BRITISH STANDARD BS EN 705:1995 BS 2782-12: Methods 1995 … · 2018-06-17 · BRITISH STANDARD BS...

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BRITISH STANDARD BS EN 705:1995 BS 2782-12: Methods 1220A to C: 1995 Plastics piping systems — Glass-reinforced thermosetting plastics (GRP) pipes and fittings — Methods for regression analyses and their use The European Standard EN 705:1994 has the status of a British Standard

Transcript of BRITISH STANDARD BS EN 705:1995 BS 2782-12: Methods 1995 … · 2018-06-17 · BRITISH STANDARD BS...

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BRITISH STANDARD BS EN 705:1995BS 2782-12: Methods 1220A to C: 1995

Plastics piping systems — Glass-reinforced thermosetting plastics (GRP) pipes andfittings — Methods for regression analyses and their use

The European Standard EN 705:1994 has the status of a British Standard

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BS EN 705:1995

This British Standard, having been prepared under the direction of the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and comes into effect on15 November 1995

© BSI 01-2000

The following BSI references relate to the work on this standard:Committee reference PRI/61Draft for comment 92/41338 DC

ISBN 0 580 24136 X

Committees responsible for this British Standard

The preparation of this British Standard was entrusted to Technical Committee PRI/61, Plastics piping systems and components, upon which the following bodies were represented:

British Gas plcBritish Plastics FederationBritish Plumbing Fittings Manufacturers’ AssociationBritish Valve and Actuator Manufacturers’ AssociationDepartment of the Environment (British Board of Agrément)Department of the Environment (Building Research Establishment)Department of the Environment (Property and Buildings Directorate)Department of TransportElectricity AssociationFederation of Civil Engineering ContractorsHealth and Safety ExecutiveInstitute of Building ControlInstitute of MaterialsInstitution of Civil EngineersInstitution of Gas EngineersInstitution of Water and Environmental ManagementNational Association of Plumbing, Heating and Mechanical Services

ContractorsPipeline Industries GuildPlastics Land Drainage Manufacturers’ AssociationSociety of British Gas IndustriesSociety of British Water IndustriesWater Companies AssociationWater Services Association of England and Wales

Amendments issued since publication

Amd. No. Date Comments

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Contents

PageCommittees responsible Inside front coverNational foreword iiForeword 2Text of EN 705 5

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BS EN 705:1995

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National foreword

This British Standard has been prepared by Technical Committee PRI/61, and is the English language version of EN 705:1994 Plastics piping systems — Glass-reinforced thermosetting plastics (GRP) pipes and fittings — Methods for regression analyses and their use, published by the European Committee for Standardization (CEN).It is incorporated into BS 2782 Methods of testing plastics — Part 12. Reinforced plastics pipes, fittings and valves, as Methods 1220A to C:1995 as follows.

Method 1220A corresponds to method A (Covariance method) of EN 705:1994.Method 1220B corresponds to method B (Regression with time as the independent variable) of EN 705:1994.Method 1220C corresponds to method C (Second order polynomial relationships) of EN 705:1994.

These methods are incorporated into BS 2782 for association with related test methods for plastics materials and plastics piping components.This test method has been prepared for reference by other standards under preparation by CEN for specification of reinforced plastics piping systems and components. It has been implemented as a national standard to enable experience of the method to be gained and for use for other fresh applications.It is also for use for the revision or amendment of other national standards as practicable, but it should not be presumed to apply to any existing standard or specification which contains or makes reference to a different method until that standard/specification has been amended or revised to make reference to this method and adjust any requirements as appropriate.A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application.

Compliance with a British Standard does not of itself confer immunity from legal obligations.

Summary of pagesThis document comprises a front cover, an inside front cover, pages i and ii, the EN title page, pages 2 to 31 and a back cover.This standard has been updated (see copyright date) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover.

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EUROPEAN STANDARD

NORME EUROPÉENNE

EUROPÄISCHE NORM

EN 705

April 1994

UDC 621.643.2-036.067.5:621.643.06:620.1:519.2

Descriptors: Pipelines, plastic tubes, pipe fittings, thermosetting resins, reinforced plastics, glass, data, statistical analysis, computation, design inspection

English version

Plastics piping systems — Glass-reinforced thermosetting plastics (GRP) pipes and fittings — Methods for regression

analyses and their use

Systèmes de canalisations plastiques — Tubes et raccords plastiques thermodurcissable renforcés de verre (PRV) — Méthodes pour une analyse de régression et leurs utilisations

Kunststoff-Rohrleitungssysteme — Rohre und Formstücke aus glasfaserverstärkten duroplastischen Kunststoffen (GFK) — Verfahren zur Regressionsanalyse und deren Anwendung

This European Standard was approved by CEN on 1994-04-11. CEN membersare bound to comply with the CEN/CENELEC Internal Regulations whichstipulate the conditions for giving this European Standard the status of anational standard without any alteration.Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to anyCEN member.This European Standard exists in three official versions (English, French,German). A version in any other language made by translation under theresponsibility of a CEN member into its own language and notified to theCentral Secretariat has the same status as the official versions.CEN members are the national standards bodies of Austria, Belgium,Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy,Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland andUnited Kingdom.

CEN

European Committee for StandardizationComité Européen de NormalisationEuropäisches Komitee für Normung

Central Secretariat: rue de Stassart 36, B-1050 Brussels

© 1994 Copyright reserved to CEN membersRef. No. EN 705:1994 E

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EN 705:1994

© BSI 01-20002

Foreword

This standard was prepared by CEN/TC 155, Plastics piping systems and ducting systems.This standard is based on document N 197 Glass-reinforced thermosetting plastics (GRP) pipes and fittings — Standard extrapolation procedures and their use, prepared by working group 1 of Subcommittee 6 of Technical Committee 138 of the International Organization for Standardization (ISO). It is a modification of ISO/TC 138/SC6/WG 1 N 197 for reasons of possible applicability to other test conditions and alignment with texts of other standards on test methods.The modifications are:

— examples have been introduced to enable validation of alternative calculation facilities;— material-dependent requirements are not given;— editorial changes have been introduced.

