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BD[ Laboratories, Inc.2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493

Analytical

Report

Energy Fuels Resources (USA) Inc.

225 Union Blvd. ,Suite 600

Lakewood, CO 80228

ACZ Project ID: L18575

Kathy Weinel:

Enclosed are the analytical results for sample(s) submitted to ACZ Laboratories, Inc. (ACZ) on May 30, 2014. This project has been assigned to ACZ's project number, L18575. Please reference this number in all future inquiries.

All analyses were performed according to ACZ's Quality Assurance Plan. The enclosed results relate only to the samples received under L18575. Each section of this report has been reviewed and approved by the appropriate Laboratory Supervisor, or a qualified substitute.

Except as noted, the test results for the methods and parameters listed on ACZ's current NELAC certificate letter (#ACZ) meet all requirements of NELAC.

This report shall be used or copied only in its entirety. ACZ is not responsible for the consequences arising from the use of a partial report.

All samples and sub-samples associated with this project will be disposed of after July 19, 2014. If the samples are determined to be hazardous, additional charges apply for disposal (typically $11/sample). If you would like the samples to be held longer than ACZ's stated policy or to be returned, please contact your Project Manager or Customer Service Representative for further details and associated costs. ACZ retains analytical raw data reports for ten years.

If you have any questions or other needs, please contact your Project Manager.

Kathy Weinel

June 19, 2014

Project ID:



Lakewood, CO 80228

Accounts Payable

Report to: Bill to:

of 34L18575-1406191513

ACZ Sample ID: L18575-01

Sample ID: BOREN WELL

Sample Matrix: Ground Water


Project ID:


Inorganic Analytical

Results

Date Sampled: 05/27/14 15:50

Date Received: 05/30/14

Parameter EPA Method Result Units MDLQual AnalystDatePQL

Metals Analysis

XQDilution

Aluminum, dissolved M200.7 ICP mg/L 0.2U aeb0.03 06/05/14 0:021

Arsenic, dissolved M200.8 ICP-MS 0.0109 mg/L 0.001 las0.0002 06/12/14 10:401

Barium, dissolved M200.7 ICP 0.071 mg/L 0.02 aeb0.003 06/05/14 0:021

Boron, dissolved M200.7 ICP 0.34 mg/L 0.05 aeb0.01 06/05/14 0:021

Cadmium, dissolved M200.8 ICP-MS mg/L 0.0005U las0.0001 06/12/14 10:401

Calcium, dissolved M200.7 ICP 88.8 mg/L 0.5 aeb0.1 06/05/14 0:021

Cesium, dissolved M200.8 ICP-MS mg/L 0.001U las0.0002* 06/12/14 10:401

Chromium, dissolved M200.7 ICP mg/L 0.05U aeb0.01 06/05/14 0:021

Copper, dissolved M200.7 ICP mg/L 0.05U aeb0.01 06/05/14 0:021

Iron, dissolved M200.7 ICP mg/L 0.05U aeb0.02 06/05/14 0:021

Lead, dissolved M200.8 ICP-MS mg/L 0.0005U las0.0001 06/12/14 10:401

Magnesium, dissolved M200.7 ICP 153 mg/L 1 aeb0.2 06/05/14 0:021

Manganese, dissolved M200.7 ICP mg/L 0.03U aeb0.005 06/05/14 0:021

Mercury, dissolved M245.1 CVAA mg/L 0.001U mfm0.0002 06/11/14 13:121

Molybdenum, dissolved M200.7 ICP mg/L 0.1U aeb0.02 06/05/14 0:021

Nickel, dissolved M200.7 ICP mg/L 0.04U aeb0.008 06/05/14 0:021

Potassium, dissolved M200.7 ICP 18.4 mg/L 1 aeb0.2 06/05/14 0:021

Selenium, dissolved M200.8 ICP-MS 0.0391 mg/L 0.0003 las0.0001 06/12/14 10:401

Silica, dissolved M200.7 ICP 16.9 mg/L 1 aeb0.2 06/05/14 0:021

Sodium, dissolved M200.7 ICP 84.6 mg/L 1 aeb0.2 06/05/14 0:021

Uranium, dissolved M200.8 ICP-MS 0.0468 mg/L 0.0005 las0.0001* 06/12/14 10:401

Vanadium, dissolved M200.7 ICP 0.014 mg/L 0.03B aeb0.005 06/05/14 0:021

Zinc, dissolved M200.7 ICP mg/L 0.05U aeb0.01 06/05/14 0:021

REPIN.02.06.05.01 * Please refer to Qualifier Reports for details.

of 34L18575-1406191513





Project ID:



Results

Date Sampled: 05/27/14 15:50



Wet Chemistry

XQDilution

Alkalinity as CaCO3 SM2320B - Titration

Bicarbonate as CaCO3

327 mg/L 20 enb2 06/05/14 0:001

Carbonate as CaCO3 mg/L 20U enb2 06/05/14 0:001

Hydroxide as CaCO3 mg/L 20U enb2 06/05/14 0:001

Total Alkalinity 327 mg/L 20 enb2 06/05/14 0:001

Carbon, total organic (TOC)

SM5310B 4.1 mg/L 5B mpb1* 06/11/14 19:441

Cation-Anion Balance Calculation

Cation-Anion Balance 2.4 % calc06/19/14 14:04

Sum of Anions 20 meq/L 0.5 calc0.1 06/19/14 14:04

Sum of Cations 21 meq/L 0.5 calc0.1 06/19/14 14:04

Chloride SM4500Cl-E 196 mg/L 20 mss25* 06/12/14 16:1610

Fluoride SM4500F-C 0.41 mg/L 0.3 abd0.05* 06/13/14 14:271

Nitrate/Nitrite as N M353.2 - H2SO4 preserved 9 mg/L 1 pjb0.2* 06/14/14 15:5310

Nitrogen, ammonia M350.1 - Automated Phenate mg/L 0.2U mpb0.05* 06/13/14 15:331

Residue, Filterable (TDS) @180C

SM2540C 1250 mg/L 20 eaa10* 06/02/14 13:141

Residue, Non-Filterable (TSS) @105C

SM2540D mg/L 20U eaa5* 06/02/14 11:531

Sulfate SM4500 SO4-D 400 mg/L 50 abd10 06/09/14 9:481

Sulfide as S SM4500S2-D mg/L 0.1U enb0.02* 06/03/14 11:321

TDS (calculated) Calculation 1160 mg/L 50 calc10 06/19/14 14:04

TDS (ratio - measured/calculated)

Calculation 1.08 calc06/19/14 14:04


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Sample ID: STONE SPRING



Project ID:



Results

Date Sampled: 05/27/14 10:30



Metals Analysis

XQDilution



Barium, dissolved M200.7 ICP 0.017 mg/L 0.02B aeb0.003 06/05/14 0:061









Magnesium, dissolved M200.7 ICP 50.8 mg/L 1 aeb0.2 06/05/14 0:061



Molybdenum, dissolved M200.7 ICP 0.02 mg/L 0.1B aeb0.02 06/05/14 0:061










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Project ID:



Results

Date Sampled: 05/27/14 10:30



Wet Chemistry

XQDilution



243 mg/L 20 enb2 06/05/14 0:001





SM5310B mg/L 5U mpb1* 06/11/14 19:441





Chloride SM4500Cl-E 57.4 mg/L 2 mss20.5* 06/12/14 16:051


Nitrate/Nitrite as N M353.2 - H2SO4 preserved 0.85 mg/L 0.1 pjb0.02* 06/14/14 14:501



SM2540C 600 mg/L 20 eaa10* 06/02/14 13:161


SM2540D mg/L 20U eaa5* 06/02/14 11:541

Sulfate SM4500 SO4-D 210 mg/L 50 abd10 06/09/14 9:501






of 34L18575-1406191513


Sample ID: STONE CREEK



Project ID:



Results

Date Sampled: 05/27/14 10:30



Metals Analysis

XQDilution






Calcium, dissolved M200.7 ICP 52 mg/L 0.5 aeb0.1 06/05/14 0:151



















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Project ID:



Results

Date Sampled: 05/27/14 10:30



Wet Chemistry

XQDilution



244 mg/L 20 enb2 06/05/14 0:001





SM5310B mg/L 5U mpb1* 06/11/14 19:441





Chloride SM4500Cl-E 57.8 mg/L 2 mss20.5* 06/12/14 16:051





SM2540C 590 mg/L 20 eaa10* 06/02/14 13:181


SM2540D mg/L 20U eaa5* 06/02/14 11:561

Sulfate SM4500 SO4-D 210 mg/L 50 eaa10 06/12/14 13:541






of 34L18575-1406191513

A C Z Laboratories, Inc.2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493

Report Header Explanations

Batch A distinct set of samples analyzed at a specific time

Found Value of the QC Type of interest

Limit Upper limit for RPD, in %.

Lower Lower Recovery Limit, in % (except for LCSS, mg/Kg)

MDL Method Detection Limit. Same as Minimum Reporting Limit. Allows for instrument and annual fluctuations.

PCN/SCN A number assigned to reagents/standards to trace to the manufacturer's certificate of analysis

PQL Practical Quantitation Limit, typically 5 times the MDL.

QC True Value of the Control Sample or the amount added to the Spike

Rec Recovered amount of the true value or spike added, in % (except for LCSS, mg/Kg)

RPD Relative Percent Difference, calculation used for Duplicate QC Types

Upper Upper Recovery Limit, in % (except for LCSS, mg/Kg)

Sample Value of the Sample of interest

QC Sample Types

AS Analytical Spike (Post Digestion) LCSWD Laboratory Control Sample - Water Duplicate

ASD Analytical Spike (Post Digestion) Duplicate LFB Laboratory Fortified Blank

CCB Continuing Calibration Blank LFM Laboratory Fortified Matrix

CCV Continuing Calibration Verification standard LFMD Laboratory Fortified Matrix Duplicate

DUP Sample Duplicate LRB Laboratory Reagent Blank

ICB Initial Calibration Blank MS Matrix Spike

ICV Initial Calibration Verification standard MSD Matrix Spike Duplicate

ICSAB Inter-element Correction Standard - A plus B solutions PBS Prep Blank - Soil

LCSS Laboratory Control Sample - Soil PBW Prep Blank - Water

LCSSD Laboratory Control Sample - Soil Duplicate PQV Practical Quantitation Verification standard

LCSW Laboratory Control Sample - Water SDL Serial Dilution

QC Sample Type Explanations

Blanks Verifies that there is no or minimal contamination in the prep method or calibration procedure.

Control Samples Verifies the accuracy of the method, including the prep procedure.

Duplicates Verifies the precision of the instrument and/or method.

Spikes/Fortified Matrix Determines sample matrix interferences, if any.

Standard Verifies the validity of the calibration.

ACZ Qualifiers (Qual)

B Analyte concentration detected at a value between MDL and PQL. The associated value is an estimated quantity.

H Analysis exceeded method hold time. pH is a field test with an immediate hold time.

L Target analyte response was below the laboratory defined negative threshold.

U The material was analyzed for, but was not detected above the level of the associated value.

The associated value is either the sample quantitation limit or the sample detection limit.

Method References

(1) EPA 600/4-83-020. Methods for Chemical Analysis of Water and Wastes, March 1983.

(2) EPA 600/R-93-100. Methods for the Determination of Inorganic Substances in Environmental Samples, August 1993.

(3) EPA 600/R-94-111. Methods for the Determination of Metals in Environmental Samples - Supplement I, May 1994.

(4) EPA SW-846. Test Methods for Evaluating Solid Waste.

(5) Standard Methods for the Examination of Water and Wastewater.

Comments

(1) QC results calculated from raw data. Results may vary slightly if the rounded values are used in the calculations.

(2) Soil, Sludge, and Plant matrices for Inorganic analyses are reported on a dry weight basis.

(3) Animal matrices for Inorganic analyses are reported on an "as received" basis.

(4) An asterisk in the "XQ" column indicates there is an extended qualifier and/or certification qualifier

associated with the result.

(5) If the MDL equals the PQL or the MDL column is omitted, the PQL is the reporting limit.

For a complete list of ACZ's Extended Qualifiers, please click: http://www.acz.com/public/extquallist.pdf

REP001.09.12.01

Inorganic

Reference

of 34L18575-1406191513


Inorganic QC

Summary

ACZ Project ID: L18575Energy Fuels Resources (USA) Inc.


ACZ ID Analyzed RecSample QualLower Upper RPDFoundType UnitsPCN/SCN LimitQC

WG365330

WG365330PBW1 06/05/14 15:07PBW 3.4 -20 20mg/L

WG365330LCSW3 06/05/14 15:25 97.6LCSW WC140527- 800.3 90 110mg/L820.0001

WG365330LCSW6 06/05/14 18:40 100LCSW WC140527- 819.9 90 110mg/L820.0001

WG365330PBW2 06/05/14 18:49PBW U -20 20mg/L


WG365330PBW3 06/05/14 22:17PBW U -20 20mg/L

L18577-02DUP 06/05/14 23:25 302DUP 289.6 4.2mg/L 20


WG365330PBW4 06/06/14 1:27PBW U -20 20mg/L

WG365330LCSW15 06/06/14 4:52 101.1LCSW WC140527- 829 90 110mg/L820.0001

Aluminum, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 100.4ICV II140512-2 2.007 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.09 0.09mg/L

WG365235PQV 06/04/14 23:44 95.2PQV II140516-2 .143 70 130mg/L.150165

WG365235SIC 06/04/14 23:47 101.5SIC II140602-1 203.4 1 200mg/L200.370165

WG365235LFB 06/04/14 23:53 107LFB II140530-2 1.071 85 115mg/L1.0011

L18575-02AS 06/05/14 0:09 U 108.2AS II140530-2 1.083 85 115mg/L1.0011

L18575-02ASD 06/05/14 0:12 U 108ASD II140530-2 1.081 0.1885 115mg/L 201.0011

WG365235CCV1 06/05/14 0:24 97.3CCV II140506-1 .973 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.09 0.09mg/L

WG365235CCV2 06/05/14 1:02 98.7CCV II140506-1 .987 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.09 0.09mg/L

WG365235CCV3 06/05/14 1:25 97.8CCV II140506-1 .978 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.09 0.09mg/L

Arsenic, dissolved M200.8 ICP-MS


WG365728

WG365728ICV 06/12/14 9:45 106.8ICV MS140513-1 .05339 90 110mg/L.05

WG365728ICB 06/12/14 9:48ICB U -0.0006 0.0006mg/L

WG365728LFB 06/12/14 9:52 92.9LFB MS140513-3 .04656 85 115mg/L.0501

WG365728CCV1 06/12/14 10:21 103CCV MS140513-2 .1032 90 110mg/L.1002

WG365728CCB1 06/12/14 10:24CCB U -0.0006 0.0006mg/L

L18575-03AS 06/12/14 10:50 .0082 106.9AS MS140513-3 .06178 70 130mg/L.0501

L18575-03ASD 06/12/14 10:53 .0082 107.5ASD MS140513-3 .06206 0.4570 130mg/L 20.0501

WG365728CCV2 06/12/14 11:00 103.9CCV MS140513-2 .1041 90 110mg/L.1002

WG365728CCB2 06/12/14 11:03CCB U -0.0006 0.0006mg/L

of 34L18575-1406191513


Inorganic QC

Summary


Barium, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 99.6ICV II140512-2 1.9918 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.009 0.009mg/L

WG365235PQV 06/04/14 23:44 86PQV II140516-2 .0129 70 130mg/L.015

WG365235SIC 06/04/14 23:47 99.2SIC II140602-1 .0992 80 120mg/L.1

WG365235LFB 06/04/14 23:53 101.4LFB II140530-2 .5069 85 115mg/L.5

L18575-02AS 06/05/14 0:09 .017 101.5AS II140530-2 .5247 85 115mg/L.5

L18575-02ASD 06/05/14 0:12 .017 102.2ASD II140530-2 .5279 0.6185 115mg/L 20.5

WG365235CCV1 06/05/14 0:24 98.5CCV II140506-1 .9848 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.009 0.009mg/L

WG365235CCV2 06/05/14 1:02 100.3CCV II140506-1 1.003 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.009 0.009mg/L

WG365235CCV3 06/05/14 1:25 100.8CCV II140506-1 1.008 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.009 0.009mg/L

Boron, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 102.7ICV II140512-2 2.054 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.03 0.03mg/L

WG365235PQV 06/04/14 23:44 113.9PQV II140516-2 .057 70 130mg/L.05005

WG365235SIC 06/04/14 23:47 102.9SIC II140602-1 .103 80 120mg/L.1001

WG365235LFB 06/04/14 23:53 104.5LFB II140530-2 .523 85 115mg/L.5005

L18575-02AS 06/05/14 0:09 .35 100.1AS II140530-2 .851 85 115mg/L.5005

L18575-02ASD 06/05/14 0:12 .35 102.5ASD II140530-2 .863 1.485 115mg/L 20.5005

WG365235CCV1 06/05/14 0:24 100.9CCV II140506-1 1.009 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.03 0.03mg/L

WG365235CCV2 06/05/14 1:02 102.3CCV II140506-1 1.023 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.03 0.03mg/L

WG365235CCV3 06/05/14 1:25 101.6CCV II140506-1 1.016 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.03 0.03mg/L

Cadmium, dissolved M200.8 ICP-MS


WG365728

WG365728ICV 06/12/14 9:45 102.9ICV MS140513-1 .05143 90 110mg/L.05

WG365728ICB 06/12/14 9:48ICB U -0.0003 0.0003mg/L

WG365728LFB 06/12/14 9:52 98.6LFB MS140513-3 .04939 85 115mg/L.0501

WG365728CCV1 06/12/14 10:21 101.9CCV MS140513-2 .1021 90 110mg/L.1002

WG365728CCB1 06/12/14 10:24CCB U -0.0003 0.0003mg/L

L18575-03AS 06/12/14 10:50 U 99.1AS MS140513-3 .04965 70 130mg/L.0501

L18575-03ASD 06/12/14 10:53 U 101.1ASD MS140513-3 .05064 1.9770 130mg/L 20.0501

WG365728CCV2 06/12/14 11:00 100.6CCV MS140513-2 .1008 90 110mg/L.1002

WG365728CCB2 06/12/14 11:03CCB U -0.0003 0.0003mg/L

WG365728CCV3 06/12/14 11:26 100.7CCV MS140513-2 .1009 90 110mg/L.1002

WG365728CCB3 06/12/14 11:29CCB U -0.0003 0.0003mg/L

of 34L18575-1406191513


Inorganic QC

Summary


Calcium, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 100.3ICV II140512-2 100.29 95 105mg/L100

WG365235ICB 06/04/14 23:41ICB U -0.3 0.3mg/L

WG365235PQV 06/04/14 23:44 94PQV II140516-2 .47 70 130mg/L.5002

WG365235SIC 06/04/14 23:47 97.8SIC II140602-1 196 1 200mg/L200.5002

WG365235LFB 06/04/14 23:53 106.7LFB II140530-2 72.55 85 115mg/L67.98099

L18575-02AS 06/05/14 0:09 51.9 104.3AS II140530-2 122.8 85 115mg/L67.98099

L18575-02ASD 06/05/14 0:12 51.9 105.2ASD II140530-2 123.4 0.4985 115mg/L 2067.98099

WG365235CCV1 06/05/14 0:24 98.7CCV II140506-1 49.34 90 110mg/L50

WG365235CCB1 06/05/14 0:27CCB U -0.3 0.3mg/L

WG365235CCV2 06/05/14 1:02 99.7CCV II140506-1 49.87 90 110mg/L50

WG365235CCB2 06/05/14 1:05CCB U -0.3 0.3mg/L

WG365235CCV3 06/05/14 1:25 98.7CCV II140506-1 49.36 90 110mg/L50

WG365235CCB3 06/05/14 1:28CCB U -0.3 0.3mg/L

Carbon, total organic (TOC) SM5310B


WG358122

WG358122ICV 01/22/14 11:52 102ICV WI131209-3 102 90 110mg/L100

WG358122ICB 01/22/14 11:52ICB U -3 3mg/L

WG365699

WG365699CCV1 06/11/14 19:44 96.4CCV WI140502-1 48.2 90 110mg/L50

WG365699CCB1 06/11/14 19:44CCB U -3 3mg/L

WG365699PQV 06/11/14 19:44 94PQV WI140502-3 4.7 70 130mg/L5

WG365699LFB 06/11/14 19:44 94.6LFB WI140502-2 47.3 90 110mg/L50

L18575-01DUP RA06/11/14 19:44 4.1DUP 4 2.5mg/L 20

L18575-02AS 06/11/14 19:44 U 95AS WI140502-2 47.5 90 110mg/L50

WG365699CCV2 06/11/14 19:44 94.6CCV WI140502-1 47.3 90 110mg/L50

WG365699CCB2 06/11/14 19:44CCB U -3 3mg/L

WG365699CCV3 06/11/14 19:44 96.2CCV WI140502-1 48.1 90 110mg/L50

WG365699CCB3 06/11/14 19:44CCB U -3 3mg/L

WG365699CCV4 06/11/14 19:44 96.2CCV WI140502-1 48.1 90 110mg/L50

WG365699CCB4 06/11/14 19:44CCB U -3 3mg/L

Cesium, dissolved M200.8 ICP-MS


WG365728

WG365728ICV 06/12/14 9:45 105.2ICV MS140513-1 .0526 90 110mg/L.05

WG365728ICB 06/12/14 9:48ICB U -0.0006 0.0006mg/L

WG365728LFB 06/12/14 9:52 102.3LFB MS140513-3 .05115 85 115mg/L.05

WG365728CCV1 06/12/14 10:21 102.4CCV MS140513-2 .1024 90 110mg/L.1

WG365728CCB1 06/12/14 10:24CCB U -0.0006 0.0006mg/L

L18575-03AS 06/12/14 10:50 U 105.6AS MS140513-3 .0528 70 130mg/L.05

L18575-03ASD 06/12/14 10:53 U 108.2ASD MS140513-3 .0541 2.4370 130mg/L 20.05

WG365728CCV2 06/12/14 11:00 101.9CCV MS140513-2 .1019 90 110mg/L.1

WG365728CCB2 06/12/14 11:03CCB U -0.0006 0.0006mg/L

WG365728CCV3 06/12/14 11:26 103.2CCV MS140513-2 .1032 90 110mg/L.1

WG365728CCB3 06/12/14 11:29CCB U -0.0006 0.0006mg/L

of 34L18575-1406191513


Inorganic QC

Summary


Chloride SM4500Cl-E


WG365759

WG365759ICB 06/12/14 15:35ICB U -1.5 1.5mg/L

WG365759ICV 06/12/14 15:35 108.6ICV WI130722-5 59.68 90 110mg/L54.945

WG365759CCV1 06/12/14 16:04 102.7CCV WI131028-1 51.34 90 110mg/L50

WG365759CCB1 06/12/14 16:04CCB U -1.5 1.5mg/L

WG365759LFB1 06/12/14 16:05 101.3LFB WI140508-1 30.39 90 110mg/L30

L18575-02DUP 06/12/14 16:05 57.4DUP 56.91 0.9mg/L 20

WG365759CCV2 06/12/14 16:06 104.1CCV WI131028-1 52.03 90 110mg/L50

WG365759CCB2 06/12/14 16:06CCB .57 -1.5 1.5mg/L

WG365759CCV3 06/12/14 16:08 102.2CCV WI131028-1 51.1 90 110mg/L50

WG365759CCB3 06/12/14 16:08CCB U -1.5 1.5mg/L

WG365759CCV4 06/12/14 16:14 102.4CCV WI131028-1 51.2 90 110mg/L50

WG365759CCB4 06/12/14 16:14CCB U -1.5 1.5mg/L

WG365759CCV5 06/12/14 16:16 101.8CCV WI131028-1 50.92 90 110mg/L50

WG365759CCB5 06/12/14 16:16CCB U -1.5 1.5mg/L

L18575-01AS M306/12/14 16:16 196 82AS 10XCL 220.6 90 110mg/L30

WG365759CCV6 06/12/14 16:22 102.4CCV WI131028-1 51.19 90 110mg/L50

WG365759CCB6 06/12/14 16:22CCB U -1.5 1.5mg/L

WG365759CCV7 06/12/14 16:23 101.3CCV WI131028-1 50.66 90 110mg/L50

WG365759CCB7 06/12/14 16:23CCB U -1.5 1.5mg/L

WG365759CCV8 06/12/14 16:28 103CCV WI131028-1 51.49 90 110mg/L50

WG365759CCB8 06/12/14 16:28CCB U -1.5 1.5mg/L

WG365759CCV9 06/12/14 16:34 101.5CCV WI131028-1 50.77 90 110mg/L50

WG365759CCB9 06/12/14 16:34CCB U -1.5 1.5mg/L

WG365759CCV10 06/12/14 16:40 102.5CCV WI131028-1 51.27 90 110mg/L50

WG365759CCB10 06/12/14 16:40CCB U -1.5 1.5mg/L

Chromium, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 98.1ICV II140512-2 1.961 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.03 0.03mg/L

WG365235PQV 06/04/14 23:44 95.8PQV II140516-2 .048 70 130mg/L.0501

WG365235SIC 06/04/14 23:47 94.8SIC II140602-1 .095 80 120mg/L.1002

WG365235LFB 06/04/14 23:53 100.4LFB II140530-2 .503 85 115mg/L.501

L18575-02AS 06/05/14 0:09 U 100.4AS II140530-2 .503 85 115mg/L.501

L18575-02ASD 06/05/14 0:12 U 101ASD II140530-2 .506 0.5985 115mg/L 20.501

WG365235CCV1 06/05/14 0:24 97CCV II140506-1 .97 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.03 0.03mg/L

WG365235CCV2 06/05/14 1:02 98.5CCV II140506-1 .985 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.03 0.03mg/L

WG365235CCV3 06/05/14 1:25 97.6CCV II140506-1 .976 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.03 0.03mg/L

of 34L18575-1406191513


Inorganic QC

Summary


Copper, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 98.2ICV II140512-2 1.963 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.03 0.03mg/L

WG365235PQV 06/04/14 23:44 104PQV II140516-2 .052 70 130mg/L.05

WG365235SIC 06/04/14 23:47 95SIC II140602-1 .095 80 120mg/L.1

WG365235LFB 06/04/14 23:53 100.6LFB II140530-2 .503 85 115mg/L.5

L18575-02AS 06/05/14 0:09 U 100.4AS II140530-2 .502 85 115mg/L.5

L18575-02ASD 06/05/14 0:12 U 101ASD II140530-2 .505 0.685 115mg/L 20.5

WG365235CCV1 06/05/14 0:24 96.7CCV II140506-1 .967 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.03 0.03mg/L

WG365235CCV2 06/05/14 1:02 98.2CCV II140506-1 .982 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.03 0.03mg/L

WG365235CCV3 06/05/14 1:25 98.8CCV II140506-1 .988 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.03 0.03mg/L

Fluoride SM4500F-C


WG365739

WG365739ICV 06/13/14 13:57 95.5ICV WC140528- 1.909 95 105mg/L2

WG365739ICB 06/13/14 14:01ICB U -0.15 0.15mg/L

WG365739PQV 06/13/14 14:07 91.7PQV WC140612- .23 70 130mg/L.25075

WG365739LFB1 06/13/14 14:15 96.6LFB WC140501- 4.843 90 110mg/L5.015

L18575-01AS 06/13/14 14:31 .41 96.2AS WC140501- 5.232 90 110mg/L5.015

L18575-01DUP RA06/13/14 14:36 .41DUP .406 1mg/L 20

WG365739CCV1 06/13/14 15:07 98.6CCV WC140528- 1.971 90 110mg/L2

WG365739CCB1 06/13/14 15:15CCB .055 -0.15 0.15mg/L

WG365739CCV2 06/13/14 16:27 101.8CCV WC140528- 2.036 90 110mg/L2

WG365739CCB2 06/13/14 16:35CCB U -0.15 0.15mg/L

WG365739LFB2 06/13/14 17:18 97.4LFB WC140501- 4.887 90 110mg/L5.015

WG365739CCV3 06/13/14 17:45 99.5CCV WC140528- 1.99 90 110mg/L2

WG365739CCB3 06/13/14 17:53CCB U -0.15 0.15mg/L

WG365739CCV4 06/13/14 18:35 102.7CCV WC140528- 2.054 90 110mg/L2

WG365739CCB4 06/13/14 18:42CCB U -0.15 0.15mg/L

WG365739CCV5 06/13/14 19:50 98.6CCV WC140528- 1.971 90 110mg/L2

WG365739CCB5 06/13/14 19:58CCB U -0.15 0.15mg/L

WG365739CCV6 06/13/14 20:14 100.4CCV WC140528- 2.008 90 110mg/L2

WG365739CCB6 06/13/14 20:21CCB U -0.15 0.15mg/L

of 34L18575-1406191513


Inorganic QC

Summary


Iron, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 99.9ICV II140512-2 1.997 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.06 0.06mg/L

WG365235PQV 06/04/14 23:44 103.9PQV II140516-2 .052 70 130mg/L.05007

WG365235SIC 06/04/14 23:47 93.9SIC II140602-1 188.1 1 200mg/L200.33007

WG365235LFB 06/04/14 23:53 102.2LFB II140530-2 1.023 85 115mg/L1.0014

L18575-02AS 06/05/14 0:09 U 102.5AS II140530-2 1.026 85 115mg/L1.0014

L18575-02ASD 06/05/14 0:12 U 103.1ASD II140530-2 1.032 0.5885 115mg/L 201.0014

WG365235CCV1 06/05/14 0:24 99.5CCV II140506-1 .995 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.06 0.06mg/L

WG365235CCV2 06/05/14 1:02 100.7CCV II140506-1 1.007 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.06 0.06mg/L

WG365235CCV3 06/05/14 1:25 100CCV II140506-1 1 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.06 0.06mg/L

Lead, dissolved M200.8 ICP-MS


WG365728

WG365728ICV 06/12/14 9:45 101.4ICV MS140513-1 .05069 90 110mg/L.05

WG365728ICB 06/12/14 9:48ICB U -0.0003 0.0003mg/L

WG365728LFB 06/12/14 9:52 97.4LFB MS140513-3 .04877 85 115mg/L.05005

WG365728CCV1 06/12/14 10:21 102.8CCV MS140513-2 .2573 90 110mg/L.25025

WG365728CCB1 06/12/14 10:24CCB U -0.0003 0.0003mg/L

L18575-03AS 06/12/14 10:50 U 100.1AS MS140513-3 .05008 70 130mg/L.05005

L18575-03ASD 06/12/14 10:53 U 101ASD MS140513-3 .05054 0.9170 130mg/L 20.05005

WG365728CCV2 06/12/14 11:00 102.3CCV MS140513-2 .256 90 110mg/L.25025

WG365728CCB2 06/12/14 11:03CCB U -0.0003 0.0003mg/L

WG365728CCV3 06/12/14 11:26 101.5CCV MS140513-2 .254 90 110mg/L.25025

WG365728CCB3 06/12/14 11:29CCB .00011 -0.0003 0.0003mg/L

Magnesium, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 97.5ICV II140512-2 97.49 95 105mg/L100

WG365235ICB 06/04/14 23:41ICB U -0.6 0.6mg/L

WG365235PQV 06/04/14 23:44 106.9PQV II140516-2 1.07 70 130mg/L1.0007

WG365235SIC 06/04/14 23:47 99.5SIC II140602-1 200.2 1 200mg/L201.1407

WG365235LFB 06/04/14 23:53 98.9LFB II140530-2 49.47 85 115mg/L50.00131

L18575-02AS 06/05/14 0:09 50.8 97.1AS II140530-2 99.34 85 115mg/L50.00131

L18575-02ASD 06/05/14 0:12 50.8 98.8ASD II140530-2 100.2 0.8685 115mg/L 2050.00131

WG365235CCV1 06/05/14 0:24 94.8CCV II140506-1 47.42 90 110mg/L50

WG365235CCB1 06/05/14 0:27CCB U -0.6 0.6mg/L

WG365235CCV2 06/05/14 1:02 96.4CCV II140506-1 48.2 90 110mg/L50

WG365235CCB2 06/05/14 1:05CCB U -0.6 0.6mg/L

WG365235CCV3 06/05/14 1:25 95.2CCV II140506-1 47.61 90 110mg/L50

WG365235CCB3 06/05/14 1:28CCB U -0.6 0.6mg/L

of 34L18575-1406191513


Inorganic QC

Summary


Manganese, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 99.3ICV II140512-2 1.9858 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.015 0.015mg/L

