phthalate 250 04/10/14 DD SW 8270ug/Kg91NDBis(2-chloroethoxy)methane 250 04/10/14 DD SW 8270ug/Kg97NDBis(2-chloroethyl)ether 250 04/10/14 DD SW 8270ug/Kg95NDBis(2-chloroisopropyl)ether 250 04/10/14 DD SW 8270ug/Kg 198NDBis(2-ethylhexyl)phthalate 250 04/10/14 DD SW 8270ug/Kg100NDCarbazole 1800 04/10/14 DD SW 8270ug/Kg270NDChrysene 250 04/10/14 DD SW 8270ug/Kg120NDDibenz(a,h)anthracene 250 04/10/14 DD SW 8270ug/Kg110NDDibenzofuran 250 04/10/14 DD SW 8270ug/Kg100NDDiethyl phthalate 250 04/10/14 DD SW 8270ug/Kg110NDDimethylphthalate 250 04/10/14 DD SW 8270ug/Kg110NDDi-n-butylphthalate 250 04/10/14 DD SW 8270ug/Kg94NDDi-n-octylphthalate 250 04/10/14 DD SW 8270ug/Kg91NDFluoranthene 250 04/10/14 DD SW 8270ug/Kg110NDFluorene 250 04/10/14 DD SW 8270ug/Kg120NDHexachlorobenzene 250 04/10/14 DD SW 8270ug/Kg100NDHexachlorobutadiene 250 04/10/14 DD SW 8270ug/Kg130NDHexachlorocyclopentadiene 250 04/10/14 DD SW 8270ug/Kg110NDHexachloroethane 250 04/10/14 DD SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 250 04/10/14 DD SW 8270ug/Kg120NDIsophorone 250 04/10/14 DD SW 8270ug/Kg98NDNaphthalene 250 04/10/14 DD SW 8270ug/Kg100NDNitrobenzene 250 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodimethylamine 250 04/10/14 DD SW 8270ug/Kg99NDN-Nitrosodi-n-propylamine 250 04/10/14 DD SW 8270ug/Kg110NDN-Nitrosodiphenylamine 250 04/10/14 DD SW 8270ug/Kg130NDPentachloronitrobenzene 250 04/10/14 DD SW 8270ug/Kg130NDPentachlorophenol 250 04/10/14 DD SW 8270ug/Kg130NDPhenanthrene 250 04/10/14 DD SW 8270ug/Kg100
Page 26 of 49 Ver 1
E-SB6 15-17Phoenix I.D.: BG30367
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDPhenol 250 04/10/14 DD SW 8270ug/Kg110NDPyrene 250 04/10/14 DD SW 8270ug/Kg120NDPyridine 250 04/10/14 DD SW 8270ug/Kg86
QA/QC Surrogates80% 2,4,6-Tribromophenol 04/10/14 DD 30 - 130 %%55% 2-Fluorobiphenyl 04/10/14 DD 30 - 130 %%77% 2-Fluorophenol 04/10/14 DD 30 - 130 %%51% Nitrobenzene-d5 04/10/14 DD 30 - 130 %%82% Phenol-d5 04/10/14 DD 30 - 130 %%56% Terphenyl-d14 04/10/14 DD 30 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 27 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB7 0-2
Phoenix ID: BG30368
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.39Silver 0.39 04/11/14 LK SW6010mg/Kg0.2310500Aluminum 39 04/11/14 LK SW6010mg/Kg7.712.2Arsenic 0.8 04/11/14 LK SW6010mg/Kg0.7775.4Barium 0.8 04/11/14 LK SW6010mg/Kg0.150.38Beryllium 0.31 04/11/14 LK SW6010mg/Kg0.15
62000Calcium 39 04/11/14 LK SW6010mg/Kg35< 0.39Cadmium 0.39 04/11/14 LK SW6010mg/Kg0.153.03Cobalt 0.39 04/11/14 LK SW6010mg/Kg0.1510.6Chromium 0.39 04/11/14 LK SW6010mg/Kg0.1525.8Copper 0.39 04/11/14 LK SW6010mg/kg0.31
15100Iron 39 04/11/14 LK SW6010mg/Kg B390.14Mercury 0.07 04/10/14 RS SW-7471mg/Kg0.041230Potassium 8 04/11/14 LK SW6010mg/Kg3.06150Magnesium 39 04/11/14 LK SW6010mg/Kg2.3328Manganese 3.9 04/11/14 LK SW6010mg/Kg1.5
1280Sodium 8 04/11/14 LK SW6010mg/Kg3.38.69Nickel 0.39 04/11/14 LK SW6010mg/Kg0.15174Lead 7.7 04/11/14 LK SW6010mg/Kg2.3
< 1.9Antimony 1.9 04/11/14 LK SW6010mg/Kg0.77< 1.5Selenium 1.5 04/11/14 LK SW6010mg/Kg1.3< 1.5Thallium 1.5 04/11/14 LK SW6010mg/Kg1.523.2Vanadium 0.4 04/11/14 LK SW6010mg/Kg0.15104Zinc 0.8 04/11/14 LK SW6010mg/Kg0.3990Percent Solid 04/09/14 I E160.3%
CompletedSoil Extraction for PCB 04/09/14 BB/V SW3545CompletedSoil Extraction for Pesticide 04/09/14 BB SW3545CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471
Page 28 of 49 Ver 1
E-SB7 0-2Phoenix I.D.: BG30368
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
CompletedTotal Metals Digest 04/09/14 CB/AG/W SW846 - 3050
CompletedField Extraction 04/08/14 SW5035
Polychlorinated BiphenylsNDPCB-1016 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1221 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1232 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1242 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1248 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1254 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1260 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1262 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1268 36 04/10/14 AW SW 8082ug/Kg36
QA/QC Surrogates54% DCBP 04/10/14 AW 30 - 150 %%44% TCMX 04/10/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDT 2.6 04/14/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDAldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDChlordane 22 04/14/14 CE SW8081ug/Kg22NDd-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan II 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan sulfate 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin ketone 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDHeptachlor 1.8 04/14/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 04/14/14 CE SW8081ug/Kg1.8NDMethoxychlor 18 04/14/14 CE SW8081ug/Kg18NDToxaphene 180 04/14/14 CE SW8081ug/Kg180
QA/QC Surrogates46% DCBP 04/14/14 CE 30 - 150 %%45% TCMX 04/14/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 7.2 04/11/14 U SW8260ug/Kg1.2ND1,1,1-Trichloroethane 7.2 04/11/14 U SW8260ug/Kg1.4ND1,1,2,2-Tetrachloroethane 7.2 04/11/14 U SW8260ug/Kg1.0ND1,1,2-Trichloroethane 7.2 04/11/14 U SW8260ug/Kg0.70ND1,1-Dichloroethane 7.2 04/11/14 U SW8260ug/Kg1.4
Page 29 of 49 Ver 1
E-SB7 0-2Phoenix I.D.: BG30368
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 7.2 04/11/14 U SW8260ug/Kg1.6ND1,1-Dichloropropene 7.2 04/11/14 U SW8260ug/Kg1.4ND1,2,3-Trichlorobenzene 7.2 04/11/14 U SW8260ug/Kg1.4ND1,2,3-Trichloropropane 7.2 04/11/14 U SW8260ug/Kg1.0ND1,2,4-Trichlorobenzene 7.2 04/11/14 U SW8260ug/Kg1.4ND1,2,4-Trimethylbenzene 7.2 04/11/14 U SW8260ug/Kg1.0ND1,2-Dibromo-3-chloropropane 7.2 04/11/14 U SW8260ug/Kg1.9ND1,2-Dibromoethane 7.2 04/11/14 U SW8260ug/Kg1.9ND1,2-Dichlorobenzene 7.2 04/11/14 U SW8260ug/Kg0.79ND1,2-Dichloroethane 7.2 04/11/14 U SW8260ug/Kg0.63ND1,2-Dichloropropane 7.2 04/11/14 U SW8260ug/Kg1.0ND1,3,5-Trimethylbenzene 7.2 04/11/14 U SW8260ug/Kg0.95ND1,3-Dichlorobenzene 7.2 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichloropropane 7.2 04/11/14 U SW8260ug/Kg0.76ND1,4-Dichlorobenzene 7.2 04/11/14 U SW8260ug/Kg1.1ND2,2-Dichloropropane 7.2 04/11/14 U SW8260ug/Kg1.2ND2-Chlorotoluene 7.2 04/11/14 U SW8260ug/Kg1.1ND2-Hexanone 36 04/11/14 U SW8260ug/Kg3.2ND2-Isopropyltoluene 7.2 04/11/14 U SW8260ug/Kg 10.99ND4-Chlorotoluene 7.2 04/11/14 U SW8260ug/Kg0.83ND4-Methyl-2-pentanone 36 04/11/14 U SW8260ug/Kg1.7NDAcetone 50 04/11/14 U SW8260ug/Kg7.1NDAcrylonitrile 14 04/11/14 U SW8260ug/Kg4.0NDBenzene 7.2 04/11/14 U SW8260ug/Kg1.4NDBromobenzene 7.2 04/11/14 U SW8260ug/Kg0.93NDBromochloromethane 7.2 04/11/14 U SW8260ug/Kg1.0NDBromodichloromethane 7.2 04/11/14 U SW8260ug/Kg0.89NDBromoform 7.2 04/11/14 U SW8260ug/Kg1.0NDBromomethane 7.2 04/11/14 U SW8260ug/Kg5.5NDCarbon Disulfide 7.2 04/11/14 U SW8260ug/Kg1.2NDCarbon tetrachloride 7.2 04/11/14 U SW8260ug/Kg0.83NDChlorobenzene 7.2 04/11/14 U SW8260ug/Kg1.1NDChloroethane 7.2 04/11/14 U SW8260ug/Kg1.7NDChloroform 7.2 04/11/14 U SW8260ug/Kg1.3NDChloromethane 7.2 04/11/14 U SW8260ug/Kg3.8NDcis-1,2-Dichloroethene 7.2 04/11/14 U SW8260ug/Kg1.6NDcis-1,3-Dichloropropene 7.2 04/11/14 U SW8260ug/Kg0.77NDDibromochloromethane 7.2 04/11/14 U SW8260ug/Kg0.80NDDibromomethane 7.2 04/11/14 U SW8260ug/Kg0.90NDDichlorodifluoromethane 7.2 04/11/14 U SW8260ug/Kg1.9NDEthylbenzene 7.2 04/11/14 U SW8260ug/Kg1.3NDHexachlorobutadiene 7.2 04/11/14 U SW8260ug/Kg1.5NDIsopropylbenzene 7.2 04/11/14 U SW8260ug/Kg1.4NDm&p-Xylene 7.2 04/11/14 U SW8260ug/Kg2.8NDMethyl Ethyl Ketone 43 04/11/14 U SW8260ug/Kg6.2NDMethyl t-butyl ether (MTBE) 14 04/11/14 U SW8260ug/Kg2.0NDMethylene chloride 7.2 04/11/14 U SW8260ug/Kg1.2NDNaphthalene 7.2 04/11/14 U SW8260ug/Kg1.9NDn-Butylbenzene 7.2 04/11/14 U SW8260ug/Kg1.3
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E-SB7 0-2Phoenix I.D.: BG30368
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 7.2 04/11/14 U SW8260ug/Kg1.3NDo-Xylene 7.2 04/11/14 U SW8260ug/Kg2.7NDp-Isopropyltoluene 7.2 04/11/14 U SW8260ug/Kg1.0NDsec-Butylbenzene 7.2 04/11/14 U SW8260ug/Kg1.3NDStyrene 7.2 04/11/14 U SW8260ug/Kg2.1NDtert-Butylbenzene 7.2 04/11/14 U SW8260ug/Kg1.1NDTetrachloroethene 7.2 04/11/14 U SW8260ug/Kg1.5NDTetrahydrofuran (THF) 14 04/11/14 U SW8260ug/Kg 16.5NDToluene 7.2 04/11/14 U SW8260ug/Kg1.1NDtrans-1,2-Dichloroethene 7.2 04/11/14 U SW8260ug/Kg1.4NDtrans-1,3-Dichloropropene 7.2 04/11/14 U SW8260ug/Kg1.5NDtrans-1,4-dichloro-2-butene 14 04/11/14 U SW8260ug/Kg13NDTrichloroethene 7.2 04/11/14 U SW8260ug/Kg1.5NDTrichlorofluoromethane 7.2 04/11/14 U SW8260ug/Kg1.6NDTrichlorotrifluoroethane 7.2 04/11/14 U SW8260ug/Kg1.1NDVinyl chloride 7.2 04/11/14 U SW8260ug/Kg2.3
QA/QC Surrogates109% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%94% Bromofluorobenzene 04/11/14 U 70 - 130 %%86% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 500 04/10/14 DD SW 8270ug/Kg250ND1,2,4-Trichlorobenzene 500 04/10/14 DD SW 8270ug/Kg220ND1,2-Dichlorobenzene 500 04/10/14 DD SW 8270ug/Kg200ND1,2-Diphenylhydrazine 500 04/10/14 DD SW 8270ug/Kg230ND1,3-Dichlorobenzene 500 04/10/14 DD SW 8270ug/Kg210ND1,4-Dichlorobenzene 500 04/10/14 DD SW 8270ug/Kg210ND2,4,5-Trichlorophenol 500 04/10/14 DD SW 8270ug/Kg390ND2,4,6-Trichlorophenol 500 04/10/14 DD SW 8270ug/Kg230ND2,4-Dichlorophenol 500 04/10/14 DD SW 8270ug/Kg250ND2,4-Dimethylphenol 500 04/10/14 DD SW 8270ug/Kg180ND2,4-Dinitrophenol 3600 04/10/14 DD SW 8270ug/Kg500ND2,4-Dinitrotoluene 500 04/10/14 DD SW 8270ug/Kg280ND2,6-Dinitrotoluene 500 04/10/14 DD SW 8270ug/Kg230ND2-Chloronaphthalene 500 04/10/14 DD SW 8270ug/Kg200ND2-Chlorophenol 500 04/10/14 DD SW 8270ug/Kg200ND2-Methylnaphthalene 500 04/10/14 DD SW 8270ug/Kg210ND2-Methylphenol (o-cresol) 330 04/10/14 DD SW 8270ug/Kg330ND2-Nitroaniline 3600 04/10/14 DD SW 8270ug/Kg730ND2-Nitrophenol 500 04/10/14 DD SW 8270ug/Kg460ND3&4-Methylphenol (m&p-cresol) 500 04/10/14 DD SW 8270ug/Kg 1280ND3,3'-Dichlorobenzidine 1400 04/10/14 DD SW 8270ug/Kg340ND3-Nitroaniline 3600 04/10/14 DD SW 8270ug/Kg1600ND4,6-Dinitro-2-methylphenol 3600 04/10/14 DD SW 8270ug/Kg780ND4-Bromophenyl phenyl ether 500 04/10/14 DD SW 8270ug/Kg210ND4-Chloro-3-methylphenol 500 04/10/14 DD SW 8270ug/Kg250ND4-Chloroaniline 1400 04/10/14 DD SW 8270ug/Kg340ND4-Chlorophenyl phenyl ether 500 04/10/14 DD SW 8270ug/Kg240
Page 31 of 49 Ver 1
E-SB7 0-2Phoenix I.D.: BG30368
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Nitroaniline 3600 04/10/14 DD SW 8270ug/Kg240ND4-Nitrophenol 3600 04/10/14 DD SW 8270ug/Kg330NDAcenaphthene 500 04/10/14 DD SW 8270ug/Kg220NDAcenaphthylene 500 04/10/14 DD SW 8270ug/Kg200NDAcetophenone 500 04/10/14 DD SW 8270ug/Kg220NDAniline 3600 04/10/14 DD SW 8270ug/Kg1500NDAnthracene 500 04/10/14 DD SW 8270ug/Kg240950Benz(a)anthracene 500 04/10/14 DD SW 8270ug/Kg240NDBenzidine 1400 04/10/14 DD SW 8270ug/Kg420790Benzo(a)pyrene 500 04/10/14 DD SW 8270ug/Kg230
1000Benzo(b)fluoranthene 500 04/10/14 DD SW 8270ug/Kg250510Benzo(ghi)perylene 500 04/10/14 DD SW 8270ug/Kg230440Benzo(k)fluoranthene 500 04/10/14 DD SW 8270ug/Kg240JNDBenzoic acid 3600 04/10/14 DD SW 8270ug/Kg 11400NDBenzyl butyl phthalate 500 04/10/14 DD SW 8270ug/Kg190NDBis(2-chloroethoxy)methane 500 04/10/14 DD SW 8270ug/Kg200NDBis(2-chloroethyl)ether 500 04/10/14 DD SW 8270ug/Kg190NDBis(2-chloroisopropyl)ether 500 04/10/14 DD SW 8270ug/Kg 1200NDBis(2-ethylhexyl)phthalate 500 04/10/14 DD SW 8270ug/Kg210NDCarbazole 3600 04/10/14 DD SW 8270ug/Kg550920Chrysene 500 04/10/14 DD SW 8270ug/Kg240NDDibenz(a,h)anthracene 330 04/10/14 DD SW 8270ug/Kg230NDDibenzofuran 500 04/10/14 DD SW 8270ug/Kg210NDDiethyl phthalate 500 04/10/14 DD SW 8270ug/Kg230NDDimethylphthalate 500 04/10/14 DD SW 8270ug/Kg220NDDi-n-butylphthalate 500 04/10/14 DD SW 8270ug/Kg190NDDi-n-octylphthalate 500 04/10/14 DD SW 8270ug/Kg190
1900Fluoranthene 500 04/10/14 DD SW 8270ug/Kg230NDFluorene 500 04/10/14 DD SW 8270ug/Kg240NDHexachlorobenzene 500 04/10/14 DD SW 8270ug/Kg210NDHexachlorobutadiene 500 04/10/14 DD SW 8270ug/Kg260NDHexachlorocyclopentadiene 500 04/10/14 DD SW 8270ug/Kg220NDHexachloroethane 500 04/10/14 DD SW 8270ug/Kg220460Indeno(1,2,3-cd)pyrene 500 04/10/14 DD SW 8270ug/Kg240JNDIsophorone 500 04/10/14 DD SW 8270ug/Kg200NDNaphthalene 500 04/10/14 DD SW 8270ug/Kg210NDNitrobenzene 500 04/10/14 DD SW 8270ug/Kg250NDN-Nitrosodimethylamine 500 04/10/14 DD SW 8270ug/Kg200NDN-Nitrosodi-n-propylamine 500 04/10/14 DD SW 8270ug/Kg230NDN-Nitrosodiphenylamine 500 04/10/14 DD SW 8270ug/Kg280NDPentachloronitrobenzene 500 04/10/14 DD SW 8270ug/Kg270NDPentachlorophenol 500 04/10/14 DD SW 8270ug/Kg270830Phenanthrene 500 04/10/14 DD SW 8270ug/Kg210NDPhenol 330 04/10/14 DD SW 8270ug/Kg230
1600Pyrene 500 04/10/14 DD SW 8270ug/Kg250NDPyridine 500 04/10/14 DD SW 8270ug/Kg180
QA/QC Surrogates73% 2,4,6-Tribromophenol 04/10/14 DD 30 - 130 %%54% 2-Fluorobiphenyl 04/10/14 DD 30 - 130 %%
Page 32 of 49 Ver 1
E-SB7 0-2Phoenix I.D.: BG30368
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
72% 2-Fluorophenol 04/10/14 DD 30 - 130 %%51% Nitrobenzene-d5 04/10/14 DD 30 - 130 %%79% Phenol-d5 04/10/14 DD 30 - 130 %%61% Terphenyl-d14 04/10/14 DD 30 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Semi-Volatile Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, a dilution was required resulting in an elevated RL for the semivolatile analysis.
Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 33 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
E-SB7 15-17
Phoenix ID: BG30369
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.38Silver 0.38 04/11/14 LK SW6010mg/Kg0.238370Aluminum 38 04/11/14 LK SW6010mg/Kg7.71.1Arsenic 0.8 04/11/14 LK SW6010mg/Kg0.77
61.5Barium 0.8 04/11/14 LK SW6010mg/Kg0.150.54Beryllium 0.31 04/11/14 LK SW6010mg/Kg0.152050Calcium 3.8 04/11/14 LK SW6010mg/Kg3.5
< 0.38Cadmium 0.38 04/11/14 LK SW6010mg/Kg0.157.71Cobalt 0.38 04/11/14 LK SW6010mg/Kg0.1518.1Chromium 0.38 04/11/14 LK SW6010mg/Kg0.1518.5Copper 0.38 04/11/14 LK SW6010mg/kg0.31
23900Iron 38 04/11/14 LK SW6010mg/Kg B38< 0.09Mercury 0.09 04/10/14 RS SW-7471mg/Kg0.062490Potassium 8 04/11/14 LK SW6010mg/Kg3.03410Magnesium 38 04/11/14 LK SW6010mg/Kg2.3480Manganese 3.8 04/11/14 LK SW6010mg/Kg1.5180Sodium 8 04/11/14 LK SW6010mg/Kg3.318.1Nickel 0.38 04/11/14 LK SW6010mg/Kg0.156.4Lead 0.8 04/11/14 LK SW6010mg/Kg0.23
< 1.9Antimony 1.9 04/11/14 LK SW6010mg/Kg0.77< 1.5Selenium 1.5 04/11/14 LK SW6010mg/Kg1.3< 1.5Thallium 1.5 04/11/14 LK SW6010mg/Kg1.529.4Vanadium 0.4 04/11/14 LK SW6010mg/Kg0.1532.2Zinc 0.8 04/11/14 LK SW6010mg/Kg0.3888Percent Solid 04/09/14 I E160.3%
CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471CompletedTotal Metals Digest 04/09/14 CB/AG/W SW846 - 3050
CompletedField Extraction 04/08/14 SW5035
Page 34 of 49 Ver 1
E-SB7 15-17Phoenix I.D.: BG30369
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 12 04/11/14 U SW8260ug/Kg2.0ND1,1,1-Trichloroethane 12 04/11/14 U SW8260ug/Kg2.4ND1,1,2,2-Tetrachloroethane 12 04/11/14 U SW8260ug/Kg1.7ND1,1,2-Trichloroethane 12 04/11/14 U SW8260ug/Kg1.2ND1,1-Dichloroethane 12 04/11/14 U SW8260ug/Kg2.4ND1,1-Dichloroethene 12 04/11/14 U SW8260ug/Kg2.7ND1,1-Dichloropropene 12 04/11/14 U SW8260ug/Kg2.4ND1,2,3-Trichlorobenzene 12 04/11/14 U SW8260ug/Kg2.4ND1,2,3-Trichloropropane 12 04/11/14 U SW8260ug/Kg1.7ND1,2,4-Trichlorobenzene 12 04/11/14 U SW8260ug/Kg2.4ND1,2,4-Trimethylbenzene 12 04/11/14 U SW8260ug/Kg1.8ND1,2-Dibromo-3-chloropropane 12 04/11/14 U SW8260ug/Kg3.3ND1,2-Dibromoethane 12 04/11/14 U SW8260ug/Kg3.2ND1,2-Dichlorobenzene 12 04/11/14 U SW8260ug/Kg1.3ND1,2-Dichloroethane 12 04/11/14 U SW8260ug/Kg1.1ND1,2-Dichloropropane 12 04/11/14 U SW8260ug/Kg1.7ND1,3,5-Trimethylbenzene 12 04/11/14 U SW8260ug/Kg1.6ND1,3-Dichlorobenzene 12 04/11/14 U SW8260ug/Kg1.8ND1,3-Dichloropropane 12 04/11/14 U SW8260ug/Kg1.3ND1,4-Dichlorobenzene 12 04/11/14 U SW8260ug/Kg1.9ND2,2-Dichloropropane 12 04/11/14 U SW8260ug/Kg2.0ND2-Chlorotoluene 12 04/11/14 U SW8260ug/Kg1.9ND2-Hexanone 61 04/11/14 U SW8260ug/Kg5.5ND2-Isopropyltoluene 12 04/11/14 U SW8260ug/Kg 11.7ND4-Chlorotoluene 12 04/11/14 U SW8260ug/Kg1.4ND4-Methyl-2-pentanone 61 04/11/14 U SW8260ug/Kg2.9NDAcetone 50 04/11/14 U SW8260ug/Kg12NDAcrylonitrile 24 04/11/14 U SW8260ug/Kg6.8NDBenzene 12 04/11/14 U SW8260ug/Kg2.4NDBromobenzene 12 04/11/14 U SW8260ug/Kg1.6NDBromochloromethane 12 04/11/14 U SW8260ug/Kg1.8NDBromodichloromethane 12 04/11/14 U SW8260ug/Kg1.5NDBromoform 12 04/11/14 U SW8260ug/Kg1.7NDBromomethane 12 04/11/14 U SW8260ug/Kg9.4NDCarbon Disulfide 12 04/11/14 U SW8260ug/Kg2.0NDCarbon tetrachloride 12 04/11/14 U SW8260ug/Kg1.4NDChlorobenzene 12 04/11/14 U SW8260ug/Kg1.8NDChloroethane 12 04/11/14 U SW8260ug/Kg2.8NDChloroform 12 04/11/14 U SW8260ug/Kg2.2NDChloromethane 12 04/11/14 U SW8260ug/Kg6.4NDcis-1,2-Dichloroethene 12 04/11/14 U SW8260ug/Kg2.7NDcis-1,3-Dichloropropene 12 04/11/14 U SW8260ug/Kg1.3NDDibromochloromethane 12 04/11/14 U SW8260ug/Kg1.4NDDibromomethane 12 04/11/14 U SW8260ug/Kg1.5NDDichlorodifluoromethane 12 04/11/14 U SW8260ug/Kg3.2NDEthylbenzene 12 04/11/14 U SW8260ug/Kg2.2NDHexachlorobutadiene 12 04/11/14 U SW8260ug/Kg2.6NDIsopropylbenzene 12 04/11/14 U SW8260ug/Kg2.3
Page 35 of 49 Ver 1
E-SB7 15-17Phoenix I.D.: BG30369
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 12 04/11/14 U SW8260ug/Kg4.8NDMethyl Ethyl Ketone 73 04/11/14 U SW8260ug/Kg11NDMethyl t-butyl ether (MTBE) 24 04/11/14 U SW8260ug/Kg3.4NDMethylene chloride 12 04/11/14 U SW8260ug/Kg2.0NDNaphthalene 12 04/11/14 U SW8260ug/Kg3.3NDn-Butylbenzene 12 04/11/14 U SW8260ug/Kg2.2NDn-Propylbenzene 12 04/11/14 U SW8260ug/Kg2.2NDo-Xylene 12 04/11/14 U SW8260ug/Kg4.6NDp-Isopropyltoluene 12 04/11/14 U SW8260ug/Kg1.8NDsec-Butylbenzene 12 04/11/14 U SW8260ug/Kg2.3NDStyrene 12 04/11/14 U SW8260ug/Kg3.5NDtert-Butylbenzene 12 04/11/14 U SW8260ug/Kg1.9NDTetrachloroethene 12 04/11/14 U SW8260ug/Kg2.6NDTetrahydrofuran (THF) 24 04/11/14 U SW8260ug/Kg 111NDToluene 12 04/11/14 U SW8260ug/Kg1.9NDtrans-1,2-Dichloroethene 12 04/11/14 U SW8260ug/Kg2.4NDtrans-1,3-Dichloropropene 12 04/11/14 U SW8260ug/Kg2.5NDtrans-1,4-dichloro-2-butene 24 04/11/14 U SW8260ug/Kg23NDTrichloroethene 12 04/11/14 U SW8260ug/Kg2.6NDTrichlorofluoromethane 12 04/11/14 U SW8260ug/Kg2.7NDTrichlorotrifluoroethane 12 04/11/14 U SW8260ug/Kg1.9NDVinyl chloride 12 04/11/14 U SW8260ug/Kg3.9
QA/QC Surrogates103% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%98% Bromofluorobenzene 04/11/14 U 70 - 130 %%103% Dibromofluoromethane 04/11/14 U 70 - 130 %%101% Toluene-d8 04/11/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 260 04/10/14 DD SW 8270ug/Kg130ND1,2,4-Trichlorobenzene 260 04/10/14 DD SW 8270ug/Kg110ND1,2-Dichlorobenzene 260 04/10/14 DD SW 8270ug/Kg110ND1,2-Diphenylhydrazine 260 04/10/14 DD SW 8270ug/Kg120ND1,3-Dichlorobenzene 260 04/10/14 DD SW 8270ug/Kg110ND1,4-Dichlorobenzene 260 04/10/14 DD SW 8270ug/Kg110ND2,4,5-Trichlorophenol 260 04/10/14 DD SW 8270ug/Kg210ND2,4,6-Trichlorophenol 260 04/10/14 DD SW 8270ug/Kg120ND2,4-Dichlorophenol 260 04/10/14 DD SW 8270ug/Kg130ND2,4-Dimethylphenol 260 04/10/14 DD SW 8270ug/Kg93ND2,4-Dinitrophenol 1900 04/10/14 DD SW 8270ug/Kg260ND2,4-Dinitrotoluene 260 04/10/14 DD SW 8270ug/Kg150ND2,6-Dinitrotoluene 260 04/10/14 DD SW 8270ug/Kg120ND2-Chloronaphthalene 260 04/10/14 DD SW 8270ug/Kg110ND2-Chlorophenol 260 04/10/14 DD SW 8270ug/Kg110ND2-Methylnaphthalene 260 04/10/14 DD SW 8270ug/Kg110ND2-Methylphenol (o-cresol) 260 04/10/14 DD SW 8270ug/Kg180ND2-Nitroaniline 1900 04/10/14 DD SW 8270ug/Kg380ND2-Nitrophenol 260 04/10/14 DD SW 8270ug/Kg240ND3&4-Methylphenol (m&p-cresol) 260 04/10/14 DD SW 8270ug/Kg 1150ND3,3'-Dichlorobenzidine 750 04/10/14 DD SW 8270ug/Kg180
Page 36 of 49 Ver 1
E-SB7 15-17Phoenix I.D.: BG30369
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND3-Nitroaniline 1900 04/10/14 DD SW 8270ug/Kg820ND4,6-Dinitro-2-methylphenol 1900 04/10/14 DD SW 8270ug/Kg400ND4-Bromophenyl phenyl ether 260 04/10/14 DD SW 8270ug/Kg110ND4-Chloro-3-methylphenol 260 04/10/14 DD SW 8270ug/Kg130ND4-Chloroaniline 750 04/10/14 DD SW 8270ug/Kg180ND4-Chlorophenyl phenyl ether 260 04/10/14 DD SW 8270ug/Kg130ND4-Nitroaniline 1900 04/10/14 DD SW 8270ug/Kg130ND4-Nitrophenol 1900 04/10/14 DD SW 8270ug/Kg170NDAcenaphthene 260 04/10/14 DD SW 8270ug/Kg110NDAcenaphthylene 260 04/10/14 DD SW 8270ug/Kg110NDAcetophenone 260 04/10/14 DD SW 8270ug/Kg120NDAniline 1900 04/10/14 DD SW 8270ug/Kg760NDAnthracene 260 04/10/14 DD SW 8270ug/Kg120NDBenz(a)anthracene 260 04/10/14 DD SW 8270ug/Kg130NDBenzidine 750 04/10/14 DD SW 8270ug/Kg220NDBenzo(a)pyrene 260 04/10/14 DD SW 8270ug/Kg120NDBenzo(b)fluoranthene 260 04/10/14 DD SW 8270ug/Kg130NDBenzo(ghi)perylene 260 04/10/14 DD SW 8270ug/Kg120NDBenzo(k)fluoranthene 260 04/10/14 DD SW 8270ug/Kg120NDBenzoic acid 1900 04/10/14 DD SW 8270ug/Kg 1750NDBenzyl butyl phthalate 260 04/10/14 DD SW 8270ug/Kg97NDBis(2-chloroethoxy)methane 260 04/10/14 DD SW 8270ug/Kg100NDBis(2-chloroethyl)ether 260 04/10/14 DD SW 8270ug/Kg100NDBis(2-chloroisopropyl)ether 260 04/10/14 DD SW 8270ug/Kg 1100NDBis(2-ethylhexyl)phthalate 260 04/10/14 DD SW 8270ug/Kg110NDCarbazole 1900 04/10/14 DD SW 8270ug/Kg290NDChrysene 260 04/10/14 DD SW 8270ug/Kg130NDDibenz(a,h)anthracene 260 04/10/14 DD SW 8270ug/Kg120NDDibenzofuran 260 04/10/14 DD SW 8270ug/Kg110NDDiethyl phthalate 260 04/10/14 DD SW 8270ug/Kg120NDDimethylphthalate 260 04/10/14 DD SW 8270ug/Kg120NDDi-n-butylphthalate 260 04/10/14 DD SW 8270ug/Kg100NDDi-n-octylphthalate 260 04/10/14 DD SW 8270ug/Kg97NDFluoranthene 260 04/10/14 DD SW 8270ug/Kg120NDFluorene 260 04/10/14 DD SW 8270ug/Kg120NDHexachlorobenzene 260 04/10/14 DD SW 8270ug/Kg110NDHexachlorobutadiene 260 04/10/14 DD SW 8270ug/Kg140NDHexachlorocyclopentadiene 260 04/10/14 DD SW 8270ug/Kg120NDHexachloroethane 260 04/10/14 DD SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 260 04/10/14 DD SW 8270ug/Kg120NDIsophorone 260 04/10/14 DD SW 8270ug/Kg110NDNaphthalene 260 04/10/14 DD SW 8270ug/Kg110NDNitrobenzene 260 04/10/14 DD SW 8270ug/Kg130NDN-Nitrosodimethylamine 260 04/10/14 DD SW 8270ug/Kg110NDN-Nitrosodi-n-propylamine 260 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodiphenylamine 260 04/10/14 DD SW 8270ug/Kg140NDPentachloronitrobenzene 260 04/10/14 DD SW 8270ug/Kg140NDPentachlorophenol 260 04/10/14 DD SW 8270ug/Kg140NDPhenanthrene 260 04/10/14 DD SW 8270ug/Kg110
Page 37 of 49 Ver 1
E-SB7 15-17Phoenix I.D.: BG30369
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDPhenol 260 04/10/14 DD SW 8270ug/Kg120NDPyrene 260 04/10/14 DD SW 8270ug/Kg130NDPyridine 260 04/10/14 DD SW 8270ug/Kg93
QA/QC Surrogates94% 2,4,6-Tribromophenol 04/10/14 DD 30 - 130 %%57% 2-Fluorobiphenyl 04/10/14 DD 30 - 130 %%81% 2-Fluorophenol 04/10/14 DD 30 - 130 %%53% Nitrobenzene-d5 04/10/14 DD 30 - 130 %%83% Phenol-d5 04/10/14 DD 30 - 130 %%61% Terphenyl-d14 04/10/14 DD 30 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 38 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
SOIL DUPLICATE 2
Phoenix ID: BG30370
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
< 0.33Silver 0.33 04/11/14 LK SW6010mg/Kg0.203800Aluminum 33 04/10/14 LK SW6010mg/Kg6.7< 0.7Arsenic 0.7 04/11/14 LK SW6010mg/Kg0.6721.4Barium 0.7 04/11/14 LK SW6010mg/Kg0.13
< 0.27Beryllium 0.27 04/11/14 LK SW6010mg/Kg0.133010Calcium 3.3 04/11/14 LK SW6010mg/Kg3.1
< 0.33Cadmium 0.33 04/11/14 LK SW6010mg/Kg0.132.92Cobalt 0.33 04/11/14 LK SW6010mg/Kg0.137.78Chromium 0.33 04/11/14 LK SW6010mg/Kg0.139.10Copper 0.33 04/11/14 LK SW6010mg/kg0.279380Iron 33 04/10/14 LK SW6010mg/Kg B33
< 0.07Mercury 0.07 04/10/14 RS SW-7471mg/Kg0.04731Potassium 7 04/11/14 LK SW6010mg/Kg2.6
2270Magnesium 3.3 04/11/14 LK SW6010mg/Kg0.20201Manganese 3.3 04/10/14 LK SW6010mg/Kg1.3142Sodium 7 04/11/14 LK SW6010mg/Kg2.97.62Nickel 0.33 04/11/14 LK SW6010mg/Kg0.132.2Lead 0.7 04/11/14 LK SW6010mg/Kg0.20
< 1.7Antimony 1.7 04/11/14 LK SW6010mg/Kg0.67< 1.3Selenium 1.3 04/11/14 LK SW6010mg/Kg1.1< 1.3Thallium 1.3 04/11/14 LK SW6010mg/Kg1.312.5Vanadium 0.3 04/11/14 LK SW6010mg/Kg0.1314.7Zinc 0.7 04/11/14 LK SW6010mg/Kg0.3395Percent Solid 04/09/14 I E160.3%
CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471CompletedTotal Metals Digest 04/09/14 CB/AG SW846 - 3050
CompletedField Extraction 04/08/14 SW5035
Page 39 of 49 Ver 1
SOIL DUPLICATE 2Phoenix I.D.: BG30370
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 7.7 04/11/14 U SW8260ug/Kg1.3ND1,1,1-Trichloroethane 7.7 04/11/14 U SW8260ug/Kg1.5ND1,1,2,2-Tetrachloroethane 7.7 04/11/14 U SW8260ug/Kg1.1ND1,1,2-Trichloroethane 7.7 04/11/14 U SW8260ug/Kg0.76ND1,1-Dichloroethane 7.7 04/11/14 U SW8260ug/Kg1.5ND1,1-Dichloroethene 7.7 04/11/14 U SW8260ug/Kg1.7ND1,1-Dichloropropene 7.7 04/11/14 U SW8260ug/Kg1.5ND1,2,3-Trichlorobenzene 7.7 04/11/14 U SW8260ug/Kg1.5ND1,2,3-Trichloropropane 7.7 04/11/14 U SW8260ug/Kg1.1ND1,2,4-Trichlorobenzene 7.7 04/11/14 U SW8260ug/Kg1.5ND1,2,4-Trimethylbenzene 7.7 04/11/14 U SW8260ug/Kg1.1ND1,2-Dibromo-3-chloropropane 7.7 04/11/14 U SW8260ug/Kg2.1ND1,2-Dibromoethane 7.7 04/11/14 U SW8260ug/Kg2.1ND1,2-Dichlorobenzene 7.7 04/11/14 U SW8260ug/Kg0.85ND1,2-Dichloroethane 7.7 04/11/14 U SW8260ug/Kg0.68ND1,2-Dichloropropane 7.7 04/11/14 U SW8260ug/Kg1.1ND1,3,5-Trimethylbenzene 7.7 04/11/14 U SW8260ug/Kg1.0ND1,3-Dichlorobenzene 7.7 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichloropropane 7.7 04/11/14 U SW8260ug/Kg0.82ND1,4-Dichlorobenzene 7.7 04/11/14 U SW8260ug/Kg1.2ND2,2-Dichloropropane 7.7 04/11/14 U SW8260ug/Kg1.3ND2-Chlorotoluene 7.7 04/11/14 U SW8260ug/Kg1.2ND2-Hexanone 39 04/11/14 U SW8260ug/Kg3.5ND2-Isopropyltoluene 7.7 04/11/14 U SW8260ug/Kg 11.1ND4-Chlorotoluene 7.7 04/11/14 U SW8260ug/Kg0.90ND4-Methyl-2-pentanone 39 04/11/14 U SW8260ug/Kg1.8NDAcetone 50 04/11/14 U SW8260ug/Kg7.7NDAcrylonitrile 15 04/11/14 U SW8260ug/Kg4.3NDBenzene 7.7 04/11/14 U SW8260ug/Kg1.5NDBromobenzene 7.7 04/11/14 U SW8260ug/Kg1.0NDBromochloromethane 7.7 04/11/14 U SW8260ug/Kg1.1NDBromodichloromethane 7.7 04/11/14 U SW8260ug/Kg0.96NDBromoform 7.7 04/11/14 U SW8260ug/Kg1.1NDBromomethane 7.7 04/11/14 U SW8260ug/Kg6.0NDCarbon Disulfide 7.7 04/11/14 U SW8260ug/Kg1.3NDCarbon tetrachloride 7.7 04/11/14 U SW8260ug/Kg0.90NDChlorobenzene 7.7 04/11/14 U SW8260ug/Kg1.1NDChloroethane 7.7 04/11/14 U SW8260ug/Kg1.8NDChloroform 7.7 04/11/14 U SW8260ug/Kg1.4NDChloromethane 7.7 04/11/14 U SW8260ug/Kg4.1NDcis-1,2-Dichloroethene 7.7 04/11/14 U SW8260ug/Kg1.7NDcis-1,3-Dichloropropene 7.7 04/11/14 U SW8260ug/Kg0.84NDDibromochloromethane 7.7 04/11/14 U SW8260ug/Kg0.87NDDibromomethane 7.7 04/11/14 U SW8260ug/Kg0.97NDDichlorodifluoromethane 7.7 04/11/14 U SW8260ug/Kg2.1NDEthylbenzene 7.7 04/11/14 U SW8260ug/Kg1.4NDHexachlorobutadiene 7.7 04/11/14 U SW8260ug/Kg1.6NDIsopropylbenzene 7.7 04/11/14 U SW8260ug/Kg1.5
