BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel:...

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BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII 901 N. 5th Street Kansas City, Kansas 66101 Black & Veatch Special Projects Corp. BVSPC Project 044720 BVSPC File E. 1.1 December 5, 2005 Subject: EPA Contract No. EP-S7-05-06 Task Order # 0075 Cleanup Status Report # 5 Dear Mr. Stewart: Enclosed are three copies of Long Term Response Action Cleanup Status Report Number 5. Per your request, I am sending a copy directly to Mr. Leo Henning at KDHE. Please feel free to call me at (913) 458-6506 if you have any questions or need additional information. Sincerely, BLACK & VEATCH SPECIAL PROJECTS CORP. Ken Wyatt Site Manager KWW cc: L. Henning (KDHE) G. Felkner 40227555 ^reRFUND RECORDS

Transcript of BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel:...

Page 1: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

BLACK & VEATCH6601 College Blvd.Overland Park, KS 66211

Tel: (913) 458-2900

USEPA Region VIIAce Services Site

Mr. Bob StewartUSEPA Region VII901 N. 5th StreetKansas City, Kansas 66101

Black & Veatch Special Projects Corp.

BVSPC Project 044720BVSPC File E. 1.1December 5, 2005

Subject: EPA Contract No. EP-S7-05-06Task Order # 0075Cleanup Status Report # 5

Dear Mr. Stewart:

Enclosed are three copies of Long Term Response Action Cleanup Status Report Number 5. Per yourrequest, I am sending a copy directly to Mr. Leo Henning at KDHE.

Please feel free to call me at (913) 458-6506 if you have any questions or need additional information.

Sincerely,

BLACK & VEATCH SPECIAL PROJECTS CORP.

Ken WyattSite Manager

KWW

cc: L. Henning (KDHE)G. Felkner

40227555

^reRFUND RECORDS

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Prepared for:U.S. Environmental Protection AgencyRegion 7901 North 5lh StreetKansas City, Kansas 66101

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1

Long Term Response ActionCleanup Status Report Number 5

April 27, 2005 to October 12, 2005

Ace Services SiteColby, Kansas

December 2, 2005

EPA Contract No.: EP-S7-05-06EPA Task Order No.: 0075

BVSPC Project No.: 044720

I

I

BLACK & VEATCHbuilding a W0rldof difference'-

E N E R G Y W A T E R I N P O R M A T I O N G O V E R N M E N T

Prepared by:Black & Veatch Special Projects Corp.6601 College Blvd.Overland Park, Kansas 66211

ProfessionalEnvironmental Engineers. Inc.

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Contents

1.0 Introduction 1-1

2.0 Long Term Response Action Objectives 2-12.1 Treatment Goals and Exit Strategy 2-12.2 Performance and Effectiveness 2-1

2.2.1 Groundwater Monitoring 2-22.2.2 Plume Capture 2-22.2.3 Groundwater Treatment System Performance Monitoring 2-42.2.4 Extraction Well Performance 2-4

2.3 System Cost Effectiveness 2-4

3.0 Bibliography 3-1

Tables

Table 2-1 Analytical Results Summary 2-6Table 2-2 Groundwater Elevation Data 2-10Table 2-3 Treatment Goals 2-13Table 2-4 Performance Monitoring Results 2-14

Figures

Figure 1-1 Site Location End of Section 1Figure 2-1 Total Chromium Isoconcentration Contour Map and Groundwater Flow

Direction - Shallow Zone End of Section 2Figure 2-2 Total Chromium Isoconcentration Contour Map and Groundwater Flow

Direction - Intermediate Zone End of Section 2Figure 2-3 Total Chromium Isoconcentration Contour Map and Groundwater Flow

Direction - Deep Zone End of Section 2Figure 2-4 Vertical Groundwater Flow Lines October 2005 End of Section 2Figure 2-5 Shallow Wells (Total Chromium) End of Section 2Figure 2-6 Intermediate Wells (Total Chromium) End of Section 2Figure 2-7 Deep Wells (Total Chromium) End of Section 2Figure 2-8 Residential Wells (Total Chromium) End of Section 2

Ace Services SiteLTRA Cleanup Siatus Report No 5 TC-1 044720

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Appendices

Appendix A Water Level Data SheetsAppendix B Well Purging FormsAppendix C Field SheetsAppendix D Chain of Custody RecordsAppendix E AirbillsAppendix F Field LogbooksAppendix G Analytical ResultsAppendix H August 2005 Quarterly Audit Report No. 7Appendix I November 2005 Quarterly Audit Report No. 8

Ace Services SiteLTRA Cleanup Status Report No 5 TC-2 044720

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1.0 Introduction

The U.S. Environmental Protection Agency (USEPA) has initiated remedial action (RA)

efforts for the Ace Services site near Colby, Kansas (CERCLIS I.D. No. KSD046746731). The

RA process is the methodology that the Superfund program has established for remediating risks

posed by uncontrolled hazardous waste sites. Included in the RA efforts are Long Term Response

Action (LTRA) activities. LTRA activities include ongoing support of treatment activities and

assessment of remedial progress. Documents detailing the methodology for LTRA activities at the

Ace Services site consist of the LTRA field sampling plan (FSP) (BVSPC 2003a), a quality

assurance project plan (QAPP) (BVSPC 2003b), a health and safety plan (HSP) (BVSPC

2003c), and the treatment plant Operation and Maintenance Plan (O&M) (BVSPC 2003d).

This Cleanup Status Report presents detailed descriptions of the remedial evaluation and

associated sampling activities performed during the performance period as part of the LTRA at the

Ace Services site. This Report includes the following items:

• Discussion of system performance and effectiveness.

Descriptions of the sampling efforts.

This Report has been prepared under USEPA Contract EP-S7-05-06 Task Order No. 0075.

The Ace Services site is located near the east edge of Colby, Kansas, at 500 East 4th Street

in Thomas County (Figure 1-1). The geographic coordinates for the site are approximately

100°02' 10" West Longitude and 39°23'47" North Latitude. The original facility was located in the

southeast quarter of Section 31, Township 7 South, Range 33 West. The groundwater contaminant

plume extends from the original facility to the east-southeast approximately 1.5 miles. The

surrounding property includes light industrial/commercial businesses and single family dwellings. A

railroad right-of-way bisects the site.

The Kansas Department of Health and Environment (KD HE) records indicate that a chrome

plating facility operated at the present location of the Ace Services site from approximately 1954

to 1990. The site was owned and operated by a company known as Northwest Manufacturing

from approximately 1954 until 1969, when Ace Services was formed and began operations at the

site. Prior to the chrome plating operations, it is alleged that a brick-making plant was located in

the vicinity, possibly around the early 1900s. Among the raw materials of the brick making process,

the brick facili ty may have used clays or fuel which contained chrome, and which may have

contributed to the chrome contamination in the area.

A source of contaminants at the site includes chromium electroplating operations by Ace

Services, Inc. The source of chromium was the chromic acid solution in the plating vats. Lead was

Ace Services Silc

LTRA Cleanup Simus Report No. 5 1-1 (W4720

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also present, probably as lead chromate, which is formed when lead anodes are used in the plating

process. Both contaminants entered the environment from plating vats, spills from transferring parts

to and from vats, and from a faulty wastewater treatment system. The treatment system

inadequately treated wastes and resulted in discharges from the facility exceeding wastewater

effluent limitations. Ace Services added a surface impoundment, or lagoon, to the system to control

discharges to the unnamed tributary of Prairie Dog Creek east of the site. Resulting sludge from

the surface impoundment and the underlying soils were found to be contaminated with lead and

chromium; groundwater in the area has been found to be contaminated with chromium.

KDHE and U SEP A involvement with the site began in 1971 after KDHE received a citizen

complaint concerning Ace Services discharging wastewater to the ground and the nearby unnamed

tributary. The Ace Services site was first identified for investigation under the Superfund program

in 1980 by KDHE. In 1981, KDHE conducted a Site Inspection of the Ace Services site. The

investigation by KDHE concluded that the Ace Services facility was the likely source of chromium

contamination in the groundwater which had contaminated publ ic water supply (P WS) Well No. 8

and caused the well to be removed from service in 1980. A Preliminary Assessment and Scanning

Site Investigation was performed by KDHE in 1989. A Listing Site Investigation was performed

by KDHE in 1991 which included the installation and sampling of three groundwater monitoring

wells. An additional round of groundwater samples were collected and analyzed by KDHE in

1995.

A KDHE removal action was initiated at the site in March 1992. Plating solutions were

removed from the vats. The vats and trough in which the vats were placed were also removed.

These wastes, primarily the plating solutions/baths, were disposed of at permitted disposal facilities.

The USEPA initiated a removal action at the site in May 1994 to prevent exposure of nearby

human populations to hazardous substances. The removal action consisted of removing residual

contamination (mainly dusts) from the building interior, excavation of a concrete trough and

underlying soils, installation of additional building support columns near the trough, demolition of

the wastewater treatment building, excavation of underlying soils, and excavation and

stabilization/treatment of lagoon soil. All waste was shipped off site for disposal, except

approximately 3,000 gallons of wastewater, which was treated on site and discharged to the

publicly owned treatment works (POTW).

USEPA initiated remedial investigation and feasibility study (RJ/FS) activities at the site in

1996 to characterize contaminants in groundwater and building materials and evaluate and select

RA efforts. A Remedial Investigation report and Risk Assessment report for the soil, buildings, and

groundwater at the Ace Services site was completed under the direction of the USEPA in October

1998. Residual contaminants assumed to exist in the soil at that time were found to pose acceptable

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health risks for industrial uses of the site. A Feasibility Study report for remediating the buildings

and groundwater at the Ace Services site was completed under the direction of the USEP A in

November 1998. The Record of Decision (ROD) for remediating the buildings and groundwater

at the Ace Services site was completed by theUSEPA in May 1999. Remedial Design (RD)

efforts for remediation of the buildings were initiated in June 1999 and were completed in

December 1999. RA activities for the existing buildings consisted of removing and disposing of

hazardous materials from the interior of the site buildings and was completed in February 2000.

RD efforts for remediation of groundwater were initiated in June 1999 and were completed

in January 2002. RA activities for contaminated groundwater include extraction of contaminated

groundwater, groundwater treatment using ion exchange resins, and discharge of treated

groundwater to the Prairie Dog Creek Tributary or beneficial use as drinking water for the City

of Colby. During demolition and excavation of the on site buildings a large amount of chromium-

contaminated soil was found which required significant removal efforts. The groundwater treatment

plant (G WTP) and extraction well field (collectively referred to as the groundwater treatment

system (G WTS)) were completed on August 12,2003, at which time groundwater extraction and

treatment began.

In October 2003, volatile organic compounds (VOC) contaminants were detected by KDHE

at low concentrations in monitoring wells and extraction wel Is located in the western portion of the

site. The source of the VOCs is believed to be the Hi-Plains Co-op leaking underground storage

tank (LUST) site located near Nashville Street and Fifth Street upgradient of the Ace Services site.

Extraction wells EX-1 -I, EX-1 -D, EX-2-I, EX-2-D, EX-2-S, and PWS-8 were taken off line

on October 17,2003, because of the presence of the VOCs in the captured groundwater. KDHE

has constructed a granular activated carbon (GAC) treatment unit to remove the VOCs. The GAC

treatment unit is positioned as a pre-treatment unit to the G WTP influent. The new GAC system

was started and the well field brought back to full operation on August 24, 2004.

Previous LTRA status reports have been prepared to describe and evaluate RA efforts. The

previous reports include:

LTRA Semi-Annual Cleanup Status Report, September and October 2003 Sample

Events (BVSPC 2004a),

L TRA A nnual Cleanup Status Report, November 2003 to April 2004 Sample Events

(BVSPC 2004c),

L TRA Cleanup Status Report Number 3, June 2004 to October 2004 Sample Events

(BVSPC 2004f), and

LTRA Cleanup Status Report Number 4, October 5, 2004 to April 30, 2005

(BVSPC 2005c).

Ace Services SiteLTRA Cleanup Slams Report No. 5 1-3 044720

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v-^i_iL_iLJl_,'| jQi I, If^ iN.;lHhi rfr

500 0 500 100015002000 FeetSite LocationThomas County

BLACK & VEATCH

Figure 1-1Site LocationAce Services Site

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2.0 Long Term Response Action Objectives

The objectives of the LTRA are to support completion of groundwater RA activities including

assessment of the RA. Assessment of the RA will include identification of treatment goals and exit

strategy, evaluation of the performance and effectiveness of the overall RA, and evaluation of

system cost-effectiveness.

2.1 Treatment Goals and Exit StrategyIn accordance with the ROD, the primary goal of the groundwater RA for the Ace Services

site is to remediate groundwater contaminated with chromium (total) to concentrations below the

current maximum contaminant level (MCL) of 100 micrograms per liter (ug/L). The RA objective

will be attained by extracting contaminated groundwater using 13 extraction wells installed at

shallow, intermediate, and deep depths and treating the contaminated groundwater by directing the

contaminated groundwater through ion exchange resin beds.

The treated water is being discharged to the Prairie Dog Creek Tributary or beneficially

used by being pumped to the City of Colby drinking water system. Treatment goals for the

extracted groundwater have been established in the ROD. Treated water discharged to the Colby

drinking water system or to the Prairie Dog Creek Tributary must contain no more than 17 ug/L

hexavalent chromium and no more than 100 ug/L total chromium.

In support of the RA goal, KDHE has extended the public water system in Colby along

Highway 24 to make public water available to residents with private wells located within or in

proximity to the chromium plume. The new water lines and meters were installed at the end of

September 2003 and connected to residential plumbing by October 15,2003. The majority of

residents with private wells chose to switch to public water with service starting between

October 17 and November 19, 2003.

The groundwater RA will be completed when groundwater is remediated to chromium (total)

concentrations below the current MCL of 100 ug/L. The RA may be revised as appropriate

because of revised regulatory framework, new treatment technologies or strategies, the goal is

determined to be unrealistic, elevated costs, changes in plume extent, ordiscovery of additional

and/or cont inuing sources of contamination.

2.2 Performance and EffectivenessEvaluation of accomplishing the groundwater RA treatment goals and exit strategy include

groundwater monitoring, evaluation of plume capture, treatment process monitoring, and evaluation

Ace Services SiteLTRA Cleanup Stains Report No. 5 2-1 (W4720

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of extraction well performance. During the performance period covered in this report (April

27, 2005 to October 12,2005), two performance audits of the operation of the GWTS were

conducted. Results of the performance audits are described in Quarterly Audit Report No. 7

(BVSPC 2005d) and Quarterly Audit Report No. 8 (BVSPC 2005e) which are included in this

report as Appendices H and I, respectively. Results of the performance audits are summarized in

the text of this report.

2.2.1 Groundwater Monitoring

Groundwater monitoring has been performed to evaluate remediation of the groundwater.

Groundwater samples were collected from site monitoring wells, extraction wells, and residential

wells and analyzed for total chromium to determine the plume extent. Groundwater elevations were

measured in all monitoring wells and extraction wells to evaluate the capture zone of the extraction

field.

Monitoring wells were sampled and analyzed for total chromium in April 2003 to determine

the extent of the chromium plume prior to groundwater extraction efforts. The results of the

baseline study are described in the Remedial Action Groundwater Contamination Baseline

Technical Memorandum (BVSPC 2003e).

Plume capture and treatment process efficiency was evaluated using groundwater monitoring

results. All wells were sampled in October 2005 as part of the semi-annual sampling effort.

Beginning in October 2004, the sampling frequency was revised from a bi-monthly sampling effort

for selected wells to a semi-annual effort for all wells. The sampling schedule is to be re-evaluated

semi-annually. The current sampling frequency of sampling all wells on a semi-annual basis appears

to be appropriate at this time.

Sampling procedures for the groundwater monitoring efforts are as described in the FSP

(BVSPC 2003a) and QAPP (BVSPC 2003b) prepared for the LTRA site activities. Completed

water level data sheets, well purging forms, sample field sheets, chain-of-custody forms, air bills,

field logbooks, and analytical result data sheets are provided in Appendices A, B, C, D, E, F and

G, respectively.

Analytical groundwater monitoring data for the site are included on Table 2-1. Groundwater

elevations in the wells that were determined from water level measurements made on October 3,

2005 are presented in Table 2-2.

2.2.2 Plume CaptureThe pumping rates are to be modified as necessary to capture the target plume as the target

plume extent varies. The target plume includes groundwater with concentrations above the current

Ace Services SiteLTRA Clcminp Slums Rcpon No. 5 2-2 044720

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cleanup goal of 100 ug/L. Approximate pumping rates for each extraction well are provided in

Table 2-3. As indicated, the pumping rates for the extraction wells are adjusted as necessary in

response to plume extent, aquifer conditions, and available well yield to capture the target plume.

Pumping rates at wells EX-2-S and EX-4-S have been turned off; wells EX-3-S and EX-5-S have

been reduced because of low watertable conditions; and wells EX-1 -I, EX-1 -D, EX-4-I/D and

EX-5-I/D have been increased to support plume capture. The other extraction wells were

operated at or above proposed pumping rates unless temporarily shut down for maintenance or

repair. Details concerning operation of the well field are provided in the attached performance

audit reports (Appendices H and I).

The capture zone of the wel 1 field can be interpreted from groundwater potentiometric surface

maps which are illustrated on Figures 2-1,2-2, and 2-3, respectively. Groundwater potentiometric

surface maps were prepared using G1S software with a contour extension which provides a

statistical approximation of the groundwater table contour. The extent of the 100 ug/L chromium

isoconcentration contours for the shallow, intermediate, and deep zones in October 2005 are

illustrated in addition to the groundwater table contour on Figures 2-1,2-2, and 2-3, respectively.

The data on the figures indicate that the capture zone created by the extraction field has created

hydraulic control of the target chromium plume. Figure 2-4 illustrates the groundwater flow

direction in vertical cross section for October 3,2005. Data plotted on Figures 2-5,2-6,2-7, and

2-8 also indicate a decreasing trend in chromium concentrations in groundwater at the site.

A comparison of the current chromium isoconcentration contours (October 2005) to the

baseline chromium isoconcentration contours (April 2003) on Figures 2-1,2-2, and 2-3 indicate

that the chromium plume has significantly reduced in extent since start-up of the GWTS in

August 2003. However, data were showing a gradual increase i n chromium concentrations in the

area of the former treatment plant. The concentration of chromium in the shallow zone of the Ace

Recovery Well (ARW), and to a lesser extent in the intermediate and deep zones, had increased

significantly since startup of the GWTS. Recently however, chromium concentrations have

decreased since the last sample round conducted in April 2005. In the shallow zone, the chromium

concentration increased from approximately 17 ug/L total chromium in April 2003 to 3810 ug/L

total chromium in April 2005 and has now decreased to 1600 ug/L. The concentration increase

at the ARW is most likely attributable to chromium leaching from residual source material that

remains on the former plating facility. To support capture of the chromium plume in this area, the

pumping rates of wells EX-1 -1 and EX-1 -D were increased immediately upon review of the draft

sampling results in April 2005 and currently remain at the higher pumping rates

Chromium concentrations in residential wells continue to remain below detection or continue

to decrease as indicaied in Table 2-1 except for well RW-5 which showed an increase in

Ace Services SiteLTRA Cleanup Slams Report No. 5 2-3 044720

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chromium to 36.2 ug/L. Chromium concentrations at RW-2 temporarily increased from non-detect

in April 2004 to 61 ug/L in October 2004, however, the chromium concentration has been

decreasing in subsequent sample rounds as indicated in Table 2-1. The chromium concentration

at well RW-8, which is located downgradient of the eastern most extraction well, has decreased

since the extraction wells were brought online which indicates sufficient extraction efforts at.

EX-4-1/D and 5-I/D to achieve adequate control of the eastern portion of the plume.

The groundwater monitoring data indicate that the remedial goals are achievable and the

groundwater monitoring program is adequate for evaluating the remedial action. The groundwater

monitoring data do not indicate the presence of contaminant source areas other than the former

plating facility.

2.2.3 Groundwater Treatment System Performance Monitoring

Performance monitoring of the GWTS includes monitoring of key plant operations and

evaluation of conformance to specified requirements for system operation by the plant operator

(City of Colby). The audits include a site visit to observe the City of Colby operators and obtain

key plant operating data on a quarterly basis. The results of the quarterly performance monitoring

evaluations are detailed in quarterly performance audit reports. The quarterly performance audit

reports prepared for the two audit periods included in this reporting period are presented in

Appendices H and I. Performance monitoring results are summarized in Table 2-4. Overall, the

GWTS is performing at design expectations.

2.2.4 Extraction Well Performance

Evaluation of extraction well performance will be conducted regularly to maintain optimum

well efficiency. Reduction of more than 10% in the specific capacity of an extraction well may

indicate well fouling. Well fouling is blockage of the well screen which occurs from bacterial

growth and chemical precipitation in the screen portion of the wells. Well rehabilitation was last

completed for all extraction wells in December 2004.

2.3 System Cost-EffectivenessAn evaluation of cost-effectiveness of the treatment system was performed to optimize RA

efforts. The evaluation compared actual costs of operation to projected costs which were

validated as cost effective in comparison to other potential remedial options. In addition, the

evaluation considered upgrades or replacement of system elements that may improve overall cost

effectiveness and/or reduce remediation time. Continuous improvement can occur by periodically

Ace Services SiteI.TRA Cleanup Slnlus Report No. 5 2-4 044720

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evaluating goals, performance, and cost effectiveness and then implementing changes from these

evaluations.

As discussed in Quarterly Performance Audit Reports No. 1 and No. 8 (Appendices H and

I), the treatment cost including only cost for resin, transportation, and disposal and excluding labor

and utilities, which are not available, is 0.155 cents per gallon during the seventh audit period and

0.152 cents per gallon during the eighth. This is an increase from 0.130 cents per gallon during the

sixth audit period when the average chromium loading was essentially the same and it is evidence

of the poor resin performance during the seventh and eighth audit periods. This is still a significant

reduction from 0.210 cents per gallon from the performance test and 0.166 cents per gallon from

the first audit period when average influent chromium concentrations were higher. These costs

demonstrate the efficiency of the ion exchange process in this application. There is insufficient data

at this time to compute the total cost per gal Ion to treat the extracted groundwater including labor

and plant utilities. However, it is anticipated that these costs will be a relatively small part of the

total.

GWTP data indicate that as the average influent chromium concentration drops below about

300 ug/L, an increase in the gallons treated per bed is not achieved. Every bed with an average

chromium influent concentration below 350 ug/L treated between 31 and 35 million gallons of

water with no correlation to chromium concentration. Substantial resin quality problems were

encountered during the seventh and eighth audit periods resulting in poor resin performance.

During this time period, resin treatment performance dropped to between 26 and 30 million gallons

treated per bed. The resin quality issues were resolved by the end of the eighth audit period.

Further details are provided in section 2.3 of the seventh and eighth audit reports (Appendicies H

and J). Now that the resin quality issues have been resolved, unless the influent chromium

concentrations again rise above 350 ug/L, each bed can be anticipated to treat approximately

33 million gallons of groundwater from the extraction wells.

Upgrades or replacement of system elements that may improve overall cost effectiveness

and/or reduce remediation time, treatment goals, performance, and cost effectiveness are evaluated

as an ongoing part of the LTRA effortand are discussed in the attached quarterly performance

audit reports.

Ace Services SileLTRA Cleanup Status Report No. 5 2-5 044720

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Table 2-1Analytical Results Summary

April 2003 through October 2005

Ace Services Site

Well

Number

Tots

(ucApril2003

October2003

Shallow WellsMW 1 SMW 2 SMW 4 SMW 5 SMW 6 SMW 7 SMW 8 SMW 9 SMW 11 SMW 12 SMW 13 SMW 14 SMW 15 SMW 16 SMW 17 SMW 18 S

ARW - SOB 1 SOB 2 S

HPMW 3 SHPMW 6 SHPMW 9 S

EX 2 SEX 3 SEX 4 SEX 5 S

1.1 U60.13.82.6

1.9(1.8)48.11850285

182

36.4 (36.1)173

133204

1.7

25.164.617.1279

360-

1.4

0.91-

.

-

15 U2315 U15 U15 U15 U15 U19

60

15 U152

51

200

15 U15 U42

55215 U61

15 U-

-

41

184

8162

April2004

15 U19.115 U15 U15 U4515 U116

19.115 U

92.8 (97.9)23.5232

15 U15U(15U)

15 U164025.8458

--

780

203

113

15 U20.4

slCr/L)

October2004

15 UJ15 U

l~ 15 U15 U15 U

314

23.1193

26.515 U

43.522.519915 U15

15 U261050.156.5

-

15 U-

10693.415 U

25.9

April2005

15 U15 U15 U15 U15 U

45.715 U15 U15 U15 U15 U15 U10315 U15 U15 U

381015 U15 UJ-

15 U--

15 U15 U15 U

October2005

10 U10 U10 U10 U10 U

10.937.659

14.210.610 U

10.6111

10 U11.410 U

160010 U

30.3-

10 U17.2

-

33.817.921.6

Ace Services SileLTKA Cleanup Status Report No. 5 2-6 044720

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Table 2-1 (Continued)Analytical Results Summary

Apr i l 2003 through October 2005Ace Services Site

Well

Number

Tots

(ucApril2003

October2003

April2004

Intermediate WellsMW 1MW 2MW 4MW 5MW 6MW 7MW 8

MW 9MW 11MW 12

MW 13MW 14MW 15MW 16MW 17MW 18

ARW -OB 1OB 2EX 1EX 2EX 3EX 4 I/CEX 5 I/C

PWS 8

0.7 U949 (1000)24.7

10.9(10.8)14.513.21960

1920267

132

283

10756.43.83.9

17.94.9155

408---

--

-

15 U955 (953)

15 U15 U15 U15 U56

416

103(105)113

110

143

171

15 U15 U15 U

26585

15 U1390527 (548)

-

156116940

15 U1580

15 U15 U15 U15 U

89.2 (87)

168019.118.3

58.644.9121

15 U15 U15 U

111077.2111

1060997

311

14593.22290

alCr/L)

October2004

15 U1160

15 U15 U15 U

29.252.5

258

15 U15 U

35.6 (24.6)30.320.515 U15 U15 U

123079.8207

1360553296

10688.21190

April2005

15U(15U)686 (678)

15 U15 U15 U15 U15 U

15.715 U15 U

15 U15 U15 U15 U15 U15 U

169015 U170

953

205145(156)

43.127.0443

October2005

10 U40610 U10 U10 U10 U

10.7(10.4)

1710 U10 U

10

13

10 U10 U10 U10 U

794

10 U132926

181135

61

51350 (344)

Ace Services SiteLIRA Cleanup Status Report No. 5 2-7 044720

Page 16: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Table 2-1 (Continued)Analytical Results Summary

April 2003 through October 2005Ace Services Site

Well

Number

Tots(uc

April2003

October2003

April2004

Deep WellsMW 1 D

MW 2 DMW 3 DMW 4 DMW 5 DMW 6 DMW 7 DMW 8 D

MW 9 DMW 11 DMW 12 DMW 13 D

MW 15 D

MW 16 DMW 17 DMW 18 D

ARW - DOB 1 DOB 2 DEX 1 DEX 2 DEX 3 D

5.6

1846.7

1.6

1.810826.1478

33406823.7 (3.6)221

1240(1260)2

22.1132

6.4

12902770

--

-

15 U

35

15 U15.9(16.4)

15 U71

15 U15 U

15 U15 U15 U70

999

15 U15 U15 U

68

99

228

34

485

409

15 U

16833515 U15 U

33.733.893.4

1620(1650)15 U15 U15 U

273

15 U15 U15 U

194

513

604

53.7485

177

j lCr/L)

October2004

15 U85.415 U

46.415 U

20.835.415 U

121

15 U15 U15 U

134

15 U15 U15 U

188(198)60.6257

53.7331

78

April2005

15 U

55.215 U15 U15 U15 U15 U15 U

15 U15 UJ15 U15 UJ

41.715 U15 U15 U

291

15 U51.9

15U(15U)11915.4

October2005

10 U

10U(10U)10 U10 U

21.110 U10 U10 U

10.110 U10 U10 U

37.210U(10U)

10 U10 U

277

10 U11.617.453.836.9

Ace Services SiteLIRA Cleanup Status Report No. 5 2-8 044720

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Table 2-1 (Continued)Analytical Results Summary

April 2003 through October 2005Ace Services Site

Well

Number

Total Cr(ug/L)

April2003

October2003

April2004

Residential WellsRW 1RW 2RW 3RW 4RW 5RW 6RW 7RW 8RW 9

27.11.93.23.66.294.147.575.72.4

-15 U15 U15 U15 U5517

63

15 U

-15 U15 U15 U15 U15 U15 U

74.315 U

October2004

-6115 U15 U15 U15 U15 U

50.115 U

April2005

-22.115 U15 U15 U15 U15 U15 U15 U

October2005

-11.210 U10 U

36.210 U10 U

29.910 U

Duplicate results in parenthesesCr = chromium

ug/L = microgram per literU = qualified as nondetectJ = qualified as nondetectS = shallow

I = intermediateD = deep

MW = monitoring wellHPMW = Hi-Plains Co-op monitoring wellOB = Observation WellARW = Ace Recovery wellPWS = public water supplyRW = residential wellEX = extraction wellSC = sample connection

Ace Services SilcLTRA Cleanup Status Report No. 5 2-9 044720

Page 18: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Table 2-2Groundwater Elevation Data

October 2005Ace Services Site

WellMW-1-S

MW-1-1

MW-1-D

MW-2-S

MW-2-I

MW-2-D

MW-3-D

MW-4-S

MW-4-I

MW-4-D

MW-5-S

MW-5-I

MW-5-D

MW-6-S

MW-6-I

MW-6-D

MW-7-S

MW-7-I

MW-7-D

MW-8-S

MW-8-I

MW-8-D

MW-9-S

MW-9-I

MW-9-D

MW-11-S

MW-11-1

MW-11-D

ConstructedTotal Depth (ft)

125

162

220

123

195

237

220

120

179

229

120

185

230

132

190

237

140

190

243

132

195

239

132

190

236

140

200

248.5

Top of CasingElevation (ft)

3141.62

3141.63

3141.11

3136.17

3136.07

3137.72

3138.15

3127.79

3128.13

3128.30

3131.75

3131.63

3132.27

3137.70

3137.78

3137.97

3149.07

3148.93

3148.74

3140.79

3140.20

3139.90

3143.63

3143.48

3143.26

3149.47

3149.88

3150.35

October 3, 2005Depth to Water

from Top ofCasing (ft)

115.22

115.35

114.95

113.33

115.59

120.33

116.57

107.12

107.76

110.93

112.72

112.65

117.20

115.18

115.53

117.48

129.53

129.70

132.29

122.50

121.96

122.22

125.99

12841

133.53

133.55

134 33

137.54

GroundwaterElevation(ft MSL)3026.40

3026.28

3026.16

3022.84

3020.48

3017.39

3021.58

3020.67

3020.37

3017.37

3019.03

3018.98

3015.07

3022.52

3022.25

3020.49

3019.54

3019.23

3016.45

3018.83

3017.98

3017.68

3015.22

3009.95

3009.73

3015.92

3015.55

3012.81

Ace Services SilcLTRA Cleanup Slams Report No. 5 2-10

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Page 19: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIIIIIIIIIIIIIIII

Table 2-2 (Continued)

Groundwater Elevation Data

October 2005

Ace Services Site

WellMW-12-S

MW-12-1

MW-12-D

MW-13-S

MW-13-1

MW-13-D

MW-14-S

MW-14-1

MW-15-S

MW-15-1

MW-15-D

MW-16-S

MW-16-1

MW-16-D

MW-17-SMW-17-1

MW-17-D

MW-18-S

MW-18-1

MW-18-D

OB-01-S

OB-01-1OB-01-D

OB-02-S

OB-02-I

OB-02-D

HPMW-3-S

HPMW-6-S

HPMW-9-S

HPMW-12-S

ConstructedTotal Depth (ft)

165

211

263.5

165

211

263.5

165

211

165

211

263.5

165

211

263.5

165

211

263.5

165

211

263.5

165

211

263.5

165

211

263.5

124.7

124.63

125

115

Top of CasingElevation (ft)

3169.43

3169.54

3169.35

3155.56

3156.39

3156.93

3161.27

3161.05

3161.53

3162.63

3163.63

3159.41

3160.29

3161.07

3165.66

3165.38

3164.78

3164.60

3165.09

3165.18

3143.88

3143.50

3143.17

3140.78

3139.84

3139.31

3139.74

reconst.

reconst.

3137.14

October 3, 2005Depth to Water

from Top ofCasing (ft)

156.02

156.67

158.00

139.99

141.59

143.95

149.77

149.99

148.38

150.64

152.22

142.60

143.67

146.08

151.67

151.61

152.37

152.78

153.55

154.55

126.34

128.05

131.89

123.39

124.06

127.95

-

113.97

112.19

110.14

GroundwaterElevation(ft MSL)3013.41

3012.87

3011.35

3015.57

3014.80

3012.98

3011.50

3011.06

3013.15

3011.99

3011.41

3016.81

3016.62

3014.99

3013.99

3013.77

3012.41

3011.82

3011.54

3010.63

3017.54

3015.45

3011.28

3017.39

3015.78

3011.36

-

-

.

3027.00

Ace Services SiteLIRA Cleanup Status Report No. 5 2-11

044720

Page 20: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Table 2-2 (Continued)Groundwater Elevation Data

October 2005Ace Services Site

WellEX-1-1

EX-1-D

EX-2-S

EX-2-I

EX-2-D

EX-3-S2

EX-3-I2

EX-3-D

EX-4-S3

EX-4-I/D

EX-5-S1

EX-5-I/D

PWS-8"

ConstructedTotal Depth (ft)

220

245

140

205

245

175

215

265

168

273

175

278

250

Top of CasingElevation (ft)

3137.62

3137.71

3145.52

3144.96

3144.98

3156.28

3155.85

3155.60

3165.52

3164.72

3162.59

3161.36

3142.10

October 3, 2005Depth to Water

from Top ofCasing (ft)

120.20

129.50

128.02

140.20

154.70

144.08

154.10

150.30

152.10

162.00

153.85

156.30

127.45

GroundwaterElevation(ft MSL)3017.42

3008.21

3017.50

3004.76

2990.28

3012.20

3001.75

3005.30

3013.42

3002.72

3008.74

3005.06

3014.65

1TOC trimmed and survey reference adjusted on 10-06-032TOC trimmed and survey reference adjusted on 03/15/04: EX-3-S = 3156.28, EX-3-I = 3155.85

^TOC trimmed and survey reference adjusted on 04/05/04. EX-4-S = 3165.52

"Survey reference adjusted on 06/08/04: MW-2-D = 3137.07 + 0.65 = 3137.72, PWS-8 = 3143.080.98 = 3142.10MSL = mean sea level

Ace Services SiteLIRA Cleanup Status Report No. 5 2-12

044720

Page 21: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Table 2-3Treatment GoalsAce Services Site

Well

EX-1-1

EX-1-D

EX-2-S

EX-2-I

EX-2-D

EX-3-S

EX-3-I

EX-3-D

EX-4-S

EX-4-I/D

EX-5-S

EX-5-I/D

PWS-8

Top ofCasing

Elevation(ft)

3137.62

3137.71

3145.52

3144.96

3144.98

3156.28

3155.85

3155.60

3165.52

3164.72

3162.59

3161.36

3142.10

GroundElevation1

(msl)

3136.4

3136.4

3143.7

3143.7

3143.7

3154.4

3154.4

3154.4

3163.6

3163.6

3160.5

3160.5

3141.3

ConstructedTotal Depth

(ft bgs)

220

245

140

205

245

175

215

265

168

273

175

278

250

WellScreenLength

(ft)

55

30

30

50

40

35

40

50

20

90

20

95

10

5

10

25

Well ScreenInterval(ft bgs)

155 - 210

205 - 235

100 - 130

145 - 195

195 - 235

130 - 165

165 - 205

205 - 255

138 - 158

173 - 263

145 - 165

173 - 268

128 - 138

145 - 150

190 - 200

215 - 240

Well ScreenInterval

Elevation(msl)

2981 - 2926

2931 - 2901

3044 - 3014

2999 - 2949

2949 - 2909

3024 - 2989

2989 - 2949

2949 - 2899

3026 - 3006

2991 - 2901

3015 - 2995

2988 - 2893

3013 - 3003

2996 - 2991

2951 - 2941

2926 - 2901

total pumping rate =

ModeledInitial

ProposedPumping

Rate (gpm)

35 2

40 2

25 2

100 2

100 2

25 2

50 2

75 2

25 2

100 3

25 2

100 3

125 2

825 gpm

April2005

PumpingRate (gpm)

35

40

O 4

85 8

100

20 5

50

75

O 6

125 7

20 5

125 7

125

800 gpm

May2005

PumpingRate (gpm)

35

40

O 4

85°

100

20 5

50

. 75

O 6

125 7

20 s

125 7

125

800 gpm

June2005

PumpingRate (gpm)

70 9

70s

O 4

85 8

100

20 5

50

75

0 s

125 7

20 =

125 7

125

865 gpm

July2005

PumpingRate (gpm)

70 9

70 9

O 4

85 8

100

20 5

50

75

O 6

125 7

20 5

125 7

125

865 gpm

August2005

PumpingRate (gpm)

70 9

70 9

O 4

85 e

100

20 5

50

75

O 6

125 7

20s

125 7

125

865 gpm

September2005

PumpingRate (gpm)

70 9

70 9

O 4

100

100

20 5

50

75

O 6

125 7

20 5

125 7

125

880 gpm

October2005

PumpingRate (gpm)

70 9

70 9

O 4

100

100

20 5

50

75

O 6

125 7

155

125 7

125

875 gpm

CurrentProposedPumping

Rate (gpm)

70 9

70 9

O 4

100

100

20 5

50

75

O 6

125 7

155

125 7

125

875 gpm

Note 1 = Pad Elevation from Carlson's Surveying & Mapping Inc. January 16, 2003;

Note 2 = Addendum No. 2 Technical Memorandum RD Sampling Activities December 19, 2001;

Note 3 = Addendum No. 3 Technical Memorandum RD Sampling Activities July 2, 2002;

Note 4 = Groundwater in EX-2-S drawn down to unsustainable pumping level by EX-2-I and EX-2-D.