WG365235PQV 06/04/14 23:44 86.8PQV II140516-2 .0217 70 130mg/L.025

WG365235SIC 06/04/14 23:47 96.7SIC II140602-1 48.48 1 200mg/L50.125

WG365235LFB 06/04/14 23:53 102LFB II140530-2 .5108 85 115mg/L.501

L18575-02AS 06/05/14 0:09 U 101.8AS II140530-2 .5102 85 115mg/L.501

L18575-02ASD 06/05/14 0:12 U 102.5ASD II140530-2 .5133 0.6185 115mg/L 20.501

WG365235CCV1 06/05/14 0:24 98.7CCV II140506-1 .9868 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.015 0.015mg/L

WG365235CCV2 06/05/14 1:02 100.7CCV II140506-1 1.007 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.015 0.015mg/L

WG365235CCV3 06/05/14 1:25 99.4CCV II140506-1 .9943 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.015 0.015mg/L

Mercury, dissolved M245.1 CVAA


WG365576

WG365576ICV 06/11/14 11:09 98.3ICV II140530-5 .00492 95 105mg/L.005005

WG365576ICB 06/11/14 11:11ICB U -0.0002 0.0002mg/L

WG365605

WG365605CCV1 06/11/14 13:03 96.3CCV II140530-5 .00482 90 110mg/L.005005

WG365605CCB1 06/11/14 13:05CCB U -0.0002 0.0002mg/L

WG365605LRB 06/11/14 13:07LRB U -0.00044 0.00044mg/L

WG365605LFB 06/11/14 13:10 95.4LFB II140520-4 .00191 85 115mg/L.002002

L18575-03LFM 06/11/14 13:19 U 95.4LFM II140520-4 .00191 85 115mg/L.002002

L18575-03LFMD 06/11/14 13:20 U 91.9LFMD II140520-4 .00184 3.7385 115mg/L 20.002002

WG365605CCV2 06/11/14 13:30 94.3CCV II140530-5 .00472 90 110mg/L.005005

WG365605CCB2 06/11/14 13:33CCB U -0.0002 0.0002mg/L

WG365605CCV3 06/11/14 13:56 94.7CCV II140530-5 .00474 90 110mg/L.005005

WG365605CCB3 06/11/14 13:58CCB U -0.0002 0.0002mg/L

WG365605CCV4 06/11/14 14:13 93.3CCV II140530-5 .00467 90 110mg/L.005005

WG365605CCB4 06/11/14 14:16CCB U -0.0002 0.0002mg/L

of 34L18575-1406191513


Inorganic QC

Summary


Molybdenum, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 101.5ICV II140512-2 2.03 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.06 0.06mg/L

WG365235PQV 06/04/14 23:44 102PQV II140516-2 .102 70 130mg/L.1

WG365235SIC 06/04/14 23:47 90SIC II140602-1 .09 80 120mg/L.1

WG365235LFB 06/04/14 23:53 102.1LFB II140530-2 .51 85 115mg/L.4995

L18575-02AS 06/05/14 0:09 .02 102.5AS II140530-2 .532 85 115mg/L.4995

L18575-02ASD 06/05/14 0:12 .02 103.5ASD II140530-2 .537 0.9485 115mg/L 20.4995

WG365235CCV1 06/05/14 0:24 99.9CCV II140506-1 .999 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.06 0.06mg/L

WG365235CCV2 06/05/14 1:02 101.4CCV II140506-1 1.014 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.06 0.06mg/L

WG365235CCV3 06/05/14 1:25 100.6CCV II140506-1 1.006 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.06 0.06mg/L

Nickel, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 98.3ICV II140512-2 1.9658 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.024 0.024mg/L

WG365235PQV 06/04/14 23:44 111.3PQV II140516-2 .0445 70 130mg/L.04

WG365235SIC 06/04/14 23:47 98.8SIC II140602-1 .0988 80 120mg/L.1

WG365235LFB 06/04/14 23:53 102.2LFB II140530-2 .5108 85 115mg/L.5

L18575-02AS 06/05/14 0:09 U 101.1AS II140530-2 .5056 85 115mg/L.5

L18575-02ASD 06/05/14 0:12 U 101.3ASD II140530-2 .5067 0.2285 115mg/L 20.5

WG365235CCV1 06/05/14 0:24 98.7CCV II140506-1 .987 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.024 0.024mg/L

WG365235CCV2 06/05/14 1:02 99.7CCV II140506-1 .9972 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.024 0.024mg/L

WG365235CCV3 06/05/14 1:25 98.8CCV II140506-1 .9879 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.024 0.024mg/L

Nitrate/Nitrite as N M353.2 - H2SO4 preserved


WG365897

WG365897ICV 06/14/14 14:33 97.9ICV WI140417-3 2.365 90 110mg/L2.416

WG365897ICB 06/14/14 14:34ICB U -0.06 0.06mg/L

WG365897LFB 06/14/14 14:38 98.8LFB WI140215-3 1.976 90 110mg/L2

L18557-01AS 06/14/14 14:40 U 98.5AS WI140215-3 1.969 90 110mg/L2

L18557-02DUP RA06/14/14 14:43 .04DUP U 200mg/L 20

WG365897CCV1 06/14/14 14:47 99.7CCV WI140607-1 1.993 90 110mg/L2

WG365897CCB1 06/14/14 14:48CCB U -0.06 0.06mg/L

WG365897CCV2 06/14/14 15:01 101.2CCV WI140607-1 2.023 90 110mg/L2

WG365897CCB2 06/14/14 15:02CCB U -0.06 0.06mg/L

WG365897CCV4 06/14/14 15:43 93.7CCV WI140607-1 1.874 90 110mg/L2

WG365897CCB4 06/14/14 15:45CCB .052 -0.06 0.06mg/L

WG365897CCV5 06/14/14 15:56 95.5CCV WI140607-1 1.909 90 110mg/L2

WG365897CCB5 06/14/14 15:58CCB U -0.06 0.06mg/L

of 34L18575-1406191513


Inorganic QC

Summary


Nitrogen, ammonia M350.1 - Automated Phenate


WG365862

WG365862ICV 06/13/14 15:27 104.1ICV WI131021-1 1.044 90 110mg/L1.003

WG365862ICB 06/13/14 15:30ICB U -0.15 0.15mg/L

WG365862LFB1 06/13/14 15:32 98.3LFB WI140113-8 .983 90 110mg/L1

L18575-01AS 06/13/14 15:34 U 95.4AS WI140113-8 .954 90 110mg/L1

L18575-02DUP RA06/13/14 15:36 UDUP U 0mg/L 20

WG365862CCV1 06/13/14 15:42 98.6CCV WI140113-6 1.971 90 110mg/L2

WG365862CCB1 06/13/14 15:44CCB U -0.15 0.15mg/L

WG365862CCV2 06/13/14 15:55 96.4CCV WI140113-6 1.928 90 110mg/L2

WG365862CCB2 06/13/14 15:57CCB U -0.15 0.15mg/L

WG365862LFB2 06/13/14 16:03 96.4LFB WI140113-8 .964 90 110mg/L1

WG365862CCV3 06/13/14 16:09 98.3CCV WI140113-6 1.965 90 110mg/L2

WG365862CCB3 06/13/14 16:10CCB U -0.15 0.15mg/L

WG365862CCV4 06/13/14 16:22 97.5CCV WI140113-6 1.949 90 110mg/L2

WG365862CCB4 06/13/14 16:23CCB U -0.15 0.15mg/L

WG365862CCV5 06/13/14 16:27 99.2CCV WI140113-6 1.984 90 110mg/L2

WG365862CCB5 06/13/14 16:28CCB U -0.15 0.15mg/L

WG365862CCV6 06/13/14 17:04 94.6CCV WI140113-6 1.892 90 110mg/L2

WG365862CCB6 06/13/14 17:05CCB U -0.15 0.15mg/L

WG365862CCV7 06/13/14 17:11 95.8CCV WI140113-6 1.916 90 110mg/L2

WG365862CCB7 06/13/14 17:12CCB U -0.15 0.15mg/L

Potassium, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 98.4ICV II140512-2 19.68 95 105mg/L20

WG365235ICB 06/04/14 23:41ICB U -0.6 0.6mg/L

WG365235PQV 06/04/14 23:44 113PQV II140516-2 1.13 70 130mg/L1

WG365235SIC 06/04/14 23:47 111SIC II140602-1 1.11 80 120mg/L1

WG365235LFB 06/04/14 23:53 100.7LFB II140530-2 100.7 85 115mg/L99.99364

L18575-02AS 06/05/14 0:09 15.8 101.8AS II140530-2 117.6 85 115mg/L99.99364

L18575-02ASD 06/05/14 0:12 15.8 101.8ASD II140530-2 117.6 085 115mg/L 2099.99364

WG365235CCV1 06/05/14 0:24 97.7CCV II140506-1 9.77 90 110mg/L10

WG365235CCB1 06/05/14 0:27CCB U -0.6 0.6mg/L

WG365235CCV2 06/05/14 1:02 98.9CCV II140506-1 9.89 90 110mg/L10

WG365235CCB2 06/05/14 1:05CCB U -0.6 0.6mg/L

WG365235CCV3 06/05/14 1:25 99.4CCV II140506-1 9.94 90 110mg/L10

WG365235CCB3 06/05/14 1:28CCB U -0.6 0.6mg/L

Residue, Filterable (TDS) @180C SM2540C


WG364992

WG364992PBW 06/02/14 12:44PBW U -20 20mg/L

WG364992LCSW 06/02/14 12:46 96.2LCSW PCN45839 250 80 120mg/L260

L18606-04DUP RA06/02/14 13:30 30DUP 36 18.2mg/L 10

of 34L18575-1406191513


Inorganic QC

Summary


Residue, Non-Filterable (TSS) @105C SM2540D


WG364983

WG364983PBW 06/02/14 11:27PBW U -15 15mg/L


L18593-04DUP RA06/02/14 12:06 UDUP U 0mg/L 10

Selenium, dissolved M200.8 ICP-MS


WG365728

WG365728ICV 06/12/14 9:45 103.5ICV MS140513-1 .05176 90 110mg/L.05

WG365728ICB 06/12/14 9:48ICB U -0.0003 0.0003mg/L

WG365728LFB 06/12/14 9:52 101.7LFB MS140513-3 .05089 85 115mg/L.05005

WG365728CCV1 06/12/14 10:21 102.7CCV MS140513-2 .2571 90 110mg/L.25025

WG365728CCB1 06/12/14 10:24CCB U -0.0003 0.0003mg/L

L18575-03AS 06/12/14 10:50 .0225 107.4AS MS140513-3 .07623 70 130mg/L.05005

L18575-03ASD 06/12/14 10:53 .0225 109.2ASD MS140513-3 .07717 1.2370 130mg/L 20.05005

WG365728CCV2 06/12/14 11:00 98CCV MS140513-2 .2452 90 110mg/L.25025

WG365728CCB2 06/12/14 11:03CCB .00012 -0.0003 0.0003mg/L

WG365728CCV3 06/12/14 11:26 98.7CCV MS140513-2 .2471 90 110mg/L.25025

WG365728CCB3 06/12/14 11:29CCB .00013 -0.0003 0.0003mg/L

Silica, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 100.3ICV II140512-2 42.91 95 105mg/L42.8

WG365235ICB 06/04/14 23:41ICB U -0.6 0.6mg/L

WG365235PQV 06/04/14 23:44 97.1PQV II140516-2 1.04 70 130mg/L1.0714

WG365235SIC 06/04/14 23:47 84SIC II140602-1 .9 80 120mg/L1.0714

WG365235LFB 06/04/14 23:53 106.1LFB II140530-2 22.73 85 115mg/L21.428

L18575-02AS 06/05/14 0:09 14.5 104.1AS II140530-2 36.81 85 115mg/L21.428

L18575-02ASD 06/05/14 0:12 14.5 105.1ASD II140530-2 37.02 0.5785 115mg/L 2021.428

WG365235CCV1 06/05/14 0:24 98.9CCV II140506-1 21.17 90 110mg/L21.4

WG365235CCB1 06/05/14 0:27CCB U -0.6 0.6mg/L

WG365235CCV2 06/05/14 1:02 100.7CCV II140506-1 21.55 90 110mg/L21.4

WG365235CCB2 06/05/14 1:05CCB U -0.6 0.6mg/L

WG365235CCV3 06/05/14 1:25 99.8CCV II140506-1 21.35 90 110mg/L21.4

WG365235CCB3 06/05/14 1:28CCB U -0.6 0.6mg/L

of 34L18575-1406191513


Inorganic QC

Summary


Sodium, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 99.4ICV II140512-2 99.39 95 105mg/L100

WG365235ICB 06/04/14 23:41ICB U -0.6 0.6mg/L

WG365235PQV 06/04/14 23:44 104.9PQV II140516-2 1.05 70 130mg/L1.001

WG365235SIC 06/04/14 23:47 105.9SIC II140602-1 1.06 80 120mg/L1.001

WG365235LFB 06/04/14 23:53 101.4LFB II140530-2 101.4 85 115mg/L100.0393

L18575-02AS 06/05/14 0:09 80.8 98.3AS II140530-2 179.1 85 115mg/L100.0393

L18575-02ASD 06/05/14 0:12 80.8 100.3ASD II140530-2 181.1 1.1185 115mg/L 20100.0393

WG365235CCV1 06/05/14 0:24 98.1CCV II140506-1 49.07 90 110mg/L50

WG365235CCB1 06/05/14 0:27CCB U -0.6 0.6mg/L

WG365235CCV2 06/05/14 1:02 99.1CCV II140506-1 49.57 90 110mg/L50

WG365235CCB2 06/05/14 1:05CCB U -0.6 0.6mg/L

WG365235CCV3 06/05/14 1:25 99.6CCV II140506-1 49.82 90 110mg/L50

WG365235CCB3 06/05/14 1:28CCB U -0.6 0.6mg/L

Sulfate SM4500 SO4-D


WG365469

WG365469PBW 06/09/14 9:35PBW U -30 30mg/L

WG365469LCSW 06/09/14 9:36 102LCSW WC131004- 102 80 120mg/L100

L18650-04DUP 06/09/14 9:58 930DUP 934 0.4mg/L 20

WG365730

WG365730PBW 06/12/14 13:50PBW U -30 30mg/L


L18697-02DUP 06/12/14 14:16 140DUP 133 5.1mg/L 20

Sulfide as S SM4500S2-D


WG365076

WG365076ICV 06/03/14 10:55 99.7ICV WC140603- .307 90 110mg/L.308

WG365076ICB 06/03/14 11:02ICB U -0.06 0.06mg/L

WG365076LFB 06/03/14 11:09 119.6LFB WC140603- .253 80 120mg/L.21156

WG365076CCV1 06/03/14 12:24 109.7CCV WC140603- .174 90 110mg/L.15867

WG365076CCB1 06/03/14 12:32CCB U -0.06 0.06mg/L

L18580-01AS 06/03/14 12:47 U 123.8AS WC140603- .262 75 125mg/L.21156

L18580-01DUP RA06/03/14 12:54 UDUP U 0mg/L 20

WG365076CCV2 06/03/14 13:54 107.1CCV WC140603- .17 90 110mg/L.15867

WG365076CCB2 06/03/14 14:01CCB U -0.06 0.06mg/L

WG365076CCV3 06/03/14 14:46 105.2CCV WC140603- .167 90 110mg/L.15867

WG365076CCB3 06/03/14 14:53CCB U -0.06 0.06mg/L

of 34L18575-1406191513


Inorganic QC

Summary


Uranium, dissolved M200.8 ICP-MS


WG365728

WG365728ICV 06/12/14 9:45 104.9ICV MS140513-1 .05244 90 110mg/L.05

WG365728ICB 06/12/14 9:48ICB U -0.0003 0.0003mg/L

WG365728LFB 06/12/14 9:52 103.8LFB MS140513-3 .0519 85 115mg/L.05

WG365728CCV1 06/12/14 10:21 109.8CCV MS140513-2 .1098 90 110mg/L.1

WG365728CCB1 BB BE06/12/14 10:24CCB .00093 -0.0003 0.0003mg/L

L18575-03AS 06/12/14 10:50 .057 100.8AS MS140513-3 .1074 70 130mg/L.05

L18575-03ASD 06/12/14 10:53 .057 102ASD MS140513-3 .108 0.5670 130mg/L 20.05

WG365728CCV2 06/12/14 11:00 102.7CCV MS140513-2 .1027 90 110mg/L.1

WG365728CCB2 BB06/12/14 11:03CCB .00143 -0.0003 0.0003mg/L

Vanadium, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 100.7ICV II140512-2 2.0132 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.015 0.015mg/L

WG365235PQV 06/04/14 23:44 100.8PQV II140516-2 .0252 70 130mg/L.025

WG365235SIC 06/04/14 23:47 95.1SIC II140602-1 .0951 80 120mg/L.1

WG365235LFB 06/04/14 23:53 102.9LFB II140530-2 .5146 85 115mg/L.5

L18575-02AS 06/05/14 0:09 .016 104.1AS II140530-2 .5365 85 115mg/L.5

L18575-02ASD 06/05/14 0:12 .016 104.4ASD II140530-2 .5381 0.385 115mg/L 20.5

WG365235CCV1 06/05/14 0:24 99.7CCV II140506-1 .9974 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.015 0.015mg/L

WG365235CCV2 06/05/14 1:02 100.8CCV II140506-1 1.008 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.015 0.015mg/L

WG365235CCV3 06/05/14 1:25 100.6CCV II140506-1 1.006 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.015 0.015mg/L

Zinc, dissolved M200.7 ICP


WG365235

WG365235ICV 06/04/14 23:35 97.8ICV II140512-2 1.955 95 105mg/L2

WG365235ICB 06/04/14 23:41ICB U -0.03 0.03mg/L

WG365235PQV 06/04/14 23:44 100PQV II140516-2 .05 70 130mg/L.05

WG365235SIC 06/04/14 23:47 94SIC II140602-1 .094 80 120mg/L.1

WG365235LFB 06/04/14 23:53 103.1LFB II140530-2 .516 85 115mg/L.5005

L18575-02AS 06/05/14 0:09 U 102.9AS II140530-2 .515 85 115mg/L.5005

L18575-02ASD 06/05/14 0:12 U 103.3ASD II140530-2 .517 0.3985 115mg/L 20.5005

WG365235CCV1 06/05/14 0:24 98.1CCV II140506-1 .981 90 110mg/L1

WG365235CCB1 06/05/14 0:27CCB U -0.03 0.03mg/L

WG365235CCV2 06/05/14 1:02 99.6CCV II140506-1 .996 90 110mg/L1

WG365235CCB2 06/05/14 1:05CCB U -0.03 0.03mg/L

WG365235CCV3 06/05/14 1:25 97.6CCV II140506-1 .976 90 110mg/L1

WG365235CCB3 06/05/14 1:28CCB U -0.03 0.03mg/L

of 34L18575-1406191513


Inorganic Extended

Qualifier Report


ACZ ID PARAMETER QUAL DESCRIPTIONMETHODWORKNUM

BB Target analyte detected in calibration blank at or above acceptance limit. Sample value was > 10X the concentration in the calibration blank.

M200.8 ICP-MSUranium, dissolvedL18575-01 WG365728

RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 10x MDL).

SM5310BCarbon, total organic (TOC)WG365699

M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level. The recovery of the associated control sample (LCS or LFB) was acceptable.

SM4500Cl-EChlorideWG365759


SM4500F-CFluorideWG365739


M353.2 - H2SO4 preservedNitrate/Nitrite as NWG365897


M350.1 - Automated PhenateNitrogen, ammoniaWG365862


SM2540CResidue, Filterable (TDS) @180CWG364992


SM2540DResidue, Non-Filterable (TSS) @105CWG364983


SM4500S2-DSulfide as SWG365076



















REPAD.15.06.05.01

of 34L18575-1406191513


Inorganic Extended

Qualifier Report





















REPAD.15.06.05.01

of 34L18575-1406191513





Project ID:


Date Sampled: 05/27/14 15:50


Locator:

RadioChemistry

Analytical Results

Gross Alpha & Beta, dissolved

M900.0

Prep Method:

Parameter Result LLDError(+/-) Units XQMeasure Date Prep Date Analyst

Gross Alpha 25 9.3 5.3 pCi/L bsg06/09/14 0:00

Gross Beta 24 8.6 11 pCi/L bsg06/09/14 0:00

Lead 210, dissolved

EICHROM, OTW01

Prep Method:


Lead 210, dissolved -0.43 2 5 pCi/L * thf06/18/14 10:22

Radium 226, dissolved

M903.1

Prep Method:


Radium 226, dissolved 0.2 0.09 0.22 pCi/L * nco06/11/14 10:45


M904.0

Prep Method:


Radium 228, dissolved 0.74 0.63 0.62 pCi/L jrd06/10/14 16:21

Thorium 230, dissolved

ESM 4506

Prep Method:


Thorium 230, dissolved 0.36 0.3 0.55 pCi/L * nco06/10/14 10:34

REPRC.02.06.05.01 * Please refer to Qualifier Reports for details.

of 34L18575-1406191513





Project ID:


Date Sampled: 05/27/14 10:30


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 21 5.8 2.6 pCi/L bsg06/09/14 0:00

Gross Beta 27 5 5.5 pCi/L bsg06/09/14 0:00

Lead 210, dissolved

EICHROM, OTW01

Prep Method:


Lead 210, dissolved -5.6 1.7 4.8 pCi/L * thf06/18/14 10:22


M903.1

Prep Method:


Radium 226, dissolved 53 1.1 0.11 pCi/L * nco06/11/14 10:47


M904.0

Prep Method:


Radium 228, dissolved -0.14 0.53 0.59 pCi/L jrd06/10/14 16:21


ESM 4506

Prep Method:


Thorium 230, dissolved -0.13 0.32 0.56 pCi/L * nco06/10/14 10:36


of 34L18575-1406191513





Project ID:


Date Sampled: 05/27/14 10:30


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 22 6 2.6 pCi/L bsg06/09/14 0:00

Gross Beta 24 5.1 5.4 pCi/L bsg06/09/14 0:00

Lead 210, dissolved

EICHROM, OTW01

Prep Method:


Lead 210, dissolved 0.48 1.8 4.5 pCi/L * thf06/18/14 10:22


M903.1

Prep Method:




M904.0

Prep Method:




ESM 4506

Prep Method:




of 34L18575-1406191513




Error(+/-) Calculated sample specific uncertainty



LCL Lower Control Limit, in % (except for LCSS, mg/Kg)

LLD Calculated sample specific Lower Limit of Detection


PQL Practical Quantitation Limit


Rec Amount of the true value or spike added recovered, in % (except for LCSS, mg/Kg)

RER Relative Error Ratio, calculation used for Dup. QC taking into account the error factor.


UCL Upper Control Limit, in % (except for LCSS, mg/Kg)


QC Sample Types

DUP Sample Duplicate MS/MSD Matrix Spike/Matrix Spike Duplicate

LCSS Laboratory Control Sample - Soil PBS Prep Blank - Soil

LCSW Laboratory Control Sample - Water PBW Prep Blank - Water


Blanks Verifies that there is no or minimal contamination in the prep method procedure.



Matrix Spikes Determines sample matrix interferences, if any.


H Analysis exceeded method hold time.

Method Prefix Reference

M EPA methodology, including those under SDWA, CWA, and RCRA

SM Standard Methods for the Examination of Water and Wastewater.

D ASTM

RP DOE

ESM DOE/ESM

Comments

(1) Solid matrices are reported on a dry weight basis.

(2) Preparation method: "Method" indicates preparation defined in analytical method.


(4) An asterisk in the "XQ" column indicates there is an extended qualifier and/or certification

qualifier associated with the result.


REP003.09.12.01

Radiochemistry

Reference

of 34L18575-1406191513


Radiochemistry QC

Summary


Alpha M900.0

ACZ ID Analyzed RecSample QualLower UpperQC FoundType ErrorPCN/SCN LimitRPD/RER

pCi/L

Error LLDLLD

Units:

WG365559

L18559-01MSA 06/09/14 1.5 93.5MS PCN45467 95100 83 1339.22 1.71.7

L18594-01DUP 06/09/14 21DUP-RER 14 24.8 0.875.2 2.32.2

WG365056LCSWA 06/09/14 123LCSW PCN45467 8266.67 83 1336.5 1

WG365056PBW 06/09/14PBW .13 21 1

L18558-01DUP 06/09/14 0.29DUP-RER .97 21.8 0.161.6 1.71.7

Beta M900.0


pCi/L

Error LLDLLD

Units:

WG365559

L18558-01DUP 06/09/14 2.2DUP-RER 4.1 23.5 0.733.2 4.64.6

L18558-01MSB 06/09/14 2.2 117.8MS PCN44647 120100 70 1297.93.2 4.64.6

L18594-01DUP 06/09/14 7.9DUP-RER 13 24.3 0.263.6 4.94.8

WG365056LCSWB 06/09/14 115.5LCSW PCN44647 7766.67 70 1294.9 2.9

WG365056PBW 06/09/14PBW .6 6.22.2 3.1

Lead 210, dissolved EICHROM, OTW01


pCi/L

Error LLDLLD

Units:

WG366164

WG365479PBW 06/18/14PBW -.06 8.41.6 4.2

WG365479LCSW 06/18/14 85.7LCSW PCN44154 8498 55 1213.7 4.7

L18578-01DUP 06/18/14 1.2DUP-RER -1.2 21.5 1.091.6 3.84.1

L18575-02MS 06/18/14 -5.6 86.3MS PCN44154 7998 55 1213.41.7 4.24.8

L18575-01DUP 06/18/14 -0.43DUP-RER -.81 21.7 0.142 4.45

of 34L18575-1406191513


Radiochemistry QC

Summary


Radium 226, dissolved M903.1


pCi/L

Error LLDLLD

Units:

WG365735

WG365305PBW 06/11/14PBW .1 0.30.12 0.15

WG365305LCSW 06/11/14 100LCSW PCN45817 2020 43 1480.61 0.24

L18570-01DUP RN06/11/14 130DUP-RER 140 21.8 4.151.6 0.380.15

L18570-01DUP 06/11/14 130DUP-RPD 140 201.81.6 0.380.15 7.4

L18570-02MS M306/11/14 640 850MS PCN45817 81020 43 1484.34 0.260.5



pCi/L

Error LLDLLD

Units:

WG365666

WG365138LCSW 06/10/14 80.6LCSW PCN44320 1518.61 47 1231.5 0.74

L18579-02MS 06/10/14 1.7 71.5MS PCN44320 1518.61 47 1231.40.84 0.760.79

L18579-01DUP 06/10/14 1.9DUP-RER 1.8 20.84 0.090.76 0.780.68

WG365138PBW 06/10/14PBW -.1 1.20.55 0.6

Thorium 230, dissolved ESM 4506


pCi/L

Error LLDLLD

Units:

WG365652

WG365080PBW 06/10/14PBW .37 1.020.27 0.51

WG365080LCSW 06/10/14 98.7LCSW RC130807-2 160162.12 91 1264.1 0.55

L18575-01DUP 06/10/14 0.36DUP-RER .15 20.28 0.510.3 0.550.55

L18578-01DUP 06/10/14 0.19DUP-RER .29 20.55 0.170.24 0.540.56

L18575-03MS 06/10/14 0.3 98.5MS RC130807-2 160162.12 91 1264.30.31 0.550.58

of 34L18575-1406191513


RadChem Extended

Qualifier Report




M903.1Radium 226, dissolvedL18575-01 WG365735

RN Sample concentration is greater than 5x LLD; RPD was used for data validation. Replicate Error Ratio (RER) is greater than 2. Precision judged to be in control.

M903.1




M903.1




M903.1

REPAD.15.06.05.01

of 34L18575-1406191513


Certification

Qualifiers


Metals Analysis

The following parameters are not offered for certification or are not covered by NELAC certificate #ACZ.


Radiochemistry




Wet Chemistry



REPAD.05.06.05.01

of 34L18575-1406191513


Sample

Receipt

Energy Fuels Resources (USA) Inc. ACZ Project ID:

Date Received:

Received By: mtb

05/30/2014 10:44

L18575

Date Printed: 5/30/2014

Chain of Custody Related Remarks

Client Contact Remarks

NANOYES

X

X

X

X

X

1) Is a foreign soil permit included for applicable samples?

2) Is the Chain of Custody or other directive shipping papers present?

3) Does this project require special handling procedures such as CLP protocol?

4) Are any samples NRC licensable material?

5) If samples are received past hold time, proceed with requested short hold time analyses?

6) Is the Chain of Custody complete and accurate?

7) Were any changes made to the Chain of Custody prior to ACZ receiving the samples?

Receipt Verification

NANOYES

X

X

X

X

X

X

X

X9) Are all containers intact and with no leaks?

10) Are all labels on containers and are they intact and legible?

11) Do the sample labels and Chain of Custody match for Sample ID, Date, and Time?

12) For preserved bottle types, was the pH checked and within limits?

13) Is there sufficient sample volume to perform all requested work?

14) Is the custody seal intact on all containers?

15) Are samples that require zero headspace acceptable?

16) Are all sample containers appropriate for analytical requirements?

17) Is there an Hg-1631 trip blank present?

18) Is there a VOA trip blank present?

19) Were all samples received within hold time?

Samples/Containers

X

X

X

X

Shipping Containers

A change was made in the invoice to section prior to ACZ custody.

Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- --------------------2714 5 12 Yes4149 5.7 12 Yes

X

Was ice present in the shipment container(s)?

Yes - Wet ice was present in the shipment container(s).

X8) Is the sampler attestation statement signed?

REPAD LPII 2012-03

of 34L18575-1406191513


Sample

Receipt


Date Received:

Received By: mtb

05/30/2014 10:44

L18575


Client must contact an ACZ Project Manager if analysis should not proceed for samples received outside of their thermal preservation acceptance criteria.

REPAD LPII 2012-03

of 34L18575-1406191513

of 34L18575-1406191513


Analytical

Report



Lakewood, CO 80228


Kathy Weinel:

Enclosed are the analytical results for sample(s) submitted to ACZ Laboratories, Inc. (ACZ) on June 06, 2014. This project has been assigned to ACZ's project number, L18718. Please reference this number in all future inquiries.






Kathy Weinel

June 30, 2014

Project ID:



Lakewood, CO 80228

Accounts Payable

Report to: Bill to:

Page 1 of 27L18718-1406301328


Sample ID: PW3



Project ID:



Results

Date Sampled: 06/03/14 13:20



Metals Analysis

XQDilution

Aluminum, dissolved M200.7 ICP mg/L 0.2U jjc0.03 06/10/14 23:361

Arsenic, dissolved M200.8 ICP- MS 0.0109 mg/L 0.001 msh0.0002 06/23/14 18:051

Barium, dissolved M200.7 ICP 0.008 mg/L 0.02B jjc0.003 06/10/14 23:361

Boron, dissolved M200.7 ICP 0.36 mg/L 0.05 jjc0.01 06/10/14 23:361

Cadmium, dissolved M200.8 ICP- MS mg/L 0.0005U msh0.0001 06/23/14 18:051

Calcium, dissolved M200.7 ICP 66.9 mg/L 0.5 jjc0.1 06/10/14 23:361

Cesium, dissolved M200.8 ICP- MS mg/L 0.001U msh0.0002* 06/23/14 18:051

Chromium, dissolved M200.7 ICP mg/L 0.05U jjc0.01 06/10/14 23:361

Copper, dissolved M200.7 ICP mg/L 0.05U jjc0.01 06/10/14 23:361

Iron, dissolved M200.7 ICP 0.02 mg/L 0.05B jjc0.02 06/10/14 23:361

Lead, dissolved M200.8 ICP- MS mg/L 0.0005U msh0.0001 06/23/14 18:051

Magnesium, dissolved M200.7 ICP 71.6 mg/L 1 jjc0.2 06/10/14 23:361

Manganese, dissolved M200.7 ICP mg/L 0.03U jjc0.005 06/11/14 11:521


Molybdenum, dissolved M200.7 ICP mg/L 0.1U jjc0.02 06/10/14 23:361

Nickel, dissolved M200.7 ICP mg/L 0.04U jjc0.008 06/10/14 23:361

Potassium, dissolved M200.7 ICP 11.7 mg/L 1 jjc0.2 06/10/14 23:361

Selenium, dissolved M200.8 ICP- MS 0.0164 mg/L 0.0003 msh0.0001 06/23/14 18:051

Silica, dissolved M200.7 ICP 15.9 mg/L 1 jjc0.2 06/10/14 23:361

Sodium, dissolved M200.7 ICP 92.7 mg/L 1 jjc0.2 06/10/14 23:361

Uranium, dissolved M200.8 ICP- MS 0.0753 mg/L 0.0005 msh0.0001 06/23/14 18:051

Vanadium, dissolved M200.7 ICP 0.018 mg/L 0.03B jjc0.005 06/10/14 23:361

Zinc, dissolved M200.7 ICP mg/L 0.05U jjc0.01 06/10/14 23:361

REPIN.02.06.05.01 * P lease refer to Qualifier Reports for details.