Page 40 of 49 Ver 1
SOIL DUPLICATE 2Phoenix I.D.: BG30370
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 7.7 04/11/14 U SW8260ug/Kg3.0NDMethyl Ethyl Ketone 46 04/11/14 U SW8260ug/Kg6.7NDMethyl t-butyl ether (MTBE) 15 04/11/14 U SW8260ug/Kg2.1NDMethylene chloride 7.7 04/11/14 U SW8260ug/Kg1.3NDNaphthalene 7.7 04/11/14 U SW8260ug/Kg2.1NDn-Butylbenzene 7.7 04/11/14 U SW8260ug/Kg1.4NDn-Propylbenzene 7.7 04/11/14 U SW8260ug/Kg1.4NDo-Xylene 7.7 04/11/14 U SW8260ug/Kg3.0NDp-Isopropyltoluene 7.7 04/11/14 U SW8260ug/Kg1.1NDsec-Butylbenzene 7.7 04/11/14 U SW8260ug/Kg1.5NDStyrene 7.7 04/11/14 U SW8260ug/Kg2.2NDtert-Butylbenzene 7.7 04/11/14 U SW8260ug/Kg1.2NDTetrachloroethene 7.7 04/11/14 U SW8260ug/Kg1.6NDTetrahydrofuran (THF) 15 04/11/14 U SW8260ug/Kg 17.0NDToluene 7.7 04/11/14 U SW8260ug/Kg1.2NDtrans-1,2-Dichloroethene 7.7 04/11/14 U SW8260ug/Kg1.5NDtrans-1,3-Dichloropropene 7.7 04/11/14 U SW8260ug/Kg1.6NDtrans-1,4-dichloro-2-butene 15 04/11/14 U SW8260ug/Kg14NDTrichloroethene 7.7 04/11/14 U SW8260ug/Kg1.6NDTrichlorofluoromethane 7.7 04/11/14 U SW8260ug/Kg1.7NDTrichlorotrifluoroethane 7.7 04/11/14 U SW8260ug/Kg1.2NDVinyl chloride 7.7 04/11/14 U SW8260ug/Kg2.5
QA/QC Surrogates106% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%96% Bromofluorobenzene 04/11/14 U 70 - 130 %%107% Dibromofluoromethane 04/11/14 U 70 - 130 %%102% Toluene-d8 04/11/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 240 04/10/14 DD SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 240 04/10/14 DD SW 8270ug/Kg100ND1,2-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg98ND1,2-Diphenylhydrazine 240 04/10/14 DD SW 8270ug/Kg110ND1,3-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg100ND1,4-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg100ND2,4,5-Trichlorophenol 240 04/10/14 DD SW 8270ug/Kg190ND2,4,6-Trichlorophenol 240 04/10/14 DD SW 8270ug/Kg110ND2,4-Dichlorophenol 240 04/10/14 DD SW 8270ug/Kg120ND2,4-Dimethylphenol 240 04/10/14 DD SW 8270ug/Kg86ND2,4-Dinitrophenol 1700 04/10/14 DD SW 8270ug/Kg240ND2,4-Dinitrotoluene 240 04/10/14 DD SW 8270ug/Kg140ND2,6-Dinitrotoluene 240 04/10/14 DD SW 8270ug/Kg110ND2-Chloronaphthalene 240 04/10/14 DD SW 8270ug/Kg99ND2-Chlorophenol 240 04/10/14 DD SW 8270ug/Kg99ND2-Methylnaphthalene 240 04/10/14 DD SW 8270ug/Kg100ND2-Methylphenol (o-cresol) 240 04/10/14 DD SW 8270ug/Kg160ND2-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg350ND2-Nitrophenol 240 04/10/14 DD SW 8270ug/Kg220ND3&4-Methylphenol (m&p-cresol) 240 04/10/14 DD SW 8270ug/Kg 1140ND3,3'-Dichlorobenzidine 690 04/10/14 DD SW 8270ug/Kg160
Page 41 of 49 Ver 1
SOIL DUPLICATE 2Phoenix I.D.: BG30370
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND3-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg760ND4,6-Dinitro-2-methylphenol 1700 04/10/14 DD SW 8270ug/Kg370ND4-Bromophenyl phenyl ether 240 04/10/14 DD SW 8270ug/Kg100ND4-Chloro-3-methylphenol 240 04/10/14 DD SW 8270ug/Kg120ND4-Chloroaniline 690 04/10/14 DD SW 8270ug/Kg160ND4-Chlorophenyl phenyl ether 240 04/10/14 DD SW 8270ug/Kg120ND4-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg120ND4-Nitrophenol 1700 04/10/14 DD SW 8270ug/Kg160NDAcenaphthene 240 04/10/14 DD SW 8270ug/Kg110NDAcenaphthylene 240 04/10/14 DD SW 8270ug/Kg97NDAcetophenone 240 04/10/14 DD SW 8270ug/Kg110NDAniline 1700 04/10/14 DD SW 8270ug/Kg700NDAnthracene 240 04/10/14 DD SW 8270ug/Kg110NDBenz(a)anthracene 240 04/10/14 DD SW 8270ug/Kg120NDBenzidine 690 04/10/14 DD SW 8270ug/Kg200NDBenzo(a)pyrene 240 04/10/14 DD SW 8270ug/Kg110NDBenzo(b)fluoranthene 240 04/10/14 DD SW 8270ug/Kg120NDBenzo(ghi)perylene 240 04/10/14 DD SW 8270ug/Kg110NDBenzo(k)fluoranthene 240 04/10/14 DD SW 8270ug/Kg120NDBenzoic acid 1700 04/10/14 DD SW 8270ug/Kg 1690NDBenzyl butyl phthalate 240 04/10/14 DD SW 8270ug/Kg90NDBis(2-chloroethoxy)methane 240 04/10/14 DD SW 8270ug/Kg96NDBis(2-chloroethyl)ether 240 04/10/14 DD SW 8270ug/Kg94NDBis(2-chloroisopropyl)ether 240 04/10/14 DD SW 8270ug/Kg 197NDBis(2-ethylhexyl)phthalate 240 04/10/14 DD SW 8270ug/Kg100NDCarbazole 1700 04/10/14 DD SW 8270ug/Kg260NDChrysene 240 04/10/14 DD SW 8270ug/Kg120NDDibenz(a,h)anthracene 240 04/10/14 DD SW 8270ug/Kg110NDDibenzofuran 240 04/10/14 DD SW 8270ug/Kg100NDDiethyl phthalate 240 04/10/14 DD SW 8270ug/Kg110NDDimethylphthalate 240 04/10/14 DD SW 8270ug/Kg110NDDi-n-butylphthalate 240 04/10/14 DD SW 8270ug/Kg92NDDi-n-octylphthalate 240 04/10/14 DD SW 8270ug/Kg90NDFluoranthene 240 04/10/14 DD SW 8270ug/Kg110NDFluorene 240 04/10/14 DD SW 8270ug/Kg110NDHexachlorobenzene 240 04/10/14 DD SW 8270ug/Kg100NDHexachlorobutadiene 240 04/10/14 DD SW 8270ug/Kg130NDHexachlorocyclopentadiene 240 04/10/14 DD SW 8270ug/Kg110NDHexachloroethane 240 04/10/14 DD SW 8270ug/Kg100NDIndeno(1,2,3-cd)pyrene 240 04/10/14 DD SW 8270ug/Kg120NDIsophorone 240 04/10/14 DD SW 8270ug/Kg97NDNaphthalene 240 04/10/14 DD SW 8270ug/Kg100NDNitrobenzene 240 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodimethylamine 240 04/10/14 DD SW 8270ug/Kg98NDN-Nitrosodi-n-propylamine 240 04/10/14 DD SW 8270ug/Kg110NDN-Nitrosodiphenylamine 240 04/10/14 DD SW 8270ug/Kg130NDPentachloronitrobenzene 240 04/10/14 DD SW 8270ug/Kg130NDPentachlorophenol 240 04/10/14 DD SW 8270ug/Kg130NDPhenanthrene 240 04/10/14 DD SW 8270ug/Kg99
Page 42 of 49 Ver 1
SOIL DUPLICATE 2Phoenix I.D.: BG30370
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDPhenol 240 04/10/14 DD SW 8270ug/Kg110NDPyrene 240 04/10/14 DD SW 8270ug/Kg120NDPyridine 240 04/10/14 DD SW 8270ug/Kg85
QA/QC Surrogates90% 2,4,6-Tribromophenol 04/10/14 DD 30 - 130 %%57% 2-Fluorobiphenyl 04/10/14 DD 30 - 130 %%81% 2-Fluorophenol 04/10/14 DD 30 - 130 %%55% Nitrobenzene-d5 04/10/14 DD 30 - 130 %%84% Phenol-d5 04/10/14 DD 30 - 130 %%65% Terphenyl-d14 04/10/14 DD 30 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 43 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
TRIP BLANK HIGH
Phoenix ID: BG30371
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
100Percent Solid 1 04/08/14 E160.3%
VolatilesND1,1,1,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg41ND1,1,1-Trichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1,2,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg36ND1,1,2-Trichloroethane 250 04/10/14 U SW8260ug/Kg25ND1,1-Dichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1-Dichloroethene 250 04/10/14 U SW8260ug/Kg55ND1,1-Dichloropropene 250 04/10/14 U SW8260ug/Kg49ND1,2,3-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,3-Trichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,2,4-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,4-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg36ND1,2-Dibromo-3-chloropropane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dibromoethane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg28ND1,2-Dichloroethane 250 04/10/14 U SW8260ug/Kg22ND1,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,3,5-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg33ND1,3-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg37ND1,3-Dichloropropane 250 04/10/14 U SW8260ug/Kg27ND1,4-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg40ND2,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg42ND2-Chlorotoluene 250 04/10/14 U SW8260ug/Kg40ND2-Hexanone 1300 04/10/14 U SW8260ug/Kg110ND2-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg 135ND4-Chlorotoluene 250 04/10/14 U SW8260ug/Kg29
Page 44 of 49 Ver 1
TRIP BLANK HIGHPhoenix I.D.: BG30371
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Methyl-2-pentanone 1300 04/10/14 U SW8260ug/Kg60NDAcetone 2500 04/10/14 U SW8260ug/Kg250NDAcrylonitrile 500 04/10/14 U SW8260ug/Kg140NDBenzene 250 04/10/14 U SW8260ug/Kg50NDBromobenzene 250 04/10/14 U SW8260ug/Kg33NDBromochloromethane 250 04/10/14 U SW8260ug/Kg37NDBromodichloromethane 250 04/10/14 U SW8260ug/Kg31NDBromoform 250 04/10/14 U SW8260ug/Kg35NDBromomethane 250 04/10/14 U SW8260ug/Kg190NDCarbon Disulfide 250 04/10/14 U SW8260ug/Kg41NDCarbon tetrachloride 250 04/10/14 U SW8260ug/Kg29NDChlorobenzene 250 04/10/14 U SW8260ug/Kg37NDChloroethane 250 04/10/14 U SW8260ug/Kg59NDChloroform 250 04/10/14 U SW8260ug/Kg46NDChloromethane 250 04/10/14 U SW8260ug/Kg130NDcis-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg55NDcis-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg27NDDibromochloromethane 250 04/10/14 U SW8260ug/Kg28NDDibromomethane 250 04/10/14 U SW8260ug/Kg32NDDichlorodifluoromethane 250 04/10/14 U SW8260ug/Kg67NDEthylbenzene 250 04/10/14 U SW8260ug/Kg46NDHexachlorobutadiene 250 04/10/14 U SW8260ug/Kg53NDIsopropylbenzene 250 04/10/14 U SW8260ug/Kg48NDm&p-Xylene 250 04/10/14 U SW8260ug/Kg99NDMethyl Ethyl Ketone 1500 04/10/14 U SW8260ug/Kg220NDMethyl t-butyl ether (MTBE) 500 04/10/14 U SW8260ug/Kg69NDMethylene chloride 250 04/10/14 U SW8260ug/Kg41NDNaphthalene 250 04/10/14 U SW8260ug/Kg67NDn-Butylbenzene 250 04/10/14 U SW8260ug/Kg46NDn-Propylbenzene 250 04/10/14 U SW8260ug/Kg45NDo-Xylene 250 04/10/14 U SW8260ug/Kg96NDp-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg36NDsec-Butylbenzene 250 04/10/14 U SW8260ug/Kg47NDStyrene 250 04/10/14 U SW8260ug/Kg72NDtert-Butylbenzene 250 04/10/14 U SW8260ug/Kg40NDTetrachloroethene 250 04/10/14 U SW8260ug/Kg53NDTetrahydrofuran (THF) 500 04/10/14 U SW8260ug/Kg 1230NDToluene 250 04/10/14 U SW8260ug/Kg40NDtrans-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg50NDtrans-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg51NDtrans-1,4-dichloro-2-butene 500 04/10/14 U SW8260ug/Kg460NDTrichloroethene 250 04/10/14 U SW8260ug/Kg53NDTrichlorofluoromethane 250 04/10/14 U SW8260ug/Kg56NDTrichlorotrifluoroethane 250 04/10/14 U SW8260ug/Kg39NDVinyl chloride 250 04/10/14 U SW8260ug/Kg81
QA/QC Surrogates105% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%95% Bromofluorobenzene 04/10/14 U 70 - 130 %%103% Dibromofluoromethane 04/10/14 U 70 - 130 %%
Page 45 of 49 Ver 1
TRIP BLANK HIGHPhoenix I.D.: BG30371
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
101% Toluene-d8 04/10/14 U 70 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 46 of 49 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/08/14SWsee "By" below
Laboratory Data
TRIP BLANK LOW
Phoenix ID: BG30372
04/09/140:00
16:26
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG30363
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
100Percent Solid 1 04/08/14 E160.3%CompletedField Extraction 04/08/14 SW5035
VolatilesND1,1,1,2-Tetrachloroethane 5.0 04/11/14 U SW8260ug/Kg0.82ND1,1,1-Trichloroethane 5.0 04/11/14 U SW8260ug/Kg1.0ND1,1,2,2-Tetrachloroethane 5.0 04/11/14 U SW8260ug/Kg0.71ND1,1,2-Trichloroethane 5.0 04/11/14 U SW8260ug/Kg0.49ND1,1-Dichloroethane 5.0 04/11/14 U SW8260ug/Kg0.99ND1,1-Dichloroethene 5.0 04/11/14 U SW8260ug/Kg1.1ND1,1-Dichloropropene 5.0 04/11/14 U SW8260ug/Kg0.97ND1,2,3-Trichlorobenzene 5.0 04/11/14 U SW8260ug/Kg1.0ND1,2,3-Trichloropropane 5.0 04/11/14 U SW8260ug/Kg0.71ND1,2,4-Trichlorobenzene 5.0 04/11/14 U SW8260ug/Kg1.0ND1,2,4-Trimethylbenzene 5.0 04/11/14 U SW8260ug/Kg0.72ND1,2-Dibromo-3-chloropropane 5.0 04/11/14 U SW8260ug/Kg1.3ND1,2-Dibromoethane 5.0 04/11/14 U SW8260ug/Kg1.3ND1,2-Dichlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.55ND1,2-Dichloroethane 5.0 04/11/14 U SW8260ug/Kg0.44ND1,2-Dichloropropane 5.0 04/11/14 U SW8260ug/Kg0.71ND1,3,5-Trimethylbenzene 5.0 04/11/14 U SW8260ug/Kg0.66ND1,3-Dichlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.74ND1,3-Dichloropropane 5.0 04/11/14 U SW8260ug/Kg0.53ND1,4-Dichlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.79ND2,2-Dichloropropane 5.0 04/11/14 U SW8260ug/Kg0.84ND2-Chlorotoluene 5.0 04/11/14 U SW8260ug/Kg0.80ND2-Hexanone 25 04/11/14 U SW8260ug/Kg2.3ND2-Isopropyltoluene 5.0 04/11/14 U SW8260ug/Kg 10.69
Page 47 of 49 Ver 1
TRIP BLANK LOWPhoenix I.D.: BG30372
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Chlorotoluene 5.0 04/11/14 U SW8260ug/Kg0.58ND4-Methyl-2-pentanone 25 04/11/14 U SW8260ug/Kg1.2NDAcetone 50 04/11/14 U SW8260ug/Kg5.0NDAcrylonitrile 10 04/11/14 U SW8260ug/Kg2.8NDBenzene 5.0 04/11/14 U SW8260ug/Kg0.99NDBromobenzene 5.0 04/11/14 U SW8260ug/Kg0.65NDBromochloromethane 5.0 04/11/14 U SW8260ug/Kg0.73NDBromodichloromethane 5.0 04/11/14 U SW8260ug/Kg0.62NDBromoform 5.0 04/11/14 U SW8260ug/Kg0.70NDBromomethane 5.0 04/11/14 U SW8260ug/Kg3.9NDCarbon Disulfide 5.0 04/11/14 U SW8260ug/Kg0.81NDCarbon tetrachloride 5.0 04/11/14 U SW8260ug/Kg0.58NDChlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.74NDChloroethane 5.0 04/11/14 U SW8260ug/Kg1.2NDChloroform 5.0 04/11/14 U SW8260ug/Kg0.91NDChloromethane 5.0 04/11/14 U SW8260ug/Kg2.6NDcis-1,2-Dichloroethene 5.0 04/11/14 U SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.0 04/11/14 U SW8260ug/Kg0.54NDDibromochloromethane 5.0 04/11/14 U SW8260ug/Kg0.56NDDibromomethane 5.0 04/11/14 U SW8260ug/Kg0.63NDDichlorodifluoromethane 5.0 04/11/14 U SW8260ug/Kg1.3NDEthylbenzene 5.0 04/11/14 U SW8260ug/Kg0.91NDHexachlorobutadiene 5.0 04/11/14 U SW8260ug/Kg1.1NDIsopropylbenzene 5.0 04/11/14 U SW8260ug/Kg0.96NDm&p-Xylene 5.0 04/11/14 U SW8260ug/Kg2.0NDMethyl Ethyl Ketone 30 04/11/14 U SW8260ug/Kg4.3NDMethyl t-butyl ether (MTBE) 10 04/11/14 U SW8260ug/Kg1.4NDMethylene chloride 5.0 04/11/14 U SW8260ug/Kg0.82NDNaphthalene 5.0 04/11/14 U SW8260ug/Kg1.3NDn-Butylbenzene 5.0 04/11/14 U SW8260ug/Kg0.91NDn-Propylbenzene 5.0 04/11/14 U SW8260ug/Kg0.90NDo-Xylene 5.0 04/11/14 U SW8260ug/Kg1.9NDp-Isopropyltoluene 5.0 04/11/14 U SW8260ug/Kg0.72NDsec-Butylbenzene 5.0 04/11/14 U SW8260ug/Kg0.94NDStyrene 5.0 04/11/14 U SW8260ug/Kg1.4NDtert-Butylbenzene 5.0 04/11/14 U SW8260ug/Kg0.80NDTetrachloroethene 5.0 04/11/14 U SW8260ug/Kg1.1NDTetrahydrofuran (THF) 10 04/11/14 U SW8260ug/Kg 14.5NDToluene 5.0 04/11/14 U SW8260ug/Kg0.79NDtrans-1,2-Dichloroethene 5.0 04/11/14 U SW8260ug/Kg1.0NDtrans-1,3-Dichloropropene 5.0 04/11/14 U SW8260ug/Kg1.0NDtrans-1,4-dichloro-2-butene 10 04/11/14 U SW8260ug/Kg9.3NDTrichloroethene 5.0 04/11/14 U SW8260ug/Kg1.1NDTrichlorofluoromethane 5.0 04/11/14 U SW8260ug/Kg1.1NDTrichlorotrifluoroethane 5.0 04/11/14 U SW8260ug/Kg0.78NDVinyl chloride 5.0 04/11/14 U SW8260ug/Kg1.6
QA/QC Surrogates103% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%93% Bromofluorobenzene 04/11/14 U 70 - 130 %%
Page 48 of 49 Ver 1
TRIP BLANK LOWPhoenix I.D.: BG30372
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
91% Dibromofluoromethane 04/11/14 U 70 - 130 %%102% Toluene-d8 04/11/14 U 70 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 49 of 49 Ver 1
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
QA/QC ReportApril 16, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG30363
LCS%
DupRPD
LCSD%
LCSRPD
%Rec
Limits
%RPD
LimitsSampleResult
DupResult
QA/QC Batch 271080, QC Sample No: BG30143 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369)
ICP Metals - SoilNC NCAluminum BRL NC11314.7 105 7.3 75 - 125 306310 7310
87.2 88.8Antimony BRL 1.884.5NC 80.6 4.7 75 - 125 301.1 <4.3
89.5 93.2Arsenic BRL 4.198.9NC 94.4 4.7 75 - 125 301.4 1.59
104 109Barium BRL 4.710310.5 97.4 5.6 75 - 125 3017.1 19.0
95.3 98.6Beryllium BRL 3.4103NC 98.6 4.4 75 - 125 300.22 0.22 B
87.8 90.5Cadmium BRL 3.095.1NC 90.2 5.3 75 - 125 30<0.39 <0.43
NC NCCalcium BRL NC1017.30 99.9 1.1 75 - 125 30798 742
97.6 102Chromium BRL 4.41067.50 100 5.8 75 - 125 309.16 9.87
94.4 97.9Cobalt BRL 3.61031.30 97.3 5.7 75 - 125 303.00 2.96
99.7 104Copper BRL 4.21042.10 100 3.9 75 - 125 306.36 6.23
NC NCIron 9.3 NC1212.70 113 6.8 75 - 125 3011100 10800
92.4 95.9Lead BRL 3.798.6NC 95.8 2.9 75 - 125 303.8 4.68
NC NCMagnesium BRL NC1091.50 102 6.6 75 - 125 301310 1330
104 107Manganese BRL 2.810712.1 102 4.8 75 - 125 3065.8 58.3
95.2 98.9Nickel BRL 3.81033.70 98.3 4.7 75 - 125 306.99 7.25
>130 >130Potassium BRL NC1211.70 112 7.7 m75 - 125 30474 466
79.1 83.0Selenium BRL 4.885.8NC 80.9 5.9 75 - 125 30<1.6 <1.7
93.9 97.3Silver BRL 3.6103NC 94.0 9.1 75 - 125 30<0.39 <0.43
NC NCSodium BRL NC1221.70 114 6.8 75 - 125 301140 1160
88.7 92.1Thallium BRL 3.898.1NC 91.1 7.4 75 - 125 30<3.5 <3.8
98.8 104Vanadium BRL 5.11061.80 102 3.8 75 - 125 3016.5 16.2
101 100Zinc BRL 1.098.65.00 93.3 5.5 75 - 125 3018.3 17.4
QA/QC Batch 271124, QC Sample No: BG30354 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369)107 92.5Mercury - Soil BRL 14.598.5NC 97.2 1.3 70 - 130 300.13 0.10
Additional Mercury criteria: LCS acceptance range for waters is 80-120% and for soils is 70-130%.
Comment:
QA/QC Batch 271068, QC Sample No: BG30370 (BG30370)
ICP Metals - SoilNC NCAluminum BRL NC1049.80 103 1.0 75 - 125 303800 4190
91.9 93.3Antimony BRL 1.5113NC 113 0.0 75 - 125 30<1.7 <1.7
88.4 89.6Arsenic BRL 1.394.2NC 92.8 1.5 75 - 125 30<0.7 0.76
101 102Barium BRL 1.010310.2 100 3.0 75 - 125 3021.4 23.7
94.8 95.2Beryllium BRL 0.4101NC 100 1.0 75 - 125 30<0.27 <0.26
87.8 88.1Cadmium BRL 0.395.9NC 94.8 1.2 75 - 125 30<0.33 <0.33
NC NCCalcium BRL NC1097.80 97.3 11.3 75 - 125 303100 3350
96.2 96.8Chromium BRL 0.61045.50 100 3.9 75 - 125 307.78 8.22
93.3 93.9Cobalt BRL 0.699.313.1 98.4 0.9 75 - 125 302.92 3.33
99.0 99.1Copper BRL 0.11051.70 102 2.9 75 - 125 309.10 9.26
NC NCIron 8.4 NC1123.60 110 1.8 75 - 125 309380 9720
90.6 91.6Lead BRL 1.194.9NC 92.6 2.5 75 - 125 302.2 2.94
Page 1 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
DupRPD
LCSD%
LCSRPD
%Rec
Limits
%RPD
LimitsSampleResult
DupResult
NC NCMagnesium BRL NC10327.0 99.6 3.4 75 - 125 302270 2980
109 94.9Manganese BRL 13.810327.1 101 2.0 75 - 125 30201 264
92.8 93.6Nickel BRL 0.999.84.70 98.2 1.6 75 - 125 307.62 7.27
>130 >130Potassium BRL NC11511.4 112 2.6 m75 - 125 30688 771
77.4 77.7Selenium BRL 0.482.8NC 81.4 1.7 75 - 125 30<1.3 <1.3
92.9 93.3Silver BRL 0.496.4NC 95.1 1.4 75 - 125 30<0.33 <0.33
129 129Sodium BRL 0.0117NC 115 1.7 m75 - 125 30124 117
88.7 89.3Thallium BRL 0.794.6NC 94.9 0.3 75 - 125 30<1.3 <1.3
100 98.0Vanadium BRL 2.010320.8 103 0.0 75 - 125 3012.5 15.4
87.9 89.8Zinc BRL 2.194.817.4 92.8 2.1 75 - 125 3014.7 17.5
QA/QC Batch 271125, QC Sample No: BG30370 (BG30370)104 101Mercury - Soil BRL 2.996.6NC 92.1 4.8 70 - 130 30<0.07 <0.08
Additional Mercury criteria: LCS acceptance range for waters is 80-120% and for soils is 70-130%.
Comment:
m = This parameter is outside laboratory ms/msd specified recovery limits.
Page 2 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
QA/QC ReportApril 16, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
QA/QC Batch 271077, QC Sample No: BG30355 (BG30363, BG30366, BG30368)
Pesticides - Solid107 834,4' -DDD ND 25.395 108 12.8 40 - 140 30
90 714,4' -DDE ND 23.689 90 1.1 40 - 140 30
82 644,4' -DDT ND 24.784 84 0.0 40 - 140 30
92 87a-BHC ND 5.681 93 13.8 40 - 140 30
93 80a-Chlordane ND 15.092 93 1.1 40 - 140 30
86 69Aldrin ND 21.981 73 10.4 40 - 140 30
98 91b-BHC ND 7.497 94 3.1 40 - 140 30
NA NAChlordane ND NCNA NA NC 40 - 140 30
77 71d-BHC ND 8.181 77 5.1 40 - 140 30
93 82Dieldrin ND 12.686 87 1.2 40 - 140 30
94 86Endosulfan I ND 8.983 91 9.2 40 - 140 30
93 80Endosulfan II ND 15.043 65 40.7 r40 - 140 30
88 79Endosulfan sulfate ND 10.860 65 8.0 40 - 140 30
96 85Endrin ND 12.294 93 1.1 40 - 140 30
85 78Endrin aldehyde ND 8.647 70 39.3 r40 - 140 30
103 95Endrin ketone ND 8.187 86 1.2 40 - 140 30
111 103g-BHC ND 7.594 93 1.1 40 - 140 30
99 82g-Chlordane ND 18.899 97 2.0 40 - 140 30
101 82Heptachlor ND 20.8103 99 4.0 40 - 140 30
103 93Heptachlor epoxide ND 10.292 93 1.1 40 - 140 30
121 102Methoxychlor ND 17.088 89 1.1 40 - 140 30
NA NAToxaphene ND NCNA NA NC 40 - 140 30
83 88% DCBP 93 5.886 95 9.9 30 - 150 30
83 81% TCMX 88 2.486 90 4.5 30 - 150 30
Alpha and gamma chlordane were spiked and analyzed instead of technical chlordane. Gamma chlordane recovery is reported in theLCS, LCSD, MS and MSD.
Comment:
QA/QC Batch 271075, QC Sample No: BG30355 (BG30363, BG30366, BG30368)
Polychlorinated Biphenyls - Solid92 98PCB-1016 ND 6.375 95 23.5 40 - 140 30
PCB-1221 ND 40 - 140 30
PCB-1232 ND 40 - 140 30
PCB-1242 ND 40 - 140 30
PCB-1248 ND 40 - 140 30
PCB-1254 ND 40 - 140 30
92 101PCB-1260 ND 9.399 91 8.4 40 - 140 30
PCB-1262 ND 40 - 140 30
PCB-1268 ND 40 - 140 30
89 87% DCBP (Surrogate Rec) 87 2.3100 90 10.5 30 - 150 30
92 90% TCMX (Surrogate Rec) 81 2.299 92 7.3 30 - 150 30
Page 3 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
QA/QC Batch 271323, QC Sample No: BG30364 (BG30363, BG30364 (91, 1X) , BG30365, BG30366, BG30367, BG30368, BG30369, BG30370, BG30371 (50X) , BG30372)
Volatiles - Solid101 1041,1,1,2-Tetrachloroethane ND 2.999 101 2.0 70 - 130 30
101 1001,1,1-Trichloroethane ND 1.092 94 2.2 70 - 130 30
92 931,1,2,2-Tetrachloroethane ND 1.190 92 2.2 70 - 130 30
102 951,1,2-Trichloroethane ND 7.195 102 7.1 70 - 130 30
95 971,1-Dichloroethane ND 2.190 97 7.5 70 - 130 30
94 951,1-Dichloroethene ND 1.185 92 7.9 70 - 130 30
100 971,1-Dichloropropene ND 3.092 95 3.2 70 - 130 30
98 981,2,3-Trichlorobenzene ND 0.090 95 5.4 70 - 130 30
95 951,2,3-Trichloropropane ND 0.095 97 2.1 70 - 130 30
96 961,2,4-Trichlorobenzene ND 0.090 94 4.3 70 - 130 30
102 1011,2,4-Trimethylbenzene ND 1.099 102 3.0 70 - 130 30
93 891,2-Dibromo-3-chloropropane ND 4.497 96 1.0 70 - 130 30
101 1011,2-Dibromoethane ND 0.0100 105 4.9 70 - 130 30
99 1001,2-Dichlorobenzene ND 1.092 94 2.2 70 - 130 30
111 1061,2-Dichloroethane ND 4.696 100 4.1 70 - 130 30
95 981,2-Dichloropropane ND 3.193 98 5.2 70 - 130 30
101 1011,3,5-Trimethylbenzene ND 0.096 98 2.1 70 - 130 30
97 981,3-Dichlorobenzene ND 1.093 95 2.1 70 - 130 30
98 1001,3-Dichloropropane ND 2.097 99 2.0 70 - 130 30
99 981,4-Dichlorobenzene ND 1.093 95 2.1 70 - 130 30
94 912,2-Dichloropropane ND 3.289 96 7.6 70 - 130 30
97 972-Chlorotoluene ND 0.090 97 7.5 70 - 130 30
84 892-Hexanone ND 5.8121 127 4.8 70 - 130 30
102 1022-Isopropyltoluene ND 0.096 99 3.1 70 - 130 30
98 1004-Chlorotoluene ND 2.092 98 6.3 70 - 130 30
101 1044-Methyl-2-pentanone ND 2.9127 133 4.6 l70 - 130 30
67 66Acetone ND 1.575 84 11.3 m70 - 130 30
93 93Acrylonitrile ND 0.091 102 11.4 70 - 130 30
97 98Benzene ND 1.094 97 3.1 70 - 130 30
98 99Bromobenzene ND 1.093 94 1.1 70 - 130 30
96 95Bromochloromethane ND 1.095 96 1.0 70 - 130 30
104 102Bromodichloromethane ND 1.994 95 1.1 70 - 130 30
100 101Bromoform ND 1.097 102 5.0 70 - 130 30
80 81Bromomethane ND 1.294 100 6.2 70 - 130 30
87 89Carbon Disulfide ND 2.387 92 5.6 70 - 130 30
100 102Carbon tetrachloride ND 2.094 94 0.0 70 - 130 30
99 99Chlorobenzene ND 0.097 96 1.0 70 - 130 30
82 83Chloroethane ND 1.290 93 3.3 70 - 130 30
102 102Chloroform ND 0.093 98 5.2 70 - 130 30
77 80Chloromethane ND 3.890 95 5.4 70 - 130 30
96 101cis-1,2-Dichloroethene ND 5.189 99 10.6 70 - 130 30
101 101cis-1,3-Dichloropropene ND 0.096 101 5.1 70 - 130 30
101 101Dibromochloromethane ND 0.0100 101 1.0 70 - 130 30
100 103Dibromomethane ND 3.097 99 2.0 70 - 130 30
72 70Dichlorodifluoromethane ND 2.888 92 4.4 70 - 130 30
99 98Ethylbenzene ND 1.097 95 2.1 70 - 130 30
97 101Hexachlorobutadiene ND 4.088 93 5.5 70 - 130 30
99 101Isopropylbenzene ND 2.092 98 6.3 70 - 130 30
100 99m&p-Xylene ND 1.097 98 1.0 70 - 130 30
Page 4 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
85 88Methyl ethyl ketone ND 3.5105 112 6.5 70 - 130 30
108 106Methyl t-butyl ether (MTBE) ND 1.993 96 3.2 70 - 130 30
90 89Methylene chloride ND 1.186 91 5.6 70 - 130 30
96 99Naphthalene ND 3.198 100 2.0 70 - 130 30
102 101n-Butylbenzene ND 1.098 101 3.0 70 - 130 30
94 95n-Propylbenzene ND 1.196 98 2.1 70 - 130 30
100 105o-Xylene ND 4.995 96 1.0 70 - 130 30
100 101p-Isopropyltoluene ND 1.097 97 0.0 70 - 130 30
97 98sec-Butylbenzene ND 1.091 92 1.1 70 - 130 30
103 104Styrene ND 1.095 97 2.1 70 - 130 30
98 99tert-Butylbenzene ND 1.094 96 2.1 70 - 130 30
98 95Tetrachloroethene ND 3.192 98 6.3 70 - 130 30
97 96Tetrahydrofuran (THF) ND 1.094 101 7.2 70 - 130 30
98 98Toluene ND 0.094 96 2.1 70 - 130 30
94 97trans-1,2-Dichloroethene ND 3.186 92 6.7 70 - 130 30
107 103trans-1,3-Dichloropropene ND 3.894 100 6.2 70 - 130 30
91 92trans-1,4-dichloro-2-butene ND 1.198 100 2.0 70 - 130 30
96 100Trichloroethene ND 4.195 98 3.1 70 - 130 30
62 63Trichlorofluoromethane ND 1.689 95 6.5 m70 - 130 30
99 101Trichlorotrifluoroethane ND 2.093 95 2.1 70 - 130 30
74 76Vinyl chloride ND 2.785 94 10.1 70 - 130 30
102 100% 1,2-dichlorobenzene-d4 102 2.099 97 2.0 70 - 130 30
103 102% Bromofluorobenzene 98 1.0102 100 2.0 70 - 130 30
103 103% Dibromofluoromethane 104 0.099 103 4.0 70 - 130 30
99 98% Toluene-d8 100 1.0101 101 0.0 70 - 130 30
Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.