Note 5 = Pumping rate reduced because of low aquifer conditions.

Note 6 = Well not running because of low aquifer conditions.

Note 7 = Pumping rate for wells EX-4-I/D and EX-5-I/D increased to supportcapture of downgradient plume (BVSPC 2004a);

Note 8 = pumping rate reduced due to partial pump failure

Note 9 = Pumping rate for well EX-1-1 and EX-1-D increasesd to support captureof increased chromium concentrations at the Ace Recovery Well.

Ace Services SiteLTRA Cleanup Status Report No. 5 2-13 044720

Page 22: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Table 2-4Performance Monitoring Results

Ace Services Site

Month(Current Reporting Period)

Last part April 2005

May 2005

June 2005

July 2005

August 2005

September 2005

Early part October 2005

Total Influent(million gallons)

3.4

32.5

32.6

36.5

37.1

34.6

15.2

Chromium Removed(kg)

3.5

26.8

25.1

29.2

29.6

23.8

10.6

Previous Performance Periods

June 13, 2003- July 18, 2004(Performance Test)

Aug. 12, 2003 -Oct. 1, 2003(Audit Report No. 1)

Oct. 1 , 2003 - Feb. 16, 2004(Audit Report No. 2)

Feb. 17, 2004- June 6, 2004(Audit Report No. 3)

June 6, 2004 - Oct. 4, 2004(Audit Report No. 4)

October 5, 2004 - Feb. 28, 2005(Audit Report No. 5)

March 1 , 2005 - April 26, 2005(Audit Report No. 6)

April 27, 2005 - July 20, 2005(Audit Report No. 7)

July 21, 2005 - October 12, 2005(Audit Report No. 8)

Groundwater Treated(million gallons)

41

54

83

71

94

140

62

90

102

Total Chromium removed June 2003 through October 2005 =

Chromium Removed

(kg)

136

105

74

48

95

184

52

72

76

842

Treatment Criteria

Max Drinking Water Acceptance Criteria =

1 7 ug^L hexavalent chromium

100 ug/L total chromium

100 ug/L total chromium

Ace Services SiteLIRA Cleanup Stain Report No. 5 2-14 044720

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Page 24: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII
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Page 26: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII
Page 27: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII
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Page 31: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I• 3.0 Bibliography

' BVSPC 1 998a, Remedial Investigation Report, Ace Services Site, October 1 998.

I BVSPC 1 998b, Final Feasibility Study, Ace Services Site, November 1 998.

| BVSPC 2003a, Field Sampling Plan, Ace Services Site, July 2003 .

| BVSPC 2003b, LTRA Quality Assurance Project Plan, Ace Services Site, July 2003.

I BVSPC 2003c, LTRA Health and Safety Plan, Ace Services Site, July 2003.

I BVSPC 2003d, General System Operation & Maintenance Manual Ground Water Treatment

Plant, Ace Services Site, May 2003.

* BVSPC 2003e, Remedial Action Groundwater Contamination Baseline Technical

M Memorandum, Ace Services Site, August 7, 2003.

BVSPC 2003 f, LTRA Audit Report No. 1, Ace Services Site, November 1 0, 2003 .^

BVSPC 2004a, LTRA Semi-Annual Cleanup Status Report, Ace Services Site, January 9,

2004.

I BVSPC 2004b, LTRA Audit Report No. 2, Ace Set-vices Site, March 1 9, 2004.

• BVSPC 2004c, LTRA Annual Cleanup Status Report, Ace Services Site, June 9, 2004.

• BVSPC 2004d, LTRA Audit Report No. 3, Ace Services Site, July 2, 2004.

_ BVSPC 2004e, LTRA Audit Report No. 4, Ace Services Site, November 1 9, 2004.

BVSPC 2004f, LTRA Cleanup Status Report Number 3, Ace Services Site, December 22,

I 2004.

IAce Services Silc

• LTRA Cleanup Status Report No. 5 3-1 044720

Page 32: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

BVSPC 2005a, LTRA Audit Report No. 5, Ace Services Site, April 22, 2005.

BVSPC 2005b, LTRA Audit Report No. 6, Ace Sen'ices Site, June 24, 2005.

BVSPC 2005c, LTRA Cleanup Status Report Number 4, Ace Services Site, July 20, 2005.

BVSPC 2005d, LTRA Audit Report No. 7, Ace Services Site, August 26, 2005.

BVSPC 2005e, LTRA Audit Report No. 8, Ace Services Site, November 18, 2005.

Fetter, C. W., 1988, Applied Hydrogeology, Merrill Publishing Co., Columbus, Ohio.

USEPA 2001, Amended Record of Decision, Ace Services Site, September 13, 2001.

USEPA 2002, Elements for Effective Management of Operating Pump and Treat Systems,

542-R-02-009, OSWER 9355.4-27FS, October 2002.

Ace Services SilcLTRA Cleanup Siauis Report No. 5 3-2 044720

Page 33: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIII

Appendix A

Water Level Data Sheets

IOctober 2005

I

I

I

I

I

iiiiii

Page 34: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

10-03-05Water Level Data Sheet

Ace Services Site LIRA PVCAfeovlE

Well Date Time

WaterLevel from

TOC (ft)

TotalDepth (ft

bgs) Well Date Time

WaterLevel from

TOC (ft)

TotalDepth (ft

bgs) Well Date Time

WaterLevel from

TOC (ft)

TotalDepth (ft

bgs)

MW-1-S KJ03 125 MW-12-S 165 ARW-S 125-135

MW-1-1 162 MW-12-1 211 ARW-I 161-171

MW-1-D 7003 i 220 MW-12-D 264 ARW-D 209-225

MW-2-S 123 MW-13-S TOOP 7635 769.39 143 NA- NA-

MW-2-I 195 MW-13-1 74/^59 206 RW-2 NA NA

MW-2-D 237 MW-13-D ATP 265 RW-3 NA NA

RW-4 NA NA

MW-3-D 220 MW-14-S m& 744C 155 RW-5 NA NA

MW-14-1 IQtCft 217 RW-6 NA NA

MW-4-S 120 RW-7 NA NA

MW-4-I 179 MW-15-S 165 RW-8 NA NA

MW-4-D

MW-5-S

229 MW-15-1 7-W57 213 RW-9 NA NA

MW-15-D 267 HPMM&10/O3120 -HPMW-S-S

10.fr125

MW-5-I 185 MW-16-S iom 155 (luA-T ye. UMW-5-D 230 MW-16-1 215 EX-1-1

MW-16-D xShstsffl 275 EX-1-D

MW-6-S 132 HPHW& 7QTJ9MW-6-I 190 MW-17-S ro/r? 158 jKEX-2-S* 140

MW-6-D 237 MW-17-1 / 0 3 A5/.6T 205 EX-2-I ,& Mos tooMW-17-D 1S16 1623? 265 I^EX-2-D

MW-7-S 140 UPHW-S 113MW-7-I 190 MW-18-S mz 165

MW-7-D 243 MW-18-1 G3 225 Iftfift .7OaT215

MW-18- 265

MW-8-S 132

MW-8-1 195 OB-1-S 130 158.70°MW-8-D 239 OB-1-1 195 ^EX-4-l/D X^OC^^s

OB-1-D 235

MW-9-S 132 JKEX-5-S /Oilf lMW-9-1 190 OB-2-S 130 EX-5-I/D fegg.a?aT27BMW-9-D 236 OB-2-I 192

OB-2-D 235 PWS-8 250

MW-11-

MW-11-1

MW-11-D

140

200 - SC-1- NA NA

249 SC-9 NA NA' t>6 Pb* Water level only

Inspector GARY E * KfM

TOP Or

Ace Services Site - LTRA

Form Revision 6/4/2004 BVSPC 46132

Page 35: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Water Level Data Sheet

Ace Services Site LTRA

Well

MW-1-S

MW-1-1

MW-1-D

MW-2-S

MW-2-I

MW-2-D

MW-3-D

MW-4-S

MW-4-I

MW-4-D

MW-5-S

MW-5-I

MW-5-D

MW-6-S

MW-6-I

MW-6-D

MW-7-S

MW-7-I

MW-7-D

MW-8-S

MW-8-I

MW-8-D

M%MB^ "

TfBtP&^m'

Mgg»

MW-11-S

MW-11-1

MW-11-D

Date

'0/3/&

&*&*

0$-±523:^£

Time

Jlo3

P-V32'-eS

IS"'2 ',50

p:-<9

2:*7P-.Y5-

?:?3

^••333,'5-t?:•>?

3'~tf

y:/7

?•'*

J:*7Z>\tt

Z'/L

D:do212'p. 21

3:0?

•J.'07

->;05

WaterLevel fromTOC (ft)

//J.3J

//s; 5-9-

l36'3*>

I07.ll

I0l.^

,/C.1*>

\&.-l3*

//5>.&sr

rtf^o

//-5, 1 1

nsv**//7,V«

.',99. S3/<? f. 70

/J*-P9

/AP-30

!*>.</(.I2.T-.L.L

133, 3?APY. o^/<?7. *T

/35-^/3V- 53

/3> s-V

As-BuiltTotal

Depth (ttbgs)

|_ 125

162 /

220

123

195

237

220

120

179

229

120

185

230

132

190

237

140

190

243

132

195

239 X

132

190 >'

236

140

200

249

Well

MW-12-S

MW-12-1

MW-12-D

MW-13-S

MW-13-1

MW-13-D

MW-14-S

MW-14-1

MW-15-S

MW-15-1

MW-15-D

MW-16-S

MW-16-1

MW-16-D

MW-17-S

MW-17-1

MW-17-D

MW-18-S

^W-18-l

MW-18-D

OB-1-S

OB- 1-1

OB-1-D

ta^^^^ar^^^^^^

T*^*OK>-

Date

°&

HfTIM-W

Time

3- It

•j:<Y

3;/a

\^/YarH«

^:V<?

^orI437

WaterLevel fromTOC (ft)

/rc.ojL/5t.b>

/5» ^a

(2^^12$^

;ii.W

05, 77/^. y/133,5-?

AS-bUlltTotal

Depth (ftbgs)

165

211

264

143

206

265

155

217

165

213

267

155

215

275

158

205

265

165

225

265

130

195

235

130

192

235

Well

ARW-S

ARW-I

ARW-D

RW-1

RW-2

RW-3

RW-4

RW-5

RW-6

RW-7

RW-8

RW-9

HPMW-3-S*

HPMW-6-S

HPMW-9-S

HPMW-12-S*

EX-1-1

EX-1-D

EX-2-S

EX-2-I

EX-2-D

EX-3-S

EX-3-I

EX-3-D

EX^I-S

EX-4-I/D

EX-5-S

EX-5-I/D

PWS-8

Date Time

WaterLevel fromTOC (ft)

NA

NA

NA

NA

NA

NA

NA

NA

NA

"

AS-bUlltTotal

Depth (ftbgs)

125-135

161-171

209-225

NA

NA

NA

NA

NA

NA

NA

NA

NA

125

125

125

115

210

235

130

195

235

165

205

255

158

263

165

268

240 -

" Water level only.

Inspector

Ace Services She

I.TKA I-SP

I

I

I

Page 36: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIIIM Appendix B

Well Purging Forms

IOctober 2005

I

iiiiiiiii

Page 37: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

1I

1

1•111111111111111

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

PffiMm&FflviCE£ LTRAP^Numbw044?iaO.O/.4?

NGUMWELL DATA 1 r\£Total Well Depth 1 iffi)

Page 1 of / .

Well Number

MW-1-S ,Date/o- n-m

Well Diameter ^L |nitial Water Level Jlfi.Sj?,Water Column Height $„ 7^Q

3 Well Volumes j(9. / qa

METHOD OF WELL DEVELOPMENTV Pumping

s

Air Lift

Well Vo(x) (height) x=.163 gal/ftlume (gals) f/j i TQ

Amount of Water Removed from Well _/;

Surging Bailing

g 2", (xY6& qal/ft @ 4"1

iy~\t(aLJ 3 aals

Other

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal 'OL/BM£RfS/E>L.E> lUMP Was Well Pumped Dry? Yes Jo)

Method of Sample Collection (DLJBMEJ^I BLJE. lUMP

Physical Appearance

Remarks

TIME

76 1W76 1R1G>£51(bcT)1G>35/Gxjo

TEMP (°C)SPECIFICCONDUC-

TIVITYpH TURBIDITY DO ORP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

WtfotfiGA-/v5.6(2>W.G4.£bLL£

ATTo/.fln?7.5tto/.^?Yorrr

jiA5r»,r^G>Gfi(o.Cofi

MPLE

-n?-1.fi-£n-£4-#/S?r

O4As*\ ^}f*3

^\ ^}^\

Off?,15 -31

TtTvO/fifing

7A9.0

Checked By Date

Version 6-11-04

Page 38: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

fOJGCl iN3JJiG ^» -^ * *"T™ " AAT.?. fiERviCFfi LIRA Project Numbej 4^7^ Q/ 47

WELL DATATotal Well DeInitial Water 1Water Colum

3 Well Volurr

METHOD OF

>pth /uJv», _/ 1 ^^J • ^ T

n Height ^O.Cftl?

es »J7/ . oa

' WELL DEVELOPMENTPumping

METHOD OF SAMPLE C

Method of Water Remova

Method of Sample Collec

Physical Appearance

Remarks

TIME

14O514 ro1414-144914,837485

Mc\u£

Is

Air Lift

Am

Well Diameter 4-

Well Vc

ount of Wate

Surging

OLLECTION/PURGING

\&LJBMERfil RLE PUMPSUBMERSIBLE PUMP

Page / of / .

Well Number

nw-i-i

(x) (height) x=.lB3 gal/ftlume (gals) L^O. ^p

r Removed from Well

Bailing

@ 2", £=^653~gal/ft @ A"

/\_j t Oj aals

Other

Was Well Pumped Dry? Yes ^c^

IAY AFTF-RNOCW. RAIM^C, ALL. DAY.

TEMP (°C)

SPECIFICCONDUC-

TIVITYPH TURBIDITY DO ORP

iFMP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

/^4?j/i4)^1546>154&ChuJ

IffRr.T9//.i9/?/.oQ9rrrS

? ?D6 5S6 GOGG>1

SMPLZ

O.fo

~/./?,•/ \5^^

O-fl?0, 70 ;Lq0.7/S*?&-£&

•PrfifV)

/SWfi'SDisS5oo.ro)

Checked By

Version 6- 14 -04

Date

1

1

1

1

1

1

1

1

1

1

1

I' •

1

1

1

Page 39: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

1E

-

1\

1

1

1

1

1

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Slack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

^^aBte£WCfiS L,TRA Project "^fo^ypQ ^ ^

F,eld lnVest,gator(s) ^ LANGLlM

WELL DATATotal Well Denitial Water IWater Colum

3 Well Volum

METHOD OFV

METHOD OF

Method of W

Method of Si

Physical App

Remarks

TIME

/44iQ

74-4?mi?,7i5fi&1SOS

pth /CTTTJevel 7 /^.£J5nHeiaht IC&.Ofi

es ft~tD5*& ga

WELL DEVPumping

• SAMPLE C

ater Remova

ample Collec

earance

ELOPMENT

Is

Air Lift

Am

Page _]_ of 7 .

Well Number

MW-1-D

Well Diameter 4+

Well Vo

ount of Wate

Surging

OLLECTION/PURGING

. SUBMERSIBLE PUMPuon £)U&MEf&tflL£ PUMP

(x) (height) x=.163gal/tt(lume(gals) ^ofi.5k9

r Removed from Well

Bailing

a 2",Oc=-653 gal/ft (^4n

\J^(^J aals

Other

Was Well Pumped Dry? Yes QNO)

TEMP (°C)SPECIFICCONDUC-

TIVITYPH TURBIDITY DO ORP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

Mx%

l5fXi>fCj.lJL}

Com

Q473R

O.^JJSn^fp•crfiA

?.fi1

?.i*n?.4&?43

MPLF.

f*\ ^\f\^f Q^

-^^g-fi.9-/23^/ft??

J2/39E<fftr^/SSc? OJDr ./CJLJ

/8//i?3££L&/8GG.V5"^9Q^

Checked By Date

Version 6- 14-04

Page 40: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

y^$£R.wc.&5 LTRAi lOIGCl iNLJf I lOcf^^fc j* ^ /^i X^ ^\ /^ W Jt 4^1

1 ^L I * ^^ -*• 1 I 1 f ^^f ^^

WELL DATATotal Well DeInitial Water LWater Colum

3 Well Volum

METHOD OFV

pth /fy!v n ievel 7 70 'C^n Heiqht &.(f7

es /O,C7 aals

WELL DEVELOPMENTPumping Air Lift

METHOD OF SAMPLE C

Method of Water Remova

Method of Sample Collec

Physical Appearance

Remarks

TIME

OflOfnsrtf09/0O91fi0313OSPfi

Page 7 of /

Well Number

MW-Q-SDate/0-CGrOq

/^ // 1Well Diameter 'f- |

(x) (height) x=. 163 gal/ftWell Volume (gals) (t).31

g2",£=.653gal/tt@4")

Amount of Water Removed from Well /OCJ aalsl

Surging Bailing

OLLECTION/PURGING

^SUBMERSIBLE PUMPion SUBMERSIBLE PtJtfP

Other I

Was Well Pumped Dry? Yes CNO)

TEMP (°C)SPECIFICCONDUC- pH

TIVITYTURBIDITY DO ORP

WATER

LEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

A9S4.14.3574,3374./SS£om

JfejL/ fi^QRw ^Aso?4t3 6.A8?43 6.A9

^crAiU^-^ #/87

fl.65aap,fi.\5Ofl.fi?^-/(D

L%8. /

(JlIJLJ 07O "y^ i>>

OfifO /"

Checked By Date

Version 6- 14-04

Page 41: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

111•

1\

111111111111111

Slack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Project Name^ fi£R]/K]& LTR6

Field investigator^)^

A/ELL DATAFotal Well Denitial Water LWater Columr

3 Well Volum

METHOD OF

\/ F

METHOD OF

Method of W

Method of SB

Physical App

Remarks

TIME

flSQS000?

Q9/£09 r 8

pth /<3vevel / /vi Height ^

es /vJO

[*roject Numbb447PO. H/.4?'NMY LANQUMa &?'y . Well Diameter 0(.

Page / of I .

Well Number

MW-fi-I75-O4-Q5

A"T.AS . (x) (height) x=. 163 gal/ft (5> 2". x={653 gal/ft 0)4"i9,4Tf

. C3 gals

WELL DEVELOPMENT3umping Air Lift

SAMPLE C

ater Remova

mple Collec

earance

TEMP (°C)

Well Volume (gals)

Amount of Water Removed from Well

Surging Bailing

OLLECTION/PURGING

i SUBMERSIBLE PUMP.aaaaaiB*-

i^Tr^J gals

Other

Was Well Pumped Dry? Yes ^Jo^

SPECIFICCONDUC- pH

TIVITYTURBIDITY DO ORP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

J6.&16.fi/G.tf

jCbLU

Checked By

cx5a G). (pQO/~ r £tfrLp t^.oflm 6.4&94 G.4

^Tv^/L/F/^ *<?,?*

^^ ^^ ^

^% ^\ ^^

fl./G5/cDUS-/-

. •

4<9£.<9447.3^|V pCj.v

"

Date

Version 6- W -04

Page 42: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Page of

Well Number

Mw-a-nProject Number Date.

JQ-Ot-OSField Investigator(s)

WELL DATATotal Well Depth _Initial Water LevelWater Column Height / ?IQ . Co r

3 Well Volumes ri^AjTVvO gals

METHOD OF WELL DEVELOPMENTPumping Air Lift

Well Diameter _(x) (height) x=.163 gal/ft @ 2", {(=.653 gal/ft"®"?

Well Volume (gals)

Amount of Water Removed from Well.

Surging Bailing

gal

Other

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal lUMP Was Well Pumped Dry? Yes Tic?

Method of Sample Collection

Physical Appearance

Remarks

TIME TEMP (°C)SPECIFICCONDUC-

TIVITYpH TURBIDITY DO ORP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

440•KJ8 P. 00 455.G

iLaaCoLLl

Checked By Date

Version 6- 14-W

Page 43: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Page 1 of

Well Number

AftV-tf-7)Date

KfrNLANCtlMELL DATA

otal Well Depthnitial Water Level /7£o.i57

Well Diameter T*

A/ater Column Height 7Qt3»4*3

Well Volumes /HiJ/^.Cfl gals

METHOD OF WELL DEVELOPMENTPumping Air Lift

(x) (height) x=.163 gal/ft@ 2",g(='.653 gal/n @ 4,Well Volume (gals) £p?.v5o

Amount of Water Removed from Well / fiT)

Surging

.gals

Bailing Other

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal

Method of Sample Collection

hysical Appearance

Remarks

Was Well Pumped Dry? Yes

Version 6-14-04

Page 44: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Page 7 of

Well Number

MlV-4-6LTRA

Project

WELL DATATotal Well Depth .Initial Water Level.Water Column Height

3 Well Volumes

Well Diameter(x) (height) x=. 163 gal/ft

Well Volume (gals) fi.4-1

gals

METHOD OF WELL DEVELOPMENTPumping Air Lift

Amount of Water Removed from Well 7i jiD

Surging Bailing

.gals

Other

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal. > I LIMP Was Well Pumped Dry? Yes

Method of Sample Collection '.PUMP

Physical Appearance

Remarks

TIME TEMP (°C)SPECIFICCONDUC-

TIVITYpH TURBIDITY DO ORP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

COLL zm?.0\ 0.0

mra zoaL 2QS,

Q8SS. t£L ^4Q

Checked By Date

Version 6

Page 45: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

1E

1

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1

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Slack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

ro)e£ am£/ . p, / TRA>A( .fc L~£irxlf f^j£~LJ K _ I / / V \

Project Numbe£ ;?rQ Q ^

Field Investigator(s) / * 1 ^~.KFN LANGUM/VELL DATA y ^Qrntal Well Depth / C^y _ _nitial Water LWater Colum

3 Well Volum

METHOD OF\/ 1

METHOD OF

Method of W

Method of Sc

Physical App

Remarks

TIME

1GSS

lG>fi?/64i&7646Itifin

evel /Ojf- QOnHeiaht Y^-^^T

es /I'V'y.e!) aa

WELL DEVELOPMENT3umpinq

SAMPLE C

ater Remova

imple Collecl

earance

s

Air Lift

OLLECTION/PURGING

i ^~)LJ$r'i&fin/ 1

ion OL/ A7^M5

Page / of T .

Well Number

MW-4-I

Well Diameter ~p-(x) (height) x=. 163 gal/ft (

Well Volume (gals) 4&.51

Amount of Water Removed from Well

Surging Bailing

P>L& PUMP'IBL£ PUMP

a 2",Cx=.653 gal/tt @ A".

1 1(5 aals

Other

Was Well Pumped Dry? Yes Qjo)

TEMP (°C)SPECIFICCONDUC-

TIVITYPH TURBIDITY DO ORP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

w.os74-.fl*/4,WGbL

?/£,

fi?l

<9O4?A9

C7^

7.PJ

?.Q9?. W?./4-

MF/,£

O.<3-QS-o.s-Q4#z?i

(S.7NG,8?Cx9t96.?v9'6-68

/flfir?

W8.?/<906/ 7S.fi

Checked By Date

Version 6- M-M

Page 46: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

-"reject Name^ ^»_^/ / —r-r-t AACE G&WlCEff LTRA project Numbe^2)447jgf) o/ 4.7

"ield Investigator(s) is— . / *.,<**,, •>KFN LANGUM

WELL DATATotal Well DeInitial Water IWater Colum

3 Well Volum

METHOD OF

I/

pth rfiRfl 'evel 1] 'Qt\j*J

n Heiaht /TS.Or

d O 1 Oes /T*;c") / . 1*1 aa

WELL DEVELOPMENTDumping

METHOD OF SAMPLE C

Method of Water Remova

Method of Sample Collec

Physical Appearance

Remarks

TIME

16COICoOfi1C*117fo7?7687foSS

Is

Air Lift

OLLECTION/PURGING

. ftuRMEPSn

Page / of / .

Well Number

MW-4--D

Well Diameter ^p-(x) (height) x=. 163 gal/ft

Well Volume (gals) 7*^09S 2",(5<=.653 gal/ft @ 4"

Amount of Water Removed from Well rt^ <vO aals

Surging Bailing

3/JF. P/JA/PtonfiuRMEf&anLE PUMP

Other

Was Well Pumped Dry? Yes (NO)

TEMP (°C)SPECIFICCONDUC-

TIVITYPH TURBIDITY DO ORP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

l&Sfi~l A* *2^^

7 C^ OO

1 &\ OO

rh^/

4*394£A-4£&

4/84.

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^vSfl

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Checked By

Version 6-14-W

Date

1

1

1

1

1

1

1

1

1

1

|•

1

1

1

Page 47: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Page 7 of

Well Number

AfW-^-fljt- • LTRA

Date10-11-05

KPN LANGUMA/ELL DATAotal Well Depth .

nitial Water LevelWater Column Height

Well Volumes

Well Diameter(x) (height) x=.163 gal/ft @ 2".CK653 gal/ft @f 4''

Well Volume (gals) <jL. 7\5

.gals Amount of Water Removed from Well ^R J .gals

METHOD OF WELL DEVELOPMENTy^* Pumping Air Lift Surging Bailing Other

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal PUBMERf fBLJ . lUtfP Was Well Pumped Dry? Yes

Method of Sample Collection ^UBME,RsS/flLE. lUMP

hysical Appearance

Remarks

TIME TEMP (°C)SPECIFICCONDUC-

TIVITYpH TURBIDITY DO ORP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

mmZ3£

11 U2S 19Z&£d<:%MPL P.

Checked By Date

Page 48: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Page / of

Well Number

MW-fi-IL.TRA "•""" n447isn.ni. 47

A/ELL DATAbtal Well Depthnitial Water Level

Water Column Height.

3 Well Volumes

Well Diameter(x) (height) x=. 163 gal/ft i

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Amount of Water Removed from Well /CflO .gals

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Version 6-14-04

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Black & Veatch Special Projects Corp.

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Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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IIIIIIIIIIIIIIIIIII

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MONITORING WELLDEVELOPMENT/PURGING DATA

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Black & Veatch Special Projects Corp.

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Page 53: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

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Page 54: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Page 55: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Page 56: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Page / of

Well Number

MW-fi-SL.TRA

WELL DATA r ,Total Well Depth /(.Initial Water LevelWater Column Height

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IBlack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Page 59: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

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Page 60: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Black & Veatch Special Projects Corp.

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Page 63: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

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Version 6-14-04

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Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Page 65: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Version 6-14-tM

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Black & Veatch Special Projects Corp.

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Version 6- 14 -O4

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Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Black & Veatch Special Projects Corp.

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Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Version 6-14-O4

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lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Page 7 of / .

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Black & Veatch Special Projects Corp.

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Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Black & Veatch

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Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Page 85: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

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Black & Veatch Special Projects Corp.

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Page 87: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

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Page 88: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

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Black & Veatch Special Projects Corp.

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Black & Veatch Special Projects Corp.

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Page 92: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Page 95: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

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Page 96: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IBlack & Veatch Special Projects Corp.

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Page 97: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

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Page 98: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IBlack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Page 100: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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Page 101: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

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Page 102: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

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11i

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MONITORING WELLDEVELOPMENT/PURGING DATA

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Version 6- H-O4

Page 104: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Page. of

Well Number

- IT'reject Name

A££ '

Project Number Date

Field Investigator(s)2A/ELL DATA ' ~ ;

otal Well Depth J^f Dnitial Water Level I XP.^-A/ater Column Height Qy

3 Well Volumes

Well Diameter(x) (height) x=.163 gal/ft @ 2", x=.653 gal/ft @ 4"

Well Volume (gals)

gals Amount of Water Removed from Well .gals

METHOD OF WELL DEVELOPMENTPumping Air Lift Surging Bailing Other

ETHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal lk£/k(,£W^ f Was Well Pumped Dry? Yes /No

Method of Sample Collection

Physical Appearance

Remarks

TIME TEMP (°C)SPECIFICCONDUC-

TIVITYPH TURBIDITY DO ORP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

3'. 15 Start Pumping

13 ; 3 15.17 7 /kl

0 :

V

Checked By Date

Version 6-14-O4

Page 105: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

111•

1111111111111111

lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Project Name « Project Number0 Y4 7J-0

Field Investigator(s)

"2.. 4, feyWELL DATA " 1 -\ ~> r- 1

otal Well Deoth (7- ) J

Page

Well

Date

10

-^-of-j^

Number

Y-l£>-ot-or

Well Diameternitial Water Level / 1 *) , <T<9 '

Water Column Height O T - 9 ;

Well Volumes qa

METHOD OF WELL DEVELOPMENT")s Pumping

METHOD OF SAMPLE C

Method of Water Remova

Method of Sample Collec

Physical Appearance

Remarks

TIME

M'.OJ

iLf.ftf

wuf « 4 ' ) 7JL|'. jQ

s

Air Lift

OLLECTION/PURG1NG

. ^ vf/L/ j. J-1 77^ ' 1 lrLT //'£,

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gal/ft @ 2'

Amount of Water Removed from Well *~v"' ^

Surging Bailing

ItLtKfk P^P

ion fic.luj?^ futr^p

, x=.653 gal/ft @ 4"

-^ qals

Other

Was Well Pumped Dry? Yes l^P

TEMP (°C)SPECIFICCONDUC-

TIVITYPH TURBIDITY DO ORP

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Page 106: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

3rojeat Name /

/V (L ) C/^tv*

Project Number

rield Investigator(s)7.. r+UM

WELL DATATotal Well DeInitial Water IWater Colum

3 Well Volum

METHOD OF

:pth f-D T_evel / f 0 . }-[) '

n Heiaht £ H • £ '

es qals

WELL DEVELOPMENTPumping Air Lift

;

Page

Well

6

i of_L

Number

Date

10 -fi^-or

Well Diameter(x) (height) x=. 163 gal/ft @ 2

Well Volume (gals)', x=.653 gal/ft @ 4"

Amount of Water Removed from Well tr~U

Surging Bailing

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal /7<W£>tf<A Pc/T^ P

Method of Sample Collec

Physical Appearance

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iv^rl$(<0)1 '• 0 5"

\9.011?. ID

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qals

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/f-flf

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Page 107: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

ProjectName /'

/V C £- /C/~(^~t~Cf f

Project Number

Oti£f7^oField Investigator(s) /••

~2- < (-^rftyWELL DATATotal Well DeInitial Water 1Water Colum

3 Well Volurr

METHOD OF

y

(

jpth ^7^.evel i^.10'n Heiaht *}fl . V

es qa

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Is

Air Lift

Page._Aof_^

Well Number

Date

Well Diameter(x) (height) x=.163

Well Volume (gals)gal/ft @ 2",

Amount of Water Removed from Well <r~£

Surging Bailing

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal My- itfrttfr PufaP

Method of Sample Collec

Physical Appearance

Remarks

TIME

ILL 1 7 (1

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/ f , 5^\^<1>~1>1 'iX

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Page 108: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Project Name /

A#l tCf(/'iLi'~>

Project Number

Field Investigators),*Z- ( L&(,eu

WELL DATA 7 ,Total Well Deoth j~7 SInitial Water LWater Colum

3 Well Volum

.evel /4H , 08 'n Heiaht ""KO. ^X'

es qal

METHOD OF WELL DEVELOPMENT^ Pumping

METHOD OF SAMPLE C

Method of Water Remova

Method of Sample Collect

Dhysical Appearance

Remarks

TIME

/ /**— 1 \i 1/ C., f *«J-

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OLLECTION/PURGING

1 /A^.fi^C-0-^L /6/Kh /

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Page 109: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

111•

1111111111111111

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Droject Name /Progc^mbe^

Page

Well

£;

of _LNumber

Date

Field Investigator(s) _~ ,

WELL DATA "} )C>Total Well Depth <f 1 'nitial Water Level <; f , 7/9 '

Water Column Heiaht £ f) • V

3 Well Volumes qa

METHOD OF WELL DEVELOPMENTX Pumping

s

Air Lift

METHOD OF SAMPLE COLLECTION/PURGING

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TIME

/5(lT£

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Am

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PUY^ f>

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= fi53 gal/tt @ 4"

tjtttf. qals

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Page 110: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONI7ORING WELLDEVELOPMENT/PURGING DATA

Project Name ..

Page -L«-L

Well Number

Project NumberTo-df-o?