The material-dependent test parameters and/or performance requirements are incorporated in the referring standard.Annex A, which is informative, describes procedures for solving the given set of equations (see 3.2.3) on a mathematical basis using the example shown in 3.2.6.No existing European Standard is superseded by this standard.This standard is one of a series of standards on test methods which support System Standards for plastics piping systems and ducting systems.This standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by October 1994, and conflicting national standards shall be withdrawn at the latest by October 1994.In accordance with the CEN/CENELEC Internal Regulations, the following countries are bound to implement this European Standard: Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland, United Kingdom.

Contents

PageForeword 2Introduction 51 Scope 52 Principle 53 Procedures for determining the

functional relationships 53.1 Linear relationships —

Methods A and B 53.2 Second order polynomial

relationships — Method C 144 Application of methods to product

design and testing 164.1 General 164.2 Design 174.3 Examples for validation of

calculation procedures for design 204.4 Procedures for verifying conformance

to product design and performance values 23

4.5 Examples for validation of calculationprocedures for design or productperformance verification 26

Annex A (informative) Mathematicalprocedures 30A.1 Matrix system 30A.2 Substitution system 30Figure 1 — Regression line from the results in Table 4 11Figure 2 — Regression line from the results in Table 7 16Figure 3 — Derived values 18Figure 4 — Extrapolated values 19Figure 5 — Example on pressure 21Figure 6 — Example for ring stiffness 24Figure 7 — Property test values 25Table 1 — Minimum values for the squared, r2, and linear coefficient of correlation, r, for acceptable data from n pairs of data 7Table 2 — Percentage points of Student’s t distribution (upper 2,5 % points; two sided 5 % level of confidence; tv for 97,5 %) 8Table 3 — Basic data for example calculation and statistical analysis validation 10Table 4 — Estimated mean values, Vm, for V 11Table 5 — Basic data for example calculation and statistical validation 13

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PageTable 6 — Estimated mean values, Vm, for V 13Table 7 — Estimated mean values, Vm, for V 16Table 8 — Initial burst test results 20Table 9 — Initial ring stiffness test results 22Table 10 — Initial burst test failure pressures for the sample 26Table 11 — Times to failure of burst tests of the sample 27Table 12 — Initial ring stiffness results for the sample 28Table 13 — Stiffness results at 1 000 h for the sample 28

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IntroductionThis standard has been prepared to describe the procedures intended for analysing the regression of test data, usually with respect to time, and the use of the results in design and assessment of conformity with performance requirements. Its applicability has been limited to use with data obtained from tests carried out on samples. The referring standards require estimates to be made of the long-term properties of the pipe for such parameters as circumferential tensile strength, deflection and creep.The committee investigated a range of statistical techniques that could be used to analyse the test data produced by tests that were destructive. Many of these simple techniques required the logarithms of the data to

a) be normally distributed;b) produce a regression line having a negative slope; andc) have a sufficiently high regression correlation (see Table 1).

Whilst the last two conditions can be satisfied, analysis has shown that there is a skew to the distribution and hence this primary condition is not satisfied. Further investigation into techniques that can handle skewed distributions resulted in the adoption of the covariance method for analysis of such data for this standard.The results from non-destructive tests, such as creep or changes in deflection with time, often satisfy these three conditions and hence simpler procedures, using time as the independent variable, can also be used in accordance with this standard.

1 ScopeThis standard specifies procedures suitable for the analysis of data which, when converted into logarithms of the values, have either a normal or a skewed distribution. It is intended for use with the test methods and referring standards for glass-reinforced plastics pipes or fittings for the analysis of properties as a function of, usually, time. However it can be used for the analysis of any other data.For use depending upon the nature of the data, three methods are specified. The extrapolation using these techniques typically extends the trend from data gathered over a period of approximately 10 000 h, to a prediction of the property at 50 years.

2 PrincipleData are analysed for regression using methods based on least squares analysis which can accommodate the incidence of a skew and/or a normal distribution and the applicability of a first order or a second order polynomial relationship.The three methods of analysis used comprise the following:

— method A: covariance using a first order relationship;— method B: least squares with time as the independent variable using a first order relationship;— method C: least squares with time as the independent variable using a second order relationship.

The methods include statistical tests for the correlation of the data and the suitability for extrapolation.

3 Procedures for determining the functional relationships3.1 Linear relationships — Methods A and B

3.1.1 Procedures common to methods A and B

Use method A (see 3.1.2) or method B (see 3.1.3) to fit a straight line of the form

where

y = a + bx (1)

y is the logarithm (lg) of the property being investigated;a is the intercept on the y axis;b is the slope;x is the logarithm (lg) of the time, in hours.

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3.1.2 Method A — Covariance method

3.1.2.1 General

For method A calculate the following variables as necessary in accordance with 3.1.2.2 to 3.1.2.5:

where

NOTE If the value of Qxy is greater than zero the slope of the line is positive and if the value of Qxy is less than zero then the slope is negative.

3.1.2.2 Suitability of data

Calculate the squared, r2, and the linear coefficient of correlation, r, using the following equations:

If the value of r2 or r is less than the applicable minimum value given in Table 1 as a function of n, consider the data unsuitable for analysis.

3.1.2.3 Functional relationships

To find a and b for the functional relationship line

first set

then calculate a and b using the following equations:

3.1.2.4 Calculation of variances

If tu is the applicable time to failure, then set

Using equations (11), (12) and (13) respectively, calculate for i = 1 to n the following sequence of statistics:— the best fit xi½ for true xi;— the best fit yi½ for true yi; and

(2)

(3)

(4)

Qy is the sum of the squared residuals parallel to the y axis divided by n;Qx is the sum of the squared residuals parallel to the x axis divided by n;Qxy is the sum of the squared residuals perpendicular to the line, divided by n;Y is the arithmetic mean of the y data, i.e.

X is the arithmetic mean of the x data, i.e.

xi, yi, are individual values;n is the total number of results (pairs of readings for xi, yi).

(5)

(6)

y = a + bx (1)

(7)

b = – (¿)0,5 (8)a = Y – bX (9)

xu – lg tu (10)

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— the error variance, Ö¸2 for x.