Comment:
QA/QC Batch 271082, QC Sample No: BG30364 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369, BG30370)
Semivolatiles - Solid84 881,2,4,5-Tetrachlorobenzene ND 4.770 78 10.8 30 - 130 30
80 841,2,4-Trichlorobenzene ND 4.968 76 11.1 30 - 130 30
82 861,2-Dichlorobenzene ND 4.871 79 10.7 30 - 130 30
92 981,2-Diphenylhydrazine ND 6.376 85 11.2 30 - 130 30
80 861,3-Dichlorobenzene ND 7.270 78 10.8 30 - 130 30
81 851,4-Dichlorobenzene ND 4.869 78 12.2 30 - 130 30
100 1022,4,5-Trichlorophenol ND 2.081 91 11.6 30 - 130 30
96 982,4,6-Trichlorophenol ND 2.180 88 9.5 30 - 130 30
77 942,4-Dichlorophenol ND 19.975 84 11.3 30 - 130 30
45 552,4-Dimethylphenol ND 20.045 50 10.5 30 - 130 30
36 272,4-Dinitrophenol ND 28.618 33 58.8 l,m,r30 - 130 30
93 992,4-Dinitrotoluene ND 6.376 87 13.5 30 - 130 30
94 972,6-Dinitrotoluene ND 3.178 87 10.9 30 - 130 30
91 942-Chloronaphthalene ND 3.277 84 8.7 30 - 130 30
86 902-Chlorophenol ND 4.573 82 11.6 30 - 130 30
85 892-Methylnaphthalene ND 4.672 80 10.5 30 - 130 30
80 792-Methylphenol (o-cresol) ND 1.369 77 11.0 30 - 130 30
114 1192-Nitroaniline ND 4.385 103 19.1 30 - 130 30
75 892-Nitrophenol ND 17.169 79 13.5 30 - 130 30
85 903&4-Methylphenol (m&p-cresol) ND 5.772 81 11.8 30 - 130 30
116 1173,3'-Dichlorobenzidine ND 0.9108 115 6.3 30 - 130 30
93 893-Nitroaniline ND 4.480 91 12.9 30 - 130 30
Page 5 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
96 994,6-Dinitro-2-methylphenol ND 3.152 76 37.5 r30 - 130 30
92 964-Bromophenyl phenyl ether ND 4.379 87 9.6 30 - 130 30
91 984-Chloro-3-methylphenol ND 7.477 87 12.2 30 - 130 30
55 524-Chloroaniline ND 5.654 57 5.4 30 - 130 30
92 944-Chlorophenyl phenyl ether ND 2.275 83 10.1 30 - 130 30
97 994-Nitroaniline ND 2.079 89 11.9 30 - 130 30
103 1034-Nitrophenol ND 0.083 101 19.6 30 - 130 30
86 90Acenaphthene ND 4.572 81 11.8 30 - 130 30
90 92Acenaphthylene ND 2.274 83 11.5 30 - 130 30
88 93Acetophenone ND 5.573 83 12.8 30 - 130 30
81 80Aniline ND 1.273 77 5.3 30 - 130 30
92 96Anthracene ND 4.376 87 13.5 30 - 130 30
93 97Benz(a)anthracene ND 4.278 86 9.8 30 - 130 30
142 135Benzidine ND 5.1174 >200 NC l,m30 - 130 30
81 86Benzo(a)pyrene ND 6.069 77 11.0 30 - 130 30
88 93Benzo(b)fluoranthene ND 5.576 85 11.2 30 - 130 30
93 103Benzo(ghi)perylene ND 10.277 87 12.2 30 - 130 30
92 97Benzo(k)fluoranthene ND 5.374 83 11.5 30 - 130 30
89 98Benzyl butyl phthalate ND 9.683 86 3.6 30 - 130 30
72 87Bis(2-chloroethoxy)methane ND 18.970 76 8.2 30 - 130 30
81 85Bis(2-chloroethyl)ether ND 4.867 76 12.6 30 - 130 30
86 88Bis(2-chloroisopropyl)ether ND 2.370 78 10.8 30 - 130 30
91 99Bis(2-ethylhexyl)phthalate ND 8.483 85 2.4 30 - 130 30
96 99Carbazole ND 3.176 90 16.9 30 - 130 30
92 97Chrysene ND 5.378 87 10.9 30 - 130 30
95 103Dibenz(a,h)anthracene ND 8.178 89 13.2 30 - 130 30
90 95Dibenzofuran ND 5.474 84 12.7 30 - 130 30
92 97Diethyl phthalate ND 5.377 84 8.7 30 - 130 30
90 92Dimethylphthalate ND 2.276 83 8.8 30 - 130 30
89 94Di-n-butylphthalate ND 5.581 86 6.0 30 - 130 30
91 99Di-n-octylphthalate ND 8.481 88 8.3 30 - 130 30
93 96Fluoranthene ND 3.278 87 10.9 30 - 130 30
94 97Fluorene ND 3.176 85 11.2 30 - 130 30
86 93Hexachlorobenzene ND 7.878 84 7.4 30 - 130 30
79 83Hexachlorobutadiene ND 4.969 75 8.3 30 - 130 30
71 70Hexachlorocyclopentadiene ND 1.454 64 16.9 30 - 130 30
80 83Hexachloroethane ND 3.768 76 11.1 30 - 130 30
94 102Indeno(1,2,3-cd)pyrene ND 8.278 87 10.9 30 - 130 30
77 92Isophorone ND 17.874 82 10.3 30 - 130 30
82 87Naphthalene ND 5.970 78 10.8 30 - 130 30
85 88Nitrobenzene ND 3.570 79 12.1 30 - 130 30
83 86N-Nitrosodimethylamine ND 3.669 76 9.7 30 - 130 30
88 92N-Nitrosodi-n-propylamine ND 4.472 81 11.8 30 - 130 30
98 101N-Nitrosodiphenylamine ND 3.080 90 11.8 30 - 130 30
93 96Pentachloronitrobenzene ND 3.280 86 7.2 30 - 130 30
92 93Pentachlorophenol ND 1.160 75 22.2 30 - 130 30
92 97Phenanthrene ND 5.378 87 10.9 30 - 130 30
89 92Phenol ND 3.374 83 11.5 30 - 130 30
94 97Pyrene ND 3.177 89 14.5 30 - 130 30
70 69Pyridine ND 1.462 65 4.7 30 - 130 30
84 92% 2,4,6-Tribromophenol 80 9.175 77 2.6 30 - 130 30
56 57% 2-Fluorobiphenyl 55 1.847 50 6.2 30 - 130 30
78 82% 2-Fluorophenol 81 5.066 71 7.3 30 - 130 30
Page 6 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG30363
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
54 55% Nitrobenzene-d5 52 1.844 49 10.8 30 - 130 30
82 85% Phenol-d5 81 3.669 75 8.3 30 - 130 30
64 65% Terphenyl-d14 62 1.653 59 10.7 30 - 130 30
Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)
Comment:
QA/QC Batch 271482, QC Sample No: BG30788 (BG30366 (71X) )
Volatiles - Solid99 971,2,3-Trichlorobenzene ND 2.0100 106 5.8 70 - 130 30
91 891,2,3-Trichloropropane ND 2.295 98 3.1 70 - 130 30
105 1031,2,4-Trichlorobenzene ND 1.9106 109 2.8 70 - 130 30
100 991,2,4-Trimethylbenzene ND 1.0114 116 1.7 70 - 130 30
94 891,2-Dibromo-3-chloropropane ND 5.594 97 3.1 70 - 130 30
96 971,2-Dichlorobenzene ND 1.0100 103 3.0 70 - 130 30
100 981,3,5-Trimethylbenzene ND 2.0111 111 0.0 70 - 130 30
100 991,3-Dichlorobenzene ND 1.0104 107 2.8 70 - 130 30
98 981,4-Dichlorobenzene ND 0.0103 106 2.9 70 - 130 30
101 1032-Chlorotoluene ND 2.0103 106 2.9 70 - 130 30
104 1022-Isopropyltoluene ND 1.9111 113 1.8 70 - 130 30
100 1004-Chlorotoluene ND 0.0107 108 0.9 70 - 130 30
99 98Bromobenzene ND 1.0100 102 2.0 70 - 130 30
95 96Hexachlorobutadiene ND 1.0103 105 1.9 70 - 130 30
102 101Isopropylbenzene ND 1.0111 111 0.0 70 - 130 30
105 102Naphthalene ND 2.9100 105 4.9 70 - 130 30
103 101n-Butylbenzene ND 2.0118 118 0.0 70 - 130 30
97 97n-Propylbenzene ND 0.0112 116 3.5 70 - 130 30
102 101p-Isopropyltoluene ND 1.0116 114 1.7 70 - 130 30
100 99sec-Butylbenzene ND 1.0107 107 0.0 70 - 130 30
98 98tert-Butylbenzene ND 0.0109 111 1.8 70 - 130 30
100 97trans-1,4-dichloro-2-butene ND 3.0105 108 2.8 70 - 130 30
101 100% 1,2-dichlorobenzene-d4 100 1.098 99 1.0 70 - 130 30
97 97% Bromofluorobenzene 100 0.0106 102 3.8 70 - 130 30
Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.
Comment:
l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.
MS - Matrix SpikePhyllis Shiller, Laboratory Director
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.
April 16, 2014MS Dup - Matrix Spike Duplicate
RPD - Relative Percent Difference
LCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate
NC - No Criteria
Intf - Interference
Page 7 of 7
Sample Criteria Exceedences ReportWednesday, April 16, 2014 Page 1 of 2
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG30363 - EBCCriteria: NY: 375, 375RRS, 375RS
RLCriteria
State: NY
HG-SM Mercury 0.180.55 0.06 mg/KgBG30363 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 6398.7 0.7 mg/KgBG30363 NY / 375-6.8 Metals / Unrestricted Use Soil 63
$8260MADPR Acetone 5068 54 ug/KgBG30366 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8270SMRDP Phenol 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Pentachlorophenol 800ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 800990 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$PCB_SMRDP PCB-1254 100210 36 ug/KgBG30366 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PESTSMDPR 4,4' -DDT 3.324 2.6 ug/KgBG30366 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3HG-SM Mercury 0.180.34 0.06 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 63156 6.7 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SMDP Zinc 109130 0.7 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 109
PB-SMDP Lead 63174 7.7 mg/KgBG30368 NY / 375-6.8 Metals / Unrestricted Use Soil 63
$8260-SMDPR Vinyl chloride 210ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Residential 210$8260-SMDPR trans-1,2-Dichloroethene 190ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 190$8260-SMDPR Methylene chloride 50ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR Methyl Ethyl Ketone 120ND 1500 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260-SMDPR Benzene 60ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260-SMDPR 1,2-Dichloroethane 20ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Vinyl chloride 20ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Acetone 50ND 2500 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50
Sample Criteria Exceedences ReportWednesday, April 16, 2014 Page 2 of 2
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG30363 - EBCCriteria: NY: 375, 375RRS, 375RS
RLCriteria
State: NY
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
NY Temperature NarrationApril 16, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG30363
The samples in this delivery group were received at 4°C.(Note acceptance criteria is above freezing up to 6°C)
Page 1 of 1
BG43036
Friday, May 16, 2014
Sample ID#s:
Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Project ID: DOMINO SUGAR SITE E
Sincerely yours,
Laboratory DirectorPhyllis Shiller
If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.
NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B
NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
GROUND WATEREBC72 Hour
05/08/14SWsee "By" below
Laboratory Data
E-MW 3
Phoenix ID: BG43036
05/09/140:00
16:47
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportMay 16, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG43036
Client ID:Project ID: DOMINO SUGAR SITE E
LOD/MDL
0.001Silver (Dissolved) 0.005 05/09/14 LK SW6010mg/L0.001B0.39Aluminum (Dissolved) 0.01 05/09/14 LK SW6010mg/L0.00260.003Arsenic, (Dissolved) 0.003 05/09/14 LK SW6010mg/L0.001B*0.100Barium (Dissolved) 0.011 05/09/14 LK SW6010mg/L0.001
< 0.001Beryllium (Dissolved) 0.001 05/09/14 LK SW6010mg/L0.00139.6Calcium (Dissolved) 0.01 05/09/14 LK SW6010mg/L0.0030.001Cadmium (Dissolved) 0.004 05/09/14 LK SW6010mg/L0.0005B
< 0.005Cobalt, (Dissolved) 0.005 05/09/14 LK SW6010mg/L0.0010.005Chromium (Dissolved) 0.001 05/09/14 LK SW6010mg/L0.0010.003Copper, (Dissolved) 0.005 05/12/14 LK SW6010mg/L0.001B*0.38Iron, (Dissolved) 0.01 05/09/14 LK SW6010mg/L0.01
< 0.0004Mercury (Dissolved) 0.0004 05/12/14 RS SW7470mg/L0.000312.5Potassium (Dissolved) 0.1 05/09/14 LK SW6010mg/L0.18.03Magnesium (Dissolved) 0.01 05/09/14 LK SW6010mg/L0.0010.019Manganese, (Dissolved) 0.005 05/09/14 LK SW6010mg/L0.00187.5Sodium (Dissolved) 1.1 05/09/14 LK SW6010mg/L1.1
< 0.004Nickel, (Dissolved) 0.004 05/09/14 LK SW6010mg/L0.0010.001Lead (Dissolved) 0.002 05/09/14 LK SW6010mg/L0.001B
< 0.003Antimony, (Dissolved) 0.003 05/12/14 RS 7010mg/L0.0030.068Selenium, (Dissolved) 0.004 05/13/14 TH 7010mg/L0.002
< 0.001Thallium , (Dissolved) 0.001 05/12/14 RS 7010mg/L0.0010.007Vanadium, (Dissolved) 0.011 05/09/14 LK SW6010mg/L0.001B0.008Zinc, (Dissolved) 0.011 05/09/14 LK SW6010mg/L0.001B
CompletedFiltration 05/09/14 AG 0.45um Filter
CompletedDissolved Mercury Digestion 05/12/14 I/I SW7470CompletedPCB Extraction (2 Liter) 05/09/14 L SW3510CompletedExtraction for Pest (2 Liter) 05/09/14 L SW3510CompletedSemi-Volatile Extraction 05/09/14 E/X SW3520
Page 1 of 6 Ver 1
E-MW 3Phoenix I.D.: BG43036
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
CompletedDissolved Metals Preparation 05/09/14 AG SW846-3005
PesticidesND4,4' -DDD 0.14 05/13/14 CE SW8081ug/L0.14ND4,4' -DDE 0.14 05/13/14 CE SW8081ug/L0.14ND4,4' -DDT 0.14 05/13/14 CE SW8081ug/L0.14NDa-BHC 0.069 05/13/14 CE SW8081ug/L0.069NDa-chlordane 0.14 05/13/14 CE SW8081ug/L0.14NDAlachlor 1.0 05/13/14 CE SW8081ug/L 11.0NDAldrin 0.021 05/13/14 CE SW8081ug/L0.021NDb-BHC 0.069 05/13/14 CE SW8081ug/L0.069NDChlordane 1.4 05/13/14 CE SW8081ug/L1.4NDd-BHC 0.069 05/13/14 CE SW8081ug/L0.069NDDieldrin 0.021 05/13/14 CE SW8081ug/L0.021NDEndosulfan I 0.14 05/13/14 CE SW8081ug/L0.14NDEndosulfan II 0.14 05/13/14 CE SW8081ug/L0.14NDEndosulfan Sulfate 0.14 05/13/14 CE SW8081ug/L0.14NDEndrin 0.14 05/13/14 CE SW8081ug/L0.14NDEndrin Aldehyde 0.14 05/13/14 CE SW8081ug/L0.14NDEndrin ketone 0.14 05/13/14 CE SW8081ug/L0.14NDg-BHC (Lindane) 0.069 05/13/14 CE SW8081ug/L0.069NDg-chlordane 0.14 05/13/14 CE SW8081ug/L0.14NDHeptachlor 0.14 05/13/14 CE SW8081ug/L0.14NDHeptachlor epoxide 0.14 05/13/14 CE SW8081ug/L0.14NDMethoxychlor 1.4 05/13/14 CE SW8081ug/L1.4NDToxaphene 3.5 05/13/14 CE SW8081ug/L3.5
QA/QC SurrogatesDiluted Out%DCBP (Surrogate Rec) 05/13/14 CE SW8081%Diluted Out%TCMX (Surrogate Rec) 05/13/14 CE SW8081%
Polychlorinated BiphenylsNDPCB-1016 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1221 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1232 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1242 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1248 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1254 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1260 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1262 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1268 0.069 05/12/14 AW 608/ 8082ug/L0.069
QA/QC Surrogates53% DCBP 05/12/14 AW 608/ 8082%67% TCMX 05/12/14 AW 608/ 8082%
VolatilesND1,1,1,2-Tetrachloroethane 1.0 05/14/14 RM SW8260ug/L0.19ND1,1,1-Trichloroethane 5.0 05/14/14 RM SW8260ug/L0.19ND1,1,2,2-Tetrachloroethane 1.0 05/14/14 RM SW8260ug/L0.15ND1,1,2-Trichloroethane 1.0 05/14/14 RM SW8260ug/L0.20ND1,1-Dichloroethane 5.0 05/14/14 RM SW8260ug/L0.23
Page 2 of 6 Ver 1
E-MW 3Phoenix I.D.: BG43036
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 1.0 05/14/14 RM SW8260ug/L0.24ND1,1-Dichloropropene 1.0 05/14/14 RM SW8260ug/L0.20ND1,2,3-Trichlorobenzene 1.0 05/14/14 RM SW8260ug/L0.20ND1,2,3-Trichloropropane 1.0 05/14/14 RM SW8260ug/L0.21ND1,2,4-Trichlorobenzene 1.0 05/14/14 RM SW8260ug/L0.18ND1,2,4-Trimethylbenzene 1.0 05/14/14 RM SW8260ug/L0.18ND1,2-Dibromo-3-chloropropane 1.0 05/14/14 RM SW8260ug/L0.36ND1,2-Dibromoethane 1.0 05/14/14 RM SW8260ug/L0.20ND1,2-Dichlorobenzene 1.0 05/14/14 RM SW8260ug/L0.16ND1,2-Dichloroethane 2.0 05/14/14 RM SW8260ug/L0.20ND1,2-Dichloropropane 1.0 05/14/14 RM SW8260ug/L0.18ND1,3,5-Trimethylbenzene 1.0 05/14/14 RM SW8260ug/L0.21ND1,3-Dichlorobenzene 5.0 05/14/14 RM SW8260ug/L0.19ND1,3-Dichloropropane 1.0 05/14/14 RM SW8260ug/L0.22ND1,4-Dichlorobenzene 5.0 05/14/14 RM SW8260ug/L0.19ND2,2-Dichloropropane 1.0 05/14/14 RM SW8260ug/L0.16ND2-Chlorotoluene 1.0 05/14/14 RM SW8260ug/L0.23ND2-Hexanone 1.0 05/14/14 RM SW8260ug/L0.27ND2-Isopropyltoluene 1.0 05/14/14 RM SW8260ug/L 10.21ND4-Chlorotoluene 1.0 05/14/14 RM SW8260ug/L0.16ND4-Methyl-2-pentanone 1.0 05/14/14 RM SW8260ug/L0.192.7Acetone 5.0 05/14/14 RM SW8260ug/L0.31JSNDAcrolein 5.0 05/14/14 RM SW8260ug/L0.95NDAcrylonitrile 5.0 05/14/14 RM SW8260ug/L0.17NDBenzene 0.70 05/14/14 RM SW8260ug/L0.19NDBromobenzene 1.0 05/14/14 RM SW8260ug/L0.20NDBromochloromethane 1.0 05/14/14 RM SW8260ug/L0.22NDBromodichloromethane 1.0 05/14/14 RM SW8260ug/L0.16NDBromoform 5.0 05/14/14 RM SW8260ug/L0.10NDBromomethane 5.0 05/14/14 RM SW8260ug/L0.25NDCarbon Disulfide 1.0 05/14/14 RM SW8260ug/L0.24NDCarbon tetrachloride 1.0 05/14/14 RM SW8260ug/L0.23NDChlorobenzene 5.0 05/14/14 RM SW8260ug/L0.20NDChloroethane 5.0 05/14/14 RM SW8260ug/L0.24NDChloroform 5.0 05/14/14 RM SW8260ug/L0.22NDChloromethane 5.0 05/14/14 RM SW8260ug/L0.21NDcis-1,2-Dichloroethene 1.0 05/14/14 RM SW8260ug/L0.23NDcis-1,3-Dichloropropene 0.40 05/14/14 RM SW8260ug/L0.15NDDibromochloromethane 1.0 05/14/14 RM SW8260ug/L0.15NDDibromomethane 1.0 05/14/14 RM SW8260ug/L0.23NDDichlorodifluoromethane 1.0 05/14/14 RM SW8260ug/L0.26NDEthylbenzene 1.0 05/14/14 RM SW8260ug/L0.19NDHexachlorobutadiene 1.0 05/14/14 RM SW8260ug/L0.13NDIsopropylbenzene 1.0 05/14/14 RM SW8260ug/L0.22NDm&p-Xylene 1.0 05/14/14 RM SW8260ug/L0.42NDMethyl ethyl ketone 1.0 05/14/14 RM SW8260ug/L0.50NDMethyl t-butyl ether (MTBE) 1.0 05/14/14 RM SW8260ug/L0.190.38Methylene chloride 3.0 05/14/14 RM SW8260ug/L0.16JSNDNaphthalene 1.0 05/14/14 RM SW8260ug/L0.19
Page 3 of 6 Ver 1
E-MW 3Phoenix I.D.: BG43036
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Butylbenzene 1.0 05/14/14 RM SW8260ug/L0.22NDn-Propylbenzene 1.0 05/14/14 RM SW8260ug/L0.20NDo-Xylene 1.0 05/14/14 RM SW8260ug/L0.45NDp-Isopropyltoluene 1.0 05/14/14 RM SW8260ug/L0.21NDsec-Butylbenzene 1.0 05/14/14 RM SW8260ug/L0.22NDStyrene 1.0 05/14/14 RM SW8260ug/L0.41NDtert-Butylbenzene 1.0 05/14/14 RM SW8260ug/L0.23NDTetrachloroethene 1.0 05/14/14 RM SW8260ug/L0.24NDTetrahydrofuran (THF) 5.0 05/14/14 RM SW8260ug/L 10.51NDToluene 1.0 05/14/14 RM SW8260ug/L0.20NDtrans-1,2-Dichloroethene 5.0 05/14/14 RM SW8260ug/L0.20NDtrans-1,3-Dichloropropene 0.40 05/14/14 RM SW8260ug/L0.14NDtrans-1,4-dichloro-2-butene 1.0 05/14/14 RM SW8260ug/L0.450.32Trichloroethene 1.0 05/14/14 RM SW8260ug/L0.18JNDTrichlorofluoromethane 1.0 05/14/14 RM SW8260ug/L0.23NDTrichlorotrifluoroethane 1.0 05/14/14 RM SW8260ug/L0.23NDVinyl chloride 1.0 05/14/14 RM SW8260ug/L0.14
QA/QC Surrogates98% 1,2-dichlorobenzene-d4 05/14/14 RM 70 - 121 %%94% Bromofluorobenzene 05/14/14 RM 59 - 113 %%98% Dibromofluoromethane 05/14/14 RM 70 - 130 %%99% Toluene-d8 05/14/14 RM 84 - 138 %%
SemivolatilesND1,2,4-Trichlorobenzene 5.0 05/14/14 KCA SW 8270ug/L1.5ND1,2-Dichlorobenzene 1.0 05/14/14 KCA SW 8270ug/L1.4ND1,2-Diphenylhydrazine 5.0 05/14/14 KCA SW 8270ug/L1.6ND1,3-Dichlorobenzene 1.0 05/14/14 KCA SW 8270ug/L1.5ND1,4-Dichlorobenzene 1.0 05/14/14 KCA SW 8270ug/L1.5ND2,4,5-Trichlorophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2,4,6-Trichlorophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2,4-Dichlorophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2,4-Dimethylphenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2,4-Dinitrophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2,4-Dinitrotoluene 5.0 05/14/14 KCA SW 8270ug/L2.0ND2,6-Dinitrotoluene 5.0 05/14/14 KCA SW 8270ug/L1.6ND2-Chloronaphthalene 5.0 05/14/14 KCA SW 8270ug/L1.4ND2-Chlorophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2-Methylnaphthalene 5.0 05/14/14 KCA SW 8270ug/L1.5ND2-Methylphenol (o-cresol) 1.0 05/14/14 KCA SW 8270ug/L1.0ND2-Nitroaniline 5.0 05/14/14 KCA SW 8270ug/L5.0ND2-Nitrophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND3&4-Methylphenol (m&p-cresol) 1.0 05/14/14 KCA SW 8270ug/L1.0ND3,3'-Dichlorobenzidine 5.0 05/14/14 KCA SW 8270ug/L2.4ND3-Nitroaniline 5.0 05/14/14 KCA SW 8270ug/L5.0ND4,6-Dinitro-2-methylphenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND4-Bromophenyl phenyl ether 5.0 05/14/14 KCA SW 8270ug/L1.5ND4-Chloro-3-methylphenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND4-Chloroaniline 3.5 05/14/14 KCA SW 8270ug/L2.3ND4-Chlorophenyl phenyl ether 5.0 05/14/14 KCA SW 8270ug/L1.7
Page 4 of 6 Ver 1
E-MW 3Phoenix I.D.: BG43036
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Nitroaniline 5.0 05/14/14 KCA SW 8270ug/L1.7ND4-Nitrophenol 1.0 05/14/14 KCA SW 8270ug/L1.0NDAcenaphthene 5.0 05/14/14 KCA SW 8270ug/L1.5NDAcetophenone 5.0 05/14/14 KCA SW 8270ug/L1.6NDAniline 3.5 05/14/14 KCA SW 8270ug/L5.0NDAnthracene 5.0 05/14/14 KCA SW 8270ug/L1.6NDBenzidine 4.5 05/14/14 KCA SW 8270ug/L2.9NDBenzoic acid 25 05/14/14 KCA SW 8270ug/L10NDBenzyl butyl phthalate 5.0 05/14/14 KCA SW 8270ug/L1.3NDBis(2-chloroethoxy)methane 5.0 05/14/14 KCA SW 8270ug/L1.4NDBis(2-chloroethyl)ether 1.0 05/14/14 KCA SW 8270ug/L1.0NDBis(2-chloroisopropyl)ether 5.0 05/14/14 KCA SW 8270ug/L1.4NDCarbazole 25 05/14/14 KCA SW 8270ug/L3.8NDDibenzofuran 5.0 05/14/14 KCA SW 8270ug/L1.5NDDiethyl phthalate 5.0 05/14/14 KCA SW 8270ug/L1.6NDDimethylphthalate 5.0 05/14/14 KCA SW 8270ug/L1.6NDDi-n-butylphthalate 5.0 05/14/14 KCA SW 8270ug/L1.3NDDi-n-octylphthalate 5.0 05/14/14 KCA SW 8270ug/L1.3NDFluoranthene 5.0 05/14/14 KCA SW 8270ug/L1.6NDFluorene 5.0 05/14/14 KCA SW 8270ug/L1.7NDHexachlorocyclopentadiene 5.0 05/14/14 KCA SW 8270ug/L1.5NDIsophorone 5.0 05/14/14 KCA SW 8270ug/L1.4NDNaphthalene 5.0 05/14/14 KCA SW 8270ug/L1.4NDN-Nitrosodimethylamine 1.0 05/14/14 KCA SW 8270ug/L1.0NDN-Nitrosodi-n-propylamine 5.0 05/14/14 KCA SW 8270ug/L1.6NDN-Nitrosodiphenylamine 5.0 05/14/14 KCA SW 8270ug/L1.9NDPhenol 1.0 05/14/14 KCA SW 8270ug/L1.6NDPyrene 5.0 05/14/14 KCA SW 8270ug/L1.7NDPyridine 10 05/14/14 KCA SW 8270ug/L1.2
QA/QC Surrogates117% 2,4,6-Tribromophenol 05/14/14 KCA 19 - 122 %%77% 2-Fluorobiphenyl 05/14/14 KCA 30 - 115 %%76% 2-Fluorophenol 05/14/14 KCA 25 - 121 %%84% Nitrobenzene-d5 05/14/14 KCA 23 - 120 %%53% Phenol-d5 05/14/14 KCA 24 - 113 %%79% Terphenyl-d14 05/14/14 KCA 18 - 137 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 0.50 05/12/14 KCA SW8270 (SIM)ug/L0.50NDAcenaphthylene 0.10 05/12/14 KCA SW8270 (SIM)ug/L0.10
0.060Benz(a)anthracene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.0200.020Benzo(a)pyrene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.0200.040Benzo(b)fluoranthene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.0200.020Benzo(ghi)perylene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDBenzo(k)fluoranthene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDBis(2-ethylhexyl)phthalate 1.0 05/12/14 KCA SW8270 (SIM)ug/L1.0
0.050Chrysene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDDibenz(a,h)anthracene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDHexachlorobenzene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDHexachlorobutadiene 0.40 05/12/14 KCA SW8270 (SIM)ug/L0.40
Page 5 of 6 Ver 1
E-MW 3Phoenix I.D.: BG43036
Client ID:DOMINO SUGAR SITE EProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDHexachloroethane 0.50 05/12/14 KCA SW8270 (SIM)ug/L0.50NDIndeno(1,2,3-cd)pyrene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDNitrobenzene 0.10 05/12/14 KCA SW8270 (SIM)ug/L0.10NDPentachloronitrobenzene 0.10 05/12/14 KCA SW8270 (SIM)ug/L0.10NDPentachlorophenol 0.80 05/12/14 KCA SW8270 (SIM)ug/L0.800.23Phenanthrene 0.10 05/12/14 KCA SW8270 (SIM)ug/L0.10
QA/QC Surrogates124% 2,4,6-Tribromophenol 05/12/14 KCA 19 - 122 %% 3
94% 2-Fluorobiphenyl 05/12/14 KCA 30 - 115 %%77% 2-Fluorophenol 05/12/14 KCA 25 - 121 %%91% Nitrobenzene-d5 05/12/14 KCA 23 - 120 %%81% Phenol-d5 05/12/14 KCA 24 - 113 %%88% Terphenyl-d14 05/12/14 KCA 18 - 137 %%
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.
Phyllis Shiller, Laboratory DirectorMay 16, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.3 = This parameter exceeds laboratory specified limits.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Bobbi Aloisa, Vice President
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 6 of 6 Ver 1
Sample Criteria Exceedences ReportFriday, May 16, 2014 Page 1 of 2
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG43036 - EBCCriteria: NY: GW
RLCriteria
State: NY
$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.04$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.0020.050 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.040 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(a)pyrene 0.0020.020 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.060 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.040 0.020 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.050 0.020 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.060 0.020 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.020 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.020 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.002$DPPEST_GA Aldrin 0.01ND 0.021 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA a-BHC 0.05ND 0.069 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.05$DPPEST_GA a-BHC 0.01ND 0.069 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.01$DPPEST_GA b-BHC 0.05ND 0.069 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.05$DPPEST_GA b-BHC 0.04ND 0.069 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.04$DPPEST_GA d-BHC 0.05ND 0.069 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.05$DPPEST_GA d-BHC 0.04ND 0.069 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.04$DPPEST_GA g-BHC (Lindane) 0.05ND 0.069 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.05$DPPEST_GA g-BHC (Lindane) 0.05ND 0.069 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.05$DPPEST_GA Chlordane 0.1ND 1.4 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$DPPEST_GA Chlordane 0.05ND 1.4 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.05$DPPEST_GA 4,4' -DDD 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA 4,4' -DDE 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA 4,4' -DDT 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA Dieldrin 0.01ND 0.021 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA Dieldrin 0.004ND 0.021 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.004$DPPEST_GA Endosulfan I 0.1ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$DPPEST_GA Endosulfan II 0.1ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$DPPEST_GA Endosulfan Sulfate 0.1ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$DPPEST_GA Endrin 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA Heptachlor 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA Heptachlor 0.04ND 0.14 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.04$DPPEST_GA Heptachlor epoxide 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA Heptachlor epoxide 0.03ND 0.14 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.03$DPPEST_GA Alachlor 0.5ND 1.0 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.5$DPPEST_GA Toxaphene 0.06ND 3.5 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.06$DPPEST_GA g-chlordane 0.1ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1
Sample Criteria Exceedences ReportFriday, May 16, 2014 Page 2 of 2
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG43036 - EBCCriteria: NY: GW
RLCriteria
State: NY
D-AL Aluminum (Dissolved) 0.10.39 0.01 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.1DFE-WMDP Iron, (Dissolved) 0.30.38 0.01 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.3D-NA Sodium (Dissolved) 2087.5 1.1 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 20DSE-WMDP Selenium, (Dissolved) 0.010.068 0.004 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.01DTL-WMDP Thallium , (Dissolved) 0.0005BRL 0.001 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.0005
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
NY Temperature NarrationMay 16, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG43036
The samples in this delivery group were received at 4°C.(Note acceptance criteria is above freezing up to 6°C)
Page 1 of 1
BG31847 - BG31850
Friday, April 18, 2014
Sample ID#s:
Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Project ID: DOMINO SUGAR SITE E
Sincerely yours,
Laboratory DirectorPhyllis Shiller
If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.
NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B
NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
AIREBC72 Hour
04/09/14SWsee "By" below
DM
Laboratory Data
E-SG2
Phoenix ID: BG31847
04/11/1410:4517:36
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 18, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG31847
Client ID:Project ID: DOMINO SUGAR SITE E
ug/m3RL
Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 11.00ND1,1,1-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1,2,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 04/15/14 KCA TO15ND 1.007.021,2,4-Trimethylbenzene 0.204 04/15/14 KCA TO1534.5 1.00ND1,2-Dibromoethane(EDB) 0.130 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 04/15/14 KCA TO15ND 1.001.891,3,5-Trimethylbenzene 0.204 04/15/14 KCA TO159.28 1.00ND1,3-Butadiene 0.452 04/15/14 KCA TO15ND 1.000.921,3-Dichlorobenzene 0.166 04/15/14 KCA TO155.53 1.00ND1,4-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 04/15/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 04/15/14 KCA TO15ND 11.001.44-Ethyltoluene 0.204 04/15/14 KCA TO156.88 11.00ND4-Isopropyltoluene 0.182 04/15/14 KCA TO15ND 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 04/15/14 KCA TO15ND 1.00163Acetone 0.421 04/15/14 KCA TO15387 1.00NDAcrylonitrile 0.461 04/15/14 KCA TO15ND 1.001.04Benzene 0.313 04/15/14 KCA TO153.32 1.00NDBenzyl chloride 0.193 04/15/14 KCA TO15ND 1.00
Page 1 of 12 Ver 1
E-SG2Phoenix I.D.: BG31847
Client ID:DOMINO SUGAR SITE EProject ID:
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
ug/m3RL
NDBromodichloromethane 0.149 04/15/14 KCA TO15ND 1.00NDBromoform 0.097 04/15/14 KCA TO15ND 1.00NDBromomethane 0.258 04/15/14 KCA TO15ND 1.00NDCarbon Disulfide 0.321 04/15/14 KCA TO15ND 1.000.08Carbon Tetrachloride 0.040 04/15/14 KCA TO150.503 0.25NDChlorobenzene 0.217 04/15/14 KCA TO15ND 1.00NDChloroethane 0.379 04/15/14 KCA TO15ND 1.00NDChloroform 0.205 04/15/14 KCA TO15ND 1.00NDChloromethane 0.484 04/15/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.000.97Cyclohexane 0.291 04/15/14 KCA TO153.34 1.00NDDibromochloromethane 0.117 04/15/14 KCA TO15ND 1.000.52Dichlorodifluoromethane 0.202 04/15/14 KCA TO152.57 1.0027.8Ethanol 0.531 04/15/14 KCA TO1552.3 11.003.42Ethyl acetate 0.278 04/15/14 KCA TO1512.3 11.003.6Ethylbenzene 0.230 04/15/14 KCA TO1515.6 1.00
2.26Heptane 0.244 04/15/14 KCA TO159.26 1.00NDHexachlorobutadiene 0.094 04/15/14 KCA TO15ND 1.001.67Hexane 0.284 04/15/14 KCA TO155.88 1.001.21Isopropylalcohol 0.407 04/15/14 KCA TO152.97 1.000.37Isopropylbenzene 0.204 04/15/14 KCA TO151.82 1.0012.8m,p-Xylene 0.230 04/15/14 KCA TO1555.5 1.008.1Methyl Ethyl Ketone 0.339 04/15/14 KCA TO1523.9 1.00NDMethyl tert-butyl ether(MTBE) 0.278 04/15/14 KCA TO15ND 1.000.36Methylene Chloride 0.288 04/15/14 KCA TO151.25 1.000.5n-Butylbenzene 0.182 04/15/14 KCA TO152.74 11.00
5.32o-Xylene 0.230 04/15/14 KCA TO1523.1 1.001.3Propylene 0.581 04/15/14 KCA TO152.24 11.00NDsec-Butylbenzene 0.182 04/15/14 KCA TO15ND 11.000.24Styrene 0.235 04/15/14 KCA TO151.02 1.000.42Tetrachloroethene 0.037 04/15/14 KCA TO152.85 0.25NDTetrahydrofuran 0.339 04/15/14 KCA TO15ND 11.0011.1Toluene 0.266 04/15/14 KCA TO1541.8 1.00NDTrans-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.00NDTrichloroethene 0.047 04/15/14 KCA TO15ND 0.250.22Trichlorofluoromethane 0.178 04/15/14 KCA TO151.24 1.00NDTrichlorotrifluoroethane 0.130 04/15/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 04/15/14 KCA TO15ND 0.25
QA/QC Surrogates104% Bromofluorobenzene % 04/15/14 KCA TO15104 %
Page 2 of 12 Ver 1
E-SG2Phoenix I.D.: BG31847
Client ID:DOMINO SUGAR SITE EProject ID:
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
ug/m3RL
Comments:
Phyllis Shiller, Laboratory DirectorApril 18, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level
Page 3 of 12 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
AIREBC72 Hour
04/09/14SWsee "By" below
DM
Laboratory Data
E-SG3
Phoenix ID: BG31848
04/11/1410:4317:36
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 18, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG31847
Client ID:Project ID: DOMINO SUGAR SITE E
ug/m3RL
Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 11.000.651,1,1-Trichloroethane 0.183 04/15/14 KCA TO153.54 1.00ND1,1,2,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 04/15/14 KCA TO15ND 1.004.981,2,4-Trimethylbenzene 0.204 04/15/14 KCA TO1524.5 1.00ND1,2-Dibromoethane(EDB) 0.130 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 04/15/14 KCA TO15ND 1.001.381,3,5-Trimethylbenzene 0.204 04/15/14 KCA TO156.78 1.00ND1,3-Butadiene 0.452 04/15/14 KCA TO15ND 1.000.31,3-Dichlorobenzene 0.166 04/15/14 KCA TO151.80 1.00ND1,4-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 04/15/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 04/15/14 KCA TO15ND 11.001.114-Ethyltoluene 0.204 04/15/14 KCA TO155.45 11.000.234-Isopropyltoluene 0.182 04/15/14 KCA TO151.26 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 04/15/14 KCA TO15ND 1.00324Acetone 0.421 04/15/14 KCA TO15769 1.00NDAcrylonitrile 0.461 04/15/14 KCA TO15ND 1.002.2Benzene 0.313 04/15/14 KCA TO157.02 1.00NDBenzyl chloride 0.193 04/15/14 KCA TO15ND 1.00
Page 4 of 12 Ver 1
E-SG3Phoenix I.D.: BG31848
Client ID:DOMINO SUGAR SITE EProject ID:
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
ug/m3RL
NDBromodichloromethane 0.149 04/15/14 KCA TO15ND 1.00NDBromoform 0.097 04/15/14 KCA TO15ND 1.00NDBromomethane 0.258 04/15/14 KCA TO15ND 1.00NDCarbon Disulfide 0.321 04/15/14 KCA TO15ND 1.00NDCarbon Tetrachloride 0.040 04/15/14 KCA TO15ND 0.25NDChlorobenzene 0.217 04/15/14 KCA TO15ND 1.00NDChloroethane 0.379 04/15/14 KCA TO15ND 1.001.77Chloroform 0.205 04/15/14 KCA TO158.64 1.00NDChloromethane 0.484 04/15/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.001.37Cyclohexane 0.291 04/15/14 KCA TO154.71 1.00NDDibromochloromethane 0.117 04/15/14 KCA TO15ND 1.000.48Dichlorodifluoromethane 0.202 04/15/14 KCA TO152.37 1.0030.8Ethanol 0.531 04/15/14 KCA TO1558.0 11.006.13Ethyl acetate 0.278 04/15/14 KCA TO1522.1 11.002.72Ethylbenzene 0.230 04/15/14 KCA TO1511.8 1.004.23Heptane 0.244 04/15/14 KCA TO1517.3 1.00NDHexachlorobutadiene 0.094 04/15/14 KCA TO15ND 1.003.8Hexane 0.284 04/15/14 KCA TO1513.4 1.00
1.84Isopropylalcohol 0.407 04/15/14 KCA TO154.52 1.000.26Isopropylbenzene 0.204 04/15/14 KCA TO151.28 1.009.8m,p-Xylene 0.230 04/15/14 KCA TO1542.5 1.00
14.2Methyl Ethyl Ketone 0.339 04/15/14 KCA TO1541.8 1.00NDMethyl tert-butyl ether(MTBE) 0.278 04/15/14 KCA TO15ND 1.00NDMethylene Chloride 0.288 04/15/14 KCA TO15ND 1.000.49n-Butylbenzene 0.182 04/15/14 KCA TO152.69 11.003.55o-Xylene 0.230 04/15/14 KCA TO1515.4 1.0013.8Propylene 0.581 04/15/14 KCA TO1523.7 11.00NDsec-Butylbenzene 0.182 04/15/14 KCA TO15ND 11.000.33Styrene 0.235 04/15/14 KCA TO151.40 1.000.97Tetrachloroethene 0.037 04/15/14 KCA TO156.57 0.25NDTetrahydrofuran 0.339 04/15/14 KCA TO15ND 11.0013.3Toluene 0.266 04/15/14 KCA TO1550.1 1.00NDTrans-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.0011.4Trichloroethene 0.047 04/15/14 KCA TO1561.2 0.250.23Trichlorofluoromethane 0.178 04/15/14 KCA TO151.29 1.00NDTrichlorotrifluoroethane 0.130 04/15/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 04/15/14 KCA TO15ND 0.25
QA/QC Surrogates96% Bromofluorobenzene % 04/15/14 KCA TO1596 %
Page 5 of 12 Ver 1
E-SG3Phoenix I.D.: BG31848
Client ID:DOMINO SUGAR SITE EProject ID:
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
ug/m3RL
Comments:
Phyllis Shiller, Laboratory DirectorApril 18, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level
Page 6 of 12 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
AIREBC72 Hour
04/09/14SWsee "By" below
DM
Laboratory Data
E-SG4
Phoenix ID: BG31849
04/11/1410:4617:36
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 18, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG31847
Client ID:Project ID: DOMINO SUGAR SITE E
ug/m3RL
Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 11.00ND1,1,1-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1,2,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 04/15/14 KCA TO15ND 1.004.941,2,4-Trimethylbenzene 0.204 04/15/14 KCA TO1524.3 1.00ND1,2-Dibromoethane(EDB) 0.130 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 04/15/14 KCA TO15ND 1.001.341,3,5-Trimethylbenzene 0.204 04/15/14 KCA TO156.58 1.00ND1,3-Butadiene 0.452 04/15/14 KCA TO15ND 1.000.461,3-Dichlorobenzene 0.166 04/15/14 KCA TO152.76 1.00ND1,4-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 04/15/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 04/15/14 KCA TO15ND 11.001.224-Ethyltoluene 0.204 04/15/14 KCA TO155.99 11.00ND4-Isopropyltoluene 0.182 04/15/14 KCA TO15ND 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 04/15/14 KCA TO15ND 1.00113Acetone 0.421 04/15/14 KCA TO15268 1.00NDAcrylonitrile 0.461 04/15/14 KCA TO15ND 1.001.09Benzene 0.313 04/15/14 KCA TO153.48 1.00NDBenzyl chloride 0.193 04/15/14 KCA TO15ND 1.00
Page 7 of 12 Ver 1
E-SG4Phoenix I.D.: BG31849
Client ID:DOMINO SUGAR SITE EProject ID:
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
ug/m3RL
NDBromodichloromethane 0.149 04/15/14 KCA TO15ND 1.00NDBromoform 0.097 04/15/14 KCA TO15ND 1.00NDBromomethane 0.258 04/15/14 KCA TO15ND 1.00NDCarbon Disulfide 0.321 04/15/14 KCA TO15ND 1.000.09Carbon Tetrachloride 0.040 04/15/14 KCA TO150.566 0.25NDChlorobenzene 0.217 04/15/14 KCA TO15ND 1.00NDChloroethane 0.379 04/15/14 KCA TO15ND 1.00NDChloroform 0.205 04/15/14 KCA TO15ND 1.00NDChloromethane 0.484 04/15/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.001.01Cyclohexane 0.291 04/15/14 KCA TO153.47 1.00NDDibromochloromethane 0.117 04/15/14 KCA TO15ND 1.000.59Dichlorodifluoromethane 0.202 04/15/14 KCA TO152.92 1.0026.2Ethanol 0.531 04/15/14 KCA TO1549.3 11.002.5Ethyl acetate 0.278 04/15/14 KCA TO159.00 11.00
3.08Ethylbenzene 0.230 04/15/14 KCA TO1513.4 1.001.76Heptane 0.244 04/15/14 KCA TO157.21 1.00NDHexachlorobutadiene 0.094 04/15/14 KCA TO15ND 1.001.45Hexane 0.284 04/15/14 KCA TO155.11 1.001.97Isopropylalcohol 0.407 04/15/14 KCA TO154.84 1.000.27Isopropylbenzene 0.204 04/15/14 KCA TO151.33 1.0010.8m,p-Xylene 0.230 04/15/14 KCA TO1546.9 1.006.23Methyl Ethyl Ketone 0.339 04/15/14 KCA TO1518.4 1.00NDMethyl tert-butyl ether(MTBE) 0.278 04/15/14 KCA TO15ND 1.000.41Methylene Chloride 0.288 04/15/14 KCA TO151.42 1.000.39n-Butylbenzene 0.182 04/15/14 KCA TO152.14 11.004.23o-Xylene 0.230 04/15/14 KCA TO1518.4 1.001.18Propylene 0.581 04/15/14 KCA TO152.03 11.00NDsec-Butylbenzene 0.182 04/15/14 KCA TO15ND 11.000.24Styrene 0.235 04/15/14 KCA TO151.02 1.000.48Tetrachloroethene 0.037 04/15/14 KCA TO153.25 0.25NDTetrahydrofuran 0.339 04/15/14 KCA TO15ND 11.009.76Toluene 0.266 04/15/14 KCA TO1536.8 1.00NDTrans-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.00NDTrichloroethene 0.047 04/15/14 KCA TO15ND 0.250.27Trichlorofluoromethane 0.178 04/15/14 KCA TO151.52 1.00NDTrichlorotrifluoroethane 0.130 04/15/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 04/15/14 KCA TO15ND 0.25
QA/QC Surrogates104% Bromofluorobenzene % 04/15/14 KCA TO15104 %
Page 8 of 12 Ver 1
E-SG4Phoenix I.D.: BG31849
Client ID:DOMINO SUGAR SITE EProject ID:
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
ug/m3RL
Comments:
Phyllis Shiller, Laboratory DirectorApril 18, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level
Page 9 of 12 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
AIREBC72 Hour
04/09/14SWsee "By" below
DM
Laboratory Data
E-SG5
Phoenix ID: BG31850
04/11/1410:2517:36
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 18, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG31847
Client ID:Project ID: DOMINO SUGAR SITE E
ug/m3RL
Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 11.000.231,1,1-Trichloroethane 0.183 04/15/14 KCA TO151.25 1.00ND1,1,2,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 04/15/14 KCA TO15ND 1.003.631,2,4-Trimethylbenzene 0.204 04/15/14 KCA TO1517.8 1.00ND1,2-Dibromoethane(EDB) 0.130 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 04/15/14 KCA TO15ND 1.001.281,3,5-Trimethylbenzene 0.204 04/15/14 KCA TO156.29 1.00ND1,3-Butadiene 0.452 04/15/14 KCA TO15ND 1.0011,3-Dichlorobenzene 0.166 04/15/14 KCA TO156.01 1.00
ND1,4-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 04/15/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 04/15/14 KCA TO15ND 11.000.964-Ethyltoluene 0.204 04/15/14 KCA TO154.72 11.00ND4-Isopropyltoluene 0.182 04/15/14 KCA TO15ND 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 04/15/14 KCA TO15ND 1.00257Acetone 0.421 04/15/14 KCA TO15610 1.00NDAcrylonitrile 0.461 04/15/14 KCA TO15ND 1.001.92Benzene 0.313 04/15/14 KCA TO156.13 1.00NDBenzyl chloride 0.193 04/15/14 KCA TO15ND 1.00
Page 10 of 12 Ver 1
E-SG5Phoenix I.D.: BG31850
Client ID:DOMINO SUGAR SITE EProject ID:
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
ug/m3RL
NDBromodichloromethane 0.149 04/15/14 KCA TO15ND 1.00NDBromoform 0.097 04/15/14 KCA TO15ND 1.00NDBromomethane 0.258 04/15/14 KCA TO15ND 1.001.81Carbon Disulfide 0.321 04/15/14 KCA TO155.63 1.00NDCarbon Tetrachloride 0.040 04/15/14 KCA TO15ND 0.25NDChlorobenzene 0.217 04/15/14 KCA TO15ND 1.00NDChloroethane 0.379 04/15/14 KCA TO15ND 1.000.38Chloroform 0.205 04/15/14 KCA TO151.85 1.00NDChloromethane 0.484 04/15/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.001.64Cyclohexane 0.291 04/15/14 KCA TO155.64 1.00NDDibromochloromethane 0.117 04/15/14 KCA TO15ND 1.000.5Dichlorodifluoromethane 0.202 04/15/14 KCA TO152.47 1.00
30.2Ethanol 0.531 04/15/14 KCA TO1556.9 11.004.12Ethyl acetate 0.278 04/15/14 KCA TO1514.8 11.003.25Ethylbenzene 0.230 04/15/14 KCA TO1514.1 1.004.7Heptane 0.244 04/15/14 KCA TO1519.2 1.00NDHexachlorobutadiene 0.094 04/15/14 KCA TO15ND 1.005.25Hexane 0.284 04/15/14 KCA TO1518.5 1.001.57Isopropylalcohol 0.407 04/15/14 KCA TO153.86 1.000.26Isopropylbenzene 0.204 04/15/14 KCA TO151.28 1.0011.1m,p-Xylene 0.230 04/15/14 KCA TO1548.2 1.0010.6Methyl Ethyl Ketone 0.339 04/15/14 KCA TO1531.2 1.00NDMethyl tert-butyl ether(MTBE) 0.278 04/15/14 KCA TO15ND 1.000.33Methylene Chloride 0.288 04/15/14 KCA TO151.14 1.000.47n-Butylbenzene 0.182 04/15/14 KCA TO152.58 11.003.9o-Xylene 0.230 04/15/14 KCA TO1516.9 1.00
29.6Propylene 0.581 04/15/14 KCA TO1550.9 11.00NDsec-Butylbenzene 0.182 04/15/14 KCA TO15ND 11.000.36Styrene 0.235 04/15/14 KCA TO151.53 1.004.18Tetrachloroethene 0.037 04/15/14 KCA TO1528.3 0.25NDTetrahydrofuran 0.339 04/15/14 KCA TO15ND 11.0014.9Toluene 0.266 04/15/14 KCA TO1556.1 1.00NDTrans-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.0010.2Trichloroethene 0.047 04/15/14 KCA TO1554.8 0.250.24Trichlorofluoromethane 0.178 04/15/14 KCA TO151.35 1.00NDTrichlorotrifluoroethane 0.130 04/15/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 04/15/14 KCA TO15ND 0.25
QA/QC Surrogates101% Bromofluorobenzene % 04/15/14 KCA TO15101 %
Page 11 of 12 Ver 1
E-SG5Phoenix I.D.: BG31850
Client ID:DOMINO SUGAR SITE EProject ID:
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
ug/m3RL
Comments:
Phyllis Shiller, Laboratory DirectorApril 18, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level
Page 12 of 12 Ver 1
QA/QC Data
ParameterBlankppbv
SampleResultppbv
SampleDupppbv
DUPRPD
QA/QC ReportApril 18, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG31847
LCS%
SampleResultug/m3
SampleDup
ug/m3
%Rec
Limits
%RPD
LimitsBlankug/m3
QA/QC Batch 271636, QC Sample No: BG32377 (BG31847, BG31848, BG31849, BG31850)
VolatilesND ND1,1,1,2-Tetrachloroethane ND NC121 ND ND 70 - 130 20ND
ND ND1,1,1-Trichloroethane ND NC109 ND ND 70 - 130 20ND
ND ND1,1,2,2-Tetrachloroethane ND NC107 ND ND 70 - 130 20ND
ND ND1,1,2-Trichloroethane ND NC110 ND ND 70 - 130 20ND
ND ND1,1-Dichloroethane ND NC98 ND ND 70 - 130 20ND
ND ND1,1-Dichloroethene ND NC96 ND ND 70 - 130 20ND
ND ND1,2,4-Trichlorobenzene ND NC111 ND ND 70 - 130 20ND
1.03 11,2,4-Trimethylbenzene ND 3.0107 5.06 4.91 70 - 130 20ND
ND ND1,2-Dibromoethane(EDB) ND NC113 ND ND 70 - 130 20ND
ND ND1,2-Dichlorobenzene ND NC108 ND ND 70 - 130 20ND
ND ND1,2-Dichloroethane ND NC104 ND ND 70 - 130 20ND
ND ND1,2-dichloropropane ND NC109 ND ND 70 - 130 20ND
ND ND1,2-Dichlorotetrafluoroethane ND NC117 ND ND 70 - 130 20ND
ND ND1,3,5-Trimethylbenzene ND NC104 ND ND 70 - 130 20ND
ND ND1,3-Butadiene ND NC102 ND ND 70 - 130 20ND
1.09 1.191,3-Dichlorobenzene ND 8.8109 6.55 7.15 70 - 130 20ND
ND ND1,4-Dichlorobenzene ND NC114 ND ND 70 - 130 20ND
ND ND1,4-Dioxane ND NC115 ND ND 70 - 130 20ND
ND ND2-Hexanone(MBK) ND NC114 ND ND 70 - 130 20ND
ND ND4-Ethyltoluene ND NC106 ND ND 70 - 130 20ND
ND ND4-Isopropyltoluene ND NC107 ND ND 70 - 130 20ND
ND ND4-Methyl-2-pentanone(MIBK) ND NC119 ND ND 70 - 130 20ND
49.3 58Acetone ND 16.299 117 138 70 - 130 20ND
ND NDAcrylonitrile ND NC105 ND ND 70 - 130 20ND
4.78 5.61Benzene ND 16.0108 15.3 17.9 70 - 130 20ND
ND NDBenzyl chloride ND NC136 ND ND l70 - 130 20ND
ND NDBromodichloromethane ND NC112 ND ND 70 - 130 20ND
ND NDBromoform ND NC126 ND ND 70 - 130 20ND
ND NDBromomethane ND NC100 ND ND 70 - 130 20ND
5.7 6.61Carbon Disulfide ND 14.8100 17.7 20.6 70 - 130 20ND
0.52 0.58Carbon Tetrachloride ND 10.9114 3.27 3.65 70 - 130 20ND
ND NDChlorobenzene ND NC104 ND ND 70 - 130 20ND
ND NDChloroethane ND NC100 ND ND 70 - 130 20ND
ND NDChloroform ND NC100 ND ND 70 - 130 20ND
0.49 0.59Chloromethane ND 18.5102 1.01 1.22 70 - 130 20ND
ND NDCis-1,2-Dichloroethene ND NC86 ND ND 70 - 130 20ND
ND NDcis-1,3-Dichloropropene ND NC113 ND ND 70 - 130 20ND
1.92 2.22Cyclohexane ND 14.5109 6.60 7.64 70 - 130 20ND
ND NDDibromochloromethane ND NC119 ND ND 70 - 130 20ND
0.66 0.64Dichlorodifluoromethane ND 3.1108 3.26 3.16 70 - 130 20ND
33.1 38.1Ethanol ND 14.0102 62.3 71.7 70 - 130 20ND
Page 1 of 2
QA/QC Data
ParameterBlankppbv
SampleResultppbv
SampleDupppbv
DUPRPD
SDG I.D.: GBG31847
LCS%
SampleResultug/m3
SampleDup
ug/m3
%Rec
Limits
%RPD
LimitsBlankug/m3
1.4 1.31Ethyl acetate ND 6.6113 5.04 4.72 70 - 130 20ND
0.98 0.91Ethylbenzene ND 7.4107 4.25 3.95 70 - 130 20ND
4.87 4.98Heptane ND 2.2104 19.9 20.4 70 - 130 20ND
ND NDHexachlorobutadiene ND NC89 ND ND 70 - 130 20ND
13.1 12.8Hexane ND 2.3103 46.1 45.1 70 - 130 20ND
1.88 2.17Isopropylalcohol ND 14.3110 4.62 5.33 70 - 130 20ND
ND NDIsopropylbenzene ND NC109 ND ND 70 - 130 20ND
4.05 3.79m,p-Xylene ND 6.6109 17.6 16.4 70 - 130 20ND
7.87 9.32Methyl Ethyl Ketone ND 16.996 23.2 27.5 70 - 130 20ND
ND NDMethyl tert-butyl ether(MTBE) ND NC102 ND ND 70 - 130 20ND
ND NDMethylene Chloride ND NC87 ND ND 70 - 130 20ND
ND NDn-Butylbenzene ND NC113 ND ND 70 - 130 20ND
1.48 1.36o-Xylene ND 8.5106 6.42 5.90 70 - 130 20ND
36.2 45.8Propylene ND 23.4111 62.3 78.8 70 - 130 20ND
ND NDsec-Butylbenzene ND NC106 ND ND 70 - 130 20ND
ND NDStyrene ND NC113 ND ND 70 - 130 20ND
0.62 0.63Tetrachloroethene ND 1.6110 4.20 4.27 70 - 130 20ND
3.96 4.61Tetrahydrofuran ND 15.2115 11.7 13.6 70 - 130 20ND
3.83 4.05Toluene ND 5.6110 14.4 15.2 70 - 130 20ND
ND NDTrans-1,2-Dichloroethene ND NC100 ND ND 70 - 130 20ND
ND NDtrans-1,3-Dichloropropene ND NC120 ND ND 70 - 130 20ND
ND NDTrichloroethene ND NC106 ND ND 70 - 130 20ND
2.47 2.83Trichlorofluoromethane ND 13.6102 13.9 15.9 70 - 130 20ND
ND NDTrichlorotrifluoroethane ND NC96 ND ND 70 - 130 20ND
ND NDVinyl Chloride ND NC100 ND ND 70 - 130 20ND
108 109% Bromofluorobenzene 101 0.9102 108 109 70 - 130 20101
l = This parameter is outside laboratory lcs/lcsd specified recovery limits.
MS - Matrix SpikePhyllis Shiller, Laboratory Director
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.
April 18, 2014MS Dup - Matrix Spike Duplicate
RPD - Relative Percent DifferenceLCS - Laboratory Control Sample
LCSD - Laboratory Control Sample Duplicate
NC - No CriteriaIntf - Interference
Page 2 of 2
Sample Criteria Exceedences ReportFriday, April 18, 2014 Page 1 of 1
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG31847 - EBCCriteria: None
RLCriteria
State: NY
#Error*** No Data to Display ***
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
BG29068 - BG29075
Tuesday, April 15, 2014
Sample ID#s:
Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Project ID: DOMINO SUGAR SITE
Sincerely yours,
Laboratory DirectorPhyllis Shiller
If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.
NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B
NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823
SDG CommentsApril 15, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG29068
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
E-SB2 0-2
Phoenix ID: BG29068
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 15, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG29068
Client ID:Project ID: DOMINO SUGAR SITE
LOD/MDL
< 0.39Silver 0.39 04/09/14 LK SW6010mg/Kg0.237520Aluminum 39 04/08/14 LK SW6010mg/Kg7.75.7Arsenic 0.8 04/09/14 LK SW6010mg/Kg0.77
84.4Barium 0.8 04/09/14 LK SW6010mg/Kg0.150.35Beryllium 0.31 04/09/14 LK SW6010mg/Kg0.15
36500Calcium 39 04/08/14 LK SW6010mg/Kg36< 0.39Cadmium 0.39 04/09/14 LK SW6010mg/Kg0.154.01Cobalt 0.39 04/09/14 LK SW6010mg/Kg0.1513.3Chromium 0.39 04/09/14 LK SW6010mg/Kg0.15153Copper 3.9 04/08/14 LK SW6010mg/kg3.1
14000Iron 39 04/08/14 LK SW6010mg/Kg B390.14Mercury 0.09 04/08/14 RS SW-7471mg/Kg0.051140Potassium 8 04/09/14 LK SW6010mg/Kg3.03460Magnesium 3.9 04/09/14 LK SW6010mg/Kg0.23173Manganese 3.9 04/08/14 LK SW6010mg/Kg1.5543Sodium 8 04/09/14 LK SW6010mg/Kg B3.315.2Nickel 0.39 04/09/14 LK SW6010mg/Kg0.15167Lead 7.7 04/08/14 LK SW6010mg/Kg2.3
< 1.9Antimony 1.9 04/09/14 LK SW6010mg/Kg0.77< 1.5Selenium 1.5 04/09/14 LK SW6010mg/Kg1.3< 1.5Thallium 1.5 04/09/14 LK SW6010mg/Kg1.528.3Vanadium 0.4 04/09/14 LK SW6010mg/Kg0.1587.1Zinc 0.8 04/10/14 LK SW6010mg/Kg0.3985Percent Solid 04/07/14 I E160.3%
CompletedSoil Extraction for PCB 04/07/14 BB/V SW3545CompletedSoil Extraction for Pesticide 04/07/14 BB SW3545CompletedSoil Extraction for SVOA 04/07/14 BB/FV SW3545CompletedMercury Digestion 04/08/14 I/I SW7471
Page 1 of 40 Ver 1
E-SB2 0-2Phoenix I.D.: BG29068
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
CompletedTotal Metals Digest 04/07/14 CB/AG/D SW846 - 3050
CompletedField Extraction 04/02/14 SW5035
Polychlorinated BiphenylsNDPCB-1016 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1221 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1232 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1242 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1248 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1254 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1260 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1262 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1268 38 04/08/14 AW SW 8082ug/Kg38
QA/QC Surrogates113% DCBP 04/08/14 AW 30 - 150 %%88% TCMX 04/08/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.8 04/09/14 CE SW8081ug/Kg2.8ND4,4' -DDE 2.8 04/09/14 CE SW8081ug/Kg2.8ND4,4' -DDT 2.8 04/09/14 CE SW8081ug/Kg2.8NDa-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDa-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDAldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDb-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDChlordane 23 04/09/14 CE SW8081ug/Kg23NDd-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDDieldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndosulfan I 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan II 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan sulfate 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndrin aldehyde 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin ketone 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDHeptachlor 1.9 04/09/14 CE SW8081ug/Kg1.9NDHeptachlor epoxide 1.9 04/09/14 CE SW8081ug/Kg1.9NDMethoxychlor 92 04/09/14 CE SW8081ug/Kg92NDToxaphene 190 04/09/14 CE SW8081ug/Kg190
QA/QC SurrogatesInterference% DCBP 04/09/14 CE 30 - 150 %%
78% TCMX 04/09/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 8.2 04/10/14 JLI SW8260ug/Kg1.4ND1,1,1-Trichloroethane 8.2 04/10/14 JLI SW8260ug/Kg1.6ND1,1,2,2-Tetrachloroethane 8.2 04/10/14 JLI SW8260ug/Kg1.2ND1,1,2-Trichloroethane 8.2 04/10/14 JLI SW8260ug/Kg0.81ND1,1-Dichloroethane 8.2 04/10/14 JLI SW8260ug/Kg1.6
Page 2 of 40 Ver 1
E-SB2 0-2Phoenix I.D.: BG29068
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 8.2 04/10/14 JLI SW8260ug/Kg1.8ND1,1-Dichloropropene 8.2 04/10/14 JLI SW8260ug/Kg1.6ND1,2,3-Trichlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.6ND1,2,3-Trichloropropane 8.2 04/10/14 JLI SW8260ug/Kg1.2ND1,2,4-Trichlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.6ND1,2,4-Trimethylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.2ND1,2-Dibromo-3-chloropropane 8.2 04/10/14 JLI SW8260ug/Kg2.2ND1,2-Dibromoethane 8.2 04/10/14 JLI SW8260ug/Kg2.2ND1,2-Dichlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg0.91ND1,2-Dichloroethane 8.2 04/10/14 JLI SW8260ug/Kg0.72ND1,2-Dichloropropane 8.2 04/10/14 JLI SW8260ug/Kg1.2ND1,3,5-Trimethylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.1ND1,3-Dichlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.2ND1,3-Dichloropropane 8.2 04/10/14 JLI SW8260ug/Kg0.87ND1,4-Dichlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.3ND2,2-Dichloropropane 8.2 04/10/14 JLI SW8260ug/Kg1.4ND2-Chlorotoluene 8.2 04/10/14 JLI SW8260ug/Kg1.3ND2-Hexanone 41 04/10/14 JLI SW8260ug/Kg3.7ND2-Isopropyltoluene 8.2 04/10/14 JLI SW8260ug/Kg 11.1ND4-Chlorotoluene 8.2 04/10/14 JLI SW8260ug/Kg0.96ND4-Methyl-2-pentanone 41 04/10/14 JLI SW8260ug/Kg2.0NDAcetone 50 04/10/14 JLI SW8260ug/Kg8.2NDAcrylonitrile 16 04/10/14 JLI SW8260ug/Kg4.6NDBenzene 8.2 04/10/14 JLI SW8260ug/Kg1.6NDBromobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.1NDBromochloromethane 8.2 04/10/14 JLI SW8260ug/Kg1.2NDBromodichloromethane 8.2 04/10/14 JLI SW8260ug/Kg1.0NDBromoform 8.2 04/10/14 JLI SW8260ug/Kg1.2NDBromomethane 8.2 04/10/14 JLI SW8260ug/Kg6.3NDCarbon Disulfide 8.2 04/10/14 JLI SW8260ug/Kg1.3NDCarbon tetrachloride 8.2 04/10/14 JLI SW8260ug/Kg0.96NDChlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.2NDChloroethane 8.2 04/10/14 JLI SW8260ug/Kg1.9NDChloroform 8.2 04/10/14 JLI SW8260ug/Kg1.5NDChloromethane 8.2 04/10/14 JLI SW8260ug/Kg4.3NDcis-1,2-Dichloroethene 8.2 04/10/14 JLI SW8260ug/Kg1.8NDcis-1,3-Dichloropropene 8.2 04/10/14 JLI SW8260ug/Kg0.89NDDibromochloromethane 8.2 04/10/14 JLI SW8260ug/Kg0.92NDDibromomethane 8.2 04/10/14 JLI SW8260ug/Kg1.0NDDichlorodifluoromethane 8.2 04/10/14 JLI SW8260ug/Kg2.2NDEthylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.5NDHexachlorobutadiene 8.2 04/10/14 JLI SW8260ug/Kg1.7NDIsopropylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.6NDm&p-Xylene 8.2 04/10/14 JLI SW8260ug/Kg3.2NDMethyl Ethyl Ketone 49 04/10/14 JLI SW8260ug/Kg7.1NDMethyl t-butyl ether (MTBE) 16 04/10/14 JLI SW8260ug/Kg2.3NDMethylene chloride 8.2 04/10/14 JLI SW8260ug/Kg1.4430Naphthalene 310 04/11/14 JLI SW8260ug/Kg82NDn-Butylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.5
Page 3 of 40 Ver 1
E-SB2 0-2Phoenix I.D.: BG29068
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.5NDo-Xylene 8.2 04/10/14 JLI SW8260ug/Kg3.1NDp-Isopropyltoluene 8.2 04/10/14 JLI SW8260ug/Kg1.2NDsec-Butylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.5NDStyrene 8.2 04/10/14 JLI SW8260ug/Kg2.4NDtert-Butylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.3NDTetrachloroethene 8.2 04/10/14 JLI SW8260ug/Kg1.7NDTetrahydrofuran (THF) 16 04/10/14 JLI SW8260ug/Kg 17.4NDToluene 8.2 04/10/14 JLI SW8260ug/Kg1.3NDtrans-1,2-Dichloroethene 8.2 04/10/14 JLI SW8260ug/Kg1.6NDtrans-1,3-Dichloropropene 8.2 04/10/14 JLI SW8260ug/Kg1.7NDtrans-1,4-dichloro-2-butene 16 04/10/14 JLI SW8260ug/Kg15NDTrichloroethene 8.2 04/10/14 JLI SW8260ug/Kg1.7NDTrichlorofluoromethane 8.2 04/10/14 JLI SW8260ug/Kg1.8NDTrichlorotrifluoroethane 8.2 04/10/14 JLI SW8260ug/Kg1.3NDVinyl chloride 8.2 04/10/14 JLI SW8260ug/Kg2.7
QA/QC Surrogates111% 1,2-dichlorobenzene-d4 04/10/14 JLI 70 - 130 %%86% Bromofluorobenzene 04/10/14 JLI 70 - 130 %%98% Dibromofluoromethane 04/10/14 JLI 70 - 130 %%102% Toluene-d8 04/10/14 JLI 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 540 04/08/14 DD SW 8270ug/Kg270ND1,2,4-Trichlorobenzene 540 04/08/14 DD SW 8270ug/Kg230ND1,2-Dichlorobenzene 540 04/08/14 DD SW 8270ug/Kg220ND1,2-Diphenylhydrazine 540 04/08/14 DD SW 8270ug/Kg250ND1,3-Dichlorobenzene 540 04/08/14 DD SW 8270ug/Kg230ND1,4-Dichlorobenzene 540 04/08/14 DD SW 8270ug/Kg230ND2,4,5-Trichlorophenol 540 04/08/14 DD SW 8270ug/Kg430ND2,4,6-Trichlorophenol 540 04/08/14 DD SW 8270ug/Kg250ND2,4-Dichlorophenol 540 04/08/14 DD SW 8270ug/Kg270ND2,4-Dimethylphenol 540 04/08/14 DD SW 8270ug/Kg190ND2,4-Dinitrophenol 3900 04/08/14 DD SW 8270ug/Kg540ND2,4-Dinitrotoluene 540 04/08/14 DD SW 8270ug/Kg310ND2,6-Dinitrotoluene 540 04/08/14 DD SW 8270ug/Kg250ND2-Chloronaphthalene 540 04/08/14 DD SW 8270ug/Kg220ND2-Chlorophenol 540 04/08/14 DD SW 8270ug/Kg2205502-Methylnaphthalene 540 04/08/14 DD SW 8270ug/Kg230ND2-Methylphenol (o-cresol) 540 04/08/14 DD SW 8270ug/Kg360ND2-Nitroaniline 3900 04/08/14 DD SW 8270ug/Kg780ND2-Nitrophenol 540 04/08/14 DD SW 8270ug/Kg490ND3&4-Methylphenol (m&p-cresol) 540 04/08/14 DD SW 8270ug/Kg 1310ND3,3'-Dichlorobenzidine 1600 04/08/14 DD SW 8270ug/Kg370ND3-Nitroaniline 3900 04/08/14 DD SW 8270ug/Kg1700ND4,6-Dinitro-2-methylphenol 3900 04/08/14 DD SW 8270ug/Kg840ND4-Bromophenyl phenyl ether 540 04/08/14 DD SW 8270ug/Kg230ND4-Chloro-3-methylphenol 540 04/08/14 DD SW 8270ug/Kg270ND4-Chloroaniline 1600 04/08/14 DD SW 8270ug/Kg360ND4-Chlorophenyl phenyl ether 540 04/08/14 DD SW 8270ug/Kg260
Page 4 of 40 Ver 1
E-SB2 0-2Phoenix I.D.: BG29068
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Nitroaniline 3900 04/08/14 DD SW 8270ug/Kg260ND4-Nitrophenol 3900 04/08/14 DD SW 8270ug/Kg350
1100Acenaphthene 540 04/08/14 DD SW 8270ug/Kg240NDAcenaphthylene 540 04/08/14 DD SW 8270ug/Kg220NDAcetophenone 540 04/08/14 DD SW 8270ug/Kg240NDAniline 3900 04/08/14 DD SW 8270ug/Kg1600
2800Anthracene 540 04/08/14 DD SW 8270ug/Kg2504800Benz(a)anthracene 540 04/08/14 DD SW 8270ug/Kg260NDBenzidine 1600 04/08/14 DD SW 8270ug/Kg460
3700Benzo(a)pyrene 540 04/08/14 DD SW 8270ug/Kg2505000Benzo(b)fluoranthene 540 04/08/14 DD SW 8270ug/Kg2701500Benzo(ghi)perylene 540 04/08/14 DD SW 8270ug/Kg2501500Benzo(k)fluoranthene 540 04/08/14 DD SW 8270ug/Kg260NDBenzoic acid 3900 04/08/14 DD SW 8270ug/Kg 11600NDBenzyl butyl phthalate 540 04/08/14 DD SW 8270ug/Kg200NDBis(2-chloroethoxy)methane 540 04/08/14 DD SW 8270ug/Kg210NDBis(2-chloroethyl)ether 540 04/08/14 DD SW 8270ug/Kg210NDBis(2-chloroisopropyl)ether 540 04/08/14 DD SW 8270ug/Kg 1220NDBis(2-ethylhexyl)phthalate 540 04/08/14 DD SW 8270ug/Kg220
1000Carbazole 3900 04/08/14 DD SW 8270ug/Kg590J4200Chrysene 540 04/08/14 DD SW 8270ug/Kg260NDDibenz(a,h)anthracene 540 04/08/14 DD SW 8270ug/Kg250
1200Dibenzofuran 540 04/08/14 DD SW 8270ug/Kg230NDDiethyl phthalate 540 04/08/14 DD SW 8270ug/Kg250NDDimethylphthalate 540 04/08/14 DD SW 8270ug/Kg240NDDi-n-butylphthalate 540 04/08/14 DD SW 8270ug/Kg210NDDi-n-octylphthalate 540 04/08/14 DD SW 8270ug/Kg200
9900Fluoranthene 540 04/08/14 DD SW 8270ug/Kg2501400Fluorene 540 04/08/14 DD SW 8270ug/Kg260NDHexachlorobenzene 540 04/08/14 DD SW 8270ug/Kg230NDHexachlorobutadiene 540 04/08/14 DD SW 8270ug/Kg280NDHexachlorocyclopentadiene 540 04/08/14 DD SW 8270ug/Kg240NDHexachloroethane 540 04/08/14 DD SW 8270ug/Kg230
1400Indeno(1,2,3-cd)pyrene 540 04/08/14 DD SW 8270ug/Kg260NDIsophorone 540 04/08/14 DD SW 8270ug/Kg220870Naphthalene 540 04/08/14 DD SW 8270ug/Kg220NDNitrobenzene 540 04/08/14 DD SW 8270ug/Kg270NDN-Nitrosodimethylamine 540 04/08/14 DD SW 8270ug/Kg220NDN-Nitrosodi-n-propylamine 540 04/08/14 DD SW 8270ug/Kg250NDN-Nitrosodiphenylamine 540 04/08/14 DD SW 8270ug/Kg300NDPentachloronitrobenzene 540 04/08/14 DD SW 8270ug/Kg290NDPentachlorophenol 540 04/08/14 DD SW 8270ug/Kg290
12000Phenanthrene 540 04/08/14 DD SW 8270ug/Kg220NDPhenol 540 04/08/14 DD SW 8270ug/Kg250
7700Pyrene 540 04/08/14 DD SW 8270ug/Kg270NDPyridine 540 04/08/14 DD SW 8270ug/Kg190
QA/QC Surrogates91% 2,4,6-Tribromophenol 04/08/14 DD 30 - 130 %%52% 2-Fluorobiphenyl 04/08/14 DD 30 - 130 %%
Page 5 of 40 Ver 1
E-SB2 0-2Phoenix I.D.: BG29068
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
73% 2-Fluorophenol 04/08/14 DD 30 - 130 %%52% Nitrobenzene-d5 04/08/14 DD 30 - 130 %%76% Phenol-d5 04/08/14 DD 30 - 130 %%47% Terphenyl-d14 04/08/14 DD 30 - 130 %%
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Semi-Volatile Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, a dilution was required resulting in an elevated RL for the semivolatile analysis.
Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 15, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 6 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
E-SB4 0-2
Phoenix ID: BG29069
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 15, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG29068
Client ID:Project ID: DOMINO SUGAR SITE
LOD/MDL
< 0.35Silver 0.35 04/09/14 LK SW6010mg/Kg0.216520Aluminum 35 04/08/14 LK SW6010mg/Kg6.97.1Arsenic 0.7 04/09/14 LK SW6010mg/Kg0.69
56.0Barium 0.7 04/09/14 LK SW6010mg/Kg0.140.28Beryllium 0.28 04/09/14 LK SW6010mg/Kg0.14
44300Calcium 35 04/08/14 LK SW6010mg/Kg32< 0.35Cadmium 0.35 04/09/14 LK SW6010mg/Kg0.142.51Cobalt 0.35 04/09/14 LK SW6010mg/Kg0.1410.7Chromium 0.35 04/09/14 LK SW6010mg/Kg0.1434.8Copper 0.35 04/09/14 LK SW6010mg/kg0.28
12200Iron 35 04/08/14 LK SW6010mg/Kg B350.09Mercury 0.07 04/08/14 RS SW-7471mg/Kg0.04905Potassium 7 04/09/14 LK SW6010mg/Kg2.7
4740Magnesium 3.5 04/09/14 LK SW6010mg/Kg0.21227Manganese 3.5 04/08/14 LK SW6010mg/Kg1.4672Sodium 7 04/09/14 LK SW6010mg/Kg B3.010.2Nickel 0.35 04/09/14 LK SW6010mg/Kg0.14108Lead 0.7 04/09/14 LK SW6010mg/Kg0.21
< 1.7Antimony 1.7 04/09/14 LK SW6010mg/Kg0.69< 1.4Selenium 1.4 04/09/14 LK SW6010mg/Kg1.2< 1.4Thallium 1.4 04/09/14 LK SW6010mg/Kg1.425.3Vanadium 0.3 04/09/14 LK SW6010mg/Kg0.14116Zinc 0.7 04/10/14 LK SW6010mg/Kg0.3586Percent Solid 04/07/14 I E160.3%
CompletedSoil Extraction for PCB 04/07/14 BB/V SW3545CompletedSoil Extraction for Pesticide 04/07/14 BB SW3545CompletedSoil Extraction for SVOA 04/07/14 BB/FV SW3545CompletedMercury Digestion 04/08/14 I/I SW7471
Page 7 of 40 Ver 1
E-SB4 0-2Phoenix I.D.: BG29069
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
CompletedTotal Metals Digest 04/07/14 CB/AG/D SW846 - 3050
CompletedField Extraction 04/02/14 SW5035
Polychlorinated BiphenylsNDPCB-1016 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1221 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1232 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1242 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1248 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1254 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1260 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1262 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1268 38 04/08/14 AW SW 8082ug/Kg38
QA/QC Surrogates96% DCBP 04/08/14 AW 30 - 150 %%88% TCMX 04/08/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.7 04/09/14 CE SW8081ug/Kg2.7ND4,4' -DDE 2.7 04/09/14 CE SW8081ug/Kg2.7ND4,4' -DDT 2.7 04/09/14 CE SW8081ug/Kg2.7NDa-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDa-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDAldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDb-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDChlordane 23 04/09/14 CE SW8081ug/Kg23NDd-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDDieldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndosulfan I 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan II 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan sulfate 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndrin aldehyde 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin ketone 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDHeptachlor 1.9 04/09/14 CE SW8081ug/Kg1.9NDHeptachlor epoxide 1.9 04/09/14 CE SW8081ug/Kg1.9NDMethoxychlor 7.6 04/09/14 CE SW8081ug/Kg7.6NDToxaphene 190 04/09/14 CE SW8081ug/Kg190
QA/QC SurrogatesInterference% DCBP 04/09/14 CE 30 - 150 %%
91% TCMX 04/09/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 8.0 04/10/14 U SW8260ug/Kg1.3ND1,1,1-Trichloroethane 8.0 04/10/14 U SW8260ug/Kg1.6ND1,1,2,2-Tetrachloroethane 8.0 04/10/14 U SW8260ug/Kg1.1ND1,1,2-Trichloroethane 8.0 04/10/14 U SW8260ug/Kg0.78ND1,1-Dichloroethane 8.0 04/10/14 U SW8260ug/Kg1.6
Page 8 of 40 Ver 1
E-SB4 0-2Phoenix I.D.: BG29069
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 8.0 04/10/14 U SW8260ug/Kg1.7ND1,1-Dichloropropene 8.0 04/10/14 U SW8260ug/Kg1.5ND1,2,3-Trichlorobenzene 8.0 04/10/14 U SW8260ug/Kg1.6ND1,2,3-Trichloropropane 8.0 04/10/14 U SW8260ug/Kg1.1ND1,2,4-Trichlorobenzene 8.0 04/10/14 U SW8260ug/Kg1.6ND1,2,4-Trimethylbenzene 8.0 04/10/14 U SW8260ug/Kg1.1ND1,2-Dibromo-3-chloropropane 8.0 04/10/14 U SW8260ug/Kg2.1ND1,2-Dibromoethane 8.0 04/10/14 U SW8260ug/Kg2.1ND1,2-Dichlorobenzene 8.0 04/10/14 U SW8260ug/Kg0.88ND1,2-Dichloroethane 8.0 04/10/14 U SW8260ug/Kg0.70ND1,2-Dichloropropane 8.0 04/10/14 U SW8260ug/Kg1.1ND1,3,5-Trimethylbenzene 8.0 04/10/14 U SW8260ug/Kg1.1ND1,3-Dichlorobenzene 8.0 04/10/14 U SW8260ug/Kg1.2ND1,3-Dichloropropane 8.0 04/10/14 U SW8260ug/Kg0.84ND1,4-Dichlorobenzene 8.0 04/10/14 U SW8260ug/Kg1.3ND2,2-Dichloropropane 8.0 04/10/14 U SW8260ug/Kg1.3ND2-Chlorotoluene 8.0 04/10/14 U SW8260ug/Kg1.3ND2-Hexanone 40 04/10/14 U SW8260ug/Kg3.6ND2-Isopropyltoluene 8.0 04/10/14 U SW8260ug/Kg 11.1ND4-Chlorotoluene 8.0 04/10/14 U SW8260ug/Kg0.92ND4-Methyl-2-pentanone 40 04/10/14 U SW8260ug/Kg1.9NDAcetone 50 04/10/14 U SW8260ug/Kg7.9NDAcrylonitrile 16 04/10/14 U SW8260ug/Kg4.5NDBenzene 8.0 04/10/14 U SW8260ug/Kg1.6NDBromobenzene 8.0 04/10/14 U SW8260ug/Kg1.0NDBromochloromethane 8.0 04/10/14 U SW8260ug/Kg1.2NDBromodichloromethane 8.0 04/10/14 U SW8260ug/Kg0.99NDBromoform 8.0 04/10/14 U SW8260ug/Kg1.1NDBromomethane 8.0 04/10/14 U SW8260ug/Kg6.1NDCarbon Disulfide 8.0 04/10/14 U SW8260ug/Kg1.3NDCarbon tetrachloride 8.0 04/10/14 U SW8260ug/Kg0.92NDChlorobenzene 8.0 04/10/14 U SW8260ug/Kg1.2NDChloroethane 8.0 04/10/14 U SW8260ug/Kg1.9NDChloroform 8.0 04/10/14 U SW8260ug/Kg1.4NDChloromethane 8.0 04/10/14 U SW8260ug/Kg4.2NDcis-1,2-Dichloroethene 8.0 04/10/14 U SW8260ug/Kg1.7NDcis-1,3-Dichloropropene 8.0 04/10/14 U SW8260ug/Kg0.86NDDibromochloromethane 8.0 04/10/14 U SW8260ug/Kg0.89NDDibromomethane 8.0 04/10/14 U SW8260ug/Kg1.0NDDichlorodifluoromethane 8.0 04/10/14 U SW8260ug/Kg2.1NDEthylbenzene 8.0 04/10/14 U SW8260ug/Kg1.4NDHexachlorobutadiene 8.0 04/10/14 U SW8260ug/Kg1.7NDIsopropylbenzene 8.0 04/10/14 U SW8260ug/Kg1.5NDm&p-Xylene 8.0 04/10/14 U SW8260ug/Kg3.1NDMethyl Ethyl Ketone 48 04/10/14 U SW8260ug/Kg6.9NDMethyl t-butyl ether (MTBE) 16 04/10/14 U SW8260ug/Kg2.2NDMethylene chloride 8.0 04/10/14 U SW8260ug/Kg1.3NDNaphthalene 8.0 04/10/14 U SW8260ug/Kg2.1NDn-Butylbenzene 8.0 04/10/14 U SW8260ug/Kg1.4
Page 9 of 40 Ver 1
E-SB4 0-2Phoenix I.D.: BG29069
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 8.0 04/10/14 U SW8260ug/Kg1.4NDo-Xylene 8.0 04/10/14 U SW8260ug/Kg3.0NDp-Isopropyltoluene 8.0 04/10/14 U SW8260ug/Kg1.1NDsec-Butylbenzene 8.0 04/10/14 U SW8260ug/Kg1.5NDStyrene 8.0 04/10/14 U SW8260ug/Kg2.3NDtert-Butylbenzene 8.0 04/10/14 U SW8260ug/Kg1.3NDTetrachloroethene 8.0 04/10/14 U SW8260ug/Kg1.7NDTetrahydrofuran (THF) 16 04/10/14 U SW8260ug/Kg 17.2NDToluene 8.0 04/10/14 U SW8260ug/Kg1.3NDtrans-1,2-Dichloroethene 8.0 04/10/14 U SW8260ug/Kg1.6NDtrans-1,3-Dichloropropene 8.0 04/10/14 U SW8260ug/Kg1.6NDtrans-1,4-dichloro-2-butene 16 04/10/14 U SW8260ug/Kg15NDTrichloroethene 8.0 04/10/14 U SW8260ug/Kg1.7NDTrichlorofluoromethane 8.0 04/10/14 U SW8260ug/Kg1.8NDTrichlorotrifluoroethane 8.0 04/10/14 U SW8260ug/Kg1.2NDVinyl chloride 8.0 04/10/14 U SW8260ug/Kg2.6
QA/QC Surrogates100% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%89% Bromofluorobenzene 04/10/14 U 70 - 130 %%97% Dibromofluoromethane 04/10/14 U 70 - 130 %%101% Toluene-d8 04/10/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 270 04/08/14 DD SW 8270ug/Kg130ND1,2,4-Trichlorobenzene 270 04/08/14 DD SW 8270ug/Kg110ND1,2-Dichlorobenzene 270 04/08/14 DD SW 8270ug/Kg110ND1,2-Diphenylhydrazine 270 04/08/14 DD SW 8270ug/Kg120ND1,3-Dichlorobenzene 270 04/08/14 DD SW 8270ug/Kg110ND1,4-Dichlorobenzene 270 04/08/14 DD SW 8270ug/Kg110ND2,4,5-Trichlorophenol 270 04/08/14 DD SW 8270ug/Kg210ND2,4,6-Trichlorophenol 270 04/08/14 DD SW 8270ug/Kg120ND2,4-Dichlorophenol 270 04/08/14 DD SW 8270ug/Kg130ND2,4-Dimethylphenol 270 04/08/14 DD SW 8270ug/Kg94ND2,4-Dinitrophenol 1900 04/08/14 DD SW 8270ug/Kg270ND2,4-Dinitrotoluene 270 04/08/14 DD SW 8270ug/Kg150ND2,6-Dinitrotoluene 270 04/08/14 DD SW 8270ug/Kg120ND2-Chloronaphthalene 270 04/08/14 DD SW 8270ug/Kg110ND2-Chlorophenol 270 04/08/14 DD SW 8270ug/Kg110ND2-Methylnaphthalene 270 04/08/14 DD SW 8270ug/Kg110ND2-Methylphenol (o-cresol) 270 04/08/14 DD SW 8270ug/Kg180ND2-Nitroaniline 1900 04/08/14 DD SW 8270ug/Kg380ND2-Nitrophenol 270 04/08/14 DD SW 8270ug/Kg240ND3&4-Methylphenol (m&p-cresol) 270 04/08/14 DD SW 8270ug/Kg 1150ND3,3'-Dichlorobenzidine 760 04/08/14 DD SW 8270ug/Kg180ND3-Nitroaniline 1900 04/08/14 DD SW 8270ug/Kg830ND4,6-Dinitro-2-methylphenol 1900 04/08/14 DD SW 8270ug/Kg410ND4-Bromophenyl phenyl ether 270 04/08/14 DD SW 8270ug/Kg110ND4-Chloro-3-methylphenol 270 04/08/14 DD SW 8270ug/Kg130ND4-Chloroaniline 760 04/08/14 DD SW 8270ug/Kg180ND4-Chlorophenyl phenyl ether 270 04/08/14 DD SW 8270ug/Kg130
Page 10 of 40 Ver 1
E-SB4 0-2Phoenix I.D.: BG29069
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Nitroaniline 1900 04/08/14 DD SW 8270ug/Kg130ND4-Nitrophenol 1900 04/08/14 DD SW 8270ug/Kg170NDAcenaphthene 270 04/08/14 DD SW 8270ug/Kg120NDAcenaphthylene 270 04/08/14 DD SW 8270ug/Kg110NDAcetophenone 270 04/08/14 DD SW 8270ug/Kg120NDAniline 1900 04/08/14 DD SW 8270ug/Kg770NDAnthracene 270 04/08/14 DD SW 8270ug/Kg120220Benz(a)anthracene 270 04/08/14 DD SW 8270ug/Kg130JNDBenzidine 760 04/08/14 DD SW 8270ug/Kg220180Benzo(a)pyrene 270 04/08/14 DD SW 8270ug/Kg120J260Benzo(b)fluoranthene 270 04/08/14 DD SW 8270ug/Kg130JNDBenzo(ghi)perylene 270 04/08/14 DD SW 8270ug/Kg120NDBenzo(k)fluoranthene 270 04/08/14 DD SW 8270ug/Kg130NDBenzoic acid 1900 04/08/14 DD SW 8270ug/Kg 1760NDBenzyl butyl phthalate 270 04/08/14 DD SW 8270ug/Kg98NDBis(2-chloroethoxy)methane 270 04/08/14 DD SW 8270ug/Kg110NDBis(2-chloroethyl)ether 270 04/08/14 DD SW 8270ug/Kg100NDBis(2-chloroisopropyl)ether 270 04/08/14 DD SW 8270ug/Kg 1110NDBis(2-ethylhexyl)phthalate 270 04/08/14 DD SW 8270ug/Kg110NDCarbazole 1900 04/08/14 DD SW 8270ug/Kg290240Chrysene 270 04/08/14 DD SW 8270ug/Kg130JNDDibenz(a,h)anthracene 270 04/08/14 DD SW 8270ug/Kg120NDDibenzofuran 270 04/08/14 DD SW 8270ug/Kg110NDDiethyl phthalate 270 04/08/14 DD SW 8270ug/Kg120NDDimethylphthalate 270 04/08/14 DD SW 8270ug/Kg120NDDi-n-butylphthalate 270 04/08/14 DD SW 8270ug/Kg100NDDi-n-octylphthalate 270 04/08/14 DD SW 8270ug/Kg98340Fluoranthene 270 04/08/14 DD SW 8270ug/Kg120NDFluorene 270 04/08/14 DD SW 8270ug/Kg130NDHexachlorobenzene 270 04/08/14 DD SW 8270ug/Kg110NDHexachlorobutadiene 270 04/08/14 DD SW 8270ug/Kg140NDHexachlorocyclopentadiene 270 04/08/14 DD SW 8270ug/Kg120NDHexachloroethane 270 04/08/14 DD SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 270 04/08/14 DD SW 8270ug/Kg130NDIsophorone 270 04/08/14 DD SW 8270ug/Kg110NDNaphthalene 270 04/08/14 DD SW 8270ug/Kg110NDNitrobenzene 270 04/08/14 DD SW 8270ug/Kg130NDN-Nitrosodimethylamine 270 04/08/14 DD SW 8270ug/Kg110NDN-Nitrosodi-n-propylamine 270 04/08/14 DD SW 8270ug/Kg120NDN-Nitrosodiphenylamine 270 04/08/14 DD SW 8270ug/Kg150NDPentachloronitrobenzene 270 04/08/14 DD SW 8270ug/Kg140NDPentachlorophenol 270 04/08/14 DD SW 8270ug/Kg140260Phenanthrene 270 04/08/14 DD SW 8270ug/Kg110JNDPhenol 270 04/08/14 DD SW 8270ug/Kg120320Pyrene 270 04/08/14 DD SW 8270ug/Kg130NDPyridine 270 04/08/14 DD SW 8270ug/Kg94
QA/QC Surrogates102% 2,4,6-Tribromophenol 04/08/14 DD 30 - 130 %%56% 2-Fluorobiphenyl 04/08/14 DD 30 - 130 %%
Page 11 of 40 Ver 1
E-SB4 0-2Phoenix I.D.: BG29069
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
79% 2-Fluorophenol 04/08/14 DD 30 - 130 %%53% Nitrobenzene-d5 04/08/14 DD 30 - 130 %%85% Phenol-d5 04/08/14 DD 30 - 130 %%55% Terphenyl-d14 04/08/14 DD 30 - 130 %%
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 15, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 12 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
E-SB4 15-17
Phoenix ID: BG29070
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 15, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG29068
Client ID:Project ID: DOMINO SUGAR SITE
LOD/MDL
< 0.36Silver 0.36 04/09/14 LK SW6010mg/Kg0.224440Aluminum 36 04/08/14 LK SW6010mg/Kg7.31.5Arsenic 0.7 04/09/14 LK SW6010mg/Kg0.73
38.8Barium 0.7 04/09/14 LK SW6010mg/Kg0.150.31Beryllium 0.29 04/09/14 LK SW6010mg/Kg0.15
15200Calcium 36 04/08/14 LK SW6010mg/Kg33< 0.36Cadmium 0.36 04/09/14 LK SW6010mg/Kg0.152.97Cobalt 0.36 04/09/14 LK SW6010mg/Kg0.158.23Chromium 0.36 04/09/14 LK SW6010mg/Kg0.1512.6Copper 0.36 04/09/14 LK SW6010mg/kg0.298940Iron 3.6 04/09/14 LK SW6010mg/Kg B3.6
< 0.08Mercury 0.08 04/08/14 RS SW-7471mg/Kg0.05997Potassium 7 04/09/14 LK SW6010mg/Kg2.8
2150Magnesium 3.6 04/09/14 LK SW6010mg/Kg0.22254Manganese 3.6 04/08/14 LK SW6010mg/Kg1.5128Sodium 7 04/09/14 LK SW6010mg/Kg B3.18.60Nickel 0.36 04/09/14 LK SW6010mg/Kg0.1539.0Lead 0.7 04/09/14 LK SW6010mg/Kg0.22< 1.8Antimony 1.8 04/09/14 LK SW6010mg/Kg0.73< 1.5Selenium 1.5 04/09/14 LK SW6010mg/Kg1.2< 1.5Thallium 1.5 04/09/14 LK SW6010mg/Kg1.515.5Vanadium 0.4 04/09/14 LK SW6010mg/Kg0.1522.2Zinc 0.7 04/10/14 LK SW6010mg/Kg0.3693Percent Solid 04/07/14 I E160.3%
CompletedSoil Extraction for SVOA 04/07/14 BB/FV SW3545CompletedMercury Digestion 04/08/14 I/I SW7471CompletedTotal Metals Digest 04/07/14 CB/AG/D SW846 - 3050
CompletedField Extraction 04/02/14 SW5035
Page 13 of 40 Ver 1
E-SB4 15-17Phoenix I.D.: BG29070
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 6.9 04/10/14 U SW8260ug/Kg1.1ND1,1,1-Trichloroethane 6.9 04/10/14 U SW8260ug/Kg1.4ND1,1,2,2-Tetrachloroethane 6.9 04/10/14 U SW8260ug/Kg0.98ND1,1,2-Trichloroethane 6.9 04/10/14 U SW8260ug/Kg0.67ND1,1-Dichloroethane 6.9 04/10/14 U SW8260ug/Kg1.4ND1,1-Dichloroethene 6.9 04/10/14 U SW8260ug/Kg1.5ND1,1-Dichloropropene 6.9 04/10/14 U SW8260ug/Kg1.3ND1,2,3-Trichlorobenzene 6.9 04/10/14 U SW8260ug/Kg1.4ND1,2,3-Trichloropropane 6.9 04/10/14 U SW8260ug/Kg0.98ND1,2,4-Trichlorobenzene 6.9 04/10/14 U SW8260ug/Kg1.4ND1,2,4-Trimethylbenzene 6.9 04/10/14 U SW8260ug/Kg0.99ND1,2-Dibromo-3-chloropropane 6.9 04/10/14 U SW8260ug/Kg1.8ND1,2-Dibromoethane 6.9 04/10/14 U SW8260ug/Kg1.8ND1,2-Dichlorobenzene 6.9 04/10/14 U SW8260ug/Kg0.76ND1,2-Dichloroethane 6.9 04/10/14 U SW8260ug/Kg0.61ND1,2-Dichloropropane 6.9 04/10/14 U SW8260ug/Kg0.98ND1,3,5-Trimethylbenzene 6.9 04/10/14 U SW8260ug/Kg0.91ND1,3-Dichlorobenzene 6.9 04/10/14 U SW8260ug/Kg1.0ND1,3-Dichloropropane 6.9 04/10/14 U SW8260ug/Kg0.73ND1,4-Dichlorobenzene 6.9 04/10/14 U SW8260ug/Kg1.1ND2,2-Dichloropropane 6.9 04/10/14 U SW8260ug/Kg1.2ND2-Chlorotoluene 6.9 04/10/14 U SW8260ug/Kg1.1ND2-Hexanone 34 04/10/14 U SW8260ug/Kg3.1ND2-Isopropyltoluene 6.9 04/10/14 U SW8260ug/Kg 10.95ND4-Chlorotoluene 6.9 04/10/14 U SW8260ug/Kg0.80ND4-Methyl-2-pentanone 34 04/10/14 U SW8260ug/Kg1.6NDAcetone 50 04/10/14 U SW8260ug/Kg6.8NDAcrylonitrile 14 04/10/14 U SW8260ug/Kg3.9NDBenzene 6.9 04/10/14 U SW8260ug/Kg1.4NDBromobenzene 6.9 04/10/14 U SW8260ug/Kg0.89NDBromochloromethane 6.9 04/10/14 U SW8260ug/Kg1.0NDBromodichloromethane 6.9 04/10/14 U SW8260ug/Kg0.85NDBromoform 6.9 04/10/14 U SW8260ug/Kg0.96NDBromomethane 6.9 04/10/14 U SW8260ug/Kg5.3NDCarbon Disulfide 6.9 04/10/14 U SW8260ug/Kg1.1NDCarbon tetrachloride 6.9 04/10/14 U SW8260ug/Kg0.80NDChlorobenzene 6.9 04/10/14 U SW8260ug/Kg1.0NDChloroethane 6.9 04/10/14 U SW8260ug/Kg1.6NDChloroform 6.9 04/10/14 U SW8260ug/Kg1.3NDChloromethane 6.9 04/10/14 U SW8260ug/Kg3.6NDcis-1,2-Dichloroethene 6.9 04/10/14 U SW8260ug/Kg1.5NDcis-1,3-Dichloropropene 6.9 04/10/14 U SW8260ug/Kg0.74NDDibromochloromethane 6.9 04/10/14 U SW8260ug/Kg0.77NDDibromomethane 6.9 04/10/14 U SW8260ug/Kg0.87NDDichlorodifluoromethane 6.9 04/10/14 U SW8260ug/Kg1.8NDEthylbenzene 6.9 04/10/14 U SW8260ug/Kg1.3NDHexachlorobutadiene 6.9 04/10/14 U SW8260ug/Kg1.4NDIsopropylbenzene 6.9 04/10/14 U SW8260ug/Kg1.3
Page 14 of 40 Ver 1
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Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 6.9 04/10/14 U SW8260ug/Kg2.7NDMethyl Ethyl Ketone 41 04/10/14 U SW8260ug/Kg6.0NDMethyl t-butyl ether (MTBE) 14 04/10/14 U SW8260ug/Kg1.9NDMethylene chloride 6.9 04/10/14 U SW8260ug/Kg1.1NDNaphthalene 6.9 04/10/14 U SW8260ug/Kg1.8NDn-Butylbenzene 6.9 04/10/14 U SW8260ug/Kg1.3NDn-Propylbenzene 6.9 04/10/14 U SW8260ug/Kg1.2NDo-Xylene 6.9 04/10/14 U SW8260ug/Kg2.6NDp-Isopropyltoluene 6.9 04/10/14 U SW8260ug/Kg0.99NDsec-Butylbenzene 6.9 04/10/14 U SW8260ug/Kg1.3NDStyrene 6.9 04/10/14 U SW8260ug/Kg2.0NDtert-Butylbenzene 6.9 04/10/14 U SW8260ug/Kg1.1NDTetrachloroethene 6.9 04/10/14 U SW8260ug/Kg1.4NDTetrahydrofuran (THF) 14 04/10/14 U SW8260ug/Kg 16.2NDToluene 6.9 04/10/14 U SW8260ug/Kg1.1NDtrans-1,2-Dichloroethene 6.9 04/10/14 U SW8260ug/Kg1.4NDtrans-1,3-Dichloropropene 6.9 04/10/14 U SW8260ug/Kg1.4NDtrans-1,4-dichloro-2-butene 14 04/10/14 U SW8260ug/Kg13NDTrichloroethene 6.9 04/10/14 U SW8260ug/Kg1.5NDTrichlorofluoromethane 6.9 04/10/14 U SW8260ug/Kg1.5NDTrichlorotrifluoroethane 6.9 04/10/14 U SW8260ug/Kg1.1NDVinyl chloride 6.9 04/10/14 U SW8260ug/Kg2.2
QA/QC Surrogates102% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%93% Bromofluorobenzene 04/10/14 U 70 - 130 %%98% Dibromofluoromethane 04/10/14 U 70 - 130 %%98% Toluene-d8 04/10/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 250 04/08/14 DD SW 8270ug/Kg130ND1,2,4-Trichlorobenzene 250 04/08/14 DD SW 8270ug/Kg110ND1,2-Dichlorobenzene 250 04/08/14 DD SW 8270ug/Kg100ND1,2-Diphenylhydrazine 250 04/08/14 DD SW 8270ug/Kg120ND1,3-Dichlorobenzene 250 04/08/14 DD SW 8270ug/Kg110ND1,4-Dichlorobenzene 250 04/08/14 DD SW 8270ug/Kg110ND2,4,5-Trichlorophenol 250 04/08/14 DD SW 8270ug/Kg200ND2,4,6-Trichlorophenol 250 04/08/14 DD SW 8270ug/Kg110ND2,4-Dichlorophenol 250 04/08/14 DD SW 8270ug/Kg130ND2,4-Dimethylphenol 250 04/08/14 DD SW 8270ug/Kg89ND2,4-Dinitrophenol 1800 04/08/14 DD SW 8270ug/Kg250ND2,4-Dinitrotoluene 250 04/08/14 DD SW 8270ug/Kg140ND2,6-Dinitrotoluene 250 04/08/14 DD SW 8270ug/Kg110ND2-Chloronaphthalene 250 04/08/14 DD SW 8270ug/Kg100ND2-Chlorophenol 250 04/08/14 DD SW 8270ug/Kg100ND2-Methylnaphthalene 250 04/08/14 DD SW 8270ug/Kg110ND2-Methylphenol (o-cresol) 250 04/08/14 DD SW 8270ug/Kg170ND2-Nitroaniline 1800 04/08/14 DD SW 8270ug/Kg360ND2-Nitrophenol 250 04/08/14 DD SW 8270ug/Kg230ND3&4-Methylphenol (m&p-cresol) 250 04/08/14 DD SW 8270ug/Kg 1140ND3,3'-Dichlorobenzidine 720 04/08/14 DD SW 8270ug/Kg170
Page 15 of 40 Ver 1
E-SB4 15-17Phoenix I.D.: BG29070
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND3-Nitroaniline 1800 04/08/14 DD SW 8270ug/Kg780ND4,6-Dinitro-2-methylphenol 1800 04/08/14 DD SW 8270ug/Kg390ND4-Bromophenyl phenyl ether 250 04/08/14 DD SW 8270ug/Kg110ND4-Chloro-3-methylphenol 250 04/08/14 DD SW 8270ug/Kg130ND4-Chloroaniline 720 04/08/14 DD SW 8270ug/Kg170ND4-Chlorophenyl phenyl ether 250 04/08/14 DD SW 8270ug/Kg120ND4-Nitroaniline 1800 04/08/14 DD SW 8270ug/Kg120ND4-Nitrophenol 1800 04/08/14 DD SW 8270ug/Kg160NDAcenaphthene 250 04/08/14 DD SW 8270ug/Kg110NDAcenaphthylene 250 04/08/14 DD SW 8270ug/Kg100NDAcetophenone 250 04/08/14 DD SW 8270ug/Kg110NDAniline 1800 04/08/14 DD SW 8270ug/Kg720NDAnthracene 250 04/08/14 DD SW 8270ug/Kg120NDBenz(a)anthracene 250 04/08/14 DD SW 8270ug/Kg120NDBenzidine 720 04/08/14 DD SW 8270ug/Kg210NDBenzo(a)pyrene 250 04/08/14 DD SW 8270ug/Kg120NDBenzo(b)fluoranthene 250 04/08/14 DD SW 8270ug/Kg120NDBenzo(ghi)perylene 250 04/08/14 DD SW 8270ug/Kg120NDBenzo(k)fluoranthene 250 04/08/14 DD SW 8270ug/Kg120NDBenzoic acid 1800 04/08/14 DD SW 8270ug/Kg 1720NDBenzyl butyl phthalate 250 04/08/14 DD SW 8270ug/Kg92NDBis(2-chloroethoxy)methane 250 04/08/14 DD SW 8270ug/Kg99NDBis(2-chloroethyl)ether 250 04/08/14 DD SW 8270ug/Kg97NDBis(2-chloroisopropyl)ether 250 04/08/14 DD SW 8270ug/Kg 1100NDBis(2-ethylhexyl)phthalate 250 04/08/14 DD SW 8270ug/Kg100NDCarbazole 1800 04/08/14 DD SW 8270ug/Kg270NDChrysene 250 04/08/14 DD SW 8270ug/Kg120NDDibenz(a,h)anthracene 250 04/08/14 DD SW 8270ug/Kg120NDDibenzofuran 250 04/08/14 DD SW 8270ug/Kg100NDDiethyl phthalate 250 04/08/14 DD SW 8270ug/Kg110NDDimethylphthalate 250 04/08/14 DD SW 8270ug/Kg110NDDi-n-butylphthalate 250 04/08/14 DD SW 8270ug/Kg95NDDi-n-octylphthalate 250 04/08/14 DD SW 8270ug/Kg92NDFluoranthene 250 04/08/14 DD SW 8270ug/Kg120NDFluorene 250 04/08/14 DD SW 8270ug/Kg120NDHexachlorobenzene 250 04/08/14 DD SW 8270ug/Kg100NDHexachlorobutadiene 250 04/08/14 DD SW 8270ug/Kg130NDHexachlorocyclopentadiene 250 04/08/14 DD SW 8270ug/Kg110NDHexachloroethane 250 04/08/14 DD SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 250 04/08/14 DD SW 8270ug/Kg120NDIsophorone 250 04/08/14 DD SW 8270ug/Kg100NDNaphthalene 250 04/08/14 DD SW 8270ug/Kg100NDNitrobenzene 250 04/08/14 DD SW 8270ug/Kg130NDN-Nitrosodimethylamine 250 04/08/14 DD SW 8270ug/Kg100NDN-Nitrosodi-n-propylamine 250 04/08/14 DD SW 8270ug/Kg120NDN-Nitrosodiphenylamine 250 04/08/14 DD SW 8270ug/Kg140NDPentachloronitrobenzene 250 04/08/14 DD SW 8270ug/Kg130NDPentachlorophenol 250 04/08/14 DD SW 8270ug/Kg140NDPhenanthrene 250 04/08/14 DD SW 8270ug/Kg100
Page 16 of 40 Ver 1
E-SB4 15-17Phoenix I.D.: BG29070
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDPhenol 250 04/08/14 DD SW 8270ug/Kg110NDPyrene 250 04/08/14 DD SW 8270ug/Kg120NDPyridine 250 04/08/14 DD SW 8270ug/Kg88
QA/QC Surrogates92% 2,4,6-Tribromophenol 04/08/14 DD 30 - 130 %%55% 2-Fluorobiphenyl 04/08/14 DD 30 - 130 %%80% 2-Fluorophenol 04/08/14 DD 30 - 130 %%53% Nitrobenzene-d5 04/08/14 DD 30 - 130 %%84% Phenol-d5 04/08/14 DD 30 - 130 %%55% Terphenyl-d14 04/08/14 DD 30 - 130 %%
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 15, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 17 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
E-SB5 0-2
Phoenix ID: BG29071
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 15, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG29068
Client ID:Project ID: DOMINO SUGAR SITE
LOD/MDL
< 0.35Silver 0.35 04/09/14 LK SW6010mg/Kg0.216340Aluminum 35 04/08/14 LK SW6010mg/Kg7.07.2Arsenic 0.7 04/09/14 LK SW6010mg/Kg0.70
80.8Barium 0.7 04/09/14 LK SW6010mg/Kg0.140.32Beryllium 0.28 04/09/14 LK SW6010mg/Kg0.14
37400Calcium 35 04/08/14 LK SW6010mg/Kg32< 0.35Cadmium 0.35 04/09/14 LK SW6010mg/Kg0.144.14Cobalt 0.35 04/09/14 LK SW6010mg/Kg0.1412.6Chromium 0.35 04/09/14 LK SW6010mg/Kg0.1457.0Copper 0.35 04/09/14 LK SW6010mg/kg0.28
16200Iron 35 04/08/14 LK SW6010mg/Kg B350.28Mercury 0.06 04/08/14 RS SW-7471mg/Kg0.04938Potassium 7 04/09/14 LK SW6010mg/Kg2.7
11200Magnesium 35 04/08/14 LK SW6010mg/Kg2.1255Manganese 3.5 04/08/14 LK SW6010mg/Kg1.4338Sodium 7 04/09/14 LK SW6010mg/Kg B3.015.1Nickel 0.35 04/09/14 LK SW6010mg/Kg0.14166Lead 7.0 04/08/14 LK SW6010mg/Kg2.1
< 1.7Antimony 1.7 04/09/14 LK SW6010mg/Kg0.70< 1.4Selenium 1.4 04/10/14 LK SW6010mg/Kg1.2< 1.4Thallium 1.4 04/09/14 LK SW6010mg/Kg1.425.8Vanadium 0.3 04/09/14 LK SW6010mg/Kg0.14121Zinc 0.7 04/10/14 LK SW6010mg/Kg0.3591Percent Solid 04/07/14 I E160.3%