Field Investigators)"Z_ . ^tC^-y

WELL DATA 'Total Well Depth nl 0 b Well DiameterInitial Water Level / 5 0. ^Q>Water Column Heiaht // f- 7 '

3 Well Volumes qa

METHOD OF WELL DEVELOPMENTV Pumping

S

Air Lift

Well Vc(x) (height) x=. 163 gal/ft @ 2"

)lume (gals)

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METHOD OF SAMPLE COLLECTION/PURGING

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\ti.U

\[\}*\

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Version 6-14 -O4

Page 111: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

111•I

111111111111111

lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

3roject Name x-/\C6, j&vlCf{

:ield lnve_stigator(s)

WELL DATAotal Well Denitial Water I

Water Colum

Well Volum

METHOD OFiL

pth.eveln Heigh

es

Project Number

e</ /&.F,/K»fi

\ 5~^. ID 't ISA1

qa

WELL DEVELOPMENTDumping

s

Air Lift

Page_/_of / •

Well Number

Date

Well Diameter(x) (height) x=.163 gal/ft @ 2

Well Volume (gals)

Amount of Water Removed from Well

Surging Bailing

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal //fy/A ^^dA \U\\V

Method of Sample Collec

Physical Appearance

Remarks

TIME

ic.?rI / - . S 6[ 1 9 7ll\00

Ull

ion Mttifoek rUr\01 i

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Version 5- 14-Ot

Page 112: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Page. of

Well Number

II

roject Narne Project Number Date

Field Investigator(s)"

NELL DATAbtal Well Depthnitial Water LevelA/ater Column Height_

5 Well Volumes

i -, V<*- ' - Well Diameter

.001(x) (height) x=.163 gal/ft @ 2", x=.653 gal/ft @ 4"

Well Volume (gals)

gals Amount of Water Removed from Well .gals

vIETHOD OF WELL DEVELOPMENTY^ Pumping Air Lift Surging Bailing Other

ETHOD OF SAMPLE COLLECTION/PURGING

ethod of Water Removal /LfjLi> LA* ™~ Was Well Pumped Dry? Yes ^Ng)

Method of Sample Collection

hysical Appearance

Remarks

TIME TEMP (°C)SPECIFICCONDUC-

TIVITYpH TURBIDITY DO ORP

WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

(',36 Start Pumping

(PI

\7

Checked By Date

Version 6- 14 -04

Page 113: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

111•

1111111111111111

lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Project Name Prgiect Number

Dage jLo'_LWell Number

Date

:ield Irivestigator(s)

WELL DATA , 'otat Well Deoth IIS

nitial Water IWater Colum

Well Volum

.evel /Sy$J 'n Heiaht 'd- 1 , I 5 '

es qa

METHOD OF WELL DEVELOPMENTX Pumping

s

Air Lift

Well Diameter(x) (height) x=. 163 gal/ft @ 2"

Well Volume (gals)

Amount of Water Removed from Well '^ ^

Surging Bailing

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal /A (A ' fa ttfi fi(Jf^ fl

Method of Sample Collect

Physical Appearance

Remarks

TIME

)7'-W— ' 9 1 ii 1

/7! /0T I 1 ff*~ U

17'.

ion (A.t&! LttJ&Oi, /x/irv/1

x=.653 gal/ft @ 4"

0 ft<&( qals

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{ KloIf, 75'^7)/frifr^pk

fio?Qoo71$

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!&&'

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'"-kw

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Date

/•^/^\

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Version 6-14-04

Page 114: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Black & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

ProjecLName -At£ W l/i6?f

Project Number

Field Investigator(s)*Z - U(^

WELL DATATotal Well DeInitial Water IWater Colum

3 Well Volum

METHOD OFK

fpth 3~~1 & '.evel JS6.10'n Heiaht X - 1 0y

es qa

WELL DEVELOPMENTDumping

s

Air Lift

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal fAc/A / /Vv^A

Method of Sample Collec

^hysical Appearance

Remarks

TIME

17-3717:47/7'.f#p:<;017 '.a

Page

Well

f,Date

/

_Lofj_Number

/

Well Diameter(x) (height) x=.163 gal/tt @ 2'

Well Volume (gals)

Amount of Water Removed from Well '"""""'

Surging Bailing

,ion /Atpl C&fak fli/VKfl

, x=.653 gal/n @ 4"

ff~0z»^( qals

Other

Was Well Pumped Dry? Yes /w>)

TEMP (°C)SPECIFICCONDUC-

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WATERLEVEL

TOTALWATER

REMOVED

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f£T£

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Page 115: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

111•

1111111111111111

lack & Veatch Special Projects Corp.

MONITORING WELLDEVELOPMENT/PURGING DATA

Project NamevAr€ ^>>&HrV^3

Project Number

:ield Investigator(s) 1 \ — ,Z-—Cr\}tl} / (j r \^€ |ci/s-v-

WELL DATAotal Well Denitial Water I

Water Colum

Well Volum

METHOD OF

xT

f t ^

pth P 2-^-1.evel \~^-~l'ti-T'n Heiqht 1 1 7,5V '

es qa

WELL DEVELOPMENTPumping

s

Air Lift

Page _o.J_

Well Number

i ^/-^"~ /Q

Date10 - ^-cp~~

Well Diameter <(x) (height) x=.163

Well Volume (gals)gal/ft @ 2", x=

Amount of Water Removed from Well £.<- -K

Surging Bailing

METHOD OF SAMPLE COLLECTION/PURGING

Method of Water Removal JU^ v' <>*i?4 tfu fi)

Method of Sample Collec

Physical Appearance

Remarks

TIME

\L^n\m, iTj/

10 '- fi}m /q

Ions

ion £\?*-L{ £**(-&{ Y(^^-~O

.653 gal/ft @ 4"

^^ qals

Other

Was Well Pumped Dry? Yes( NoJ

TEMP (°C)SPECIFICCONDUC-

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WATERLEVEL

TOTALWATER

REMOVED

FLOWRATE

Start Pumping

JS.^IS o^

I }-Oo

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Date

ter^{

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Page 116: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIIIM Appendix C

Field Sheets

IOctober 2005

"S

IIIIIIIIII

Page 117: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIIIIii

rfl.Sample Collection Field Sheet

US EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 1 QC Code: _ Matrix: Water Tag ID: 2775-1- _

Project ID: RS07GEProject Desc: Ace Service Inc. - LIRA GW samples

City: ColbyProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER

Project Manager: Robert Stewart

State: Kansas

Site ID: 07GE Site OU: 02

Location Desc:

Expected Cone:

Latitude:

Longitude:

External Sample Number: W~ MW~t

(or Circle One: Low Medium High) Date

Sample Collection: Start:

End:

Time(24 hr)

oa:<a&

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

I

I

I

I

I

I

I

TEMPSC

DOORP

" 6.4

= 4?0.

Sample Collected By: GF

1 of 1

Page 118: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 2 QC Code: Matrix: Water Tag ID: 2775-2-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: ColbyProgram: Superfund

State: Kansas

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

1 oration Desc: MVv~£,~ D

Expected Cone: (or

Latitude:

Longitude:

Laboratory Analyses:

External Sample Number: M/-AfiA/-£~7> 70040 )

Circle One: Low Medium High) Date Time(24 hr)

Sample Collection: Start: JQjQ&Q5 1L.3S

End: / / :

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP =SCPH •

DOORP =

Sample Collected By: GF

43? /LAS/cm6.36

?.G4mq/L463.3 mv

1 of 1

1

1

I•

1

•"

1

1

1

1

1

1

1

1

1

1

Page 119: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I•

11•

1

1•

1

1

1111111

1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

% ft>ASR Number: 2775 Sample Number: ,3 QC Code: Matrix: Water Tag

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

ID: 2775-^-_

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

1 oration Desc: [*1W'~ fZ~ LJ

External Sample Number: l/V"* r*/KV ~/S.

Expected Cone: (or Circle One: Low Medium High) Date

Latitude: Sample Collection: Start: JQjQ&QQ

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TGMP s /G.(5/8°CCV* — 4.QC2 cyAy

pH * 6.36

T" VS — *3 f* A //LAJ i.U>T*rnQ/L(^\Bp a 4LQO r\U/%r TOj.iSmv

Sample Collected By: GF

1 of 1

-D-/OO4n?m mm mm 1 k^V^

Time(24 hr)

f_L'-j3G.

Page 120: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 4 QC Code: Matrix: Water Tag ID: 2775-4-

Project ID: RS07GEProject Desc: Ace Service Inc. - LIRA GW samples

City: ColbyProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER

Project Manager: Robert Stewart

State: Kansas

Site ID: 07GE Site OU: 02

Location Desc:

Expected Cone:

Latitude:

Longitude:

External Sample Number: W~ MW~ 13~ D"

(or Circle One: Low Medium High) Date

Sample Collection: Start: JQjQ&/C&

End: / /

*Time(24 hr) •

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMPSCFH

DOORP

- £63uShm

m /L

Sample Collected By: GF

1 of 1

Page 121: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

IASR Number: 2775 Sample Number: 5 QC Code: Matrix: Water Tag ID: 2775-5-

Project ID: RS07GE Project Manager: Robert Stewart• Project Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: A/yV"

External Sample Number:

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 7Q/Q£Q5

• Longitude: End: / /

Laboratory Analyses:

I Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

| (N/A)

I TfiMP =

• 6C 3 4?<3uS/cm• — / / 2 A-» f^f^'- 3.7?

DO a 8.I ORP s 604.6 r&

I

I

IM Sample Collected By: GF

Il of 1

Page 122: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 6 QC Code: Matrix: Water Tag ID: 2775-6- •

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples •

City: Colby State: Kansas |Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 •

Location Desc:

External Sample Number: W~MW~ IS ** T~

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: IQjQ&QB H1&

Longitude: End: / / :

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

= 1S.83°C

PH =

Z33 - 8.£9m/LQRP • 44.9.

Sample Collected By: GF

1 of 1

Page 123: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

I

ASR Number: 2775 Sample Number: 7 QC Code: _ Matrix: Water Tag ID: 2775-7- _•

Project ID: RS07GE Project Manager: Robert Stewart

I Project Desc: Ace Sen/ice Inc. - LIRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: MW~1&~S _

I External Sample Number: W'MW" lfi~S~

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 7Q/Q&.Q5ILongitude: End:

Laboratory Analyses:

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitalner HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

» IS.89°C3 681 uS/cmpH - 6.86

DO = a3/mq/LI ORP = 49fi./crlv

I

I

I_ Sample Collected By: GF

I1 of 1

Page 124: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field Sheet •US EPA Region 7Kansas City, KS I

ASR Number: 2775 Sample Number: 8 QC Code: Matrix: Water Tag ID: 2775-8-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples •

City: Colby State: Kansas |Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: M\A/-1&~D _

External Sample Number: W~ MW~ \fi~D~ 1OC&O& •

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) •

I

Latitude: Sample Collection: Start: /QjOS'OS Q9.:fiD

Longitude: End: / / : •

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments: ~~~

(N/A) I

I

TenpWW i^j r >JVwr/vjii<

/

DO = ?.6Qmq/L •OKP = (34&<5mv |

I

I

ISample Collected By: GF •

1 of 1

I

Page 125: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I• Sample Collection Field Sheet

US EPA Region 7• Kansas City, KS

I ASR Number: 2775 Sample Number: 9 QC Code: Matrix: Water Tag ID: 2775-9-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

I

_ Location Desc: r/l/V" J4> " JL

• External Sample Number: W~MW~ f^I* IQO&Ctf

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: /OyQ5.Q5 Q2..59

n Longitude: End: / / :

Laboratory Analyses:

Container Preservative Holding Time Analysis

1 - 1 Liter Cubltainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

| (N/A)

" TEMP =

• SC * 6?<9 uS/cm1 -- = ?.aarI

JJU = uGG IDQ/JL/I ORP = 352.0

I

1

Ig Sample Collected By: GF

I1 of 1

Page 126: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 10 QC Code: _ Matrix: Water Tag ID: 2775-10- _

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: MW"1?"T

External Sample Number: W" MW~ /7~ T"

Expected Cone; (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: /Qj DS

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP =

DO -- <9.44m/LORP -

Sample Collected By: GF

1 of 1

Page 127: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I• Sample Collection Field Sheet

US EPA Region 7• Kansas City, KS

IASR Number: 2775 Sample Number: 11 QC Code: _ Matrix: Water Tag ID: 2775-11- _

Project ID: RS07GE Project Manager: Robert Stewart

I Project Desc: Ace Service Inc. - LIRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

_ Location Desc: MI/V~ 1?"3

• External Sample Number: M/"* M(A/~ 1?~\S~

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 1QjQ5<35

Longitude: End: / /= =

Laboratory Analyses:

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

I (N/A)

I• TEMP =A3.00°C

= 896 uS/c~ C? no-/

I DOORP ;

I

I_ Sample Collected By: GF

I

I1 of 1

Page 128: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ISample Collection Field Sheet

US EPA Region 7 _Kansas City, KS •

ASR Number: 2775 Sample Number: 12 QC Code: Matrix: Water Tag ID: 2775-12- I

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples •

City: Colby State: Kansas •Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 I

• nation DeSC: MIA/-17-D

External Sample Number:

Expected Cone: (or Circle One: Low Medium High)

Latitude: Sample Collection: Start

Longitude: End

Laboratory Analyses:Container Preservative Holding Time Analysis

•W-MW- rr-n-imm^

Date Time(24 hr) I

: 1GL&5QQ li:5&

: _J_I : I

11 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP •

Sample Comments:

(N/A)

TZMP * 7v5.S6°C6C * 46 / uS/cm_» / / •• ^2 £* f *'DO = 8.34-mq/LORP " (389. £rw

Sample Collected By: GF

1 of 1

1B

1

1

1

1

1

1

1

Page 129: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I• Sample Collection Field Sheet

US EPA Region 7• Kansas City, KS

• ASR Number: 2775 Sample Number: 13 QC Code: Matrix: Water Tag ID: 2775-13-

Project ID: RS07GE Project Manager: Robert Stewart

I Project Desc: Ace Service Inc. - LIRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

_ Location Desc: MIA/" /fi~O

• External Sample Number: M/~MW~ /fi~S~

Latitude: Sample Collection: Start:

I

ISample Comments:

| (N/A)

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End: /

• Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals In Water by ICP

SC = 890uS/cmI pH » G.5?

• DO a d.OSmq/L| OKP = 465.<S

I

I

I_ Sample Collected By: GF

I1 of 1

Page 130: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field Sheet •US EPA Region 7Kansas City, KS •

IASR Number: 2775 Sample Number: 14 QC Code: Matrix: Water Tag ID: 2775-14-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples •

City: Colby State: Kansas IProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: MlAf~lfi~D -

1

1

External Sample Number: \AJ~ MIA/" /<9-D" /QQ5Qff

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) •

Latitude: Sample Collection: Start: 1CL/CQQ& :

Longitude: End: / / : •

ILaboratory Analyses:

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A) I

TEHP = 16.SA-°C 'GC ~ 4?8jjS/cm •pH = ?.47^ |

TV*\ = O OD ^^>/lUU o.rvjiornQ/AjORP = 434.8 mv I

I

I

ISample Collected By: -SP **Jd M

I1 of 1

Page 131: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

1™ Sample Collection Field Sheet

US EPA Region 7I Kansas City, KS

8 ASR Number: 2775 Sample Number: 15 QC Code: _ Matrix: Water Tag ID: 2775-15- _

Project ID: RS07GE Project Manager: Robert Stewart

IProject Desc: Ace Service Inc. - LTRA GW samples

-•

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc:

External Sample Number: W~ MW~ 1fi"I"

Longitude: End:

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 1QjQ&QS

ILaboratory Analyses:

I Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals In Water by ICP

Sample Comments:

(N/A)

I

t TEMP -1&11°C1 SC = 62Ou£/cm

I 1X3 = 8.4O mq/LORP =^3S./m^

I

I• Sample Collected By: -6P

1

I1 of 1

Page 132: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 16 QC Code: _ Matrix: Water Tag ID: 2775-16- _

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: Afyv~yC"O

X External Sample Number: W~ MW~ /5 ~ S~

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End:

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMPSCpH = 6,33

DOORP * 353.6 nfv

Sample Collected By: -Sf1

\j1 of 1

Page 133: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

™ Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

B ASR Number: 2775 Sample Number: 17 QC Code: Matrix: Water Tag ID: 2775-17-

Project ID: RS07GE Project Manager: Robert Stewart

I Project Desc: Ace Service Inc. - LIRA GW samplesCity: Colby State: Kansas

Program: Superfundft Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

_ Location Desc: MW~3~D

I ^ External Sample Number: tV~/W~<9 ~ D~ 10O&05

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: IQjQ&OS1• Longitude: End: /

Laboratory Analyses:

IContainer Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals In Water by ICP

I

Sample Comments:

(N/A)I

TEMPI 6C

. DO1 QRP =(35?.6m^iii

Sample Collected By: -6f

\j1 of 1

Page 134: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 18 QC Code: Matrix: Water Tag ID: 2775-18-

Project ID: RS07GEProject Desc: Ace Service Inc. - LIRA GW samples

City: ColbyProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER

Project Manager: Robert Stewart

State: Kansas

III

Site ID: 07GE Site OU: 02 IExternal Sample Number: W- MW~ fG " J" 1CC&C& 9

Location Desc:

Expected Cone:

Latitude:

~ /(o~*Z

(or Circle One: Low Medium High) Date Time(24 hr)

Sample Collection: Start: 1QjC5tfQ5 /i.:!

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TZMP = 11.81 °Cc*/~f *• s\ /* /••* f* toC - "rGo u6/crr)

'DO = 8.09 ma/LC\PP a Od.C^ D J^-»v Or* i . jo m v

Sample Collected By: €f- r^p

<\j

1 of 1

1

1

1

1

1

1

1

1

1

1

Page 135: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I•

1I ASR Number: 2775 Sample

Project ID: RS07GE

1 Project Desc: Ace Service Inc.City: Colby

Program: Superfund

I Site Name: ACE SERVICES -

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

Number: 19 QC Code: _ Matrix: Water Tag ID: 2775-19-_

Project Manager: Robert Stewart- LTRA GW samples

State: Kansas

- GROUNDWATER Site ID: 07GE Site OU: 02

M ^ **/' A-xf 1 A / f ^ f_*

Location Desc: r]Yv~ /lO~O

A External Sample Number: l/V~MW~ 1(L~S~ /ODGf

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude:

Longitude:

Laboratory Analyses:

Sample Collection: Start: /QjQS'QS J&L.1&

End: / /__ _:

Container Preservative Holding Time Analysis1 - 1 Liter Cubitainer HNO3 acidify

Sample Comments:

1 (N/A)

1

• TEMP1 SCI nUpH

1 DO. ORP1

1

i•

Sample Collected By: €f^<*r(/

%

1

, 4 Deg C 180 Days 1 Metals in Water by ICP

= JQ S9°C= ??8 uS/cm~ "? Q /

= ?.99mq/L= GSS.&rii

•%j

. ;s^1 Of 1

Page 136: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 20 QC Code: _ Matrix: Water Tag ID: 2775-20- _

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: MW-1G>~D

^s External Sample Number: W~MlA/~ 1G~D~

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End:

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMPSC

DO =<S./4mq/LORP s <3£3,2 r*v

Sample Collected By:

1 of 1

Page 137: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIiiiiii

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 21 QC Code: _ Matrix: Water Tag ID: 2775-21 -_£D

Project ID: RS07GEProject Desc: Ace Service Inc. - LIRA GW samples

City: ColbyProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER

Project Manager: Robert Stewart

State: Kansas

Site ID: 07GE Site OU: 02

Location Desc: Ml/V~ 1G"D

Expected Cone:

Latitude:

Longitude:

External Sample Number: l/V"M\N~ 1G>".

(or Circle One: Low Medium High) Date

Sample Collection: Start: /Q/0&Q5

Time(24 hr)

End:

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

ITCMPSC

I

iii

DOORP

= 8.74 mq/L

Sample Collected By:

I1 of 1

Page 138: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 22 QC Code: Matrix: Water Tag ID: 2775-22-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: M M/" ?~ D

External Sample Number: W~ MW~ T3- D"

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End: /_

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

- 15. 1G°C

DO a ?.80ma/LORP =

Sample Collected By:

\j1 of 1

Page 139: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I Sample Collection Field Sheet_ US EPA Region 7• Kansas City, KS

|

«>jj PV-V?ASR Number: 2775 Sample Number: 27* QC Code: Matrix: Water Tag ID: 2775-^f-

Project ID: RS07GE Project Manager: Robert Stewart

•Project Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

I Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: nn-a-nExternal Sample Number: lA/~ OS "/T, "LJ~

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: ]QjC[8Q£) Q3.:QQ

• Longitude: End: / / :

Laboratory Analyses:• Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)I

i

n SCI pH

I DO /O.Q9mq/L• ORP ~ 3'W.Gmv

I

II Sample Collected By:

I1 of 1

Page 140: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field Sheet ™US EPA Region 7Kansas City, KS I

ASR Number: 2775 Sample Number: 24 QC Code: Matrix: Water Tag ID: 2775-24-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples •

City: Colby State: Kansas •Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 •

Location Desc: A/i/V"* r "- I M

^ External Sample Number: W~ MW~ ?" I" ?QQfing '

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) •

Latitude: Sample Collection: Start: lQjC&Q5 1&L:4G>

Longitude: End: / / : •

ILaboratory Analyses:

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A) I

•TEMP = H.4&CSC = GGxSuS/cm Ir-jll - P OQ 'l^ti » • *-J m

DO ~ ?.S1 rm/L |C\DD - Q^v4 O d. "w/>/ VJA^TT*. (\j triV

I

I

It is*Sample Collected By: f^T^ -m

I1 of 1

Page 141: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I•

1I ASR Number: 2775 Sample

Project ID: RS07GE

Project Desc: Ace Service IncCity: Colby

Program: Superfund• Site Name: ACE SERVICES

1Location Desc: MW~ ?~\

^

Sample Collection Field SheetUS EPA Region 7Kansas City, KS(

Number: 25 QC Code: _ Matrix: Water Tag ID: 2775-25-

Project Manager: Robert Stewart. - LIRA GW samples

State: Kansas

- GROUNDWATER Site ID: 07GE Site OU: 02

External Sample Number: l/V~M(A/~ P- S~ 700(50^

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude:

•Longitude:

Laboratory Analyses:

Sample Collection: Start: 1Q&ffQ5 /fi.:Q9End: / / :

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

| (N/A)

1_ TEMP1 SC

• DO1 ORP1

1

1m Sample Collected By: Gt-^f

1 3

1

= i A 1 O 0/^V/ T*. /O L/

: ^3^5/cm

= ?"9/rm/L

•%njo

1 of 1

Page 142: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 26 QC Code: _ Matrix: Water Tag ID: 2775-26- _

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: "^^ " .L

External Sample Number: tV~UQ"/8"" T~

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 10/Oft05

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP a /4..6S°CSC =

DO = ?.89mq/L

ORP

Sample Collected By: -6F- 7\0

1 of 1

Page 143: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

1m Sample Collection Field Sheet

1• ASR Number: 2775 Sample Number

Project ID: RS07GE

US EPA Region 7Kansas City, KS

: 27 QC Code: Matrix: Water Tag ID: 2775-27-

Project Manager: Robert Stewart

1 Project Desc: Ace Service Inc. - LIRA GW samplesCity: Colby

Program: SuperfundState: Kansas

• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

/o£3« i _ r")

II nratinn Desc: \ /// / /./

1 Expected Cone: (or Circle One

Latitude:

•Longitude:

Laboratory Analyses:

1 Container Preservative

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C

Sample Comments:

| (N/A)

TBMP = i1 SG

C7/J - /

IPrl (

, DO =11 ORP =61

1

1

Sample Collected By: -Sf- SK0_j

1

External Samole Number: W~QB~ /" D~ 1QO 'cOfa

: Low Medium High) Date Time(24 hr)

Sample Collection: Start: A3_/Q2?Q5 /7 : 7iJ

End: / / :

Holding Time Analysis

180 Days 1 Metals in Water by ICP

1 Cf Q^P^C*

4-1?u6/Cm9 C?Q • **J\J

"3 *^r\ //< co rnq/L66.c3 my

1 of 1

Page 144: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 28 QC Code: Matrix: Water Tag ID: 2775-28- •

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples •

City: Colby State: Kansas |Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 •

Location Desc: LJIJ" I "" -I _

External Sample Number: W~ OB' 1" J" ICCffCfi •

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) •

Latitude: Sample Collection: Start: JO/CMOS

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP - 16.33°CSC 3

DO =

OFF " 4£0.<3 mv

Sample Collected By: -GF-

1 of 1

Page 145: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field Sheet

1

I ASR Number: 2775 Sample Number— _ —

Project ID: RS07GE

US EPA Region 7Kansas City, KS

: 29 QC Code: Matrix: Water Tag ID: 2775-29-

Project Manager: Robert Stewart

1 Project Desc: Ace Service Inc. - LTRA GW samplesCity: Colby

Program: SuperfundState: Kansas

I Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

M\Al- 1 ~ TLocation Desc: / //v / J,

Expected Cone: (or Circle One

Latitude:

1Longitude:

Laboratory Analyses:^ Container Preservative• 1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C

Sample Comments:

I (N/A)

1

• TEMP1 SC| pH -

TURBIDITY =1 DO. ORP1

1

1Sample Collected By: -SP-^/Lj

• XJ

1

External Samole Number: IA/~ MIA/- T- I" lOICCft

' Low Medium High) Date Time(24 hr)

Sample Collection: Start: /£L(1Q/Q5 /4- ;i8ff

End: _J_J :

Holding Time Analysis180 Days ' 1 Metals in Water by ICP

/.i3Q9mS7cm6.6 /- /.<5 A/71/0. 1£ ma/LiCXJ.Cp rnv

1 of 1

Page 146: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 30 QC Code: _ Matrix: Water Tag ID: 2775-30- _

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: /^/I/V" / ~ D

External Sample Number: W~ MlA/~ 1"D"

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: /Qy/QQ5 A5.:Q5

Longitude: End: / / :

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days " 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP = 15.88°CSC =

TURBIDITY = -8,9 NTUDO = ?.<8cSm/LOFF =

Sample Collected By:

\J1 of 1

Page 147: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

1•

1Sample Collection Field Sheet

US EPA Region 7Kansas City, KS

1 ASR Number: 2775 Sample Number: 31 QC Code: Matrix: Water Tag

Project ID: RS07GE

Project Desc: Ace Service Inc. •City: Colby

Program: Superfund• Site Name: ACE SERVICES -

_ Location Desc: MIA/" 1 ~ S

1

Project Manager: Robert Stewart- LTRA GW samples

State: Kansas

GROUNDWATER Site ID: 07GE

ID: 2775-31-_

Site OU: 02

External Sample Number: W" MM/" 1~&~ 1Q1CC&

1 Expected Cone: (or Circle One: Low Medium High) Date

Latitude:

1 Longitude:

Laboratory Analyses:

1Container Preservative

1 - 1 Liter Cubitainer HNO3 acidify,

Sample Comments:

| (N/A)

1TfzMP ~

1 sc• PH• TURBIDITY =• DO1 ORP1

1

1_ Sample Collected By: -6f=- WfT

1 \

1

Sample Collection: Start: fQj1Q/QQ

End: / /

Holding Time Analysis

4 Deg C 180 Days 1 Metals in Water by ICP

f A-* x- >f cy-*7o. 64 C1.306 mS/cmG.GS

-£.4 Am/0.38 mq/L,754.6 mv

./1 of 1

Time(24 hr)

/jG.:<3Sm

Page 148: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 32 QC Code: Matrix: Water Tag ID: 2775-32-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: MW"3"I

External Sample Number : IN"

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: ___ Sample Collection: Start: /Q/H/05Longitude: ___ End: _ / _ / _

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP = 7*.8/°C- <599mS/cm

TuPBtDITY * -}.? NTU

DO =ORP =

Sample Collected By:

1 of 1

Page 149: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

1• •

11•

1

1•

1w

11111•

111

1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 33 QC Code: Matrix: Water Tag

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE

Location Desc: f*fW~&~ D

External Sample Number: /V"~/v/l/Y~vT

Expected Cone: (or Circle One: Low Medium High) Date

Latitude: Sample Collection: Start: 70 l11lQF)

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP - 1<5.1G°CSC s 313mS/cm

TURBIDITY * -/.8 NTUTY^S •«- ^ /* O //JJJ - c.(s& ma/L

S^CJD ~ 7QQ O v(Jf\r /C5O .O HIV

Sample Collected By: -Of- U/"

\ lof l

ID: 2775-33-_

Site OU: 02

-D-1Q11C&Time(24 hr)

7Q.£?

Page 150: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 34 QC Code: Matrix: Water Tag ID: 2775-34-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

_ i q _CVLocation Desc:

External Sample Number:

Expected Cone: (or Circle One: Low Medium High) Dftf Time(24 hr)•

Latitude: ___ Sample Collection: Start: JQjJ&QS

Longitude: ___ End:

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP - £1. 13°CSC - aOSmS/cm

TURBIDITY = 100.6 NTUCO = ?.7Smq/LORP =

Sample Collected By:-Gf-

1 of 1

Page 151: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

IASR Number: 2775 Sample Number: 35 QC Code: _ Matrix: Water Tag ID: 2775-35- _

Project ID: RS07GE Project Manager: Robert Stewart

Project Desc: Ace Service Inc. - LIRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc:_ _

• External Sample Number: W~ NM/- v5 ~ I~ /O7/Q?

Latitude: ___ Sample Collection: Start: JQjLL/05

II

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: ___ Sample Collection: Start:

Longitude: ___ End:

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP = A3.68°CI SC =. PH = 7.36• TURBIDITY = 0.8 NTUm DO = ?.30mq/L1 ORPI

I

Ig Sample Collected By: -Gf-

1 of 1

Page 152: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 36 QC Code: _ Matrix: Water Tag ID: 2775-36- _

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

: MIA/" C) " LJLocation Desc

External Sample Number:

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) •

Latitude: Sample Collection: Start: fQjtt/QS ** ***

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP

PH = ?.55TURBIDITY = -

6.36 mq/Ln?v

Sample Collected By:

°\^ l o f l

Page 153: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field Sheet

1US EPA Region 7Kansas City, KS

I ASR Number: 2775 Sample Number: 37 QC Code: Matrix: Water Tag ID: 2775-37-— — — —

Project ID: RS07GE Project Manager: Robert Stewart

1 Project Desc: Ace Service Inc. - LIRA GW samplesCity: Colby

Program: Superfund

State

• Site Name: ACE SERVICES - GROUNDWATER

_ Location Desc: MW~£"~S

1 External Sample Number:

• Expected Cone: (or Circle One: Low Medium High)

Latitude:

1 Longitude:

Laboratory Analyses:

1Container Preservative

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg

Sample Comments:

| (N/A)

|TEMP

1 SCPH

I TURBIDITY*. DO1 CKP1

1

1Sample Collected By: •&£- (J/*

I ^\. }

1

Sample Collection: Start:

End:

Holding Time Analysis

: Kansas

Site ID: 07GE Site OU: 02

W-MW-fi-f>-1011CfiDate Time(24 hr)

iQ/njos a-.Q3' * • * -^~-^^ § *~ ^^f^^

C 180 Days 1 Metals in Water by ICP

/w. / r* 0

/. 1S8 mS/cmj ^\ * *

131. 1 NTU?.45 mq/L

19?.8 nil

1 of 1

Page 154: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 38 QC Code: _ Matrix: Water Tag ID: 2775-38- _

Project ID: RS07GEProject Desc: Ace Service Inc. - LTRA GW samples

City: ColbyProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER

Project Manager: Robert Stewart

State: Kansas

Site ID: 07GE Site OU: 02

Location Desc: M]N~4-~I

Expected Cone:

Latitude:

Longitude:

External Sample Number: W"MW" 4

(or Circle One: Low Medium High) Date Time(24 hr)

Sample Collection: Start: IQjUjQS

End: _ / _ / _

Laboratory Analyses:Container Preservative Holding Time

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 DaysAnalysis

1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP -SC =pH »TURBIDITY*DO =CRP =

?83 mS/cm?. 74

-0.4- NTUG.?3m/L

Sample Collected By: -6F^ I of 1

Page 155: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

11I A.SR Number: 2775 Sample

_Project ID: RS07GE

Project Desc: Ace Service Inc.City: Colby

Program: Superfund

I Site Name: ACE SERVICES •

Location Desc: /*/( ( /V "~ nr

1

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

Number: 39 QC Code: Matrix: Water Tag ID: 2775-39-

Project Manager: Robert Stewart- LIRA GW samples

State: Kansas

• GROUNDWATER Site ID: 07GE

nExternal Sample Number: W~ MW~ A- ~

M Expected Cone: (or Circle One: Low Medium High) Date

• Latitude:

1Longitude:

Laboratory Analyses:

Sample Collection: Start: JQ/U/Q5

End: _/_/

Site OU: 02

D-iaiicfiTime(24 hr)

1Q_.SS.

_ Container Preservative Holding Time Analysis

I 1-1 Liter Cubitainer HN03 acidify

Sample Comments:

• (N/A)

1 TEMP• SC

pH1 TuPBIDITf *

DO1 OPP

1

1

1Sample Collected By: €4^ Uf'

1 3

1

, 4 Deg C 180 Days 1 Metals in Water by ICP

7.5.33 °C434-mS/cm?.S7-0.5 NTU?. 7i3 mg/L/G3. ?mv

•»>

L >

1 Of 1

Page 156: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 40 QC Code: _ Matrix: Water Tag ID: 2775-40- _

Project ID: RS07GEProject Desc: Ace Service Inc. - LTRA GW samples

City: ColbyProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER

Project Manager: Robert Stewart

State: Kansas

Site ID: 07GE Site OU: 02

Location Desc:

Expected Cone:

Latitude:

Longitude:

External Sample Number: 1/V" MW~

(or Circle One: Low Medium High) Date

Sample Collection: Start: JQjI&Q*}

End: __/ /

Time(24 hr)

09.-.S5

Laboratory Analyses:Container Preservative Holding Time

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days

Analysis

1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP

pHTURBIDITYDOORP

?.0£-0.3 NTU6.33 rna/L

Sample Collected By: -6f-

\J1 of 1

Page 157: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

I ASR Number: 2775 Sample Number: 41 QC Code: Matrix: Water Tag ID: 2775-41-

Project ID: RS07GE Project Manager: Robert Stewart

•Project Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

I Location Desc: MW~CQ-P

External Sample Number: W~MW-CtrD- /Q/PA

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 1Qjf£jC& 11 : A3

• Longitude: End: / / :

Laboratory Analyses:

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

_ Sample Comments:

| (N/A)

I T&IP = A5.S3°CSC = .4-ttmS/cmPH " ?.58

. TURBIDITY • 33.3 NTH1 DO = 6.3 / md/L

ORP = /GG.9mv

I

I

I

I

Sample Collected By:-Gf-

<f .1 of 1

Page 158: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 42 QC Code: _ Matrix: Water Tag ID: 2775-42- _ •

Project ID: RS07GE Project Manager: Robert Stewart 'Project Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: Kansas IProgram: Superfund ™

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: RfMSATE &AMPLE _ ___

External Sample Number: W~ RfM ~ 1O l&Ofi ~ R |

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: ___ Sample Collection: Start: IQjl&QS 1&: J(p

Longitude: ___ End: _ / _ / _ _ : _

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

(BLANK)

Sample Collected By:

1 of 1

Page 159: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

• ASR Number: 2775 Sample Number: 43 QC Code: Matrix: Water Tag ID: 2775-43-

Project ID: RS07GE Project Manager: Robert Stewart

Project Desc: Ace Service Inc. - LTRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

— Location Desc: M\N~G*~L ;

• External Sample Number: W"MW"C^"T." /O/P/15

Latitude: Sample Collection: Start: JQjl£/C&

I

I

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End: /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

| TEMPSC = -64-7 mS/cm

I pH a ?.1?m TURBIDITY = ~1-3 NTU• DO Ci.31 mq/L• OKP

I

I

I• Sample Collected By:

I1 of 1

Page 160: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field Sheet •US EPA Region 7Kansas City, KS •

ASR Number: 2775 Sample Number: 44 QC Code: _ Matrix: Water Tag ID: 2775-44- _ •

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples •

City: Colby State: Kansas |Program: Super-fund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 •

Location Desc: A/K/-fp-£ _ .

External Sample Number: W~ MW~ ffl " £r /O 7/PA5 *

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) •

Latitude: ___ Sample Collection: Start: 1Q/1&/Q5 /<2.:/35

Longitude: ___ End: — / — / _ _ : _ •

Laboratory Analyses:Container Preservative Holding Time Analysis •

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP |

Sample Comments:

(N/A) I

TEMP B

.pH - f.39 •TURBIDITY - o.<3 NTU •no = ?.56mq/L *ORP =

Sample Collected B

<\J

1 of 1

III•I

I

Page 161: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

1 Sample Collection Field SheetUS EPA Region 7Kansas City, KS

I ASR Number: 2775 Sample Number: 45 QC Code: Matrix: Water Tag ID: 2775-45-

Project ID: RS07GE

1Project Desc: Ace Service Inc.

City: ColbyProgram: Superfund

ISite Name: ACE SERVICES -

Location Desc: M\A/" 1 1" .

1

Project Manager: Robert Stewart- LIRA GW samples

State: Kansas

GROUNDWATER Site ID: 07GE Site OU: 02

rExternal Samole Number: ]A/"MIA/"11" I" 7O/PO

1 Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude:

1 Longitude:

Laboratory Analyses:

Sample Collection: Start: /Q/£2OJ3 /T»: Tc?