Page 2 of 27L18718-1406301328


Sample ID: PW3



Project ID:



Results

Date Sampled: 06/03/14 13:20



Wet Chemistry

XQDilution



277 mg/L 20 abd2 06/14/14 0:001

Carbonate as CaCO3 mg/L 20U abd2 06/14/14 0:001

Hydroxide as CaCO3 mg/L 20U abd2 06/14/14 0:001

Total Alkalinity 277 mg/L 20 abd2 06/14/14 0:001


SM5310B mg/L 5U mpb1* 06/18/14 23:091

Cation- Anion Balance Calculation

Cation- Anion Balance - 3.5 % calc06/30/14 11:50

Sum of Anions 14.6 meq/L calc06/30/14 11:50

Sum of Cations 13.6 meq/L calc06/30/14 11:50

Chloride SM4500Cl- E 37.8 mg/L 2 mpb0.5 06/20/14 10:131

Fluoride SM4500F- C 0.52 mg/L 0.3 abd0.05 06/19/14 12:291




SM2540C 850 mg/L 20 nml10* 06/09/14 3:421


SM2540D mg/L 20U nml5* 06/06/14 12:251

Sulfate SM4500 SO4- D 380 mg/L 50 eaa10 06/12/14 14:181

Sulfide as S SM4500S2- D mg/L 0.1U enb0.02* 06/10/14 11:351

TDS (calculated) Calculation 850 mg/L calc06/30/14 11:50




Page 3 of 27L18718-1406301328








P CN/SCN A number assigned to reagents/standards to trace to the manufacturer's certificate of analysis

P QL Practical Quantitation Limit, typically 5 times the MDL.



RP D Relative Percent Difference, calculation used for Duplicate QC Types



QC Sample Types








ICSAB Inter-element Correction Standard - A plus B solutions P BS Prep Blank - Soil

LCSS Laboratory Control Sample - Soil P BW Prep Blank - Water

LCSSD Laboratory Control Sample - Soil Duplicate P QV Practical Quantitation Verification standard














Method References






Comments








REP001.09.12.01

Inorganic

Reference

Page 4 of 27L18718-1406301328


Inorganic QC

Summary




WG365861

WG365861PBW1 06/13/14 15:15PBW 2.4 -20 20mg/L



WG365861PBW2 06/13/14 19:31PBW U -20 20mg/L


WG365861PBW3 06/13/14 22:38PBW 2.3 -20 20mg/L


WG365861PBW4 06/14/14 2:10PBW 2.1 -20 20mg/L

L18722-04DUP 06/14/14 3:41 82DUP 82.8 1mg/L 20


Aluminum, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 98.6ICV II140512-2 1.972 95 105mg/L2

WG365596ICB 06/10/14 23:20ICB U -0.09 0.09mg/L

WG365596PQV 06/10/14 23:24 81.2PQV II140609-2 .122 70 130mg/L.150165

WG365596SIC 06/10/14 23:27 102SIC II140602-1 204.3 1 200mg/L200.370165

WG365596LFB 06/10/14 23:33 102.3LFB II140530-2 1.024 85 115mg/L1.0011

L18718-01AS 06/10/14 23:39 U 106.5AS II140530-2 1.066 85 115mg/L1.0011

L18718-01ASD 06/10/14 23:42 U 105.6ASD II140530-2 1.057 0.8585 115mg/L 201.0011

WG365596CCV1 06/11/14 0:04 98.2CCV II140506-1 .982 90 110mg/L1

WG365596CCB1 06/11/14 0:07CCB U -0.09 0.09mg/L

Arsenic, dissolv ed M200.8 ICP-MS


WG366370

WG366370ICV 06/23/14 17:55 104.7ICV MS140513-1 .05236 90 110mg/L.05

WG366370ICB 06/23/14 17:58ICB U -0.0006 0.0006mg/L

WG366370LFB 06/23/14 18:02 90.2LFB MS140513-3 .0452 85 115mg/L.0501

L18719-01AS 06/23/14 18:11 U 102.4AS MS140513-3 .10256 70 130mg/L.1002

L18719-01ASD 06/23/14 18:15 U 104.6ASD MS140513-3 .10478 2.1470 130mg/L 20.1002

WG366370CCV1 06/23/14 18:31 97.2CCV MS140513-2 .09741 90 110mg/L.1002

WG366370CCB1 06/23/14 18:34CCB .00021 -0.0006 0.0006mg/L

WG366370CCV2 06/23/14 19:10 99.2CCV MS140513-2 .09936 90 110mg/L.1002

WG366370CCB2 06/23/14 19:13CCB U -0.0006 0.0006mg/L

WG366370CCV3 06/23/14 19:36 99.8CCV MS140513-2 .1 90 110mg/L.1002

WG366370CCB3 06/23/14 19:39CCB .00021 -0.0006 0.0006mg/L

Page 5 of 27L18718-1406301328


Inorganic QC

Summary


Barium, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 98.8ICV II140512-2 1.9763 95 105mg/L2

WG365596ICB 06/10/14 23:20ICB U -0.009 0.009mg/L

WG365596PQV 06/10/14 23:24 74.7PQV II140609-2 .0112 70 130mg/L.015

WG365596SIC 06/10/14 23:27 97.9SIC II140602-1 .0979 80 120mg/L.1

WG365596LFB 06/10/14 23:33 98.4LFB II140530-2 .4919 85 115mg/L.5

L18718-01AS 06/10/14 23:39 .008 100AS II140530-2 .5081 85 115mg/L.5

L18718-01ASD 06/10/14 23:42 .008 99.9ASD II140530-2 .5076 0.185 115mg/L 20.5

WG365596CCV1 06/11/14 0:04 100.1CCV II140506-1 1.001 90 110mg/L1

WG365596CCB1 06/11/14 0:07CCB U -0.009 0.009mg/L

WG365596CCV2 06/11/14 0:43 98.8CCV II140506-1 .9877 90 110mg/L1

WG365596CCB2 06/11/14 0:46CCB U -0.009 0.009mg/L

WG365596CCV3 06/11/14 1:05 100.5CCV II140506-1 1.005 90 110mg/L1

WG365596CCB3 06/11/14 1:08CCB U -0.009 0.009mg/L

Boron, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 100.9ICV II140512-2 2.017 95 105mg/L2

WG365596ICB 06/10/14 23:20ICB U -0.03 0.03mg/L

WG365596PQV 06/10/14 23:24 89.9PQV II140609-2 .045 70 130mg/L.05005

WG365596SIC 06/10/14 23:27 90.9SIC II140602-1 .091 80 120mg/L.1001

WG365596LFB 06/10/14 23:33 99.7LFB II140530-2 .499 85 115mg/L.5005

L18718-01AS 06/10/14 23:39 .36 102.5AS II140530-2 .873 85 115mg/L.5005

L18718-01ASD 06/10/14 23:42 .36 101.3ASD II140530-2 .867 0.6985 115mg/L 20.5005

WG365596CCV1 06/11/14 0:04 101.6CCV II140506-1 1.016 90 110mg/L1

WG365596CCB1 06/11/14 0:07CCB U -0.03 0.03mg/L

WG365596CCV2 06/11/14 0:43 101.8CCV II140506-1 1.018 90 110mg/L1

WG365596CCB2 06/11/14 0:46CCB U -0.03 0.03mg/L

WG365596CCV3 06/11/14 1:05 102.3CCV II140506-1 1.023 90 110mg/L1

WG365596CCB3 06/11/14 1:08CCB U -0.03 0.03mg/L

Cadmium, dissolv ed M200.8 ICP-MS


WG366370

WG366370ICV 06/23/14 17:55 99.2ICV MS140513-1 .04961 90 110mg/L.05

WG366370ICB 06/23/14 17:58ICB U -0.0003 0.0003mg/L

WG366370LFB 06/23/14 18:02 99.3LFB MS140513-3 .04975 85 115mg/L.0501

L18719-01AS 06/23/14 18:11 U 101.5AS MS140513-3 .1017 70 130mg/L.1002

L18719-01ASD 06/23/14 18:15 U 103ASD MS140513-3 .1032 1.4670 130mg/L 20.1002

WG366370CCV1 06/23/14 18:31 97.2CCV MS140513-2 .09744 90 110mg/L.1002

WG366370CCB1 06/23/14 18:34CCB U -0.0003 0.0003mg/L

WG366370CCV2 06/23/14 19:10 95.9CCV MS140513-2 .09611 90 110mg/L.1002

WG366370CCB2 06/23/14 19:13CCB U -0.0003 0.0003mg/L

WG366370CCV3 06/23/14 19:36 96.4CCV MS140513-2 .09659 90 110mg/L.1002

WG366370CCB3 06/23/14 19:39CCB U -0.0003 0.0003mg/L

Page 6 of 27L18718-1406301328


Inorganic QC

Summary


Calcium, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 100.1ICV II140512-2 100.11 95 105mg/L100

WG365596ICB 06/10/14 23:20ICB U -0.3 0.3mg/L

WG365596PQV 06/10/14 23:24 94PQV II140609-2 .47 70 130mg/L.5002

WG365596SIC 06/10/14 23:27 99SIC II140602-1 198.4 1 200mg/L200.5002

WG365596LFB 06/10/14 23:33 105.5LFB II140530-2 71.69 85 115mg/L67.98099

L18718-01AS 06/10/14 23:39 66.9 105AS II140530-2 138.3 85 115mg/L67.98099

L18718-01ASD 06/10/14 23:42 66.9 103.4ASD II140530-2 137.2 0.885 115mg/L 2067.98099

WG365596CCV1 06/11/14 0:04 100.7CCV II140506-1 50.35 90 110mg/L50

WG365596CCB1 06/11/14 0:07CCB U -0.3 0.3mg/L

WG365596CCV2 06/11/14 0:43 99.8CCV II140506-1 49.9 90 110mg/L50

WG365596CCB2 06/11/14 0:46CCB U -0.3 0.3mg/L

WG365596CCV3 06/11/14 1:05 100.2CCV II140506-1 50.12 90 110mg/L50

WG365596CCB3 06/11/14 1:08CCB U -0.3 0.3mg/L



WG358122

WG358122ICV 01/22/14 11:52 102ICV WI131209-3 102 90 110mg/L100

WG358122ICB 01/22/14 11:52ICB U -3 3mg/L

WG366155

WG366155CCV1 06/18/14 23:09 96.4CCV WI140502-1 48.2 90 110mg/L50

WG366155CCB1 06/18/14 23:09CCB U -3 3mg/L

WG366155PQV 06/18/14 23:09 96PQV WI140502-3 4.8 70 130mg/L5

WG366155LFB1 06/18/14 23:09 95.4LFB WI140502-2 47.7 90 110mg/L50

L18793-03DUP RA06/18/14 23:09 4.8DUP 4.7 2.1mg/L 20

WG366155CCV2 06/18/14 23:09 95.2CCV WI140502-1 47.6 90 110mg/L50

WG366155CCB2 06/18/14 23:09CCB U -3 3mg/L

L18795-08AS 06/18/14 23:09 5.1 96.2AS WI140502-2 53.2 90 110mg/L50

WG366155CCV3 06/18/14 23:09 96CCV WI140502-1 48 90 110mg/L50

WG366155CCB3 06/18/14 23:09CCB U -3 3mg/L

WG366155LFB2 06/18/14 23:09 96.6LFB WI140502-2 48.3 90 110mg/L50

WG366155CCV4 06/18/14 23:09 95.4CCV WI140502-1 47.7 90 110mg/L50

WG366155CCB4 06/18/14 23:09CCB U -3 3mg/L

WG366155CCV5 06/18/14 23:09 93.8CCV WI140502-1 46.9 90 110mg/L50

WG366155CCB5 06/18/14 23:09CCB U -3 3mg/L

Page 7 of 27L18718-1406301328


Inorganic QC

Summary


Cesium, dissolv ed M200.8 ICP-MS


WG366370

WG366370ICV 06/23/14 17:55 102ICV MS140513-1 .05101 90 110mg/L.05

WG366370ICB 06/23/14 17:58ICB U -0.0006 0.0006mg/L

WG366370LFB 06/23/14 18:02 102.8LFB MS140513-3 .05138 85 115mg/L.05

L18719-01AS 06/23/14 18:11 U 111.4AS MS140513-3 .11138 70 130mg/L.1

L18719-01ASD 06/23/14 18:15 U 112.8ASD MS140513-3 .11282 1.2870 130mg/L 20.1

WG366370CCV1 06/23/14 18:31 100.7CCV MS140513-2 .1007 90 110mg/L.1

WG366370CCB1 06/23/14 18:34CCB U -0.0006 0.0006mg/L

WG366370CCV2 06/23/14 19:10 100.4CCV MS140513-2 .1004 90 110mg/L.1

WG366370CCB2 06/23/14 19:13CCB U -0.0006 0.0006mg/L

WG366370CCV3 06/23/14 19:36 101.7CCV MS140513-2 .1017 90 110mg/L.1

WG366370CCB3 06/23/14 19:39CCB U -0.0006 0.0006mg/L

Chloride SM4500Cl-E


WG366258

WG366258ICB 06/20/14 9:34ICB U -1.5 1.5mg/L

WG366258ICV 06/20/14 9:34 105.4ICV WI130722-5 57.92 90 110mg/L54.945

WG366258CCV1 06/20/14 10:13 107.8CCV WI131028-1 53.89 90 110mg/L50

WG366258CCB1 06/20/14 10:13CCB U -1.5 1.5mg/L

WG366258LFB1 06/20/14 10:13 108.6LFB WI140508-1 32.59 90 110mg/L30

L18718-01DUP 06/20/14 10:13 37.8DUP 37.77 0.1mg/L 20

WG366258CCV2 06/20/14 10:15 108.1CCV WI131028-1 54.04 90 110mg/L50

WG366258CCB2 06/20/14 10:15CCB U -1.5 1.5mg/L

WG366258CCV3 06/20/14 10:17 108.1CCV WI131028-1 54.06 90 110mg/L50

WG366258CCB3 06/20/14 10:17CCB U -1.5 1.5mg/L

WG366258LFB2 06/20/14 10:17 108.5LFB WI140508-1 32.55 90 110mg/L30

WG366258CCV4 06/20/14 10:23 107.1CCV WI131028-1 53.55 90 110mg/L50

WG366258CCB4 06/20/14 10:23CCB U -1.5 1.5mg/L

WG366258CCV5 06/20/14 10:25 107.8CCV WI131028-1 53.88 90 110mg/L50

WG366258CCB5 06/20/14 10:25CCB U -1.5 1.5mg/L

L18719-01AS 06/20/14 10:25 229 101AS 10XCL 259.3 90 110mg/L30

WG366258CCV6 06/20/14 10:30 108CCV WI131028-1 54.02 90 110mg/L50

WG366258CCB6 06/20/14 10:30CCB U -1.5 1.5mg/L

WG366258CCV7 06/20/14 10:32 107.9CCV WI131028-1 53.97 90 110mg/L50

WG366258CCB7 06/20/14 10:32CCB U -1.5 1.5mg/L

WG366258CCV8 06/20/14 10:53 107.3CCV WI131028-1 53.63 90 110mg/L50

WG366258CCB8 06/20/14 10:53CCB U -1.5 1.5mg/L

WG366258CCV9 06/20/14 10:54 106.9CCV WI131028-1 53.45 90 110mg/L50

WG366258CCB9 06/20/14 10:54CCB U -1.5 1.5mg/L

Page 8 of 27L18718-1406301328


Inorganic QC

Summary


Chromium, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 97ICV II140512-2 1.94 95 105mg/L2

WG365596ICB 06/10/14 23:20ICB U -0.03 0.03mg/L

WG365596PQV 06/10/14 23:24 71.9PQV II140609-2 .036 70 130mg/L.0501

WG365596SIC 06/10/14 23:27 86.8SIC II140602-1 .087 80 120mg/L.1002

WG365596LFB 06/10/14 23:33 96.4LFB II140530-2 .483 85 115mg/L.501

L18718-01AS 06/10/14 23:39 U 96.8AS II140530-2 .485 85 115mg/L.501

L18718-01ASD 06/10/14 23:42 U 97.6ASD II140530-2 .489 0.8285 115mg/L 20.501

WG365596CCV1 06/11/14 0:04 98.5CCV II140506-1 .985 90 110mg/L1

WG365596CCB1 06/11/14 0:07CCB U -0.03 0.03mg/L

WG365596CCV2 06/11/14 0:43 98.1CCV II140506-1 .981 90 110mg/L1

WG365596CCB2 06/11/14 0:46CCB U -0.03 0.03mg/L

WG365596CCV3 06/11/14 1:05 99CCV II140506-1 .99 90 110mg/L1

WG365596CCB3 06/11/14 1:08CCB U -0.03 0.03mg/L

Copper, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 96.8ICV II140512-2 1.935 95 105mg/L2

WG365596ICB 06/10/14 23:20ICB U -0.03 0.03mg/L

WG365596PQV 06/10/14 23:24 92PQV II140609-2 .046 70 130mg/L.05

WG365596SIC 06/10/14 23:27 94SIC II140602-1 .094 80 120mg/L.1

WG365596LFB 06/10/14 23:33 97LFB II140530-2 .485 85 115mg/L.5

L18718-01AS 06/10/14 23:39 U 98.4AS II140530-2 .492 85 115mg/L.5

L18718-01ASD 06/10/14 23:42 U 97.8ASD II140530-2 .489 0.6185 115mg/L 20.5

WG365596CCV1 06/11/14 0:04 97.4CCV II140506-1 .974 90 110mg/L1

WG365596CCB1 06/11/14 0:07CCB U -0.03 0.03mg/L

WG365596CCV2 06/11/14 0:43 96.3CCV II140506-1 .963 90 110mg/L1

WG365596CCB2 06/11/14 0:46CCB U -0.03 0.03mg/L

WG365596CCV3 06/11/14 1:05 97CCV II140506-1 .97 90 110mg/L1

WG365596CCB3 06/11/14 1:08CCB U -0.03 0.03mg/L

Page 9 of 27L18718-1406301328


Inorganic QC

Summary


Fluoride SM4500F-C


WG366199

WG366199ICV 06/19/14 12:15 98.3ICV WC140616- 1.965 95 105mg/L2

WG366199ICB 06/19/14 12:20ICB .068 -0.15 0.15mg/L

WG366199PQV 06/19/14 12:23 100.5PQV WC140618- .252 70 130mg/L.25075

WG366199LFB1 06/19/14 12:26 94.8LFB WC140501- 4.756 90 110mg/L5.015

L18718-01AS 06/19/14 12:32 .52 91.7AS WC140501- 5.12 90 110mg/L5.015

L18718-01DUP 06/19/14 12:37 .52DUP .444 15.8mg/L 20

WG366199CCV1 06/19/14 13:20 99.2CCV WC140616- 1.983 90 110mg/L2

WG366199CCB1 06/19/14 13:28CCB U -0.15 0.15mg/L

WG366199CCV3 06/19/14 15:04 98.7CCV WC140616- 1.974 90 110mg/L2

WG366199CCB3 06/19/14 15:11CCB U -0.15 0.15mg/L

WG366199CCV4 06/19/14 15:58 99.2CCV WC140616- 1.983 90 110mg/L2

WG366199CCB4 06/19/14 16:06CCB U -0.15 0.15mg/L

WG366199CCV5 06/19/14 16:51 96.1CCV WC140616- 1.921 90 110mg/L2

WG366199CCB5 06/19/14 16:57CCB U -0.15 0.15mg/L

WG366199CCV6 06/19/14 17:08 98.7CCV WC140616- 1.974 90 110mg/L2

WG366199CCB6 06/19/14 17:16CCB U -0.15 0.15mg/L

Iron, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 98.3ICV II140512-2 1.965 95 105mg/L2

WG365596ICB 06/10/14 23:20ICB U -0.06 0.06mg/L

WG365596PQV 06/10/14 23:24 87.9PQV II140609-2 .044 70 130mg/L.05007

WG365596SIC 06/10/14 23:27 96SIC II140602-1 192.3 1 200mg/L200.33007

WG365596LFB 06/10/14 23:33 99.9LFB II140530-2 1 85 115mg/L1.0014

L18718-01AS 06/10/14 23:39 .03 102.2AS II140530-2 1.043 85 115mg/L1.0014

L18718-01ASD 06/10/14 23:42 .03 101.7ASD II140530-2 1.038 0.4885 115mg/L 201.0014

WG365596CCV1 06/11/14 0:04 105.1CCV II140506-1 1.051 90 110mg/L1

WG365596CCB1 06/11/14 0:07CCB U -0.06 0.06mg/L

Lead, dissolv ed M200.8 ICP-MS


WG366370

WG366370ICV 06/23/14 17:55 102.3ICV MS140513-1 .05116 90 110mg/L.05

WG366370ICB 06/23/14 17:58ICB U -0.0003 0.0003mg/L

WG366370LFB 06/23/14 18:02 99.5LFB MS140513-3 .04979 85 115mg/L.05005

L18719-01AS 06/23/14 18:11 U 108.9AS MS140513-3 .10904 70 130mg/L.1001

L18719-01ASD 06/23/14 18:15 U 109.2ASD MS140513-3 .10932 0.2670 130mg/L 20.1001

WG366370CCV1 06/23/14 18:31 99.8CCV MS140513-2 .2498 90 110mg/L.25025

WG366370CCB1 06/23/14 18:34CCB U -0.0003 0.0003mg/L

WG366370CCV2 06/23/14 19:10 99.2CCV MS140513-2 .2482 90 110mg/L.25025

WG366370CCB2 06/23/14 19:13CCB .00012 -0.0003 0.0003mg/L

WG366370CCV3 06/23/14 19:36 99.4CCV MS140513-2 .2488 90 110mg/L.25025

WG366370CCB3 06/23/14 19:39CCB .00011 -0.0003 0.0003mg/L

Page 10 of 27L18718-1406301328


Inorganic QC

Summary


Magnesium, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 97.3ICV II140512-2 97.26 95 105mg/L100

WG365596ICB 06/10/14 23:20ICB U -0.6 0.6mg/L

WG365596PQV 06/10/14 23:24 99.9PQV II140609-2 1 70 130mg/L1.0007

WG365596SIC 06/10/14 23:27 100.6SIC II140602-1 202.3 1 200mg/L201.1407

WG365596LFB 06/10/14 23:33 97.9LFB II140530-2 48.93 85 115mg/L50.00131

L18718-01AS 06/10/14 23:39 71.6 97.8AS II140530-2 120.5 85 115mg/L50.00131

L18718-01ASD 06/10/14 23:42 71.6 96ASD II140530-2 119.6 0.7585 115mg/L 2050.00131

WG365596CCV1 06/11/14 0:04 97.1CCV II140506-1 48.55 90 110mg/L50

WG365596CCB1 06/11/14 0:07CCB U -0.6 0.6mg/L

WG365596CCV2 06/11/14 0:43 97CCV II140506-1 48.51 90 110mg/L50

WG365596CCB2 06/11/14 0:46CCB U -0.6 0.6mg/L

WG365596CCV3 06/11/14 1:05 97.2CCV II140506-1 48.6 90 110mg/L50

WG365596CCB3 06/11/14 1:08CCB U -0.6 0.6mg/L

Manganese, dissolv ed M200.7 ICP


WG365649

WG365649ICV 06/11/14 11:30 99.2ICV II140512-2 1.9832 95 105mg/L2

WG365649ICB 06/11/14 11:36ICB U -0.015 0.015mg/L

WG365649PQV 06/11/14 11:39 99.2PQV II140609-2 .0248 70 130mg/L.025

WG365649SIC 06/11/14 11:43 97.8SIC II140602-1 49.02 1 200mg/L50.125

WG365649LFB 06/11/14 11:49 99.3LFB II140530-2 .4976 85 115mg/L.501

L18718-01AS 06/11/14 11:55 U 100.4AS II140530-2 .5031 85 115mg/L.501

L18718-01ASD 06/11/14 11:58 U 100.5ASD II140530-2 .5037 0.1285 115mg/L 20.501

WG365649CCV1 06/11/14 12:20 97.7CCV II140506-1 .9774 90 110mg/L1

WG365649CCB1 06/11/14 12:23CCB U -0.015 0.015mg/L

WG365649CCV2 06/11/14 12:57 98.2CCV II140506-1 .982 90 110mg/L1

WG365649CCB2 06/11/14 13:00CCB U -0.015 0.015mg/L

WG365649CCV3 06/11/14 13:16 98CCV II140506-1 .9795 90 110mg/L1

WG365649CCB3 06/11/14 13:19CCB U -0.015 0.015mg/L

Mercury, dissolv ed M245.1 CVAA


WG366069

WG366069ICV 06/19/14 11:14 95.9ICV II140616-2 .0048 95 105mg/L.005005

WG366069ICB 06/19/14 11:16ICB U -0.0002 0.0002mg/L

WG366069LRB 06/19/14 11:19LRB U -0.00044 0.00044mg/L

WG366069LFB 06/19/14 11:21 95.4LFB II140616-4 .00191 85 115mg/L.002002

L18849-01LFM 06/19/14 11:32 U 94.9LFM II140616-4 .0019 85 115mg/L.002002


WG366069CCV1 06/19/14 11:40 98.7CCV II140616-2 .00494 90 110mg/L.005005

WG366069CCB1 06/19/14 11:42CCB U -0.0002 0.0002mg/L

WG366069CCV2 06/19/14 12:06 96.9CCV II140616-2 .00485 90 110mg/L.005005

WG366069CCB2 06/19/14 12:08CCB U -0.0002 0.0002mg/L

WG366069CCV3 06/19/14 12:24 96.3CCV II140616-2 .00482 90 110mg/L.005005

WG366069CCB3 06/19/14 12:26CCB U -0.0002 0.0002mg/L

Page 11 of 27L18718-1406301328


Inorganic QC

Summary


Molybdenum, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 99.7ICV II140512-2 1.994 95 105mg/L2

WG365596ICB 06/10/14 23:20ICB U -0.06 0.06mg/L

WG365596PQV 06/10/14 23:24 97PQV II140609-2 .097 70 130mg/L.1

WG365596SIC 06/10/14 23:27 88SIC II140602-1 .088 80 120mg/L.1

WG365596LFB 06/10/14 23:33 99.7LFB II140530-2 .498 85 115mg/L.4995

L18718-01AS 06/10/14 23:39 U 103.5AS II140530-2 .517 85 115mg/L.4995

L18718-01ASD 06/10/14 23:42 U 103.3ASD II140530-2 .516 0.1985 115mg/L 20.4995

WG365596CCV1 06/11/14 0:04 101.4CCV II140506-1 1.014 90 110mg/L1

WG365596CCB1 06/11/14 0:07CCB U -0.06 0.06mg/L

WG365596CCV2 06/11/14 0:43 101.4CCV II140506-1 1.014 90 110mg/L1

WG365596CCB2 06/11/14 0:46CCB U -0.06 0.06mg/L

WG365596CCV3 06/11/14 1:05 101CCV II140506-1 1.01 90 110mg/L1

WG365596CCB3 06/11/14 1:08CCB U -0.06 0.06mg/L

Nickel, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 98.3ICV II140512-2 1.965 95 105mg/L2

WG365596ICB 06/10/14 23:20ICB U -0.024 0.024mg/L

WG365596PQV 06/10/14 23:24 101.3PQV II140609-2 .0405 70 130mg/L.04

WG365596SIC 06/10/14 23:27 105.9SIC II140602-1 .1059 80 120mg/L.1

WG365596LFB 06/10/14 23:33 99.8LFB II140530-2 .4988 85 115mg/L.5

L18718-01AS 06/10/14 23:39 U 99.4AS II140530-2 .497 85 115mg/L.5

L18718-01ASD 06/10/14 23:42 U 100ASD II140530-2 .4999 0.5885 115mg/L 20.5

WG365596CCV1 06/11/14 0:04 100.9CCV II140506-1 1.009 90 110mg/L1

WG365596CCB1 06/11/14 0:07CCB U -0.024 0.024mg/L

WG365596CCV2 06/11/14 0:43 101.2CCV II140506-1 1.012 90 110mg/L1

WG365596CCB2 06/11/14 0:46CCB U -0.024 0.024mg/L

WG365596CCV3 06/11/14 1:05 101.5CCV II140506-1 1.015 90 110mg/L1

WG365596CCB3 06/11/14 1:08CCB U -0.024 0.024mg/L

Page 12 of 27L18718-1406301328


Inorganic QC

Summary




WG366446

WG366446ICV 06/24/14 20:58 92.6ICV WI140417-3 2.238 90 110mg/L2.416

WG366446ICB 06/24/14 20:59ICB U -0.06 0.06mg/L

WG366449

WG366449CCV1 06/24/14 22:15 105.7CCV WI140617-1 2.114 90 110mg/L2

WG366449CCB1 06/24/14 22:17CCB U -0.06 0.06mg/L

WG366449PQV 06/24/14 22:18 118PQV WI140215-4 .118 70 130mg/L.1

WG366449LFB1 06/24/14 22:19 101.1LFB WI140215-3 2.021 90 110mg/L2

L18718-01AS M106/24/14 22:21 .67 150.1AS WI140215-3 3.672 90 110mg/L2

WG366449CCV2 06/24/14 22:30 104.9CCV WI140617-1 2.097 90 110mg/L2

WG366449CCB2 06/24/14 22:31CCB U -0.06 0.06mg/L

WG366449CCV3 06/24/14 22:44 104.5CCV WI140617-1 2.089 90 110mg/L2

WG366449CCB3 06/24/14 22:45CCB U -0.06 0.06mg/L

WG366449LFB2 06/24/14 22:53 99.2LFB WI140215-3 1.984 90 110mg/L2

WG366449CCV4 06/24/14 22:58 103.8CCV WI140617-1 2.075 90 110mg/L2

WG366449CCB4 06/24/14 22:59CCB U -0.06 0.06mg/L

L18719-01DUP 06/24/14 23:11 11.2DUP 11.23 0.3mg/L 20

WG366449CCV5 06/24/14 23:13 103.6CCV WI140617-1 2.071 90 110mg/L2

WG366449CCB5 06/24/14 23:14CCB U -0.06 0.06mg/L

WG366449CCV6 06/24/14 23:18 102.7CCV WI140617-1 2.054 90 110mg/L2

WG366449CCB6 06/24/14 23:19CCB U -0.06 0.06mg/L



WG366600

WG366600ICV 06/26/14 15:52 98.4ICV WI131021-1 .987 90 110mg/L1.003

WG366600ICB 06/26/14 15:55ICB U -0.15 0.15mg/L

WG366600LFB1 06/26/14 15:56 99.2LFB WI140113-8 .992 90 110mg/L1

L18718-01AS 06/26/14 15:58 U 95.8AS WI140113-8 .958 90 110mg/L1

L18732-02DUP RA06/26/14 16:01 .24DUP .263 9.1mg/L 20

WG366600CCV1 06/26/14 16:07 102.3CCV WI140113-6 2.045 90 110mg/L2

WG366600CCB1 06/26/14 16:08CCB U -0.15 0.15mg/L

WG366600CCV2 06/26/14 16:20 103.8CCV WI140113-6 2.075 90 110mg/L2

WG366600CCB2 06/26/14 16:21CCB U -0.15 0.15mg/L

WG366600LFB2 06/26/14 16:28 99.2LFB WI140113-8 .992 90 110mg/L1

WG366600CCV3 06/26/14 16:33 100.8CCV WI140113-6 2.016 90 110mg/L2

WG366600CCB3 06/26/14 16:34CCB U -0.15 0.15mg/L

WG366600CCV4 06/26/14 16:46 100.8CCV WI140113-6 2.015 90 110mg/L2

WG366600CCB4 06/26/14 16:47CCB U -0.15 0.15mg/L

Page 13 of 27L18718-1406301328


Inorganic QC

Summary


Potassium, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 99.1ICV II140512-2 19.81 95 105mg/L20