CompletedSoil Extraction for PCB 04/07/14 BB/V SW3545CompletedSoil Extraction for Pesticide 04/07/14 BB SW3545CompletedSoil Extraction for SVOA 04/07/14 BB/FV SW3545CompletedMercury Digestion 04/08/14 I/I SW7471
Page 18 of 40 Ver 1
E-SB5 0-2Phoenix I.D.: BG29071
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
CompletedTotal Metals Digest 04/07/14 CB/AG/D SW846 - 3050
CompletedField Extraction 04/02/14 SW5035
Polychlorinated BiphenylsNDPCB-1016 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1221 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1232 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1242 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1248 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1254 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1260 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1262 36 04/08/14 AW SW 8082ug/Kg36NDPCB-1268 36 04/08/14 AW SW 8082ug/Kg36
QA/QC Surrogates96% DCBP 04/08/14 AW 30 - 150 %%81% TCMX 04/08/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.6 04/09/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 04/09/14 CE SW8081ug/Kg2.6ND4,4' -DDT 2.6 04/09/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 04/09/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.6 04/09/14 CE SW8081ug/Kg3.6NDAldrin 1.8 04/09/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 04/09/14 CE SW8081ug/Kg1.8NDChlordane 22 04/09/14 CE SW8081ug/Kg22NDd-BHC 1.8 04/09/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 04/09/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.6 04/09/14 CE SW8081ug/Kg3.6NDEndosulfan II 3.6 04/09/14 CE SW8081ug/Kg3.6NDEndosulfan sulfate 3.6 04/09/14 CE SW8081ug/Kg3.6NDEndrin 1.8 04/09/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.6 04/09/14 CE SW8081ug/Kg3.6NDEndrin ketone 1.8 04/09/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 04/09/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.6 04/09/14 CE SW8081ug/Kg3.6NDHeptachlor 1.8 04/09/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 04/09/14 CE SW8081ug/Kg1.8NDMethoxychlor 22 04/09/14 CE SW8081ug/Kg22NDToxaphene 180 04/09/14 CE SW8081ug/Kg180
QA/QC Surrogates140% DCBP 04/09/14 CE 30 - 150 %%89% TCMX 04/09/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 9.8 04/10/14 U SW8260ug/Kg1.6ND1,1,1-Trichloroethane 9.8 04/10/14 U SW8260ug/Kg2.0ND1,1,2,2-Tetrachloroethane 9.8 04/10/14 U SW8260ug/Kg1.4ND1,1,2-Trichloroethane 9.8 04/10/14 U SW8260ug/Kg0.96ND1,1-Dichloroethane 9.8 04/10/14 U SW8260ug/Kg1.9
Page 19 of 40 Ver 1
E-SB5 0-2Phoenix I.D.: BG29071
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 9.8 04/10/14 U SW8260ug/Kg2.1ND1,1-Dichloropropene 9.8 04/10/14 U SW8260ug/Kg1.9ND1,2,3-Trichlorobenzene 9.8 04/10/14 U SW8260ug/Kg2.0ND1,2,3-Trichloropropane 9.8 04/10/14 U SW8260ug/Kg1.4ND1,2,4-Trichlorobenzene 9.8 04/10/14 U SW8260ug/Kg2.0ND1,2,4-Trimethylbenzene 9.8 04/10/14 U SW8260ug/Kg1.4ND1,2-Dibromo-3-chloropropane 9.8 04/10/14 U SW8260ug/Kg2.6ND1,2-Dibromoethane 9.8 04/10/14 U SW8260ug/Kg2.6ND1,2-Dichlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.1ND1,2-Dichloroethane 9.8 04/10/14 U SW8260ug/Kg0.87ND1,2-Dichloropropane 9.8 04/10/14 U SW8260ug/Kg1.4ND1,3,5-Trimethylbenzene 9.8 04/10/14 U SW8260ug/Kg1.3ND1,3-Dichlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.5ND1,3-Dichloropropane 9.8 04/10/14 U SW8260ug/Kg1.0ND1,4-Dichlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.6ND2,2-Dichloropropane 9.8 04/10/14 U SW8260ug/Kg1.7ND2-Chlorotoluene 9.8 04/10/14 U SW8260ug/Kg1.6ND2-Hexanone 49 04/10/14 U SW8260ug/Kg4.4ND2-Isopropyltoluene 9.8 04/10/14 U SW8260ug/Kg 11.4ND4-Chlorotoluene 9.8 04/10/14 U SW8260ug/Kg1.1ND4-Methyl-2-pentanone 49 04/10/14 U SW8260ug/Kg2.312Acetone 50 04/10/14 U SW8260ug/Kg9.8JSNDAcrylonitrile 20 04/10/14 U SW8260ug/Kg5.5NDBenzene 9.8 04/10/14 U SW8260ug/Kg1.9NDBromobenzene 9.8 04/10/14 U SW8260ug/Kg1.3NDBromochloromethane 9.8 04/10/14 U SW8260ug/Kg1.4NDBromodichloromethane 9.8 04/10/14 U SW8260ug/Kg1.2NDBromoform 9.8 04/10/14 U SW8260ug/Kg1.4NDBromomethane 9.8 04/10/14 U SW8260ug/Kg7.6NDCarbon Disulfide 9.8 04/10/14 U SW8260ug/Kg1.6NDCarbon tetrachloride 9.8 04/10/14 U SW8260ug/Kg1.1NDChlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.5NDChloroethane 9.8 04/10/14 U SW8260ug/Kg2.3NDChloroform 9.8 04/10/14 U SW8260ug/Kg1.8NDChloromethane 9.8 04/10/14 U SW8260ug/Kg5.2NDcis-1,2-Dichloroethene 9.8 04/10/14 U SW8260ug/Kg2.1NDcis-1,3-Dichloropropene 9.8 04/10/14 U SW8260ug/Kg1.1NDDibromochloromethane 9.8 04/10/14 U SW8260ug/Kg1.1NDDibromomethane 9.8 04/10/14 U SW8260ug/Kg1.2NDDichlorodifluoromethane 9.8 04/10/14 U SW8260ug/Kg2.6NDEthylbenzene 9.8 04/10/14 U SW8260ug/Kg1.8NDHexachlorobutadiene 9.8 04/10/14 U SW8260ug/Kg2.1NDIsopropylbenzene 9.8 04/10/14 U SW8260ug/Kg1.9NDm&p-Xylene 9.8 04/10/14 U SW8260ug/Kg3.9NDMethyl Ethyl Ketone 59 04/10/14 U SW8260ug/Kg8.5NDMethyl t-butyl ether (MTBE) 20 04/10/14 U SW8260ug/Kg2.7NDMethylene chloride 9.8 04/10/14 U SW8260ug/Kg1.6NDNaphthalene 9.8 04/10/14 U SW8260ug/Kg2.6NDn-Butylbenzene 9.8 04/10/14 U SW8260ug/Kg1.8
Page 20 of 40 Ver 1
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Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 9.8 04/10/14 U SW8260ug/Kg1.8NDo-Xylene 9.8 04/10/14 U SW8260ug/Kg3.8NDp-Isopropyltoluene 9.8 04/10/14 U SW8260ug/Kg1.4NDsec-Butylbenzene 9.8 04/10/14 U SW8260ug/Kg1.8NDStyrene 9.8 04/10/14 U SW8260ug/Kg2.8NDtert-Butylbenzene 9.8 04/10/14 U SW8260ug/Kg1.6NDTetrachloroethene 9.8 04/10/14 U SW8260ug/Kg2.1NDTetrahydrofuran (THF) 20 04/10/14 U SW8260ug/Kg 18.9NDToluene 9.8 04/10/14 U SW8260ug/Kg1.6NDtrans-1,2-Dichloroethene 9.8 04/10/14 U SW8260ug/Kg2.0NDtrans-1,3-Dichloropropene 9.8 04/10/14 U SW8260ug/Kg2.0NDtrans-1,4-dichloro-2-butene 20 04/10/14 U SW8260ug/Kg18NDTrichloroethene 9.8 04/10/14 U SW8260ug/Kg2.1NDTrichlorofluoromethane 9.8 04/10/14 U SW8260ug/Kg2.2NDTrichlorotrifluoroethane 9.8 04/10/14 U SW8260ug/Kg1.5NDVinyl chloride 9.8 04/10/14 U SW8260ug/Kg3.2
QA/QC Surrogates103% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%88% Bromofluorobenzene 04/10/14 U 70 - 130 %%98% Dibromofluoromethane 04/10/14 U 70 - 130 %%99% Toluene-d8 04/10/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 500 04/08/14 DD SW 8270ug/Kg250ND1,2,4-Trichlorobenzene 500 04/08/14 DD SW 8270ug/Kg210ND1,2-Dichlorobenzene 500 04/08/14 DD SW 8270ug/Kg200ND1,2-Diphenylhydrazine 500 04/08/14 DD SW 8270ug/Kg230ND1,3-Dichlorobenzene 500 04/08/14 DD SW 8270ug/Kg210ND1,4-Dichlorobenzene 500 04/08/14 DD SW 8270ug/Kg210ND2,4,5-Trichlorophenol 500 04/08/14 DD SW 8270ug/Kg390ND2,4,6-Trichlorophenol 500 04/08/14 DD SW 8270ug/Kg230ND2,4-Dichlorophenol 500 04/08/14 DD SW 8270ug/Kg250ND2,4-Dimethylphenol 500 04/08/14 DD SW 8270ug/Kg180ND2,4-Dinitrophenol 3500 04/08/14 DD SW 8270ug/Kg500ND2,4-Dinitrotoluene 500 04/08/14 DD SW 8270ug/Kg280ND2,6-Dinitrotoluene 500 04/08/14 DD SW 8270ug/Kg220ND2-Chloronaphthalene 500 04/08/14 DD SW 8270ug/Kg200ND2-Chlorophenol 500 04/08/14 DD SW 8270ug/Kg200ND2-Methylnaphthalene 500 04/08/14 DD SW 8270ug/Kg210ND2-Methylphenol (o-cresol) 500 04/08/14 DD SW 8270ug/Kg330ND2-Nitroaniline 3500 04/08/14 DD SW 8270ug/Kg720ND2-Nitrophenol 500 04/08/14 DD SW 8270ug/Kg450ND3&4-Methylphenol (m&p-cresol) 500 04/08/14 DD SW 8270ug/Kg 1280ND3,3'-Dichlorobenzidine 1400 04/08/14 DD SW 8270ug/Kg340ND3-Nitroaniline 3500 04/08/14 DD SW 8270ug/Kg1500ND4,6-Dinitro-2-methylphenol 3500 04/08/14 DD SW 8270ug/Kg760ND4-Bromophenyl phenyl ether 500 04/08/14 DD SW 8270ug/Kg210ND4-Chloro-3-methylphenol 500 04/08/14 DD SW 8270ug/Kg250ND4-Chloroaniline 1400 04/08/14 DD SW 8270ug/Kg330ND4-Chlorophenyl phenyl ether 500 04/08/14 DD SW 8270ug/Kg240
Page 21 of 40 Ver 1
E-SB5 0-2Phoenix I.D.: BG29071
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Nitroaniline 3500 04/08/14 DD SW 8270ug/Kg240ND4-Nitrophenol 3500 04/08/14 DD SW 8270ug/Kg320NDAcenaphthene 500 04/08/14 DD SW 8270ug/Kg220NDAcenaphthylene 500 04/08/14 DD SW 8270ug/Kg200NDAcetophenone 500 04/08/14 DD SW 8270ug/Kg220NDAniline 3500 04/08/14 DD SW 8270ug/Kg1400240Anthracene 500 04/08/14 DD SW 8270ug/Kg230J
1400Benz(a)anthracene 500 04/08/14 DD SW 8270ug/Kg240NDBenzidine 1400 04/08/14 DD SW 8270ug/Kg420
1200Benzo(a)pyrene 500 04/08/14 DD SW 8270ug/Kg2301800Benzo(b)fluoranthene 500 04/08/14 DD SW 8270ug/Kg240380Benzo(ghi)perylene 500 04/08/14 DD SW 8270ug/Kg230J480Benzo(k)fluoranthene 500 04/08/14 DD SW 8270ug/Kg240JNDBenzoic acid 3500 04/08/14 DD SW 8270ug/Kg 11400NDBenzyl butyl phthalate 500 04/08/14 DD SW 8270ug/Kg180NDBis(2-chloroethoxy)methane 500 04/08/14 DD SW 8270ug/Kg200NDBis(2-chloroethyl)ether 500 04/08/14 DD SW 8270ug/Kg190NDBis(2-chloroisopropyl)ether 500 04/08/14 DD SW 8270ug/Kg 1200NDBis(2-ethylhexyl)phthalate 500 04/08/14 DD SW 8270ug/Kg200NDCarbazole 3500 04/08/14 DD SW 8270ug/Kg540
1300Chrysene 500 04/08/14 DD SW 8270ug/Kg240NDDibenz(a,h)anthracene 500 04/08/14 DD SW 8270ug/Kg230NDDibenzofuran 500 04/08/14 DD SW 8270ug/Kg210NDDiethyl phthalate 500 04/08/14 DD SW 8270ug/Kg220NDDimethylphthalate 500 04/08/14 DD SW 8270ug/Kg220NDDi-n-butylphthalate 500 04/08/14 DD SW 8270ug/Kg190NDDi-n-octylphthalate 500 04/08/14 DD SW 8270ug/Kg180
2100Fluoranthene 500 04/08/14 DD SW 8270ug/Kg230NDFluorene 500 04/08/14 DD SW 8270ug/Kg230NDHexachlorobenzene 500 04/08/14 DD SW 8270ug/Kg210NDHexachlorobutadiene 500 04/08/14 DD SW 8270ug/Kg260NDHexachlorocyclopentadiene 500 04/08/14 DD SW 8270ug/Kg220NDHexachloroethane 500 04/08/14 DD SW 8270ug/Kg210370Indeno(1,2,3-cd)pyrene 500 04/08/14 DD SW 8270ug/Kg240JNDIsophorone 500 04/08/14 DD SW 8270ug/Kg200NDNaphthalene 500 04/08/14 DD SW 8270ug/Kg200NDNitrobenzene 500 04/08/14 DD SW 8270ug/Kg250NDN-Nitrosodimethylamine 500 04/08/14 DD SW 8270ug/Kg200NDN-Nitrosodi-n-propylamine 500 04/08/14 DD SW 8270ug/Kg230NDN-Nitrosodiphenylamine 500 04/08/14 DD SW 8270ug/Kg270NDPentachloronitrobenzene 500 04/08/14 DD SW 8270ug/Kg260NDPentachlorophenol 500 04/08/14 DD SW 8270ug/Kg270
1200Phenanthrene 500 04/08/14 DD SW 8270ug/Kg200NDPhenol 500 04/08/14 DD SW 8270ug/Kg230
1900Pyrene 500 04/08/14 DD SW 8270ug/Kg240NDPyridine 500 04/08/14 DD SW 8270ug/Kg170
QA/QC Surrogates86% 2,4,6-Tribromophenol 04/08/14 DD 30 - 130 %%55% 2-Fluorobiphenyl 04/08/14 DD 30 - 130 %%
Page 22 of 40 Ver 1
E-SB5 0-2Phoenix I.D.: BG29071
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
74% 2-Fluorophenol 04/08/14 DD 30 - 130 %%52% Nitrobenzene-d5 04/08/14 DD 30 - 130 %%78% Phenol-d5 04/08/14 DD 30 - 130 %%53% Terphenyl-d14 04/08/14 DD 30 - 130 %%
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Semi-Volatile Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, a dilution was required resulting in an elevated RL for the semivolatile analysis.
Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 15, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 23 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
E-SB5 12-14
Phoenix ID: BG29072
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 15, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG29068
Client ID:Project ID: DOMINO SUGAR SITE
LOD/MDL
< 0.42Silver 0.42 04/09/14 LK SW6010mg/Kg0.256000Aluminum 42 04/09/14 LK SW6010mg/Kg8.3137Arsenic 0.8 04/09/14 LK SW6010mg/Kg0.83126Barium 0.8 04/09/14 LK SW6010mg/Kg0.170.74Beryllium 0.33 04/09/14 LK SW6010mg/Kg0.17
21400Calcium 42 04/09/14 LK SW6010mg/Kg388.19Cadmium 0.42 04/09/14 LK SW6010mg/Kg0.1718.1Cobalt 0.42 04/09/14 LK SW6010mg/Kg0.1718.9Chromium 0.42 04/09/14 LK SW6010mg/Kg0.17185Copper 4.2 04/09/14 LK SW6010mg/kg3.3
78600Iron 42 04/09/14 LK SW6010mg/Kg B420.23Mercury 0.10 04/08/14 RS SW-7471mg/Kg0.061330Potassium 8 04/09/14 LK SW6010mg/Kg3.22600Magnesium 4.2 04/09/14 LK SW6010mg/Kg0.25435Manganese 4.2 04/09/14 LK SW6010mg/Kg1.7326Sodium 8 04/09/14 LK SW6010mg/Kg B3.639.6Nickel 0.42 04/09/14 LK SW6010mg/Kg0.17308Lead 8.3 04/09/14 LK SW6010mg/Kg2.5
< 2.1Antimony 2.1 04/09/14 LK SW6010mg/Kg0.83< 1.7Selenium 1.7 04/10/14 LK SW6010mg/Kg1.4< 1.7Thallium 1.7 04/09/14 LK SW6010mg/Kg1.759.0Vanadium 0.4 04/09/14 LK SW6010mg/Kg0.171480Zinc 8.3 04/10/14 LK SW6010mg/Kg4.280Percent Solid 04/07/14 I E160.3%
CompletedSoil Extraction for SVOA 04/07/14 BB/FV SW3545CompletedMercury Digestion 04/08/14 I/I SW7471CompletedTotal Metals Digest 04/07/14 CB/AG/D SW846 - 3050
CompletedField Extraction 04/02/14 SW5035
Page 24 of 40 Ver 1
E-SB5 12-14Phoenix I.D.: BG29072
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
VolatilesND1,1,1,2-Tetrachloroethane 8.9 04/10/14 U SW8260ug/Kg1.5ND1,1,1-Trichloroethane 8.9 04/10/14 U SW8260ug/Kg1.8ND1,1,2,2-Tetrachloroethane 8.9 04/10/14 U SW8260ug/Kg1.3ND1,1,2-Trichloroethane 8.9 04/10/14 U SW8260ug/Kg0.88ND1,1-Dichloroethane 8.9 04/10/14 U SW8260ug/Kg1.8ND1,1-Dichloroethene 8.9 04/10/14 U SW8260ug/Kg1.9ND1,1-Dichloropropene 8.9 04/10/14 U SW8260ug/Kg1.7ND1,2,3-Trichlorobenzene 280 04/11/14 U SW8260ug/Kg56ND1,2,3-Trichloropropane 280 04/11/14 U SW8260ug/Kg40ND1,2,4-Trichlorobenzene 280 04/11/14 U SW8260ug/Kg56ND1,2,4-Trimethylbenzene 280 04/11/14 U SW8260ug/Kg41ND1,2-Dibromo-3-chloropropane 280 04/11/14 U SW8260ug/Kg75ND1,2-Dibromoethane 8.9 04/10/14 U SW8260ug/Kg2.4ND1,2-Dichlorobenzene 280 04/11/14 U SW8260ug/Kg31ND1,2-Dichloroethane 8.9 04/10/14 U SW8260ug/Kg0.79ND1,2-Dichloropropane 8.9 04/10/14 U SW8260ug/Kg1.3ND1,3,5-Trimethylbenzene 280 04/11/14 U SW8260ug/Kg37ND1,3-Dichlorobenzene 280 04/11/14 U SW8260ug/Kg42ND1,3-Dichloropropane 8.9 04/10/14 U SW8260ug/Kg0.95ND1,4-Dichlorobenzene 280 04/11/14 U SW8260ug/Kg44ND2,2-Dichloropropane 8.9 04/10/14 U SW8260ug/Kg1.5ND2-Chlorotoluene 280 04/11/14 U SW8260ug/Kg45ND2-Hexanone 45 04/10/14 U SW8260ug/Kg4.0ND2-Isopropyltoluene 280 04/11/14 U SW8260ug/Kg 139ND4-Chlorotoluene 280 04/11/14 U SW8260ug/Kg33ND4-Methyl-2-pentanone 45 04/10/14 U SW8260ug/Kg2.149Acetone 50 04/10/14 U SW8260ug/Kg8.9JS'NDAcrylonitrile 18 04/10/14 U SW8260ug/Kg5.0NDBenzene 8.9 04/10/14 U SW8260ug/Kg1.8NDBromobenzene 280 04/11/14 U SW8260ug/Kg37NDBromochloromethane 8.9 04/10/14 U SW8260ug/Kg1.3NDBromodichloromethane 8.9 04/10/14 U SW8260ug/Kg1.1NDBromoform 8.9 04/10/14 U SW8260ug/Kg1.3NDBromomethane 8.9 04/10/14 U SW8260ug/Kg6.9NDCarbon Disulfide 8.9 04/10/14 U SW8260ug/Kg1.4NDCarbon tetrachloride 8.9 04/10/14 U SW8260ug/Kg1.0NDChlorobenzene 8.9 04/10/14 U SW8260ug/Kg1.3NDChloroethane 8.9 04/10/14 U SW8260ug/Kg2.1NDChloroform 8.9 04/10/14 U SW8260ug/Kg1.6NDChloromethane 8.9 04/10/14 U SW8260ug/Kg4.7NDcis-1,2-Dichloroethene 8.9 04/10/14 U SW8260ug/Kg1.9NDcis-1,3-Dichloropropene 8.9 04/10/14 U SW8260ug/Kg0.97NDDibromochloromethane 8.9 04/10/14 U SW8260ug/Kg1.0NDDibromomethane 8.9 04/10/14 U SW8260ug/Kg1.1NDDichlorodifluoromethane 8.9 04/10/14 U SW8260ug/Kg2.4NDEthylbenzene 8.9 04/10/14 U SW8260ug/Kg1.6NDHexachlorobutadiene 280 04/11/14 U SW8260ug/Kg59NDIsopropylbenzene 280 04/11/14 U SW8260ug/Kg54
Page 25 of 40 Ver 1
E-SB5 12-14Phoenix I.D.: BG29072
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDm&p-Xylene 8.9 04/10/14 U SW8260ug/Kg3.5NDMethyl Ethyl Ketone 54 04/10/14 U SW8260ug/Kg7.8NDMethyl t-butyl ether (MTBE) 18 04/10/14 U SW8260ug/Kg2.5NDMethylene chloride 8.9 04/10/14 U SW8260ug/Kg1.5NDNaphthalene 280 04/11/14 U SW8260ug/Kg75NDn-Butylbenzene 280 04/11/14 U SW8260ug/Kg51NDn-Propylbenzene 280 04/11/14 U SW8260ug/Kg51NDo-Xylene 8.9 04/10/14 U SW8260ug/Kg3.4NDp-Isopropyltoluene 280 04/11/14 U SW8260ug/Kg41NDsec-Butylbenzene 280 04/11/14 U SW8260ug/Kg53NDStyrene 8.9 04/10/14 U SW8260ug/Kg2.6NDtert-Butylbenzene 280 04/11/14 U SW8260ug/Kg45NDTetrachloroethene 8.9 04/10/14 U SW8260ug/Kg1.9NDTetrahydrofuran (THF) 18 04/10/14 U SW8260ug/Kg 18.0NDToluene 8.9 04/10/14 U SW8260ug/Kg1.4NDtrans-1,2-Dichloroethene 8.9 04/10/14 U SW8260ug/Kg1.8NDtrans-1,3-Dichloropropene 8.9 04/10/14 U SW8260ug/Kg1.8NDtrans-1,4-dichloro-2-butene 560 04/11/14 U SW8260ug/Kg520NDTrichloroethene 8.9 04/10/14 U SW8260ug/Kg1.9NDTrichlorofluoromethane 8.9 04/10/14 U SW8260ug/Kg2.0NDTrichlorotrifluoroethane 8.9 04/10/14 U SW8260ug/Kg1.4NDVinyl chloride 8.9 04/10/14 U SW8260ug/Kg2.9
QA/QC Surrogates99% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%95% Bromofluorobenzene 04/11/14 U 70 - 130 %%108% Dibromofluoromethane 04/10/14 U 70 - 130 %%97% Toluene-d8 04/10/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 290 04/08/14 DD SW 8270ug/Kg150ND1,2,4-Trichlorobenzene 290 04/08/14 DD SW 8270ug/Kg130ND1,2-Dichlorobenzene 290 04/08/14 DD SW 8270ug/Kg120ND1,2-Diphenylhydrazine 290 04/08/14 DD SW 8270ug/Kg140ND1,3-Dichlorobenzene 290 04/08/14 DD SW 8270ug/Kg120ND1,4-Dichlorobenzene 290 04/08/14 DD SW 8270ug/Kg120ND2,4,5-Trichlorophenol 290 04/08/14 DD SW 8270ug/Kg230ND2,4,6-Trichlorophenol 290 04/08/14 DD SW 8270ug/Kg130ND2,4-Dichlorophenol 290 04/08/14 DD SW 8270ug/Kg150ND2,4-Dimethylphenol 290 04/08/14 DD SW 8270ug/Kg100ND2,4-Dinitrophenol 2100 04/08/14 DD SW 8270ug/Kg290ND2,4-Dinitrotoluene 290 04/08/14 DD SW 8270ug/Kg160ND2,6-Dinitrotoluene 290 04/08/14 DD SW 8270ug/Kg130ND2-Chloronaphthalene 290 04/08/14 DD SW 8270ug/Kg120ND2-Chlorophenol 290 04/08/14 DD SW 8270ug/Kg1201802-Methylnaphthalene 290 04/08/14 DD SW 8270ug/Kg120JND2-Methylphenol (o-cresol) 290 04/08/14 DD SW 8270ug/Kg200ND2-Nitroaniline 2100 04/08/14 DD SW 8270ug/Kg420ND2-Nitrophenol 290 04/08/14 DD SW 8270ug/Kg260ND3&4-Methylphenol (m&p-cresol) 290 04/08/14 DD SW 8270ug/Kg 1160ND3,3'-Dichlorobenzidine 830 04/08/14 DD SW 8270ug/Kg200
Page 26 of 40 Ver 1
E-SB5 12-14Phoenix I.D.: BG29072
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND3-Nitroaniline 2100 04/08/14 DD SW 8270ug/Kg900ND4,6-Dinitro-2-methylphenol 2100 04/08/14 DD SW 8270ug/Kg450ND4-Bromophenyl phenyl ether 290 04/08/14 DD SW 8270ug/Kg120ND4-Chloro-3-methylphenol 290 04/08/14 DD SW 8270ug/Kg150ND4-Chloroaniline 830 04/08/14 DD SW 8270ug/Kg190ND4-Chlorophenyl phenyl ether 290 04/08/14 DD SW 8270ug/Kg140ND4-Nitroaniline 2100 04/08/14 DD SW 8270ug/Kg140ND4-Nitrophenol 2100 04/08/14 DD SW 8270ug/Kg190NDAcenaphthene 290 04/08/14 DD SW 8270ug/Kg130820Acenaphthylene 290 04/08/14 DD SW 8270ug/Kg120NDAcetophenone 290 04/08/14 DD SW 8270ug/Kg130NDAniline 2100 04/08/14 DD SW 8270ug/Kg840
1200Anthracene 290 04/08/14 DD SW 8270ug/Kg1409300Benz(a)anthracene 290 04/08/14 DD SW 8270ug/Kg140NDBenzidine 830 04/08/14 DD SW 8270ug/Kg240
8300Benzo(a)pyrene 290 04/08/14 DD SW 8270ug/Kg14011000Benzo(b)fluoranthene 290 04/08/14 DD SW 8270ug/Kg1403200Benzo(ghi)perylene 290 04/08/14 DD SW 8270ug/Kg1303700Benzo(k)fluoranthene 290 04/08/14 DD SW 8270ug/Kg140NDBenzoic acid 2100 04/08/14 DD SW 8270ug/Kg 1830NDBenzyl butyl phthalate 290 04/08/14 DD SW 8270ug/Kg110NDBis(2-chloroethoxy)methane 290 04/08/14 DD SW 8270ug/Kg110NDBis(2-chloroethyl)ether 290 04/08/14 DD SW 8270ug/Kg110NDBis(2-chloroisopropyl)ether 290 04/08/14 DD SW 8270ug/Kg 1120NDBis(2-ethylhexyl)phthalate 290 04/08/14 DD SW 8270ug/Kg120690Carbazole 2100 04/08/14 DD SW 8270ug/Kg320J
8600Chrysene 290 04/08/14 DD SW 8270ug/Kg140NDDibenz(a,h)anthracene 290 04/08/14 DD SW 8270ug/Kg130200Dibenzofuran 290 04/08/14 DD SW 8270ug/Kg120JNDDiethyl phthalate 290 04/08/14 DD SW 8270ug/Kg130NDDimethylphthalate 290 04/08/14 DD SW 8270ug/Kg130NDDi-n-butylphthalate 290 04/08/14 DD SW 8270ug/Kg110NDDi-n-octylphthalate 290 04/08/14 DD SW 8270ug/Kg110
18000Fluoranthene 290 04/08/14 DD SW 8270ug/Kg130230Fluorene 290 04/08/14 DD SW 8270ug/Kg140JNDHexachlorobenzene 290 04/08/14 DD SW 8270ug/Kg120NDHexachlorobutadiene 290 04/08/14 DD SW 8270ug/Kg150NDHexachlorocyclopentadiene 290 04/08/14 DD SW 8270ug/Kg130NDHexachloroethane 290 04/08/14 DD SW 8270ug/Kg120
3400Indeno(1,2,3-cd)pyrene 290 04/08/14 DD SW 8270ug/Kg140NDIsophorone 290 04/08/14 DD SW 8270ug/Kg120590Naphthalene 290 04/08/14 DD SW 8270ug/Kg120NDNitrobenzene 290 04/08/14 DD SW 8270ug/Kg150NDN-Nitrosodimethylamine 290 04/08/14 DD SW 8270ug/Kg120NDN-Nitrosodi-n-propylamine 290 04/08/14 DD SW 8270ug/Kg130NDN-Nitrosodiphenylamine 290 04/08/14 DD SW 8270ug/Kg160NDPentachloronitrobenzene 290 04/08/14 DD SW 8270ug/Kg150NDPentachlorophenol 290 04/08/14 DD SW 8270ug/Kg160
5800Phenanthrene 290 04/08/14 DD SW 8270ug/Kg120
Page 27 of 40 Ver 1
E-SB5 12-14Phoenix I.D.: BG29072
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDPhenol 290 04/08/14 DD SW 8270ug/Kg13016000Pyrene 290 04/08/14 DD SW 8270ug/Kg140
NDPyridine 290 04/08/14 DD SW 8270ug/Kg100
QA/QC Surrogates90% 2,4,6-Tribromophenol 04/08/14 DD 30 - 130 %%51% 2-Fluorobiphenyl 04/08/14 DD 30 - 130 %%75% 2-Fluorophenol 04/08/14 DD 30 - 130 %%49% Nitrobenzene-d5 04/08/14 DD 30 - 130 %%79% Phenol-d5 04/08/14 DD 30 - 130 %%53% Terphenyl-d14 04/08/14 DD 30 - 130 %%
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Volatile Comment:There was a suppression of the last internal standard in the low level analysis, all affected compounds are reported from the methanol preserved high level analysis which did not exhibit this interference.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 15, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 28 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
SOIL DUPLICATE 1
Phoenix ID: BG29073
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 15, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG29068
Client ID:Project ID: DOMINO SUGAR SITE
LOD/MDL
< 0.36Silver 0.36 04/09/14 LK SW6010mg/Kg0.227570Aluminum 36 04/09/14 LK SW6010mg/Kg7.25.2Arsenic 0.7 04/09/14 LK SW6010mg/Kg0.72110Barium 0.7 04/09/14 LK SW6010mg/Kg0.140.39Beryllium 0.29 04/09/14 LK SW6010mg/Kg0.14
28100Calcium 36 04/09/14 LK SW6010mg/Kg33< 0.36Cadmium 0.36 04/09/14 LK SW6010mg/Kg0.143.82Cobalt 0.36 04/09/14 LK SW6010mg/Kg0.1412.7Chromium 0.36 04/09/14 LK SW6010mg/Kg0.1451.2Copper 0.36 04/09/14 LK SW6010mg/kg0.29
12200Iron 36 04/09/14 LK SW6010mg/Kg B360.12Mercury 0.08 04/08/14 RS SW-7471mg/Kg0.051090Potassium 7 04/09/14 LK SW6010mg/Kg2.82590Magnesium 3.6 04/09/14 LK SW6010mg/Kg0.22160Manganese 3.6 04/09/14 LK SW6010mg/Kg1.4613Sodium 7 04/09/14 LK SW6010mg/Kg B3.113.0Nickel 0.36 04/09/14 LK SW6010mg/Kg0.14156Lead 7.2 04/09/14 LK SW6010mg/Kg2.2
< 1.8Antimony 1.8 04/09/14 LK SW6010mg/Kg0.72< 1.4Selenium 1.4 04/09/14 LK SW6010mg/Kg1.2< 1.4Thallium 1.4 04/09/14 LK SW6010mg/Kg1.429.1Vanadium 0.4 04/09/14 LK SW6010mg/Kg0.1481.8Zinc 0.7 04/10/14 LK SW6010mg/Kg0.3684Percent Solid 04/07/14 I E160.3%
CompletedSoil Extraction for PCB 04/07/14 BB/V SW3545CompletedSoil Extraction for Pesticide 04/07/14 BB SW3545CompletedSoil Extraction for SVOA 04/07/14 BB/FV SW3545CompletedMercury Digestion 04/08/14 I/I SW7471
Page 29 of 40 Ver 1
SOIL DUPLICATE 1Phoenix I.D.: BG29073
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
CompletedTotal Metals Digest 04/07/14 CB/AG/D SW846 - 3050
CompletedField Extraction 04/02/14 SW5035