Calculate the following quantities:

Calculate the variance C of the slope b using the following equation:

Table 1 — Minimum values for the squared, r2, and linear coefficient of correlation, r, for acceptable data from n pairs of data

3.1.2.5 Check for the suitability of data for extrapolation

If it is intended to extrapolate the line, calculate T using the following equation:

If the absolute value|T|(i.e. ignoring signs) of T is equal to or greater than the applicable value for Student’s t, tv, shown in Table 2 for (n – 2) degrees of freedom then consider the data suitable for extrapolation.

(11)

yi½ = a + bxi½ (12)(13)

(14)

(15)

C = D(1 + E) (16)

(n – 2)Minimum values

(n – 2)Minimum values

r2 r r2 r

11 0,6416 0,8010 23 0,3816 0,617712 0,6084 0,7800 24 0,3689 0,607413 0,5781 0,7603 25 0,3569 0,597414 0,5506 0,7420 30 0,3070 0,5541

15 0,5250 0,7246 35 0,2693 0,518916 0,5018 0,7084 40 0,2397 0,489617 0,4805 0,6932 45 0,2160 0,464818 0,4606 0,6787 50 0,1965 0,4433

19 0,4425 0,6652 60 0,1663 0,407820 0,4256 0,6524 70 0,1443 0,379921 0,4099 0,6402 80 0,1273 0,356822 0,3953 0,6287 90 0,1139 0,3375

100 0,1031 0,3211NOTE In Table 1 and elsewhere in this standard, the equations and corresponding values for r2 and r are given, for convenience of use in conjunction with reference data published elsewhere in terms of only r2 or r.

(17)

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Table 2 — Percentage points of Student’s t distribution (upper 2,5 % points; two sided 5 % level of confidence; tv for 97,5 %)

Degree of freedom (n – 2)

Student’s t valuetv

Degree of freedom

(n – 2)

Student’s t valuetv

Degree of freedom

(n – 2)

Student’s t valuetv

1 12,7062 36 2,0281 71 1,9939

2 4,3027 37 2,0262 72 1,9935

3 3,1824 38 2,0244 73 1,9930

4 2,7764 39 2,0227 74 1,9925

5 2,5706 40 2,0211 75 1,9921

6 2,4469 41 2,0195 76 1,9917

7 2,3646 42 2,0181 77 1,9913

8 2,3060 43 2,0167 78 1,9908

9 2,2622 44 2,0154 79 1,9905

10 2,2281 45 2,0141 80 1,9901

11 2,2010 46 2,0129 81 1,9897

12 2,1788 47 2,0112 82 1,9893

13 2,1604 48 2,0106 83 1,9890

14 2,1448 49 2,0096 84 1,9886

15 2,1315 50 2,0086 85 1,9883

16 2,1199 51 2,0076 86 1,9879

17 2,1098 52 2,0066 87 1,9876

18 2,1009 53 2,0057 88 1,9873

19 2,0930 54 2,0049 89 1,9870

20 2,0860 55 2,0040 90 1,9867

21 2,0796 56 2,0032 91 1,9864

22 2,0739 57 2,0025 92 1,9861

23 2,0687 58 2,0017 93 1,9858

24 2,0639 59 2,0010 94 1,9855

25 2,0595 60 2,0003 95 1,9853

26 2,0555 61 1,9996 96 1,9850

27 2,0518 62 1,9990 97 1,9847

28 2,0484 63 1,9983 98 1,9845

29 2,0452 64 1,9977 99 1,9842

30 2,0423 65 1,9971 100 1,9840

31 2,0395 66 1,9966

32 2,0369 67 1,9960

33 2,0345 68 1,9955

34 2,0322 69 1,9949

35 2,0301 70 1,9944

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3.1.2.6 Validation of statistical procedures by an example calculation

The data given in Table 3 together with the results given in this example are for use to verify that the other statistical procedures as adopted by users will produce results similar to those obtained from the equations given in this standard. For the purposes of example, the property in question is represented by V, the values for which are of a typical magnitude and in no particular units. Because of rounding errors, it is unlikely that the results will agree exactly, so for the calculation procedure to be acceptable, the results obtained for r, r2, b, a, and the mean value of V, Vm, shall agree to within ± 0,1 % of the values given in this example, as applicable. The values of other statistics are provided to assist checking of the procedure.Sums of squares

Coefficient of correlation

Functional relationships

Calculated variances (see 3.1.2.4)

Check of the suitability for extrapolation (see 3.1.2.5)

The estimated mean values for V at various times are given in Table 4 and shown in Figure 1.

Qx = 0,79812;

Qy = 0,00088;

Qxy = – 0,02484.

r2 = 0,87999;

r = 0,93808.

¿ = 0,00110;

b = – 0,03317;

a = 1,62731.

E = 3,5202 × 10–2;

D = 4,8422 × 10–6;

C = 5,0127 × 10–6 (the variance of b);

Ö¸2 = 5,2711 × 10–2 (the error variance for x).

n = 32;tv = 2,0423;T = – 0,03317/(5,0127 × 10–6)0,5 = – 14,8167;|T| = 14,8167 > 2,0423.

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Table 3 — Basic data for example calculation and statistical analysis validation

n V y(lg V)

Timeh

x(lg time)

(time in h)

1 30,8 1,4886 5 184 3,7147

2 30,8 1,4886 2 230 3,3483

3 31,5 1,4983 2 220 3,3464

4 31,5 1,4983 12 340 4,0913

5 31,5 1,4983 10 900 4,0374

6 31,5 1,4983 12 340 4,0913

7 31,5 1,4983 10 920 4,0382

8 32,2 1,5079 8 900 3,9494

9 32,2 1,5079 4 173 3,6204

10 32,2 1,5079 8 900 3,9494

11 32,2 1,5079 878 3,9435

12 32,9 1,5172 4 110 3,6138

13 32,9 1,5172 1 301 3,1143

14 32,9 1,5172 3 816 3,5816

15 32,9 1,5172 669 2,8254

16 33,6 1,5263 1 430 3,1553

17 33,6 1,5263 2 103 3,3228

18 33,6 1,5263 589 2,7701

19 33,6 1,5263 1 710 3,2330

20 33,6 1,5263 1 299 3,1136

21 35,0 1,5441 272 2,4346

22 35,0 1,5441 446 2,6493

23 35,0 1,5441 466 2,6684

24 35,0 1,5441 684 2,8351

25 36,4 1,5611 104 2,0170

26 36,4 1,5611 142 2,1523

27 36,4 1,5611 204 2,3096

28 36,4 1,5611 209 2,3201

29 38,5 1,5855 9 0,9542

30 38,5 1,5855 13 1,1139

31 38,5 1,5855 17 1,2304

32 38,5 1,5855 17 1,2304Means: Y = 1,5301; X = 2,9305

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Table 4 — Estimated mean values, Vm, for V