WG365596ICB 06/10/14 23:20ICB U -0.6 0.6mg/L

WG365596PQV 06/10/14 23:24 107PQV II140609-2 1.07 70 130mg/L1

WG365596SIC 06/10/14 23:27 108SIC II140602-1 1.08 80 120mg/L1

WG365596LFB 06/10/14 23:33 99.7LFB II140530-2 99.66 85 115mg/L99.99364

L18718-01AS 06/10/14 23:39 11.7 102.3AS II140530-2 114 85 115mg/L99.99364

L18718-01ASD 06/10/14 23:42 11.7 101.6ASD II140530-2 113.3 0.6285 115mg/L 2099.99364

WG365596CCV1 06/11/14 0:04 99.6CCV II140506-1 9.96 90 110mg/L10

WG365596CCB1 06/11/14 0:07CCB U -0.6 0.6mg/L

WG365596CCV2 06/11/14 0:43 98.6CCV II140506-1 9.86 90 110mg/L10

WG365596CCB2 06/11/14 0:46CCB U -0.6 0.6mg/L

WG365596CCV3 06/11/14 1:05 99.6CCV II140506-1 9.96 90 110mg/L10

WG365596CCB3 06/11/14 1:08CCB U -0.6 0.6mg/L



WG365515

WG365515PBW 06/09/14 2:50PBW U -20 20mg/L


L18690-03DUP RA RO06/09/14 3:21 UDUP U 0mg/L 10



WG365398

WG365398PBW 06/06/14 11:34PBW U -15 15mg/L


L18722-01DUP RA06/06/14 12:29 UDUP U 0mg/L 10

Selenium, dissolv ed M200.8 ICP-MS


WG366370

WG366370ICV 06/23/14 17:55 102.9ICV MS140513-1 .05143 90 110mg/L.05

WG366370ICB 06/23/14 17:58ICB .00011 -0.0003 0.0003mg/L

WG366370LFB 06/23/14 18:02 104.3LFB MS140513-3 .05222 85 115mg/L.05005

L18719-01AS 06/23/14 18:11 .0011 122.2AS MS140513-3 .12346 70 130mg/L.1001

L18719-01ASD 06/23/14 18:15 .0011 124.1ASD MS140513-3 .12528 1.4670 130mg/L 20.1001

WG366370CCV1 06/23/14 18:31 100.1CCV MS140513-2 .2505 90 110mg/L.25025

WG366370CCB1 06/23/14 18:34CCB U -0.0003 0.0003mg/L

WG366370CCV2 06/23/14 19:10 100.3CCV MS140513-2 .2511 90 110mg/L.25025

WG366370CCB2 06/23/14 19:13CCB .00011 -0.0003 0.0003mg/L

WG366370CCV3 06/23/14 19:36 100.3CCV MS140513-2 .2511 90 110mg/L.25025

WG366370CCB3 BE06/23/14 19:39CCB .00046 -0.0003 0.0003mg/L

Page 14 of 27L18718-1406301328


Inorganic QC

Summary


Silica, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 99.3ICV II140512-2 42.49 95 105mg/L42.8

WG365596ICB 06/10/14 23:20ICB U -0.6 0.6mg/L

WG365596PQV 06/10/14 23:24 84.9PQV II140609-2 .91 70 130mg/L1.0714

WG365596SIC 06/10/14 23:27 83.1SIC II140602-1 .89 80 120mg/L1.0714

WG365596LFB 06/10/14 23:33 102.8LFB II140530-2 22.02 85 115mg/L21.428

L18718-01AS 06/10/14 23:39 15.9 103.5AS II140530-2 38.07 85 115mg/L21.428

L18718-01ASD 06/10/14 23:42 15.9 102.7ASD II140530-2 37.9 0.4585 115mg/L 2021.428

WG365596CCV1 06/11/14 0:04 99.8CCV II140506-1 21.35 90 110mg/L21.4

WG365596CCB1 06/11/14 0:07CCB U -0.6 0.6mg/L

WG365596CCV2 06/11/14 0:43 99.8CCV II140506-1 21.35 90 110mg/L21.4

WG365596CCB2 06/11/14 0:46CCB U -0.6 0.6mg/L

WG365596CCV3 06/11/14 1:05 100.2CCV II140506-1 21.44 90 110mg/L21.4

WG365596CCB3 06/11/14 1:08CCB U -0.6 0.6mg/L

Sodium, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 98.8ICV II140512-2 98.84 95 105mg/L100

WG365596ICB 06/10/14 23:20ICB U -0.6 0.6mg/L

WG365596PQV 06/10/14 23:24 103.9PQV II140609-2 1.04 70 130mg/L1.001

WG365596SIC 06/10/14 23:27 105.9SIC II140602-1 1.06 80 120mg/L1.001

WG365596LFB 06/10/14 23:33 99.4LFB II140530-2 99.47 85 115mg/L100.0393

L18718-01AS 06/10/14 23:39 92.7 102.4AS II140530-2 195.1 85 115mg/L100.0393

L18718-01ASD 06/10/14 23:42 92.7 99.8ASD II140530-2 192.5 1.3485 115mg/L 20100.0393

WG365596CCV1 06/11/14 0:04 99.1CCV II140506-1 49.53 90 110mg/L50

WG365596CCB1 06/11/14 0:07CCB U -0.6 0.6mg/L

WG365596CCV2 06/11/14 0:43 98CCV II140506-1 49.01 90 110mg/L50

WG365596CCB2 06/11/14 0:46CCB U -0.6 0.6mg/L

WG365596CCV3 06/11/14 1:05 99CCV II140506-1 49.48 90 110mg/L50

WG365596CCB3 06/11/14 1:08CCB U -0.6 0.6mg/L



WG365730

WG365730PBW 06/12/14 13:50PBW U -30 30mg/L


L18774-03DUP 06/12/14 14:29 440DUP 456 3.6mg/L 20

Page 15 of 27L18718-1406301328


Inorganic QC

Summary




WG365569

WG365569ICV 06/10/14 11:00 100.1ICV WC140610- .299 90 110mg/L.29866

WG365569ICB 06/10/14 11:07ICB U -0.06 0.06mg/L

WG365569LFB 06/10/14 11:14 111.2LFB WC140610- .258 80 120mg/L.232

L18748-03AS 06/10/14 12:10 U 117.7AS WC140610- .273 75 125mg/L.232

L18748-03DUP RA06/10/14 12:17 UDUP U 0mg/L 20

WG365569CCV1 06/10/14 12:25 101.1CCV WC140610- .176 90 110mg/L.174

WG365569CCB1 06/10/14 12:32CCB U -0.06 0.06mg/L

WG365569CCV2 06/10/14 13:42 100.6CCV WC140610- .175 90 110mg/L.174

WG365569CCB2 06/10/14 13:50CCB U -0.06 0.06mg/L

Uranium, dissolv ed M200.8 ICP-MS


WG366370

WG366370ICV 06/23/14 17:55 102.8ICV MS140513-1 .05138 90 110mg/L.05

WG366370ICB 06/23/14 17:58ICB U -0.0003 0.0003mg/L

WG366370LFB 06/23/14 18:02 102.9LFB MS140513-3 .05146 85 115mg/L.05

L18719-01AS 06/23/14 18:11 .0182 119.6AS MS140513-3 .13776 70 130mg/L.1

L18719-01ASD 06/23/14 18:15 .0182 120.5ASD MS140513-3 .13874 0.7170 130mg/L 20.1

WG366370CCV1 06/23/14 18:31 104.4CCV MS140513-2 .1044 90 110mg/L.1

WG366370CCB1 06/23/14 18:34CCB U -0.0003 0.0003mg/L

WG366370CCV2 06/23/14 19:10 105.6CCV MS140513-2 .1056 90 110mg/L.1

WG366370CCB2 06/23/14 19:13CCB U -0.0003 0.0003mg/L

WG366370CCV3 06/23/14 19:36 106.5CCV MS140513-2 .1065 90 110mg/L.1

WG366370CCB3 06/23/14 19:39CCB U -0.0003 0.0003mg/L

Vanadium, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 100.2ICV II140512-2 2.0042 95 105mg/L2

WG365596ICB 06/10/14 23:20ICB U -0.015 0.015mg/L

WG365596PQV 06/10/14 23:24 88PQV II140609-2 .022 70 130mg/L.025

WG365596SIC 06/10/14 23:27 90.2SIC II140602-1 .0902 80 120mg/L.1

WG365596LFB 06/10/14 23:33 101.2LFB II140530-2 .5058 85 115mg/L.5

L18718-01AS 06/10/14 23:39 .018 103.8AS II140530-2 .5372 85 115mg/L.5

L18718-01ASD 06/10/14 23:42 .018 102.9ASD II140530-2 .5324 0.985 115mg/L 20.5

WG365596CCV1 06/11/14 0:04 101.2CCV II140506-1 1.012 90 110mg/L1

WG365596CCB1 06/11/14 0:07CCB U -0.015 0.015mg/L

WG365596CCV2 06/11/14 0:43 100CCV II140506-1 1 90 110mg/L1

WG365596CCB2 06/11/14 0:46CCB U -0.015 0.015mg/L

WG365596CCV3 06/11/14 1:05 100.5CCV II140506-1 1.005 90 110mg/L1

WG365596CCB3 06/11/14 1:08CCB U -0.015 0.015mg/L

Page 16 of 27L18718-1406301328


Inorganic QC

Summary


Zinc, dissolv ed M200.7 ICP


WG365596

WG365596ICV 06/10/14 23:14 96.7ICV II140512-2 1.934 95 105mg/L2

WG365596ICB 06/10/14 23:20ICB U -0.03 0.03mg/L

WG365596PQV 06/10/14 23:24 100PQV II140609-2 .05 70 130mg/L.05

WG365596SIC 06/10/14 23:27 92SIC II140602-1 .092 80 120mg/L.1

WG365596LFB 06/10/14 23:33 99.9LFB II140530-2 .5 85 115mg/L.5005

L18718-01AS 06/10/14 23:39 U 101.3AS II140530-2 .507 85 115mg/L.5005

L18718-01ASD 06/10/14 23:42 U 99.9ASD II140530-2 .5 1.3985 115mg/L 20.5005

WG365596CCV1 06/11/14 0:04 108.7CCV II140506-1 1.087 90 110mg/L1

WG365596CCB1 06/11/14 0:07CCB .01 -0.03 0.03mg/L

Page 17 of 27L18718-1406301328


Inorganic Extended

Qualifier Report




SM5310BCarbon, total organic (TOC)L18718-01 WG366155

M1 Matrix spike recovery was high, the recovery of the associated control sample (LCS or LFB) was acceptable.






RO The duplicate originally assigned to this sample was not used for precision assessment because residue density exceeded the method limits. Another duplicate in the batch was used to assess precision. Method required duplicate frequency was not met.

SM2540C





REPAD.15.06.05.01

Page 18 of 27L18718-1406301328


Sample ID: PW3



Project ID:


Date Sampled: 06/03/14 13:20


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 39 8.8 3.3 pCi/L nco06/23/14 12:49

Gross Beta 33 6.3 7 pCi/L nco06/23/14 12:49

Lead 210, dissolved

EICHROM, OTW01

Prep Method:


Lead 210, dissolved -1.2 3.2 9.7 pCi/L * jrd06/24/14 14:25


M903.1

Prep Method:




M904.0

Prep Method:


Radium 228, dissolved 0.2 0.55 0.58 pCi/L thf06/23/14 13:52


ESM 4506

Prep Method:



REPRC.02.06.05.01 * P lease refer to Qualifier Reports for details.

Page 19 of 27L18718-1406301328










P QL Practical Quantitation Limit







QC Sample Types


LCSS Laboratory Control Sample - Soil P BS Prep Blank - Soil

LCSW Laboratory Control Sample - Water P BW Prep Blank - Water











D ASTM

RP DOE

ESM DOE/ESM

Comments







REP003.09.12.01

Radiochemistry

Reference

Page 20 of 27L18718-1406301328


Radiochemistry QC

Summary


Alpha M900.0


pCi/L

Error LLDLLD

Units:

WG366410

WG366047PBW 06/23/14PBW 0 21.1 1

WG366047LCSWA 06/23/14 105LCSW PCN45468 7066.67 83 1336.1 1

L18718-01DUP 06/23/14 39DUP-RER 37 29.1 0.168.8 3.53.3

L18877-01DUP 06/23/14 2.3DUP-RER 27 215 1.3710 9.89.7

L18733-02MSA 06/23/14 0.08 99.9MS PCN45468 100100 83 1339.52.1 1.61.8

Beta M900.0


pCi/L

Error LLDLLD

Units:

WG366410

WG366047PBW 06/23/14PBW .03 6.22.1 3.1

WG366047LCSWB 06/23/14 117LCSW PCN44650 7866.67 70 1294.9 2.9

L18718-01DUP 06/23/14 33DUP-RER 34 27 0.116.3 7.17

L18877-01DUP 06/23/14 17DUP-RER 4.4 213 0.6913 2020

L18864-01MSB 06/23/14 10 120MS PCN44650 160125 70 129105.1 66.6

Lead 210, dissolv ed EICHROM, OTW01


pCi/L

Error LLDLLD

Units:

WG366481

WG366030PBW 06/24/14PBW 1.3 12.42.1 6.2

WG366030LCSW 06/24/14 65.3LCSW PCN44120 6497.95 55 1213.4 6.1

L18774-02DUP 06/24/14 -3.4DUP-RER 0 21.9 1.172.2 5.66.8

L18719-03DUP 06/24/14 -0.91DUP-RER -.67 22.1 0.082.1 6.26.6

L18774-03MS 06/24/14 -1 69.4MS PCN44120 6797.95 55 1214.22.2 8.26.8

Page 21 of 27L18718-1406301328


Radiochemistry QC

Summary


Radium 226, dissolv ed M903.1


pCi/L

Error LLDLLD

Units:

WG366104

WG365571PBW 06/17/14PBW .1 0.20.09 0.1

WG365571LCSW 06/17/14 90LCSW PCN45817 1820 43 1480.48 0.1

L18697-03DUP RM06/17/14 7.4DUP-RER 5.2 20.28 4.910.35 0.220.28

L18697-04MS 06/17/14 13 90MS PCN45817 3120 43 1480.650.43 0.160.14



pCi/L

Error LLDLLD

Units:

WG366424

WG365899LCSW 06/23/14 70.2LCSW PCN46177 1419.95 47 1231.2 0.52

WG365899PBW 06/23/14PBW .51 0.80.4 0.4

L18829-01MS 06/24/14 1.7 91.8MS PCN46177 2019.94 47 1231.40.58 0.590.49

L18718-01DUP 06/24/14 0.2DUP-RER 1.8 20.58 20.55 0.490.58

Thorium 230, dissolv ed ESM 4506


pCi/L

Error LLDLLD

Units:

WG366524

WG365760PBW 06/24/14PBW .25 1.10.26 0.55

WG365760LCSW 06/24/14 104.9LCSW RC130807-2 170162.12 91 1264.4 0.6

L18718-01DUP 06/24/14 0.1DUP-RER .21 20.25 0.290.29 0.60.56

L18774-01DUP 06/24/14 0.31DUP-RER -.39 20.62 0.980.36 0.540.58

L18774-02MS 06/24/14 0.34 104.7MS RC130807-2 170162.12 91 1264.60.32 0.590.61

Page 22 of 27L18718-1406301328


RadChem Extended

Qualifier Report



RM For a water matrix, the duplicate precision assessment (RPD or RER) exceeded the control limit. High sediment, turbidity, or presence of an immiscible liquid attributed to non-homogeneity of the sample.


REPAD.15.06.05.01

Page 23 of 27L18718-1406301328


Certification

Qualifiers


Metals Analysis



Radiochemistry




Wet Chemistry



REPAD.05.06.05.01

Page 24 of 27L18718-1406301328


Sample

Receipt


Date Received:

Received By: mtb

06/06/2014 08:57

L18718




NANOYES

X

X

X

X

X

X









NANOYES

X

X

X

X

X

X

X












Samples/Containers

X

X

X

Shipping Containers


The sample matrix was entered per the requested quotation.

Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- --------------------3778 3.6 13 Yes

X



REPAD LPII 2012-03

Page 25 of 27L18718-1406301328

of 27L18718-1406301328


Analytical

Report



Lakewood, CO 80228


Kathy Weinel:







Kathy Weinel

July 01, 2014

Project ID:



Lakewood, CO 80228

Accounts Payable

Report to: Bill to:

Page 1 of 35L18774-1407011208


Sample ID: MW6



Project ID:



Results

Date Sampled: 06/06/14 10:35



Metals Analysis

XQDilution


Arsenic, dissolved M200.8 ICP-MS mg/L 0.002U msh0.0004 06/27/14 15:362



Cadmium, dissolved M200.8 ICP-MS mg/L 0.001U msh0.0002 06/27/14 15:362

Calcium, dissolved M200.7 ICP 163 mg/L 0.5 aeb0.1 06/11/14 19:051

Cesium, dissolved M200.8 ICP-MS mg/L 0.002U msh0.0004* 06/27/14 15:362


Copper, dissolved M200.7 ICP mg/L 0.05U aeb0.01* 06/11/14 15:451


Lead, dissolved M200.8 ICP-MS mg/L 0.001U msh0.0002 06/27/14 15:362

Magnesium, dissolved M200.7 ICP 325 mg/L 1 aeb0.2* 06/11/14 15:451

Manganese, dissolved M200.7 ICP 0.010 mg/L 0.03B aeb0.005 06/11/14 15:451





Selenium, dissolved M200.8 ICP-MS 0.0004 mg/L 0.0005B msh0.0002 06/27/14 15:362


Sodium, dissolved M200.7 ICP 214 mg/L 1 aeb0.2 06/11/14 15:451

Uranium, dissolved M200.8 ICP-MS mg/L 0.001U msh0.0002 06/27/14 15:362

Vanadium, dissolved M200.7 ICP mg/L 0.03U aeb0.005 06/11/14 15:451



Page 2 of 35L18774-1407011208


Sample ID: MW6



Project ID:



Results

Date Sampled: 06/06/14 10:35



Wet Chemistry

XQDilution



403 mg/L 20 abd2 06/17/14 0:001



Total Alkalinity 403 mg/L 20 abd2* 06/17/14 0:001


SM5310B mg/L 5U mpb1* 06/18/14 23:091


Cation-Anion Balance -1.3 % calc07/01/14 9:27



Chloride SM4500Cl-E 175 mg/L 20 mpb5 06/24/14 18:5810


Nitrate/Nitrite as N M353.2 - H2SO4 preserved mg/L 0.1U pjb0.02 06/26/14 22:471

Nitrogen, ammonia M350.1 - Automated Phenate 1.05 mg/L 0.2 mpb0.05* 06/26/14 16:021


SM2540C 2870 mg/L 20 jrd10 06/12/14 16:301


SM2540D 9 mg/L 20B nml5* 06/13/14 9:131


Sulfide as S SM4500S2-D 15 mg/L 4 abd0.8* 06/11/14 9:2537.5





Page 3 of 35L18774-1407011208


Sample ID: PW1



Project ID:



Results

Date Sampled: 06/06/14 13:45



Metals Analysis

XQDilution


Arsenic, dissolved M200.8 ICP-MS 0.0013 mg/L 0.001 msh0.0002 06/27/14 15:391








Iron, dissolved M200.7 ICP 0.70 mg/L 0.05 aeb0.02 06/11/14 15:551


Magnesium, dissolved M200.7 ICP 78.4 mg/L 1 aeb0.2* 06/11/14 15:551

Manganese, dissolved M200.7 ICP 0.033 mg/L 0.03 aeb0.005 06/11/14 15:551





Selenium, dissolved M200.8 ICP-MS 0.0123 mg/L 0.0003 msh0.0001 06/27/14 15:391



Uranium, dissolved M200.8 ICP-MS 0.0719 mg/L 0.0005 msh0.0001 06/27/14 15:391




Page 4 of 35L18774-1407011208


Sample ID: PW1



Project ID:



Results

Date Sampled: 06/06/14 13:45



Wet Chemistry

XQDilution



235 mg/L 20 abd2 06/17/14 0:001





SM5310B mg/L 5U mpb1* 06/18/14 23:091





Chloride SM4500Cl-E 36.4 mg/L 2 mpb0.5 06/24/14 18:471


Nitrate/Nitrite as N M353.2 - H2SO4 preserved 1.47 mg/L 0.1 pjb0.02 06/26/14 22:501


Residue, Filterable (TDS) @ 180C

SM2540C 810 mg/L 20 jrd10 06/12/14 16:351

Residue, Non-Filterable (TSS) @ 105C

SM2540D 18 mg/L 20B nml5* 06/13/14 9:181


Sulfide as S SM4500S2-D mg/L 0.1U abd0.02* 06/11/14 9:311





Page 5 of 35L18774-1407011208


Sample ID: PW2



Project ID:



Results

Date Sampled: 06/06/14 12:40



Metals Analysis

XQDilution


Arsenic, dissolved M200.8 ICP-MS mg/L 0.001U msh0.0002 06/27/14 15:421








Iron, dissolved M200.7 ICP 1.03 mg/L 0.05 aeb0.02 06/11/14 15:581


Magnesium, dissolved M200.7 ICP 62.2 mg/L 1 aeb0.2* 06/11/14 15:581

Manganese, dissolved M200.7 ICP 0.093 mg/L 0.03 aeb0.005 06/11/14 15:581












Page 6 of 35L18774-1407011208


Sample ID: PW2



Project ID:



Results

Date Sampled: 06/06/14 12:40



Wet Chemistry

XQDilution



228 mg/L 20 abd2 06/17/14 0:001





SM5310B mg/L 5U mpb1* 06/18/14 23:091





Chloride SM4500Cl-E 31.1 mg/L 2 mpb0.5 06/24/14 18:471


Nitrate/Nitrite as N M353.2 - H2SO4 preserved 0.32 mg/L 0.1 pjb0.02 06/26/14 22:521