Polychlorinated BiphenylsNDPCB-1016 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1221 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1232 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1242 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1248 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1254 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1260 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1262 38 04/08/14 AW SW 8082ug/Kg38NDPCB-1268 38 04/08/14 AW SW 8082ug/Kg38
QA/QC Surrogates118% DCBP 04/08/14 AW 30 - 150 %%83% TCMX 04/08/14 AW 30 - 150 %%
Pesticides - SoilND4,4' -DDD 2.8 04/09/14 CE SW8081ug/Kg2.8ND4,4' -DDE 2.8 04/09/14 CE SW8081ug/Kg2.8ND4,4' -DDT 2.8 04/09/14 CE SW8081ug/Kg2.8NDa-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDa-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDAldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDb-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDChlordane 23 04/09/14 CE SW8081ug/Kg23NDd-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDDieldrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndosulfan I 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan II 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndosulfan sulfate 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin 1.9 04/09/14 CE SW8081ug/Kg1.9NDEndrin aldehyde 3.8 04/09/14 CE SW8081ug/Kg3.8NDEndrin ketone 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-BHC 1.9 04/09/14 CE SW8081ug/Kg1.9NDg-Chlordane 3.8 04/09/14 CE SW8081ug/Kg3.8NDHeptachlor 1.9 04/09/14 CE SW8081ug/Kg1.9NDHeptachlor epoxide 1.9 04/09/14 CE SW8081ug/Kg1.9NDMethoxychlor 58 04/09/14 CE SW8081ug/Kg58NDToxaphene 190 04/09/14 CE SW8081ug/Kg190
QA/QC Surrogates128% DCBP 04/09/14 CE 30 - 150 %%76% TCMX 04/09/14 CE 30 - 150 %%
VolatilesND1,1,1,2-Tetrachloroethane 8.5 04/10/14 U SW8260ug/Kg1.4ND1,1,1-Trichloroethane 8.5 04/10/14 U SW8260ug/Kg1.7ND1,1,2,2-Tetrachloroethane 8.5 04/10/14 U SW8260ug/Kg1.2ND1,1,2-Trichloroethane 8.5 04/10/14 U SW8260ug/Kg0.83ND1,1-Dichloroethane 8.5 04/10/14 U SW8260ug/Kg1.7
Page 30 of 40 Ver 1
SOIL DUPLICATE 1Phoenix I.D.: BG29073
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND1,1-Dichloroethene 8.5 04/10/14 U SW8260ug/Kg1.9ND1,1-Dichloropropene 8.5 04/10/14 U SW8260ug/Kg1.7ND1,2,3-Trichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.7ND1,2,3-Trichloropropane 8.5 04/10/14 U SW8260ug/Kg1.2ND1,2,4-Trichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.7ND1,2,4-Trimethylbenzene 8.5 04/10/14 U SW8260ug/Kg1.2ND1,2-Dibromo-3-chloropropane 8.5 04/10/14 U SW8260ug/Kg2.3ND1,2-Dibromoethane 8.5 04/10/14 U SW8260ug/Kg2.3ND1,2-Dichlorobenzene 8.5 04/10/14 U SW8260ug/Kg0.94ND1,2-Dichloroethane 8.5 04/10/14 U SW8260ug/Kg0.75ND1,2-Dichloropropane 8.5 04/10/14 U SW8260ug/Kg1.2ND1,3,5-Trimethylbenzene 8.5 04/10/14 U SW8260ug/Kg1.1ND1,3-Dichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.3ND1,3-Dichloropropane 8.5 04/10/14 U SW8260ug/Kg0.90ND1,4-Dichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.3ND2,2-Dichloropropane 8.5 04/10/14 U SW8260ug/Kg1.4ND2-Chlorotoluene 8.5 04/10/14 U SW8260ug/Kg1.4ND2-Hexanone 43 04/10/14 U SW8260ug/Kg3.8ND2-Isopropyltoluene 8.5 04/10/14 U SW8260ug/Kg 11.2ND4-Chlorotoluene 8.5 04/10/14 U SW8260ug/Kg0.99ND4-Methyl-2-pentanone 43 04/10/14 U SW8260ug/Kg2.030Acetone 50 04/10/14 U SW8260ug/Kg8.5JSNDAcrylonitrile 17 04/10/14 U SW8260ug/Kg4.8NDBenzene 8.5 04/10/14 U SW8260ug/Kg1.7NDBromobenzene 8.5 04/10/14 U SW8260ug/Kg1.1NDBromochloromethane 8.5 04/10/14 U SW8260ug/Kg1.2NDBromodichloromethane 8.5 04/10/14 U SW8260ug/Kg1.1NDBromoform 8.5 04/10/14 U SW8260ug/Kg1.2NDBromomethane 8.5 04/10/14 U SW8260ug/Kg6.6NDCarbon Disulfide 8.5 04/10/14 U SW8260ug/Kg1.4NDCarbon tetrachloride 8.5 04/10/14 U SW8260ug/Kg0.99NDChlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.3NDChloroethane 8.5 04/10/14 U SW8260ug/Kg2.0NDChloroform 8.5 04/10/14 U SW8260ug/Kg1.5NDChloromethane 8.5 04/10/14 U SW8260ug/Kg4.5NDcis-1,2-Dichloroethene 8.5 04/10/14 U SW8260ug/Kg1.9NDcis-1,3-Dichloropropene 8.5 04/10/14 U SW8260ug/Kg0.92NDDibromochloromethane 8.5 04/10/14 U SW8260ug/Kg0.95NDDibromomethane 8.5 04/10/14 U SW8260ug/Kg1.1NDDichlorodifluoromethane 8.5 04/10/14 U SW8260ug/Kg2.3NDEthylbenzene 8.5 04/10/14 U SW8260ug/Kg1.5NDHexachlorobutadiene 8.5 04/10/14 U SW8260ug/Kg1.8NDIsopropylbenzene 8.5 04/10/14 U SW8260ug/Kg1.6NDm&p-Xylene 8.5 04/10/14 U SW8260ug/Kg3.4NDMethyl Ethyl Ketone 51 04/10/14 U SW8260ug/Kg7.4NDMethyl t-butyl ether (MTBE) 17 04/10/14 U SW8260ug/Kg2.3NDMethylene chloride 8.5 04/10/14 U SW8260ug/Kg1.4390Naphthalene 320 04/11/14 U SW8260ug/Kg84NDn-Butylbenzene 8.5 04/10/14 U SW8260ug/Kg1.5
Page 31 of 40 Ver 1
SOIL DUPLICATE 1Phoenix I.D.: BG29073
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
NDn-Propylbenzene 8.5 04/10/14 U SW8260ug/Kg1.5NDo-Xylene 8.5 04/10/14 U SW8260ug/Kg3.3NDp-Isopropyltoluene 8.5 04/10/14 U SW8260ug/Kg1.2NDsec-Butylbenzene 8.5 04/10/14 U SW8260ug/Kg1.6NDStyrene 8.5 04/10/14 U SW8260ug/Kg2.5NDtert-Butylbenzene 8.5 04/10/14 U SW8260ug/Kg1.4NDTetrachloroethene 8.5 04/10/14 U SW8260ug/Kg1.8NDTetrahydrofuran (THF) 17 04/10/14 U SW8260ug/Kg 17.7NDToluene 8.5 04/10/14 U SW8260ug/Kg1.3NDtrans-1,2-Dichloroethene 8.5 04/10/14 U SW8260ug/Kg1.7NDtrans-1,3-Dichloropropene 8.5 04/10/14 U SW8260ug/Kg1.7NDtrans-1,4-dichloro-2-butene 17 04/10/14 U SW8260ug/Kg16NDTrichloroethene 8.5 04/10/14 U SW8260ug/Kg1.8NDTrichlorofluoromethane 8.5 04/10/14 U SW8260ug/Kg1.9NDTrichlorotrifluoroethane 8.5 04/10/14 U SW8260ug/Kg1.3NDVinyl chloride 8.5 04/10/14 U SW8260ug/Kg2.8
QA/QC Surrogates105% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%84% Bromofluorobenzene 04/10/14 U 70 - 130 %%101% Dibromofluoromethane 04/10/14 U 70 - 130 %%97% Toluene-d8 04/10/14 U 70 - 130 %%
SemivolatilesND1,2,4,5-Tetrachlorobenzene 270 04/08/14 DD SW 8270ug/Kg140ND1,2,4-Trichlorobenzene 270 04/08/14 DD SW 8270ug/Kg120ND1,2-Dichlorobenzene 270 04/08/14 DD SW 8270ug/Kg110ND1,2-Diphenylhydrazine 270 04/08/14 DD SW 8270ug/Kg130ND1,3-Dichlorobenzene 270 04/08/14 DD SW 8270ug/Kg110ND1,4-Dichlorobenzene 270 04/08/14 DD SW 8270ug/Kg110ND2,4,5-Trichlorophenol 270 04/08/14 DD SW 8270ug/Kg210ND2,4,6-Trichlorophenol 270 04/08/14 DD SW 8270ug/Kg120ND2,4-Dichlorophenol 270 04/08/14 DD SW 8270ug/Kg140ND2,4-Dimethylphenol 270 04/08/14 DD SW 8270ug/Kg95ND2,4-Dinitrophenol 1900 04/08/14 DD SW 8270ug/Kg270ND2,4-Dinitrotoluene 270 04/08/14 DD SW 8270ug/Kg150ND2,6-Dinitrotoluene 270 04/08/14 DD SW 8270ug/Kg120ND2-Chloronaphthalene 270 04/08/14 DD SW 8270ug/Kg110ND2-Chlorophenol 270 04/08/14 DD SW 8270ug/Kg1103302-Methylnaphthalene 270 04/08/14 DD SW 8270ug/Kg110ND2-Methylphenol (o-cresol) 270 04/08/14 DD SW 8270ug/Kg180ND2-Nitroaniline 1900 04/08/14 DD SW 8270ug/Kg390ND2-Nitrophenol 270 04/08/14 DD SW 8270ug/Kg240ND3&4-Methylphenol (m&p-cresol) 270 04/08/14 DD SW 8270ug/Kg 1150ND3,3'-Dichlorobenzidine 770 04/08/14 DD SW 8270ug/Kg180ND3-Nitroaniline 1900 04/08/14 DD SW 8270ug/Kg840ND4,6-Dinitro-2-methylphenol 1900 04/08/14 DD SW 8270ug/Kg410ND4-Bromophenyl phenyl ether 270 04/08/14 DD SW 8270ug/Kg110ND4-Chloro-3-methylphenol 270 04/08/14 DD SW 8270ug/Kg140ND4-Chloroaniline 770 04/08/14 DD SW 8270ug/Kg180ND4-Chlorophenyl phenyl ether 270 04/08/14 DD SW 8270ug/Kg130
Page 32 of 40 Ver 1
SOIL DUPLICATE 1Phoenix I.D.: BG29073
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Nitroaniline 1900 04/08/14 DD SW 8270ug/Kg130ND4-Nitrophenol 1900 04/08/14 DD SW 8270ug/Kg170690Acenaphthene 270 04/08/14 DD SW 8270ug/Kg120NDAcenaphthylene 270 04/08/14 DD SW 8270ug/Kg110NDAcetophenone 270 04/08/14 DD SW 8270ug/Kg120NDAniline 1900 04/08/14 DD SW 8270ug/Kg780
1700Anthracene 270 04/08/14 DD SW 8270ug/Kg1303300Benz(a)anthracene 270 04/08/14 DD SW 8270ug/Kg130NDBenzidine 770 04/08/14 DD SW 8270ug/Kg230
2500Benzo(a)pyrene 270 04/08/14 DD SW 8270ug/Kg1303700Benzo(b)fluoranthene 270 04/08/14 DD SW 8270ug/Kg130940Benzo(ghi)perylene 270 04/08/14 DD SW 8270ug/Kg120
1200Benzo(k)fluoranthene 270 04/08/14 DD SW 8270ug/Kg130NDBenzoic acid 1900 04/08/14 DD SW 8270ug/Kg 1770NDBenzyl butyl phthalate 270 04/08/14 DD SW 8270ug/Kg99NDBis(2-chloroethoxy)methane 270 04/08/14 DD SW 8270ug/Kg110NDBis(2-chloroethyl)ether 270 04/08/14 DD SW 8270ug/Kg100NDBis(2-chloroisopropyl)ether 270 04/08/14 DD SW 8270ug/Kg 1110NDBis(2-ethylhexyl)phthalate 270 04/08/14 DD SW 8270ug/Kg110610Carbazole 1900 04/08/14 DD SW 8270ug/Kg290J
2800Chrysene 270 04/08/14 DD SW 8270ug/Kg130NDDibenz(a,h)anthracene 270 04/08/14 DD SW 8270ug/Kg120690Dibenzofuran 270 04/08/14 DD SW 8270ug/Kg110NDDiethyl phthalate 270 04/08/14 DD SW 8270ug/Kg120NDDimethylphthalate 270 04/08/14 DD SW 8270ug/Kg120NDDi-n-butylphthalate 270 04/08/14 DD SW 8270ug/Kg100NDDi-n-octylphthalate 270 04/08/14 DD SW 8270ug/Kg99
6000Fluoranthene 270 04/08/14 DD SW 8270ug/Kg120840Fluorene 270 04/08/14 DD SW 8270ug/Kg130NDHexachlorobenzene 270 04/08/14 DD SW 8270ug/Kg110NDHexachlorobutadiene 270 04/08/14 DD SW 8270ug/Kg140NDHexachlorocyclopentadiene 270 04/08/14 DD SW 8270ug/Kg120NDHexachloroethane 270 04/08/14 DD SW 8270ug/Kg120890Indeno(1,2,3-cd)pyrene 270 04/08/14 DD SW 8270ug/Kg130NDIsophorone 270 04/08/14 DD SW 8270ug/Kg110560Naphthalene 270 04/08/14 DD SW 8270ug/Kg110NDNitrobenzene 270 04/08/14 DD SW 8270ug/Kg130NDN-Nitrosodimethylamine 270 04/08/14 DD SW 8270ug/Kg110NDN-Nitrosodi-n-propylamine 270 04/08/14 DD SW 8270ug/Kg120NDN-Nitrosodiphenylamine 270 04/08/14 DD SW 8270ug/Kg150NDPentachloronitrobenzene 270 04/08/14 DD SW 8270ug/Kg140NDPentachlorophenol 270 04/08/14 DD SW 8270ug/Kg150
5700Phenanthrene 270 04/08/14 DD SW 8270ug/Kg110NDPhenol 270 04/08/14 DD SW 8270ug/Kg120
4800Pyrene 270 04/08/14 DD SW 8270ug/Kg130NDPyridine 270 04/08/14 DD SW 8270ug/Kg95
QA/QC Surrogates93% 2,4,6-Tribromophenol 04/08/14 DD 30 - 130 %%54% 2-Fluorobiphenyl 04/08/14 DD 30 - 130 %%
Page 33 of 40 Ver 1
SOIL DUPLICATE 1Phoenix I.D.: BG29073
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
77% 2-Fluorophenol 04/08/14 DD 30 - 130 %%54% Nitrobenzene-d5 04/08/14 DD 30 - 130 %%80% Phenol-d5 04/08/14 DD 30 - 130 %%56% Terphenyl-d14 04/08/14 DD 30 - 130 %%
Comments:
Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.
Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.
Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 15, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 34 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
TRIP BLANK HIGH
Phoenix ID: BG29074
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 15, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG29068
Client ID:Project ID: DOMINO SUGAR SITE
LOD/MDL
100Percent Solid 1 04/02/14 E160.3%CompletedField Extraction 04/02/14 SW5035
VolatilesND1,1,1,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg41ND1,1,1-Trichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1,2,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg36ND1,1,2-Trichloroethane 250 04/10/14 U SW8260ug/Kg25ND1,1-Dichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1-Dichloroethene 250 04/10/14 U SW8260ug/Kg55ND1,1-Dichloropropene 250 04/10/14 U SW8260ug/Kg49ND1,2,3-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,3-Trichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,2,4-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,4-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg36ND1,2-Dibromo-3-chloropropane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dibromoethane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg28ND1,2-Dichloroethane 250 04/10/14 U SW8260ug/Kg22ND1,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,3,5-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg33ND1,3-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg37ND1,3-Dichloropropane 250 04/10/14 U SW8260ug/Kg27ND1,4-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg40ND2,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg42ND2-Chlorotoluene 250 04/10/14 U SW8260ug/Kg40ND2-Hexanone 1300 04/10/14 U SW8260ug/Kg110ND2-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg 135
Page 35 of 40 Ver 1
TRIP BLANK HIGHPhoenix I.D.: BG29074
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Chlorotoluene 250 04/10/14 U SW8260ug/Kg29ND4-Methyl-2-pentanone 1300 04/10/14 U SW8260ug/Kg60NDAcetone 2500 04/10/14 U SW8260ug/Kg250NDAcrylonitrile 500 04/10/14 U SW8260ug/Kg140NDBenzene 250 04/10/14 U SW8260ug/Kg50NDBromobenzene 250 04/10/14 U SW8260ug/Kg33NDBromochloromethane 250 04/10/14 U SW8260ug/Kg37NDBromodichloromethane 250 04/10/14 U SW8260ug/Kg31NDBromoform 250 04/10/14 U SW8260ug/Kg35NDBromomethane 250 04/10/14 U SW8260ug/Kg190NDCarbon Disulfide 250 04/10/14 U SW8260ug/Kg41NDCarbon tetrachloride 250 04/10/14 U SW8260ug/Kg29NDChlorobenzene 250 04/10/14 U SW8260ug/Kg37NDChloroethane 250 04/10/14 U SW8260ug/Kg59NDChloroform 250 04/10/14 U SW8260ug/Kg46NDChloromethane 250 04/10/14 U SW8260ug/Kg130NDcis-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg55NDcis-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg27NDDibromochloromethane 250 04/10/14 U SW8260ug/Kg28NDDibromomethane 250 04/10/14 U SW8260ug/Kg32NDDichlorodifluoromethane 250 04/10/14 U SW8260ug/Kg67NDEthylbenzene 250 04/10/14 U SW8260ug/Kg46NDHexachlorobutadiene 250 04/10/14 U SW8260ug/Kg53NDIsopropylbenzene 250 04/10/14 U SW8260ug/Kg48NDm&p-Xylene 250 04/10/14 U SW8260ug/Kg99NDMethyl Ethyl Ketone 1500 04/10/14 U SW8260ug/Kg220NDMethyl t-butyl ether (MTBE) 500 04/10/14 U SW8260ug/Kg69NDMethylene chloride 250 04/10/14 U SW8260ug/Kg41NDNaphthalene 250 04/10/14 U SW8260ug/Kg67NDn-Butylbenzene 250 04/10/14 U SW8260ug/Kg46NDn-Propylbenzene 250 04/10/14 U SW8260ug/Kg45NDo-Xylene 250 04/10/14 U SW8260ug/Kg96NDp-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg36NDsec-Butylbenzene 250 04/10/14 U SW8260ug/Kg47NDStyrene 250 04/10/14 U SW8260ug/Kg72NDtert-Butylbenzene 250 04/10/14 U SW8260ug/Kg40NDTetrachloroethene 250 04/10/14 U SW8260ug/Kg53NDTetrahydrofuran (THF) 500 04/10/14 U SW8260ug/Kg 1230NDToluene 250 04/10/14 U SW8260ug/Kg40NDtrans-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg50NDtrans-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg51NDtrans-1,4-dichloro-2-butene 500 04/10/14 U SW8260ug/Kg460NDTrichloroethene 250 04/10/14 U SW8260ug/Kg53NDTrichlorofluoromethane 250 04/10/14 U SW8260ug/Kg56NDTrichlorotrifluoroethane 250 04/10/14 U SW8260ug/Kg39NDVinyl chloride 250 04/10/14 U SW8260ug/Kg81
QA/QC Surrogates99% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%95% Bromofluorobenzene 04/10/14 U 70 - 130 %%
Page 36 of 40 Ver 1
TRIP BLANK HIGHPhoenix I.D.: BG29074
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
95% Dibromofluoromethane 04/10/14 U 70 - 130 %%100% Toluene-d8 04/10/14 U 70 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 15, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 37 of 40 Ver 1
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
SOLIDEBC72 Hour
04/02/14SWsee "By" below
Laboratory Data
TRIP BLANK LOW
Phoenix ID: BG29075
04/07/140:00
17:33
Parameter ResultRL/PQL Units Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 15, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG29068
Client ID:Project ID: DOMINO SUGAR SITE
LOD/MDL
100Percent Solid 1 04/02/14 E160.3%CompletedField Extraction 04/02/14 SW5035
VolatilesND1,1,1,2-Tetrachloroethane 5.0 04/10/14 U SW8260ug/Kg0.82ND1,1,1-Trichloroethane 5.0 04/10/14 U SW8260ug/Kg1.0ND1,1,2,2-Tetrachloroethane 5.0 04/10/14 U SW8260ug/Kg0.71ND1,1,2-Trichloroethane 5.0 04/10/14 U SW8260ug/Kg0.49ND1,1-Dichloroethane 5.0 04/10/14 U SW8260ug/Kg0.99ND1,1-Dichloroethene 5.0 04/10/14 U SW8260ug/Kg1.1ND1,1-Dichloropropene 5.0 04/10/14 U SW8260ug/Kg0.97ND1,2,3-Trichlorobenzene 5.0 04/10/14 U SW8260ug/Kg1.0ND1,2,3-Trichloropropane 5.0 04/10/14 U SW8260ug/Kg0.71ND1,2,4-Trichlorobenzene 5.0 04/10/14 U SW8260ug/Kg1.0ND1,2,4-Trimethylbenzene 5.0 04/10/14 U SW8260ug/Kg0.72ND1,2-Dibromo-3-chloropropane 5.0 04/10/14 U SW8260ug/Kg1.3ND1,2-Dibromoethane 5.0 04/10/14 U SW8260ug/Kg1.3ND1,2-Dichlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.55ND1,2-Dichloroethane 5.0 04/10/14 U SW8260ug/Kg0.44ND1,2-Dichloropropane 5.0 04/10/14 U SW8260ug/Kg0.71ND1,3,5-Trimethylbenzene 5.0 04/10/14 U SW8260ug/Kg0.66ND1,3-Dichlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.74ND1,3-Dichloropropane 5.0 04/10/14 U SW8260ug/Kg0.53ND1,4-Dichlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.79ND2,2-Dichloropropane 5.0 04/10/14 U SW8260ug/Kg0.84ND2-Chlorotoluene 5.0 04/10/14 U SW8260ug/Kg0.80ND2-Hexanone 25 04/10/14 U SW8260ug/Kg2.3ND2-Isopropyltoluene 5.0 04/10/14 U SW8260ug/Kg 10.69
Page 38 of 40 Ver 1
TRIP BLANK LOWPhoenix I.D.: BG29075
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
ND4-Chlorotoluene 5.0 04/10/14 U SW8260ug/Kg0.58ND4-Methyl-2-pentanone 25 04/10/14 U SW8260ug/Kg1.2NDAcetone 50 04/10/14 U SW8260ug/Kg5.0NDAcrylonitrile 10 04/10/14 U SW8260ug/Kg2.8NDBenzene 5.0 04/10/14 U SW8260ug/Kg0.99NDBromobenzene 5.0 04/10/14 U SW8260ug/Kg0.65NDBromochloromethane 5.0 04/10/14 U SW8260ug/Kg0.73NDBromodichloromethane 5.0 04/10/14 U SW8260ug/Kg0.62NDBromoform 5.0 04/10/14 U SW8260ug/Kg0.70NDBromomethane 5.0 04/10/14 U SW8260ug/Kg3.9NDCarbon Disulfide 5.0 04/10/14 U SW8260ug/Kg0.81NDCarbon tetrachloride 5.0 04/10/14 U SW8260ug/Kg0.58NDChlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.74NDChloroethane 5.0 04/10/14 U SW8260ug/Kg1.2NDChloroform 5.0 04/10/14 U SW8260ug/Kg0.91NDChloromethane 5.0 04/10/14 U SW8260ug/Kg2.6NDcis-1,2-Dichloroethene 5.0 04/10/14 U SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.0 04/10/14 U SW8260ug/Kg0.54NDDibromochloromethane 5.0 04/10/14 U SW8260ug/Kg0.56NDDibromomethane 5.0 04/10/14 U SW8260ug/Kg0.63NDDichlorodifluoromethane 5.0 04/10/14 U SW8260ug/Kg1.3NDEthylbenzene 5.0 04/10/14 U SW8260ug/Kg0.91NDHexachlorobutadiene 5.0 04/10/14 U SW8260ug/Kg1.1NDIsopropylbenzene 5.0 04/10/14 U SW8260ug/Kg0.96NDm&p-Xylene 5.0 04/10/14 U SW8260ug/Kg2.0NDMethyl Ethyl Ketone 30 04/10/14 U SW8260ug/Kg4.3NDMethyl t-butyl ether (MTBE) 10 04/10/14 U SW8260ug/Kg1.4NDMethylene chloride 5.0 04/10/14 U SW8260ug/Kg0.82NDNaphthalene 5.0 04/10/14 U SW8260ug/Kg1.3NDn-Butylbenzene 5.0 04/10/14 U SW8260ug/Kg0.91NDn-Propylbenzene 5.0 04/10/14 U SW8260ug/Kg0.90NDo-Xylene 5.0 04/10/14 U SW8260ug/Kg1.9NDp-Isopropyltoluene 5.0 04/10/14 U SW8260ug/Kg0.72NDsec-Butylbenzene 5.0 04/10/14 U SW8260ug/Kg0.94NDStyrene 5.0 04/10/14 U SW8260ug/Kg1.4NDtert-Butylbenzene 5.0 04/10/14 U SW8260ug/Kg0.80NDTetrachloroethene 5.0 04/10/14 U SW8260ug/Kg1.1NDTetrahydrofuran (THF) 10 04/10/14 U SW8260ug/Kg 14.5NDToluene 5.0 04/10/14 U SW8260ug/Kg0.79NDtrans-1,2-Dichloroethene 5.0 04/10/14 U SW8260ug/Kg1.0NDtrans-1,3-Dichloropropene 5.0 04/10/14 U SW8260ug/Kg1.0NDtrans-1,4-dichloro-2-butene 10 04/10/14 U SW8260ug/Kg9.3NDTrichloroethene 5.0 04/10/14 U SW8260ug/Kg1.1NDTrichlorofluoromethane 5.0 04/10/14 U SW8260ug/Kg1.1NDTrichlorotrifluoroethane 5.0 04/10/14 U SW8260ug/Kg0.78NDVinyl chloride 5.0 04/10/14 U SW8260ug/Kg1.6
QA/QC Surrogates100% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%96% Bromofluorobenzene 04/10/14 U 70 - 130 %%
Page 39 of 40 Ver 1
TRIP BLANK LOWPhoenix I.D.: BG29075
Client ID:DOMINO SUGAR SITEProject ID:
Parameter ResultRL/PQL Units Date/Time By Reference
LOD/MDL
101% Dibromofluoromethane 04/10/14 U 70 - 130 %%101% Toluene-d8 04/10/14 U 70 - 130 %%
Comments:
TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%
All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.
Phyllis Shiller, Laboratory DirectorApril 15, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit
Page 40 of 40 Ver 1
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
QA/QC ReportApril 15, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG29068
LCS%
DupRPD
LCSD%
LCSRPD
%Rec
Limits
%RPD
LimitsSampleResult
DupResult
QA/QC Batch 270840, QC Sample No: BG28884 (BG29068, BG29069, BG29070, BG29071, BG29072, BG29073)113 114Mercury - Soil BRL 0.9103NC 104 1.0 70 - 130 30<0.07 <0.08
Additional Mercury criteria: LCS acceptance range for waters is 80-120% and for soils is 70-130%.
Comment:
QA/QC Batch 270800, QC Sample No: BG29062 (BG29068, BG29069, BG29070, BG29071, BG29072, BG29073)
ICP Metals - SoilNC NCAluminum BRL NC1072.90 107 0.0 75 - 125 305060 5210
93.0 95.1Antimony BRL 2.296.5NC 101 4.6 75 - 125 30<1.9 <1.9
93.9 94.0Arsenic BRL 0.195.3NC 96.8 1.6 75 - 125 303.3 2.78
98.0 110Barium BRL 11.512015.4 101 17.2 75 - 125 3047.5 40.7
97.4 98.8Beryllium BRL 1.4101NC 101 0.0 75 - 125 30<0.31 <0.31
89.8 91.0Cadmium BRL 1.397.0NC 94.0 3.1 75 - 125 30<0.39 <0.39
NC NCCalcium BRL NC93.744.8 92.3 1.5 r75 - 125 3027400 43200
95.9 96.0Chromium BRL 0.11038.00 103 0.0 75 - 125 3019.5 18.0
93.3 93.9Cobalt BRL 0.6101NC 98.8 2.2 75 - 125 301.94 1.77
86.3 85.6Copper BRL 0.810613.1 104 1.9 75 - 125 30203 178
NC NCIron 9.7 NC1068.10 108 1.9 75 - 125 306900 7480
90.1 92.2Lead BRL 2.310122.6 96.9 4.1 75 - 125 3049.8 39.7
NC NCMagnesium BRL NC101116 101 0.0 r75 - 125 302200 8330
93.0 94.7Manganese BRL 1.810316.1 100 3.0 75 - 125 3084.5 99.3
91.7 91.8Nickel BRL 0.11023.90 99.1 2.9 75 - 125 3010.5 10.1
128 >130Potassium BRL NC10929.7 113 3.6 m75 - 125 301320 979
82.3 82.7Selenium BRL 0.586.8NC 84.3 2.9 75 - 125 30<1.6 <1.6
99.6 100Silver BRL 0.498.2NC 99.5 1.3 75 - 125 30<0.39 <0.39
>130 >130Sodium 5.6 NC1133.80 112 0.9 m75 - 125 30234 243
94.8 95.8Thallium BRL 1.098.4NC 96.1 2.4 75 - 125 30<1.6 <1.6
99.0 100Vanadium BRL 1.010416.6 102 1.9 75 - 125 309.4 11.1
NC NCZinc BRL NC99.256.9 95.6 3.7 r75 - 125 30117 210
m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.
Page 1 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
QA/QC ReportApril 15, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG29068
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
QA/QC Batch 270774, QC Sample No: BG28598 (BG29068, BG29069, BG29071, BG29073)
Pesticides - Solid101 1074,4' -DDD ND 5.8107 92 15.1 40 - 140 30
85 984,4' -DDE ND 14.2100 86 15.1 40 - 140 30
102 1094,4' -DDT ND 6.6106 91 15.2 40 - 140 30
96 102a-BHC ND 6.197 84 14.4 40 - 140 30
96 100a-Chlordane ND 4.1102 89 13.6 40 - 140 30
87 89Aldrin ND 2.397 84 14.4 40 - 140 30
96 106b-BHC ND 9.998 87 11.9 40 - 140 30
NA NAChlordane ND NCNA NA NC 40 - 140 30
74 80d-BHC ND 7.875 65 14.3 40 - 140 30
87 96Dieldrin ND 9.898 84 15.4 40 - 140 30
100 105Endosulfan I ND 4.9101 90 11.5 40 - 140 30
100 105Endosulfan II ND 4.971 80 11.9 40 - 140 30
83 96Endosulfan sulfate ND 14.585 76 11.2 40 - 140 30
101 110Endrin ND 8.5102 90 12.5 40 - 140 30
85 101Endrin aldehyde ND 17.278 79 1.3 40 - 140 30
100 107Endrin ketone ND 6.8102 90 12.5 40 - 140 30
100 108g-BHC ND 7.7101 88 13.8 40 - 140 30
93 97g-Chlordane ND 4.299 86 14.1 40 - 140 30
94 96Heptachlor ND 2.1101 88 13.8 40 - 140 30
97 105Heptachlor epoxide ND 7.9101 88 13.8 40 - 140 30
104 111Methoxychlor ND 6.5111 98 12.4 40 - 140 30
NA NAToxaphene ND NCNA NA NC 40 - 140 30
90 98% DCBP 104 8.597 83 15.6 30 - 150 30
87 90% TCMX 94 3.493 78 17.5 30 - 150 30
Alpha and gamma chlordane were spiked and analyzed instead of technical chlordane. Gamma chlordane recovery is reported in theLCS, LCSD, MS and MSD.