3.1.3 Regression with time as the independent variable

3.1.3.1 General

For method B calculate the following variables:

(The sum of the squared residuals parallel to the y axis)

timeh

Vm

0,1 45,76

1,0 42,39

10,0 39,28

100,0 36,39

1 000 33,71

10 000 31,23

100 000 28,94

438 000 27,55

Figure 1 — Regression line from the results in Table 4

Sy = C (yi – Y)2 (18)

Sx = C (xi – X)2 (19)

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(The sum of the squared residuals parallel to the x axis)

(The sum of the squared residuals perpendicular to the line)where

3.1.3.2 Suitability of data

Calculate the squared, r2, and the linear coefficient of correlation, r, using the following equations:

If the value of r2, or r, is less than the applicable minimum value given in Table 1 as a function of n, consider the data unsuitable for analysis.

3.1.3.3 Functional relationships

Calculate a and b for the functional relationship line [see equation (1)], using the following equations:

3.1.3.4 Check for the suitability of data for extrapolation

If it is intended to extrapolate the line, calculate M using the following equation:

where

If M is equal to or less than zero consider the data unsuitable for extrapolation.

3.1.3.5 Validation of statistical procedures by an example calculation

Use the data given in Table 5 for the calculation procedures described in 3.1.3.2 to 3.1.3.4 to ensure that the statistical procedures to be used in conjunction with this method will give results for r, r2, a, b and Vm to within ± 0,1 % of the values given in this example.

Sxy = C {(xi – X) (yi – Y)} (20)

Y is the arithmetic mean of the y data, i.e.

X is the arithmetic mean of the x data, i.e.

xi, yi are individual values;n is the total number of results (pairs of readings for xi, yi).

NOTE If the value of Sxy is greater than zero the slope of the line is positive and if the value of Sxy is less than zero then the slope is negative.

(21)

r =|(r2)0,5| (22)

(23)

a = Y – bX (24)

(25)

tv is the applicable value for Student’s t determined from Table 2.

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Table 5 — Basic data for example calculation and statistical validation

Sums of squares

Coefficient of correlation

Functional relationships (see 3.1.3.3)

Check of the suitability for extrapolation (see 3.1.3.4)

Table 6 — Estimated mean values, Vm, for V

n Timeh

x(lg t)

(t in h)

V y(lg V)

1 0,10 – 1,0000 7 114 3,85212 0,27 – 0,5686 6 935 3,84103 0,50 – 0,3010 6 824 3,83414 1,00 0 6 698 3,82595 3,28 0,5159 6 533 3,8151

6 7,28 0,8621 6 453 3,80987 20,0 1,3010 6 307 3,79998 45,9 1,6618 6 199 3,79239 72,0 1,8573 6 133 3,7877

10 166 2,2201 5 692 3,7552

11 219 2,3404 5 508 3,741012 384 2,5843 5 393 3,731813 504 2,7024 5 364 3,729514 3 000 3,4771 5 200 3,716015 10 520 4,0220 4 975 3,6968Means: X = 1,4450 Y = 3,7819

Sx = 31,6811;Sy = 0,0347;Sxy = – 1,0242.

r2 = 0,9556;r = 0,9775.

a = 3,8286;b = – 0,0323.

tv = 2,1604;M = 942,21.

Timeh

Vm

0,1 7 2591,0 6 739

10,0 6 256100,0 5 808

1 000 5 39110 000 5 005

100 000 4 646438 000 4 428

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3.2 Second order polynomial relationships — Method C

3.2.1 General

This method fits a curved line of the form

where

3.2.2 Variables

For method C calculate the following variables:

where

3.2.3 Solution system

Determine c, d and e (see 3.2.1) using the following matrix:

NOTE Examples showing the procedures that can be used are detailed in Annex A.

3.2.4 Suitability of data

Calculate the squared, r2, and the linear coefficient of correlation, r, using the following equations:

y = c + dx + ex2 (26)

y is the logarithm (lg) of the property being investigated;c is the intercept on the y axis;d, e are the coefficients to the two orders of x;x is the logarithm (lg) of the time, in hours.

Cxi (sum of all individual x data);Cxi

2 (sum of all squared x data);

Cxi3 (sum of all x data to the third power);

Cxi4 (sum of all x data to the fourth power);

Cyi (sum of all individual y data);(Cyi)2 (squared sum of all individual y data);

Cyi2 (sum of all squared y data);

C(xiyi) (sum of all products xiyi);C(xi

2 yi) (sum of all products xi2 yi);

Sx = C (xi – X)2 (sum of the squared residuals parallel to the x axis for the linear part);

Sxx = C (xi2 – X2)2 (sum of the squared residuals parallel to the x axis for the quadratic part);

Sy = C (yi – Y)2 (sum of the squared residuals parallel to the y axis);Sxy = C[(xi – X)(yi – Y)] (sum of the squared residuals perpendicular to the line for the linear part);Sxxy = C[(xi

2 – X2)(yi – Y)] (sum of the squared residuals perpendicular to the line for the quadratic part).

Y is the arithmetic mean of the y data, i.e.

X is the arithmetic mean of the x data, i.e.

Cyi = cn + dCxi + eCxi2 (27a)

C(xiyi) = cCxi + dCxi2 + eCxi

3 (27b)C(xi

2yi) = cCxi2 + dCxi

3 + eCxi4 (27c)

(28)

r =|(r2)0,5| (29)

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If the value of r2, or r, is less than the applicable minimum value given in Table 1 as a function of n, consider the data unsuitable for analysis.