SM2540C 880 mg/L 20H nml10* 06/17/14 11:261


SM2540D 25 mg/L 20 nml5* 06/13/14 9:201


Sulfide as S SM4500S2-D mg/L 0.1U abd0.02* 06/11/14 9:361





Page 7 of 35L18774-1407011208















QC Sample Types
























Method References






Comments








REP001.09.12.01

Inorganic

Reference

Page 8 of 35L18774-1407011208


Inorganic QC

Summary




WG366038

WG366038PQV2 06/17/14 16:54 106PQV WC140210- 21.2 50 150mg/L20

WG366038PBW1 06/17/14 17:01PBW U -20 20mg/L


L18782-02DUP RA06/17/14 18:53 9DUP 9.3 3.3mg/L 20


WG366038PBW2 06/17/14 20:51PBW U -20 20mg/L


WG366038PBW3 06/18/14 0:29PBW 2.1 -20 20mg/L


WG366038PBW4 06/18/14 3:38PBW 2.2 -20 20mg/L




WG365668

WG365668ICV 06/11/14 14:10 96.4ICV II140512-2 1.927 95 105mg/L2

WG365668ICB 06/11/14 14:16ICB U -0.09 0.09mg/L

WG365668PQV 06/11/14 14:19 93.9PQV II140609-2 .141 70 130mg/L.150165

WG365668SIC 06/11/14 14:22 98.2SIC II140602-1 196.8 1 200mg/L200.370165

WG365668LFB 06/11/14 14:28 101LFB II140530-2 1.011 85 115mg/L1.0011

WG365668CCV1 06/11/14 15:00 96.2CCV II140506-1 .962 90 110mg/L1

WG365668CCB1 06/11/14 15:03CCB U -0.09 0.09mg/L

WG365668CCV2 06/11/14 15:39 94.8CCV II140506-1 .948 90 110mg/L1

WG365668CCB2 06/11/14 15:42CCB U -0.09 0.09mg/L

L18774-01AS 06/11/14 15:48 U 105.1AS II140530-2 1.052 85 115mg/L1.0011

L18774-01ASD 06/11/14 15:51 U 106.8ASD II140530-2 1.069 1.685 115mg/L 201.0011

WG365668CCV3 06/11/14 16:01 96.2CCV II140506-1 .962 90 110mg/L1

WG365668CCB3 06/11/14 16:04CCB U -0.09 0.09mg/L



WG366565

WG366565ICV 06/27/14 15:26 106.2ICV MS140513-1 .05311 90 110mg/L.05

WG366565ICB 06/27/14 15:29ICB U -0.0006 0.0006mg/L

WG366565LFB 06/27/14 15:33 98.7LFB MS140625-3 .04946 85 115mg/L.0501

L18774-03AS 06/27/14 15:46 U 99.3AS MS140625-3 .04974 70 130mg/L.0501

L18774-03ASD 06/27/14 15:49 U 101.2ASD MS140625-3 .05072 1.9570 130mg/L 20.0501

WG366565CCV1 06/27/14 16:02 94.1CCV MS140513-2 .09433 90 110mg/L.1002

WG366565CCB1 06/27/14 16:05CCB U -0.0006 0.0006mg/L

WG366565CCV2 06/27/14 16:41 92.3CCV MS140513-2 .09246 90 110mg/L.1002

WG366565CCB2 06/27/14 16:44CCB U -0.0006 0.0006mg/L

WG366565CCV3 06/27/14 17:07 92.6CCV MS140513-2 .09281 90 110mg/L.1002

WG366565CCB3 06/27/14 17:10CCB U -0.0006 0.0006mg/L

Page 9 of 35L18774-1407011208


Inorganic QC

Summary




WG365668

WG365668ICV 06/11/14 14:10 96.6ICV II140512-2 1.9325 95 105mg/L2

WG365668ICB 06/11/14 14:16ICB .0037 -0.009 0.009mg/L

WG365668PQV 06/11/14 14:19 105.3PQV II140609-2 .0158 70 130mg/L.015

WG365668SIC 06/11/14 14:22 98.3SIC II140602-1 .0983 80 120mg/L.1

WG365668LFB 06/11/14 14:28 97.1LFB II140530-2 .4853 85 115mg/L.5

WG365668CCV1 06/11/14 15:00 97.1CCV II140506-1 .9705 90 110mg/L1

WG365668CCB1 06/11/14 15:03CCB U -0.009 0.009mg/L

WG365668CCV2 06/11/14 15:39 96.7CCV II140506-1 .9674 90 110mg/L1

WG365668CCB2 06/11/14 15:42CCB U -0.009 0.009mg/L

L18774-01AS 06/11/14 15:48 .019 96.9AS II140530-2 .5033 85 115mg/L.5

L18774-01ASD 06/11/14 15:51 .019 98.8ASD II140530-2 .5129 1.8985 115mg/L 20.5

WG365668CCV3 06/11/14 16:01 97.1CCV II140506-1 .971 90 110mg/L1

WG365668CCB3 06/11/14 16:04CCB U -0.009 0.009mg/L



WG365668

WG365668ICV 06/11/14 14:10 98.5ICV II140512-2 1.97 95 105mg/L2

WG365668ICB 06/11/14 14:16ICB U -0.03 0.03mg/L

WG365668PQV 06/11/14 14:19 79.9PQV II140609-2 .04 70 130mg/L.05005

WG365668SIC 06/11/14 14:22 80.9SIC II140602-1 .081 80 120mg/L.1001

WG365668LFB 06/11/14 14:28 98.1LFB II140530-2 .491 85 115mg/L.5005

WG365668CCV1 06/11/14 15:00 99.2CCV II140506-1 .992 90 110mg/L1

WG365668CCB1 06/11/14 15:03CCB U -0.03 0.03mg/L

WG365668CCV2 06/11/14 15:39 99.4CCV II140506-1 .994 90 110mg/L1

WG365668CCB2 06/11/14 15:42CCB U -0.03 0.03mg/L

L18774-01AS 06/11/14 15:48 2.42 86.5AS II140530-2 2.853 85 115mg/L.5005

L18774-01ASD 06/11/14 15:51 2.42 102.1ASD II140530-2 2.931 2.785 115mg/L 20.5005

WG365668CCV3 06/11/14 16:01 101CCV II140506-1 1.01 90 110mg/L1

WG365668CCB3 06/11/14 16:04CCB U -0.03 0.03mg/L



WG366565

WG366565ICV 06/27/14 15:26 105.1ICV MS140513-1 .05256 90 110mg/L.05

WG366565ICB 06/27/14 15:29ICB U -0.0003 0.0003mg/L

WG366565LFB 06/27/14 15:33 96.7LFB MS140625-3 .04843 85 115mg/L.0501

L18774-03AS 06/27/14 15:46 U 95.6AS MS140625-3 .04789 70 130mg/L.0501

L18774-03ASD 06/27/14 15:49 U 98.2ASD MS140625-3 .04919 2.6870 130mg/L 20.0501

WG366565CCV1 06/27/14 16:02 95.8CCV MS140513-2 .09598 90 110mg/L.1002

WG366565CCB1 06/27/14 16:05CCB U -0.0003 0.0003mg/L

WG366565CCV2 06/27/14 16:41 95CCV MS140513-2 .09522 90 110mg/L.1002

WG366565CCB2 06/27/14 16:44CCB U -0.0003 0.0003mg/L

WG366565CCV3 06/27/14 17:07 95.2CCV MS140513-2 .09544 90 110mg/L.1002

WG366565CCB3 06/27/14 17:10CCB U -0.0003 0.0003mg/L

Page 10 of 35L18774-1407011208


Inorganic QC

Summary




WG365697

WG365697ICV 06/11/14 17:46 99.7ICV II140512-2 99.72 95 105mg/L100

WG365697ICB 06/11/14 17:52ICB U -0.3 0.3mg/L

WG365697PQV 06/11/14 17:55 82PQV II140609-2 .41 70 130mg/L.5002

WG365697SIC 06/11/14 17:58 100.4SIC II140602-1 201.3 1 200mg/L200.5002

WG365697LFB 06/11/14 18:05 106.9LFB II140530-2 72.7 85 115mg/L67.98099

WG365697CCV1 06/11/14 18:36 99.4CCV II140506-1 49.68 90 110mg/L50

WG365697CCB1 06/11/14 18:39CCB U -0.3 0.3mg/L

L18774-01AS 06/11/14 19:08 163 97.4AS II140530-2 229.2 85 115mg/L67.98099

L18774-01ASD 06/11/14 19:12 163 96.1ASD II140530-2 228.3 0.3985 115mg/L 2067.98099

WG365697CCV2 06/11/14 19:15 99.3CCV II140506-1 49.66 90 110mg/L50

WG365697CCB2 06/11/14 19:18CCB U -0.3 0.3mg/L

WG365697CCV3 06/11/14 19:28 99.2CCV II140506-1 49.58 90 110mg/L50

WG365697CCB3 06/11/14 19:31CCB U -0.3 0.3mg/L



WG358122

WG358122ICV 01/22/14 11:52 102ICV WI131209-3 102 90 110mg/L100

WG358122ICB 01/22/14 11:52ICB U -3 3mg/L

WG366155

WG366155CCV1 06/18/14 23:09 96.4CCV WI140502-1 48.2 90 110mg/L50

WG366155CCB1 06/18/14 23:09CCB U -3 3mg/L

WG366155PQV 06/18/14 23:09 96PQV WI140502-3 4.8 70 130mg/L5

WG366155LFB1 06/18/14 23:09 95.4LFB WI140502-2 47.7 90 110mg/L50

L18793-03DUP RA06/18/14 23:09 4.8DUP 4.7 2.1mg/L 20

WG366155CCV2 06/18/14 23:09 95.2CCV WI140502-1 47.6 90 110mg/L50

WG366155CCB2 06/18/14 23:09CCB U -3 3mg/L

L18795-08AS 06/18/14 23:09 5.1 96.2AS WI140502-2 53.2 90 110mg/L50

WG366155CCV3 06/18/14 23:09 96CCV WI140502-1 48 90 110mg/L50

WG366155CCB3 06/18/14 23:09CCB U -3 3mg/L

WG366155LFB2 06/18/14 23:09 96.6LFB WI140502-2 48.3 90 110mg/L50

WG366155CCV4 06/18/14 23:09 95.4CCV WI140502-1 47.7 90 110mg/L50

WG366155CCB4 06/18/14 23:09CCB U -3 3mg/L

WG366155CCV5 06/18/14 23:09 93.8CCV WI140502-1 46.9 90 110mg/L50

WG366155CCB5 06/18/14 23:09CCB U -3 3mg/L

Page 11 of 35L18774-1407011208


Inorganic QC

Summary




WG366565

WG366565ICV 06/27/14 15:26 107.2ICV MS140513-1 .05361 90 110mg/L.05

WG366565ICB 06/27/14 15:29ICB U -0.0006 0.0006mg/L

WG366565LFB 06/27/14 15:33 99.9LFB MS140625-3 .04996 85 115mg/L.05

L18774-03AS 06/27/14 15:46 U 102.2AS MS140625-3 .05111 70 130mg/L.05

L18774-03ASD 06/27/14 15:49 U 104.6ASD MS140625-3 .05231 2.3270 130mg/L 20.05

WG366565CCV1 06/27/14 16:02 97.2CCV MS140513-2 .09715 90 110mg/L.1

WG366565CCB1 06/27/14 16:05CCB U -0.0006 0.0006mg/L

WG366565CCV2 06/27/14 16:41 99.3CCV MS140513-2 .09931 90 110mg/L.1

WG366565CCB2 06/27/14 16:44CCB U -0.0006 0.0006mg/L

WG366565CCV3 06/27/14 17:07 98.5CCV MS140513-2 .09854 90 110mg/L.1

WG366565CCB3 06/27/14 17:10CCB U -0.0006 0.0006mg/L

Chloride SM4500Cl-E


WG366442

WG366442ICB 06/24/14 17:19ICB U -1.5 1.5mg/L

WG366442ICV 06/24/14 17:19 106.6ICV WI130722-5 58.57 90 110mg/L54.945

WG366442CCV1 06/24/14 18:47 108CCV WI131028-1 53.98 90 110mg/L50

WG366442CCB1 06/24/14 18:47CCB U -1.5 1.5mg/L

WG366442LFB1 06/24/14 18:47 107.8LFB WI140508-1 32.33 90 110mg/L30

L18774-02DUP 06/24/14 18:47 36.4DUP 36.1 0.8mg/L 20

WG366442CCV2 06/24/14 18:49 107.6CCV WI131028-1 53.82 90 110mg/L50

WG366442CCB2 06/24/14 18:49CCB U -1.5 1.5mg/L

WG366442CCV3 06/24/14 18:51 108CCV WI131028-1 54 90 110mg/L50

WG366442CCB3 06/24/14 18:51CCB U -1.5 1.5mg/L

WG366442LFB2 06/24/14 18:51 109.7LFB WI140508-1 32.92 90 110mg/L30

WG366442CCV4 06/24/14 18:57 107.5CCV WI131028-1 53.77 90 110mg/L50

WG366442CCB4 06/24/14 18:57CCB U -1.5 1.5mg/L

WG366442CCV5 06/24/14 18:58 108CCV WI131028-1 54 90 110mg/L50

WG366442CCB5 06/24/14 18:58CCB U -1.5 1.5mg/L

L18774-01AS 06/24/14 18:58 175 99.3AS 10XCL 204.8 90 110mg/L30

WG366442CCV6 06/24/14 18:59 107.6CCV WI131028-1 53.81 90 110mg/L50

WG366442CCB6 06/24/14 18:59CCB U -1.5 1.5mg/L

WG366442CCV7 06/24/14 19:07 108.5CCV WI131028-1 54.23 90 110mg/L50

WG366442CCB7 06/24/14 19:07CCB U -1.5 1.5mg/L

WG366442CCV8 06/24/14 19:28 107.2CCV WI131028-1 53.61 90 110mg/L50

WG366442CCB8 06/24/14 19:28CCB U -1.5 1.5mg/L

WG366442CCV9 06/24/14 19:29 107.5CCV WI131028-1 53.76 90 110mg/L50

WG366442CCB9 06/24/14 19:29CCB U -1.5 1.5mg/L

WG366442CCV10 06/24/14 19:55 107.5CCV WI131028-1 53.75 90 110mg/L50

WG366442CCB10 06/24/14 19:55CCB U -1.5 1.5mg/L

WG366442CCV11 06/24/14 19:56 106.9CCV WI131028-1 53.47 90 110mg/L50

WG366442CCB11 06/24/14 19:56CCB U -1.5 1.5mg/L

Page 12 of 35L18774-1407011208


Inorganic QC

Summary




WG365724

WG365724ICV 06/12/14 15:56 97.1ICV II140512-2 1.942 95 105mg/L2

WG365724ICB 06/12/14 16:02ICB U -0.03 0.03mg/L

WG365724PQV 06/12/14 16:05 89.8PQV II140609-2 .045 70 130mg/L.0501

WG365724SIC 06/12/14 16:08 92.8SIC II140602-1 .093 80 120mg/L.1002

WG365724LFB 06/12/14 16:14 99.6LFB II140611-2 .499 85 115mg/L.501

L18774-02AS 06/12/14 16:30 U 98.8AS II140611-2 .495 85 115mg/L.501

L18774-02ASD 06/12/14 16:33 U 98.8ASD II140611-2 .495 085 115mg/L 20.501

WG365724CCV 06/12/14 16:39 97CCV II140506-1 .97 90 110mg/L1

WG365724CCB 06/12/14 16:42CCB U -0.03 0.03mg/L



WG365668

WG365668ICV 06/11/14 14:10 94.7ICV II140512-2 1.894 95 105mg/L2

WG365668ICB 06/11/14 14:16ICB U -0.03 0.03mg/L

WG365668PQV 06/11/14 14:19 96PQV II140609-2 .048 70 130mg/L.05

WG365668SIC 06/11/14 14:22 95SIC II140602-1 .095 80 120mg/L.1

WG365668LFB 06/11/14 14:28 97.2LFB II140530-2 .486 85 115mg/L.5

WG365668CCV1 06/11/14 15:00 95.3CCV II140506-1 .953 90 110mg/L1

WG365668CCB1 06/11/14 15:03CCB U -0.03 0.03mg/L

WG365668CCV2 06/11/14 15:39 95.5CCV II140506-1 .955 90 110mg/L1

WG365668CCB2 06/11/14 15:42CCB U -0.03 0.03mg/L

L18774-01AS M206/11/14 15:48 U 79.6AS II140530-2 .398 85 115mg/L.5

L18774-01ASD M206/11/14 15:51 U 82.4ASD II140530-2 .412 3.4685 115mg/L 20.5

WG365668CCV3 06/11/14 16:01 95.8CCV II140506-1 .958 90 110mg/L1

WG365668CCB3 06/11/14 16:04CCB U -0.03 0.03mg/L

Page 13 of 35L18774-1407011208


Inorganic QC

Summary


Fluoride SM4500F-C


WG366490

WG366490ICV 06/25/14 12:28 99.8ICV WC140616- 1.996 95 105mg/L2

WG366490ICB 06/25/14 12:32ICB U -0.15 0.15mg/L

WG366490PQV 06/25/14 12:37 93.3PQV WC140624- .234 70 130mg/L.25075

L18774-01AS M206/25/14 12:46 .46 77AS WC140501- 4.324 90 110mg/L5.015

WG366490LFB1 06/25/14 12:51 92.7LFB WC140501- 4.65 90 110mg/L5.015

L18774-01DUP RA06/25/14 12:54 .46DUP .388 17mg/L 20

WG366490CCV1 06/25/14 13:20 98.5CCV WC140616- 1.969 90 110mg/L2

WG366490CCB1 06/25/14 13:28CCB U -0.15 0.15mg/L

WG366490CCV2 06/25/14 14:25 101.2CCV WC140616- 2.023 90 110mg/L2

WG366490CCB2 06/25/14 14:32CCB U -0.15 0.15mg/L

WG366490LFB2 06/25/14 15:02 91.4LFB WC140501- 4.586 90 110mg/L5.015

WG366490CCV3 06/25/14 15:21 99.4CCV WC140616- 1.987 90 110mg/L2

WG366490CCB3 06/25/14 15:29CCB U -0.15 0.15mg/L

WG366490CCV4 06/25/14 16:30 101.2CCV WC140616- 2.023 90 110mg/L2

WG366490CCB4 06/25/14 16:37CCB U -0.15 0.15mg/L

WG366490CCV5 06/25/14 17:16 99.4CCV WC140616- 1.987 90 110mg/L2

WG366490CCB5 06/25/14 17:24CCB U -0.15 0.15mg/L

WG366490CCV6 06/25/14 17:34 101.6CCV WC140616- 2.032 90 110mg/L2

WG366490CCB6 06/25/14 17:42CCB U -0.15 0.15mg/L



WG365668

WG365668ICV 06/11/14 14:10 96.3ICV II140512-2 1.926 95 105mg/L2

WG365668ICB 06/11/14 14:16ICB U -0.06 0.06mg/L

WG365668PQV 06/11/14 14:19 89.9PQV II140609-2 .045 70 130mg/L.05007

WG365668SIC 06/11/14 14:22 92.7SIC II140602-1 185.7 1 200mg/L200.33007

WG365668LFB 06/11/14 14:28 97.7LFB II140530-2 .978 85 115mg/L1.0014

WG365668CCV1 06/11/14 15:00 98.4CCV II140506-1 .984 90 110mg/L1

WG365668CCB1 06/11/14 15:03CCB U -0.06 0.06mg/L

WG365668CCV2 06/11/14 15:39 98.9CCV II140506-1 .989 90 110mg/L1

WG365668CCB2 06/11/14 15:42CCB U -0.06 0.06mg/L

L18774-01AS 06/11/14 15:48 U 96.6AS II140530-2 .967 85 115mg/L1.0014

L18774-01ASD 06/11/14 15:51 U 98.7ASD II140530-2 .988 2.1585 115mg/L 201.0014

WG365668CCV3 06/11/14 16:01 99.6CCV II140506-1 .996 90 110mg/L1

WG365668CCB3 06/11/14 16:04CCB U -0.06 0.06mg/L

Page 14 of 35L18774-1407011208


Inorganic QC

Summary




WG366565

WG366565ICV 06/27/14 15:26 102.7ICV MS140513-1 .05133 90 110mg/L.05

WG366565ICB 06/27/14 15:29ICB U -0.0003 0.0003mg/L

WG366565LFB 06/27/14 15:33 95.5LFB MS140625-3 .04782 85 115mg/L.05005

L18774-03AS 06/27/14 15:46 U 96.8AS MS140625-3 .04843 70 130mg/L.05005

L18774-03ASD 06/27/14 15:49 U 98.2ASD MS140625-3 .04915 1.4870 130mg/L 20.05005

WG366565CCV1 06/27/14 16:02 96.3CCV MS140513-2 .241 90 110mg/L.25025

WG366565CCB1 06/27/14 16:05CCB U -0.0003 0.0003mg/L

WG366565CCV2 06/27/14 16:41 95.9CCV MS140513-2 .2401 90 110mg/L.25025

WG366565CCB2 06/27/14 16:44CCB U -0.0003 0.0003mg/L

WG366565CCV3 06/27/14 17:07 94.2CCV MS140513-2 .2358 90 110mg/L.25025

WG366565CCB3 06/27/14 17:10CCB U -0.0003 0.0003mg/L



WG365668

WG365668ICV 06/11/14 14:10 97.2ICV II140512-2 97.15 95 105mg/L100

WG365668ICB 06/11/14 14:16ICB U -0.6 0.6mg/L

WG365668PQV 06/11/14 14:19 80.9PQV II140609-2 .81 70 130mg/L1.0007

WG365668SIC 06/11/14 14:22 99.7SIC II140602-1 200.5 1 200mg/L201.1407

WG365668LFB 06/11/14 14:28 99.1LFB II140530-2 49.55 85 115mg/L50.00131

WG365668CCV1 06/11/14 15:00 97.2CCV II140506-1 48.61 90 110mg/L50

WG365668CCB1 06/11/14 15:03CCB U -0.6 0.6mg/L

WG365668CCV2 06/11/14 15:39 98.2CCV II140506-1 49.1 90 110mg/L50

WG365668CCB2 06/11/14 15:42CCB U -0.6 0.6mg/L

L18774-01AS M306/11/14 15:48 325 80.6AS II140530-2 365.3 85 115mg/L50.00131

L18774-01ASD 06/11/14 15:51 325 92.6ASD II140530-2 371.3 1.6385 115mg/L 2050.00131

WG365668CCV3 06/11/14 16:01 98.5CCV II140506-1 49.24 90 110mg/L50

WG365668CCB3 06/11/14 16:04CCB U -0.6 0.6mg/L



WG365668

WG365668ICV 06/11/14 14:10 96ICV II140512-2 1.9198 95 105mg/L2

WG365668ICB 06/11/14 14:16ICB U -0.015 0.015mg/L

WG365668PQV 06/11/14 14:19 88.8PQV II140609-2 .0222 70 130mg/L.025

WG365668SIC 06/11/14 14:22 97.3SIC II140602-1 48.79 1 200mg/L50.125

WG365668LFB 06/11/14 14:28 98.5LFB II140530-2 .4936 85 115mg/L.501

WG365668CCV1 06/11/14 15:00 98.3CCV II140506-1 .9829 90 110mg/L1

WG365668CCB1 06/11/14 15:03CCB U -0.015 0.015mg/L

WG365668CCV2 06/11/14 15:39 98.6CCV II140506-1 .986 90 110mg/L1

WG365668CCB2 06/11/14 15:42CCB U -0.015 0.015mg/L

L18774-01AS 06/11/14 15:48 .01 97.5AS II140530-2 .4987 85 115mg/L.501

L18774-01ASD 06/11/14 15:51 .01 99.4ASD II140530-2 .508 1.8585 115mg/L 20.501

WG365668CCV3 06/11/14 16:01 98.9CCV II140506-1 .9894 90 110mg/L1

WG365668CCB3 06/11/14 16:04CCB U -0.015 0.015mg/L

Page 15 of 35L18774-1407011208


Inorganic QC

Summary




WG366022

WG366022ICV2 06/18/14 10:00 95.9ICV II140616-2 .0048 95 105mg/L.005005

WG366022ICB 06/18/14 10:02ICB U -0.0002 0.0002mg/L

WG366099

WG366099CCV1 06/18/14 14:00 93.1CCV II140616-2 .00466 90 110mg/L.005005

WG366099CCB1 06/18/14 14:02CCB U -0.0002 0.0002mg/L

WG366099LRB 06/18/14 14:04LRB U -0.00044 0.00044mg/L

WG366099LFB 06/18/14 14:06 96.9LFB II140616-4 .00194 85 115mg/L.002002

L18774-03LFM 06/18/14 14:14 U 98.9LFM II140616-4 .00198 85 115mg/L.002002


WG366099CCV2 06/18/14 14:24 95.3CCV II140616-2 .00477 90 110mg/L.005005

WG366099CCB2 06/18/14 14:26CCB U -0.0002 0.0002mg/L

WG366099CCV3 06/18/14 14:49 94.5CCV II140616-2 .00473 90 110mg/L.005005

WG366099CCB3 06/18/14 14:52CCB U -0.0002 0.0002mg/L

WG366099CCV4 06/18/14 15:05 94.9CCV II140616-2 .00475 90 110mg/L.005005

WG366099CCB4 06/18/14 15:07CCB U -0.0002 0.0002mg/L



WG365668

WG365668ICV 06/11/14 14:10 98ICV II140512-2 1.96 95 105mg/L2

WG365668ICB 06/11/14 14:16ICB U -0.06 0.06mg/L

WG365668PQV 06/11/14 14:19 99PQV II140609-2 .099 70 130mg/L.1

WG365668SIC 06/11/14 14:22 96SIC II140602-1 .096 80 120mg/L.1

WG365668LFB 06/11/14 14:28 98.5LFB II140530-2 .492 85 115mg/L.4995

WG365668CCV1 06/11/14 15:00 98.5CCV II140506-1 .985 90 110mg/L1

WG365668CCB1 06/11/14 15:03CCB U -0.06 0.06mg/L

WG365668CCV2 06/11/14 15:39 99.3CCV II140506-1 .993 90 110mg/L1

WG365668CCB2 06/11/14 15:42CCB U -0.06 0.06mg/L

L18774-01AS 06/11/14 15:48 U 96.3AS II140530-2 .481 85 115mg/L.4995

L18774-01ASD 06/11/14 15:51 U 98.3ASD II140530-2 .491 2.0685 115mg/L 20.4995

WG365668CCV3 06/11/14 16:01 99.7CCV II140506-1 .997 90 110mg/L1

WG365668CCB3 06/11/14 16:04CCB U -0.06 0.06mg/L

Page 16 of 35L18774-1407011208


Inorganic QC

Summary




WG365668

WG365668ICV 06/11/14 14:10 96.7ICV II140512-2 1.933 95 105mg/L2

WG365668ICB 06/11/14 14:16ICB U -0.024 0.024mg/L

WG365668PQV 06/11/14 14:19 100.3PQV II140609-2 .0401 70 130mg/L.04

WG365668SIC 06/11/14 14:22 92SIC II140602-1 .092 80 120mg/L.1

WG365668LFB 06/11/14 14:28 100.6LFB II140530-2 .5028 85 115mg/L.5

WG365668CCV1 06/11/14 15:00 99.2CCV II140506-1 .9924 90 110mg/L1

WG365668CCB1 06/11/14 15:03CCB U -0.024 0.024mg/L

WG365668CCV2 06/11/14 15:39 100.9CCV II140506-1 1.009 90 110mg/L1

WG365668CCB2 06/11/14 15:42CCB U -0.024 0.024mg/L

L18774-01AS 06/11/14 15:48 U 96.4AS II140530-2 .4819 85 115mg/L.5

L18774-01ASD 06/11/14 15:51 U 100.2ASD II140530-2 .5011 3.9185 115mg/L 20.5

WG365668CCV3 06/11/14 16:01 101.1CCV II140506-1 1.011 90 110mg/L1

WG365668CCB3 06/11/14 16:04CCB U -0.024 0.024mg/L



WG366626

WG366626ICV 06/26/14 21:09 97.5ICV WI140417-3 2.356 90 110mg/L2.416

WG366626ICB 06/26/14 21:11ICB U -0.06 0.06mg/L

WG366634

WG366634CCV1 06/26/14 22:44 99.8CCV WI140625-1 1.996 90 110mg/L2

WG366634CCB1 06/26/14 22:45CCB U -0.06 0.06mg/L

WG366634LFB1 06/26/14 22:46 99.6LFB WI140215-3 1.991 90 110mg/L2

L18774-01AS 06/26/14 22:49 U 101.8AS WI140215-3 2.036 90 110mg/L2

L18774-02DUP 06/26/14 22:51 1.47DUP 1.468 0.1mg/L 20

WG366634CCV2 06/26/14 22:58 99.7CCV WI140625-1 1.994 90 110mg/L2

WG366634CCB2 06/26/14 22:59CCB U -0.06 0.06mg/L

WG366634CCV3 06/26/14 23:12 101.1CCV WI140625-1 2.021 90 110mg/L2

WG366634CCB3 06/26/14 23:13CCB U -0.06 0.06mg/L

WG366634LFB2 06/26/14 23:21 99.3LFB WI140215-3 1.986 90 110mg/L2

WG366634CCV4 06/26/14 23:26 101.5CCV WI140625-1 2.03 90 110mg/L2

WG366634CCB4 06/26/14 23:28CCB U -0.06 0.06mg/L

WG366634CCV5 06/26/14 23:38 100.5CCV WI140625-1 2.009 90 110mg/L2

WG366634CCB5 06/26/14 23:39CCB U -0.06 0.06mg/L

WG366634CCV6 06/26/14 23:44 100CCV WI140625-1 1.999 90 110mg/L2

WG366634CCB6 06/26/14 23:45CCB U -0.06 0.06mg/L

WG366634CCV7 06/26/14 23:50 100CCV WI140625-1 1.999 90 110mg/L2

WG366634CCB7 06/26/14 23:51CCB U -0.06 0.06mg/L

Page 17 of 35L18774-1407011208


Inorganic QC

Summary




WG366600

WG366600ICV 06/26/14 15:52 98.4ICV WI131021-1 .987 90 110mg/L1.003

WG366600ICB 06/26/14 15:55ICB U -0.15 0.15mg/L

WG366600LFB1 06/26/14 15:56 99.2LFB WI140113-8 .992 90 110mg/L1

L18718-01AS 06/26/14 15:58 U 95.8AS WI140113-8 .958 90 110mg/L1

L18732-02DUP RA06/26/14 16:01 .24DUP .263 9.1mg/L 20

WG366600CCV1 06/26/14 16:07 102.3CCV WI140113-6 2.045 90 110mg/L2

WG366600CCB1 06/26/14 16:08CCB U -0.15 0.15mg/L

WG366600CCV2 06/26/14 16:20 103.8CCV WI140113-6 2.075 90 110mg/L2

WG366600CCB2 06/26/14 16:21CCB U -0.15 0.15mg/L

WG366600LFB2 06/26/14 16:28 99.2LFB WI140113-8 .992 90 110mg/L1

WG366600CCV3 06/26/14 16:33 100.8CCV WI140113-6 2.016 90 110mg/L2

WG366600CCB3 06/26/14 16:34CCB U -0.15 0.15mg/L

WG366600CCV4 06/26/14 16:46 100.8CCV WI140113-6 2.015 90 110mg/L2

WG366600CCB4 06/26/14 16:47CCB U -0.15 0.15mg/L



WG365668

WG365668ICV 06/11/14 14:10 98.6ICV II140512-2 19.71 95 105mg/L20

WG365668ICB 06/11/14 14:16ICB U -0.6 0.6mg/L

WG365668PQV 06/11/14 14:19 93PQV II140609-2 .93 70 130mg/L1

WG365668SIC 06/11/14 14:22 90SIC II140602-1 .9 80 120mg/L1

WG365668LFB 06/11/14 14:28 100LFB II140530-2 100 85 115mg/L99.99364

WG365668CCV1 06/11/14 15:00 99.1CCV II140506-1 9.91 90 110mg/L10

WG365668CCB1 06/11/14 15:03CCB U -0.6 0.6mg/L

WG365668CCV2 06/11/14 15:39 98.6CCV II140506-1 9.86 90 110mg/L10

WG365668CCB2 06/11/14 15:42CCB U -0.6 0.6mg/L

L18774-01AS 06/11/14 15:48 99.7 99.8AS II140530-2 199.5 85 115mg/L99.99364

L18774-01ASD 06/11/14 15:51 99.7 102.6ASD II140530-2 202.3 1.3985 115mg/L 2099.99364

WG365668CCV3 06/11/14 16:01 98.7CCV II140506-1 9.87 90 110mg/L10

WG365668CCB3 06/11/14 16:04CCB U -0.6 0.6mg/L



WG365787

WG365787PBW 06/12/14 16:05PBW U -20 20mg/L


L18838-03DUP 06/12/14 17:05 580DUP 628 7.9mg/L 10

WG366006

WG366006PBW 06/17/14 11:05PBW U -20 20mg/L


L18793-01DUP 06/17/14 11:31 4790DUP 4952 3.3mg/L 10

Page 18 of 35L18774-1407011208


Inorganic QC

Summary




WG365821

WG365821PBW 06/13/14 8:50PBW U -6 6mg/L

WG365821LCSW 06/13/14 8:52 95LCSW PCN45833 152 80 120mg/L160

L18774-01DUP RA06/13/14 9:16 9DUP 6 40mg/L 10

L18793-04DUP RA06/13/14 9:31 9DUP 9 0mg/L 10



WG366565

WG366565ICV 06/27/14 15:26 103.9ICV MS140513-1 .05193 90 110mg/L.05

WG366565ICB 06/27/14 15:29ICB U -0.0003 0.0003mg/L

WG366565LFB 06/27/14 15:33 97.4LFB MS140625-3 .04873 85 115mg/L.05005

L18774-03AS 06/27/14 15:46 .0089 101.6AS MS140625-3 .05976 70 130mg/L.05005

L18774-03ASD 06/27/14 15:49 .0089 102.4ASD MS140625-3 .06016 0.6770 130mg/L 20.05005

WG366565CCV1 06/27/14 16:02 95.4CCV MS140513-2 .2388 90 110mg/L.25025

WG366565CCB1 06/27/14 16:05CCB U -0.0003 0.0003mg/L

WG366565CCV2 06/27/14 16:41 96.3CCV MS140513-2 .241 90 110mg/L.25025

WG366565CCB2 06/27/14 16:44CCB U -0.0003 0.0003mg/L

WG366565CCV3 06/27/14 17:07 96.3CCV MS140513-2 .241 90 110mg/L.25025

WG366565CCB3 06/27/14 17:10CCB .00017 -0.0003 0.0003mg/L



WG365668

WG365668ICV 06/11/14 14:10 99.3ICV II140512-2 42.51 95 105mg/L42.8

WG365668ICB 06/11/14 14:16ICB U -0.6 0.6mg/L

WG365668PQV 06/11/14 14:19 102.7PQV II140609-2 1.1 70 130mg/L1.0714

WG365668SIC 06/11/14 14:22 98SIC II140602-1 1.05 80 120mg/L1.0714

WG365668LFB 06/11/14 14:28 100.7LFB II140530-2 21.57 85 115mg/L21.428

WG365668CCV1 06/11/14 15:00 100.7CCV II140506-1 21.55 90 110mg/L21.4

WG365668CCB1 06/11/14 15:03CCB U -0.6 0.6mg/L

WG365668CCV2 06/11/14 15:39 100.1CCV II140506-1 21.43 90 110mg/L21.4

WG365668CCB2 06/11/14 15:42CCB U -0.6 0.6mg/L

L18774-01AS 06/11/14 15:48 9.6 101.5AS II140530-2 31.35 85 115mg/L21.428

L18774-01ASD 06/11/14 15:51 9.6 103.9ASD II140530-2 31.86 1.6185 115mg/L 2021.428

WG365668CCV3 06/11/14 16:01 100.6CCV II140506-1 21.52 90 110mg/L21.4

WG365668CCB3 06/11/14 16:04CCB U -0.6 0.6mg/L

Page 19 of 35L18774-1407011208


Inorganic QC

Summary




WG365668

WG365668ICV 06/11/14 14:10 99.1ICV II140512-2 99.14 95 105mg/L100

WG365668ICB 06/11/14 14:16ICB U -0.6 0.6mg/L

WG365668PQV 06/11/14 14:19 101.9PQV II140609-2 1.02 70 130mg/L1.001

WG365668SIC 06/11/14 14:22 101.9SIC II140602-1 1.02 80 120mg/L1.001

WG365668LFB 06/11/14 14:28 100.3LFB II140530-2 100.3 85 115mg/L100.0393

WG365668CCV1 06/11/14 15:00 99.5CCV II140506-1 49.76 90 110mg/L50

WG365668CCB1 06/11/14 15:03CCB U -0.6 0.6mg/L

WG365668CCV2 06/11/14 15:39 99.2CCV II140506-1 49.62 90 110mg/L50

WG365668CCB2 06/11/14 15:42CCB U -0.6 0.6mg/L

L18774-01AS 06/11/14 15:48 214 99.7AS II140530-2 313.7 85 115mg/L100.0393

L18774-01ASD 06/11/14 15:51 214 105.5ASD II140530-2 319.5 1.8385 115mg/L 20100.0393

WG365668CCV3 06/11/14 16:01 99.6CCV II140506-1 49.8 90 110mg/L50

WG365668CCB3 06/11/14 16:04CCB U -0.6 0.6mg/L



WG365730

WG365730PBW 06/12/14 13:50PBW U -30 30mg/L


L18774-03DUP 06/12/14 14:29 440DUP 456 3.6mg/L 20



WG365635

WG365635ICV 06/11/14 9:10 98.1ICV WC140610- .293 90 110mg/L.29866

WG365635ICB 06/11/14 9:15ICB U -0.06 0.06mg/L

WG365635LFB 06/11/14 9:20 115.5LFB WC140610- .268 80 120mg/L.232

WG365635CCV1 06/11/14 10:13 102.9CCV WC140610- .179 90 110mg/L.174

WG365635CCB1 06/11/14 10:18CCB U -0.06 0.06mg/L

L18785-06AS 06/11/14 10:29 U 117.8AS WC140610- 2.05 75 125mg/L1.74

L18785-06DUP RA06/11/14 10:34 UDUP U 0mg/L 20

WG365635CCV2 06/11/14 11:16 100.6CCV WC140610- .175 90 110mg/L.174

WG365635CCB2 06/11/14 11:22CCB U -0.06 0.06mg/L

WG365635CCV3 06/11/14 11:53 100CCV WC140610- .174 90 110mg/L.174

WG365635CCB3 06/11/14 11:59CCB U -0.06 0.06mg/L

Page 20 of 35L18774-1407011208


Inorganic QC

Summary




WG366565

WG366565ICV 06/27/14 15:26 104.3ICV MS140513-1 .05217 90 110mg/L.05

WG366565ICB 06/27/14 15:29ICB U -0.0003 0.0003mg/L

WG366565LFB 06/27/14 15:33 97.4LFB MS140625-3 .04877 85 115mg/L.05005

L18774-03AS 06/27/14 15:46 .0283 102.7AS MS140625-3 .07971 70 130mg/L.05005

L18774-03ASD 06/27/14 15:49 .0283 104ASD MS140625-3 .08033 0.7770 130mg/L 20.05005

WG366565CCV1 06/27/14 16:02 96.1CCV MS140513-2 .0961 90 110mg/L.1

WG366565CCB1 06/27/14 16:05CCB U -0.0003 0.0003mg/L

WG366565CCV2 06/27/14 16:41 95.8CCV MS140513-2 .09576 90 110mg/L.1

WG366565CCB2 06/27/14 16:44CCB U -0.0003 0.0003mg/L

WG366565CCV3 06/27/14 17:07 94CCV MS140513-2 .09401 90 110mg/L.1

WG366565CCB3 06/27/14 17:10CCB U -0.0003 0.0003mg/L



WG365668

WG365668ICV 06/11/14 14:10 98ICV II140512-2 1.9595 95 105mg/L2

WG365668ICB 06/11/14 14:16ICB U -0.015 0.015mg/L

WG365668PQV 06/11/14 14:19 101.6PQV II140609-2 .0254 70 130mg/L.025

WG365668SIC 06/11/14 14:22 99.3SIC II140602-1 .0993 80 120mg/L.1

WG365668LFB 06/11/14 14:28 100.2LFB II140530-2 .5009 85 115mg/L.5

WG365668CCV1 06/11/14 15:00 99CCV II140506-1 .9903 90 110mg/L1

WG365668CCB1 06/11/14 15:03CCB U -0.015 0.015mg/L

WG365668CCV2 06/11/14 15:39 99.3CCV II140506-1 .993 90 110mg/L1

WG365668CCB2 06/11/14 15:42CCB U -0.015 0.015mg/L

L18774-01AS 06/11/14 15:48 U 99.5AS II140530-2 .4977 85 115mg/L.5

L18774-01ASD 06/11/14 15:51 U 101.4ASD II140530-2 .5068 1.8185 115mg/L 20.5

WG365668CCV3 06/11/14 16:01 99.3CCV II140506-1 .993 90 110mg/L1

WG365668CCB3 06/11/14 16:04CCB U -0.015 0.015mg/L



WG365668

WG365668ICV 06/11/14 14:10 97.2ICV II140512-2 1.944 95 105mg/L2

WG365668ICB 06/11/14 14:16ICB U -0.03 0.03mg/L

WG365668PQV 06/11/14 14:19 98PQV II140609-2 .049 70 130mg/L.05

WG365668SIC 06/11/14 14:22 97SIC II140602-1 .097 80 120mg/L.1

WG365668LFB 06/11/14 14:28 100.9LFB II140530-2 .505 85 115mg/L.5005

WG365668CCV1 06/11/14 15:00 97.7CCV II140506-1 .977 90 110mg/L1

WG365668CCB1 06/11/14 15:03CCB U -0.03 0.03mg/L

WG365668CCV2 06/11/14 15:39 98.2CCV II140506-1 .982 90 110mg/L1

WG365668CCB2 06/11/14 15:42CCB U -0.03 0.03mg/L

L18774-01AS 06/11/14 15:48 U 101.1AS II140530-2 .506 85 115mg/L.5005

L18774-01ASD 06/11/14 15:51 U 103.3ASD II140530-2 .517 2.1585 115mg/L 20.5005

WG365668CCV3 06/11/14 16:01 98.8CCV II140506-1 .988 90 110mg/L1

WG365668CCB3 06/11/14 16:04CCB U -0.03 0.03mg/L

Page 21 of 35L18774-1407011208


Inorganic Extended

Qualifier Report



M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable.

M200.7 ICPCopper, dissolvedL18774-01 WG365668


M200.7 ICPMagnesium, dissolved






SM4500F-C








SM2320B - TitrationTotal AlkalinityWG366038










SM4500F-C









REPAD.15.06.05.01

Page 22 of 35L18774-1407011208


Inorganic Extended

Qualifier Report












SM4500F-C



HC Initial analysis within holding time. Reanalysis was past holding time, which was required due to a QC failure during the initial analysis.




QD Reported value is the background-corrected concentration, as described by the method.



SM4500S2-D



REPAD.15.06.05.01

Page 23 of 35L18774-1407011208


Sample ID: MW6



Project ID:


Date Sampled: 06/06/14 10:35


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 0.0 9.4 9.7 pCi/L nco06/23/14 12:53

Gross Beta 98 18 20 pCi/L nco06/23/14 12:53

Lead 210, dissolved

EICHROM, OTW01

Prep Method:




M903.1

Prep Method:


Radium 226, dissolved 2.7 0.24 0.23 pCi/L nco06/24/14 9:41


M904.0

Prep Method:


Radium 228, dissolved 5.5 0.78 0.5 pCi/L * thf06/24/14 12:05


ESM 4506

Prep Method:




Page 24 of 35L18774-1407011208


Sample ID: PW1



Project ID:


Date Sampled: 06/06/14 13:45


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 39 8.3 3 pCi/L nco06/23/14 12:55

Gross Beta 23 5.5 6.2 pCi/L nco06/23/14 12:55

Lead 210, dissolved

EICHROM, OTW01

Prep Method:




M903.1

Prep Method:




M904.0

Prep Method:




ESM 4506

Prep Method:




Page 25 of 35L18774-1407011208


Sample ID: PW2



Project ID:


Date Sampled: 06/06/14 12:40


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 15 5.7 3.1 pCi/L nco06/23/14 12:56

Gross Beta 24 5.3 6 pCi/L nco06/23/14 12:56

Lead 210, dissolved

EICHROM, OTW01

Prep Method:


Lead 210, dissolved -1 2.2 6.8 pCi/L * jrd06/24/14 15:58


M903.1

Prep Method:




M904.0

Prep Method:




ESM 4506

Prep Method:




Page 26 of 35L18774-1407011208






Limit Upper limit for RPD, in % .