End: f_J :

_ Container Preservative Holding Time Analysis

• 1-1 Liter Cubitainer HN03 acidify,

Sample Comments:

I (N/A)

1 TEMPSC

1 pHm TURBIDITY s

• DO| ORP

1

1

1_ Sample Collected By: -6pW(2

4 Deg C 180 Days 1 Metals in Water by ICP

JG.CO°CGOS m£i/Cmr!$3-1.8 NTU6.?<9rrg/L181.0 mv

»»

1 \,

11 of 1

Page 162: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 46 QC Code: Matrix: Water Tag ID: 2775-46-_

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: MW-11~D

External Sample Number: \N~MW~ 1 /" D"

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 1Qj1£/Q5Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

= 1G.OO°CSC *"* T- fki nPH - ?.dOTURBIDITY = -1.9 NTUDO = ?.39mq/LOFF " 169.8ms

Sample Collected By:-OF

1 of 1

Page 163: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

ASR Number: 2775 Sample Number: 47 QC Code: Matrix: Water Tag ID: 2775-47-IProject ID: RS07GE Project Manager: Robert Stewart

Project Desc: Ace Service Inc. - LIRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

ksf t A / Y *f C?

Location Desc: iiV^J" I I "*O

External Sample Number: W" MW~ 11" S ~

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 1Qjl£/Q&

• Longitude: End: / /

Laboratory Analyses:

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

| (IM/A)

| TEMP = 15M°C• 5C

I PH. TURBIDITY = 139.3 NTU• DO| ORP

I

I

I• Sample Collected By: -6f=-

I1 of 1

Page 164: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 48 QC Code: Matrix: Water Tag

Project ID: RS07GEProject Desc: Ace Service Inc. -

City: ColbyProgram: Superfund

Project Manager: Robert StewartLTRA GW samples

State: Kansas

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE

Location Desc: MW~8~ I1 A / t^. ji 1 A 0 f^

External Sample Number: /V~ P/ /Y"C!

Expected Cone: (or Circle One: Low Medium High) Date

Latitude:

Longitude:

Laboratory Analyses:Container Preservative

1 - 1 Liter Cubitainer HN03 acidify, 4

Sample Comments:

(N/A)

TEMPscpHTURBIDITY *DOOFF

i //•»Sample Collected Byi^F-^-fto

Sample Collection: Start: /Q/ffiyQS)

End: / /

Holding Time Analysis

Deg C 180 Days 1 Metals in Water by ICP

/C0 .CJrw 0

633 mS/cmP. /SO

£0.3 NTH6.7? mq/L1GQ.9 mv

f

1 of 1

1•

1ID: 2775-48-__ •

Site OU: 02 •1

, ^ ,^,_,,

Time(24 hr) •

7fl:JS

1

1•

1

1

1

1

Page 165: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

IASR Number: 2775 Sample Number: >8* QC Code: Matrix: Water Tag ID: 2775-&3-FD

Project ID: RS07GE Project Manager: Robert Stewart

Project Desc: Ace Service Inc. - LIRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

_ Location Desc: MiA/~Q~ T

• External Sample Number: W~MW-&~I~

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: _, Sample Collection: Start:

Longitude: End:

Latitude: Sample Collection: Start: 1QjJ&Q5

ILaboratory Analyses:

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

I (N/A)

TEMP * 1G.02°CI SC " 633mS/cm

pH ~ ?!(90I TURBIDITY• = £0.3 NTU

I

• DO - 6.??mq/L1 OPP = 763.3 mvI

I

ISample Collected By:-6f-

<;1 Of 1

Page 166: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 49 QC Code: Matrix: Water Tag ID: 2775-49-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: MW"S"D

External Sample Number: W~M\A/~fi- D" /Q/£Qg|

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) —

Latitude: Sample Collection: Start: jQj!S/QS /_2.:4Q •

Longitude: End: / / : ^

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

" 15.90°CSC = 4?9mS/cmpH -TURBIDITY* -DO = ?.33mq/LORP = /?e./mv

Sample Collected By: GE-^K-

1 of 1

Page 167: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

• ASR Number: 2775 Sample Number: 55 QC Code: _ Matrix: Water Tag ID: 2775-55- _

Project ID: RS07GE Project Manager: Robert Stewart

Project Desc: Ace Service Inc. - LIRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

_ Location Desc: Oft" I "O _ :

• External Sample Number: \N~ OB " 1~&-

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: ___ Sample Collection: Start: /Q/&3/G6 11 :OS

• Longitude: ___ End: _ / _ / _ _ : _

Laboratory Analyses:

I Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by TCP

Sample Comments:

(N/A)

I T&iP "SC =4/1 mSfan

I pH = ?.d?TURBIDITY = 8.8 NTU

I DO = G.?1 mq/LORP =

III_ Sample Collected By:

I1 of 1

Page 168: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 56 QC Code: Matrix: Water Tag ID: 2775-56-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc:

External Sample Number: \nJ~~Qo" K~J"O "

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) I

Latitude: Sample Collection: Start: fQjQ/QB 11:4$

Longitude: End: / / : I

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

= £0.3/8SC =pH "TURBIDITY * ~L? NTUEC = ?.31mq/LORP * 1?L?mv

Sample Collected By:

'<?1 of 1

Page 169: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field Sheet

1US EPA Region 7Kansas City, KS

I ASR Number: 2775 Sample Number: 57 QC Code: Matrix: Water Tag—

Project ID: RS07GE Project Manager: Robert Stewart

ID: 2775-57-

1 Project Desc: Ace Service Inc. - LTRA GW samplesCity: Colby

Program: Super-fundState: Kansas

• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE

_ Location Desc: MW~fi~S

1m Expected Cone: (or Circle

Latitude:

Longitude:

~Laboratory Analyses:

Container Preservative

Site OU: 02

External Sample Number: W~ MW~fi ~S~ JO /fld?

One: Low Medium High) Date

Sample Collection: Start: IQj&GS

End: _J_J

Holding Time Analysis

Time(24 hr)

/ .'-C^.

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

| (N/A)

I TEMPSC

1 pHm TURB/D/TY *• DO| ORP

1

1

1— Sample Collected By: -6P 7\~

1 *L1

1G.8?°C669rnS/ClnPOO

-/ . / NTU6.36mq/L,309. 9 mv

1 of 1

Page 170: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 58 QC Code: Matrix: Water Tag ID: 2775-58- •

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples •

City: Colby State: Kansas |Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 fl

Location Desc:

External Sample Number: V\/~MW~/<8~S~

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 1Qj]QC£5

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

TEMP = 75.35 °CSC = 5,08 mSlcm

TURBIDITY* -O.?NTUDO « Z63 mq/L(~\l3p = on^ >t J

Sample Collected By:

^ 1 of 1

Page 171: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

• ASR Number: 2775 Sample Number: 59 QC Code: Matrix: Water Tag ID: 2775-59-

Project ID: RS07GE Project Manager: Robert Stewart

Project Desc: Ace Service Inc. - LTRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: R/N&ATZ SAMPLE

I External Sample Number: W" R/N" /Q/i9Q5~ R

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End:

Laboratory Analyses:

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

| (N/A)

R/NSAT&&AMPLE (BLANK)I

I

I

I

I

I^ Sample Collected By:

I1 of 1

Page 172: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 60 QC Code: Matrix: Water Tag ID: 2775-60- I

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples I

City: Colby State: Kansas ™Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 I

Location Desc: A/iA/" 7/8 "*X •

External Sample Number: W~ MW" 1&~I~ 1O ISCX?

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) I

Latitude: Sample Collection: Start: JQjl3/C£ /(P:G3

Longitude: End: / / : I

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments: " "

(N/A)

TEMPSC = 4 9 9 mS/CmPH = ?.38TURBIDITY - -£.ONTUDOORP

Sample Collected By:

1 of 1

Page 173: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

• ASR Number: 2775 Sample Number: 61 QC Code: Matrix: Water Tag ID: 2775-61-

Project ID: RS07GE Project Manager: Robert Stewart

IProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

. Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: MIA/"/<d"".

I Externa. Sample Number: W~MW~ IJS'D-

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 1Qjl3/Q5 /? :Q3ILongitude: End:

ILaboratory Analyses:

M Container preservative Holding Time Analysis

I 1-1 Liter Cubitalner HN03 acidify, 4 Deg C 180 Days 1 Metals In Water by 1CP

Sample Comments:

(N/A)

TEMP " 7G.Ofi°C| SC « 39G>mS/cm_ pH = ?.4&I TURBIDITY'' -1.S.NTU. DO = ?.31ma/L1 ORP -I

I

I^ Sample Collected By

I

Sample Collected By:

\ ,1 of 1

Page 174: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7 _Kansas City, KS •

ASR Number: 2775 Sample Number: 66 QC Code: Matrix: Water Tag ID: 2775-66- I

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples •

City: Colby State: Kansas ™Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 I

Location Desc:

External Sample Number:

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End: /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

'-\1,\1T-I

D 0, L *9 A) '

Sample Collected By: GF/ "

1 of 1

Page 175: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

I ASR Number: 2775 Sample Number: 67 QC Code: Matrix: Water Tag ID: 2775-67-

Project ID: RS07GE Project Manager: Robert Stewart

•Project Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

m Location Desc:

* External Sample Number: l/^/AU'-M ( -

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: /0/<2£/_&T JL'-il

I Longitude: End: / f :

Laboratory Analyses:

Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

| (N/A)

I

I

I

I

I

I

I• Sample Collected By: GF

I1 of 1

Page 176: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 68 QC Code: Matrix: Water Tag ID: 2775-68-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

_

Location Desc: _/

External Sample Number: \S~Afl- \s- $ - /p 6 O<T

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End: /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

(,,L L / ^ - 10 top

, f t . , V = (17. f

Sample Collected By: GF/" /

1 of 1

Page 177: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

• ASR Number: 2775 Sample Number: 69 QC Code: Matrix: Water Tag ID: 2775-69-

Project ID: RS07GE Project Manager: Robert Stewart

Project Desc: Ace Service Inc. - LTRA GW samplesCity: Colby State: Kansas

Program: Superfundm Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

I

ii

Location Desc:

External Sample Number:

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End:

Laboratory Analyses:

IContainer Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

iiiii

Sample Collected By: GF (^ ^ /

I1 of 1

Page 178: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 70 QC Code: Matrix: Water Tag ID: 2775-70-_

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: 1External Sample Number:

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End: /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

j > - ~ 7 / 7

. 0' U Iti ~- 1.1®

Sample Collected By: GF/f^U '-' /

1 of 1

Page 179: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

IASR Number: 2775 Sample Number: 71 QC Code: Matrix: Water Tag ID: 2775-71-

Project ID: RS07GE Project Manager: Robert Stewart

IProject Desc: Ace Service Inc. - LTRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc:

I External Sample Number:

Longitude: End:

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: \Oj06jOS

ILaboratory Analyses:

Container Preservative Holding Time Analysis1-1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

| (N/A)

I

I

I

I

I

I

I_ Sample Collected By: GF

11 of 1

Page 180: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 73 QC Code: Matrix: Water Tag ID: 2775-73-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 _

Location Desc: ]W 5 ~~ u

External Sample Number:

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: iQjQijJg' I0.\l5_

Longitude: End: / / :

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

* I $.00

0. =

otp'--

Sample Collected By: GF}W- '

1 of 1

Page 181: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

1111111111111

11111

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

73

ASR Number: 2775 Sample Numben-^r QC Code: JJJ Matrix: Water Tag ID: 2775-Jfp-F/)

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE

Location Desc: r-™-5 " / ^ > ~~ 0

External Sample NumbeK/r k^f ~ 0 ~~ (0

Expected Cone: (or Circle One: Low Medium High) Date

Latitude: Sample Collection: Start: /0/0^/or-

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

/ / /? / ^ *^ — / I * C )O\ L $r\ js Ls ' '

/

f) $ P — ^Lr~7 0 {/^

Sample Collected By: GF '^l.J, J

1 of 1

Site OU: 02

O<fn? £/)

Time(24 hr)

&:/£

Page 182: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 75 QC Code: Matrix: Water Tag ID: 2775-75-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: ' / •

-1 y/-X -loo y#r •External Sample Number:

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: {QjQ$JLS~

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

f

Sample Collected By: GF

1 of 1

Page 183: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I Sample Collection Field SheetUS EPA Region 7

« Kansas City, KS

I

_

ASR Number: 2775 Sample Number: 76 QC Code: Matrix: Water Tag ID: 2775-76-

Project ID: RS07GE Project Manager: Robert Stewart

— Project Desc: Ace Service Inc. - LIRA GW samples• City: Colby State: Kansas

Program: Superfund_ Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc:

I External Sample Number: It/"- ft1/ -<T 'JOQ^ 0 S~

— Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

B Latitude: Sample Collection: Start:

Longitude: End:

III

I

Laboratory Analyses:Container Preservative Holding Time Analysis

I 1-1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

I ~.o. ~-

Sample Collected By: GF

1 of 1

Page 184: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I Sample Collection Field SheetUS EPA Region 7

m Kansas City, KS

IIIIIIII

ASR Number: 2775 Sample Number: 77 QC Code: Matrix: Water Tag ID: 2775-77-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: T S

External Sample Number: \S~ E fr- £ -

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: ___ Sample Collection: Start: tQj_C$_£>S>

Longitude: ___ End: _ / _ / _

Laboratory Analyses:Container Preservative Holding Time Analysis

1-1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

9.17

III

I

Sample Collected By: GFt" c

1 of 1

Page 185: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 78 QC Code: Matrix: Water Tag ID: 2775-78-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples I

City: Colby State: Kansas BProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 I

Location Desc: E^ A " ±, L,

External Sample Number: w~ jby ~]_T "

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) I

Latitude: Sample Collection: Start: .JQ/_0/_0$" 0_: J>5^

Longitude: End: / / : I

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

H= 7.1 r

Sample Collected By: GF-W L- it

1 of 1

Page 186: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

•_

|

m

•_

ASR Number: 2775 Sample Number: 79 QC Code: _ Matrix: Water Tag ID: 2775-79- _

Project ID: RS07GEProject Desc: Ace Service Inc. - LIRA GW samples

City: ColbyProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER

Project Manager: Robert Stewart

State: Kansas

Site ID: 07GE Site OU: 02

Location Desc: FX~ 1 j)

Expected Cone:

Latitude:

Longitude:

External Sample Number: V/"~ £)(.-]_/) ~

(or Circle One: Low Medium High) Date Time(24 hr)

Sample Collection: Start:

End:

Laboratory Analyses:Container Preservative Holding Time

1-1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days

Analysis1 Metals in Water by ICP

Sample Comments:

(N/A)

I

I

I

I

Sample Collected By: GF

1 of 1

Page 187: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 80 QC Code: _ Matrix: Water Tag ID: 2775-80- _

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: ^ X"V- L ) _ _

External Sample Number: l//

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: ___ Sample Collection: Start: [

Longitude: ___ End: _ /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

/>// '1.11

Sample Collected By: GF

y* r1 of 1

Page 188: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

• ASR Number: 2775 Sample Number: 81 QC Code: Matrix: Water Tag ID: 2775-81-

Project ID: RS07GE Project Manager: Robert Stewart• Project Desc: Ace Service Inc. - LIRA GW samplesI City: Colby State: Kansas

Program: Superfund_ Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc:

_ Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

g

External Sample Number:

Latitude: ___ Sample Collection: Start:

Longitude: ___ End:

1

I

I

I

I

I

Laboratory Analyses:Container Preservative Holding Time Analysis

I 1-1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

• (N/A)

OSample Collected By: GF '

1 of 1

Page 189: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 82 QC Code: _ Matrix: Water Tag ID: 2775-82- _ •

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LTRA GW samples •

City: Colby State: Kansas |Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 •

Location Desc: £ A ~~£-j

External Sample Number: It/"- £/- ^-S ~

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: [fij'0$'O_T

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

Sample Collected By: GF^'(s r

1 of 1

Page 190: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIIIIII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 83 QC Code: _ Matrix: Water Tag ID: 2775-83- _

Project ID: RS07GE

Project Desc: Ace Service Inc. - LIRA GW samplesCity: Colby

Program: SuperfundSite Name: ACE SERVICES - GROUNDWATER

Project Manager: Robert Stewart

State: Kansas

Site ID: 07GE Site OU: 02

Location Desc:

Expected Cone:

Latitude:

Longitude:

External Sample Number:

(or Circle One: Low Medium High)

Sample Collection: Start:

End:

~ E X " 3 X

Date Time(24 hr)

Laboratory Analyses:Container Preservative Holding Time

1-1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days

Analysis1 Metals in Water by 1CP

Sample Comments:

(N/A)

I

I

IIIII

Sample Collected By: GF

1 of 1

Page 191: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 84 QC Code: Matrix: Water Tag ID: 2775-84-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples •

City: Colby State: Kansas |Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: A

External Sample Number : l/l/" E^"l> D~

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: ___ Sample Collection: Start: [

Longitude: ___ End: _ /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

^i ' LSample Collected By: GF V///7 \

1 of 1

Page 192: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIIIIIIIIIIIIIIII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 85 QC Code: _ Matrix: Water Tag ID: 2775-85- _

Project ID: RS07GEProject Desc: Ace Service Inc. - LIRA GW samples

City: ColbyProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER

Project Manager: Robert Stewart

State: Kansas

Site ID: 07GE Site OU: 02

Location Desc:

Expected Cone:

Latitude:

Longitude:

~ 7.L

External Sample Number:

(or Circle One: Low Medium High)

~ £X-*fZ~

Date Time(24 hr)

Sample Collection: Start: /0/O# '_&S

End: _ / _ /

Laboratory Analyses:Container Preservative Holding Time

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days

Analysis

1 Metals in Water by ICP

Sample Comments:

(N/A)

•.. /ji>pn~T.i

OH f.

Sample Collected By: GF ~\/

1 of 1

Page 193: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 86 QC Code: Matrix: Water Tag ID: 2775-86-

Project ID: RS07GEProject Desc: Ace Service Inc. - LTRA GW samples

City: ColbyProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER

Project Manager: Robert Stewart

State: Kansas

Site ID: 07GE Site OU: 02

Location Desc:

Expected Cone:

Latitude:

Longitude:

J J

External Sample Number:

(or Circle One: Low Medium High)

- jE~TS -

Date Time(24 hr)

Sample Collection: Start: \QJC£kjgS'

End: I I

Laboratory Analyses:Container Preservative Holding Time

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days

Analysis

1 Metals in Water by TCP

Sample Comments:

(N/A)

Sample Collected By: GF

1 of 1

Page 194: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I Sample Collection Field SheetUS EPA Region 7

_ Kansas City, KS

m ASR Number: 2775 Sample Number: 87 QC Code: Matrix: Water Tag ID: 2775-87-

Project ID: RS07GE Project Manager: Robert Stewart_ Project Desc: Ace Service Inc. - LIRA GW samplesI City: Colby State: Kansas

Program: SuperfundSite Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc:

External Sample Number: l -~ <CX~5~.Zr

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

I Latitude: Sample Collection: Start: lOjCtt/AS~

Longitude: End: / /

Laboratory Analyses:Container Preservative Holding Time Analysis

1-1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP8

Sample Comments:

|

"

I

I

I

ISample Collected By: GF

1 of 1

I

Page 195: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 88 QC Code: Matrix: Water Tag ID: 2775-88-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc:

External Sample Number: I//- /? U- X " /OO^Q$

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start:

Longitude: End: /_

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals In Water by ICP

Sample Comments:

(N/A)

Sample Collected By: GF

1 of 1

Page 196: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 89 QC Code: Matrix: Water Tag ID: 2775-89-_

Project ID: RS07GEProject Desc: Ace Service Inc. - LIRA GW samples

City: ColbyProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER

IIIIIIIIIIIIIIIII

Sample Collected By: GF L

| y

I

Project Manager: Robert Stewart

State: Kansas

Site ID: 07GE Site OU: 02

Location Desc:

Expected Cone:

Latitude:

Longitude:

External Sample Number

(or Circle One: Low Medium High)

V-Date Time(24 hr)

Sample Collection: Start: lOj^J^S'

End: _J /

Laboratory Analyses:Container Preservative Holding Time

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days

Analysis

1 Metals in Water by ICP

Sample Comments:

(N/A)

0.6.

1 of 1

Page 197: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7 BKansas City, KS •

ASR Number: 2775 Sample Number: 90 QC Code: _ Matrix: Water Tag ID: 2775-90- _ I

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples •

City: Colby State: Kansas •Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02 I

Location Desc: At-/

External Sample Number;!/'/?. W- ty ~ /O

Sample Collected By: GF/"

1 of 1

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr) I

Latitude: Sample Collection: Start: /Q / Otf OS I/ :3 ff

Longitude: End: / / : I

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - l Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

,is.n

Page 198: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

I Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

• ASR Number: 2775 Sample Number: 91 QC Code: _ Matrix: Water Tag ID: 2775-91- _

Project ID: RS07GE Project Manager: Robert Stewart

B , Project Desc: Ace Service Inc. - LIRA GW samplesI City: Colby State: Kansas

Program: Superfund_ Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: " [

External Sample Numbers'/I W 6 -

_ Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

•_

Latitude: ___ Sample Collection: Start:

Longitude: ___ End:

Laboratory Analyses:Container Preservative Holding Time Analysis

• 1-1 Liter Cubitainer HNO3 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

• (N/A)

r

II1

Sample Collected By: GF "

1 of 1

I

Page 199: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 92 QC Code: Matrix: Water Tag ID: 2775-92-

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: ft V- j( *\

External Sample Number: (/

Expected Cone: (or Circle One: Low Medium High)

Latitude: Sample Collection: Start:

Longitude: End:

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

f >U- -7 .$ l

0.0.

Sample Collected By: GF

1 of 1

Page 200: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

I

ASR Number: 2775 Sample Number: 93 QC Code: _ Matrix: Water Tag ID: 2775-93- _

Project ID: RS07GE Project Manager: Robert Stewart

Project Desc: Ace Service Inc. - LTRA GW samplesCity: Colby State: Kansas

Program: Superfund• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

111

0Location Desc: P>

Expected Cone:

Latitude:

Lonqitude:

I/'" p. ft

(or Circle

External Sample Number: \

One: Low Medium High)

Sample Collection: Start:

End:

/- |lw ~yDate

(£L/QS/_0$-

l - / 0 ( ? S T f l q

Time(24 hr)

Laboratory Analyses:

IContainer Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

1 (N/A)

III_ Sample Collected By: GF

I1 of 1

Page 201: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Sample Collection Field SheetUS EPA Region 7Kansas City, KS

ASR Number: 2775 Sample Number: 94 QC Code: _ Matrix: Water Tag ID: 2775-94- _

Project ID: RS07GE Project Manager: Robert StewartProject Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Location Desc: H f A\ W - A S _

^ External Sample Number: \A/- tf /V'1 ' ' 10 °^O £"

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: ___ Sample Collection: Start: {tijQ&jbS |5_: $

Longitude: ___ End: _ /

Laboratory Analyses:Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

(N/A)

f/l- 6 ,W

f—1

Sample Collected By: GF

1 of 1

Page 202: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• Sample Collection Field SheetUS EPA Region 7

• Kansas City, KS

I SR Number: 2775 Sample Number: 95 QC Code: Matrix: Water Tag ID: 2775-95-_

Project ID: RS07GE Project Manager: Robert Stewart•Project Desc: Ace Service Inc. - LIRA GW samples

City: Colby State: KansasProgram: Superfund

• Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

ILocation Desc:: H \fl\S' I ->

External Sample Number: V'Hf^' ]$-/<><?£ 0$

• Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: \bjohj£$

• Longitude: End: / /

Laboratory Analyses:« Container Preservative Holding Time Analysis

1 - 1 Liter Cubitainer HN03 acidify, 4 Deg C 180 Days 1 Metals in Water by ICP

Sample Comments:

Bw\o L O ~ Ik// <

. , f1 D. a CM '*-')'&'> 7

I

I

I

I• Sample Collected By: GF

I1 of!

Page 203: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

October 2005

IIII1II Appendix D

_ Chain of Custody Records

I

I

iiiIiiIii

Page 204: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

CHAIN OF CUSTODY RECORDENVIRONMENTAL PROTECTION AGENCY REGION VII

ACTIVITY LEADEfl(Print) NAME OF SURVEY OR ACTIVITY D)

Bo £> ^TB^AKT -A£g ^E HI/ICES LT£A L \TE OF COLLECTION SHEETrt-K io Ittos . ofi •DAY MONTH YEAR | | /

CONTENTS OF SHIPMENT

SAMPLENUMBER

^L77f- 7 8

)- 7 7£ - 790^775-77JL77S-7M377 C- 731773 - 7CD-77C " &0X775 - 1LX775-UV?7S- 8£

X77S- 831-77C- ^70-775- S/^77S- ftH-

177S-B).^771; v- Bf

CUBITAINER BOTTLE BOTTLE BOHLEVGA SET

(2 VIALS EA)

NUMBERS OF CONTAINERS PER SAMPLE NUMBER

1

|

\

\

— f '» i t\

SAMPLED MEDIA

TV

J(

)(

)(

xxjfXJ(XXXXXAXX

§ sedi

men

t

iolhei

RECEIVING LABORATORYREMARKS/OTHER INFORMATION(condition ot simples upon receipt,

other sample numbers, etc.)

DESCRIPTION OF SHIPMENT MODE OF SHIPMENT

1 b piprF(^) r

1 ICE CHEST

ONSISTING 0

.<;)• HTHFR

: ROXIFS) —A-COMME

COIIRIE•'' ••• — • SflMPL

RCIAL CARRIEf

R

ER CONVEYED

,- UP*

PERSONNEL CUSTODY RECORDF1ELINQUISHED BY (SAMPLER) DATE TIME RECEIVED BY

s£] SEALED UNSEALED p "^'SEALED UNSEALED ["RELINQUISHED BY DATE TIME RECEIVED BY

"ISEALED UNSEALED]" HSEALED UNSEALED fRELINQUISHED BY DATE TIME RECEIVED BY

~1 SEALED UNSEALEO| "[SEALED UNSEALEDf"

5.ZoE8L0fLLljtolli7$(SHIPPING DOCUMENT NUMBER)

REASON FOR CHANGE OF CUSTODY

•REASON FOR CHANGE OF CUSTODY

REASON FOR CHANGE OF CUSTODY

7-EPA-9262(Rev.sed 0/85)

Page 205: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

CHAIN OF CUSTODY RECORDENVIRONMENTAL PROTECTION AGENCY REGION VII

AC IIVITY LEADER(Print) NAME OF SURVEY OR ACTIVITY D

$o& sTEM/?r A-CB $££!/]: CPt LTrtA LATE OF COLLECTION, ShEET 1

2£ ggg. y^^ j oil i •

CONTENTS OF SHIPMENT ~[

SAMPLENUMBER

X77<T~ Ij3L77.r I "*>X77£-£f~^X)-77^'ftmt' \O ')-77C" f \J-77T- /IJ)-711

7f- ]

^77^- <)0J-T^-I**377C- 9 /D77f "ff?^"77C- 5"^7<T- 1 -F/l

1;77S- 9)<?>

CUBITAINER BOHLE BOHLE

NUMBERS OF CONTAINERS

1

IN1

(

BOHLEVOA SET

(2 VIALS EA)

PER SAMPLE NUMBER

DESCRIPTION OF SHIPMENT

J ICE CHEST

ONSISTING 0

SV OTHER

F ROX

SAMPLED MEDIA

£

*

y%XXKXXXKKX)(

XA1

XX

o sedi

men

t

iother

RECEIVING LABORATORY ^REMARKS/OTHER INFORMATION •(condition ol samples upon receipt. •

other sample numoers. etc.) T

j

1j

1]I]41jij•II•

1.

i•

MODE OF SHIPMENT ^

ESI __XCOMMECOURIE

SAMPLI

RCIAL CARRIEF

R

:R CONVEYED

,. M ^<J2.n£8 /tfU/il/Cfc/I(SHIPPING DOCUMENT NUMBER) "*/

PERSONNEL CUSTODY RECORD •F1ELINQUISHED BY (SAMPLER) DATE

53 SEALED UNSEALED (

RELINQUISHED BY DATE

ISEALED UNSEALED(~~RELINQUISHED BY DATE

~I SEALED UNSEALEDf"

TIME RECEIVED BY

^ SEALED UNSEALED ["

TIME RECEIVED BY

~)SEALED UNSEALED \~

TIME RECEIVED BY

"[SEALED UNSEALED)"

REASON FOR CHANGE OF CUSTODY J§

Delbtr ^0 Lai |REASON FOR CHANGE OF CUSTODY jf.

•REASON FOR CHANGE OF CUSTODY •

7-EPA-926?(Revised 5/85)

Page 206: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

CHAIN OF CUSTODY RECORDENVIRONMENTAL PROTECTION AGENCY REGION VII

ACTIVITY LEADER(Print) NAME OF SURVEY OR ACTIVITY

Afstt F1&56.F: LTRACONTENTS OF SHIPMENT

SAMPLENUMBER

3L77C-7/^7 7^_ 7 0

V77fW<|V77r-6fe^77C~ftr?7 r- /r?3-7 7 C-^V77r-^Cl^r-X/s

fr™* / / ) tk

rf~""^ / / x "" * fl

"X7~?r-|k171*- ISX7iq-lH177^-79-77 9 -^V

TYPE OF

CUBITAINER BOTTLE

CONTAINERS

BOTTLENUMBERS OF CONTAINERS

1

\

1

1

1

ru

BOnLEVOA SET

(2 VIALS EA)

PER SAMPLE NUMBER

i//1>

DESCRIPTION OF SHIPMENT

_LtL_ PIECE(S) C

4^ ICE CHEST

ONSISTINGO

SV CITHER

c R

uATE OF.COLLEC1 ION , SHEET->Y-M< 6»<^M^x io7< i loll ;

DAY MONTH YEAR | | 1 /

SAMPLED MEDIA

£re

*

XKXXXXXAKXXXXyyX

g1

1

other

MODE OF SHIPMENT

OX(ES)

PERSONNEL CUSTODY RECORDRELINQUISHED BY (SAMPLER) DATE

33 SEALED UNSEALED pRELINQUISHED BY DATE

"~]SEALED UNSEALED!"RELINQUISHED BY DATE

~1 SEALED UNSEALED(~~

5-

X COMME

COIIRIE

bAIWU

RCIALCARRIEFR

ER CONVEYED

\

RECEIVING LABORATORYREMARKS/OTHER INFORMATION(condition of samples upon receipt,

other sample numbers, etc.)

UK\~LOL9, JOU^3LX/OOI|J8^(SHIPPING DOCUMENT NUMBER)

TIME RECEIVED BY

og.'/JL ^ U%y\ SEALED UNSEALED

TIME DECEIVED BY

~|SEALED UNSEALED

r

rTIME RECEIVED BY

~]SEALED UNSEALED^

REASON FOR CHANGE OF CUSTODY

UCJI^'&'f CD L-^ 0

REASON FOR CHANGE OF CUSTODY

REASON FOR CHANGE OF CUSTODY

7-EPA-9262(Revised 5/85)

Page 207: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

CHAIN OF CUSTODY RECORDENVIRONMENTAL PROTECTION AGENCY REGION VII

ACTIVITY LEADER(Print) NAME OF SURVEY OR ACTIVITY

A35 SERVICES LTRA XMiFtiSpyhoBDAY MONTH YEAR

SHEE"!

/0.

CONTENTS OF SHIPMENT

SAMPLENUMBER

23?6- 1?£??&- 19£?'?5~£D-FL£7?5-£4-,S7? -/S5(277i*>-iS3(S7?«*5 "£G

P?7^-/^2W5-29277/5-30Z??fi-31

P.775-A3£77,5-35£775-5(0/^ -

TYPE OF CONTAINERS

CUBITAINER BOTTLE BOTTLE

NUMBERS OF CONTAINERS

I

1

1

/

J

J/////11///

- — - — "

DESCRIPTION OF SHIPMENT

/LQ PIFCF(S) r.

/ ICE CHEST

[INSISTING 0

SV DTHFR

PERSONNEL CUSTODY RECORDRELINQUISHED BY (SAMPLER) ^^^

"ISEALED UNSEALEDf~

RELINQUISHED BY

~1 SEALED UNSEALEDf"

BOHLEVOA SET

(2 VIALS EA)

PER SAMPLE NUMBER

£ND'

RDX

DATE

"*«,DATE

DATE

,- — — —

^-—

SAMPLED MEDIA

C

1

XXXXXXXXXXXXXXx)(•r-»i

O

^K

sedi

men

t

^

1•o

-*-

olher

>

RECEIVING LA60RATORVREMARKS/OTHER INFORMATION(condition ol samples upon receipt,

other sample numbers etc.)

MODE OF SHIPMENT

ES) ^COMMERCIAL CARRIEF\s rnnnipn

<;iWPi ER CONVEYED

V

(SHIPPING DOCUMENT NUMBER)

TIME RECEIVED BY

— ] SEALED UNSEALED f

TIME RECEIVED BY

~]SEALED UNSEALED [~TIME RECEIVED BY

~JSEALED UNSEALED^

REASON FOR CHANGE OF CUSTODY

D&JVER To LABREASON FOR CHANGE

REASON FOR CHANGE

OF CUSTODY

OF CUSTODY

7-EPA-9262(Revised 5/85)

Page 208: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

CHAIN OF CUSTODY RECORDENVIRONMENTAL PROTECTION AGENCY REGION VII

ACTIVITY LEADER(Print)

BOB STEWARDNAME OF SURVEY OR ACTIVITY

ACE SERVICES LTRACONTENTS OF SHIPMENT

SAMPLENUMBER

£775-37

ggg

£775-4-1<277i5-4££775-43£775 -44£775-46£775-46£775 -4-T5

£775-4££2fl5H8-•ffS77S-49£775-340)^

yftJEO: COLLECTION SHEET JP-C CxTf, <T*XX5 o oil •DAY MONTH YEAR K-» 1 1 •

1TYPE OF CONTAINERS

CUBITAINER BOHLE

NUMBERS OF

/

/

^/ii/iii]i}i11

•"- — _

BOTTLE

CONTAINERS

*

BOTTLEVOA SET

(? VIALS EA)

PER SAMPLE NUMBER

avD S -.

DESCRIPTION OF SHIPMENT

/(j PIECE)

/ ICE CH

S ) C

EST

ONSISTING 0

S): OTHER

F Rny ES)

PERSONNEL CUSTODY RECORDRELINQUISHED

(4fJW&~~\ SEALED /

"1 SEALEDRELINQUISHED

"1 SEALED

BY (SAMPLER)

'pmnurrrvJ/flSEALEO p

1* (J

UNSEALED f~BY

UNSEALED)

DATE

DATE

DATE

TIME

TIME

TIME

- —

SAMPLED MEDIA

_

re

XXXXXXXXXXXXXXXXy

6

sedi

men

t

T3

otherRECEIVING LABORATORY J

REMARKS/OTHER INFORMATION •(condition ol samples upon receipt. •

other simple numbers, etc ) •

J1JI

1•

1.

|

'

1•

^COMMEV miiPig

.^flUPL

RCIALCARRIEF

R

ER CONVEYED

5- —

1(SHIPPING DOCUMENT NUMBER)

»RECEIVED BY

~~| SEALED UNSEALED f

RECEIVED BY

^SEALED UNSEALED f

RECEIVED BY

] SEALED UNSEALEDP

REASON FOR CHANGE OF CUSTODN^

DELIVER To LAELREASON FOR CHANGE OF CUSTOD1^

•REASON FOR CHANGE OF CUSTOUM

7-EPA-9262(Revised

Page 209: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

CHAIN OF CUSTODY RECORDENVIRONMENTAL PROTECTION AGENCY REGION VII

ACTIVITY LEADER(Print) NAME OF SURVEY OR ACTIVITY 0

fiofl STEWART ACE SERVICES LTRACONTENTS OF SHIPMENT

SAMPLE

NUMBER

/£??£- 5(2>£?7£-6?£77*5 --58£7?5-59£775 -GO£7715-67

^ —

ATEOFCpLJCTION SHEET

A\3 O*/ JaJQS o ofl oDAY MONTH YEAR O T 1 05

TYPE OF CONTAINERS

CUBITAINER BOTTLE BOTTLE

NUMBERS OF CONTAINERS

/

/

/

/

7/

• — --d

BOTTLEVOA SET

(2 VIALS EA)

PER SAMPLE NUMBER

END r — -

'

DESCRIPTION OF SHIPMENT

_UL_ PIECE(S) C

/ ICE CHEST

ONSISTINGO

S)- OTHER

: RflX

PERSONNEL CUSTODY RECORD

RELINQUISHED BY (SAMPLER) DATE

I/SEALED / y^NSEALED | \jQ

"[SEALED UNSEALED[~RELINQUISHED BY DATE

~1 SEALED UNSEALED]""

ES)

TIME

TIME

TIME

^ •

SAMPLED MEDIA

SI

XXXXXX'-

a

cft>E

iiolhcr

RECEIVING LABORATORYREMARKS/OTHER INFORMATION(condition ol samples upon receipt,

other sample numbers etc.)