3.2.5 Check for the suitability of data for extrapolation

If it is intended to extrapolate the line, calculate M using the following equation:

If M is equal to or less than zero consider the data unsuitable for extrapolation.

3.2.6 Validation of statistical procedures by an example calculation

Use the data given in Table 5 for the calculation procedures described in 3.2.2 to 3.2.5 to ensure that the statistical procedures to be used in conjunction with this method will give results for r, r2, a, b and Vm to within ± 0,1 % of the values given in this example (n = 15).Sums of squares and other variables

Solution system (see 3.2.3)

Coefficient of correlation (see 3.2.4)

Check of the suitability for extrapolation (see 3.2.5)

The estimated mean values, Vm, for V at various times are given in Table 7 and shown in Figure 2.

(30)

Cxi = 21,671;Cxi

2 = 62,989;

Cxi3 = 180,623;

Cxi4 = 584,233;

Cyi = 56,728;(Cyi)2 = 3218,09;

Cyi2 = 214,574;

Cxiyi = 80,932;Cxi

2yi = 235,175;Sx = 31,681;Sxx = 386,638;Sy = 0,347;Sxy = – 1,0242;Sxxy = – 3,0418.

c = 3,8288;d = – 0,0262;e = – 0,0022.

r2 = 0,9647;r = 0,9822.

tv = 2,1604;M = 15859,6.

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Table 7 — Estimated mean values, Vm, for V

4 Application of methods to product design and testing4.1 General

The referring standards specify limiting requirements for the properties and performance of a product. Some of these are based on destructive tests, for example hoop tensile strength, whilst others are based on actual or derived physical properties, such as stiffness.

Timeh

Vm

0,1 7 125

1,0 6 742

10,0 6 315

100,0 5 856

1 000 5 375

10 000 4 884

100 000 4 393

438 000 4 091

Figure 2 — Regression line from the results in Table 7

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Where the physical property being determined enables both method B and method C to be used then both procedures shall be performed. The value for r2 and/or r determined for each procedure shall be compared and the value for the property determined using the procedure with the highest r2 or r value shall be taken as the value for the property. If the referring standard specifies for such properties a method then only that procedure shall be performed.In either case, many of these properties need an extrapolated long-term (e.g. 50 years) value for comparison with the requirement. This extrapolated value is determined by inserting, as necessary, the values for a, b, c, d and e, determined in accordance with 3.1 or 3.2 as appropriate, into equations (31) or (32) respectively.

where

Solving the equation, (31) or (32), for y gives the extrapolated value for comparison with the requirement specified in the referring standard.For supplementary procedures, where relevant, for the application of the results to derive design requirements, see 4.2 and the worked examples given in 4.3 to enable validation of any calculation facilities used.For their use for testing products, to predict and verify the ability of a product to conform to a specified requirement, see 4.4 and the examples given in 4.5 to enable validation of any calculation facilities used.The wording of 4.2 to 4.5 is appropriate to specification limits in terms of minimum values, long-term performance at 50 years and short-term performance at 6 min. For limits comprising maximum values or other time periods, appropriate adjustments are necessary.In conjunction with sampling requirements and limits on the acceptable levels, if any, on the quantity of non-conforming products to be specified by referring standards and in certification or quality plans, as appropriate, these methods can be used for quality control purposes.

4.2 Design

4.2.1 Regression values

4.2.1.1 Derived long-term values

Where it is assumed that, from initial short-term tests on pipe representative of such a design, the mean value of the property being investigated, V0,m, and the estimated standard deviation, Ö, of the initial test results are known, the procedures for designing a pipe to conform to a requirement of a referring standard are as follows.If a safety factor, FS, is specified, calculate the minimum long-term (50 years) value for the property, V50, min., (see Figure 4), using the following equation:

otherwise:

where

4.2.1.2 Regression ratio (see Figure 3)

Calculate the regression ratio, RR, using the following equation:

where both the 50 year and the 6 min extrapolated property values are calculated using equation (31) or (32), as applicable, except that for the 6 min value the logarithm of 0,1 h (6 min), i.e. – 1, is used in place of 5,64147.

lg y = a + btL (31)lg y = c + dtL + etL

2 (32)

tL is the logarithm (lg) of the long-term period, in hours, [for 50 years (438 000 h), tL = 5,64147].

V50,min. = FsV50,s, min. (33)

V50,min. = V50,s,min. (34)

V50,s,min. is the specified minimum long-term (50 years) requirement.

(35)

RRextrapolated long-term (50 year) property valueextrapolated short-term (6 min) property value------------------------------------------------------------------------------------------------------------------------------------=

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4.2.1.3 Factor C (see Figure 3)

Calculate the factor C, which relates the extrapolated 6 min value to the test result for the initial tests on the pipes, using the following equation:

4.2.2 Initial values

4.2.2.1 Minimum initial property value (V0,min.)

Derive the minimum initial property value, V0,min., using the following equation:

where

4.2.2.2 Property design values

Derive the design value for the initial property, V0,d, using the following equation:

where

Figure 3 — Derived values

(36)

(37)

C is calculated using equation (36);V50,min. is calculated using equation (33) or (34);RR is calculated using equation (35).

V0,d = V0,min. + 1,96Ö (38)

Ö is the standard deviation of the short-term test results for this property.

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The factor 1,96 assumes that a 2,5 % failure criteria is acceptable. Where other percentage failure criteria are specified in the referring standard then the relevant factor obtained from standard statistical references shall be substituted for 1,96.NOTE Where the standard deviation can be expected to increase with an increase in mean property values, and vice versa, then the design property values for different levels of the property can be obtained using a constant coefficient of variation.

Determine the short-term (6 min) and long-term (50 years) design property values, and hence the design line as follows:

— determine the estimated 6 min design property value, V6,d, using the following equation:

where

— determine the estimated 50 years property value, V50,d, using the following equation:

where

— if applicable (see 4.1), determine the equation for the linear design line as follows:

where

Figure 4 — Extrapolated values

(39)

C is determined in accordance with 4.2.1.3;

V50,d = RRV6,d (40)

RR is the regression ratio determined in accordance with 4.2.1.2;

lg Vt,d = ad + (b × lg t) (41)

Vt,d is the design property value at a given time t;b is the slope of both the minimum and the mean linear regression lines;

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where

where

— if applicable (see 4.1), determine the equation for the second order design curve as follows:

where

where

where

4.3 Examples for validation of calculation procedures for design

4.3.1 General

Use the data given in 4.3.2 and 4.3.3, as applicable, to verify that the calculation procedures used will give results for a, b, c, d, e, r2, r, V50,min., V6,min., V0,min. and V0,d to within ± 0,1 % of the example values.