LCL Lower Control Limit, in % ( except for LCSS, mg /Kg )


P CN/SCN A numb er assig ned to reag ents/standards to trace to the manufacturer's certificate of analy sis


QC True V alue of the Control Sample or the amount added to the Spik e

Rec Amount of the true value or spik e added recovered, in % ( except for LCSS, mg /Kg )

RER Relative Error Ratio, calculation used for Dup. QC tak ing into account the error factor.

RP D Relative Percent Difference, calculation used for Duplicate QC Ty pes

UCL U pper Control Limit, in % ( except for LCSS, mg /Kg )

Sample V alue of the Sample of interest

QC Sample Types

DUP Sample Duplicate MS/MSD Matrix Spik e/Matrix Spik e Duplicate

LCSS Lab oratory Control Sample - Soil P BS Prep Blank - Soil

LCSW Lab oratory Control Sample - Water P BW Prep Blank - Water


Blank s V erifies that there is no or minimal contamination in the prep method procedure.

Control Samples V erifies the accuracy of the method, including the prep procedure.

Duplicates V erifies the precision of the instrument and/or method.

Matrix Spik es Determines sample matrix interferences, if any .


H Analy sis exceeded method hold time.


M EPA methodolog y , including those under SDWA, CWA, and RCRA


D ASTM

RP DOE

ESM DOE/ESM

Comments

( 1) Solid matrices are reported on a dry weig ht b asis.

( 2) Preparation method: "Method" indicates preparation defined in analy tical method.

( 3) QC results calculated from raw data. Results may vary slig htly if the rounded values are used in the calculations.

( 4) An asterisk in the "XQ" column indicates there is an extended q ualifier and/or certification

q ualifier associated with the result.

For a complete list of ACZ's Extended Qualifiers, please click : http://www.acz.com/pub lic/extq uallist.pdf

REP003.09.12.01

Radiochemistry

Reference

Page 27 of 35L18774-1407011208


Radiochemistry QC

Summary


Alpha M900.0


pCi/L

Error LLDLLD

Units:

WG366410

WG366047PBW 06/23/14PBW 0 21.1 1

WG366047LCSWA 06/23/14 105LCSW PCN45468 7066.67 83 1336.1 1

L18718-01DUP 06/23/14 39DUP-RER 37 29.1 0.168.8 3.53.3

L18877-01DUP 06/23/14 2.3DUP-RER 27 215 1.3710 9.89.7

L18733-02MSA 06/23/14 0.08 99.9MS PCN45468 100100 83 1339.52.1 1.61.8

Beta M900.0


pCi/L

Error LLDLLD

Units:

WG366410

WG366047PBW 06/23/14PBW .03 6.22.1 3.1

WG366047LCSWB 06/23/14 117LCSW PCN44650 7866.67 70 1294.9 2.9

L18718-01DUP 06/23/14 33DUP-RER 34 27 0.116.3 7.17

L18877-01DUP 06/23/14 17DUP-RER 4.4 213 0.6913 2020

L18864-01MSB 06/23/14 10 120MS PCN44650 160125 70 129105.1 66.6



pCi/L

Error LLDLLD

Units:

WG366481

WG366030PBW 06/24/14PBW 1.3 12.42.1 6.2

WG366030LCSW 06/24/14 65.3LCSW PCN44120 6497.95 55 1213.4 6.1

L18774-03MS 06/24/14 -1 69.4MS PCN44120 6797.95 55 1214.22.2 8.26.8

L18774-02DUP 06/24/14 -3.4DUP-RER 0 21.9 1.172.2 5.66.8

L18719-03DUP 06/24/14 -0.91DUP-RER -.67 22.1 0.082.1 6.26.6

Page 28 of 35L18774-1407011208


Radiochemistry QC

Summary




pCi/L

Error LLDLLD

Units:

WG366465

WG366007PBW 06/24/14PBW .18 0.480.11 0.24

WG366007LCSW 06/24/14 80LCSW PCN45817 1620 43 1480.55 0.24

L18723-02DUP 06/24/14 21DUP-RER 20 20.61 1.080.7 0.210.26

L18827-02DUP 06/24/14 0.22DUP-RER .22 20.09 00.13 0.260.17

L18774-01MS 06/24/14 2.7 91.5MS PCN45817 2120 43 1480.570.24 0.140.23



pCi/L

Error LLDLLD

Units:

WG366424

WG365899LCSW 06/23/14 70.2LCSW PCN46177 1419.95 47 1231.2 0.52

WG365899PBW 06/23/14PBW .51 0.80.4 0.4

L18829-01MS 06/24/14 1.7 91.8MS PCN46177 2019.94 47 1231.40.58 0.590.49

L18724-01DUP RM06/24/14 21DUP-RER 34 21.7 5.571.6 0.610.73

L18718-01DUP 06/24/14 0.2DUP-RER 1.8 20.58 20.55 0.490.58



pCi/L

Error LLDLLD

Units:

WG366524

WG365760PBW 06/24/14PBW .25 1.10.26 0.55

WG365760LCSW 06/24/14 104.9LCSW RC130807-2 170162.12 91 1264.4 0.6

L18718-01DUP 06/24/14 0.1DUP-RER .21 20.25 0.290.29 0.60.56

L18774-01DUP 06/24/14 0.31DUP-RER -.39 20.62 0.980.36 0.540.58

L18774-02MS 06/24/14 0.34 104.7MS RC130807-2 170162.12 91 1264.60.32 0.590.61

Page 29 of 35L18774-1407011208


RadChem Extended

Qualifier Report









REPAD.15.06.05.01

Page 30 of 35L18774-1407011208


Certification

Qualifiers


Metals Analysis



Radiochemistry




Wet Chemistry



REPAD.05.06.05.01

Page 31 of 35L18774-1407011208


Sample

Receipt


Date Received:

Received By: mtb

06/10/2014 09:59

L18774




NANOYES

X

X

X

X

X









NANOYES

X

X

X

X

X

X

X












Samples/Containers

X

X

X

X

Shipping Containers


A change was made in the analysis requested section prior to ACZ custody.

Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- --------------------3526 2.3 15 Yes3769 4.3 14 N/A

X



REPAD LPII 2012-03

Page 32 of 35L18774-1407011208


Sample

Receipt


Date Received:

Received By: mtb

06/10/2014 09:59

L18774


REPAD LPII 2012-03

Page 33 of 35L18774-1407011208

of 35L18774-1407011208


Analytical

Report



Lakewood, CO 80228


Kathy Weinel:





All samples and sub-samples associated with this project will be disposed of after August 10, 2014. If the samples are determined to be hazardous, additional charges apply for disposal (typically $11/sample). If you would like the samples to be held longer than ACZ's stated policy or to be returned, please contact your Project Manager or Customer Service Representative for further details and associated costs. ACZ retains analytical raw data reports for ten years.


Kathy Weinel

July 11, 2014

Project ID:



Lakewood, CO 80228

Accounts Payable

Report to: Bill to:

Page 1 of 34L18871-1407111615


Sample ID: MW9



Project ID:



Results

Date Sampled: 06/11/14 13:45



Metals Analysis

XQDilution

Aluminum, dissolved M200.7 ICP 0.14 mg /L 0.2B jjc0.03 06/18/14 20:441

Arsenic, dissolved M200.8 ICP-MS 0.0055 mg /L 0.001 msh0.0002 06/28/14 5:041

Barium, dissolved M200.7 ICP 0.023 mg /L 0.02 jjc0.003 06/18/14 20:441

Boron, dissolved M200.7 ICP 7.11 mg /L 0.05 jjc0.01* 06/18/14 20:441

Cadmium, dissolved M200.8 ICP-MS mg /L 0.0005U msh0.0001 06/28/14 5:041

Calcium, dissolved M200.7 ICP 28.4 mg /L 0.5 jjc0.1 06/18/14 20:441

Cesium, dissolved M200.8 ICP-MS mg /L 0.001U msh0.0002* 06/28/14 5:041

Chromium, dissolved M200.7 ICP mg /L 0.05U aeb0.01 06/19/14 19:351

Copper, dissolved M200.7 ICP mg /L 0.05U jjc0.01 06/18/14 20:441

Iron, dissolved M200.7 ICP 0.07 mg /L 0.05 jjc0.02 06/18/14 20:441

Lead, dissolved M200.8 ICP-MS 0.0004 mg /L 0.0005B msh0.0001 06/28/14 5:041

Mag nesium, dissolved M200.7 ICP 15.2 mg /L 1 jjc0.2 06/18/14 20:441

Mang anese, dissolved M200.7 ICP mg /L 0.03U jjc0.005 06/18/14 20:441

Mercury, dissolved M245.1 CVAA mg /L 0.001U mfm0.0002 06/25/14 13:051

Molyb denum, dissolved M200.7 ICP 0.05 mg /L 0.1B jjc0.02 06/18/14 20:441

Nickel, dissolved M200.7 ICP mg /L 0.04U jjc0.008 06/18/14 20:441

Potassium, dissolved M200.7 ICP 24.2 mg /L 1 jjc0.2 06/18/14 20:441

Selenium, dissolved M200.8 ICP-MS 0.0004 mg /L 0.0003 msh0.0001 06/28/14 5:041

Silica, dissolved M200.7 ICP 13.3 mg /L 1 jjc0.2 06/18/14 20:441

Sodium, dissolved M200.7 ICP 514 mg /L 1 jjc0.2* 06/18/14 20:441

Uranium, dissolved M200.8 ICP-MS 0.0482 mg /L 0.0005 msh0.0001 06/28/14 5:041

Vanadium, dissolved M200.7 ICP 0.016 mg /L 0.03B jjc0.005 06/18/14 20:441

Zinc, dissolved M200.7 ICP 0.02 mg /L 0.05B jjc0.01 06/18/14 20:441


Page 2 of 34L18871-1407111615


Sample ID: MW9



Project ID:



Results

Date Sampled: 06/11/14 13:45



Wet Chemistry

XQDilution


Bicarb onate as CaCO3

484 mg /L 20 ab d2* 06/20/14 0:001

Carb onate as CaCO3 mg /L 20U ab d2* 06/20/14 0:001

Hydroxide as CaCO3 mg /L 20U ab d2* 06/20/14 0:001

Total Alkalinity 484 mg /L 20 ab d2* 06/20/14 0:001

Carb on, total org anic (TOC)

SM5310B mg /L 100U mpb20* 06/30/14 13:5320



Sum of Anions 26 meq/L calc07/11/14 8:34

Sum of Cations 26 meq/L calc07/11/14 8:34

Chloride SM4500Cl-E 30.4 mg /L 2 b su0.5 07/01/14 16:061

Fluoride SM4500F-C 0.69 mg /L 0.3 ab d0.05 06/27/14 15:041

Nitrate/Nitrite as N M353.2 - H2SO4 preserved 20.9 mg /L 2 pjb0.3* 07/02/14 0:5215

Nitrog en, ammonia M350.1 - Automated Phenate 0.15 mg /L 0.2B mss20.05* 06/27/14 14:361

Residue, Filterab le (TDS) @180C

SM2540C 1870 mg /L 100 id50* 06/16/14 16:135

Residue, Non-Filterab le (TSS) @105C

SM2540D 1300 mg /L 400 enb100* 06/16/14 13:4620

Sulfate SM4500 SO4-D 720 mg /L 50 id10* 06/26/14 9:241

Sulfide as S SM4500S2-D mg /L 0.4U enb0.08* 06/17/14 12:013.75

TDS (calculated) Calculation 1650 mg /L calc07/11/14 8:34




Page 3 of 34L18871-1407111615


Sample ID: MW7



Project ID:



Results

Date Sampled: 06/10/14 12:30



Metals Analysis

XQDilution




Boron, dissolved M200.7 ICP 0.39 mg/L 0.05 jjc0.01* 06/18/14 20:541

Cadmium, dissolved M200.8 ICP-MS 0.0001 mg/L 0.0005B msh0.0001 06/28/14 5:071

Calcium, dissolved M200.7 ICP 100 mg/L 0.5 jjc0.1 06/18/14 20:541




Iron, dissolved M200.7 ICP mg/L 0.05U jjc0.02 06/18/14 20:541

Lead, dissolved M200.8 ICP-MS 0.0004 mg/L 0.0005B msh0.0001 06/28/14 5:071









Sodium, dissolved M200.7 ICP 74.6 mg/L 1 jjc0.2* 06/18/14 20:541



Zinc, dissolved M200.7 ICP 0.02 mg/L 0.05B jjc0.01 06/18/14 20:541


Page 4 of 34L18871-1407111615


Sample ID: MW7



Project ID:



Results

Date Sampled: 06/10/14 12:30



Wet Chemistry

XQDilution



180 mg/L 20 abd2 06/21/14 0:001



Total Alkalinity 180 mg/L 20 abd2 06/21/14 0:001


SM5310B 2.0 mg/L 5B mpb1* 06/30/14 13:531





Chloride SM4500Cl-E 24.1 mg/L 2 bsu0.5 07/01/14 16:061

Fluoride SM4500F-C 0.33 mg/L 0.3 abd0.05 06/27/14 15:081


Nitrogen, ammonia M350.1 - Automated Phenate mg/L 0.2U mss20.05* 06/27/14 14:371


SM2540C 990 mg/L 20 id10* 06/16/14 16:141


SM2540D 50 mg/L 20 enb5* 06/16/14 13:481

Sulfate SM4500 SO4-D 490 mg/L 50 id10* 06/26/14 9:291

Sulfide as S SM4500S2-D 0.03 mg/L 0.1B enb0.02* 06/17/14 12:061





Page 5 of 34L18871-1407111615


Sample ID: MW5



Project ID:



Results

Date Sampled: 06/11/14 12:05



Metals Analysis

XQDilution



Barium, dissolved M200.7 ICP 0.023 mg/L 0.02 jjc0.003 06/18/14 20:571

Boron, dissolved M200.7 ICP 0.42 mg/L 0.05 jjc0.01* 06/18/14 20:571

Cadmium, dissolved M200.8 ICP-MS 0.0001 mg/L 0.0005B msh0.0001 06/28/14 5:111

Calcium, dissolved M200.7 ICP 69.6 mg/L 0.5 jjc0.1 06/18/14 20:571




Iron, dissolved M200.7 ICP mg/L 0.05U jjc0.02 06/18/14 20:571










Sodium, dissolved M200.7 ICP 82.3 mg/L 1 jjc0.2* 06/18/14 20:571



Zinc, dissolved M200.7 ICP 0.10 mg/L 0.05 jjc0.01 06/18/14 20:571


Page 6 of 34L18871-1407111615


Sample ID: MW5



Project ID:



Results

Date Sampled: 06/11/14 12:05



Wet Chemistry

XQDilution



220 mg/L 20 abd2* 06/21/14 0:001

Carbonate as CaCO3 mg/L 20U abd2* 06/21/14 0:001

Hydroxide as CaCO3 mg/L 20U abd2* 06/21/14 0:001



SM5310B 6.6 mg/L 5 mpb1* 06/30/14 13:531





Chloride SM4500Cl-E 21.4 mg/L 2 bsu0.5 07/01/14 16:061



Nitrogen, ammonia M350.1 - Automated Phenate mg/L 0.2U mss20.05* 06/27/14 14:381


SM2540C 810 mg/L 40 id20* 06/16/14 16:152


SM2540D 278 mg/L 20 enb5* 06/16/14 13:491

Sulfate SM4500 SO4-D 370 mg/L 50 id10* 06/26/14 9:351

Sulfide as S SM4500S2-D mg/L 0.2U enb0.03* 06/17/14 12:111.5





Page 7 of 34L18871-1407111615





Limit U pper limit for RPD, in % .

Lower Lower Recovery Limit, in % ( except for LCSS, mg /Kg )




QC True V alue of the Control Sample or the amount added to the Spik e

Rec Recovered amount of the true value or spik e added, in % (except for LCSS, mg /Kg )


Upper Upper Recovery Limit, in % (except for LCSS, mg /Kg )


QC Sample Types

AS Analytical Spike (Post Dig estion) LCSWD Lab oratory Control Sample - Water Duplicate

ASD Analytical Spike (Post Dig estion) Duplicate LFB Lab oratory Fortified Blank

CCB Continuing Calib ration Blank LFM Lab oratory Fortified Matrix

CCV Continuing Calib ration Verification standard LFMD Lab oratory Fortified Matrix Duplicate

DUP Sample Duplicate LRB Lab oratory Reag ent Blank

ICB Initial Calib ration Blank MS Matrix Spike

ICV Initial Calib ration Verification standard MSD Matrix Spike Duplicate


LCSS Lab oratory Control Sample - Soil P BW Prep Blank - Water

LCSSD Lab oratory Control Sample - Soil Duplicate P QV Practical Quantitation Verification standard

LCSW Lab oratory Control Sample - Water SDL Serial Dilution


Blanks Verifies that there is no or minimal contamination in the prep method or calib ration procedure.




Standard Verifies the validity of the calib ration.


B Analyte concentration detected at a value b etween MDL and PQL. The associated value is an estimated quantity.


L Targ et analyte response was b elow the lab oratory defined neg ative threshold.

U The material was analyzed for, b ut was not detected ab ove the level of the associated value.


Method References


(2) EPA 600/R-93-100. Methods for the Determination of Inorg anic Sub stances in Environmental Samples, Aug ust 1993.




Comments

(1) QC results calculated from raw data. Results may vary slig htly if the rounded values are used in the calculations.

(2) Soil, Sludg e, and Plant matrices for Inorg anic analyses are reported on a dry weig ht b asis.

(3) Animal matrices for Inorg anic analyses are reported on an "as received" b asis.