MODE OF SHIPMENT

v .COURIE

.SAMPL

RCIALCARRIEF

R

ER CONVEYED

I"

(SHIPPING DOCUMENT NUMBER)

RECEIVED BY

— | SEALED UNSEALED f

RECEIVED BY

"[SEALED UNSEALED/^

RECEIVED BY

~~ [SEALED UNSEALED)"

REASON FOR CHANGE OF CUSTODY

DELIVER To LABREASON FOR CHANGE OF CUSTODY

REASON FOR CHANGE OF CUSTODY

7-EPA.9262(Revised 5/85)

Page 210: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIII• Appendix E

Airbills

I_ October 2005

I

iiiiiiiii

Page 211: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

SHIPPER'S f

COPY

^a'ssj ~t~

instructions on back. Call 1-80O-PICK-UPS (800-742-5877)

additional information.FOB WDRLCWICE EXPRESS SWPNB^S

DOCUMENTS]ONLY

Mark m'Jf in lis box ishJcrnert onlyocxlans cteuments at no conrmnad wjua

1Z OE8 10W 22 1001 270 5 SATURDAYDEUVERY

REFERENCE NUMBER

An Additional Handling Charge applies lor cenain!em». See Instructions.

BLACK & VE£TCH SPEetppjbj CORP

CITY, AND STATED ZIP CODE

KS 67701 EXPIRATION •DATE

THIRD PARTY'S COMPANY- NAME

STREET ADDRESS

STREET ADDRESS

CITY AND STATE (INCLUDE COUNTRY IF INTERNATIONAL) • LZIPCODE

0101911202609 8/00 MM

SHIPPER'S

COPY

See instructions on back. Call 1-8OO-PICK-UPS (800-742-5877)

for additional information. tvtort an'>f In Ms «K it riitmsil onrycotalns documnts d no oornmrdal value.

1Z OE8 10W 22 1001 271 4

An Additional Handling Charge applies for certainitems. See instructions.

BLACK &VEAtCH

CITY AND STATED*. it?, tt^r 'COLBf EXPIRATION

DATE

HIRD PARTY'S COMPANY NAME

STREET ADDRESS! urn

|lhttf.

CITY AND STATE ZIP CODE

CITY AND STATE ( INCLUDE COUNTRY IF INTERNATIONAL) i ZIP CODE

It^S

M-tiSDATE OF SHIPMENT

10 I Of 105

Page 212: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

See instructions on back. Call 1-80O-PICK-UPS (8OO-742-5877)for additional information.

TRACKING NUMBER 1Z OE8 10W 22 1001 198 4

REFERENCE NUMBER

046132.0147NAME '.- TELEPHONE•

O. V.C: 785-460-0116- •COMPANY

BLACK &'VEAtCH SPEC.PRCfl CORPSTREET-ADDRESS ^ -.. ft JXO**'

500E4TH§TCZIP CODE

KS 677012:EXTREMELY3uRGENCTlELIVERYT

NAME

NICOLE ROBLEZ

TELEPHONE

913-551-5130COMPANY ' :

US EPA REGION 7 LABSTREET ADDRESS DEPT./FLR.

300 MINNESOTA AVECITY AND STATE ( INCLUDE COUMTRY If INTERNATIONAL) i ZIP CODE :

KANSAS CITY KS

ENTER "ITR"IF LETTER

WEIGHT

^J RECOVERS/THIRD PARTYS UPS Acer. NO. OR MAJOR CREDTT CARONO. EXPIRATION *j5|J

THIRD PARTY'S COMPANY NAME

STREET ADDRESS

' ''

CITY AND STATE ZIP CODE

O SHIPPER'SSIGNATURE .

DATE OF SHIPMENTill

0101811202609 6/00 M./V

I

I

I

I

I

I

I

I

I

I

I

I

I

Page 213: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIiIIM Appendix F

Field Logbooks

IOctober 2005

iiiiiiiiii

Page 214: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

[ 3 en a. en en

r^:^S^-!\-

Page 215: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII
Page 216: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

fft/J[

3

A n;.

<9ut>\

'1 —

'

W//Il(l0 Wet ;

; lW-oO

n1779-79

w// /A row (g.

er

Page 217: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII
Page 218: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII
Page 219: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII
Page 220: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

/|/?/ii. ),/-(>$ i I ^ o, //*;

.1 US Bif\i/itn>/\iy^i"'l

Page 221: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

• ; ' . . . - • ' • ' ^ . • • • r • : ' . . . " . ',•;*-•'•: -w^-V^1

• - ? . ' • , ' • . . • . ' , • • ' • ; ' . ' • -'"•„' "*-«.:; >v<• •? . , -> -.-;'.' *'

Page 222: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

cm • cm cm"' C±D; cm •'. cz : c m ' . : ' . : - - ' - c ± 3 - .-"cm

S it r^ *" ?•; ' !; •• ;"j-' • :•'.;/K#i:.; '•'.. •:•;' >;-i :- *••.'...;£,;. i-''i'--. v-',-1- . - ' i i •*»"'•-,•*> •%tFi?*Tff*'S''f'St=??-' '••'•''• "c>K'1^S'-"-:-''%'i'*:J''*'''''ti^'W'1!*;!^ r'^'^S'" 'r?J6i:':;''V- •' ~'-Jt %"--- .-7 ".*"•"-;: '••• V *•••'. -'-.I ••''*••.'~ ' • ' • ' ' ' . . . . • : ' . ."'•• '':.':---.-" • - - . " ' • • « • :

: ;;:;ff |g||ljS|fe

Page 223: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII
Page 224: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII
Page 225: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII
Page 226: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

iroc/ceo083?-

0301-

- QaMjudtzjd

®jjjdUb-76MIA/- &-S

0945-

1001- 1809

1833

1133-

1156-

<&MJlM>-1Q 0010

I J

Page 227: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

CB3&I08.45-

, 0.932-

OB-l^.D

&&?•-: '• •• :'ljjlrj^J

Page 228: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

113?-I14Q-

MW-1rD u

- 7! -

(TTMurrifibu

p.bb Q

10-11 -OS

..... „.5 i ! : ^ •o6

^amw&u cdbMJtM;

a±>

vdb W?-

10-11-06

-so

cub

' O

r>i

Ji i.!-

Page 229: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

TGWTP(&(Wnd>...

CQjrdimue.

151Z-.15321

jnjas,-" T1.4G3

16851

GS8-

uO L

joaws^^jtrnJ^ajnousT^

Page 230: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

DGWTP

Q-Du:- a

^bJ&UrrnJV\

v

10

10-12,-OScmj

i 4*-^' M~*~**-:s \J**~> cc'A'O*—' ^f

053- QMuSwdj Jrajctu® QWTP

Page 231: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Gwte-A

-JUMMJL

ccbWvmw • a \ i ! =

'ibbLtM&kli

> QfitfEi

10-1Q-Q5

Page 232: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

1703-

sasnd Iv ./aasH

WJO&WJiMVLb.

Page 233: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIII• Appendix G

Analytical Results

I

^ October 2005

9

I

iiiiiiiii

Page 234: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

11" RPD Calculations— Ace Services Site: October 2005

I

1

1

e•viiI

i

Result of primary

Result of duplicate

Result of primary

Result of duplicate

Result of primary

Result of duplicate

Result of primary

Result of duplicate

I RPD = relative percent difference

RPD = (D1-D2)/(0.5(D1+D2))

ANALYTE = total chromiumsample analyte = <10 ug/L

sample analyte = <10 ug/L

RPD = 0%

ANALYTE = total chromiumsample analyte = <10 ug/L

sample analyte = <10 ug/L

RPD = 0%

ANALYTE = total chromiumsample analyte = 10.7 ug/L

sample analyte = 10.4 ug/L

RPD = 3%

ANALYTE = total chromiumsample analyte = 350 ug/L

sample analyte = 344 ug/L

RPD = 2%

Sample No.MW-16-D

MW-16-D-FD

Sample No.MW-2-D

MW-2-D-FD

Sample No.MW-8-I

MW-8-I-FD

Sample No.PWS-8

PWS-8-FD

RPD goal +/-20 percent for water media (BVSPC 2003b)

1

1

itii

Ace Services Site

•| LTRA Cleanup Status Report No. 5 I of 1 044720

Page 235: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIiI

ft* JT.

I

I

I

I

iIiiIiiIIi

United States Environmental Protection AgencyRegion 7

901 N. 5th StreetKansas City, KS 66101

Date:

Subject: Transmittal of Sample Analysis Results for ASR #: 2775

Project ID: RS07GE

Project Description: Ace Service Inc. - LIRA GW samples

From: Dale I. Bates, DirectorRegional Laboratory, Environmental Services Division

To: Robert StewartSUPR/IANE

Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) andProject. The Regional Laboratory has reviewed and verified the results in accordance with proceduresdescribed in our Quality Manual (QM). In addition to all of the analytical results, this transmittalcontains pertinent information that may have influenced the reported results and documents anydeviations from the established requirements of the QM.

Please contact us within 14 days of receipt of this package if you determine there is a need for anychanges. Please complete the enclosed Customer Satisfaction Survey and Data Disposition memo forthis ASR.

If you have any questions or concerns relating to this data package, contact our customer service lineat 913-551-5295.

Enclosures

cc: Analytical Data File.

Page 1 of 30

Page 236: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775 Summary of Project Information 11/01/2005

Project Manager: Robert Stewart Org: SUPR/IANE Phone: 913-551-7654

Project ID: RS07GE

Project Desc: Ace Service Inc. - LTRA GW samples

Location: Colby State: Kansas Program: Superfund

Site Name: ACE SERVICES - GROUNDWATER Site ID: 07GE Site OU: 02

Purpose: Compliance Monitoring

October 2005 semi-annual sampling event.

Explanation of Codes, Units and Qualifiers used on this report

Sample QC Codes: QC Codes identify the type of Units: Specific units in which results aresample for quality control purpose. reported.

= Field Sample Deg C = Degrees CelsiusFD = Field Duplicate NTU = Nephelometric Turbidity Units

SU = Standard Units (pH)mg/L = Milligrams per Literug/L = Micrograms per Liter

umhos/cm = Micromhos per Centimeter

Data Qualifiers: Specific codes used in conjunction with data values to provide additional informationon the quality of reported results, or used to explain the absence of a specific value.

(Blank)= Values have been reviewed and found acceptable for use.U = The analyte was not detected at or above the reporting limit.

Page 2 of 30

Page 237: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIiiiIiiii1iiiiiiii

ASR Number: 2775

Project ID: RS07GE

Sample Information Summary

Project Desc: Ace Service Inc. - LIRA GW samples

11/01/2005

Sample QCNo Code Matrix

1 - _ Water

2 - _ Water

2 - FD Water

4 - Water

5 - Water

6 - Water

7 - _ Water

8 - Water

9 - Water

10 - Water

11 -_ Water

12 -_ Water

13 - _ Water

14 -_ Water

15 - _ Water

16 - Water

17 - _ Water

18 - _ Water

19 - _ Water

20 - Water

20 - FD Water

22 - _ Water

23 - _ Water

24 - _ Water

Location Description

MW-2-I

MW-2-D

MW-2-D/Field Duplicate of sample2

MW-13-D

MW-13-I

MW-15-I

MW-15-S

MW-15-D

MW-14-I

MW-17-I

MW-17-S

MW-17-D

MW-18-S

MW-18-D

MW-18-I

MW-2-S

MW-3D

MW-16-I

MW-16-S

MW-16-D

MW-16-D/Field Duplicate ofsample 20MW-7-D

OB-2-D

MW-7-I

ExternalSample No

W-MW-2-1-100405W-MW-2-D-100405W-MW-2-D-100405W-MW-13-D-100405W-MW-13-1-100405W-MW-15-1-100405W-MW-15-S-100405W-MW-15-D-100505W-MW-14-1-100505W-MW-17-1-100505W-MW-17-S-100505W-MW-17-D-100505W-MW-18-S-100505W-MW-18-D-100505W-MW-18-1-100505W-MW-2-S-100605

W-MW-16-1-100605

W-MW-16-D-100605

W-MW-7-D-100605

StartDate

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/05/2005

10/05/2005

10/05/2005

10/05/2005

10/05/2005

10/05/2005

10/05/2005

10/05/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/07/2005

10/06/2005

Start EndTime Date

09:22

11:35

11:36

15:01

15:24

17:12

17:32

09:20

09:59

11:36

12:06

14:52

15:30

17:24

09:25

10:01

11:53

12:1514:50

14:51

09:08

16:46

End ReceiptTime Date

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/11/2005

10/11/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/11/2005

10/11/2005

10/11/2005

10/14/2005

10/11/2005

10/14/2005

10/11/2005

10/14/2005

10/11/2005

10/14/2005

10/14/2005

Page 3 of 30

Page 238: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775

Project ID: RS07GE

Sample Information Summary

Project Desc: Ace Service Inc. - LIRA GW samples

11/01/2005

Sample QCNo Code

25 -_

26 -_

27 -_

28 -_

29 -_

30 -_

31 -

32 -_

33 -_

34 -_

35 -_

36 -_

37 -_

38 -_

39 -_

40 -_41 -

42 -_

43 -_44 - _

45 -_

46 -_47 -

48 -_

48 - FD

49 - _

55 -_

56 -_

57 - _

58 -_

59 -_

60 -__

61 -__66 - _

67 -_

68 - _

69 - _

70 - _

71 - _

Matrix Location Description

Water MW-7-S

Water OB-2-I

Water OB-l-D

Water OB-l-I

Water MW-l-IWater MW-l-D

Water MW-l-SWater MW-9-I

Water MW-9-D

Water MW-9-S

Water MW-5-IWater MW-5-DWater MW-5-SWater MW-4-I

Water MW-4-D

Water MW-4-SWater MW-6-D

Water Rinsate sample

Water MW-6-IWater MW-6-S

Water MW-ll-I

Water MW-ll-DWater MW-ll-S

Water MW-8-IWater MW-8-I/Field Duplicate of sample

48Water MW-8-D

Water OB-l-SWater OB-2-S

Water MW-8-S

Water MW-12-S

Water Rinsate sample

Water MW-12-I

Water MW-12-D

Water MW-13S

Water MW-14S

Water ARW-S

Water ARW-I

Water ARW-D

Water Rinsate Blank sample

ExternalSample No

W-MW-13-S-100605W-MW-14-S-100605W-ARW-S-100605W-ARW-1-100605W-ARW-D-100605W-RIN-100605-R

StartDate

10/06/2005

10/07/2005

10/07/2005

10/07/2005

10/10/2005

10/10/2005

10/10/2005

10/11/2005

10/11/2005

10/13/2005

10/11/2005

10/11/2005

10/11/2005

10/11/2005

10/11/2005

10/12/2005

10/12/2005

10/12/2005

10/12/2005

10/12/2005

10/12/2005

10/12/2005

10/12/2005

10/12/2005

10/12/2005

10/12/2005

10/13/2005

10/13/2005

10/13/2005

10/13/2005

10/13/2005

10/13/2005

10/13/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

10/06/2005

Start EndTime Date

18:09

09:32

11:15

11:40

14:25

15:05

16:38

10:02

10:27

12:20

13:26

14:45

13:03

16:50

16:25

09:25

11:13

15:16

10:50

12:25

14:15

14:40

15:58

18:12

18:14

17:40

11:03

11:45

14:08

14:55

15:41

16:39

17:03

12:51

11:43

14:54

14:28

13:56

16:12

End ReceiptTime Date

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/14/2005

10/11/2005

10/11/2005

10/11/2005

10/11/2005

10/11/2005

10/11/2005

Page 4 of 30

Page 239: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIiIiiiiiiiiiiiiiii

ASR Number: 2775

Project ID: RS07GE

Sample Information Summary

Project Desc: Ace Service Inc. - LIRA GW samples

11/01/2005

Sample QCNo Code

73 -

73 - FD

75 -_

76 -_

77 -_

78 -

79 -_

80 -_

81 -_

82 -_

83 -_

84 -

85 -_

86 -_

87 -_

88 -_

89 -

90 -_

91 -_

92 -_

93 -_

94 -_

95 -_

Matrix

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Location Description

PWS-8

PWS-8/Field Duplicate of sample73

RW-7

RW-5

EX-4S

EX- 11

EX- ID

EX-2D

EX-2I

EX-3S

EX-3I

EX-3D

EX-4I

EX-5S

EX-5I

RW-2

RW-3

RW-4

RW-6

RW-/ ^ J|X,1 7 il* l *^» '

RW-^ 8

HPMW-6S

HPMW-9S

ExternalSample No

W-PWS-8-100405W-PWS-8-100405-FDW-RW-7-100405W-RW-5-100405W-EX-4S-100405W-EX-1I-100405W-EX-1D-100405W-EX-2D-100405W-EX-2I-100405W-EX-2S-100405W-EX-3I-100405W-EX-3D-100405W-EX-4I-100405W-EX-5S-100405W-EX-5I-100405W-RW-2-100505W-RW-3-100505W-RW-4-100505W-RW-6-100505 qW-RW-I-100505W-RW-/-8100505W-HPMW-6-S-100605W-HPMW-9-S-100605

StartDate

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/04/2005

10/05/2005

10/05/2005

10/05/2005

10/05/2005

10/05/2005

10/05/2005

10/06/2005

10/06/2005

Start EndTime Date

10:15

10:15

10:43

11:25

12:00

13:35

14:18

14:50

15:10

15:41

16:00

16:21

16:51

17:23

17:53

12:35

12:03

11:38

10:52

10:06

09:34

15:50

16:33

End ReceiptTime Date

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/07/2005

10/11/2005

10/11/2005

Page 5 of 30

Page 240: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number:2775 RLAB Approved Analysis Comments 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis Comments About Results For This Analysis

1 Conductivity by Field MeasurementLab: (Field Measurement)

Method: Measurement of field parameter (no SOP)

Samples: 1- 2- 2-FD 4- 5- 6- 7-8-15-22-__29-36-44-55-_67-__76-83-_90-

Q_

1 O™

23-_30-_37-45-_56-_68-_77-84-_91-

10-17-24-_31-38-_46-_57-_69-_78-_85-92-

11-18-25-_32-_39-_47-_58-_70-_79-_86-_93-_

12-19-26-_33-_40-_48-_60-_73-_80-_87-_94-_

13-20-_27-34-41-48-FD61-73-FD81-88-_95-_

14-20-FD28-_35-_43-49-_66-_75-_82-_89-

Comments:(N/A)

Metals in Water by ICPLab: Contract Lab Program (Out-Source)

Method: CLP Statement of Work

Samples: 1- 2-1-8-15-22 -_29-36-43-_49-__61-73-_80-_87-_94-_

2-9-16-23-_30-_37-_44-55-_66-_73-FD81-88-_95-_

2-FD

17-24-31-38-_45-_56-_67-_75-_82-_89-_

11-18-25-32-__39-46-_57-68-__76-_83-_90-__

12~19-26-_33-40-_47-_58-69-_77-_84-_91-

13~20-_27-_34-_41-48-_59-_70-_78-_85-_92-_

7-14-20-FD28-_35-_42-_48-FD60-_71-79-_86-_93-

Comments:(N/A)

1 pH of Water by Field MeasurementLab: (Field Measurement)

Method: Measurement of field parameter (no SOP)

Samples: !-__ 2-_ 2-FD 4-__ 5-_ 6-_ 7-_

Page 6 of 30

Page 241: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

11ii

iPii•

ASR Number:2775 RLAB Approved Analysis Comments

Project ID: RS07GE Project Desc: Ace Service Inc. - LTRA GW samples

11/01/2005

Analysis Comments About Results For This Analysis

Samples: 8-

22-_29-_36-_44-55-_67-_76-_83-_90-_

Comments:(N/A)

1 Temperature of Water by

16~23-_30-_37-_45-_56-_68-_77-_84-_

91-_

1°--24-_31-38-_46-_57-_69-_78-_85-_92-_

18-~25-_32-_39-_47-_58-_70-_79-_86-_93-_

19-~26-_33-_40-_48-_60-_73-_80-_87-_94-_

20-27-_34-

41-_48-FD61-73-FD81-88-_95-_

14-

20-FD28-.35-.43-49-.66-75-82-89-

_

Field MeasurementLab: (Field Measurement)

i

iw••I1

Method: Measurement of field

Samples: 1-

it22-_29-_36-44-_55-_67-76-83-_90-_

Comments:(N/A)

1 Total Dissolved Oxygen in

2-9-

23-_30-_37-_45-_56-_68-_77-_84-_91-_

Water by

parameter

2-FD

17-~24-_31-38-_46-_57-_69-_78-_85-92-_

(no SOP)

4-

it25-_32-_39-_47-_58-_70-_79-_86-_93-_

5-

19-~26-_33-_40-_48-_60-_73-_80-_87-_94-_

6-

20-_27-34-_

48-FD61-73-FD

88-95-_

7-_

20-FD28-35-43-49-66-75-82-89-

_

Field MeasurementLab: (Field Measurement)

1 Method: Measurement of field

E•

1

1

1

Samples: 1-8-15 I_22-_29-_36-_44 -_

2-_Q_

1 D~

23-_30-_37-_

45-_

parameter

2-FD

10-

17-Z24-_31-38-_

46-_

(no SOP)

4-

11-18-25-_32-_

39-_47-_

5-_12-

19-Z26-_33-_

40-_

48-_

6-_13-20-_27-34-_

48-FD

7-_14-20-FD28-35-43-

49-—

Page 7 of 30

Page 242: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number:2775 RLAB Approved Analysis Comments 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LTRA GW samples

Analysis Comments About Results For This

Samples: 55-67-76-_83-90-_

56-_68-77-84-91-_

57-_69-_78-_85-92-_

Analysis

58-_70-79-_86-93-_

60-_73-80-_87-_94-_

61-_73-FD81-_88-95-_

66-_75-82-89-

Comments:(N/A)

Turbidity of Water by Field MeasurementLab: (Field Measurement)

Method: Measurement of field parameter (no SOP)

Samples: 29-_ 30-_ 31-_ 32-_ 33-_ 34-_ 35-36-_ 37-_ 38-_ 39-_ 40- 41-_ 43-44-_ 45-_ 46-_ 47-_ 48-_ 48-FD 49-55-_ 56-_ 57- 58-_ 60-_ 61-_

Comments:(N/A)

Page 8 of 30

Page 243: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

I Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 1- 2- 2-FD 4-

• 1 Conductivity by Field MeasurementConductivity umhos/cm 894 437 437 497

_ 1 Metals in Water by ICP• Chromium ug/L 406 10.0 U 10.0 U 10.0 U

1 pH of Water by Field Measurement

I

I

I

I

I

iiiiiIiiii

pH SU 6.4 6.96 6.96 5.53

1 Temperature of Water by Field MeasurementTemperature Deg C 16.52 16.62 16.62 18.78

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 3.20 7.64 7.64 8.26

Page 9 of 30

Page 244: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 5- 6- 7- 8-

1 Conductivity by Field MeasurementConductivity umhos/crn 473 479 581 454

1 Metals in Water by ICPChromium ug/L 10.2 10.0 U ill 37.2

1 pH of Water by Field MeasurementpH SU 5.77 7.24 6.96 7.33

1 Temperature of Water by Field MeasurementTemperature Deg C 24.04 15.83 19.89 15.40

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 8.27 8.29 8.31 7.68

Page 10 of 30

Page 245: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

• Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 9- 10- 11- 12-

• 1 Conductivity by Field MeasurementConductivity umhos/cm 679 529 895 461

~ 1 Metals in Water by ICP• Chromium ug/L 12.5 10.0 U 11.4 10.0 U

1 pH of Water by Field MeasurementpH SU 7.22 7.28 7.23 7.56

I I Temperature of Water by Field MeasurementTemperature Deg C 14.75 14.89 13.00 15.98

1 Total Dissolved Oxygen in Water by Field Measurementfl Dissolved Oxygen mg/L 7.66 8.44 8.23 8.34

I

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iiiiiIii• Page 11 of 30

I

Page 246: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 13- 14- 15- 16-

1 Conductivity by Field MeasurementConductivity umhos/cm 890 478 520 743

1 Metals in Water by ICPChromium ug/L 10.0 U 10.0 U 10.0 U 10.0 U

1 pH of Water by Field MeasurementpH SU 6.97 7.47 7.30 6.93

1 Temperature of Water by Field MeasurementTemperature Deg C 17.58 15.24 15.11 14.23

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 9.03 8.22 8.40 8.27

Page 12 of 30

Page 247: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

• Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 17- 18- 19- 20-

I 1 Conductivity by Field MeasurementConductivity umhos/cm 503 465 778 468

I I Metals in Water by ICPChromium ug/L 10.0 U 10.0 U 10.0 U 10.0 U

1 pH of Water by Field MeasurementpH SU 7.09 7.28 7.19 7.53

• 1 Temperature of Water by Field Measurement• Temperature Deg C 15.24 14.81 13.99 15.38

^ 1 Total Dissolved Oxygen in Water by Field Measurement• Dissolved Oxygen mg/L 7.82 8.29 7.99 8.14

I

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I

Page 248: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 20-FD 22- 23- 24-

1 Conductivity by Field MeasurementConductivity umhos/cm 468 424 419 668

1 Metals in Water by ICPChromium ug/L 10.0 U 10.0 U 11.6 10.0 U

1 pH of Water by Field MeasurementpH SU 7.53 7.46 7.58 7.29

1 Temperature of Water by Field MeasurementTemperature Deg C 15.38 15.16 7.84 14.42

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 8.14 7.80 10.08 7.21

Page 14 of 30

Page 249: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

I Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 25- 26- 27- 28-

| 1 Conductivity by Field MeasurementConductivity umhos/cm 633 527 417 549

II Metals in Water by ICP

Chromium ug/L 10.9 132 10.0 U 10.0 U

1 pH of Water by Field MeasurementpH SU 7.26 7.20 7.53 7.35

I I Temperature of Water by Field MeasurementTemperature Deg C 14.13 14.68 15.37 15.23

1 Total Dissolved Oxygen in Water by Field Measurement• Dissolved Oxygen mg/L 7.91 7.89 7.73 7.54

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I

Page 250: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LTRA GW samples

Analysis/ Analyte Units 29- 30- 31- 32-

1 Conductivity by Field MeasurementConductivity umhos/cm 1.309 0.472 1.306 599

1 Metals in Water by ICPChromium ug/L 10.0 U 10.0 U 10.0 U 17.1

1 pH of Water by Field MeasurementpH SU 6.61 7.49 6.65 7.10

1 Temperature of Water by Field MeasurementTemperature Deg C 15.46 15.88 15.64 14.81

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 0.12 7.28 0.32 6.87

1 Turbidity of Water by Field MeasurementTurbidity NTU -1.5 -2.9 -2.4 -1.7

Page 16 of 30

Page 251: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

• Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 33- 34- 35- 36-

I 1 Conductivity by Field MeasurementConductivity umhos/cm 513 805 771 434

I I Metals in Water by ICPChromium ug/L 10.1 59.0 10.0 U 21.1

1 pH of Water by Field Measurement

IpH SU 7.34 7.22 7.35 7.55

1 Temperature of Water by Field MeasurementTemperature Deg C 15.16 21.13 13.62 15.48

_ 1 Total Dissolved Oxygen in Water by Field Measurement• Dissolved Oxygen mg/L 7.69 7.16 7.30 6.96

1 Turbidity of Water by Field MeasurementTurbidity NTU -1.8 130.5 0.8 -0.2

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• Page 17 of 30

I

Page 252: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 37- 38- 39- 40-

1 Conductivity by Field MeasurementConductivity umhos/cm 1.198 783 424 1.153

1 Metals in Water by ICPChromium ug/L 10.0 U 10.0 U 10.0 U 10.0 U

1 pH of Water by Field MeasurementpH SU 7.32 7.14 7.57 7.02

1 Temperature of Water by Field MeasurementTemperature Deg C 15.14 14.84 15.32 15.20

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 7.45 6.79 7.12 6.93

1 Turbidity of Water by Field MeasurementTurbidity NTU 131.1 -0.4 -0.5 -0.9

Page 18 of 30

Page 253: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

• Project ID: RS07GE Project Desc: Ace Service Inc. - LTRA GW samples

Analysis/ Analyte Units 41- 42- 43- 44-

| 1 Conductivity by Field MeasurementConductivity umhos/cm 0.414 0.641 577

I I Metals in Water by ICPChromium ug/L 10.0 U 10.0 U 10.0 U 10.0 U

1 pH of Water by Field Measurement_ pH SU 7.58 7.17 7.39

• 1 Temperature of Water by Field MeasurementTemperature Deg C 15.82 15.32 15.29

— 1 Total Dissolved Oxygen in Water by Field MeasurementB Dissolved Oxygen rng/L 6.91 6.91 7.36

• 1 Turbidity of Water by Field MeasurementTurbidity NTU 39.5 -1.3 0.3

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• Page 19 of 30

I

Page 254: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 45- 46- 47- 48-

1 Conductivity by Field MeasurementConductivity

1 Metals in Water by ICPChromium

1 pH of Water by Field MeasurementPH

1 Temperature of Water by Field MeasurementTemperature

umhos/cm

ug/L

SU

DegC

602

10.0 U

7.32

16.00

472

10.0 U

7.50

16.00

725

14.2

7.16

15.94

623

10.7

7.20

16.02

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen

1 Turbidity of Water by Field MeasurementTurbidity

mg/L

NTU

6.78

-1.8

7.39

-1.9

7.27

129.8

6.77

20.3

Page 20 of 30

Page 255: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

II

ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

• Analysis/ Analyte Units 48-FD 49- _ 55- _ 56- _

* 1 Conductivity by Field MeasurementConductivity umhos/cm 623 479 411 747

I I Metals in Water by ICPChromium ug/L 10.4 10.0 U 10.0 U 30.3

1 pH of Water by Field Measurement

I PH SU 7.20 7.39 7.57 7.21

1 Temperature of Water by Field MeasurementTemperature Deg C 16.02 15.90 19.45 20.82

I I Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 6.77 7.33 6.71 7.31

1 Turbidity of Water by Field Measurementg Turbidity NTU 20.3 -2.6 2.8 -1.7

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Page 21 of 30

Page 256: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775

Project ID: RS07GE

Analysis/ Analyte

RLAB Approved Sample Analysis Results

Project Desc: Ace Service Inc. - LIRA GW samples

11/01/2005

Units

1 Conductivity by Field MeasurementConductivity

1 Metals in Water by TCPChromium

1 pH of Water by Field MeasurementpH

1 Temperature of Water by Field MeasurementTemperature

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen

1 Turbidity of Water by Field MeasurementTurbidity

57- 58- 59- 60-

umhos/cm

ug/L

SU

DegC

jrementmg/L

NTU

669

37.6

7.00

16.87

6.36

-1.1

528

10.6

7.28

15.95

7.63

-0.7

499

10.0 U 10.0 U

7.38

19.63

7.64

-2.0

Page 22 of 30

Page 257: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

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Project ID: RS07GE Project Desc: Ace Service Inc. - LTRA GW samples

Analysis/ Analyte Units 61- 66- 67- 68-

1 Conductivity by Field MeasurementConductivity umhos/cm 396 814 811 1063

I I Metals in Water by ICPChromium ug/L 10.0 U 10.0 U 10.6 1600

1 pH of Water by Field Measurement

I pH SU 7.42 7.15 7.23 6.84

1 Temperature of Water by Field MeasurementTemperature Deg C 16.02 17.17 16.80 16.99

I I Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 7.34 7.50 8.63 1.16

1 Turbidity of Water by Field Measurement^ Turbidity NTU -1.2

Page 23 of 30

Page 258: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 69- 70- 71- 73-

1 Conductivity by Field MeasurementConductivity umhos/cm 902 617 690

1 Metals in Water by ICPChromium ug/L 794 277 10.0 U 350

1 pH of Water by Field MeasurementpH SU 6.94 7.17 6.96

1 Temperature of Water by Field MeasurementTemperature Deg C 16.51 15.89 15.00

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 3.88 7.18 7.65

Page 24 of 30

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ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

IAnalysis/ Analyte Units 73-FD 75- 76- 77-_

1 Conductivity by Field MeasurementConductivity umhos/cm 690 488 487 511

1 Metals in Water by TCPChromium ug/L 344 10.0 U 36.2 17.9

1 pH of Water by Field Measurement

I pH SU 6.96 7.36 7.36 8.17

1 Temperature of Water by Field MeasurementTemperature Deg C 15.00 15.10 16.26 14.96

I I Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 7.65 8.66 8.43 1.51

Page 25 of 30

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ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Sen/ice Inc. - LIRA GW samples

Analysis/ Analyte Units 78- 79- 80- 81-

1 Conductivity by Field MeasurementConductivity umhos/cm 673 451 500 642

1 Metals in Water by ICPChromium ug/L 926 17.4 53.8 181

1 pH of Water by Field MeasurementpH SU 7.25 7.46 7.11 6.25

1 Temperature of Water by Field MeasurementTemperature Deg C 15.17 15.34 15.22 14.76

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 6.83 8.31 8.32 8.40

Page 26 of 30

Page 261: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

• Analysis/Analyte Units 82- 83- 84- 85-—

1 Conductivity by Field MeasurementConductivity umhos/cm 821 520 511 607

I I Metals in Water by ICPChromium ug/L 33.8 135 36.9 61.0

1 pH of Water by Field Measurement• pH SU 6.54 6.18 5.60 6.16

1 Temperature of Water by Field MeasurementTemperature Deg C 14.52 14.18 15.40 14.90

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 8.66 8.28 8.34 8.63

Page 27 of 30

Page 262: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 86- 87- 88- 89-

1 Conductivity by Field MeasurementConductivity umhos/cm 798 547 427 504

1 Metals in Water by ICPChromium ug/L 21.6 50.7 11.2 10.0 U

1 pH of Water by Field MeasurementpH SU 6.65 7.07 7.63 7.55

1 Temperature of Water by Field MeasurementTemperature Deg C 14.73 14.96 15.02 14.98

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 8.74 8.41 8.95 8.13

Page 28 of 30

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ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LTRA GW samples

Analysis/ Analyte Units 90- 91- 92- 93-

1 Conductivity by Field MeasurementConductivity umhos/cm 502 498 476 587

I I Metals in Water by ICPChromium ug/L 10.0 U 10.0 U 10.0 U 29.9

1 pH of Water by Field Measurement

I pH SU 7.63 7.68 7.53 7.37

1 Temperature of Water by Field MeasurementTemperature Deg C 15.21 14.71 15.03 14.85

I I Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 8.15 8.87 8.35 8.65

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Page 264: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

ASR Number: 2775 RLAB Approved Sample Analysis Results 11/01/2005

Project ID: RS07GE Project Desc: Ace Service Inc. - LIRA GW samples

Analysis/ Analyte Units 94- 95-

1 Conductivity by Field MeasurementConductivity umhos/cm 1231 1389

1 Metals in Water by ICPChromium ug/L 10.0 U 17.2

1 pH of Water by Field MeasurementpH SU 6.90 6.74

1 Temperature of Water by Field MeasurementTemperature Deg C 17.78 16.97

1 Total Dissolved Oxygen in Water by Field MeasurementDissolved Oxygen mg/L 0.43 0.57

Page 30 of 30

Page 265: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

United States Environmental Protection AgencyRegion VII

901 N. 5th StreetKansas City, KS 66101

Date:

Subject: Data Disposition for ASR #: 2775

Project ID: RS07GE

Project Description: Ace Service Inc. - LIRA GW samples

From: Robert StewartSUPR/IANE

To: Dee SimmonsENSV/RLAB/CATS

I have received and reviewed the Transmittal of Sample Analysis Results for the above-referencedAnalytical Services Request(ASR) and have indicated my findings below by checking one of the boxes.

rj After reviewing the data, I have found that NO CHANGES ARE NECESSARY. Please change theASR status to 'RELEASED1 so that the electronic form of the data are available on the LAN inR7LIMS for my use. I realize that this will make these results available in read-only form to allRegion 7 employees and contractors that have R7LJMS 'Customer' account.