4.3.2 Example 1. Linear relationship; destructive test failure behaviour

4.3.2.1 The problem

Assuming thata) the data given in Table 3 are burst test pressure results, in bars;b) Table 4 comprises the results of the regression analysis of these burst test data for a pressure pipe;c) initial burst test data are available in Table 8 for a pipe with a comparable wallbuild-up, as given under a) and b),

determine the design values for a PN 10 (nominal pressure) pipe with a safety factor, FS, of 1,8.Table 8 — Initial burst test results

ad is the constant of the linear design line;

ad = a + ¸d (42)

a is the constant of the property value mean linear line [see equation (1)];

(43)

lg Vt,d = cd + (d × lg t) + {e × (lg t)2} (44)

Vt,d is the design property value at a given time t;d, e are the coefficients of both the design curve and the mean second order regression curve;cd is the constant of the second order design curve;

cd = c + ¸d (45)

c is the constant of the second order mean regression curve [see equation (26)];

Values in bars1)

52,0 44,5 49,0 50,3 46,7 51,147,3 49,7 53,3 51,1 46,0 50,345,9 49,1 48,8 46,7 49,8 53,6Mean initial burst pressure p0,m = 49,18Standard deviation Ö = 2,591) 1 bar = 105 N/m2 = 0,1 MPa

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4.3.2.2 Calculations and final results

For the data in Table 3 (see 3.1.2.6):a = 1,62731;b = – 0,03317,

and hence (Table 4):p6 = 45,76 bar;

p50 = 27,55 bar.

Using equation (35):

Using equation (36):

The design values for the PN 10 pipe with a safety factor of 1,8 then become:using equation (33):

and using equation (35) and (37):p0,min. = C p6,min. = 1,0747 × 29,9 bar = 32,1 bar;

Figure 5 — Example on pressure

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using equation (38):p0,d = p0,min. + 1,96 Ö = 32,1 + 1,96 × 2,59 = 37,18 bar.

The 6 min and 50 years design values are derived using equations (39) and (40):

p50,d = RR p6,d = 0,6021 × 34,6 bar = 20,83 bar

These equations give rise to the plots shown in Figure 5.

4.3.3 Example 2. Second order relationship; non-destructive test (creep) behaviour

4.3.3.1 The problem

Assuming thata) the data given in Table 5 are ring stiffness test results, in newtons per square metre;b) Table 6 and Table 7 comprise the results of the regression analysis of these ring stiffness test data;c) initial ring stiffness test data are available in Table 9 for pipes with a comparable wall build-up as for a) and b),

determine the design values for a SN 5000 pipe with a minimum long-term ring stiffness of 2 000 N/m2 and a safety factor, FS, of 1,0.

Table 9 — Initial ring stiffness test results

4.3.3.2 Calculations and definitive results

Using method B (linear relationship, see 3.1.3.2 and 3.1.3.5):

r2 = 0,9556;r = 0,9775.

Using method C (polynomial relationship, see 3.2.4 and 3.2.6):

r2 = 0,9647;r = 0,9822.

Because r2, or r, obtained using method C is greater than that obtained using method B, the line derived using method C is the more appropriate and therefore the results given in 3.2.6, calculated from the data in Table 5, are the following:

c = 3,8288;d = – 0,0262;e = – 0,0022,

and hence (Table 7):

S6 = 7 125 N/m2;

S50 = 4 091 N/m2.

From these results, it follows that: using equation (35):

using equation (36) and the results given in Table 9:

Values in newtons per square metre

7 540 7 200 6 970 7 190 7 7607 170 7 100 7 310 6 990 7 180Mean initial ring stiffness S0,m = 7 241Standard deviation Ö = 243

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The design values for a SN 5000 pipe with minimum long-term ring stiffness of 2 000 N/m2 and a factor of safety of 1,0 then become:using equation (34):

S50,min. = S50,s,min. = 2 000 N/m2;

and using the equations (35) and (37):

S0,min. = C S6,min. = 1,0163 × 3 483 N/m2 = 3 540 N/m2.

The value for S0,min from the initial requirement (5 000 N/m2) is greater than the one from the long-term requirement (3 540 N/m2), therefore the relevant value is:

S0,min. = 5 000 N/m2.

Hence, using equation (38) and the results given in Table 9:

S0,d = S0,min + 1,96 Ö = 5 000 + (1,96 × 243) = 5 476 N/m2.

The 6 min and 50 years design values are derived using equations (39) and (40):

S50,d = RR × S6,d = 0,5742 – 5 388 N/m2 = 3 094 N/m2

Based on the initial requirement (5 000 N/m2) the 6 min and 50 years minimum values are also derived using equations (39) and (40):

S0,50,min. = RR S0,6min. = 0,5742 × 4 920 N/m2 = 2 825 N/m2

These equations give rise to the plots shown in Figure 6.

4.4 Procedures for verifying conformance to product design and performance values

4.4.1 General

Given the following assumptions:a) a pipe design is to be verified by short-term tests or by both short-term and long-term tests on a product;b) the design value, V0,d, of the property being investigated has been determined in accordance with 4.2,

use the following procedures as applicable to show that the product conforms to the design requirements, where:

— method 1 (see 4.4.2) is valid for destructive test behaviour;— method 2 (see 4.4.3) is valid for non-destructive test behaviour.