REP001.09.12.01

Inorganic

Reference

Page 8 of 34L18871-1407111615


Inorganic QC

Summary




WG366285

WG366285PQV2 06/20/14 17:03 132.5PQV WC140210- 26.5 50 150mg /L20

WG366285PBW1 06/20/14 17:09PBW U -20 20mg /L

WG366285LCSW3 06/20/14 17:29 101.5LCSW WC140610- 831.9 90 110mg /L820.0001


WG366285PBW2 06/20/14 20:51PBW U -20 20mg /L

L18871-02DUP 06/21/14 0:14 180DUP 180.2 0.1mg /L 20


WG366285PBW3 06/21/14 0:43PBW 2.3 -20 20mg /L

L18873-02DUP RA06/21/14 1:16 7DUP 6.8 2.9mg /L 20

WG366285LCSW12 06/21/14 3:53 101.5LCSW WC140610- 832 90 110mg /L820.0001

WG366285PBW4 06/21/14 4:03PBW 2.2 -20 20mg /L




WG366108

WG366108ICV 06/18/14 20:22 97.5ICV II140512-2 1.949 95 105mg /L2

WG366108ICB 06/18/14 20:28ICB U -0.09 0.09mg /L

WG366108PQV 06/18/14 20:31 87.9PQV II140609-2 .132 70 130mg /L.150165

WG366108SIC 06/18/14 20:34 100.6SIC II140602-1 201.6 1 200mg /L200.370165

WG366108LFB 06/18/14 20:41 107.4LFB II140611-2 1.075 85 115mg /L1.0011

L18871-01AS 06/18/14 20:47 .14 107.7AS II140611-2 1.218 85 115mg /L1.0011

L18871-01ASD 06/18/14 20:50 .14 111.8ASD II140611-2 1.259 3.3185 115mg /L 201.0011

WG366108CCV1 06/18/14 21:13 96.8CCV II140506-1 .968 90 110mg /L1

WG366108CCB1 06/18/14 21:16CCB U -0.09 0.09mg /L

WG366108CCV2 06/18/14 21:51 97.5CCV II140506-1 .975 90 110mg /L1

WG366108CCB2 06/18/14 21:54CCB U -0.09 0.09mg /L

WG366108CCV3 06/18/14 22:13 95.9CCV II140506-1 .959 90 110mg /L1

WG366108CCB3 06/18/14 22:16CCB U -0.09 0.09mg /L



WG366709

WG366709ICV 06/28/14 4:38 103.1ICV MS140513-1 .05157 90 110mg /L.05

WG366709ICB 06/28/14 4:41ICB U -0.0006 0.0006mg /L

WG366709LFB 06/28/14 4:44 101.5LFB MS140625-3 .05087 85 115mg /L.0501

L18864-03AS 06/28/14 4:57 .011 97.8AS MS140625-3 .256 70 130mg /L.2505

L18864-03ASD 06/28/14 5:01 .011 100.2ASD MS140625-3 .2619 2.2870 130mg /L 20.2505

WG366709CCV1 06/28/14 5:14 95.5CCV MS140513-2 .09569 90 110mg /L.1002

WG366709CCB1 06/28/14 5:17CCB U -0.0006 0.0006mg /L

WG366709CCV2 06/28/14 5:53 96.2CCV MS140513-2 .09637 90 110mg /L.1002

WG366709CCB2 06/28/14 5:56CCB U -0.0006 0.0006mg /L

WG366709CCV3 06/28/14 6:19 96.6CCV MS140513-2 .09682 90 110mg /L.1002

WG366709CCB3 06/28/14 6:22CCB U -0.0006 0.0006mg /L

Page 9 of 34L18871-1407111615


Inorganic QC

Summary




WG366108

WG366108ICV 06/18/14 20:22 98.7ICV II140512-2 1.9732 95 105mg /L2

WG366108ICB 06/18/14 20:28ICB U -0.009 0.009mg /L

WG366108PQV 06/18/14 20:31 94PQV II140609-2 .0141 70 130mg /L.015

WG366108SIC 06/18/14 20:34 100.5SIC II140602-1 .1005 80 120mg /L.1

WG366108LFB 06/18/14 20:41 101.8LFB II140611-2 .509 85 115mg /L.5

L18871-01AS 06/18/14 20:47 .023 100.5AS II140611-2 .5255 85 115mg /L.5

L18871-01ASD 06/18/14 20:50 .023 101.2ASD II140611-2 .5292 0.785 115mg /L 20.5

WG366108CCV1 06/18/14 21:13 99.5CCV II140506-1 .9953 90 110mg /L1

WG366108CCB1 06/18/14 21:16CCB U -0.009 0.009mg /L

WG366108CCV2 06/18/14 21:51 98.7CCV II140506-1 .9865 90 110mg /L1

WG366108CCB2 06/18/14 21:54CCB U -0.009 0.009mg /L

WG366108CCV3 06/18/14 22:13 98.4CCV II140506-1 .984 90 110mg /L1

WG366108CCB3 06/18/14 22:16CCB U -0.009 0.009mg /L



WG366108

WG366108ICV 06/18/14 20:22 101.4ICV II140512-2 2.028 95 105mg /L2

WG366108ICB 06/18/14 20:28ICB U -0.03 0.03mg /L

WG366108PQV 06/18/14 20:31 101.9PQV II140609-2 .051 70 130mg /L.05005

WG366108SIC 06/18/14 20:34 88.9SIC II140602-1 .089 80 120mg /L.1001

WG366108LFB 06/18/14 20:41 104.1LFB II140611-2 .521 85 115mg /L.5005

L18871-01AS M306/18/14 20:47 7.11 41.4AS II140611-2 7.317 85 115mg /L.5005

L18871-01ASD M306/18/14 20:50 7.11 42.6ASD II140611-2 7.323 0.0885 115mg /L 20.5005

WG366108CCV1 06/18/14 21:13 101.6CCV II140506-1 1.016 90 110mg /L1

WG366108CCB1 06/18/14 21:16CCB U -0.03 0.03mg /L

WG366108CCV2 06/18/14 21:51 101CCV II140506-1 1.01 90 110mg /L1

WG366108CCB2 06/18/14 21:54CCB U -0.03 0.03mg /L

WG366108CCV3 06/18/14 22:13 100.6CCV II140506-1 1.006 90 110mg /L1

WG366108CCB3 06/18/14 22:16CCB U -0.03 0.03mg /L



WG366709

WG366709ICV 06/28/14 4:38 99ICV MS140513-1 .0495 90 110mg /L.05

WG366709ICB 06/28/14 4:41ICB U -0.0003 0.0003mg /L

WG366709LFB 06/28/14 4:44 98.7LFB MS140625-3 .04943 85 115mg /L.0501

L18864-03AS 06/28/14 4:57 .0099 93.5AS MS140625-3 .24415 70 130mg /L.2505

L18864-03ASD 06/28/14 5:01 .0099 93.8ASD MS140625-3 .2449 0.3170 130mg /L 20.2505

WG366709CCV1 06/28/14 5:14 96.1CCV MS140513-2 .0963 90 110mg /L.1002

WG366709CCB1 06/28/14 5:17CCB U -0.0003 0.0003mg /L

WG366709CCV2 06/28/14 5:53 96.5CCV MS140513-2 .09667 90 110mg /L.1002

WG366709CCB2 06/28/14 5:56CCB U -0.0003 0.0003mg /L

WG366709CCV3 06/28/14 6:19 97.6CCV MS140513-2 .09778 90 110mg /L.1002

WG366709CCB3 06/28/14 6:22CCB U -0.0003 0.0003mg /L

Page 10 of 34L18871-1407111615


Inorganic QC

Summary




WG366108

WG366108ICV 06/18/14 20:22 99.9ICV II140512-2 99.93 95 105mg /L100

WG366108ICB 06/18/14 20:28ICB U -0.3 0.3mg /L

WG366108PQV 06/18/14 20:31 76PQV II140609-2 .38 70 130mg /L.5002

WG366108SIC 06/18/14 20:34 98.3SIC II140602-1 197.1 1 200mg /L200.5002

WG366108LFB 06/18/14 20:41 109.9LFB II140611-2 74.74 85 115mg /L67.98099

L18871-01AS 06/18/14 20:47 28.4 107.1AS II140611-2 101.2 85 115mg /L67.98099

L18871-01ASD 06/18/14 20:50 28.4 106.5ASD II140611-2 100.8 0.485 115mg /L 2067.98099

WG366108CCV1 06/18/14 21:13 101.5CCV II140506-1 50.77 90 110mg /L50

WG366108CCB1 06/18/14 21:16CCB U -0.3 0.3mg /L

WG366108CCV2 06/18/14 21:51 100.2CCV II140506-1 50.1 90 110mg /L50

WG366108CCB2 06/18/14 21:54CCB U -0.3 0.3mg /L

WG366108CCV3 06/18/14 22:13 102CCV II140506-1 51 90 110mg /L50

WG366108CCB3 06/18/14 22:16CCB U -0.3 0.3mg /L



WG358122

WG358122ICV 01/22/14 11:52 102ICV WI131209-3 102 90 110mg /L100

WG358122ICB 01/22/14 11:52ICB U -3 3mg /L

WG366762

WG366762CCV1 06/30/14 13:53 95.4CCV WI140502-1 47.7 90 110mg /L50

WG366762CCB1 06/30/14 13:53CCB U -3 3mg /L

WG366762PQV 06/30/14 13:53 96PQV WI140502-3 4.8 70 130mg /L5

WG366762LFB 06/30/14 13:53 91.8LFB WI140502-2 45.9 90 110mg /L50

L18991-04AS 06/30/14 13:53 9.6 90.6AS WI140502-2 54.9 90 110mg /L50

L18991-04DUP RA06/30/14 13:53 9.6DUP 9.7 1mg /L 20

WG366762CCV2 06/30/14 13:53 95.8CCV WI140502-1 47.9 90 110mg /L50

WG366762CCB2 06/30/14 13:53CCB U -3 3mg /L

WG366762CCV3 06/30/14 13:53 93.4CCV WI140502-1 46.7 90 110mg /L50

WG366762CCB3 06/30/14 13:53CCB U -3 3mg /L

WG366762CCV4 06/30/14 13:53 95.4CCV WI140502-1 47.7 90 110mg /L50

WG366762CCB4 06/30/14 13:53CCB U -3 3mg /L



WG366709

WG366709ICV 06/28/14 4:38 100.1ICV MS140513-1 .05005 90 110mg /L.05

WG366709ICB 06/28/14 4:41ICB U -0.0006 0.0006mg /L

WG366709LFB 06/28/14 4:44 103LFB MS140625-3 .05152 85 115mg /L.05

L18864-03AS 06/28/14 4:57 .002 103AS MS140625-3 .2596 70 130mg /L.25

L18864-03ASD 06/28/14 5:01 .002 101.7ASD MS140625-3 .2563 1.2870 130mg /L 20.25

WG366709CCV1 06/28/14 5:14 96.6CCV MS140513-2 .09664 90 110mg /L.1

WG366709CCB1 06/28/14 5:17CCB U -0.0006 0.0006mg /L

WG366709CCV2 06/28/14 5:53 98.1CCV MS140513-2 .09813 90 110mg /L.1

WG366709CCB2 06/28/14 5:56CCB U -0.0006 0.0006mg /L

WG366709CCV3 06/28/14 6:19 98.7CCV MS140513-2 .09868 90 110mg /L.1

WG366709CCB3 06/28/14 6:22CCB U -0.0006 0.0006mg /L

Page 11 of 34L18871-1407111615


Inorganic QC

Summary


Chloride SM4500Cl-E


WG366890

WG366890ICB 07/01/14 11:09ICB U -1.5 1.5mg /L

WG366890ICV 07/01/14 11:09 105.5ICV WI140701-3 58.03 90 110mg /L55

WG366890CCV1 07/01/14 16:05 106.3CCV WI131028-1 53.17 90 110mg /L50

WG366890CCB1 07/01/14 16:06CCB U -1.5 1.5mg /L

WG366890LFB1 07/01/14 16:06 107.1LFB WI140508-1 32.12 90 110mg /L30

L18864-01AS 07/01/14 16:06 28.4 103.5AS WI140508-1 59.44 90 110mg /L30

L18864-02DUP 07/01/14 16:06 33.8DUP 33.59 0.6mg /L 20

WG366890CCV2 07/01/14 16:07 105.9CCV WI131028-1 52.95 90 110mg /L50

WG366890CCB2 07/01/14 16:07CCB U -1.5 1.5mg /L

WG366890CCV3 07/01/14 16:07 106CCV WI131028-1 53.02 90 110mg /L50

WG366890CCB3 07/01/14 16:07CCB U -1.5 1.5mg /L

WG366890CCV4 07/01/14 16:15 106.7CCV WI131028-1 53.33 90 110mg /L50

WG366890CCB4 07/01/14 16:15CCB U -1.5 1.5mg /L

WG366890CCV5 07/01/14 16:18 107.9CCV WI131028-1 53.94 90 110mg /L50

WG366890CCB5 07/01/14 16:18CCB .56 -1.5 1.5mg /L

WG366890LFB2 07/01/14 16:18 107.2LFB WI140508-1 32.17 90 110mg /L30

WG366890CCV6 07/01/14 16:19 106.7CCV WI131028-1 53.37 90 110mg /L50

WG366890CCB6 07/01/14 16:19CCB U -1.5 1.5mg /L

WG366890CCV7 07/01/14 16:28 106.7CCV WI131028-1 53.35 90 110mg /L50

WG366890CCB7 07/01/14 16:28CCB U -1.5 1.5mg /L

WG366890CCV8 07/01/14 16:40 107.9CCV WI131028-1 53.97 90 110mg /L50

WG366890CCB8 07/01/14 16:40CCB .57 -1.5 1.5mg /L

WG366890CCV9 07/01/14 16:40 106.3CCV WI131028-1 53.13 90 110mg /L50

WG366890CCB9 07/01/14 16:40CCB U -1.5 1.5mg /L

WG366890CCV10 07/01/14 16:55 106.5CCV WI131028-1 53.25 90 110mg /L50

WG366890CCB10 07/01/14 16:55CCB U -1.5 1.5mg /L

WG366890CCV11 07/01/14 16:56 106.4CCV WI131028-1 53.19 90 110mg /L50

WG366890CCB11 07/01/14 16:56CCB U -1.5 1.5mg /L



WG366172

WG366172ICV 06/19/14 19:14 97.1ICV II140512-2 1.942 95 105mg /L2

WG366172ICB 06/19/14 19:20ICB U -0.03 0.03mg /L

WG366172PQV 06/19/14 19:23 111.8PQV II140609-2 .056 70 130mg /L.0501

WG366172SIC 06/19/14 19:26 102.8SIC II140602-1 .103 80 120mg /L.1002

WG366172LFB 06/19/14 19:32 99.8LFB II140611-2 .5 85 115mg /L.501

L18894-01AS 06/19/14 19:57 U 94.6AS II140611-2 2.37 85 115mg /L2.505

L18894-01ASD 06/19/14 20:00 U 94.1ASD II140611-2 2.358 0.5185 115mg /L 202.505

WG366172CCV1 06/19/14 20:03 98.8CCV II140506-1 .988 90 110mg /L1

WG366172CCB1 06/19/14 20:06CCB U -0.03 0.03mg /L

WG366172CCV2 06/19/14 20:41 98.8CCV II140506-1 .988 90 110mg /L1

WG366172CCB2 06/19/14 20:44CCB U -0.03 0.03mg /L

WG366172CCV3 06/19/14 20:50 98.4CCV II140506-1 .984 90 110mg /L1

WG366172CCB3 06/19/14 20:53CCB U -0.03 0.03mg /L

Page 12 of 34L18871-1407111615


Inorganic QC

Summary




WG366108

WG366108ICV 06/18/14 20:22 96.7ICV II140512-2 1.934 95 105mg /L2

WG366108ICB 06/18/14 20:28ICB U -0.03 0.03mg /L

WG366108PQV 06/18/14 20:31 100PQV II140609-2 .05 70 130mg /L.05

WG366108SIC 06/18/14 20:34 102SIC II140602-1 .102 80 120mg /L.1

WG366108LFB 06/18/14 20:41 103LFB II140611-2 .515 85 115mg /L.5

L18871-01AS 06/18/14 20:47 U 101.2AS II140611-2 .506 85 115mg /L.5

L18871-01ASD 06/18/14 20:50 U 101.8ASD II140611-2 .509 0.5985 115mg /L 20.5

WG366108CCV1 06/18/14 21:13 98.3CCV II140506-1 .983 90 110mg /L1

WG366108CCB1 06/18/14 21:16CCB U -0.03 0.03mg /L

WG366108CCV2 06/18/14 21:51 96.9CCV II140506-1 .969 90 110mg /L1

WG366108CCB2 06/18/14 21:54CCB U -0.03 0.03mg /L

WG366108CCV3 06/18/14 22:13 97.2CCV II140506-1 .972 90 110mg /L1

WG366108CCB3 06/18/14 22:16CCB U -0.03 0.03mg /L

Page 13 of 34L18871-1407111615


Inorganic QC

Summary


Fluoride SM4500F-C


WG366655

WG366655ICV 06/27/14 14:35 95.4ICV WC140626- 1.908 95 105mg /L2

WG366655ICB 06/27/14 14:43ICB U -0.15 0.15mg /L

WG366655PQV 06/27/14 14:47 78.6PQV WC140626- .197 70 130mg /L.25075

WG366655LFB1 06/27/14 14:50 96.1LFB WC140501- 4.818 90 110mg /L5.015

L18809-01AS 06/27/14 14:58 .88 95AS WC140501- 5.646 90 110mg /L5.015

L18809-01DUP 06/27/14 15:01 .88DUP .866 1.6mg /L 20

WG366655CCV1 06/27/14 15:42 92.3CCV WC140626- 1.846 90 110mg /L2

WG366655CCB1 06/27/14 15:49CCB U -0.15 0.15mg /L

WG366655CCV2 06/27/14 16:47 98.1CCV WC140626- 1.962 90 110mg /L2

WG366655CCB2 06/27/14 16:50CCB U -0.15 0.15mg /L

WG366655LFB2 06/27/14 17:28 92.5LFB WC140501- 4.64 90 110mg /L5.015

WG366655CCV3 06/27/14 17:50 95.8CCV WC140626- 1.916 90 110mg /L2

WG366655CCB3 06/27/14 17:55CCB U -0.15 0.15mg /L

WG366655CCV4 06/27/14 18:52 97.7CCV WC140626- 1.953 90 110mg /L2

WG366655CCB4 06/27/14 19:00CCB U -0.15 0.15mg /L

WG366655CCV5 06/27/14 19:55 94.1CCV WC140626- 1.881 90 110mg /L2

WG366655CCB5 06/27/14 20:03CCB U -0.15 0.15mg /L

WG366655CCV6 06/27/14 20:12 100.9CCV WC140626- 2.017 90 110mg /L2

WG366655CCB6 06/27/14 20:20CCB U -0.15 0.15mg /L

WG366770

WG366770ICV 06/30/14 14:05 98.7ICV WC140626- 1.973 95 105mg /L2

WG366770ICB 06/30/14 14:09ICB .058 -0.15 0.15mg /L

WG366770PQV 06/30/14 14:13 98.1PQV WC140630- .246 70 130mg /L.25075

WG366770LFB1 06/30/14 14:15 95.4LFB WC140501- 4.782 90 110mg /L5.015

L18871-03AS 06/30/14 14:25 .65 95.5AS WC140501- 5.441 90 110mg /L5.015

L18871-03DUP 06/30/14 14:28 .65DUP .569 13.3mg /L 20

WG366770CCV1 06/30/14 14:55 101.8CCV WC140626- 2.036 90 110mg /L2

WG366770CCB1 06/30/14 15:00CCB U -0.15 0.15mg /L

WG366770CCV2 06/30/14 15:39 104.6CCV WC140626- 2.091 90 110mg /L2

WG366770CCB2 06/30/14 15:47CCB U -0.15 0.15mg /L

WG366770LFB2 06/30/14 16:11 96.2LFB WC140501- 4.826 90 110mg /L5.015

WG366770CCV3 06/30/14 16:30 103.2CCV WC140626- 2.063 90 110mg /L2

WG366770CCB3 06/30/14 16:38CCB U -0.15 0.15mg /L

WG366770CCV4 06/30/14 17:20 105CCV WC140626- 2.1 90 110mg /L2

WG366770CCB4 06/30/14 17:28CCB U -0.15 0.15mg /L

WG366770CCV5 06/30/14 18:17 103.2CCV WC140626- 2.063 90 110mg /L2

WG366770CCB5 06/30/14 18:25CCB U -0.15 0.15mg /L

WG366770CCV6 06/30/14 18:35 106CCV WC140626- 2.119 90 110mg /L2

WG366770CCB6 06/30/14 18:42CCB U -0.15 0.15mg /L

Page 14 of 34L18871-1407111615


Inorganic QC

Summary




WG366108

WG366108ICV 06/18/14 20:22 98.2ICV II140512-2 1.964 95 105mg/L2

WG366108ICB 06/18/14 20:28ICB U -0.06 0.06mg/L

WG366108PQV 06/18/14 20:31 103.9PQV II140609-2 .052 70 130mg/L.05007

WG366108SIC 06/18/14 20:34 94.5SIC II140602-1 189.3 1 200mg/L200.33007

WG366108LFB 06/18/14 20:41 103.2LFB II140611-2 1.033 85 115mg/L1.0014

L18871-01AS 06/18/14 20:47 .07 101.4AS II140611-2 1.085 85 115mg/L1.0014

L18871-01ASD 06/18/14 20:50 .07 102.7ASD II140611-2 1.098 1.1985 115mg/L 201.0014

WG366108CCV1 06/18/14 21:13 100.1CCV II140506-1 1.001 90 110mg/L1

WG366108CCB1 06/18/14 21:16CCB U -0.06 0.06mg/L

WG366108CCV2 06/18/14 21:51 98.3CCV II140506-1 .983 90 110mg/L1

WG366108CCB2 06/18/14 21:54CCB U -0.06 0.06mg/L

WG366108CCV3 06/18/14 22:13 100.3CCV II140506-1 1.003 90 110mg/L1

WG366108CCB3 06/18/14 22:16CCB U -0.06 0.06mg/L



WG366709

WG366709ICV 06/28/14 4:38 100.4ICV MS140513-1 .05018 90 110mg/L.05

WG366709ICB 06/28/14 4:41ICB U -0.0003 0.0003mg/L

WG366709LFB 06/28/14 4:44 99LFB MS140625-3 .04955 85 115mg/L.05005

L18864-03AS 06/28/14 4:57 .0006 99.2AS MS140625-3 .2488 70 130mg/L.25025

L18864-03ASD 06/28/14 5:01 .0006 100.7ASD MS140625-3 .25265 1.5470 130mg/L 20.25025

WG366709CCV1 06/28/14 5:14 102CCV MS140513-2 .2552 90 110mg/L.25025

WG366709CCB1 06/28/14 5:17CCB U -0.0003 0.0003mg/L

WG366709CCV2 06/28/14 5:53 99.8CCV MS140513-2 .2497 90 110mg/L.25025

WG366709CCB2 06/28/14 5:56CCB .00011 -0.0003 0.0003mg/L

WG366709CCV3 06/28/14 6:19 98.6CCV MS140513-2 .2467 90 110mg/L.25025

WG366709CCB3 06/28/14 6:22CCB .00011 -0.0003 0.0003mg/L



WG366108

WG366108ICV 06/18/14 20:22 96.7ICV II140512-2 96.74 95 105mg/L100

WG366108ICB 06/18/14 20:28ICB U -0.6 0.6mg/L

WG366108PQV 06/18/14 20:31 90.9PQV II140609-2 .91 70 130mg/L1.0007

WG366108SIC 06/18/14 20:34 99.5SIC II140602-1 200.1 1 200mg/L201.1407

WG366108LFB 06/18/14 20:41 101.7LFB II140611-2 50.86 85 115mg/L50.00131

L18871-01AS 06/18/14 20:47 15.2 99.8AS II140611-2 65.12 85 115mg/L50.00131

L18871-01ASD 06/18/14 20:50 15.2 99.4ASD II140611-2 64.92 0.3185 115mg/L 2050.00131

WG366108CCV1 06/18/14 21:13 97.6CCV II140506-1 48.81 90 110mg/L50

WG366108CCB1 06/18/14 21:16CCB U -0.6 0.6mg/L

WG366108CCV2 06/18/14 21:51 96.2CCV II140506-1 48.11 90 110mg/L50

WG366108CCB2 06/18/14 21:54CCB U -0.6 0.6mg/L

WG366108CCV3 06/18/14 22:13 98.1CCV II140506-1 49.07 90 110mg/L50

WG366108CCB3 06/18/14 22:16CCB U -0.6 0.6mg/L

Page 15 of 34L18871-1407111615


Inorganic QC

Summary




WG366108

WG366108ICV 06/18/14 20:22 98.2ICV II140512-2 1.9645 95 105mg/L2

WG366108ICB 06/18/14 20:28ICB U -0.015 0.015mg/L

WG366108PQV 06/18/14 20:31 87.6PQV II140609-2 .0219 70 130mg/L.025

WG366108SIC 06/18/14 20:34 96.8SIC II140602-1 48.54 1 200mg/L50.125

WG366108LFB 06/18/14 20:41 102.8LFB II140611-2 .5152 85 115mg/L.501

L18871-01AS 06/18/14 20:47 U 102.9AS II140611-2 .5157 85 115mg/L.501

L18871-01ASD 06/18/14 20:50 U 102.9ASD II140611-2 .5157 085 115mg/L 20.501

WG366108CCV1 06/18/14 21:13 100.5CCV II140506-1 1.005 90 110mg/L1

WG366108CCB1 06/18/14 21:16CCB U -0.015 0.015mg/L

WG366108CCV2 06/18/14 21:51 98.6CCV II140506-1 .9855 90 110mg/L1

WG366108CCB2 06/18/14 21:54CCB U -0.015 0.015mg/L

WG366108CCV3 06/18/14 22:13 99.7CCV II140506-1 .9972 90 110mg/L1

WG366108CCB3 06/18/14 22:16CCB U -0.015 0.015mg/L



WG366461

WG366461ICV 06/25/14 12:56 97.3ICV II140616-2 .00487 95 105mg/L.005005

WG366461ICB 06/25/14 12:58ICB U -0.0002 0.0002mg/L

WG366461LRB 06/25/14 13:00LRB U -0.00044 0.00044mg/L

WG366461LFB 06/25/14 13:02 88.4LFB II140616-4 .00177 85 115mg/L.002002

L18871-03LFM 06/25/14 13:11 U 89.4LFM II140616-4 .00179 85 115mg/L.002002


WG366461CCV1 06/25/14 13:22 97.5CCV II140616-2 .00488 90 110mg/L.005005

WG366461CCB1 06/25/14 13:24CCB U -0.0002 0.0002mg/L

WG366461CCV2 06/25/14 13:50 98.9CCV II140616-2 .00495 90 110mg/L.005005

WG366461CCB2 06/25/14 13:53CCB U -0.0002 0.0002mg/L

WG366461CCV3 06/25/14 14:09 98.7CCV II140616-2 .00494 90 110mg/L.005005

WG366461CCB3 06/25/14 14:11CCB U -0.0002 0.0002mg/L



WG366108

WG366108ICV 06/18/14 20:22 99.8ICV II140512-2 1.996 95 105mg/L2

WG366108ICB 06/18/14 20:28ICB U -0.06 0.06mg/L

WG366108PQV 06/18/14 20:31 103PQV II140609-2 .103 70 130mg/L.1

WG366108SIC 06/18/14 20:34 91SIC II140602-1 .091 80 120mg/L.1

WG366108LFB 06/18/14 20:41 102.9LFB II140611-2 .514 85 115mg/L.4995

L18871-01AS 06/18/14 20:47 .05 102.5AS II140611-2 .562 85 115mg/L.4995

L18871-01ASD 06/18/14 20:50 .05 102.3ASD II140611-2 .561 0.1885 115mg/L 20.4995

WG366108CCV1 06/18/14 21:13 100.9CCV II140506-1 1.009 90 110mg/L1

WG366108CCB1 06/18/14 21:16CCB U -0.06 0.06mg/L

WG366108CCV2 06/18/14 21:51 99.8CCV II140506-1 .998 90 110mg/L1

WG366108CCB2 06/18/14 21:54CCB U -0.06 0.06mg/L

WG366108CCV3 06/18/14 22:13 100.2CCV II140506-1 1.002 90 110mg/L1

WG366108CCB3 06/18/14 22:16CCB U -0.06 0.06mg/L

Page 16 of 34L18871-1407111615


Inorganic QC

Summary




WG366108

WG366108ICV 06/18/14 20:22 99.4ICV II140512-2 1.9882 95 105mg/L2

WG366108ICB 06/18/14 20:28ICB U -0.024 0.024mg/L

WG366108PQV 06/18/14 20:31 115PQV II140609-2 .046 70 130mg/L.04

WG366108SIC 06/18/14 20:34 95.1SIC II140602-1 .0951 80 120mg/L.1

WG366108LFB 06/18/14 20:41 104.1LFB II140611-2 .5205 85 115mg/L.5

L18871-01AS 06/18/14 20:47 U 102.9AS II140611-2 .5145 85 115mg/L.5

L18871-01ASD 06/18/14 20:50 U 103ASD II140611-2 .5152 0.1485 115mg/L 20.5

WG366108CCV1 06/18/14 21:13 101.9CCV II140506-1 1.019 90 110mg/L1

WG366108CCB1 06/18/14 21:16CCB U -0.024 0.024mg/L

WG366108CCV2 06/18/14 21:51 100.1CCV II140506-1 1.001 90 110mg/L1

WG366108CCB2 06/18/14 21:54CCB U -0.024 0.024mg/L

WG366108CCV3 06/18/14 22:13 101.6CCV II140506-1 1.016 90 110mg/L1

WG366108CCB3 06/18/14 22:16CCB U -0.024 0.024mg/L



WG366903

WG366903ICV 07/01/14 21:46 97.8ICV WI140417-3 2.362 90 110mg/L2.416

WG366903ICB 07/01/14 21:47ICB U -0.06 0.06mg/L

WG366907

WG366907CCV1 07/01/14 23:45 101.7CCV WI140625-1 2.033 90 110mg/L2

WG366907CCB1 07/01/14 23:46CCB U -0.06 0.06mg/L

WG366907LFB1 07/01/14 23:48 94.6LFB WI140215-3 1.892 90 110mg/L2

L18864-01AS 07/01/14 23:50 U 102.3AS WI140215-3 2.046 90 110mg/L2

L18864-02DUP RA07/01/14 23:52 .04DUP .04 0mg/L 20

WG366907CCV2 07/02/14 0:00 100.9CCV WI140625-1 2.018 90 110mg/L2

WG366907CCB2 07/02/14 0:01CCB U -0.06 0.06mg/L

WG366907CCV3 07/02/14 0:14 101.1CCV WI140625-1 2.022 90 110mg/L2

WG366907CCB3 07/02/14 0:15CCB U -0.06 0.06mg/L

WG366907LFB2 07/02/14 0:22 101.4LFB WI140215-3 2.027 90 110mg/L2

WG366907CCV4 07/02/14 0:28 101.4CCV WI140625-1 2.027 90 110mg/L2

WG366907CCB4 07/02/14 0:29CCB U -0.06 0.06mg/L

WG366907CCV5 07/02/14 0:37 100.4CCV WI140625-1 2.007 90 110mg/L2

WG366907CCB5 07/02/14 0:38CCB U -0.06 0.06mg/L

WG366907CCV6 07/02/14 0:49 100.8CCV WI140625-1 2.015 90 110mg/L2

WG366907CCB6 07/02/14 0:51CCB U -0.06 0.06mg/L

WG366907CCV7 07/02/14 0:59 100.4CCV WI140625-1 2.008 90 110mg/L2

WG366907CCB7 07/02/14 1:00CCB U -0.06 0.06mg/L

Page 17 of 34L18871-1407111615


Inorganic QC

Summary




WG366677

WG366677ICV 06/27/14 14:18 101.3ICV WI131021-1 1.016 90 110mg/L1.003

WG366677ICB 06/27/14 14:21ICB U -0.15 0.15mg/L

WG366677LFB1 06/27/14 14:22 104.4LFB WI140113-8 1.044 90 110mg/L1

L18825-01AS 06/27/14 14:24 3.15 99.9AS WI140113-8 4.149 90 110mg/L1

L18825-02DUP RA06/27/14 14:26 UDUP U 0mg/L 20

WG366677CCV1 06/27/14 14:33 101.9CCV WI140113-6 2.037 90 110mg/L2

WG366677CCB1 06/27/14 14:34CCB U -0.15 0.15mg/L

L18871-03AS 06/27/14 14:39 U 104AS WI140113-8 1.04 90 110mg/L1

L18973-01DUP RA06/27/14 14:41 UDUP U 0mg/L 20

WG366677CCV2 06/27/14 14:46 101.1CCV WI140113-6 2.022 90 110mg/L2

WG366677CCB2 06/27/14 14:47CCB U -0.15 0.15mg/L

WG366677LFB2 06/27/14 14:53 100.8LFB WI140113-8 1.008 90 110mg/L1

WG366677CCV3 06/27/14 14:59 101.7CCV WI140113-6 2.034 90 110mg/L2

WG366677CCB3 06/27/14 15:00CCB U -0.15 0.15mg/L

WG366677CCV4 06/27/14 15:12 101.3CCV WI140113-6 2.026 90 110mg/L2

WG366677CCB4 06/27/14 15:13CCB U -0.15 0.15mg/L

WG366677CCV5 06/27/14 15:40 101.4CCV WI140113-6 2.027 90 110mg/L2

WG366677CCB5 06/27/14 15:41CCB U -0.15 0.15mg/L

WG366677CCV6 06/27/14 15:45 101.2CCV WI140113-6 2.024 90 110mg/L2

WG366677CCB6 06/27/14 15:46CCB U -0.15 0.15mg/L



WG366108

WG366108ICV 06/18/14 20:22 99ICV II140512-2 19.8 95 105mg/L20

WG366108ICB 06/18/14 20:28ICB U -0.6 0.6mg/L

WG366108PQV 06/18/14 20:31 101PQV II140609-2 1.01 70 130mg/L1

WG366108SIC 06/18/14 20:34 101SIC II140602-1 1.01 80 120mg/L1

WG366108LFB 06/18/14 20:41 103.8LFB II140611-2 103.8 85 115mg/L99.99364

L18871-01AS 06/18/14 20:47 24.2 102AS II140611-2 126.2 85 115mg/L99.99364

L18871-01ASD 06/18/14 20:50 24.2 102.3ASD II140611-2 126.5 0.2485 115mg/L 2099.99364

WG366108CCV1 06/18/14 21:13 100.2CCV II140506-1 10.02 90 110mg/L10

WG366108CCB1 06/18/14 21:16CCB U -0.6 0.6mg/L

WG366108CCV2 06/18/14 21:51 98.8CCV II140506-1 9.88 90 110mg/L10

WG366108CCB2 06/18/14 21:54CCB U -0.6 0.6mg/L

WG366108CCV3 06/18/14 22:13 99CCV II140506-1 9.9 90 110mg/L10

WG366108CCB3 06/18/14 22:16CCB U -0.6 0.6mg/L



WG365961

WG365961PBW 06/16/14 16:00PBW 18 -20 20mg/L


WG365961PQV 06/16/14 16:02 110PQV WC140325- 22 50 150mg/L20

L18881-03DUP 06/16/14 16:29 220DUP 218 0.9mg/L 10

Page 18 of 34L18871-1407111615


Inorganic QC

Summary




WG365951

WG365951PBW 06/16/14 13:21PBW U -15 15mg/L


L18873-03DUP RA06/16/14 13:56 UDUP U 0mg/L 10



WG366709

WG366709ICV 06/28/14 4:38 102ICV MS140513-1 .051 90 110mg/L.05

WG366709ICB 06/28/14 4:41ICB U -0.0003 0.0003mg/L

WG366709LFB 06/28/14 4:44 98.1LFB MS140625-3 .04912 85 115mg/L.05005

L18864-03AS 06/28/14 4:57 .005 93.2AS MS140625-3 .23835 70 130mg/L.25025

L18864-03ASD 06/28/14 5:01 .005 94.7ASD MS140625-3 .242 1.5270 130mg/L 20.25025

WG366709CCV1 06/28/14 5:14 91.1CCV MS140513-2 .2279 90 110mg/L.25025

WG366709CCB1 06/28/14 5:17CCB U -0.0003 0.0003mg/L

WG366709CCV2 06/28/14 5:53 95.5CCV MS140513-2 .2389 90 110mg/L.25025

WG366709CCB2 06/28/14 5:56CCB .00017 -0.0003 0.0003mg/L

WG366709CCV3 06/28/14 6:19 95.8CCV MS140513-2 .2398 90 110mg/L.25025

WG366709CCB3 06/28/14 6:22CCB .0002 -0.0003 0.0003mg/L



WG366108

WG366108ICV 06/18/14 20:22 99.5ICV II140512-2 42.6 95 105mg/L42.8

WG366108ICB 06/18/14 20:28ICB U -0.6 0.6mg/L

WG366108PQV 06/18/14 20:31 103.6PQV II140609-2 1.11 70 130mg/L1.0714

WG366108SIC 06/18/14 20:34 98.9SIC II140602-1 1.06 80 120mg/L1.0714

WG366108LFB 06/18/14 20:41 105LFB II140611-2 22.5 85 115mg/L21.428

L18871-01AS 06/18/14 20:47 13.3 103.1AS II140611-2 35.39 85 115mg/L21.428

L18871-01ASD 06/18/14 20:50 13.3 103.9ASD II140611-2 35.56 0.4885 115mg/L 2021.428

WG366108CCV1 06/18/14 21:13 101CCV II140506-1 21.62 90 110mg/L21.4

WG366108CCB1 06/18/14 21:16CCB U -0.6 0.6mg/L

WG366108CCV2 06/18/14 21:51 100.3CCV II140506-1 21.46 90 110mg/L21.4

WG366108CCB2 06/18/14 21:54CCB U -0.6 0.6mg/L

WG366108CCV3 06/18/14 22:13 100.5CCV II140506-1 21.51 90 110mg/L21.4

WG366108CCB3 06/18/14 22:16CCB U -0.6 0.6mg/L

Page 19 of 34L18871-1407111615


Inorganic QC

Summary




WG366108

WG366108ICV 06/18/14 20:22 98.8ICV II140512-2 98.79 95 105mg/L100

WG366108ICB 06/18/14 20:28ICB U -0.6 0.6mg/L

WG366108PQV 06/18/14 20:31 101.9PQV II140609-2 1.02 70 130mg/L1.001

WG366108SIC 06/18/14 20:34 104.9SIC II140602-1 1.05 80 120mg/L1.001

WG366108LFB 06/18/14 20:41 103.8LFB II140611-2 103.8 85 115mg/L100.0393

L18871-01AS M306/18/14 20:47 514 78.1AS II140611-2 592.1 85 115mg/L100.0393

L18871-01ASD M306/18/14 20:50 514 75.7ASD II140611-2 589.7 0.4185 115mg/L 20100.0393

WG366108CCV1 06/18/14 21:13 99.6CCV II140506-1 49.81 90 110mg/L50

WG366108CCB1 06/18/14 21:16CCB U -0.6 0.6mg/L

WG366108CCV2 06/18/14 21:51 98.9CCV II140506-1 49.46 90 110mg/L50

WG366108CCB2 06/18/14 21:54CCB U -0.6 0.6mg/L

WG366108CCV3 06/18/14 22:13 98.9CCV II140506-1 49.45 90 110mg/L50

WG366108CCB3 06/18/14 22:16CCB U -0.6 0.6mg/L



WG366559

WG366559PBW 06/26/14 9:13PBW U -30 30mg/L


L18985-04DUP RA06/26/14 10:19 20DUP 17 16.2mg/L 20



WG366002

WG366002ICV 06/17/14 10:28 102.2ICV WC140617- .319 90 110mg/L.312

WG366002ICB 06/17/14 10:33ICB U -0.06 0.06mg/L

WG366002LFB 06/17/14 10:38 117.9LFB WC140617- .283 80 120mg/L.24

WG366002CCV1 06/17/14 11:30 101.1CCV WC140617- .182 90 110mg/L.18

WG366002CCB1 06/17/14 11:35CCB U -0.06 0.06mg/L

L18873-02AS 06/17/14 12:22 U 99.6AS WC140617- .239 75 125mg/L.24

L18873-02DUP RA06/17/14 12:27 UDUP U 0mg/L 20

WG366002CCV2 06/17/14 12:32 100CCV WC140617- .18 90 110mg/L.18

WG366002CCB2 06/17/14 12:37CCB U -0.06 0.06mg/L

WG366002CCV3 06/17/14 13:08 98.3CCV WC140617- .177 90 110mg/L.18

WG366002CCB3 06/17/14 13:13CCB U -0.06 0.06mg/L

Page 20 of 34L18871-1407111615


Inorganic QC

Summary




WG366709

WG366709ICV 06/28/14 4:38 103ICV MS140513-1 .05148 90 110mg/L.05

WG366709ICB 06/28/14 4:41ICB U -0.0003 0.0003mg/L

WG366709LFB 06/28/14 4:44 101.4LFB MS140625-3 .05076 85 115mg/L.05005

L18864-03AS 06/28/14 4:57 .738 97.5AS MS140625-3 .982 70 130mg/L.25025

L18864-03ASD 06/28/14 5:01 .738 99.7ASD MS140625-3 .9875 0.5670 130mg/L 20.25025

WG366709CCV1 06/28/14 5:14 98.3CCV MS140513-2 .09829 90 110mg/L.1

WG366709CCB1 06/28/14 5:17CCB U -0.0003 0.0003mg/L

WG366709CCV2 06/28/14 5:53 96.4CCV MS140513-2 .09642 90 110mg/L.1

WG366709CCB2 06/28/14 5:56CCB U -0.0003 0.0003mg/L

WG366709CCV3 06/28/14 6:19 96.7CCV MS140513-2 .09668 90 110mg/L.1

WG366709CCB3 06/28/14 6:22CCB U -0.0003 0.0003mg/L



WG366108

WG366108ICV 06/18/14 20:22 99.5ICV II140512-2 1.9892 95 105mg/L2

WG366108ICB 06/18/14 20:28ICB U -0.015 0.015mg/L

WG366108PQV 06/18/14 20:31 98.8PQV II140609-2 .0247 70 130mg/L.025

WG366108SIC 06/18/14 20:34 99.7SIC II140602-1 .0997 80 120mg/L.1

WG366108LFB 06/18/14 20:41 105.7LFB II140611-2 .5284 85 115mg/L.5

L18871-01AS 06/18/14 20:47 .016 105.4AS II140611-2 .5429 85 115mg/L.5

L18871-01ASD 06/18/14 20:50 .016 105.4ASD II140611-2 .543 0.0285 115mg/L 20.5

WG366108CCV1 06/18/14 21:13 101.1CCV II140506-1 1.011 90 110mg/L1

WG366108CCB1 06/18/14 21:16CCB U -0.015 0.015mg/L

WG366108CCV2 06/18/14 21:51 99.8CCV II140506-1 .9976 90 110mg/L1

WG366108CCB2 06/18/14 21:54CCB U -0.015 0.015mg/L

WG366108CCV3 06/18/14 22:13 100.8CCV II140506-1 1.008 90 110mg/L1

WG366108CCB3 06/18/14 22:16CCB U -0.015 0.015mg/L



WG366108

WG366108ICV 06/18/14 20:22 99ICV II140512-2 1.979 95 105mg/L2

WG366108ICB 06/18/14 20:28ICB U -0.03 0.03mg/L

WG366108PQV 06/18/14 20:31 104PQV II140609-2 .052 70 130mg/L.05

WG366108SIC 06/18/14 20:34 100SIC II140602-1 .1 80 120mg/L.1

WG366108LFB 06/18/14 20:41 105.7LFB II140611-2 .529 85 115mg/L.5005

L18871-01AS 06/18/14 20:47 .02 106.7AS II140611-2 .554 85 115mg/L.5005

L18871-01ASD 06/18/14 20:50 .02 106.1ASD II140611-2 .551 0.5485 115mg/L 20.5005

WG366108CCV1 06/18/14 21:13 99.3CCV II140506-1 .993 90 110mg/L1

WG366108CCB1 06/18/14 21:16CCB U -0.03 0.03mg/L

WG366108CCV2 06/18/14 21:51 98.8CCV II140506-1 .988 90 110mg/L1

WG366108CCB2 06/18/14 21:54CCB U -0.03 0.03mg/L

WG366108CCV3 06/18/14 22:13 99.3CCV II140506-1 .993 90 110mg/L1

WG366108CCB3 06/18/14 22:16CCB U -0.03 0.03mg/L

Page 21 of 34L18871-1407111615


Inorganic Extended

Qualifier Report




M200.7 ICPBoron, dissolvedL18871-01 WG3661 08


M200.7 ICPSodium, dissolved

ZW Method deviation. The sample was centrifuged prior to analysis due to high solid content.

SM2320B - TitrationBicarbonate as CaCO3WG366285

DF Sample required dilution due to high sediment.SM5 31 0BCarbon, total organic (TOC)WG366762

RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 1 0x MDL).

SM5 31 0B


SM2320B - TitrationCarbonate as CaCO3WG366285


SM2320B - TitrationHydroxide as CaCO3


M35 3.2 - H2SO4 preservedNitrate/Nitrite as NWG366907


M35 0.1 - Automated PhenateNitrogen, ammoniaWG366677


SM25 40CResidue, Filterable (TDS) @1 80CWG365 961


SM25 40DResidue, Non-Filterable (TSS) @1 05 CWG365 95 1


SM45 00 SO4-DSulfateWG3665 5 9

DD Sample required dilution due to matrix color or odor.SM45 00S2-DSulfide as SWG366002

DF Sample required dilution due to high sediment.SM45 00S2-D


SM45 00S2-D


SM45 00S2-D



REPAD.1 5 .06.05 .01

Page 22 of 34L18871-1407111615


Inorganic Extended

Qualifier Report








SM5 31 0BCarbon, total organic (TOC)WG366762












SM45 00S2-DSulfide as SWG366002

REPAD.1 5 .06.05 .01

Page 23 of 34L18871-1407111615


Inorganic Extended

Qualifier Report










SM5 31 0BCarbon, total organic (TOC)WG366762




SM2320B - TitrationHydroxide as CaCO3

RA Relative Percent Difference (RPD) was not used for data

validation because the sample concentration is too low for accurate evaluation (< 1 0x MDL).










DF Sample required dilution due to high sediment.SM45 00S2-DSulfide as SWG366002

QD Reported value is the background-corrected concentration,

as described by the method.