Comment:
QA/QC Batch 270799, QC Sample No: BG29065 (BG29068, BG29069, BG29070, BG29071, BG29072, BG29073)
Semivolatiles - Solid81 821,2,4,5-Tetrachlorobenzene ND 1.274 75 1.3 30 - 130 30
79 781,2,4-Trichlorobenzene ND 1.372 73 1.4 30 - 130 30
82 811,2-Dichlorobenzene ND 1.275 75 0.0 30 - 130 30
86 921,2-Diphenylhydrazine ND 6.785 83 2.4 30 - 130 30
81 801,3-Dichlorobenzene ND 1.275 75 0.0 30 - 130 30
81 801,4-Dichlorobenzene ND 1.275 75 0.0 30 - 130 30
97 972,4,5-Trichlorophenol ND 0.084 82 2.4 30 - 130 30
96 942,4,6-Trichlorophenol ND 2.177 77 0.0 30 - 130 30
87 882,4-Dichlorophenol ND 1.180 79 1.3 30 - 130 30
54 542,4-Dimethylphenol ND 0.048 48 0.0 30 - 130 30
2.8 3.02,4-Dinitrophenol ND 6.9<10 <10 NC l,m30 - 130 30
90 922,4-Dinitrotoluene ND 2.282 82 0.0 30 - 130 30
Page 2 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG29068
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
90 912,6-Dinitrotoluene ND 1.182 83 1.2 30 - 130 30
89 892-Chloronaphthalene ND 0.082 80 2.5 30 - 130 30
88 862-Chlorophenol ND 2.379 78 1.3 30 - 130 30
84 852-Methylnaphthalene ND 1.277 78 1.3 30 - 130 30
81 812-Methylphenol (o-cresol) ND 0.075 71 5.5 30 - 130 30
108 1192-Nitroaniline ND 9.7105 104 1.0 30 - 130 30
83 862-Nitrophenol ND 3.668 67 1.5 30 - 130 30
87 863&4-Methylphenol (m&p-cresol) ND 1.279 77 2.6 30 - 130 30
101 1053,3'-Dichlorobenzidine ND 3.9116 115 0.9 30 - 130 30
89 893-Nitroaniline ND 0.089 89 0.0 30 - 130 30
78 844,6-Dinitro-2-methylphenol ND 7.422 23 4.4 l30 - 130 30
88 904-Bromophenyl phenyl ether ND 2.280 81 1.2 30 - 130 30
91 924-Chloro-3-methylphenol ND 1.184 83 1.2 30 - 130 30
56 544-Chloroaniline ND 3.662 59 5.0 30 - 130 30
86 884-Chlorophenyl phenyl ether ND 2.380 80 0.0 30 - 130 30
96 984-Nitroaniline ND 2.189 84 5.8 30 - 130 30
107 1084-Nitrophenol ND 0.992 90 2.2 30 - 130 30
83 83Acenaphthene ND 0.076 76 0.0 30 - 130 30
87 86Acenaphthylene ND 1.279 79 0.0 30 - 130 30
86 87Acetophenone ND 1.280 78 2.5 30 - 130 30
79 78Aniline ND 1.380 77 3.8 30 - 130 30
91 91Anthracene ND 0.082 82 0.0 30 - 130 30
91 92Benz(a)anthracene ND 1.182 83 1.2 30 - 130 30
141 136Benzidine ND 3.6>200 >200 NC l,m30 - 130 30
80 82Benzo(a)pyrene ND 2.573 73 0.0 30 - 130 30
88 88Benzo(b)fluoranthene ND 0.082 76 7.6 30 - 130 30
92 95Benzo(ghi)perylene ND 3.285 84 1.2 30 - 130 30
91 88Benzo(k)fluoranthene ND 3.478 83 6.2 30 - 130 30
95 93Benzyl butyl phthalate ND 2.186 86 0.0 30 - 130 30
82 82Bis(2-chloroethoxy)methane ND 0.076 75 1.3 30 - 130 30
81 80Bis(2-chloroethyl)ether ND 1.274 71 4.1 30 - 130 30
84 84Bis(2-chloroisopropyl)ether ND 0.079 76 3.9 30 - 130 30
93 94Bis(2-ethylhexyl)phthalate ND 1.184 84 0.0 30 - 130 30
100 98Carbazole ND 2.087 88 1.1 30 - 130 30
90 91Chrysene ND 1.181 82 1.2 30 - 130 30
93 96Dibenz(a,h)anthracene ND 3.285 84 1.2 30 - 130 30
88 88Dibenzofuran ND 0.080 81 1.2 30 - 130 30
90 90Diethyl phthalate ND 0.082 83 1.2 30 - 130 30
88 87Dimethylphthalate ND 1.180 80 0.0 30 - 130 30
89 88Di-n-butylphthalate ND 1.182 82 0.0 30 - 130 30
88 89Di-n-octylphthalate ND 1.181 79 2.5 30 - 130 30
94 92Fluoranthene ND 2.284 86 2.4 30 - 130 30
87 90Fluorene ND 3.482 82 0.0 30 - 130 30
85 88Hexachlorobenzene ND 3.580 80 0.0 30 - 130 30
77 77Hexachlorobutadiene ND 0.070 72 2.8 30 - 130 30
64 65Hexachlorocyclopentadiene ND 1.663 64 1.6 30 - 130 30
80 80Hexachloroethane ND 0.074 73 1.4 30 - 130 30
92 96Indeno(1,2,3-cd)pyrene ND 4.384 83 1.2 30 - 130 30
88 88Isophorone ND 0.081 80 1.2 30 - 130 30
82 82Naphthalene ND 0.075 75 0.0 30 - 130 30
84 84Nitrobenzene ND 0.078 76 2.6 30 - 130 30
74 73N-Nitrosodimethylamine ND 1.471 70 1.4 30 - 130 30
86 87N-Nitrosodi-n-propylamine ND 1.280 77 3.8 30 - 130 30
Page 3 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG29068
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
91 93N-Nitrosodiphenylamine ND 2.286 86 0.0 30 - 130 30
88 92Pentachloronitrobenzene ND 4.480 83 3.7 30 - 130 30
96 96Pentachlorophenol ND 0.039 40 2.5 30 - 130 30
91 91Phenanthrene ND 0.082 83 1.2 30 - 130 30
90 90Phenol ND 0.083 80 3.7 30 - 130 30
96 95Pyrene ND 1.085 87 2.3 30 - 130 30
66 65Pyridine ND 1.568 66 3.0 30 - 130 30
87 96% 2,4,6-Tribromophenol 63 9.878 76 2.6 30 - 130 30
55 54% 2-Fluorobiphenyl 54 1.849 48 2.1 30 - 130 30
80 79% 2-Fluorophenol 77 1.370 69 1.4 30 - 130 30
54 54% Nitrobenzene-d5 53 0.049 48 2.1 30 - 130 30
83 83% Phenol-d5 81 0.075 73 2.7 30 - 130 30
67 66% Terphenyl-d14 60 1.558 60 3.4 30 - 130 30
Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)
Comment:
QA/QC Batch 270809, QC Sample No: BG29071 (BG29068, BG29069, BG29071, BG29073)
Polychlorinated Biphenyls - Solid100 94PCB-1016 ND 6.2102 99 3.0 40 - 140 30
PCB-1221 ND 40 - 140 30
PCB-1232 ND 40 - 140 30
PCB-1242 ND 40 - 140 30
PCB-1248 ND 40 - 140 30
PCB-1254 ND 40 - 140 30
102 96PCB-1260 ND 6.198 95 3.1 40 - 140 30
PCB-1262 ND 40 - 140 30
PCB-1268 ND 40 - 140 30
106 99% DCBP (Surrogate Rec) 81 6.8101 96 5.1 30 - 150 30
102 96% TCMX (Surrogate Rec) 74 6.1105 102 2.9 30 - 150 30
QA/QC Batch 271316, QC Sample No: BG29076 (BG29068, BG29069)
Volatiles - Solid97 971,1,1,2-Tetrachloroethane ND 0.098 95 3.1 70 - 130 30
95 961,1,1-Trichloroethane ND 1.096 92 4.3 70 - 130 30
97 1001,1,2,2-Tetrachloroethane ND 3.094 90 4.3 70 - 130 30
94 951,1,2-Trichloroethane ND 1.199 95 4.1 70 - 130 30
93 961,1-Dichloroethane ND 3.293 89 4.4 70 - 130 30
92 911,1-Dichloroethene ND 1.188 88 0.0 70 - 130 30
94 971,1-Dichloropropene ND 3.199 93 6.3 70 - 130 30
91 911,2,3-Trichlorobenzene ND 0.098 94 4.2 70 - 130 30
101 971,2,3-Trichloropropane ND 4.097 92 5.3 70 - 130 30
92 891,2,4-Trichlorobenzene ND 3.398 91 7.4 70 - 130 30
100 991,2,4-Trimethylbenzene ND 1.0105 100 4.9 70 - 130 30
95 961,2-Dibromo-3-chloropropane ND 1.0101 93 8.2 70 - 130 30
96 991,2-Dibromoethane ND 3.1102 101 1.0 70 - 130 30
96 951,2-Dichlorobenzene ND 1.096 93 3.2 70 - 130 30
96 1001,2-Dichloroethane ND 4.1100 96 4.1 70 - 130 30
99 1001,2-Dichloropropane ND 1.098 95 3.1 70 - 130 30
100 981,3,5-Trimethylbenzene ND 2.099 96 3.1 70 - 130 30
97 971,3-Dichlorobenzene ND 0.098 92 6.3 70 - 130 30
96 991,3-Dichloropropane ND 3.1100 93 7.3 70 - 130 30
95 951,4-Dichlorobenzene ND 0.096 90 6.5 70 - 130 30
89 902,2-Dichloropropane ND 1.198 91 7.4 70 - 130 30
Page 4 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG29068
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
99 992-Chlorotoluene ND 0.097 90 7.5 70 - 130 30
119 1102-Hexanone ND 7.9131 118 10.4 l70 - 130 30
103 1032-Isopropyltoluene ND 0.0103 98 5.0 70 - 130 30
97 934-Chlorotoluene ND 4.299 94 5.2 70 - 130 30
101 1014-Methyl-2-pentanone ND 0.0133 129 3.1 l70 - 130 30
67 63Acetone ND 6.291 85 6.8 m70 - 130 30
95 96Acrylonitrile ND 1.094 98 4.2 70 - 130 30
98 99Benzene ND 1.099 93 6.3 70 - 130 30
100 100Bromobenzene ND 0.099 92 7.3 70 - 130 30
94 96Bromochloromethane ND 2.196 92 4.3 70 - 130 30
95 99Bromodichloromethane ND 4.199 94 5.2 70 - 130 30
98 104Bromoform ND 5.9101 99 2.0 70 - 130 30
100 104Bromomethane ND 3.995 85 11.1 70 - 130 30
93 96Carbon Disulfide ND 3.290 87 3.4 70 - 130 30
94 96Carbon tetrachloride ND 2.199 93 6.3 70 - 130 30
94 97Chlorobenzene ND 3.1100 93 7.3 70 - 130 30
90 92Chloroethane ND 2.295 91 4.3 70 - 130 30
95 97Chloroform ND 2.196 91 5.3 70 - 130 30
87 89Chloromethane ND 2.395 89 6.5 70 - 130 30
97 94cis-1,2-Dichloroethene ND 3.199 93 6.3 70 - 130 30
98 96cis-1,3-Dichloropropene ND 2.199 98 1.0 70 - 130 30
94 99Dibromochloromethane ND 5.2100 92 8.3 70 - 130 30
97 96Dibromomethane ND 1.0100 98 2.0 70 - 130 30
85 85Dichlorodifluoromethane ND 0.095 90 5.4 70 - 130 30
93 99Ethylbenzene ND 6.396 90 6.5 70 - 130 30
91 94Hexachlorobutadiene ND 3.295 87 8.8 70 - 130 30
102 103Isopropylbenzene ND 1.0102 96 6.1 70 - 130 30
95 100m&p-Xylene ND 5.199 93 6.3 70 - 130 30
90 89Methyl ethyl ketone ND 1.1121 117 3.4 70 - 130 30
102 103Methyl t-butyl ether (MTBE) ND 1.097 93 4.2 70 - 130 30
85 86Methylene chloride ND 1.290 85 5.7 70 - 130 30
100 99Naphthalene ND 1.0103 99 4.0 70 - 130 30
97 97n-Butylbenzene ND 0.0102 94 8.2 70 - 130 30
98 98n-Propylbenzene ND 0.0104 99 4.9 70 - 130 30
103 106o-Xylene ND 2.998 90 8.5 70 - 130 30
100 99p-Isopropyltoluene ND 1.0100 96 4.1 70 - 130 30
98 96sec-Butylbenzene ND 2.197 90 7.5 70 - 130 30
99 104Styrene ND 4.9103 94 9.1 70 - 130 30
101 98tert-Butylbenzene ND 3.0101 95 6.1 70 - 130 30
95 97Tetrachloroethene ND 2.194 90 4.3 70 - 130 30
99 99Tetrahydrofuran (THF) ND 0.0100 95 5.1 70 - 130 30
94 99Toluene ND 5.299 97 2.0 70 - 130 30
91 93trans-1,2-Dichloroethene ND 2.289 86 3.4 70 - 130 30
95 101trans-1,3-Dichloropropene ND 6.1103 97 6.0 70 - 130 30
101 98trans-1,4-dichloro-2-butene ND 3.0105 101 3.9 70 - 130 30
96 100Trichloroethene ND 4.199 95 4.1 70 - 130 30
90 91Trichlorofluoromethane ND 1.194 88 6.6 70 - 130 30
95 97Trichlorotrifluoroethane ND 2.195 91 4.3 70 - 130 30
89 89Vinyl chloride ND 0.094 89 5.5 70 - 130 30
104 97% 1,2-dichlorobenzene-d4 102 7.0100 101 1.0 70 - 130 30
99 99% Bromofluorobenzene 96 0.0101 98 3.0 70 - 130 30
101 100% Dibromofluoromethane 100 1.0104 100 3.9 70 - 130 30
99 101% Toluene-d8 102 2.0100 101 1.0 70 - 130 30
Page 5 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG29068
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.
Comment:
QA/QC Batch 271311, QC Sample No: BG29079 (BG29070, BG29071, BG29072 (50, 1X) , BG29073 (63, 1X) , BG29074 (50X) , BG29075)
Volatiles - Solid98 971,1,1,2-Tetrachloroethane ND 1.092 98 6.3 70 - 130 30
101 981,1,1-Trichloroethane ND 3.089 93 4.4 70 - 130 30
93 951,1,2,2-Tetrachloroethane ND 2.183 91 9.2 70 - 130 30
94 971,1,2-Trichloroethane ND 3.191 98 7.4 70 - 130 30
98 961,1-Dichloroethane ND 2.189 97 8.6 70 - 130 30
105 1021,1-Dichloroethene ND 2.992 94 2.2 70 - 130 30
100 961,1-Dichloropropene ND 4.189 93 4.4 70 - 130 30
93 791,2,3-Trichlorobenzene ND 16.398 91 7.4 70 - 130 30
97 1031,2,3-Trichloropropane ND 6.090 99 9.5 70 - 130 30
88 761,2,4-Trichlorobenzene ND 14.695 90 5.4 70 - 130 30
95 921,2,4-Trimethylbenzene ND 3.295 97 2.1 70 - 130 30
88 861,2-Dibromo-3-chloropropane ND 2.388 92 4.4 70 - 130 30
95 971,2-Dibromoethane ND 2.190 98 8.5 70 - 130 30
94 911,2-Dichlorobenzene ND 3.291 94 3.2 70 - 130 30
96 961,2-Dichloroethane ND 0.091 96 5.3 70 - 130 30
95 951,2-Dichloropropane ND 0.092 97 5.3 70 - 130 30
98 951,3,5-Trimethylbenzene ND 3.192 95 3.2 70 - 130 30
94 901,3-Dichlorobenzene ND 4.391 94 3.2 70 - 130 30
95 941,3-Dichloropropane ND 1.191 97 6.4 70 - 130 30
92 881,4-Dichlorobenzene ND 4.491 93 2.2 70 - 130 30
94 892,2-Dichloropropane ND 5.590 94 4.3 70 - 130 30
96 942-Chlorotoluene ND 2.190 94 4.3 70 - 130 30
76 762-Hexanone ND 0.098 107 8.8 70 - 130 30
99 962-Isopropyltoluene ND 3.192 94 2.2 70 - 130 30
95 924-Chlorotoluene ND 3.293 97 4.2 70 - 130 30
89 894-Methyl-2-pentanone ND 0.0102 114 11.1 70 - 130 30
82 81Acetone ND 1.2126 109 14.5 70 - 130 30
88 91Acrylonitrile ND 3.483 94 12.4 70 - 130 30
97 96Benzene ND 1.090 93 3.3 70 - 130 30
97 95Bromobenzene ND 2.192 94 2.2 70 - 130 30
97 96Bromochloromethane ND 1.090 96 6.5 70 - 130 30
96 96Bromodichloromethane ND 0.089 95 6.5 70 - 130 30
88 92Bromoform ND 4.489 97 8.6 70 - 130 30
110 88Bromomethane ND 22.2108 91 17.1 70 - 130 30
99 94Carbon Disulfide ND 5.290 94 4.3 70 - 130 30
98 96Carbon tetrachloride ND 2.190 95 5.4 70 - 130 30
97 95Chlorobenzene ND 2.191 95 4.3 70 - 130 30
96 100Chloroethane ND 4.196 102 6.1 70 - 130 30
99 98Chloroform ND 1.090 95 5.4 70 - 130 30
89 85Chloromethane ND 4.697 100 3.0 70 - 130 30
98 97cis-1,2-Dichloroethene ND 1.090 94 4.3 70 - 130 30
91 91cis-1,3-Dichloropropene ND 0.088 93 5.5 70 - 130 30
91 94Dibromochloromethane ND 3.292 98 6.3 70 - 130 30
93 94Dibromomethane ND 1.189 96 7.6 70 - 130 30
81 78Dichlorodifluoromethane ND 3.899 103 4.0 70 - 130 30
99 97Ethylbenzene ND 2.090 93 3.3 70 - 130 30
99 89Hexachlorobutadiene ND 10.696 94 2.1 70 - 130 30
Page 6 of 7
QA/QC Data
Parameter BlankMS%
MSD%
MSRPD
SDG I.D.: GBG29068
LCS%
LCSD%
LCSRPD
%Rec
Limits
%RPD
Limits
99 97Isopropylbenzene ND 2.092 94 2.2 70 - 130 30
98 95m&p-Xylene ND 3.190 94 4.3 70 - 130 30
80 81Methyl ethyl ketone ND 1.2101 116 13.8 70 - 130 30
99 100Methyl t-butyl ether (MTBE) ND 1.087 93 6.7 70 - 130 30
97 96Methylene chloride ND 1.092 98 6.3 70 - 130 30
94 80Naphthalene ND 16.194 88 6.6 70 - 130 30
94 88n-Butylbenzene ND 6.694 95 1.1 70 - 130 30
98 94n-Propylbenzene ND 4.297 100 3.0 70 - 130 30
98 96o-Xylene ND 2.191 95 4.3 70 - 130 30
97 93p-Isopropyltoluene ND 4.293 96 3.2 70 - 130 30
99 95sec-Butylbenzene ND 4.189 92 3.3 70 - 130 30
95 94Styrene ND 1.194 96 2.1 70 - 130 30
100 98tert-Butylbenzene ND 2.091 95 4.3 70 - 130 30
100 94Tetrachloroethene ND 6.292 95 3.2 70 - 130 30
88 90Tetrahydrofuran (THF) ND 2.282 91 10.4 70 - 130 30
98 95Toluene ND 3.190 94 4.3 70 - 130 30
104 100trans-1,2-Dichloroethene ND 3.992 96 4.3 70 - 130 30
91 92trans-1,3-Dichloropropene ND 1.188 94 6.6 70 - 130 30
81 86trans-1,4-dichloro-2-butene ND 6.089 93 4.4 70 - 130 30
100 98Trichloroethene ND 2.093 97 4.2 70 - 130 30
106 105Trichlorofluoromethane ND 0.996 103 7.0 70 - 130 30
105 98Trichlorotrifluoroethane ND 6.998 102 4.0 70 - 130 30
96 94Vinyl chloride ND 2.195 99 4.1 70 - 130 30
100 99% 1,2-dichlorobenzene-d4 99 1.0100 99 1.0 70 - 130 30
96 97% Bromofluorobenzene 97 1.099 99 0.0 70 - 130 30
101 103% Dibromofluoromethane 100 2.0100 102 2.0 70 - 130 30
99 99% Toluene-d8 99 0.099 100 1.0 70 - 130 30
Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.
Comment:
QA/QC Batch 271482, QC Sample No: BG30788 (BG29068 (63X) )
Volatiles - Solid105 102Naphthalene ND 2.9100 105 4.9 70 - 130 30
Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.
Comment:
l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.
MS - Matrix SpikePhyllis Shiller, Laboratory Director
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.
April 15, 2014MS Dup - Matrix Spike Duplicate
RPD - Relative Percent Difference
LCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate
NC - No Criteria
Intf - Interference
Page 7 of 7
Sample Criteria Exceedences ReportTuesday, April 15, 2014 Page 1 of 3
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG29068 - EBCCriteria: NY: 375, 375RRS, 375RS
RLCriteria
State: NY
$8270SMRDP Phenol 330ND 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benz(a)anthracene 10004800 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10004800 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10004800 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10004200 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 39004200 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Chrysene 10004200 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10005000 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10005000 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10005000 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 10001500 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(k)fluoranthene 8001500 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10003700 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10003700 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10003700 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5001400 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 5001400 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 5001400 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 330ND 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Dibenz(a,h)anthracene 330ND 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Dibenz(a,h)anthracene 330ND 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330CU-SM Copper 50153 3.9 mg/kgBG29068 NY / 375-6.8 Metals / Unrestricted Use Soil 50PB-SMDP Lead 63167 7.7 mg/KgBG29068 NY / 375-6.8 Metals / Unrestricted Use Soil 63
PB-SMDP Lead 63108 0.7 mg/KgBG29069 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SMDP Zinc 109116 0.7 mg/KgBG29069 NY / 375-6.8 Metals / Unrestricted Use Soil 109
$8270SMRDP Phenol 330ND 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benz(a)anthracene 10001400 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10001400 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10001400 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10001300 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 10001300 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10001800 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10001800 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10001800 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(a)pyrene 10001200 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10001200 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10001200 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Dibenz(a,h)anthracene 330ND 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential 330
Sample Criteria Exceedences ReportTuesday, April 15, 2014 Page 2 of 3
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG29068 - EBCCriteria: NY: 375, 375RRS, 375RS
RLCriteria
State: NY
$8270SMRDP Dibenz(a,h)anthracene 330ND 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Dibenz(a,h)anthracene 330ND 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330CU-SM Copper 5057.0 0.35 mg/kgBG29071 NY / 375-6.8 Metals / Unrestricted Use Soil 50HG-SM Mercury 0.180.28 0.06 mg/KgBG29071 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 63166 7.0 mg/KgBG29071 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SMDP Zinc 109121 0.7 mg/KgBG29071 NY / 375-6.8 Metals / Unrestricted Use Soil 109
$8270SMRDP Benz(a)anthracene 10009300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10009300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10009300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10008600 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 39008600 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Chrysene 10008600 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 100011000 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 100011000 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 100011000 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 10003700 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(k)fluoranthene 8003700 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10008300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10008300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10008300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5003400 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 5003400 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 5003400 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500AS-SM Arsenic 16137 0.8 mg/KgBG29072 NY / 375-6.8 Metals / Residential 16AS-SM Arsenic 16137 0.8 mg/KgBG29072 NY / 375-6.8 Metals / Residential Restricted 16AS-SM Arsenic 13137 0.8 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 13CD-SM Cadmium 2.58.19 0.42 mg/KgBG29072 NY / 375-6.8 Metals / Residential 2.5CD-SM Cadmium 4.38.19 0.42 mg/KgBG29072 NY / 375-6.8 Metals / Residential Restricted 4.3CD-SM Cadmium 2.58.19 0.42 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 2.5CU-SM Copper 50185 4.2 mg/kgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 50HG-SM Mercury 0.180.23 0.10 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18NI-SM Nickel 3039.6 0.42 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 30PB-SMDP Lead 63308 8.3 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SMDP Zinc 1091480 8.3 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 109
$8270SMRDP Benz(a)anthracene 10003300 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10003300 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10003300 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10002800 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 10002800 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10003700 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000
Sample Criteria Exceedences ReportTuesday, April 15, 2014 Page 3 of 3
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG29068 - EBCCriteria: NY: 375, 375RRS, 375RS
RLCriteria
State: NY
$8270SMRDP Benzo(b)fluoranthene 10003700 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10003700 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 10001200 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(k)fluoranthene 8001200 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10002500 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10002500 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10002500 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500890 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500890 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500890 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500CU-SM Copper 5051.2 0.36 mg/kgBG29073 NY / 375-6.8 Metals / Unrestricted Use Soil 50PB-SMDP Lead 63156 7.2 mg/KgBG29073 NY / 375-6.8 Metals / Unrestricted Use Soil 63
$8260-SMDPR Vinyl chloride 210ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Residential 210$8260-SMDPR Vinyl chloride 20ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR 1,2-Dichloroethane 20ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Acetone 50ND 2500 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR Benzene 60ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260-SMDPR Methyl Ethyl Ketone 120ND 1500 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260-SMDPR Methylene chloride 50ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR trans-1,2-Dichloroethene 190ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 190
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.
NY Temperature NarrationApril 15, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG29068
The samples in this delivery group were received at 4°C.(Note acceptance criteria is above freezing up to 6°C)
Page 1 of 1
BG34092
Tuesday, April 22, 2014
Sample ID#s:
Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Project ID: DOMINO SUGAR SITE E
Sincerely yours,
Laboratory DirectorPhyllis Shiller
If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.
NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B
NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301
This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.
This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.
A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.
587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823
Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:
Collected by:Received by:Analyzed by:
AIREBC72 Hour
04/17/14SWsee "By" below
DM
Laboratory Data
E-SG1
Phoenix ID: BG34092
04/17/1411:1217:15
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406
Analysis ReportApril 22, 2014
Date Time
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG ID: GBG34092
Client ID:Project ID: DOMINO SUGAR SITE E
ug/m3RL
Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 04/18/14 KCA TO15ND 11.000.581,1,1-Trichloroethane 0.183 04/18/14 KCA TO153.16 1.00ND1,1,2,2-Tetrachloroethane 0.146 04/18/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 04/18/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 04/18/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 04/18/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 04/18/14 KCA TO15ND 1.00ND1,2,4-Trimethylbenzene 0.204 04/18/14 KCA TO15ND 1.00ND1,2-Dibromoethane(EDB) 0.130 04/18/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 04/18/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 04/18/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 04/18/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 04/18/14 KCA TO15ND 1.00ND1,3,5-Trimethylbenzene 0.204 04/18/14 KCA TO15ND 1.00ND1,3-Butadiene 0.452 04/18/14 KCA TO15ND 1.00ND1,3-Dichlorobenzene 0.166 04/18/14 KCA TO15ND 1.00ND1,4-Dichlorobenzene 0.166 04/18/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 04/18/14 KCA TO15ND 1.001.292-Hexanone(MBK) 0.244 04/18/14 KCA TO155.28 11.00ND4-Ethyltoluene 0.204 04/18/14 KCA TO15ND 11.00ND4-Isopropyltoluene 0.182 04/18/14 KCA TO15ND 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 04/18/14 KCA TO15ND 1.00107Acetone 0.421 04/18/14 KCA TO15254 1.00NDAcrylonitrile 0.461 04/18/14 KCA TO15ND 1.00NDBenzene 0.313 04/18/14 KCA TO15ND 1.00NDBenzyl chloride 0.193 04/18/14 KCA TO15ND 1.00
Page 1 of 3 Ver 1
E-SG1Phoenix I.D.: BG34092
Client ID:DOMINO SUGAR SITE EProject ID:
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
ug/m3RL
NDBromodichloromethane 0.149 04/18/14 KCA TO15ND 1.00NDBromoform 0.097 04/18/14 KCA TO15ND 1.00NDBromomethane 0.258 04/18/14 KCA TO15ND 1.00NDCarbon Disulfide 0.321 04/18/14 KCA TO15ND 1.000.06Carbon Tetrachloride 0.040 04/18/14 KCA TO150.377 0.25NDChlorobenzene 0.217 04/18/14 KCA TO15ND 1.00NDChloroethane 0.379 04/18/14 KCA TO15ND 1.000.78Chloroform 0.205 04/18/14 KCA TO153.81 1.00NDChloromethane 0.484 04/18/14 KCA TO15ND 1.000.67Cis-1,2-Dichloroethene 0.252 04/18/14 KCA TO152.65 1.00NDcis-1,3-Dichloropropene 0.220 04/18/14 KCA TO15ND 1.00NDCyclohexane 0.291 04/18/14 KCA TO15ND 1.00NDDibromochloromethane 0.117 04/18/14 KCA TO15ND 1.000.33Dichlorodifluoromethane 0.202 04/18/14 KCA TO151.63 1.004.99Ethanol 0.531 04/18/14 KCA TO159.40 11.00NDEthyl acetate 0.278 04/18/14 KCA TO15ND 11.00NDEthylbenzene 0.230 04/18/14 KCA TO15ND 1.000.28Heptane 0.244 04/18/14 KCA TO151.15 1.00NDHexachlorobutadiene 0.094 04/18/14 KCA TO15ND 1.00NDHexane 0.284 04/18/14 KCA TO15ND 1.001.98Isopropylalcohol 0.407 04/18/14 KCA TO154.86 1.00NDIsopropylbenzene 0.204 04/18/14 KCA TO15ND 1.000.24m,p-Xylene 0.230 04/18/14 KCA TO151.04 1.006.74Methyl Ethyl Ketone 0.339 04/18/14 KCA TO1519.9 1.00NDMethyl tert-butyl ether(MTBE) 0.278 04/18/14 KCA TO15ND 1.000.46Methylene Chloride 0.288 04/18/14 KCA TO151.60 1.00NDn-Butylbenzene 0.182 04/18/14 KCA TO15ND 11.00NDo-Xylene 0.230 04/18/14 KCA TO15ND 1.003.03Propylene 0.581 04/18/14 KCA TO155.21 11.00NDsec-Butylbenzene 0.182 04/18/14 KCA TO15ND 11.00NDStyrene 0.235 04/18/14 KCA TO15ND 1.000.3Tetrachloroethene 0.037 04/18/14 KCA TO152.03 0.25NDTetrahydrofuran 0.339 04/18/14 KCA TO15ND 11.000.48Toluene 0.266 04/18/14 KCA TO151.81 1.00NDTrans-1,2-Dichloroethene 0.252 04/18/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 04/18/14 KCA TO15ND 1.004.49Trichloroethene 0.047 04/18/14 KCA TO1524.1 0.250.24Trichlorofluoromethane 0.178 04/18/14 KCA TO151.35 1.00NDTrichlorotrifluoroethane 0.130 04/18/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 04/18/14 KCA TO15ND 0.25
QA/QC Surrogates108% Bromofluorobenzene % 04/18/14 KCA TO15108 %
Page 2 of 3 Ver 1
E-SG1Phoenix I.D.: BG34092
Client ID:DOMINO SUGAR SITE EProject ID:
Parameterppbv
ResultppbvRL
ug/m3Result Date/Time By Reference
ug/m3RL
Comments:
Phyllis Shiller, Laboratory DirectorApril 22, 2014
1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.
Reviewed and Released by: Greg Lawrence, Assistant Lab Director
RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level
Page 3 of 3 Ver 1
QA/QC Data
ParameterBlankppbv
SampleResultppbv
SampleDupppbv
DUPRPD
QA/QC ReportApril 22, 2014
587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823
Environmental Laboratories, Inc.
SDG I.D.: GBG34092
LCS%
SampleResultug/m3
SampleDup
ug/m3
%Rec
Limits
%RPD
LimitsBlankug/m3
QA/QC Batch 272020, QC Sample No: BG34092 (BG34092)
VolatilesND ND1,1,1,2-Tetrachloroethane ND NC110 ND ND 70 - 130 20ND
0.58 0.481,1,1-Trichloroethane ND 18.9101 3.16 2.62 70 - 130 20ND
ND ND1,1,2,2-Tetrachloroethane ND NC104 ND ND 70 - 130 20ND
ND ND1,1,2-Trichloroethane ND NC102 ND ND 70 - 130 20ND
ND ND1,1-Dichloroethane ND NC97 ND ND 70 - 130 20ND
ND ND1,1-Dichloroethene ND NC94 ND ND 70 - 130 20ND
ND ND1,2,4-Trichlorobenzene ND NC109 ND ND 70 - 130 20ND
ND ND1,2,4-Trimethylbenzene ND NC107 ND ND 70 - 130 20ND
ND ND1,2-Dibromoethane(EDB) ND NC104 ND ND 70 - 130 20ND
ND ND1,2-Dichlorobenzene ND NC108 ND ND 70 - 130 20ND
ND ND1,2-Dichloroethane ND NC100 ND ND 70 - 130 20ND
ND ND1,2-dichloropropane ND NC101 ND ND 70 - 130 20ND
ND ND1,2-Dichlorotetrafluoroethane ND NC114 ND ND 70 - 130 20ND
ND ND1,3,5-Trimethylbenzene ND NC105 ND ND 70 - 130 20ND
ND ND1,3-Butadiene ND NC99 ND ND 70 - 130 20ND
ND ND1,3-Dichlorobenzene ND NC110 ND ND 70 - 130 20ND
ND ND1,4-Dichlorobenzene ND NC109 ND ND 70 - 130 20ND
ND ND1,4-Dioxane ND NC104 ND ND 70 - 130 20ND
1.29 1.022-Hexanone(MBK) ND 23.4104 5.28 4.18 70 - 130 20ND
ND ND4-Ethyltoluene ND NC105 ND ND 70 - 130 20ND
ND ND4-Isopropyltoluene ND NC107 ND ND 70 - 130 20ND
ND ND4-Methyl-2-pentanone(MIBK) ND NC103 ND ND 70 - 130 20ND
111 83.3Acetone ND 28.596 264 198 70 - 130 20ND
ND NDAcrylonitrile ND NC98 ND ND 70 - 130 20ND
ND NDBenzene ND NC102 ND ND 70 - 130 20ND
ND NDBenzyl chloride ND NC124 ND ND 70 - 130 20ND
ND NDBromodichloromethane ND NC101 ND ND 70 - 130 20ND
ND NDBromoform ND NC115 ND ND 70 - 130 20ND
ND NDBromomethane ND NC96 ND ND 70 - 130 20ND
ND NDCarbon Disulfide ND NC97 ND ND 70 - 130 20ND
0.06 0.05Carbon Tetrachloride ND 18.2104 0.377 0.314 70 - 130 20ND
ND NDChlorobenzene ND NC99 ND ND 70 - 130 20ND
ND NDChloroethane ND NC95 ND ND 70 - 130 20ND
0.78 0.7Chloroform ND 10.888 3.81 3.42 70 - 130 20ND
ND NDChloromethane ND NC95 ND ND 70 - 130 20ND
0.67 0.55Cis-1,2-Dichloroethene ND 19.798 2.65 2.18 70 - 130 20ND
ND NDcis-1,3-Dichloropropene ND NC102 ND ND 70 - 130 20ND
ND NDCyclohexane ND NC102 ND ND 70 - 130 20ND
ND NDDibromochloromethane ND NC109 ND ND 70 - 130 20ND
0.33 0.38Dichlorodifluoromethane ND 14.1104 1.63 1.88 70 - 130 20ND
4.99 4.74Ethanol ND 5.191 9.40 8.92 70 - 130 20ND
Page 1 of 2
QA/QC Data
ParameterBlankppbv
SampleResultppbv
SampleDupppbv
DUPRPD
SDG I.D.: GBG34092
LCS%
SampleResultug/m3
SampleDup
ug/m3
%Rec
Limits
%RPD
LimitsBlankug/m3
ND NDEthyl acetate ND NC102 ND ND 70 - 130 20ND
ND NDEthylbenzene ND NC105 ND ND 70 - 130 20ND
0.28 0.31Heptane ND 10.297 1.15 1.27 70 - 130 20ND
ND NDHexachlorobutadiene ND NC88 ND ND 70 - 130 20ND
ND NDHexane ND NC87 ND ND 70 - 130 20ND
1.98 1.5Isopropylalcohol ND 27.6101 4.86 3.68 70 - 130 20ND
ND NDIsopropylbenzene ND NC106 ND ND 70 - 130 20ND
0.24 NDm,p-Xylene ND NC106 1.04 ND 70 - 130 20ND
6.74 5.31Methyl Ethyl Ketone ND 23.7100 19.9 15.6 70 - 130 20ND
ND NDMethyl tert-butyl ether(MTBE) ND NC103 ND ND 70 - 130 20ND
0.46 0.29Methylene Chloride ND 45.386 1.60 1.01 70 - 130 20ND
ND NDn-Butylbenzene ND NC113 ND ND 70 - 130 20ND
ND NDo-Xylene ND NC105 ND ND 70 - 130 20ND
3.03 2.08Propylene ND 37.2105 5.21 3.58 70 - 130 20ND
ND NDsec-Butylbenzene ND NC106 ND ND 70 - 130 20ND
ND NDStyrene ND NC108 ND ND 70 - 130 20ND
0.3 0.24Tetrachloroethene ND 22.2103 2.03 1.63 70 - 130 20ND
ND NDTetrahydrofuran ND NC108 ND ND 70 - 130 20ND
0.48 0.39Toluene ND 20.7103 1.81 1.47 70 - 130 20ND
ND NDTrans-1,2-Dichloroethene ND NC97 ND ND 70 - 130 20ND
ND NDtrans-1,3-Dichloropropene ND NC105 ND ND 70 - 130 20ND
4.49 4.51Trichloroethene ND 0.498 24.1 24.2 70 - 130 20ND
0.24 0.19Trichlorofluoromethane ND 23.398 1.35 1.07 70 - 130 20ND
ND NDTrichlorotrifluoroethane ND NC94 ND ND 70 - 130 20ND
ND NDVinyl Chloride ND NC96 ND ND 70 - 130 20ND
108 102% Bromofluorobenzene 104 5.7100 108 102 70 - 130 20104
MS - Matrix SpikePhyllis Shiller, Laboratory Director
If there are any questions regarding this data, please call Phoenix Client Services at extension 200.
April 22, 2014MS Dup - Matrix Spike Duplicate
RPD - Relative Percent DifferenceLCS - Laboratory Control Sample
LCSD - Laboratory Control Sample Duplicate
NC - No CriteriaIntf - Interference
Page 2 of 2
Sample Criteria Exceedences ReportTuesday, April 22, 2014 Page 1 of 1
Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis
UnitsCriteria
GBG34092 - EBCCriteria: None
RLCriteria
State: NY
#Error*** No Data to Display ***
Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.