4.4.2 Method 1 — Verification using destructive test data

4.4.2.1 Relationship between design and/or minimum line and test results of products

Using the property design values determined in accordance with 4.2.2.2 unless otherwise specified in the referring standard the following requirements shall be used to assess conformity with the standard.When a large group, i.e. more than 20 consecutive results, is being assessed then the following conditions shall be satisfied to show conformity with the referring standard:

a) the mean of the results shall be equal to or greater than the design value (see 4.2);b) no individual result shall be less than 80 % of the minimum value (see 4.2).When a small sample, i.e. up to and including five consecutive results, is being assessed then the following conditions shall be satisfied unless the referring standard specifies otherwise:c) the mean of the sample shall not be less than the design value minus the standard deviation used to determine the design value (see 4.2);d) no individual result shall be less than 80 % of the minimum value (see 4.2).

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4.4.2.2 Relationship between design line and product data

Where times other than zero, 6 min or 50 years are specified in the referring standard then equation (41) (see 4.2.2.2) shall be used to determine the design value, Vt,d (see Figure 7).

4.4.2.3 Relationship between minimum line and product data (see Figure 7)

Where times other than zero, 6 min or 50 years are specified in the referring standard then the following equation shall be used to determine the minimum required value, Vt,min..

where

where

where

Figure 6 — Example for ring stiffness

lg Vt,min. = amin. + (b × lg t) (46)

Vt,min. is the minimum property value at a given time t;b is the slope of both the minimum and the mean line;amin. is the constant of the minimum line;

amin. = a + ¸min. (47)

a is the constant of the mean property value line [see equation (1)];

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4.4.2.4 Conformance to a design property value, Vt,d, after a specified time t (see Figure 7)

Where either the time to failure for the design line, td, or the time to failure for the minimum line, tmin., is to be verified the appropriate one of the following equations shall be used:

4.4.3 Method 2 — Verification using non-destructive test dataNOTE Non-destructive tests for verification of long-term design or physical property behaviour are usually creep tests. It is assumed that the period of time for testing, tC, and related property requirements are specified in the referring standard (see also 4.4.1).

4.4.3.1 Relationship between design and/or minimum line and test results of products

For these relationships the assumptions and requirements given in 4.4.2.1 are applicable.

4.4.3.2 Relationship between design line and product data

Where times other than zero, 6 min or 50 years are specified in the referring standard then equations (41) and (44) as well as equations (46), (47) and (48) (see 4.2.2.2) shall be used to determine the design value, Vt,d (for principle see Figure 7).

4.4.3.3 Relationship between minimum line and product data

4.4.3.3.1 Linear relationship (see Figure 7)For the linear relationship, the assumptions, procedures and equations given in 4.4.2.3 are applicable.

Figure 7 — Property test values

(49)

(50)

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4.4.3.3.2 Second order polynomial relationship (for principle see Figure 7)Where times other than zero, 6 min or 50 years are specified in the referring standard then the following equation shall be used to determine the minimum required value, Vt,min..

where

4.4.3.4 Conformance to a design property value, Vt,d, after a specified time t (see Figure 7)

To verify that a product conforms to a design value Vt,d, or a minimum value Vt,min., after a time tc specified in the referring standard the following equations shall be used to determine the relevant values where t is to be replaced with tc:for the linear relationship:

and for the second order polynomial relationship:

4.5 Examples for validation of calculation procedures for design or product performance verification

4.5.1 General

Use the data given in 4.5.2 and 4.5.3 to verify that the calculation procedures to be used will give results for pt,d, tmin., St,d and St,min. to within ± 0,1 % of the results given in 4.5.2 and 4.5.3, as applicable.

4.5.2 Example 3. Linear relationship; destructive test failure behaviour

4.5.2.1 The problem

A series of pipes has been produced based on the design described in 4.3.2. The properties of test pieces have been measured by short-term (initial burst) and long-term (100 h) pressure resistance tests. The short-term test results are given in Table 10. The long-term test results, obtained from three test pieces subjected to a test pressure, pt,d, determined as described in 4.5.2.3, are given in Table 11. Do the pipes conform to 4.4.2.1 and 4.4.2.4?

Table 10 — Initial burst test failure pressures for the sample

lg Vt,min. = cmin. + (d × lg t) + {e × (lg t)2} (51)

Vt,min. is the minimum property value at a given time t;d, e are the coefficients of both the minimum and the mean regression line;cmin. is the constant of the minimum line;

wherecmin. = c + ¸min. (52)

wherec is the constant of the mean property value line [see equation (26)];

(53)

lg Vt,d = ad + (b × lg t) (41)lg Vt,min. = amin. + (b × lg t) (46)

lg Vt,d = cd + (d × lg t) + {e × (lg t)2} (44)lg Vt,min. = cmin. + (d × lg t) + [e × (lg t)2] (51)

Values in bars

38,6 38,5 31,9 38,436,7 39,8 39,2 40,132,6 37,5 34,9 38,336,9 40,0 39,4 41,738,6 38,5 31,9 38,436,7 37,7 39,2 37,8Mean initial burst pressure p0,m = 37,6Minimum initial burst pressure p0,min. = 31.9

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Table 11 — Times to failure of burst tests of the sample

4.5.2.2 Calculations and final results

4.5.2.2.1 Determination of conformance to initial burst pressure requirements

From Table 10, p0,m (sample) = 37,6 bars and p0,min. (sample) = 31,9 bars;from 4.3.2.2, p0,d = 37,36 bars and p0,min. (design) = 32 bars;therefore p0,m (sample) > p0,d and p0,min. (sample) > 0,8 × p0,min.(design) (= 25,6 bars) and the product sample conforms to 4.4.2.1 a) and 4.4.2.1 b).

4.5.2.2.2 Determination of conformance to long-term (100 h) pressure resistance requirements

Determine the equation of the design line as follows:a) using equation (43):

b) using equation (42):ad = a + ¸d = 1,62731 + (– 0,1178) = 1,5095;

c) using equation (41):

Determine the equation of the minimum line as follows:d) using equation (48):

e) using equation (47):amin. = a + ¸min. = 1,62731 + (– 0,1851) = 1,4423.

Determine the equation of the minimum time to failure for a given pressure as follows:f) using equation (50):

Assuming that the referring standard requires a 100 h pressure test, determine the test pressure, pt,d, to be used to test a sample and the minimum time to failure, tmin., as follows:

g) using equation (58): lg pt,d = 1,44316

hence:pt,d = 27,74 bar;

h) using equation (55):lg tmin. = – 0,02593

hence: tmin. = 0,942 h.