Q After reviewing the data, I have found that NO CHANGES ARE NECESSARY. Please change theASR status to 'PM Available' so that the electronic form of the data are available on the LAN inR7LIMS for my use only.

Q After reviewing the data, I have found that NO CHANGES ARE NECESSARY. Please DO NOTchange the ASR status to 'RELEASED' or 'PM Available' as THIS DATA IS OF A SENSITIVENATURE. I realize that this data will be archived on-line and any future reports or electronicdata dumps must be requested through the laboratory.

rj After reviewing the data, I have found that SOME CHANGES ARE NECESSARY. PLEASE MAKETHE CHANGES DETAILED IN THE ATTACHED LIST and re-transmit this data package. I realizethat if I wait more than 14 days after the date of the data transmittal the data may already bearchived and additional time may be required to make these changes.

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IIIIIIg Appendix H

Quarterly Audit Report No. 7

IAugust 2005

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Page 267: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIffIfIftf0

nIIIInllllIIllll

rftf

Prepared for:U.S. Environmental Protection AgencyRegion 790i" North 5th StreetKansas City. Kansas 66101

Long Term Response ActionAudit Report No. 7

Ace Services SiteColby, Kansas

August 26, 2005

EPA Contract No.: EP-S7-05-06EPA Task Order No.: 0075

BVSPC Project No.: 044720.01.49

Prepared by:FJ ?!:ACK £,Y^ATCH Black & Veatch Special Projects Corp.H> M hinldinn a uunrln nl riittpfpnrp'- ^ • r

6601 College Blvd.Overland Park. Kansas 66211

!_ building £ vyof|() ol ditleience

I N i R E l W«l [ f I N I O F M A 1 I O N G O V I R N M E M "

ProfessionalEnvironmental Engineers. Inc.

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Table of Contents

Table of Contents 1

1.0 Introduction .....1-1

2.0 Observations on General System Operation 2-1

2.7 Well Field 2-2

2.2 Treatment Plant 2-6

2.3 Resin Issues •. 2-77

3.0 Sampling and Record Keeping ;3-l

4.0 Eva luation of System Performance ; 4-1

5.0 Action Summary ;...5-l

IiIiiIIfIffiK. Figure 4-1 Gallons Treated vs. Chromium Concentration

I•E Appendix A - Resin information from US Filter

niiif

• Ace Services Site TC-1 44720.01.49Mm, LTRA Audit Repon No. 7

Tables

Table 4-1 Selected Flow and Chromium Concentration Data

Figures

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1.0 Introduction

As part of Work Order 0075, USEPA contract no. EP-S7-05-06, Black & Veatch

Special Projects Corp. (BVSPC) is to monitor key plant operations and evaluate the plant

operator's conformance to specified requirements for system operation at the Ace

Services Site, Ground Water Treatment Plant (GWTP) in Colby, Kansas. These

evaluations or audits are to occur on a quarterly basis. The audits include a site visit to

observe the City of Colby operators and obtain key plant operating data. This report

summarizes the findings from the seventh such audit conducted on July 19 through July

22, 2005. This report covers the period from April 27 through July 20, 2005. The results

of the first audit are summarized in the Lone. Term Response Action (LTRA) Audit Report^

No. ;, dated November 10, 2003. The results of the second audit are summarized in Long

Term Response Action Audit Report No. 2, dated March 19, 2004. The results of the third

audit are summarized in Long Term Response Action Audit Report No. 3, dated July 2,

2004. The results of the fourth audit are summarized in Long Term Response Action

Audit Report No. 4, dated November 19, 2004. The results of the fifth audit are

summarized in Long Term Response Action Audit Report No. 5, dated April 22, 2005.

The results of the sixth audit are summarized in Lone Term Response Action Audit Report

No. 6, dated June 24, 2005.

Ace Services Site M 044720.01.49LTRA Audit Report No. 7

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I 2.0 Observations on General System Operation

During the audit site visit (July 19 through July 22, 2005), BVSPC representatives

H arrived at the GWTP at around 7:00 A.M. each morning and did not leave the plant until

after 6:00 P.M. each evening. This allowed observation of the city operators throughout

I the regular staff hours.

The City staffing of the plant was unchanged from the last several audits. Mr. Jim

I Helus with the City of Colby Public Works Department is assigned as the full time

operator for the treatment system. Mr. Helus generally arrives at the treatment plant at

| 8:00 A.M. and spends the majority of the day tending to the plant and well field systems.

Mr. Helus is occasionally supplemented by other city staff on an as needed basis. A

I; second operator is often at the plant on Wednesdays to assist with the extra work

associated with collecting, preparing, and shipping the weekly sample splits for off-site

K laboratory analysis. Mr. Helus is responsible for system operation Monday through

^ Friday. Weekend staffing is provided by various other members of the Colby Public

E Works Department; however, Mr. Helus remains on-call for plant alarms seven days a

__ week.

B As noted in previous audits, the assignment of a single primary operator is

resulting in good follow-through on maintenance, supplies inventory, record keeping, and

H problem resolution.

mm The response to alarms during hours that the plant was not staffed was reasonably

H timely. The auto-dialer has been programmed to dial out all important alarms including

^^ tank level alarms. The auto dialer goes through a progression of phone numbers until a

•» response is obtained. Mr. Helus generally responds to all off-hours alarms.

_— The plant, office, storage, and lab areas were clean and very well organized.

II Organization of the office files and plant storage room is excellent. The operating staff

Hcontinues to express positive attitudes regarding the facility and their jobs. Mr. Helus

remains particularly well engaged in his position as plant operator and his skill levels

H regarding the more complex plant subsystems continue to improve. Mr. Helus, as well as

other plant staff, frequently call BVSPC for advice and assistance as needed.

IIAce Services Site 2-1 044720.01.49LIRA Audit Report No. 7

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Specific details of system operation, including problems noted during the audit,

are provided in the following sections of this report.

2.1 Well Field

As discussed in the previous audit reports, several of the extraction wells had been

shut down to prevent drawing 1,2-dichloroethane (1,2-DCA) from the Hi-Plains Co-op

plume into the ground water treatment system (GWTS). A new granular activated carbon

(GAC) treatment system installed by Kansas Department of Health and Environment

(KDHE) to remove the 1,2-DCA and other volatile organic compounds (VOC) from the

well water prior to entering the GWTP was started on August 24, 2004. Since that date

(including throughout the entire seventh audit period) all wells have been allowed to run

unless a particular well was shut down for some other reason unique to that well. There

had been numerous problems at various well locations that prevented several individual

wells from running during part or all of the fifth audit period. These are discussed in

detail in the fifth audit report. Repair and upgrade activities performed at the end of the

fifth audit period corrected all the problems in the well field and returned all wells to full

operation with the exception of wells EX-2s and EX-4s. Both of these wells were shut

down due to insufficient water level in the well. Well EX-2s has been shut down due to

lack of water since the very beginning of long term system operation and is being used as

a source of spare parts for other wells.

The entire well field was shut down on May 6, 2005 to allow the influent tank to

be drained and checked for excessive sediment buildup. No excessive buildup was noted.

The well filed was restarted later the same day.

A review of the groundwater sampling data from April 2005 showed a continuing

trend of increasing hexavalent chromium concentration in the Ace recovery well (ARW)

particularly in the shallow zone (A more complete discussion of this is provided in the

LTRA Cleanup Status report dated July 20, 2005). This area of increasing chromium

concentration is immediately up gradient from extraction wells EX-li and EX-ld. In

order to more quickly capture this contamination, the pumping rates were increased at

EX-li and Id on June 23, 2005 from 35 and 40 gpm to 60 and 70 gpm respectively. EX-

li was further increased to 70 gpm on July 21, 2005.

Ace Services Site 2-2 044720.01.49

LTRA Audit Report No. 7

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Individual well flows at the end of the seventh audit period were as follows:

Well

EX-li

EX-ld

EX-2s

EX-2i

EX-2d

EX-3s

EX-31

EX-3d

EX-4s

EX-4i

EX-5s

EX-5i

PWS-8

Total flow from

Design flow

35 gpm

40 gpm

25 gpm

1 00 gpm

1 00 gpm

25 gpm

50 gpm

75 gpm

25 gpm

100 gpm

25 gpm

1 00 gpm

125 gpm

the wells was 861

Actual flow

70 gpm

70 gpm

0 gpm (well off-low water)

86 gpm

100 gpm

20 gpm

50 gpm

75 gpm

0 gpm (well off-low water)

125 gpm

1 5 gpm

125 gpm

125 gpm

gallons per minute (gpm).

A review of sampling records shows that at the beginning of the sever

period, the hexavalent chromium concentration in the composite ground water entering

the GWTP was approximately 200 to 215 micrograms per liter (ug/L). This decreased

slightly to about 185 to 200 ug/L by the end of the seventh audit period.

Problems and anomalies noted regarding operation of the well field are described

below.

1. Well field power failure; Power was lost to wells EX-li, Id, 2i, 2d,

3s, 3i, 3d and PWS-8 mid evening on May 11, 2005. Power was

restored and the wells restarted to following morning at 7:35 am.

•I 2. Sticking lock at EX-ld well houses; The door lock at the EX-Id well

house has become difficult to operate and needs to be lubricated.

II

IIII

Ace Slices Site 2-3 044720.01.49LIRA Audit Repon No. 7

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3. Clean strainers in well houses. It is recommended that the piping

strainers in all the wells be blown-down and cleaned. This was listed as

Action Item number 7 in the sixth audit report.

4. Low flow condition at well EX-2i. Beginning on November 14, 2004,

the flow rate from well EX-2i dropped from 100 gpm to a little over 80

gpm. The well continued to flow only 80 to 85 gpm throughout the

remainder of the fifth, sixth and seventh audit periods even thought the

well flow controls were set to a 100 gpm set point. A complete

discussion of this issue is provided in the fifth audit report as item 4 of

section 2.1. It was originally decided to leave the pump in operation

flowing 80 to 85 gpm and replace it if it loses another stage or the flow

drops below 80 gpm. The level, probe at well EX-21 is now

malfunctioning (see item 5) and is scheduled for replacement. Since

replacing the probe involves pulling the pump out of the well, the pump

will be repaired or replaced when the level probe is replaced

5. Level probe malfunction at wells EX-2i, EX-2d and EX-5i; The well

level probe in well EX-2i began sending a false low signal causing the

well pump to shut down on June 17, 2005. The problem was

intermittent. Investigation revealed that the probe vent line had become

disconnected from the bellows allowing condensation to contaminate

the vent line. On July 1, 2005 the level probe began intermittent

malfunction at well EX-5i. The probes at well EX-2i and EX-5i are

scheduled to be replaced in August 2005. The level probe in well EX-

2d is showing a false low reading of approximately 66 feet however it

has held steady at this value and has not caused a low level alarm.

Replacement of the level probe at well EX-2d will not be scheduled

unless the problem worsens.

6. Various control problems at well EX-5i. During the seventh audit

period, several control related problems occurred on an intermittent

Ace Services Siie 2'4 044720.0].49LIRA Audi t Report No. 7

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basis at well EX-5i. The problems included erroneous flow meter

readings, failure of the flow control system to adequately modulate flow

from the well and communication system failures. The well pump was

operated in "hand" as needed to keep the well running. On July 19,

2005 the fiber optic system lost communication with the well

completely. A brief investigation on July 20 revealed that the fiber

optic interface card in the panel at the well house was faulty. The card

was replaced with a new one on hand in the spares inventory at the

GWTP. 100% communication was restored and all other control

functions resumed normal operation. No further problems were noted

at EX-Si.

" 7. Low water at well EX-5s. It was noted during the sixth audit that the

Mi water level at EX-5s was very low and the well was only able to sustain

™ . a pumping rate of 20 gpm. The water level at EX-5s when pumping at

•| 20 gpm was drawn down to only 6 feet above the pump. It was noted

. that this may ultimately result in pump failure from air entrained in the

B| water entering the pump as has happened at other shallow wells.

BVSPC recommended reducing the well flow from 20 gpm to 15 gpm.

9M This flow adjustment was made on July 19, 2005. At a flow rate of 15

gpm the well level was running at only 6.7 feet above the pump. It is

likely that this well will have to be shut down as has been done with

shallow wells EX-2s and EX-4s due to low water level in the well.

8. Improper valve setting at well PWS-8. During the field audit it was

_ noted that the isolation valve at well PWS-8 had been left fully opened.

mm This valve is to be left partially closed to help balance water flow and

——. allow the motor operated flow control valve to stay in a range that

•H provides good flow modulation. With the manual valve at full open the

Hautomatic flow control valve was modulated down to less than 20%

open which provides poor modulation and causes cavitation in the

valve. The manual valve was returned to the previously marked,

Ace Services Site 2-5 044720.01.49LTRA Audit Report No. 7

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partially closed position which allowed the automatic flow control

valve to return to approximately 60% open. Ideal modulation range for

the automatic flow control valves is 50% to 85% open

9. Excessive dust in the well houses. The well house ventilation systems

have no filters on the air intake. This is resulting in quick accumulation

of dust in the well houses particularly during dry, high wind conditions

that are typical in Colby during many months of the year. It is

important that dust levels in the well houses be kept low to protect the

fiber optic equipment in the control cabinets. BVSPC proposed adding

a filter just inside the intake louver on the well houses to alleviate this

problem. A standard 24" x 24" furnace filter could be easily

accommodated in this location. The City of Colby plant operators were

advised to solicit bids for this modification from a local HVAC

contractor.

] 0. Open pipe end at well EX-2s: Well EX-2s has been abandon due to

low water level. The end of the pipe which connects to the common

ground water collection piping system has been left open inside the well

house. This pipe end should be capped. This was listed in item 10 of

section 2.1 in the sixth audit report.

2.2 Treatment Plant

The treatment plant ran continuously throughout the seventh audit period with the

exception of brief shut downs May 25 to 27; 2005 due to problems with the resin as well

as on May 4. June 7 and June 28, 2005 to allow for resin replacement. There were no

shut downs due to equipment failures at the plant. The treatment system was operated at

full normal capacity of 800 gpm from the beginning of the seventh audit period through

June 23. 2005 when the flow was increased to 850+ gpm to accommodate increased flow

from wells EX-l i and EX-ld (see section 2.1 above). Table 4-1 provides a day-by-day

accounting of total plant flow throughout the seventh audit period.

Ace Services Silt 2-6 044720.01.49LIRA Aud i t Repon No. 7

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The new GAC system does not appear to have had any significant impact on the

GWTS with the exception of occasional clogging of the bag filters with carbon fines

(particularly when the GAC beds are backwashed) and elimination of hexavalent

chromium loading to the GWTP for several days when a fresh GAC bed is brought on

line. On May 6, 2005 the influent tank was drained to a level of about 18 inches and

inspected for excessive build-up of carbon fines or other material. The inspection

revealed no excessive accumulation of solids in the tanks bottom. It was noted that most

of the material in the tank heel was resin. This indicates that the backwash flow rate is

too high and needs to be reduced.

Two major incidents occurred at the plant during the seventh audit period both

involving the ion exchange resin. These two incidents occurred on May 25, 2005 and

July 20, 2005. Details of these incidents and all related issues are discussed in section 2.3

below.

Overall the GWTP treated approximately 90.4 million gallons during the audit

period averaging about 1.063,000 gallons per day (gpd).

Milestones for resin management activities were as follows.

TRAIN A:

April 27, 2005 - Beginning of seventh audit period. Bed Al is lead,

A2 is lag and standby bed A3 has exhausted resin (Train A has been in

this configuration since April 5, 2005).

- May 4. 2005 - Resin is replaced in Bed A3

- May 25, 2005 - Beds advanced to put Bed A2 lead and Bed A3 lag.

- May 27, 2005 - Beds reverted to Bed Al lead and A2 lag due to bad

resin in Bed A3 (see section 2.3 below).

June 7. 2005 - Resin is replaced in Bed A3.

June 7. 2005 - Beds advanced to put Bed A2 lead and Bed A3 lag.

June 28, 2005 - Resin is replaced in bed Al

- July 20, 2005 - Beds advanced to put Bed A3 lead and Bed Al lag.

Ace Services She 2-7 044720.01.49LIRA Audit Report No. 7

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July 20, 2005 - End of seventh audit period. Bed A3 is lead and Bed

Al is lag. Resin in bed A2 is exhausted. Plant is discharging to the

surface creek to rinse bed Al. This continued until July 22, 2005.

TRAIN B:

- April 27, 2005 - Beginning of seventh audit period, Bed Bl is lead, B2

is lag and standby bed B3 has exhausted resin (Train B has been in this

configuration since April 5, 2005).

May 3, 2005 - Resin is replaced in bed B3.

- May 25, 2005 - Beds advanced to put Bed B2 lead and Bed B3 lag.

- May 27, 2005 - Beds reverted to Bed Bl lead and B2 lag due to bad

resin in Bed B3 (see section 2.3 below).

- June 8. 2005-Resin is replaced in Bed B3.

- June 8, 2005 - Beds advanced to put Bed B2 lead and Bed B3 lag.

- June 28, 2005 - Resin is replaced in Bed Bl.

- July 20, 2005 - Beds advanced to put Bed B3 lead and Bed Bl lag

- July 20, 2005 - End of seventh audit period. Bed B3 is lead and Bed

Bl is lag. Resin in bed B2 is exhausted. Plant is discharging to the

surface creek to rinse bed Bl. This continued until July 22, 2005.

The status of the treatment system as of the end of the seventh audit period was

both trains operating at approximately 430 gpm with Beds A3 and B3 in lead and Beds

Al and B3 in lag service. Stand-by Beds A2 and B2 had exhausted resin. The water

quality from the discharge of Beds Al and Bl was not adequate for delivery to the City

of Colby drinking water system. The system effluent was diverted to the surface

discharge until July 22 when the resin in Beds Al and Bl rinsed out and the effluent pH

stabilized above 7.0. Details of the resin related problem encountered during the seventh

audit period are provided in section 2.3 of this report.

A few problems and anomalies were noted regarding plant operation during the

audit period. These are described below.

Ace Services Site 2-8 044720.01.49LTRA Audit Report No. 7

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1. Resin quality issues. There were two incidents during the seventh

audit period when the effluent water quality from a pair of lag beds that

had just been put on line was inadequate for use as drinking water. This

issue is discussed in detail in section 2.3 of this report.

2. Incomplete installation of piping modifications. During the sixth field

audit measurements were taken to design an alteration to the bed

discharge piping which would add a valve just upstream of the resin

trap. This would allow the trap to be isolated and pulled out for

cleaning in a matter of minutes. BVSPC completed the design of this

alteration and made arrangements for fabrication of the new piping

pieces. All the new piping pieces and hardware were shipped to the

GWTP. By the end of the seventh audit period the installation of the

modifications was complete on 4 out of 6 beds except that the bolt

isolation sleeves were not installed as they should have been.

H 3. Damaged conductivity meters and probes. As was noted in the fourth

audit report, the conductivity meters on both ion exchange trains were

H flashing error and out of range. As noted in the fifth audit report, it was

determined that the conductivity measurement probes were ruined

|PI because they had not been kept wet when the treatment trains are

drained. Plans were made to order new probes plus new hot tap probe

B mounts that will allow the probes to be pulled while the system is still

operating and under pressure. At the time of the sixth field audit, this

modification had not yet been done, primarily due to delays in acquiring

the new probes and equipment from Pedrotti Controls. By the end of

the seventh audit period, the new probes and pipe fittings had been

received at the GWTP but the equipment had not yet been installed.

This was action item 2 in the sixth audit report.

Ace Services Si.c 2-9 04.720.01.49LIRA Audil Report No. 7

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4. Mismatch of plant flow meter totalizers. During review of the

treatment plant flow records from the fifth and sixth audits was noted

that the monthly flow totals for the two treatment train influent flow

meters was approximately 500.000 to 700.000 gallons less than the total

of the well field flow meter (FM-1). This is also noted in the data from

the seventh audit. During the sixth field audit investigations showed no

leaking valves or other apparent causes for this discrepancy. During the

seventh audit further investigation revealed that the influent flow meter

for train B (FE-10201) was indicating a flow rate that was

approximately 20 gpm below the actual flow to the train. This was

verified by comparing the readings on this flow meter to the lead bed

flow meter, the lag bed flow meter and the train effluent flow meter.

All the flow meters matched with the exception of FE-10201. The 20

gpm differential would account for as much as a 860,000 gallon

monthly difference depending on how many hours the plant is operated

/ during a given month. Beginning with the month of August 2005

individual train flows will be recorded using data for the train effluent

flow meters FM-3A and FM-3B which were verified to be properly

calibrated.

Significant upgrades or changes in the treatment plant during the seventh audit

period included modification of four of the ion exchange beds discharge piping to

facilitate quick cleaning of the resin strainers. The other two will be modified during the

eighth audit period. The hot taps for the conductivity probes will also be installed during

the eight audit period.

Operator follow-through to address problems at the plant has been excellent. Ten

items were listed in section 2.2 of the sixth audit report. All items have either been

completely resolved or resolutions are in-progress.

Ace Services She 2-10 044720.01.49LIRA Audi! Report No. 7

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2.3 Resin Issues

Late in the afternoon of May 25, 2005 the ion exchange beds were advanced to

place standby beds A3 and B3 into lag service. Fresh Purolite A-300 resin had been

placed in these beds by US Filter on May 3 and 4, 2005. Early in the evening of May 25

the City of Colby public works department received complaints from residents of

"foamy" water. A quick investigation revealed that the water passing out of lag Beds A3

and B3 was effervescent and was at a pH of less than 6.0. The plant was immediately

shut off. A slight downward pH shift is normal when new beds are put on line as the

bicarbonate in the raw water reaches equilibrium on the resin. This shift has been seen

every time the beds have been advanced at the GWTP and it has always been limited to a

few tenths of a pH unit, returning to neutral in a day or two. The pH had never dropped

below the drinking water limit of 6.5 until beds A3 and B3 were placed on-line on May

25.

The manufacturing process for the ion exchange resin used at the GWTP involves

the use of very strong acids including hydrochloric acid (HCL) when placed in the

chloride form as is done for the GWTP. It was assumed that the resins in beds A3 and B3

were not adequately rinsed to remove all the acids. Subsequent testing conducted by US

Filter later confirmed this assumption (see Appendix A).

As noted above, the plant was shut off during the evening of May 25, 2005. US

Filter was contacted during the morning of May 26. 2005 and arrangements were made to

remove the resin from Beds A3 and B3 and replace it with new resin that had been tested

to assure it had been rinsed properly. After consultation with EPA and KDHE, the plant

was restarted on May 27. 2005 by reverting back to running Al and Bl as lead beds and

A2 and B2 as lag beds. Even though lead Beds Al and Bl were mostly expended and

were allowing hexavalent chromium breakthrough of approximately 60 ug/1 with an

influent concentration of approximately 200 ug/1, the beds were still removing about 70%

mm of the chromium. The relatively unloaded lag beds A2 and B2 easily removed the

™" remaining chromium. The system could be safely run this way for several weeks if

mm needed. Even though the risk of exceeding the required effluent standard for hexavalent

™ chromium was very slight, the discharge of the GWTP was directed to the surface rather

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IIAce Services Si.e 2-11 044720.01.49LIRA Audii Rcpon No. 7

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than to the city drinking water system until new resin could be placed in beds A3 and B3

and effluent quality verified.

US Filter performed a 16 hour soak test for pH and total organic concentration

(TOC) on all of the lots of Purolite A-300 in inventory following May 25. The data

indicated that there was considerable variability from lot to lot and that three lots had a

pH lower than 6.0 and the TOC varied from 34.5 mg/1 to as high as 446.5 mg/1 (see

Appendix A). This data suggests that the resin manufacturing process was producing

inconsistent results with some lots entirely unsuitable for a drinking water application

without further processing and/or rinsing.

US Filter filled two 600 cubic foot tanker loads of new Purolite resin after testing

each resin lot to assure acceptable quality. The fresh resin was trucked to the plant to

replace the unacceptable resin in beds A3 and B3 on June 7 and 8, 2005. The ion

exchange trains were advanced to put beds A2 and B2 in lead service with A3 and B3 in

lag service as soon as the new resin was put into the beds. There were no water quality

issues when the fresh resin beds were put in service on June 7 and 8, 2005 and discharge

to the city drinking water system was resumed.

Following this incident directors from US Filter met with BVSCP and EPA to

discuss new QC procedures to prevent a future occurrence of this problem as well as to

discuss a new resin service contract which included the option to supply Dow resin to the

GWTP in lieu of the Purolite product. US Filter's in-house testing of Dow SAR resin

indicated much less variability from lot to lot and much lower TOC values (see Appendix

A). The conclusions reached at the meeting were that each resin lot would be tested for

pH and TOC prior to shipment to the GWTP and that no resin lot with a pH below 6.5 or

a TOC level in excess of 40 mg/1 would be included in the shipment.

On June 28. 2005 the spent resins in beds Al and Bl were replaced with fresh

resin. Each lot that comprised these resin loads were to have been soak tested for pH and

TOC as agreed. When the beds were again advanced on July 20, 2005 to place the new

resin in beds Al and Bl into lag service a large pH swing to below 6.0 accompanied by

color throw and effervescence was once again observed in the water leaving the new lag

beds. The GWTP was diverted to surface discharge so that none of effervescent, low pH

water was placed into the city drinking water system. A quick investigation revealed that

Ace Services Siic 2-] 2 044720.01.49LIRA Audii Report No. 7

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US Filter had passed the lot-by-lot pH and TOC testing down to Purolite. US Filter had

• only done testing of a sample of the composite load. When US Filter's sampling

procedures were investigated it was clear that the sample collection method did not

• obtain a representative composite sample. The pH leaving bed Al was substantially

lower than the pH leaving bed Bl, once again demonstrating considerable lot to lot

• variability in the resin. The pH swing and effervescence were not as severe as the May

25 incident and it was believed that the new resin would rinse out fairly quickly.

• Consequently it was decided to leave the resin in service and continue to discharge to the

surface until the resin rinsed out and the pH returned to neutral. The pH climbed slowly

• over the following 36 hours finally reaching 7.0 on both trains by 5:00 am on July 22. At

that time the GWTP was switched back to city water discharge. Approximately 2 million

• gallons of groundwater was run through the two beds before neutral pH was reached.

As noted above, a new resin service contract is being negotiated. In order to

• assure the quality of future resin deliveries, the new contract will require a substantial

increase in lot by lot resin testing and analytical work prior to shipment to the GWTP.

I] This will include full 21 CFR 173.25 testing protocols in addition to in-house 16 hour

soak tests for pH and TOC. Negotiations for the new service contract were under way as

KJ of the end of the seventh audit period. In addition to the new resin QC requirements, new

procedures have been established at the GWTP to switch GWTP effluent to surface

K discharge prior to advancing resin beds and switch back to city discharge only after the

effluent quality has been verified.

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LTRA Audi! Repon No. 7

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3.0 Sampling and Record Keeping

As part of the audit, the in-plant records kept by the City operators were reviewed

for completeness and conformity to requirements. During the review, emphasis was

placed on water flow and chromium concentration data that are critical to evaluation of

treatment system performance. The daily records were well organized in notebooks kept

at the plant. The daily records were organized by month and date and were complete and

easy to access. The City operators have continued to enter the flow meter totalizer

readings and sample analysis results in Excel spreadsheets to facilitate trend tracking and

quick data retrieval. The sample record sheets include free chlorine results now that the

discharge to the city water system is active.

The operators have continued to fill out the new GAC system log sheet each day.

This new log sheet records critical flow and pressure data for the new GAC system.

The City operating staff has done an excellent job with the sampling and record

keeping requirements during the seventh audit period. The only significant irregularity

noted in the audit or subsequent review of records was that all of the flow data had been

entered into the spread sheets with the date shifted one day later so that, for example, the

zero flow condition on May 26, 2005 was recorded as zero flow on May 27, 2005.

Recommendations and/or improvements regarding plant sampling are as follows:

]. End-of-service laboratory' sample. BVSPC had previously advised the plant

operators that a sample is to be collected and sent for off-site laboratory

^_ analysis when a resin bed is taken out of service due to chromium

IB breakthrough to provide dependable end of service results. Recently, when

on-site sample results indicate that one of the lead resin beds show break

through, the operators have been leaving the bed in service until the following

Wednesday before removing the bed from service so the that the required end-

of-service sample can be taken as one of the regular weekly Wednesday lab

samples. This practice is acceptable so long as lead bed effluent hexavalent

chromium concentration does not exceed 60 ug/L. In the event that this level

is exceeded prior to the Wednesday lab sample collection, BVSPC

Ace Services She 3-1 044720.01.49LIRA Audi t Report No. 7

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recommends thai the bed be taken out of service and the confirmatory end-of-

service laboratory sample be collected as an additional sample at that time.

2. Sample transfer methods for on-site analysis. BVSPC has previously

recommended that the plant operators use pre-calibrated disposable pipettes or

pipettors to transfer the precise correct volume of sample from the large

sample collection jars to the small vials used for sample analysis in the

spectropholometers. The plant operators instituted this change in procedures

during the seventh audit period.

There were no other significant changes regarding plant sampling and record

keeping during the seventh audit period.

Ace Sen-ices Site 3-2 044720.01.49LIRA Audi t Report No. 7

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IIIIII1I

4.0 Evaluation of System Performance

The new GAC system constructed by KDHE was started on August 24, 2004

(during the fourth audit period). Data were again closely monitored during the seventh

audit period to determine if there were any significant impacts on the GWTS as a result

of the GAC system being on line. The only day-to-day impacts noted were the

occasional loading of carbon fines on the bag filters and the additional head pressure

required of the extraction pumps to push through the GAC beds. When a fresh GAC bed

is placed into service, the fresh GAC removes the majority of the hexavalent chromium

from the ground water for a period of several days.

The ability to capture and control the chromium plume in the ground water is

periodically assessed via sampling and ground water elevation measurement. These data

are analyzed and the findings summarized in semi-annual Cleanup Status Reports. The

most recent report (Cleanup Status Report Number 4, dated July 20, 2005) indicates that

the extraction wells are providing good plume containment and capture.

^ / Selected flow and sampling data from April 27, 2005, through July 20, 2005, are

presented in Table 4-1. Table 4-1 also shows the amount of hexavalent chromium

B removed by the treatment system. As shown in Table 4-1, the concentration of

hexavalent chromium in the raw water entering the treatment system during the seventh

jfi audit period began at about 200 ug/1 in late April and slowly dropped only slightly to

— about 190 ug/1 by late July.

0 The data show that the system treated 90.4 million gallons from April 27, 2005,

through July 20. 2005: 45.46 million gallons in Train A and 44.91 million gallons in

Train B. A total of 72.45 kilograms (kg) (159.73 pounds) of chromium were removed

^— during this period. Four beds of ion exchange resin (Beds Al. A2, Bl and B2) reached

!• exhaustion during this period as shown in Table 4-1. The resin performance for each of

__ the exhausted beds is shown below:

H_« Bed Al: 27.74 million gallons: 43.82 Ibs chromium: 36.14 gr/cf *

II Bed.Bl: 26.75 million gallons: 42.27 Ibs chromium: 34.86 gr/cf*

_- Bed A2: 30.13 mill ion gallons: 51.68 Ibs chromium: 42.62 gr/cf *

Ace Services Siic 4-] 044720.01.49LIRA Audi l Kcpon No. 7

II

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Bed B2: 30.11 million gallons: 53.58 Ibs chromium: 42.54 gr/cf *

* gr/cf = grams of chromium per cubic foot of resin

The relative performance data from the previous periods are shown below along

with the data for Beds Al, A2. Bl and B2 from this audit period. Data from the early

periods are shown as an average per 550 cubic foot bed of resin.

Time Period

Performance test:

First audit period:

Quantity of

Water Treated

20.5 million gal:

27.0 million gal:

Second audit period: 32.5 million gal:

Third Audit Period: 32.3 million gal:

Fourth Audit period:

Bed A3:

BedB2

BedB3

Fifth Audit period:

BedAl

BedBl

BedA2

BedB2

Sixth Audit Period:

Bed A3

BedB3

Seventh Audit Period:

BedAl 27.74 million gal

BedBl 26.75 million gal

BedA2 30.13 mill ion gal

BedB2 30.11 million gal

31.1 million gal:

31.1 million gal:

33.9 million gal

25.72 million gal

25.35 million gal

40.37 million gal

30.71 million gal

32.04 million gal:

35.08 million gal:

Chromium held

On resin

121.4 gr/cf*

93.6 gr/cf*

51.2 gr/cf*

41.9 gr/cf*

71.3 5 gr/cf*

34.28 gr/cf*

29.53 gr/cf*

75.1 gr/cf*

88.18 gr/cf*

90.81 gr/cf*

73.06 gr/cf*

57.67 gr/cf*

63.87 gr/cf*

36.14 gr/cf*

34.86 gr/cf*

42.62 gr/cf*

42.54 gr/cf*

* gr/cf = grams of chromium per cubic foot of resin

Ace Services SiteLIRA Audi! Report No. 7

4-2 044720.01.49

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The chromium holding capacity of the resin is expected to decrease with

diminishing influent bexavalent chromium concentrations due to the lower equilibrium.

This is clearly seen in the data above as well as in Figure 4-1. More gallons of water are

treated with the same 550 cubic feet of resin but at diminishing resin holding capacity.

During the entire period of time covered by the second and third audits, the wells

with the highest chromium concentrations were shut down awaiting design and

completion of the GAC system. During that time, chromium concentrations entering the

GWTP were averaging only around 120 to 150 ug/L. Once the GAC system was brought

on line in late August 2004 and all the extraction wells were restarted, the influent

chromium concentrations jumped up to as high a 7.00 ug/L and have been dropping

steadily since but the chromium concentration is still holding above the low levels seen in

the second and third audit periods. The affects of this can be seen in the higher grams per

cubic fool holding capacity of the resin late in the fourth audit period (Bed A3) and

throughout the fifth audit period. Chromium concentration in the influent ground water

continued to drop during the seventh audit period to around 190 ug/L by the end of the

period which is only a little higher than the very low levels seen during the second and

third audit periods and very similar to the concentration during the sixth audit period.

Note that the total gallons treated per bed during the sixth audit period are very similar to

the results during the second and third audit periods. The total gallons treated by each

bed during the seventh audit period are substantially lower than during second, third and

sixth periods, particularly Beds Al and Bl, even though the influent chromium

concentrations were similar. There is no apparent reason for this poor resin performance.

As noted in section 2.3 above, there have been some serious quality problems with the

resin supplied to the GWTP in recent months. This may be related to the poor resin

performance, however more study is needed.

As the hexavalent chromium concentration drops, a point is eventually reached

where the gallons treated by a given amount of resin will no longer increase. This is due

to the presence of other anions in the influent water that take up resin exchange capacity.

The data presented above as well as in Figure 4-L suggest that a 550 cubic foot volume

of resin cannot treat more than 31 to 34 mill ion gallons of Colby ground water regardless

<--,„ 4-3 044720.01.49Ace Services Site *t ->LIRA Audi t Rep°n No- 7

Page 288: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

of hexavalent chromium concentration. Bed A2 in the fifth audit period is an obvious

exception, treating over 40 million gallons at a fairly high chromium loading rate. A

possible explanation is that the bed was loaded with more than the usual 550 cubic feet of

resin. Each bed has a total volume of 1100 cubic feet and is intended to run only half full

of resin to allow plenty of head space for air bump and backwash operations. If 650 to

700 cubic feet of resin were loaded into the bed there would be no indication of the extra

resin except a slightly higher pressure drop through the bed. A review of the pressure

drop data during the time that Bed A2 was in lead position does in fact show a pressure

drop that is consistently 20% to 30% greater than the other bed in the same train. Based

on the data it is very likely that Bed A2 contained 650 to 700 cubic feet of resin during its

run in the fifth audit period. This data point is not included in Figure 4-1 since it is not

representative.