When three test pieces were tested using the test pressure of 27,74 bar, i.e. pt,d, the results given inTable 11 were obtained.

Values in hours

125,3 101,3 97,4Mean time to failure tm = 108Minimum time to failure tmin. = 97.4

lg pt,d = 1,5095 – (0, 03317 × lg t). (58)

(55)

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From Table 11, tm (sample) = 108 h and tmin. (sample) = 97,4 h; from 4.5.2.1 td = 100 h and from 4.5.2.2 h) tmin. = 0,942 h; therefore tm (sample) > td and tmin. (sample) > tmin. and the product conforms to 4.4.2.1 c) and 4.4.2.1 d).

4.5.3 Example 4. Polynomial relationship; creep behaviour

4.5.3.1 The problem

A series of pipes has been produced based on the design described in 4.3.3. The properties of test pieces have been measured by short-term (initial ring stiffness) and long-term (1 000 h creep) tests. The short-term test results are given in Table 12 and the long-term test results in Table 13. Do the pipes conform to 4.4.3.1 and 4.4.3.3?

Table 12 — Initial ring stiffness results for the sample

Table 13 — Stiffness results at 1 000 h for the sample

4.5.3.2 Calculation and final results

4.5.3.2.1 Determination of compliance with initial ring stiffness requirements

From Table 12, S0,m (sample) = 5 569 N/m2 and S0,min. (sample) = 4 980 N/m2; from 4.3.3.2, S0, d = 5 486 N/m2 and S0,min. (design) = 5 000 N/m2; therefore S0,m (sample) > S0,d and S0,min. (sample) > 0,8 × S0,min. (design) (= 4 000 N/m2) and the product sample conforms to 4.4.2.1 a) and 4.4.2.1 b) (through reference by 4.2.2.2).

4.5.3.2.2 Determination of conformance to long-term (1 000 h) ring stiffness requirements

Determine the equation of the design line as follows:a) using equation (46):

b) using equation (45):cd = c + ¸d = 3,8288 + – 0,1205 = 3,7083;

c) using equation (44)

Determine the equation of the minimum line as follows:d) using equation (53):

e) using equation (52): cmin. = c + ¸min. = 3,8288 + (– 0,1608) = 3,668;

f) using equation (51):

lg St,min. = 3,668 – (0,0262 × lg t) – {0,0022 × (lg t)2}.

Values in newtons per square metre

5 600 4 980 5 720 5 620 5 690 5 695

5 550 5 980 5 020 5 720 560v0 5 2955 560 5 680 5 550 5 620 5 795 5 570Mean initial ring stiffness S0,m = 5 569Minimum initial ring stiffness S0,min. = 4 980

Values in newtons per square metre

4 012 4 205 4 161Mean long-term ring stiffness Sm = 4 126Minimum long-term ring stiffness Smin. = 4 012

lg St,d = 3,7083 – (0, 0262 × lg t) {– 0,0022 × (lg t)2}. (56)

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Since the control procedure requires a 1 000 h ring stiffness test, determine the design stiffness, St,d, and the minimum stiffness, St,min., as follows:

g) using equation (56): lg St,d = 36 099

hence:

St,d = 4 073 N/m2;

h) using equation (57): lg St,min. = 3,5696

hence:

St,min. = 3 712 N/m2.

When three test pieces were tested for ring stiffness at 1 000 h, the results given in Table 13 were obtained.From Table 13, Sm (sample) = 4 126 N/m2 and Smin. (sample) = 4 012 N/m2;from item g) St,d = 4 073 N/m2 and from item h) St,min. = 3 712 N/m2;therefore Sm (sample) > St, d and Smin. (sample) > St,min. and the product conforms to 4.4.2.1 c) and 4.4.2.1 d).

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EN 705:1994

30 © BSI 01-2000

Annex A (informative) Mathematical proceduresA.1 Matrix systemUsing the equations (27a), (27b) and (27c) given in 3.2.3 the solution using a matrix system is described. Based on these equations the following matrix equation (A.1) can be constructed:

Using the values given in 3.2.6 for the respective variable the matrix equation (A.1) becomes equation (A.2):

Following mathematical rules the 3 × 3-matrix on the left hand side of equation (A.2) is inverted which results in matrix (A.3):

Multiplying both sides of the matrix equation (A.2) by matrix (A.3) results in the new equation (A.4):

Solving matrix equation (A.4) results in equation (A.5):

This rector matrix equation gives the solution for the variables c, d and e shown in 3.2.3 and in 3.2.6.A.2 Substitution systemWith the same set of equations (see 3.2.3) and with the data given in 3.2.6 an alternative way of solving the problem is as follows.NOTE Because the following section is worked out with rounded numbers the results may differ slightly when worked out on different calculators.From equation (27a):

From equation (27b):

From equation (27c):

(A.1)

(A.2)

(A.3)

(A.4)

(A.5)

56,728 = 15,000c + 21,671d + 62,989e (A.6)

80,932 = 21,671c + 62, 989d + 180,623e (A.7)

235,175 = 62,989c + 180, 623d + 584,233e (A.8)

Solving equation (A.8) to produce an equation for e results in equation (A.9):e = 0,4025 – 0,1078c – 0,3092d (A.9)

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Substituting this equation (A.9) into equations (A.6) and (A.7) results in equations (A.10) and (A.11):

Substituting this equation (A.12) for d into equation (A.10) results in equation (A.13):

and hence:

Using the result from equation (A.14) and substituting this for c in equation (A.12) results in equation (A.15) for d:

Using the values from equations (A.14) and (A.15) for c and d respectively in equation (A.9) gives a value for e of:

As can be seen the results from both methods are the same (but see note in A.2).

31,375 = 8,210c + 2,195d (A.10)8,231 = 2,200c + 7,140d (A.11)

Solving equation (A.11) to produce an equation for d results in equation (A.12):

d = 1,1528 – 0,3081c (A.12)

7,5337c = 28,8446 (A.13)

c = 3,8288 (A.14)

d = – 0,0262 (A.15)

e = – 0,0022 (A.16)

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BS EN705:1995BS 2782-12: Methods 1220A to C:1995

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