Figure 4-1 is a plot of gallons of water treated by an ion exchange bed vs. the

average chromium concentration of the water treated by the bed before significant

chromium breakthrough. This figure very clearly depicts the trends and limits noted

above. Beds Al and Bl from the seventh audit period do not fit the clear pattern

establish previously, but as noted above there were resin quality concerns that are likely

responsible for this offset. As seen in Figure 4-1, the gallons of water treated increases as

the chromium loading decreases in almost a linear relationship. However, once the

average chromium concentration in the GWTP influent water drops below about 300

ug/L, no more increase in the gallons treated per bed is seen. Every bed with an average

chromium influent concentration below 350 ug/L treated between 31 and 35 million

gallons of water (except during the seventh audit period during which resin quality

problems were encountered) with no correlation to chromium concentration. This can

now be used as planning tool for scheduling bed change-outs. Unless the influent

chromium concentrations again rise above 350 ug/1. each bed can be anticipated to treat

33 +/- 2 million gallons of water.

Ion exchange is often used as a polishing process in water treatment because it is

very cost efficient compared to other treatment technologies at low contaminant

concentrations. The relatively low concentration of hexavalent chromium seen in the

composite influent groundwater is an excellent application for ion exchange. The total

Ace Services Sue 4-4 044720.01.49LIRA Audii Repon No. '

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resin cost including transportation and disposal was 0.155 cents per gallon of water

treated for the seventh audit period. This is up from 0.130 cents per gallon from the sixth

audit period when the average chromium loading was essentially the same and it is

further evidence of the poor resin performance during the seventh audit period. This is

still a significant reduction from 0.210 cents per gallon from the performance test and

0.166 cents per gallon from the first audit period when average influent chromium

concentrations were higher. This diminishing cost as the chromium loading drops

demonstrates the efficiency of the ion exchange process in this application. Labor and

utility cost data are not available at this time to allow determination of the total cost per

gallon to treat the extracted ground water.

Ace Services Site 4-5 044720.01.49LIRA Audit Report No. 7

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Table 4-1Selected Flow and Chromium Concentration Data

Ace Services Site

Date

27-Apr-05282930

Hexavalent ChromiumAt sample location SC-1Henna unit

(ug/L)

Totals for month

ContinentalLabs (ug/L)

205205205205

TRAIN AGallonsTreatedx 1000

545610573559

1742

ChromiumRemoved

(kg)0.4230.4740.4450.4341.776

TRAINSGallonsTreatedxlOOO

526592556541

1689

ChromiumRemoved

(kg)0.4100.46004320.4201.721

RemarksA1 & B1 lead, A2 & B2 lag

Ace Services SilfLIRA Audi! Repon #~ 4-6 044720

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Table 4-1Selected Flow and Chromium Concentration Data

Ace Services Site .

Date

1-May-052345678910111213141516171819202122232425262728293031

Hexavalent ChromiumAt sample location SC-1Hanna unit

(UQ/L)

ii

Totals for month

ContinentalLabs (ug/L)

205205205202202202202202202202216216216216216216216212212212212212212212215215215215215215215

TRAIN AGallonsTreatedX1000

5885615635695915794985655955316195645685/956557155456757657358056353161251 1

0663581562577560

16534

ChromiumRemoved

(kg)0.4560.4360.4370.4350.4520.4430.3810.4320.4550.4060.5060.4610.4650.4740.4620.4670.4530.4550.4620.4600.4660.4520.4260.4910.420.0000.5400.4730.4580.470.45

13.65

TRAIN BGallonsTreatedxlOOO

57054554552257353548354857851459754655156054755553854856055556544515950

6556545554

1597

ChromiumRemoved

(kg)0.4430.4230.4230.3990.4380.4090.3690.4190.4420.3930.4880.447

• 0.4510.4580.4470.4540.4400.4400.4500.4460.4500.4370.4110.4770.4090.0000.5350.45E0.4430.45^0.441

13.19(

Remarks

Switched to A2 and B2 lead•

Reverted to A1 and B1 lead•

'

Ace Services SheLTRA Audit Report "7

4-7 014720

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Table 4-1Selected Flow and Chromium Concentration Data

Ace Services Site

Date

1-Jun-052345678910111213141516171819202122

2324252627282930

Hexsvalent ChromiumAt sample location SC-1Hanna unit

(ug/L)

Totals for month

ContinentalLabs (ug/L)

185185185185185185185208208208208208208208208208208208208208208185185185185185185185194194

TRAIN AGallonsTreatedx 1000

562581581547568612552584587560578588558548575556587582569580553518576578563576575535596606

1656S

ChromiumRemoved

(kg)0.3940.4070.4070.3830.3980.4290.3870.4600.4620.4410.4550.4630.4400.4320.4530.4380.4620.4580.4480.4570.4360.3630.4040.4050.3940.4040.4030.3750.4380.44

12.74

TRAIN BGallonsTreatedxlOOO

544562562529549592532565570541560569540555558539568563551561535502556559545555515458

1602

ChromiumRemoved

(kg)0.3810.3940.3940.3710.3850.4150.3730.4450.4490.4260.4410.4480.4250.4370.4400.4250.4470.440.43

• 0.440.420.350.390.390.380.390.390.360.390.43

12.32

Remarks

Switched to A2 and B2 lead

Ace Services Siie

LTRA Audit Report #7 4-8 044720

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IIIIIIIfffIIJn

Table 4-1Selected Flow and Chromium Concentration Data

Ace Services Site

Date

1-Jul-0523456789101112131415

. 1617181920

Hexavalent ChromiumAt sample location SC-1Hanna unit

(ug/L)185219212212190213219198180192153189201203193197204183195192

Tot.'ds for month

ContinentalLabs (ug/L)

TRAIN AGallonsTreatedX1000

588520514536554548443545634568583575536612578551568615558577

10615

ChromiumRemoved

(kg)0.4120.4310.4130.4300.3990.4420.3670.4090.4320.4130.3380.4120.4080.4700.4220.4110.4390.4260.4120.4208.306

TRAIN BGallonsTreatedxlOOO

571503497517534528572572627620632626580666629603620665604623

11218

ChromiumRemoved

(kg)0.4000.4170.3990.4150.3840.4260.4740.4290.4270.4510.3660.4480.4410.5120.4600.4500.4790.460.440.458.73

Remarks

switched to A3 and B3 lead

II

H

II

IIAce Services SiteLIRA Audit Report #7 4-9 044720

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Figure 4-1Gallons treated vs chromium concentration

40

~ 35 -

1 30O

= 25

co

20

15

=5 10O

5

0

0 200 400 600 800

Chromium (ug/L)

1000 1200

Page 4-10

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II

p

5.0 Action Summary

The following is a list of recommended actions or changes to improve system

• operation or record keeping procedures based on observations made during the seventh

audit. This is a summary list. This list also includes any needed equipment repairs or

• adjustments identified during this audit. Further details can be found in the body of this

audit report. It is noted that action items 2, 6 and 7 are carried over from the sixth audit

I report.

1. Lubricate the lock at well house EX-ld.

• 2. The conductivity probes on both trains need to be replaced and the meters

recalibrated.

I/ 3. Replace the level probes at wells EX-5i and EX-2i.

V /4. Repair or replace the pump at well EX-2i

V5. Cap the open pipe end at well EX-2s.

^ 6. Complete the installation of the new valves and piping spool pieces needed to

^ allow removal and cleaning of the resin trap without draining the vessel.

0 7. Clean out the piping strainers in all the well houses.

nIIIIIIII

8. Install filters in all the well house ventilation inlets as described in section 2.1,

item 9.

9. Switch to using flow meters FM-3A and FM-3B to record flow through each

treatment train as described in section 2.1, item 4.

Ace Services Si.e 5-1 044720.01.49LIRA Audi t Report No. 7

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IIIf

APPENDIX AP

RESIN INFORMATIONFROM US FILTER

HH

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11IIII

11

't=s S^TZS.E* 14950 HEATHROW FOREST PKWY SUITE 250= = =?^=^= HOUSTON TX 77032

A Siemens Business

June 8, 2005

Mr. Ken WyattBlack and Veatch6601 College BlvdOverland Park, KS 662 11

Subject: Purolite A-300E resin incident at Colby, KS Chrome removal site.

Dear Ken:

Enclosed are our findings in regards to the foamy water and low pH incident at the Colby, KS Chromeremoval site. As we discussed on the phone, we need to be more cautious in the future, and establishappropriate QA/QC expectations.

Attached is Purolite's findings and corrective action statement. We believe in addition to the improvedQA/QC work done by Purolite, USFilter will need to check the resin lots and verify the resin meets therequirements. We will require Purolite to provide Certificates of Analysis showing the pH and if requested

the TOO levels.

USFilter has performed some analytical testing of the Purolile resin lots that were in Rockford prior toloading them into the tankers for the replacement load. The results are enclosed. In addition, we haverequested their recommendations based on the data. They recommended USFilter to use all lots that testedabove 6.5 pH units. Based on the above, four lots were rejected for pH and one for being the wrongmaterial (macroporous anion). In addition, we performed composite TOC testing on each tanker weshipped this week..

You requested USFilter to investigate alternate sources of resin for this application. We have contactedDow Chemical for pricing on their MSF approved resin for this application (Dowex SAR). Since we usethis material for internal applications, we do have significant TOC data on this resin. We have included the

results in this report.

Thank you for your understanding in this matter, and your continued support of USFilter. We look forwardto establishing the proper QA/QC" requirements for this application, and continuing to support The City ofColby, the EPA and Black and Veatch.

Re

Robert LokenNorth American Sales DirectorAftermarket Business CenterService and Products Group

Enclosure: .

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1IIIIIIII

*HHHHliH

'—§='£1; ' 14650 HEATHROW FOREST PKWY SUITE 250HOUSTON TX 77032

A Siemens Business

Colby, KS PuroJite Resin Event:

Event:

On May 26, 2005, USFilter received a call from The City of Colby that they had received complaints froma few residents of foamy water coming from their taps. In addition the site was seeing pH 5.9 coming outof the new Purolite beds.

USFilfer Response:

We examined the remaining Purolite A-300E lots (19) for pH, resin type, foam and resin color. Some lotswere further examined for conductivity and TOC. We requested samples of the tanker retains from the siteand core samples of the resin in the vessels. Based on the initial test results., we also investigated applyingour standard cleaning procedures on the worst lot in the lab.

We contacted Purolite to initiate a root cause corrective action report. We shared our early findings withthem and requested replacement resin.

Testing Parameters:

Composite resin samples were taken from each Purolite resin Lot.

The pH testing was on a known amount of resin added to a clean beaker with a known amount of softenedwater. A stir bar was added and the water tested for pH. In addition, a few lots were tested on RockfordCity water and Brine. In addition, a few lots conductivity was tested.

Visual examination of the water and resin for foaming and resin color were also performed.

Total Oreanic Carbon (TOC) testing was performed on selected lots and the composite. The test procedureconsists of a known amount of resin placed in a clean glass sealed container with a known amount of Dlwater for 16 hours at 1 00°F. The water extract is tested for TOC level.

Results:

The results of our testing are summarized in table 1 of this report. As expected the resin lowered the pH asthe alkalinity absorption dispJaces the chJoride ion. This is typically. 0.5 pH units. Four lots were found tohave low pH values (2273/04/6, 2049/04/6, 2182/04/6, and 2279/04/6). One lot was determined to bemacroporous anion (46/04/6).

The tanker retain samples from Colby, lots AIW050422AI and A] W050225A1, results were 6.2 and 6.5respectfully. The vessel samples pH was 7.0 - 7.2.

The TOC results from the lowest pH lots were 253.7 ppm and 446.5 ppm. These values are much higherthan expected and they both had a color throw. We typically expect the TOC level to be below 100 ppm;

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=• = ~ "=1 ==" 1/!550 HEATHROW FOREST PKWY SUITE 250— — ~ HOUSTON TX 77032

A Siemens Business

and in electronics applications below 50 ppm for OH form Type 1 resins. Since Type II resin is less stablethan type 1, we see higher TOC levels in the OH form. Since the chloride form is significantly more stablethan the OH form, we would expect the results to be lower than the OH form for the same type of resin.The TOC results in table 2 indicate the Purolite resin is not as clean as the Dow based resin, and may needadditional cleaning.

Conclusion:

Purolite shipped resin to Rockford had not been properly rinsed for the application. The test resultsindicate residual HCL and organic manufacturing by-products were still in the resin. Purolite hasidentified a need on their end to analyze for these parameters instead of rinsing based on gallons throughput Purolite will need to supply improved resin lots and certification the resin meets the pH and otherestablished parameters.

Corrective Action:

Since QA/QC specification parameters had not been established for this application, Purolite nor USFiltertested the resin for pH or TOC contribution. Since this is a potable water application, proper precautionswill need to be implemented. .We believe the corrective action is to establish QA/QC parametersappropriate for the application. In addition, the resin will need to be tested by USFilter or an outside labfor verification.

/USFilter does not have GCMS instrumentation to perform complete NSF-61 testing, and is proposing pHand TOC parameters be used. We do not guarantee that these two tests will prevent another type of issue,but it will address the pH and foaming issue (residual organic manufacturing products). Please keep inmind that Purolite supplies 18-25 lots to make 1,200 CF of resin. If outside testing is required, the numberof lots will increase the costs of analytical testing. Black and Veatch and the EPA will need to establishthe appropriate testing parameters for this application.

Alternate resin or additional post manufacturing processing of the resin may be required, depending on theQA/QC requirements established by Black and Veatch and the EPA. USFilter will test the resin or processthe resin within the limits of our capabilities.

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iIiiiiif

i

Table 1

Colby Resin Issue

Lot Number

Soft Water

City Water

Brine

Retain Samples

287/04/6

2367/04/6

249/04/6

55/04/6

2051/04/6

2072/05/6

2340/04/6

2073/05/6

2117/04/6

2295/04/6

4753/04/6

46/04/6

229/04/6

2273/04/6

2049/04/6

2)82/04/6

2279/04/6

544/04/6

63/04/6

pH(soft

water)7.5n/an/a

6.76.5

6.86.5

6.66.96.97

7.17.17.27.2

7.)5

6.3S^

5.7

5.7

6.66.7

pH(ci ty

\vater)n/a

7.5n/a

6.76.5

6.86.6

PH(brine)

n/an/a5.9

6.77.6

7.96.7

Conduct iv i ty

(us)

589--

-*

--

-------

748967

769138]

785

738765

TOCmg/LC)

253.7

446.5

.

Resin

(type)

---

GG

GG

GGGGGGG

MP

GG

GG

G

GG

Foam

none

verylightsome

veryliehtsome

minor

some

some

minor

some

minor

some

rrunor

some

some

verylight

verylightrrunor

verylight

Other

Macroporousresin.Confirmedas aru'on.

Darkercoloredresin; colorthrow.Confirmedas anion.

Darkercoloredresin; colorthrow.Confirmedas anion.Sample wasre-tested forpH value.

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Colby ResinSamplesSoft Water

Train A

Train BA1W050422A1

A1W050225A1

Processed ResinSampleSoft Water2182.04.6

New Lot2051.04.64633.05.34619.05.3

New Resin TankersAIW050606A1A1W050603A1

7.4

7

7.26.2

6.5

7.57.2 138.6 '

4043.6

34.5

41.6108.3

some

some

foamy

light

Most foamof allsamples.Odor present

No colorthrow

//

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I

IIi1IIf

TOC Resin AnalysisTable 2

f

f

f

I

*

*

*0

A-244 (Dow Mfg.)15.8

1.36.96.6

10.83.67.9

C*y

7.33.9

- 4 .6

3.35.8

/ 7 R/ 7'6

5.25

4.57.7

42.61.93.9

5.693.18

AverageS Dev

AverageS Dev

Dow AveragDow S Dev

SAR

11.35.15.27.97.95.86.9

18.911.318.96.7

9.635.04

7.004.26

A-300E

4041.634.5

38.73.72

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I

I1IIIfif

I

*nHii

ION EXCHANGE RESINS

June 2, 2005

Robert LokenU.S. Filter4669 Shepherd TrailRockford,IL61105

Dear Mrr Loken,

We have investigated your complaint filed with Purolile's Terry Heller concerning thelow pH and foaming in A300E resin. A root cause analysis has found that the problem isrelated to the final rinsing steps employed in the manufacturing process.

The process requires rinsing with hot Dl water to a pH endpoint of 6.5 or greater. This isdone to remove residual organics and acids used in production of the resins. In reviewingthe process it was found that this target was routinely achieved within a certain volume ofwater. The procedure was thus changed to require only the set volume of water as therinse step. Unfortunately at some point the pH monitoring was discontinued.

The pH monitoring siep and limit has been reinstated.

In addition, all batches wil l be retested in Philadelphia prior to shipment to U.S. Filter forpH and foam residuals.

The material presently in your inventory that is over pH 6.5 should perform properly inservice.

We apologize for the problems caused by the process change. Please be assured that wewill take every step necessary to prevent this or similar problems in the future.

Regards,

Joe D'AlessandroTechnical ManagerPurolite USA

Cc: T. HellerD. BrodieA. Gotthardt

The P i i r o l i n - C u j u p i i n v . l > i i W - i n n l ' H n i - T i x l i ( . . 'nrporai ion. ISO M.nuimci i l Kosi l . IJala Cyimvd. 1 'A800-.V.VI50U <i l lMJl>S-J l i i . ' )H l-'ai f i](J-4W-M.v9 . - - 1 1 1 1 1 I I : jn l i i&'- imrol i i f l . 'SA. fom »i-h>ilr: www.nurnli i f lJSA.fom

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IIiiiig Appendix I

Quarterly Audit Report No. 8

I November 2005

I

iiiiiiiiIi

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iffiIiiiiiiiiiiii

Prepared for:U.S. Environmental Protection AgencyRegion 7901 North 5th StreetKansas City, Kansas 66101

Long Term Response ActionAudit Report No. 8

Ace Services SiteColby, Kansas

November 18, 2005

EPA Contract No.: EP-S7-05-06EPA Task .Order No.: 0075

BVSPC Project No.: 044725.01.49

Prepared by:Fl PkACK ?!,YIATCH Black & Veatch Special Projects Corp.^_4 bmldmo a iMnrmof difference™ r J f

6601 College Blvd.Overland Park. Kansas 66211

|_ building a Qf|(J of difference'

E N E R G Y W A T E R I N F O R M A T I O N G O V E R N M E N T

ProfessionalEnvironmental Engineers. Inc.

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Table of Contents

1.0 Introduction 1-1

2.0 Observations on General System Operation 2-1

2.1 Well Field 2-2

2.2 Treatment Plant , 2-6

2.3 Resin Issues 2-75

3.0 Sampling and Record Keeping 3-1

4.0 . Evaluation of System Performance 4-1

5.0 Action Summary 5-1

tf

*iifriiiii_ Figures

I Figure 4-1 Gallons Treated vs. Chromium Concentration

I£ Appendix A - Resin pH Run-in Charts

I

1

I

i

I

Tables

Table 4-1 Selected Flow and Chromium Concentration Data

Ace Services Sile TC-1 044720.01.49LIRA Audit Report No. 8

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0

f

I

f

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

1.0 Introduction

As part of Work Order 0075, USEPA Contract no. EP-S7-05-06, Black & Veatch

Special Projects Corp. (BVSPC) is to monitor key plant operations and evaluate the plant

operator's conformance to specified requirements for system operation at the Ace

Services Site, Ground Water Treatment Plant (GWTP) in Colby, Kansas. These

evaluations or audits are to occur on a quarterly basis. The audits include a site visit to

observe the City of Colby operators and obtain key plant operating data/This report

summarizes the findings from the eighth such audit conducted on October 11 through

October 14, 2005. This report covers the period from July 21 through October 12, 2005.

The results of the first audit are summarized in the Long Term Response Action Audit

Report No. 1, dated November 10, 2003. The results of the second audit are summarized

in Long Term Response Action Audit Report No. 2, dated March 19, 2004. The results of

the third audit are summarized in Long Term Response Ad ion Audit Report No. 3. dated

July 2, 2004. The results of the fourth audjt are summarized in Long Term Response

Action Audit Report No. 4, dated November 19, 2004. The results of the fifth audit are

summarized in Long Term Response Action Audit Report No. 5, dated April 22, 2005.

The results of the Sixth audit are summarized in Long Term Response Action Audit

Report No. 6, dated June 24, 2005. The results of the seventh audit are summarized in

Lonz Term Response Action Audit Report No. 7, dated August 26, 2005.

Ace Services Site 1-1 044720.01.49LTRA Audit Report No. 8

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IIIIIIIIIIIIIIIIIII

2.0 Observations on General System Operation

During the audit site visit (October 11 through October 14, 2005), BVSPC

representatives arrived at the GWTP at around 7:00 A.M. each morning and did not leave

the plant until between 5:00 and 6:00 P.M. each evening. This allowed observation of the

city operators throughout the regular staff hours.

The City staffing of the plant was unchanged from the last several audits. Mr. Jim

Helus with the City of Colby Public Works Department is assigned as the full time

operator for the treatment system. Mr. Helus generally arrives at the treatment plant at

8:00 A.M. and spends the majority of the day tending to the plant and well field systems.

Mr. Helus is occasionally supplemented by other city staff on an as needed basis. A

second operator is often at the plant on Wednesdays to assist with the extra work

associated with collecting, preparing, and shipping the weekly sample splits for off-site

laboratory analysis. Mr. Helus is responsible for system operation Monday through

Friday. Weekend staffing is provided by various other members of the Colby Public

Works Department; however, Mr. Helus remains on-call for plant alarms seven days a

week.

As noted in previous audits, the assignment of a single primary operator is

resulting in good follow-through on maintenance, supplies inventory, record keeping, and

problem resolution.

The response to alarms during hours that the plant was not staffed was reasonably

timely. The auto-dialer has been programmed to dial out all important alarms including

tank level alarms. The auto dialer goes through a progression of phone numbers until a

response is obtained. Mr. Helus generally responds to all off-hours alarms.

The plant, office, storage, and lab areas were clean and very well organized.

Organization of the office files and plant storage room is excellent. The operating staff

continues to express positive attitudes regarding the facility and their jobs. Mr. Helus

remains particularly well engaged in his job as plant operator and his skill levels

regarding the more complex plant subsystems continue to improve. Mr. Helus, as well as

other plant staff, frequently call BVSPC for advice and assistance as needed.

Ace Services Site 2-1 044720.01.49LIRA Audit Report No. 8

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IIIIIIIiiiiiiiiiiii

Specific details of system operation, including problems noted during the audit,

are provided in the following sections of this report.

2.1 Well Field

As discussed in the previous audit reports, several of the extraction wells had been

shut down to prevent drawing ] ,2-dichloroethane (1,2-DCA) from the Hi-Plains Co-op

plume into the ground water treatment system (GWTS). A new granular activated carbon

(GAC) treatment system installed by Kansas Department of Health and Environment

(KDHE) to remove the 1,2-DCA and other volatile organic compounds (VOC) from the

well water prior to entering the GWTP was started on August 24, 2004. Since that date

(including throughout the entire eighth audit period) all wells have been allowed to run

unless a particular well was shut down for some other reason unique to that well.

Wells EX-li and EX-3d were shut off and the flow from wells EX-Id and PWS-8

were significantly reduced for several days early in September 2005. This was done to

temporarily reduce the hexavalem chromium concentration in the raw water entering the

GWTP to extend the run time of beds A3 and B3 until September 14 to support resin tests

scheduled for the week of September 14, 2005. See section 2.3 of this report for details

of the resin testing.

There had been numerous problems at various well locations that prevented

several individual wells from running during part or all of the previous (fifth) audit

period. These are discussed in detail in the fifth audit report. Repair and upgrade

activities performed at the end of the fifth audit period corrected all the problems in the

well field and returned all wells to full operation with the exception of wells EX-2s and

EX-4s. Both of these wells were shut down due to insufficient water level in the well.

Well EX-2s has been shut down due to lack of water since the very beginning of long

term system operation and is being used as a source of spare parts for other wells.

Water level probes failed at wells EX-2i, EX-4i and EX-5i during the eighth audit

period, however these wells were kept operating in manual mode. The flow rates at wells

Ex-li and EX-Id were increased during the seventh audit period in response to rapidly

rising hexavalent chromium concentrations in the nearby Ace Recovery Well. No flow

rate adjustments were made during the eighth audi t period with the exception of well EX-

Ace Services Site 2-2 044720.01.49LTRA Audit Report No. 8

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fffff1IIIIIIIIIIIII

2d being returned to it's design pumping rate of 100 gpm following repair of the well

pump. Individual well flows at the end of the eighth audit period were as follows:

Well

EX-li

EX- Id

EX-2s

EX-2i

EX-2d

EX-3s

EX-3i

EX-3d

EX-4s

EX-4i

EX-5s

EX-5i

PWS-8

Design flow

35 gpm

40 gpm

25 gpm

100 gpm

100 gpm

25 gpm

50 gpm

75 gpm

25 gpm

1 00 gpm

25 gpm

1 00 gpm

125 gpm

Actual flow

70 gpm

70 gpm

0 gpm (well

100 gpm

1 00 gpm

20 gpm

50 gpm

75 gpm

0 gpm (well

125 gpm

15 gpm

125 gpm

125 gpm

off-low water)

off-low water)

Total flow from the wells was 875 gallons per minute (gpm). Note that this is the

highest total pumping rate since the plant began operation.

A review of sampling records shows that at the beginning of the eighth audit

period, the hexavalent chromium concentration in the composite ground water entering

the GWTP was approximately 210 to 220 micrograms per liter (ug/L). This decreased

slightly too about 185 ug/L by the end of the eighth audit period.

It has been noted that the chromium concentrations in wells EX-4i, EX-5i and

EX-5s are below the Clean-up goal of 100 ug/L. The results of samples collected from

these wells in April 2005 ranged from less than 15 ug/L up to 43 ug/L. Field analysis

conducted in the lab at the GWTP during the eighth field audit of samples from these

three wells yielded very similar results. Wells EX-4i and EX-5i have been pumping at

125 gpm, which is over the design pumping rate of 100 gpm since the western wells were

temporarily shut down due to possible DCA contamination in October of 2003. As has

been noted in several previous audit reports, the influent concentration of hexavalent

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chromium entering the GWTP has dropped so low that resin life is a direct function of

water flow. BVSPC has proposed to EPA that a surge pumping technique be considered

for wells EX-4i, EX-5i and EX-5s to reduce total water flow to the plant and extend the

resin life.

Problems and anomalies noted regarding operation of the well field are described

below.

1. Low flow condition at well EX-2i. Beginning on November 14, 2004,

the flow rate from well EX-2i dropped from 100 gpm to a little over 80

gpm. The well continued to flow only 80 to 85 gpm throughout the

remainder of the fifth, sixth and seventh audit periods even thought the

well flow controls were set to a 100 gpm set point. A complete

discussion of this issue is provided in the fifth audit report as item 4 of

section 2.1. It was decided to leave the pump in operation flowing 80 to

85 gpm and replace it if it loses another stage or the flow droped below

80 gpm. The malfunctioning level probe at well EX-2i was replaced on

August 23, 2005. Since this work required pulling out the well pump, a

new pump was installed at that time. The new pump is operating as

expected and the well has pumped at the 100 gpm design rate since the

new pump was installed. Replacement of this pump was listed as

Action Item 4 in the seventh audit report.

2. Low water at well EX-5s. It was noted during the sixth audit that the

water level at EX-5s was very low and the well could no longer sustain

the design flow rate of 25 gpm. The flow from well EX-5s was reduced

to 20 gpm during the sixth audit period and then further reduced to 15

gpm at the end of the seventh audit period. It was noted during the

eighth filed audit that the water level at EX-5s when pumping at only

15 gpm is drawn down to only 5 feet above the pump. This may

ultimately result in pump failure from air entrained in the water entering

the pump as has happened at other shallow wells. BVSPC recommends

that the well pump be shut off as has been done at wells EX-4s and 2s

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until the water level rises enough to allow pumping without

endangering the pump. The existing pump in well EX-5s cannot be

turned down much below 15 gpm without damaging the pump motor.

The semi-annual ground water evaluation will assess the effect of the

lower flow rate on plume capture.

3. Level probe malfunctions at wells EX-2i. EX-2d. EX-4i and EX-5i:

The level probes at wells EX-2i and EX-5i began malfunctioning during

the seventh audit period and were replaced during the eighth audit

period on August 23, 2005. The level probe at well EX-4i failed on

August 17, 2005. A replacement probe was ordered and installation is

scheduled for late October, 2005. The level probe at well EX-2'd has

been showing a false low reading of about 66 feet for several audit

periods however it has held steady and has not caused a pump

shutdown. Replacement of the level probe at well EX-2d will not be

scheduled until the problem worsens. Note that replacement of the

level probes at wells EX-2i and EX-5i was listed as Action Item 3 in the

seventh audit report.

4. Excessive dust in the well houses: As was noted in the seventh audit

report, the lack of filtration for the well house ventilation intakes is

allowing excessive dust to enter the well house during dry windy

weather (which is quite common in Colby, KS). The excessive dust is a

threat to the fiber optic equipment in the well house panels. In the

seventh audit report, BVSPC recommended that the intake louver skirts

be modified by a local HVAC contractor to accommodate a standard

24" x 24" furnace filter between the louver and isolation damper. A bid

was solicited from McKee Inc. for this work. The bid price was $125

per well house. McKee is scheduled to begin this work on October 12,.

2005. This was listed as Action item 8 in the seventh audit report.

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I1I 2.2 Treatment Plant

• The treatment plant ran continuously throughout the eighth audit period. The

™ treatment system was operated at full normal capacity of 800 + gpm throughout the sixth

• audit period. Table 4-1 provides a day-by-day accounting of total plant flow throughout

™ the eighth audit period.

• The new GAC system does not appear to have had any significant impact on the

GWTS with the exception of occasional clogging of the bag filters with carbon fines

• (particularly when the GAC beds are backwashed) and elimination of the hexavalent

chromium loading to the GWTP for several days when a fresh GAC bed is brought on

line. There were no fresh GAC beds brought on-line during the eighth audit period.

There were two major upsets during the previous (seventh) audit period involving

the ion exchange resin. These events are detailed in section 2.3 of the seventh audit

report. Several investigations and filed trials were conducted during the eighth audit

period to determine a permanent resolution to the resin issues. These results of these

investigations are presented in section 2.3 of this eighth audit report.

The only serious event during the eighth audit period was the appearance of a

significant water hammer when the city water transfer pumps shut off. This problem is

described in detail below.

Overall the GWTP treated approximately 101.5 million gallons during the eighth

audit period averaging about 1,208,000 gallons per day (gpd).

Milestones for resin management activities were as follows.

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TRAIN A;

- July 21, 2005 - Beginning of eighth audit period. Bed A3 is lead, Al

is lag (Train A was just placed in this configuration the previous day -

July 20, 2005).

- August 16, 2005 - Resin is replaced in Bed A2 (note: Purolite A300

resin, cycled and placed 60% in bicarbonate form).

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September 14, 2005 - Beds advanced to put Bed Al lead and Bed A2

lag. (Note: This bed advancement should have occurred on

September 7, 2005 when hexavalent chromium breakthrough reach 60

ug/L, however it was delayed one week to allow for testing)

September 22, 2005 - Resin is replaced in Bed A3 (Note: Dow SAR

resin, untreated).

October 12, 2005 - End of sixth eighth period. Bed Al is lead and

Bed A2 is lag. Resin in bed A3 is fresh, untreated Dow SAR.

TRAIN B:

July 21, 2005 - Beginning of eighth audit period, Bed B3 is lead, Bl is

lag (Train B was just placed in this configuration the previous day -

July 20, 2005).

- August 15, 2005 - Resin is replaced in bed B2 (note: Purolite A300

resin, cycled and placed 60% in bicarbonate form).

- September 14, 2005 - Beds advanced to put Bed Bl lead and Bed B2

lag. (Note: This bed advancement should have occurred on September

7, 2005 when hexavalent chromium breakthrough reach 60 ug/L,

however it was delayed one week to allow for testing)

- September 22, 2005: _ Resin is replaced in Bed B3 (Note: Dow SAR

resin, placed 40% in bicarbonate form).

- October 12, 2005 - End of sixth eighth audit period. Bed Bl is lead

and Bed B2 is lag. Resin in bed B3 is fresh Dow SAR, 35%

bicarbonate.

The status of the treatment system as of the end of the eighth audit period was

both trains operating at approximately 440 gpm with Beds Al and Bl in lead and Beds

A2 and B2 in lag service. Stand-by Beds A3 and B3 had fresh resin. As noted in the

seventh audit report, the resin service contract with US Filter (USF) has been renewed

and required a switch from Purolite A300 to Dow SAR resin. The resin in beds A3 and

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B3 are the first loads of Dow SAR resin to be delivered to the plant under the new

contract. Bed A3 was loaded with pure, untreated Dow SAR however bed B3 was loaded

with Dow SAR that had been partially converted from the chloride to the bicarbonate

form. This was done as the last in a series of experiments regarding the pH of the

effluent water when a fresh resin bed is first placed into service. Further details are

provided in section 2.3 of this report.

A few problems and anomalies were noted regarding plant operation during the

audit period. These are described below.

1. Resin quality issues. There were two incidents when the effluent water

quality from lag beds that had just been placed in service was not

suitable for use as drinking water due to low pH excursions and organic

contaminants. One incident occurred on May 25, 2005 during the

seventh audit period and the other occurred on July 20, 2005 just at the

beginning of the eight audit period. Details regarding these incidents

including resolutions for this problem are provided in section 2.3 of the

seventh audit report as well as section 2.3 of this eighth audit report.

2. Low backwash flow rate. The plant operators had noted that the

backwash flow rate had dropped below 200 gpm. The rate had been

well over 300 gpm in the past. BVSPC recommended changing the bag

elements in the backwash filter. It then became apparent that the plant

operators were not aware thai there was a backwash filter provided in

the plant. A quick inspection reveled that the bag elements were badly

clogged. This was not surprising considering that these filter bags had

never been changed in the life of the plant. BVSPC instructed the plant

operators on how to change the backwash filter bags and pointed out

that this unit uses the same filter bag as the plant influent feed bag

filters. Changing the filter bags corrected the low flow condition.

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3. Incomplete installation of piping modifications. During the sixth field

audit measurements were taken by BVSPC to design an alteration of

each ion exchange vessels discharge piping. The design allowed for the

installation of an isolation valve just upstream of the resin traps that

would allow removal of the traps for cleaning without draining the

entire vessel. By the end of the seventh audit period, 4 of the 6 resin

vessels had been altered and all the parts were on hand to finish the

installation. By the end of the eighth audit period, all six valve sets had

been installed however installation of the bolt isolation sleeves was not

complete. Experience with the new arraignment has been very positive.

Prior.to this modification, cleaning a resin trap required a full day.

With the modification in place, this activity requires less than 30

minutes.

4. Damaged conductivity meters and probes. As was noted in the fourth

audit report, the conductivity meters on both ion exchange trains were

flashing error and out of range. As noted in the fifth audit report, it was

determined that the conductivity measurement probes were ruined

because they had not been kept wet when the treatment trains are

drained. Plans were made to order new probes plus new hot tap probe

mounts that will allow the probes to be pulled while the system is still

operating and under pressure. At the time of the sixth field audit, this

modification had not yet been done, primarily due to delays in acquiring

the new probes and equipment from Pedrotti Controls. By the end of

the seventh audit period, the new probes and pipe fittings had been

received at the plant but not yet installed. As of the end of the eighth

audit period, the installation had still not been done. This was listed as

action item 2 in the fifth, sixth and seventh audit reports.

5. Mismatch of plant flow meter totalizers. During review of the

treatment plant flow records from the fifth, sixth and seventh audits it

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was noted that the monthly flow totals for the two treatment train

influent flow meters was approximately 500,000 to 700,000 gallons less

than the total of the well field flow meter (FM-1). This is also noted in

the data from the eighth audit. As described in the seventh audit report

an investigation conducted during the seventh field audit revealed that

the influent flow meter for train B (FE-10201) was indicating a flow

that was approximately 20 gpm below the actual flow. Beginning with

the month of August 2005 the plant operators were instructed to record

individual train flows using the train effluent meters FM-3A and FM-

3B which had been verified to be properly calibrated. A review of the

flow data since August of 2005 shows that using the readings from FM-

3A and 3B has eliminated the discrepancy. The data from the eighth

audit period shows less than a 0.1% variance.

6. New procedures for resin management. No representative of BVSPC

has ever been present at the GWTP when new resin has been delivered

to the plant. During recent discussions with plant and US Filter

personnel it came to light that when the fresh ion exchange resin is first

transferred into the process vessels, the USF and plant operators were

performing a very brief and inadequate backwash. The plant operators

were then performing a more extensive backwash as the resin is brought

on line several weeks later. This is not the correct procedure. A

complete backwash should be conducted when the new resin is first

placed in the process vessel to remove the resin fines created during

transportation and sluicing of the resin. When the resin is placed on-

line later, only rinse and recycle steps are needed. The plant operators

were not performing complete backwash as new resin was first loaded

primarily because they were not aware that the backwash step can be

conducted on the standby bed with the process train in full operation.

They had thought that the process train had to be shut down and they

were trying to minimize the downtime. This misunderstanding has

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been cleared up and the correct resin management procedures are now

being followed. The correct procedure is as follows: 1) When the resin

is first transferred into the standby process bed, a full 9000 gallon

backwash should be conducted followed by a minimum of 15 minutes

settling time and then a 9000 gallon rinse. 2) When the resin is later

placed on-line, the operators should conduct a 9000 gallon rinse

followed by a 9000 gallon recycle and then into lead service. No

backwash is required.

7. Water hammer and related damage to chlorine loop. Mid-evening on

October 11, 2005 the city water transfer pump TWP-1 started and then

abruptly stopped. When the pump stopped a water hammer of extreme

intensity occurred in the city water discharge system. The pressure

wave from the water hammer was so strong that it traveled out into the

city water distribution system and reflected back to the plant and then

back out to the distribution system then once again back to the plant

making three full cycles before it dissipated. The BVSPC site manager

happened to be at the GWTP when this occurred. The energy of the

. pressure wave significantly displaced the large 8" and 10" welded steel

piping that makes up the city water discharge system and was sufficient

to literally shake the; building. A brief investigation into the cause of

the hammer revealed that the city water tower had reach "full" level just

as the transfer pump had spooled up to full speed. When the water

tower reaches full, the city control system removes the "city requests

water" command from the GWTP PLC thereby shutting down the

pump. There is a speed controlled isolation valve (CV-6) on the city

water discharge from the GWTP that is set to close slowly when the

pump shutdown command is given. The PLC is programmed to delay

the pump shut down for several seconds to allow this speed controlled

isolation valve to reach near full closed thereby significantly reducing

the flow rale before the pump shuts off. The express purpose of this

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control sequence is to assure there are no abrupt large changes in flow

which could produce a water hammer. The isolation valve is also

speed controlled on opening to prevent sudden increase in flow rate to

the city system. The only plausible explanation thus far identified for

the extreme water hammer is that the valve was still completing the

opening cycle when the request for water was suddenly taken away. By

the time the valve could complete venting the opening side of the

actuator, reverse direction and close, the time delay on pump shut down

had elapsed and the pump shut off with the valve still significantly

open. It should be noted that each of the transfer pumps is provided

with a triple duty discharge valve that operates as a non-slam check

valve. When the transfer pump shut down that evening, the triple duty

valve slammed closed and bounced off its seat several times. The triple

duty valves are equipped with a spring behind the sealing disk which is

intended to prevent exactly this kind of bounce. It is not clear weather

the non-slam, non-bounce features of the triple duty valve failed or if

(he force of the wafer hammer was simply too great to be resisted even

by a properly functioning valve. It should be noted that even if all the

events occurred as proposed above the force of the water hammer

experienced that evening was still far in excess of what would be

expected even in the worst of circumstances. In fact during the original

GWTP system lesling conducted in the summer of 2003, the transfer

pumps were stopped.numerous time with the isolation valve full open

and the resulting water hammer was much less intense and never had

enough energy to reflect out through the distribution and return. The

City of Colby has added a new production well that pumps into the

same main as the GWTP. This may be contributing to the problem

since the velocity in this main has increased but it would not account

for the intensity of the shock that occurred on October 11, 2005. On

October 12, 2005 the transfer pumps were cycled again and a water

hammer resulted although of much less intensity than the evening

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0before. The pumps were cycled several more times to allow for

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refining the isolation valve speed control and pump shut down sequence

in an effort to minimize the water hammer. The intensity of the water

hammer was reduced significantly (to a soft bump) but it could not be

eliminated completely. When the city discharge system was finally put

back on-line there would occasionally be a somewhat more intense

hammer even though nothing was changed at the GWTP The severe

intensity of the water hammer which occurred on October 11, 2005

damaged several elements of the chlorine booster loop which have

subsequently failed including the following:

- Chlorine Ejector. The Chlorine, ejector is made from PCV. The

ejector body cracked when the water hammer hit creating a slow water

leak through the crack. The water in the chlorine loop is chlorinated to

a fairly high concentration as it passes through the ejector. The leak

was sufficient to cause the chlorine alarm in the chlorine shed to trip,

however the water is not sufficiently chlorinated to produce a

dangerous atmosphere. The A new chlorine ejector was ordered on

October 12, and was received and installed on October 13 allowing the

city water discharge to resume operating.

Ball valve union nut. The day after the intense water hammer

occurred while the transfer pumps were being cycled for testing, A

union nut on the PVC true-union style 2" ball valve in the chlorine

booster loop broke completely apart resulting in a 2" opening in the

system spraying water with full city water pressure behind it. The

loop was isolated to stop the flow. A new valve was ordered which

was received and installed by October 14, 2005. It is assumed that the

union nut was damaged in the very intense water hammer event the

evening prior but didn't fail until the next day.

- Fitting in buried pipe of chlorine loop. On October 27, 2005 a fitting

in the below ground portion of the chJorine Joop failed. Once again h

is assumed that the buried fitting was initially damaged in the incident

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on October 11, 2005. The location of this pipe failure is not

accessible. It was decided to reroute the chlorine loop entirely inside

the GWTP. This will relocate the chlorine ejector from the chlorine

shed to inside the GWTP. This is acceptable because the chlorine gas

feed line to the ejector requires vacuum created by the ejector to flow

any chlorine. All the pressurized elements of the chlorine loop will

remain out in the chlorine shed. The relocation of the ejector to inside

the plant was approved by KDHE BOW.

The chlorine loop is the weak spot in the GWTP city water discharge

system. The loop is Schedule 80 CPVC to provide resistance to high

concentrations of chlorine. The other elements of the piping system

are welded steel and butt fusion welded SDR 11 HOPE and are much

less prone to failure from a pressure surge. Following the third failure

of a chlorine loop element on October 27, 2005 consideration was

given to adding a surge arrester in the loop to protect this weak point.

At the time of writing of this eighth audit report, EPA is considering

this proposal. Estimated cost is approximately $15,000.

Significant changes or upgrades to the treatment plant during the eighth audit

period included modification of the last two ion exchange beds discharge piping to

facilitate quick cleaning of the resin strainers. A switch was made to Dow SAR ion

exchange resin during the eighth audit period to hopefully improve resin performance and

reduce problems as new resin is brought on line. Further discussion is provided in

Section 2.3. Upgrades planned for the ninth audit period include modification of the

chlorine loop and addition of hot taps for the conductivity probes.

Operator follow-through to address problems at the plant has been excellent.

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2.3 Resin Issues

Section 2.3 of the seventh audit report summarized two significant water quality

incidents related to poor resin quality. The first incident occurred on May 25, 2005 as

standby beds A3 and B3 were placed into lag service. Once the beds were on-line the

effluent water was noted to be foamy, cloudy and had a distinct organic odor. In addition

the pH of the effluent water shifted down to less than 6.0. The GWTP was reverted back

to running with beds A2 and B2 as lag beds until replacement resin was loaded into beds

A3 and B3 on June 7 and 8, 2005. There were no water quality issues when these beds

were brought on line. Subsequent testing of the resin that produced the foamy water

revealed extremely high concentrations of organics that had not been rinsed from the

resin following manufacturing. When standby beds Al and Bl were placed into lag

service on July 20, 2005 the effluent water was once again foamy, cloudy and had an

odor. The pH shift was once again below 6.0. A decision was made to let this water

rinse-in while discharging the effluent to the surface stream. The two new lag beds (Al

and Bl) required approximately 2 million gallons of rinse before the pH equalized. The

lot by lot total organic concentration (TOC) testing performed by US filter included lots

of Purolite A300 that the resin service contract for the GWTP then called for as well as

Dow SAR resin. Both of these resins are strong base anion resins in chloride form and

are functional equivalents for removal of hexavalent chromium. This data showed the

Dow resin to be much cleaner than the Purolite resin that had been delivered to the plant

(this data is included as Appendix A to1 the seventh audit report). The contaminants in the

Purolite resin were suspected to be the cause of the foaming, odor and color throw. The

large pH excursions associated with these two incidents had not been noted before at the

GWTP and would not be the explained by high TOC levels in the resin. As of the end of

the seventh audit period, negotiations were underway with US Filter (USF) to switch

resin supply to the Dow SAR. In addition, new quality control (QC) requirements were

placed on USF to conduct a 16 hour soak test for TOC on every batch of resin. In

addition the proposed new resin contract would require full 21 CFR 173.25 testing

protocol for leachable organics.

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The information in the paragraph above is presented in greater detail in section

2.3 of the seventh audit report. Investigations into the resin issues continued throughout

the eighth audit period. Following the July 20 incident, Both Purolite and USF sent

representative to the GWTP to take samples of the raw groundwater entering the ion

exchange process on August 4, 2005. It was Purolite's contention that the problem was

not with their resin but that the incoming water quality had significantly changed. The

results of the raw water samples taken on August 4, 2005 demonstrated that had been no

substantial change in any of the influent water quality parameters with the sole exception

of lower hexavalent chromium concentration. Following this testing, negotiations were

finalized on the new resin service contract with USF. The new contract requires the

provision of virgin Dow SAR resin and a 16 hour soak test for TOC on every resin batch

prior to delivery to the GWTP with a provisional limit of 10 ppm. In addition, the

contract requires that the first ten batches of Dow SAR be tested in accordance with 21

CFR 173.25 (FDA testing protocols) to establish a relationship between the 16 hour soak

test results and the full FDA protocol. These first ten batches will be used to establish a

permanent limit on TOC concentration from the 16 hour soak test. Following this initial

period, one batch of resin will be tested by FDA protocols at least twice annually to

verify that the soak test data continues to provide complete assurance that the resin is

suitable for use in a drinking water system. The first two batches of Dow SAR resin were

delivered to the GWTP and loaded into beds A3 and B3 on September 22, 2005. The 21

CFR 173.25 testing yielded less than 1 ppm TOC for both batches. The 16 hour soak test

produced TOC levels of 1.0 ppm for one batch and 3.0 on the other. In short this resin is

extremely clean.

In order to better understand the pH shift several tests were conducted at the

GWTP. Continuous flow column tests of both Purolite A300 and Dow SAR resin were

performed at the GWTP on September 12 through 16, 2005. Three small test columns of

Purolite A300 were tested, each pretreated in a different way. One column was rinsed

only, one column was cycled (exhausted and then regenerated back to the chloride form)

and rinsed. The third column was cycled, rinsed and then placed completely in the

bicarbonate form. The most plausible explanation for the large downward pH shift was

Ace Services Siie 2-16 044720.01.49LTRAAudi l Report No. 8

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that the fresh resin was removing alkalinity from the raw water until equilibrium was

reached. It was theorized that by first placing the resin in the bicarbonate form, enough

bicarbonate would come off of the resin during the initial run-in to buffer the downward

pH shift. In addition to the three small test columns of Purolite A300, a single column of

Dow SAR was tested. The Dow SAR resin had not been treated in any fashion and was

exactly as it came from Dow's manufacturing process. The column tests were conducted

to simulate the conditions that occur when a fresh resin bed is first brought online in lag

service. The rinsed Purolite resin dropped to a pH of 6.27 after a water flow through the

column equal to 33 resin bed volumes (BV), the cycled and rinsed Purolite resin

exhibited less shift dropping to pH 6.45 at 33 BV. The Purolite resin that was cycled and

placed in the bicarbonate form actually caused an upward pH shift to 7.24 immediately at

start-up. The untreated Dow SAR resin exhibited the most extreme pH shift, dropping to

a low of pH 4.8 at about 10 BV followed by a rapid recovery to 6.45 at around 100 BV.

The three test columns that were not in the bicarbonate form all reached a pH of 7.0 by

260 BV. The bicarbonate form resin stayed above 7.0 through the conclusion of the test

at about 350 BV. Data from these column tests are included in Appendix A of this

report. The conclusions to be drawn from these column tests are as follows: 1) A

temporary pH shift to below 6.5 (the lowest allowed for drinking water) is likely unless

the resin is at least partially converted to the bicarbonate form. 2) 100% conversion to

bicarbonate is more than needed to prevent an excessive downward pH shift. Only

partial conversion is needed. 3) More water run through the resin during pre-treatment

correlates to a less severe downward pH shift. 4) The Purolite A300 resin seems to be

adequately clean once it has been cycled and fully rinsed. These column tests left some

important questions unanswered including what is the minimum required bicarbonate

conversion to prevent a pH shift to below 6.5 and how much of the pH shift is mitigated

by all the water that is passed through the resin as it is sluiced through the tanker, transfer

vessel and process vessel prior to being put on-line in lag service at the GWTP.

Standby process beds A2 and B2 were placed into lag service on September 14,

2005. The resin in these two beds was Purolite A300 that had been cycled and placed

60% in the bicarbonate form. A flow through test cell was set up on the effluent of both

Ace Services Site 2-17 044720.01.49LTRA Audil Report No. 8

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IIIIIIIIIIIIIIIiiti

beds to closely monitor the pH as the beds went into service. The pH dropped only

slightly to a low of 6.7 just at start-up and rose quickly and steadily to 7.0 in only 50 BV.

It was noted that this resin had actually been cycled twice prior to delivery to the GWTP.

Purolite had cycled the resin before delivery to USF. Due to the problems that residual

contaminants in the resin had caused recently, USF cycled the resin again prior to the

partial bicarbonate conversion. When this resin was placed in service at the GWTP no

foaming, odor or color throw was evident. This run in demonstrated that partial

bicarbonate conversion will limit the downward pH shift to acceptable levels. Data from

this bed run-in test is included in Appendix A,

One final set of resin tests were conducted at the GWTP. Theses tests were full

scale process tests aimed at determining the impact on the pH shift caused by the normal

sluicing of the resin and secondarily to help the determine the minimum percent

bicarbonate conversion needed with the DOW SAR resin to limit the pH shift to above

6.5. Beds A3 and B3 had been loaded with the first batches of Dow SAR under the new

supply contract with USF on September 22, 2005. Bed A3 was loaded with untreated

Dow SAR like the Dow resin in the small column test conducted September 12 through

16, 2005 described above. The difference this time was that since this resin was a full

batch loaded into the process vessel this resin had been sluiced into the transportation

tanker were is remained flooded for two or three days in transit to the GWTP. Once the

tanker arrived at the GWTP, the resin was sluiced out of the tanker into the GWTP

transfer vessel and then sluiced again from the transfer vessel into the process vessel.

Once in the process vessel the resin was backwashed with 9000 gallons, settled and

rinsed with another 9000 gallons then left in the process vessel for about 5 weeks from

September 22 until October 26, 2005 when both beds A3 and B3 were placed in lag

service. This handling is typical for all resin deliveries the GWTP. Bed B3 was loaded

with Dow SAR that had been converted to approximately 35% bicarbonate from, but was

otherwise handled in the same manner as the untreated resin in bed A3. Flow through

cells were set up on the effluent of both beds prior to placing them into lag service and

the pH was closely monitored during the run-in. The effluent pH from the untreated resin

in bed A3 drop to a low of pH 5.89 at 30 BV and then steadily recovered reaching pH 6.5

Ace Services Site 2-18 044720.01.49

LTRA Audit Report No. 8

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ItfffIIIIIIIIIIIIII

at around 110 BV then full equilibrium (in=out) at 322 BV. Note that all the water

passed through this resin in the normal course of handling reduced the severity of the pH

offset from 4.8 to only 5.89. The partial bicarbonate form Dow resin in bed B3 hit a low

of Ph 6.59 in only 3 BV, rising steadily to a plateau around pH 6.90 after 58 BV. The

effluent pH held nearly steady from 58 to 166 BV then resumed rising to equilibrium (in

= out) at 322 BV. Data from this bed run-in test is included in Appendix A

The results of the testing done the week of October 25, 2005 indicate that a

complete solution to the resin issues at the GWTP would include using Dow SAR

converted to about 35% bicarbonate form. Pricing was negotiated with USF for the

bicarbonate conversion and the supply contract was modified accordingly. The cost for

the bicarbonate conversion is $5.87 per cubic foot of resin. This represents an increase of

about 5.6% over the base cost of the Dow SAR. The contract originally signed with USF

for supply of Dow SAR allowed for a 10% annual price escalation. The modification to

this contract to include the bicarbonate conversion limits the first annual escalation to

13% including the 5.6% cost of the bicarbonate conversion, thus USF is sharing some of

the cost with EPA. The contract modification was placed in force during the week of

October 31,2005. '

The first resin beds with Dow SAR resin (beds A3 and B3) will not cycle though

and out of lead service until some time late in the ninth audit period. It is expected that

the Dow SAR will have somewhat better chromium holding performance than the

Purolite A300 thereby offsetting some of the increase in resin costs. This will be

evaluated in the ninth audit report.

Ace Services Sue 2-19 044720.01.49LIRA Audit Report No. 8

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IIIIIIIIIIIIIIIIIII

3.0 Sampling and Record Keeping

As part of the audit, the in-plant records kept by the City operators were reviewed

for completeness and conformity to requirements. During the review, emphasis was

placed on water flow and chromium concentration data that are critical to evaluation of

treatment system performance. The daily records were well organized in notebooks kept

at the plant. The daily records were organized by month and date and were complete and

easy to access. The City operators have continued to enter the flow meter totalizer

readings and sample analysis results in Excel spreadsheets to facilitate trend tracking and

quick data retrieval. The sample record sheets have been expanded to include free

chlorine results now when the discharge to the city water system is active.

The operators have continued to fill out the new GAC system log sheet each day.

This new log sheet records critical flow and pressure data for the new GAC system.

Samples taken and analyzed by KDHE from the GAC system upstream of the

GWTP indicated the possibility of the presence of trivalent chromium in the raw

groundwater. This would be a significant problem since the anion resin used at the

GWTP cannot remove trivalent chromium. A careful review of the influent water sample

results from the GWTP show no indication of any trivalent chromium. In addition,

effluent samples from the GWTP sent for laboratory analysis indicate no detectable

chromium in the effluent of any species (total chrome analysis). Any measurable amount

of trivalent chromium in the GWTP influent would necessarily show up in total chrome

analysis of the GWTP effluent. As a precaution, the regular morning plant influent

sample will now be analyzed on-site for both total and hexavalent chromium. A total

value in excess of the hexavalent value would indicate the possibility of trivalent chrome

in the influent.

The City operating staff has done an excellent job with the sampling and record

keeping requirements during the sixth audit period. Only one significant irregularity was

noted in the audit and subsequent review of records. The hexavalent chromium

concentration data at the GWTP influent (sample locations SC-1 and SC-2) are higher in

the off-site laboratory analysis than those recorded from in-plant analysis. If this trend

Ace Services Site 3-1 044720.01.49LIRA Audit Report No. 8

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continues it may be necessary to replace the GWTP lab spectrophotometer.

Recommendations regarding plant sampling are as follows:

1. Addition of total chrome analysis for plant influent. As described above, the

daily GWTP influent sample will be analyzed for both total and hexavalent

chromium as a precaution to look for evidence of trivalent chromium in the

raw water. The. plant sample record form was revised to record total

chromium results for the sample taken at location SC-1.

2. Sample transfer methods for on-site analysis. BVSPC had recommended

that the plant operators use pre-calibrated disposable pipettes or pipettors to

transfer the precise correct volume of sample from the large sample collection

jars to the small vials used for sample analysis in the spectrophotometers.

During the seventh audit period, the plant operators instituted this change,

choosing to use a fixed volume disposable pipette. Shortly after making the

change in procedure, the supplier of the bulb style pipette discontinued that

product. On BVSPC recommendation, the operators began using an

adjustable volume plunger style pipettor with a disposable tip. The operators

report that this has been a marked improvement and making sample transfer

simpler while reducing the possibility of cross sample contamination.

i

There have been no significant changes regarding plant sampling and record

keeping during the eighth audit period with the exception of adding once daily total

chromium analysis at sample location SC-1.

Ace Services Site 3-2 044720.01.49LIRA Audit Report No. 8

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4.0 Evaluation of System Performance

The new GAC system constructed by KDHE was started on August 24, 2004

(during the fourth audit period). Data were closely monitored during the eighth audit

period to determine if there were any significant impacts on the GWTS as a result of the

GAC system being on line. The only day-to-day impacts noted were the occasional

loading of carbon fines on the bag filters and the additional head pressure required of the

extraction pumps to push through the GAC beds.

The ability to capture and control the chromium plume in the ground water is

periodically assessed via sampling and ground water elevation measurement. These data

are analyzed and the findings summarized in semi-annual Cleanup Status Reports. The

most recent report (Cleanup Status Report Number 4, dated July 20, 2005) indicates that

the extraction wells are providing good plume containment and capture.

Selected flow and sampling data from July 21, 2005, through October 12, 2005,

are presented in Table 4-1. Table 4-1 also shows the amount of hexavalent chromium

removed by the treatment system. As shown in Table 4-1, the concentration of

hexavalent chromium in the raw water entering the treatment system during the eighth

audit period began at about 220 ug/1 in late July and dropped slightly to about 185 ug/l.by

early October.

The data show that the system treated 101.5 million gallons from July 21, 2005,

through October 12, 2005: 51.56 million gallons in Train A and 49.96 million gallons in

Train B. A total of 76.14 kilograms (kg) (167.86 pounds) of chromium were removed

during this period. Two beds of ion exchange resin (Beds A3 and B3) were exhausted

during this period as shown in Table 4-1. The resin performance for each of the

exhausted beds is shown below:

Bed A3: 29.44 million gallons: 50.45 Ibs chromium: 41.61 gr/cf*

Bed B3: 29.11 million gallons: 49.89 Ibs chromium: 41.14 gr/cP

* gr/cf = grams of chromium per cubic foot of resin

Ace Services Site 4-1 044720.01.49LIRA Audil Report No. 8

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IThe relative performance data from the previous periods are shown below along

• with the data for Beds A3 and B3 from this audit period. Data from the early periods are

shown as an average per 550 cubic foot bed of resin.

Performance test: 20.5 million gal: 121.4 gr/cf*

ft First audit period: 27.0 million gal: 93.6 gr/cf*

Second audit period: 32.5 million gal: 51.2 gr/cf*

• Third Audit Period: 32.3 million gal: 41.9 gr/cf*

Fourth Audit period:

• Bed A3: 31.1 million gal: 71.35 gr/cf*

Bed B2 31.1 million gal: 34.28 gr/cf*

• BedB3 33.9 million gal 29.53 gr/cf*

Fifth Audit period:

I BedAl 25.72 million gal 75.1 gr/cf *

BedBl 25.35 million gaJ 88.18 gr/cf*

1 BedA2 40.37 million gal 90.81 gr/cf*

BedB2 30.71 million gal 73.06 gr/cf*

I Sixth Audit Period: 1

Bed A3 32.04 million gal: 57.67 gr/cf*

| BedB3 35.08 million gal: 63.87 gr/cf*

Seventh Audit Period:

| BedAl 27.74 million gal 36.14 gr/cf*

Bed B1 26.75 million gal 34.86 gr/cf *

| BedA2 30.13 million gal 42.62 gr/cf*

Bed B2 30.11 million gal 42.54 gr/cf *

J Eighth Audit Period:

Bed A3 29.44 million gal 41.61 gr/cf*

I BedB3 29.11 million gal 41.14 gr/cf*

I* gr/cf = grams of chromium per cubic foot of resin

I

Ace Services Site 4-2 044720.01.49LIRA Audit Report No. 8

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The chromium holding capacity of the resin is expected to diminish with

diminishing influent hexavalent chromium concentrations due to the lower equilibrium.

This is clearly seen in the data above as well as in Figure 4-1. More gallons of water are

treated with the same 550 cubic feet of resin but at diminishing resin holding capacity.

During the entire period of time covered by the second and third audits, the wells

with the highest chromium concentrations were shut down awaiting design and

completion of the GAC system. During that time, chromium concentrations entering the

GWTP were averaging only around 120 to 150 ug/L. Once the GAC system was brought

on line in late August 2004 and all the extraction wells were restarted, the influent

chromium concentrations jumped up to as high a 700 ug/L and have been dropping

steadily since but the chromium concentration is still holding above the low levels seen in

the second and third audit periods. The affects of this can be seen in the higher grams per

cubic foot holding capacity of the resin late in the fourth audit period (Bed A3) and

throughout the fifth audit period. Chromium concentration in the influent ground water

continued to drop during the eighth audit period to around 185 ug/L by the end of the

period which is only a little higher than the very low levels seen during the second and

third audit periods and very similar to the concentration during the sixth and seventh

audit periods. Note that the total gallons treated per bed during the sixth audit period are

very similar to the results during the second and third audit periods. Total gallons treated

during the seventh and eighth audit periods are substantially lower than during the

second, third and sixth periods even though the influent chromium concentrations were

similar. There is no obvious reason for this poor performance. As noted in section 2.3

above, there have been significant issues regarding the quality and condition of the resin

supplied to the GWTP during the seventh and eighth audit periods. The last batches of

Purolite A300 are in lead service (beds A2 and B2) as of the time of writing this report.

The first batches of Dow SAR (beds A3 and B3) will cycle through lead service by the

end of the ninth audit period. The treatment performance of the new resin will be closely

monitored. It is anticipated that the Dow SAR resin will show improved performance.

As the hexavalent chromium concentration drops, a point is eventually reached

where the gallons treated by a given amount of resin will no longer increase. This is due

Ace Services Silt 4-3 044720.01.49LIRA Audit Report No. 8

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IIIIIIIIIIIIIIIIIII

to the presence of other anions in the influent water that take up resin exchange capacity.

The data presented above suggest that a 550 cubic foot volume of resin cannot treat more

than 31 to 34 million gallons of Colby ground water regardless of hexavalent chromium

concentration. Bed A2 in the fifth audit period is an obvious exception, treating over 40

million gallons at a fairly high chromium loading rate. A possible explanation is that the

bed was loaded with more than the usual 550 cubic feet of resin. Each bed has a total

volume of 1100 cubic feet and is intended to run only half full of resin to allow plenty of

head space for air bump and backwash operations. If 650 to 700 cubic feet of resin were

loaded into the bed there would be no indication of the extra resin except a slightly higher

pressure drop through the bed. A review of the pressure drop data during the time that

Bed A2 was in lead position does in fact show a pressure drop that is consistently 20% to

30% greater than the other bed in the same train. Based on the data it is very likely that

Bed A2 contained 650 to 700 cubic feet of resin during its run in the fifth audit period.

This data point is not included in Figure 4-1 since it is not representative.

Figure 4-1 is a plot of gallons of water treated by an ion exchange bed vs. the

average chromium concentration of the water treated by the bed before significant

chromium breakthrough. This figure very clearly depicts the trends and limits noted

above. As seen in Figure 4-1, the gallons of water treated increases as the chromium

loading decreases in almost a linear relationship. However, once the average chromium

concentration in the GWTP influent water drops below about 300 ug/L, no more increase

in the gallons treated per bed is seen. Every bed with an average chromium influent

concentration below 350 ug/L treated between 31 and 35 million gallons of water (except

during the seventh and eighth audit periods while resin quality issues were encountered)

with no correlation to chromium concentration. This can be used as planning tool for

scheduling bed change-outs. Unless the influent chromium concentrations again rise

above 350 ug/1, each bed can be anticipated to treat 33 +/- 2 million gallons of water.

The change to Dow SAR resin may or may not have an impact on this value.

Ion exchange is often used as a polishing process in water treatment because it is

very cost efficient compared to other treatment technologies at low contaminant

concentrations. The relatively low concentration of hexavalent chromium seen in the

composite influent groundwater is an excellent application for ion exchange. The total

Ace Services Site 4-4 044720.01.49LIRA Audit Report No. 8

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resin cost including transportation and disposal was 0.152 cents per gallon of water

treated for the eighth audit period. This is essentially the same as the .0155 cents per

gallon from the seventh audit period. This cost is up considerably from 0.130 cents per

gallon during the sixth audit period when the average chromium loading was essentially

the same and is further evidence of poor resin performance during the seventh and eighth

audit periods. This is still a significant reduction from 0.210 cents per gallon from the

performance test and 0.166 cents per gallon from the first audit period when average

chromium concentrations were higher. This diminishing cost as the chromium loading

drops demonstrates the efficiency of the ion exchange process in this application. There

is not sufficient data at this time to determine the total cost per gallon to treat the

extracted ground water including labor and plant utilities.

Ace Services Site 4-5 044720.01.49LTRA Audit Report No. 8

Page 334: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

IIIIIIIIIIIIIIIIIII

Table 4-1Selected Flow and Chromium Concentration Data

Ace Services Site

. Date

20-Jul-052122232425262728293031

Hexavalent ChromiumAt sample location SC-1Hach unit

(ug/L)

Totals for Month

ContinentalLabs (ug/L)

218218218218218218218223223223223223

TRAIN AGallonsTreatedx 1000

597558695592651564604655586676604635

7417

ChromiumRemoved

(kg)0.4930.4610.5740.4890.5370.4660.4990.5530.4950.5710.5100.5366.183

TRAIN BGallonsTreatedx l O O O

606538670570627543618631564651582612

7212

ChromiumRemoved

(kg)0.5000.4440.5530.4710.5180.4480.5100.5330.4760.5500.4910.5176.012

RemarksBeds A3 and B3 are lead

Ace Services SiteLIRA Audit Repon #8 4-6 044720.01.49

I

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IIfIffIIIIIIIIIIIII

Table 4-1Selected Flow and Chromium Concentration Data

Ace Services Site

Date

1-Aug-052345678910 '111213141516171819202122232425262728293031

Hexavalent ChromiumAt sample location SC-1Hach unit

(ug/L)

Totals for Month

ContinentalLabs (ug/L)

223223209209209209209209209215215215215215215215206206206206206206206210210210210210210210202

TRAIN AGallonsTreatedx l O O O

604574684616659614624602536606561556569572516615578549562559566558567694637626612654632598672

18572

ChromiumRemoved

(kg)0.5100.4850.5410.4880.5220.4860.4940.4760.4240.4930.4570.4530.4630.4660.4200.5010.4510.4280.4380.4360.4420.4350.4420.5520.5070.4980.4870.5200.5030.4760.514

14.807

TRAIN BGallonsTreatedx 1000

603572683615627613622601536604562554568572508612578549560558565557

.- 56669263662361165463598672

18502

ChromiumRemoved

(kg)0.5090.4830.5410.4870.4960.4850.4920.4760.4240.4920.4580.4510.4620.4660.4140.4980.4510.4280.4370.4350.440.4350.4420.5500.5060.4950.4860.520.500.470.51

14.75

Remarks

Ace Services SiteLIRA Audi t Report #8 4-7 044720.01.49

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IIIIIIIIIIIIIIIIIII

Table 4-1Selected Flow and Chromium Concentration Data

Ace Services Site

Date

1-Sept-0523456789101112131415161718192021222324252627282930

Hexavalent ChromiumAt sample location SC-1Hach unit

(ug/L)

Totals for Month

ContinentalLabs (ug/L)

145145145145145145145174174174174174174194194194194194194194194201201201201201201201182182182

TRAIN AGallonsTreatedx 1000

478547482497487489471580651594644635586642621667639,618634649574636687634634627586698615657

17959

ChromiumRemoved

(kg)0.2620.3000.2650.2730.2670.2690.2590.3820.4290.3910.4240.4180.3860.4720.4560.4900.4690.4540.4660.4770.4220.4840.5230.4830.4830.4770.4460.5310.4240.453

12.336

TRAIN BGallonsTreatedx 1000

476546480449487488470340382348380406585643619668639618633648570639686632634626585697614655

16643

ChromiumRemoved

(kg)0.2610.3000.2640.2470.2670.2680.2580.2240.2520.2290.2500.2680.3850.4720.4550.4910.4690.4540.4650.4760.4190.4860.5220.4810.4830.4770.4450.530.4230.45

11.474

Remarks

Switch to A1, B1 lead

Ace Services SiteLIRA Audi t Report #8 4-8 044720.01.49

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Table 4-1Selected Flow and Chromium Concentration Data

Ace Services Site

Date.

1-Oct-0523456789101112

Hexavalent ChromiumAt sample location SC-1Hach unit

(ug/L)

Totals for Month

ContinentalLabs (ug/L)

182182182182182185185185185185185185

TRAIN AGallonsTreatedx 1000

621636634648651553692626645630647624

7607

ChromiumRemoved

(kg)0.4280.4380.4370.4470.4490.3870.4850.4390.4520.4410.4530.4375.293

TRAIN BGallonsTreatedx 1000

620635633649653554690625]644628645623

7599

ChromiumRemoved

(kg)0.4270.4380.4360.4470.4500.3880.4830.4380.4510.4400.4520.4365.288

Remarks

Beds A 1, 81 lead

Ace Services SiteLIRA Audi t Report #8 4-9 044720.OI.49

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40

c 30

Figure 4-1Gallons treated vs chromium concentration

•5. 20 -(/>

^ 1

0

-' V.. i ' ' • ' ' * • . ' • " A -•".

'*''~'

• - • - • • , .•, •/''"%-j'f •: >'•/ ' ' •

0 200 400 600 800 1000 1200

Ghromium (ug/L)

Page 4-10

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5.0 Action Summary

The following is a list of recommended actions or changes to improve system

operation or record keeping procedures based on observations made during the eighth

audit. This is a summary list. This list also includes any needed equipment repairs or

adjustments identified during this audit. Further details can be found in the body of this

audit report. It is noted that action items 1, 2, and 4 are carried over from the seventh

audit report.

1. Install filters in the well house ventilation inlets as described in Section 2.1,

item 4.

2. Install the new conductivity probes on both trains and recalibrate the meters.

3. Rescale the PLC for the new 0 to 200 foot range to match the new level probe

in well EX-4i

4. Install the remaining bolt isolation sleeves included in the piping

modifications described in Section 2.2, Item 3.

5. Re-route the chlorine booster loop to locate the ejector inside the GWTP and

install a surge arrester on the loop to cushion this piping from water hammer.

Ace Services Site 5-1 044720.01.49LIRA Audil Repon No. 8

Page 340: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

•I•111 APPENDIX A

V Resin pH Run-in Charts

1I

IIIIIII

Page 341: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Column tests Sept 12-16, 2005Purolite A300 and Dow SAR

•Purolite, cycled•Purolite, rinsedPurolite 100% bicarbDow SAR, untreated

Bed Volumes

Page 342: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Process Bed A2 Purolite A300 cycled and placed 60% bicarbonate: Sept 14, 2005

-Series'!

2 3 4 5 6 7 8 , 1 0 1 1 2 1 3 1 4 1 5 1 . 1 7 1 8 1 9 2 0 2 1 2 2 2 3 2 4 2 5 2 8 2 9 3 2 3 6 3 . 4 1 4 4 4 7 5 0 6 6

Bed Volumes

Page 343: BLACK & VEATCH · 2020. 11. 21. · BLACK & VEATCH 6601 College Blvd. Overland Park, KS 66211 Tel: (913) 458-2900 USEPA Region VII Ace Services Site Mr. Bob Stewart USEPA Region VII

Beds A3 and B3: DOW SAR October 26, 2005

7.10

6.90

6.70 is—rJF

6.50

6.30

6.10

5.90 -

5.70

5.50

50 100 150 200

Bed Volumes

Untreated Dow SAR35% bicab Dow SAR

250 300 350