SM45 00S2-D


SM45 00S2-D




SM2320B - Titration

REPAD.1 5 .06.05 .01

Page 24 of 34L18871-1407111615


Sample ID: MW9



Project ID:


Date Sampled: 06/11/14 13:45


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 32 1 1 5.3 pCi/L * nco06/25/1 4 1 4:00

Gross Beta 28 8.6 1 1 pCi/L nco06/25/1 4 1 4:00

Lead 21 0, dissolved

EICHROM, OTW01

Prep Method:


Lead 21 0, dissolved -8.2 2.1 7.6 pCi/L * jrd07/01 /1 4 1 4:59


M903.1

Prep Method:


Radium 226, dissolved 0.39 0.1 0.1 4 pCi/L nco06/24/1 4 1 0:01


M904.0

Prep Method:


Radium 228, dissolved 1 .8 1 .1 1 .1 pCi/L jrd06/30/1 4 21 :41


ESM 4506

Prep Method:


Thorium 230, dissolved 0.34 0.33 0.56 pCi/L * nco07/09/1 4 1 5:21


Page 25 of 34L18871-1407111615


Sample ID: MW7



Project ID:


Date Sampled: 06/10/14 12:30


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 55 1 1 3.4 pCi/L * nco06/25/1 4 1 4:01

Gross Beta 29 6.4 7 pCi/L nco06/25/1 4 1 4:01

Lead 21 0, dissolved

EICHROM, OTW01

Prep Method:


Lead 21 0, dissolved -5.2 2.1 7.4 pCi/L * jrd07/01 /1 4 1 4:59


M903.1

Prep Method:


Radium 226, dissolved 0.2 0.09 0.4 pCi/L nco06/24/1 4 1 0:03


M904.0

Prep Method:


Radium 228, dissolved 1 .3 0.77 0.73 pCi/L jrd06/30/1 4 21 :41


ESM 4506

Prep Method:


Thorium 230, dissolved 0.24 0.29 0.55 pCi/L * nco07/09/1 4 1 5:22


Page 26 of 34L18871-1407111615


Sample ID: MW5



Project ID:


Date Sampled: 06/11/14 12:05


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 50 9.1 2.8 pCi/L * nco06/25/14 14:03

Gross Beta 36 5.9 5.6 pCi/L nco06/25/14 14:03

Lead 210, dissolved

EICHROM, OTW01

Prep Method:




M903.1

Prep Method:




M904.0

Prep Method:




ESM 4506

Prep Method:




Page 27 of 34L18871-1407111615



Batch A distinct set of samples analyz ed at a specific time

Error(+/-) C alculated sample specific uncertainty

Found V alue of the QC Type of interest

Limit U pper limit for RPD, in %.

LCL Lower Control Limit, in % (except for LCSS, mg /Kg )


P CN/SCN A numb er assig ned to reag ents/standards to trace to the manufacturer's certificate of analysis



Rec Amount of the true value or spike added recovered, in % (except for LCSS, mg /Kg )



UCL Upper Control Limit, in % (except for LCSS, mg /Kg )


QC Sample Types


LCSS Lab oratory Control Sample - Soil P BS Prep Blank - Soil

LCSW Lab oratory Control Sample - Water P BW Prep Blank - Water









M EPA methodolog y, including those under SDWA, CWA, and RCRA


D ASTM

RP DOE

ESM DOE/ESM

Comments

(1) Solid matrices are reported on a dry weig ht b asis.





For a complete list of ACZ's Extended Qualifiers, please click: http://www.acz.com/pub lic/extquallist.pdf

REP003.09.12.01

Radiochemistry

Reference

Page 28 of 34L18871-1407111615


Radiochemistry QC

Summary


Alpha M900.0


pC i/L

Error LLDLLD

Units:

WG366557

WG3661 36PBW 06/25/1 4PBW 0 21 .1 1

WG3661 36LCSWA 06/25/1 4 1 1 5.5LCSW PCN45468 7766.67 83 1 336.4 1

L1 8871 -01 DUP 06/25/1 4 32DUP-RER 34 21 2 0.1 21 1 5.45.3

L1 8871 -02MSA M206/25/1 4 55 28MS PCN45468 951 42.86 83 1 331 31 1 3.43.4

Beta M900.0


pC i/L

Error LLDLLD

Units:

WG366557

WG3661 36PBW 06/25/1 4PBW .32 6.22.2 3.1

WG3661 36LCSWB 06/25/1 4 1 1 2.5LCSW PCN44650 7566.67 70 1 294.8 2.9

L1 8871 -01 DUP 06/25/1 4 28DUP-RER 43 29.9 1 .1 48.6 1 11 1

L1 8871 -03MSB 06/25/1 4 36 1 1 1 .6MS PCN44650 1 601 1 1 .1 1 70 1 299.55.9 5.55.6



pC i/L

Error LLDLLD

Units:

WG366950

WG366408PBW 07/01 /1 4PBW -1 4 1 4.81 .9 7.4

WG366408LCSW 07/01 /1 4 67.4LCSW PCN441 22 6697.89 55 1 213.2 6.5

L1 9028-01 DUP 07/01 /1 4 21DUP-RER 26 22.5 1 .392.6 6.27

L1 9028-04DUP 07/01 /1 4 -8DUP-RER -7.4 22 0.212 77.2

L1 9028-05MS 07/01 /1 4 -9.6 84.4MS PCN441 22 7397.89 55 1 2142.1 9.27.7

Page 29 of 34L18871-1407111615


Radiochemistry QC

Summary


Radium 226, dissolved M903. 1


pC i/L

Error LLDLLD

Units:

WG366465

WG366007PBW 06/24/1 4PBW .1 8 0.480.1 1 0.24

WG366007LCSW 06/24/1 4 80LCSW PCN4581 7 1 620 43 1 480.55 0.24

L1 8723-02DUP 06/24/1 4 21DUP-RER 20 20.61 1 .080.7 0.210.26

L1 8827-02DUP 06/24/1 4 0.22DUP-RER .22 20.09 00.1 3 0.260.1 7

L1 8774-01 MS 06/24/1 4 2.7 91 .5MS PCN4581 7 2120 43 1 480.570.24 0.1 40.23



pC i/L

Error LLDLLD

Units:

WG366956

WG36661 1 LCSW 06/30/1 4 86.6LCSW PCN44321 1 61 8.48 47 1 231 .3 0.58

WG36661 1 PBW 06/30/1 4PBW .32 0.680.34 0.34

L1 8871 -01 DUP 07/01 /1 4 1 .8DUP-RER .95 20.83 0.621 .1 0.821 .1

L1 8871 -02MS 07/01 /1 4 1 .3 85MS PCN44321 1 71 8.48 47 1 231 .70.77 0.920.73

L1 9039-01 DUP 07/01 /1 4 2.3DUP-RER 2.8 21 .1 0.40.62 0.960.49



pC i/L

Error LLDLLD

Units:

WG367377

WG366799PBW 07/09/1 4PBW .41 1 .060.3 0.53

WG366799LCSW 07/09/1 4 1 04.9LCSW RC 1 30807-2 1 701 62.1 2 91 1 264.6 0.62

L1 8871 -02DUP 07/09/1 4 0.24DUP-RER .38 20.56 0.220.29 0.520.55

L1 901 4-01 DUP 07/09/1 4 -0.1 9DUP-RER .09 20.98 0.270.36 0.540.61

L1 8871 -03MS 07/09/1 4 0.1 4 1 04.8MS RC 1 30807-2 1 701 62.1 2 91 1 264.50.31 0.610.57

Page 30 of 34L18871-1407111615


RadChem Extended

Qualifier Report




M900.0Gross AlphaL18871-01 WG366557





REPAD.1 5.06.05.01

Page 31 of 34L18871-1407111615


Certification

Qualifiers


Metals Analysis


C esium, dissolved M200.8 IC P-MS

Radiochemistry


Lead 21 0, dissolved EICHROM, OTW01


Wet C hemistry



REPAD.05.06.05.01

Page 32 of 34L18871-1407111615


Sample

Receipt


Date Received:

Received By: ear

06/1 3/201 4 1 0:44

L1 8871

Date Printed: 6/1 3/201 4



NANOYES

X

X

X

X

X

X

1 ) Is a foreign soil permit included for applicable samples?

2) Is the C hain of C ustody or other directive shipping papers present?

3) Does this project require special handling procedures such as C LP protocol?



6) Is the C hain of C ustody complete and accurate?

7) Were any changes made to the C hain of C ustody prior to ACZ receiving the samples?


NANOYES

X

X

X

X

X

X

X



1 0) Do the sample labels and C hain of C ustody match for Sample ID, Date, and Time?

1 1 ) For preserved bottle types, was the pH checked and within limits?

1 2) Is there sufficient sample volume to perform all requested work?

1 3) Is the custody seal intact on all containers?

1 4) Are samples that require zero headspace acceptable?

1 5) Are all sample containers appropriate for analytical requirements?

1 6) Is there an Hg-1 631 trip blank present?

1 7) Is there a VOA trip blank present?

1 8) Were all samples received within hold time?

Samples/Containers

X

X

X

Shipping Containers

C lient must contact an ACZ Project Manager if analysis should not proceed for samples received outside of their thermal preservation acceptance criteria.

Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- --------------------3565 5.2 14 Yes3931 0.6 13 Yes

X



REPAD LPII 201 2-03

Page 33 of 34L18871-1407111615

of 34L18871-1407111615


Analytical

Report



Lakewood, CO 80228

ACZ Project ID: L1 901 4

Kathy Weinel:

Enclosed are the analytical results for sample(s) submitted to ACZ Laboratories, Inc. (ACZ) on June 20, 201 4. This project has been assigned to AC Z's project number, L1 901 4. Please reference this number in all future inquiries.

All analyses were performed according to ACZ's Quality Assurance Plan. The enclosed results relate only to the samples received under L1 901 4. Each section of this report has been reviewed and approved by the appropriate Laboratory Supervisor, or a qualified substitute.

Except as noted, the test results for the methods and parameters listed on AC Z's current NELAC certificate letter (#ACZ) meet all requirements of NELAC .


All samples and sub-samples associated with this project will be disposed of after August 1 0, 201 4. If the samples are determined to be hazardous, additional charges apply for disposal (typically $ 1 1 /sample). If you would like the samples to be held longer than ACZ's stated policy or to be returned, please contact your Project Manager or C ustomer Service Representative for further details and associated costs. ACZ retains analytical raw data reports for ten years.


Kathy Weinel

July 1 1 , 201 4

Project ID:



Lakewood, CO 80228

Accounts Payable

Report to: Bill to:

Page 1 of 28L19014-1407111618


Case

Narrative


ACZ Project ID: L1 901 4

July 1 1 , 201 4

Sample Receipt

Sample Analysis

Holding Times

Text1 0:ACZ Laboratories, Inc. (ACZ) received 1 ground water sample from Energy Fuels Resources (USA) Inc. on June 20, 201 4. The sample was received in good condition. Upon receipt, the sample custodian removed the sample from the cooler, inspected the contents, and logged the sample into ACZ's computerized Laboratory Information Management System (LIMS). The sample was assigned AC Z LIMS project number L1 901 4. The custodian verified the sample information entered into the computer against the chain of custody (COC ) forms and sample bottle labels.

Text1 0:This sample was analyzed for inorganic, radiochemistry parameters. The individual methods are referenced on both the ACZ invoice and the analytical reports. The extended qualifier reports may contain footnotes qualifying specific elements due to QC failures. In addition the following has been noted with this specific project:

The Gross Alpha results for L1 901 4-01 have been qualified with the N1 flag on the radiochemistry extended qualifier report. The chemist noted precision statistic failures due to uneven residue distribution on the planchet. Data qualification may be necessary.

Text1 0:Any analyses not performed within EPA recommended holding times have been qualified with an "H" flag.

Project ID:

REPAD.03.06.05.01 Page 2 of 28L19014-1407111618


Sample ID: MW8



Project ID:



Results

Date Sampled: 06/16/14 12:40



Metals Analysis

XQDilution

Aluminum, dissolved M200.7 ICP mg/L 0.2U jjc0.03* 06/23/14 23:571


Barium, dissolved M200.7 ICP 0.029 mg/L 0.02 jjc0.003 06/23/14 23:571



Calcium, dissolved M200.7 ICP 303 mg/L 0.5 jjc0.1 06/23/14 23:571




Iron, dissolved M200.7 ICP 1.02 mg/L 0.05 jjc0.02 06/23/14 23:571


Magnesium, dissolved M200.7 ICP 212 mg/L 1 jjc0.2 06/23/14 23:571

Manganese, dissolved M200.7 ICP 0.373 mg/L 0.03 jjc0.005 06/23/14 23:571

Mercury, dissolved M245.1 CVAA mg/L 0.001U mfm0.0002* 06/25/14 13:401

Molyb denum, dissolved M200.7 ICP mg/L 0.1U jjc0.02 06/23/14 23:571





Sodium, dissolved M200.7 ICP 23.2 mg/L 1 jjc0.2 06/23/14 23:571


Vanadium, dissolved M200.7 ICP mg/L 0.03U jjc0.005 06/23/14 23:571

Zinc, dissolved M200.7 ICP mg/L 0.05U jjc0.01 06/23/14 23:571


Page 3 of 28L19014-1407111618


Sample ID: MW8



Project ID:



Results

Date Sampled: 06/16/14 12:40



Wet Chemistry

XQDilution



405 mg/L 20 jad2* 06/27/14 0:001

Carb onate as CaCO3 mg/L 20U jad2* 06/27/14 0:001

Hydroxide as CaCO3 mg/L 20U jad2* 06/27/14 0:001

Total Alkalinity 405 mg/L 20 jad2* 06/27/14 0:001

Carb on, total organic (TOC)

SM5310B mg/L 50U mpb10* 07/02/14 18:5010





Chloride SM4500Cl-E 29.2 mg/L 2 mss20.5 07/08/14 9:381

Fluoride SM4500F-C 0.66 mg/L 0.3 ab d0.05* 07/07/14 14:081

Nitrate/Nitrite as N M353.2 - H2SO4 preserved mg/L 0.1U pjb0.02* 07/09/14 0:081

Nitrogen, ammonia M350.1 - Automated Phenate 0.05 mg/L 0.2B b su0.05* 07/02/14 16:531

Residue, Filterab le (TDS) @180C

SM2540C 1930 mg/L 100 eaa50 06/20/14 17:075

Residue, Non-Filterab le (TSS) @105C

SM2540D 2740 mg/L 40 eaa10* 06/23/14 14:012

Sulfate SM4500 SO4-D 1120 mg/L 50 eaa10* 07/02/14 15:381

Sulfide as S SM4500S2-D mg/L 2U ab d0.3* 06/23/14 16:4615





Page 4 of 28L19014-1407111618






Lower Lower Recovery Limit, in % (except for LCSS, mg /Kg )


P CN/SCN A numb er assig ned to reag ents/standards to trace to the manufacturer's certificate of analysis



Rec Recovered amount of the true value or spike added, in % (except for LCSS, mg /Kg )


Upper Upper Recovery Limit, in % (except for LCSS, mg /Kg )


QC Sample Types

AS Analytical Spike (Post Dig estion) LCSWD Lab oratory Control Sample - Water Duplicate

ASD Analytical Spike (Post Dig estion) Duplicate LFB Lab oratory Fortified Blank

CCB Continuing Calib ration Blank LFM Lab oratory Fortified Matrix

CCV Continuing Calib ration Verification standard LFMD Lab oratory Fortified Matrix Duplicate

DUP Sample Duplicate LRB Lab oratory Reag ent Blank

ICB Initial Calib ration Blank MS Matrix Spike

ICV Initial Calib ration Verification standard MSD Matrix Spike Duplicate


LCSS Lab oratory Control Sample - Soil P BW Prep Blank - Water

LCSSD Lab oratory Control Sample - Soil Duplicate P QV Practical Quantitation Verification standard

LCSW Lab oratory Control Sample - Water SDL Serial Dilution


Blanks Verifies that there is no or minimal contamination in the prep method or calib ration procedure.




Standard Verifies the validity of the calib ration.


B Analyte concentration detected at a value b etween MDL and PQL. The associated value is an estimated quantity.


L Targ et analyte response was b elow the lab oratory defined neg ative threshold.

U The material was analyzed for, b ut was not detected ab ove the level of the associated value.


Method References


(2) EPA 600/R-93-100. Methods for the Determination of Inorg anic Sub stances in Environmental Samples, Aug ust 1993.




Comments


(2) Soil, Sludg e, and Plant matrices for Inorg anic analyses are reported on a dry weig ht b asis.

(3) Animal matrices for Inorg anic analyses are reported on an "as received" b asis.





REP001.09.12.01

Inorganic

Reference

Page 5 of 28L19014-1407111618


Inorganic QC

Summary




WG366660

WG366660PBW1 06/27/14 1 5:01PBW U -20 20mg/L

WG366660LCSW3 06/27/1 4 1 5:21 1 01LCSW WC 1 4061 0- 828.5 90 1 1 0mg/L820.0001

L1 901 4-01 DUP 06/27/1 4 1 7:57 405DUP 392.1 3.2mg/L 20

WG366660LCSW6 06/27/1 4 1 8:1 7 1 01 .8LCSW WC 1 4061 0- 834.5 90 1 1 0mg/L820.0001

WG366660PBW2 06/27/1 4 1 8:26PBW 2.5 -20 20mg/L

WG366660LCSW9 06/27/1 4 21 :47 1 01 .5LCSW WC 1 4061 0- 832 90 1 1 0mg/L820.0001

WG366660PBW3 06/27/1 4 21 :56PBW 2.6 -20 20mg/L

WG366660LCSW1 2 06/28/1 4 1 :46 1 02.1LCSW WC 1 4061 0- 837.5 90 1 1 0mg/L820.0001

WG366660PBW4 06/28/1 4 1 :56PBW 2.8 -20 20mg/L

WG366660LCSW1 5 06/28/1 4 5:52 1 03.1LCSW WC 1 4061 0- 845.8 90 1 1 0mg/L820.0001



WG366352

WG366352ICV 06/23/1 4 23:26 1 00.1IC V II1 4051 2-2 2.001 95 1 05mg/L2

WG366352ICB 06/23/1 4 23:32IC B U -0.09 0.09mg/L

WG366352PQV 06/23/1 4 23:35 97.2PQV II1 40609-2 .1 46 70 1 30mg/L.1 501 65

WG366352SIC 06/23/1 4 23:39 1 02.2SIC II1 40602-1 204.8 1 200mg/L200.3701 65

WG366352LFB 06/23/1 4 23:45 1 08.4LFB II1 4061 1 -2 1 .085 85 1 1 5mg/L1 .001 1

L1 901 4-01 AS MA06/24/1 4 0:00 U 1 1 5.5AS II1 4061 1 -2 1 .1 56 85 1 1 5mg/L1 .001 1

L1 901 4-01 ASD 06/24/1 4 0:03 U 1 1 4.9ASD II1 4061 1 -2 1 .1 5 0.5285 1 1 5mg/L 201 .001 1

WG366352CCV1 06/24/1 4 0:1 6 99.4C CV II1 40506-1 .994 90 1 1 0mg/L1

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.09 0.09mg/L

WG366352CCV2 06/24/1 4 0:54 98.8C CV II1 40506-1 .988 90 1 1 0mg/L1

WG366352CCB2 06/24/1 4 0:57C CB U -0.09 0.09mg/L

WG366352CCV3 06/24/1 4 1 :1 6 99.6C CV II1 40506-1 .996 90 1 1 0mg/L1

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.09 0.09mg/L



WG367132

WG3671 32ICV 07/07/1 4 21 :38 1 03.5IC V MS1 4051 3-1 .051 75 90 1 1 0mg/L.05

WG3671 32ICB 07/07/1 4 21 :41IC B U -0.0006 0.0006mg/L

WG3671 32LFB 07/07/1 4 21 :45 1 01 .4LFB MS1 40625-3 .05078 85 1 1 5mg/L.0501

L1 91 1 7-02AS 07/07/1 4 21 :58 U 1 1 0.1AS MS1 40625-3 .0551 8 70 1 30mg/L.0501

L1 91 1 7-02ASD 07/07/1 4 22:01 U 1 1 3.1ASD MS1 40625-3 .05664 2.6170 1 30mg/L 20.0501

WG3671 32C CV1 07/07/1 4 22:1 4 1 00.7C CV MS1 4051 3-2 .1 009 90 1 1 0mg/L.1 002

WG3671 32C CB1 07/07/1 4 22:1 7C CB U -0.0006 0.0006mg/L

WG3671 32C CV2 07/07/1 4 22:53 99.9C CV MS1 4051 3-2 .1 001 90 1 1 0mg/L.1 002

WG3671 32C CB2 07/07/1 4 22:56C CB U -0.0006 0.0006mg/L

WG3671 32C CV3 07/07/1 4 23:1 9 99.3C CV MS1 4051 3-2 .09954 90 1 1 0mg/L.1 002

WG3671 32C CB3 07/07/1 4 23:22C CB U -0.0006 0.0006mg/L

Page 6 of 28L19014-1407111618


Inorganic QC

Summary




WG366352

WG366352ICV 06/23/1 4 23:26 98.4IC V II1 4051 2-2 1 .968 95 1 05mg/L2

WG366352ICB 06/23/1 4 23:32IC B U -0.009 0.009mg/L

WG366352PQV 06/23/1 4 23:35 96PQV II1 40609-2 .01 44 70 1 30mg/L.01 5

WG366352SIC 06/23/1 4 23:39 1 00.9SIC II1 40602-1 .1 009 80 1 20mg/L.1

WG366352LFB 06/23/1 4 23:45 1 00.1LFB II1 4061 1 -2 .5005 85 1 1 5mg/L.5

L1 901 4-01 AS 06/24/1 4 0:00 .029 1 02.1AS II1 4061 1 -2 .5395 85 1 1 5mg/L.5

L1 901 4-01 ASD 06/24/1 4 0:03 .029 1 02.4ASD II1 4061 1 -2 .5409 0.2685 1 1 5mg/L 20.5

WG366352CCV1 06/24/1 4 0:1 6 99.5C CV II1 40506-1 .9952 90 1 1 0mg/L1

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.009 0.009mg/L

WG366352CCV2 06/24/1 4 0:54 99.8C CV II1 40506-1 .9976 90 1 1 0mg/L1

WG366352CCB2 06/24/1 4 0:57C CB U -0.009 0.009mg/L

WG366352CCV3 06/24/1 4 1 :1 6 99.5C CV II1 40506-1 .9947 90 1 1 0mg/L1

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.009 0.009mg/L



WG366352

WG366352ICV 06/23/1 4 23:26 1 01 .8IC V II1 4051 2-2 2.035 95 1 05mg/L2

WG366352ICB 06/23/1 4 23:32IC B U -0.03 0.03mg/L

WG366352PQV 06/23/1 4 23:35 1 01 .9PQV II1 40609-2 .051 70 1 30mg/L.05005

WG366352SIC 06/23/1 4 23:39 97.9SIC II1 40602-1 .098 80 1 20mg/L.1 001

WG366352LFB 06/23/1 4 23:45 1 04.3LFB II1 4061 1 -2 .522 85 1 1 5mg/L.5005

L1 901 4-01 AS 06/24/1 4 0:00 .53 98.7AS II1 4061 1 -2 1 .024 85 1 1 5mg/L.5005

L1 901 4-01 ASD 06/24/1 4 0:03 .53 1 00.1ASD II1 4061 1 -2 1 .031 0.6885 1 1 5mg/L 20.5005

WG366352CCV1 06/24/1 4 0:1 6 1 01 .9C CV II1 40506-1 1 .01 9 90 1 1 0mg/L1

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.03 0.03mg/L

WG366352CCV2 06/24/1 4 0:54 1 00.8C CV II1 40506-1 1 .008 90 1 1 0mg/L1

WG366352CCB2 06/24/1 4 0:57C CB U -0.03 0.03mg/L

WG366352CCV3 06/24/1 4 1 :1 6 1 01 .9C CV II1 40506-1 1 .01 9 90 1 1 0mg/L1

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.03 0.03mg/L



WG367132

WG3671 32ICV 07/07/1 4 21 :38 95.7IC V MS1 4051 3-1 .04785 90 1 1 0mg/L.05

WG3671 32ICB 07/07/1 4 21 :41IC B U -0.0003 0.0003mg/L

WG3671 32LFB 07/07/1 4 21 :45 93.8LFB MS1 40625-3 .04698 85 1 1 5mg/L.0501

L1 91 1 7-02AS 07/07/1 4 21 :58 U 98AS MS1 40625-3 .0491 1 70 1 30mg/L.0501

L1 91 1 7-02ASD 07/07/1 4 22:01 U 97.5ASD MS1 40625-3 .04886 0.5170 1 30mg/L 20.0501

WG3671 32C CV1 07/07/1 4 22:1 4 94.3C CV MS1 4051 3-2 .09447 90 1 1 0mg/L.1 002

WG3671 32C CB1 07/07/1 4 22:1 7C CB U -0.0003 0.0003mg/L

WG3671 32C CV2 07/07/1 4 22:53 92.1C CV MS1 4051 3-2 .09233 90 1 1 0mg/L.1 002

WG3671 32C CB2 07/07/1 4 22:56C CB U -0.0003 0.0003mg/L

WG3671 32C CV3 07/07/1 4 23:1 9 90.3C CV MS1 4051 3-2 .0905 90 1 1 0mg/L.1 002

WG3671 32C CB3 07/07/1 4 23:22C CB U -0.0003 0.0003mg/L

Page 7 of 28L19014-1407111618


Inorganic QC

Summary




WG366352

WG366352ICV 06/23/1 4 23:26 1 00.1IC V II1 4051 2-2 1 00.1 1 95 1 05mg/L1 00

WG366352ICB 06/23/1 4 23:32IC B U -0.3 0.3mg/L

WG366352PQV 06/23/1 4 23:35 84PQV II1 40609-2 .42 70 1 30mg/L.5002

WG366352SIC 06/23/1 4 23:39 98.6SIC II1 40602-1 1 97.7 1 200mg/L200.5002

WG366352LFB 06/23/1 4 23:45 1 08.3LFB II1 4061 1 -2 73.59 85 1 1 5mg/L67.98099

L1 901 4-01 AS 06/24/1 4 0:00 303 87.4AS II1 4061 1 -2 362.4 85 1 1 5mg/L67.98099

L1 901 4-01 ASD 06/24/1 4 0:03 303 88ASD II1 4061 1 -2 362.8 0.1 185 1 1 5mg/L 2067.98099

WG366352CCV1 06/24/1 4 0:1 6 99.9C CV II1 40506-1 49.93 90 1 1 0mg/L50

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.3 0.3mg/L

WG366352CCV2 06/24/1 4 0:54 99.4C CV II1 40506-1 49.68 90 1 1 0mg/L50

WG366352CCB2 06/24/1 4 0:57C CB U -0.3 0.3mg/L

WG366352CCV3 06/24/1 4 1 :1 6 1 00.6C CV II1 40506-1 50.31 90 1 1 0mg/L50

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.3 0.3mg/L

Carbon, total organic (TOC) SM531 0B


WG358122

WG3581 22ICV 01 /22/1 4 1 1 :52 1 02IC V WI1 31 209-3 1 02 90 1 1 0mg/L1 00

WG3581 22ICB 01 /22/1 4 1 1 :52IC B U -3 3mg/L

WG366937

WG366937CCV1 07/02/1 4 1 8:50 1 00.4C CV WI1 40502-1 50.2 90 1 1 0mg/L50

WG366937CCB1 07/02/1 4 1 8:50C CB U -3 3mg/L

WG366937PQV 07/02/1 4 1 8:50 1 04PQV WI1 40502-3 5.2 70 1 30mg/L5

WG366937LFB1 07/02/1 4 1 8:50 96LFB WI1 40502-2 48 90 1 1 0mg/L50

L1 901 4-01 DUP RA07/02/1 4 1 8:50 UDUP U 0mg/L 20

L1 9069-01 AS 07/02/1 4 1 8:50 2 95.2AS WI1 40502-2 49.6 90 1 1 0mg/L50

WG366937CCV2 07/02/1 4 1 8:50 99.6C CV WI1 40502-1 49.8 90 1 1 0mg/L50

WG366937CCB2 07/02/1 4 1 8:50C CB U -3 3mg/L

WG366937CCV3 07/02/1 4 1 8:50 1 00.2C CV WI1 40502-1 50.1 90 1 1 0mg/L50

WG366937CCB3 07/02/1 4 1 8:50C CB U -3 3mg/L

WG366937LFB2 07/02/1 4 1 8:50 99.2LFB WI1 40502-2 49.6 90 1 1 0mg/L50

WG366937CCV4 07/02/1 4 1 8:50 99.8C CV WI1 40502-1 49.9 90 1 1 0mg/L50

WG366937CCB4 07/02/1 4 1 8:50C CB U -3 3mg/L

WG366937CCV5 07/02/1 4 1 8:50 1 00.6C CV WI1 40502-1 50.3 90 1 1 0mg/L50

WG366937CCB5 07/02/1 4 1 8:50C CB U -3 3mg/L

Page 8 of 28L19014-1407111618


Inorganic QC

Summary




WG367132

WG3671 32ICV 07/07/1 4 21 :38 1 04.2IC V MS1 4051 3-1 .0521 1 90 1 1 0mg/L.05

WG3671 32ICB 07/07/1 4 21 :41IC B U -0.0006 0.0006mg/L

WG3671 32LFB 07/07/1 4 21 :45 1 03.5LFB MS1 40625-3 .051 74 85 1 1 5mg/L.05

L1 91 1 7-02AS 07/07/1 4 21 :58 U 1 06.5AS MS1 40625-3 .05326 70 1 30mg/L.05

L1 91 1 7-02ASD 07/07/1 4 22:01 U 1 05.6ASD MS1 40625-3 .0528 0.8770 1 30mg/L 20.05

WG3671 32C CV1 07/07/1 4 22:1 4 1 02.1C CV MS1 4051 3-2 .1 021 90 1 1 0mg/L.1

WG3671 32C CB1 07/07/1 4 22:1 7C CB U -0.0006 0.0006mg/L

WG3671 32C CV2 07/07/1 4 22:53 1 01 .3C CV MS1 4051 3-2 .1 01 3 90 1 1 0mg/L.1

WG3671 32C CB2 07/07/1 4 22:56C CB U -0.0006 0.0006mg/L

WG3671 32C CV3 07/07/1 4 23:1 9 1 02.6C CV MS1 4051 3-2 .1 026 90 1 1 0mg/L.1

WG3671 32C CB3 07/07/1 4 23:22C CB U -0.0006 0.0006mg/L

Chloride SM4500C l-E


WG367155

WG3671 55ICB 07/08/1 4 8:44IC B U -1 .5 1 .5mg/L

WG3671 55ICV 07/08/1 4 8:44 1 04.8IC V WI1 40701 -3 57.66 90 1 1 0mg/L55

WG3671 55C CV1 07/08/1 4 9:32 1 09C CV WI1 31 028-1 54.5 90 1 1 0mg/L50

WG3671 55C CB1 07/08/1 4 9:32C CB U -1 .5 1 .5mg/L

WG3671 55LFB1 07/08/1 4 9:38 1 07.3LFB WI1 40508-1 32.2 90 1 1 0mg/L30

L1 901 4-01 AS 07/08/1 4 9:38 29.2 99.8AS WI1 40508-1 59.1 5 90 1 1 0mg/L30

WG3671 55C CV2 07/08/1 4 9:38 1 09.1C CV WI1 31 028-1 54.55 90 1 1 0mg/L50

WG3671 55C CB2 07/08/1 4 9:38C CB U -1 .5 1 .5mg/L

WG3671 55C CV3 07/08/1 4 9:39 1 09C CV WI1 31 028-1 54.52 90 1 1 0mg/L50

WG3671 55C CB3 07/08/1 4 9:39C CB U -1 .5 1 .5mg/L

WG3671 55C CV4 07/08/1 4 9:40 1 09.8C CV WI1 31 028-1 54.89 90 1 1 0mg/L50

WG3671 55C CB4 07/08/1 4 9:40C CB U -1 .5 1 .5mg/L

WG3671 55LFB2 07/08/1 4 9:42 1 09.4LFB WI1 40508-1 32.81 90 1 1 0mg/L30

WG3671 55C CV5 07/08/1 4 9:42 1 09.5C CV WI1 31 028-1 54.74 90 1 1 0mg/L50

WG3671 55C CB5 07/08/1 4 9:42C CB U -1 .5 1 .5mg/L

WG3671 55C CV6 07/08/1 4 9:48 1 09.5C CV WI1 31 028-1 54.75 90 1 1 0mg/L50

WG3671 55C CB6 07/08/1 4 9:48C CB U -1 .5 1 .5mg/L

WG3671 55C CV7 07/08/1 4 1 0:07 1 08.4C CV WI1 31 028-1 54.21 90 1 1 0mg/L50

WG3671 55C CB7 07/08/1 4 1 0:07C CB U -1 .5 1 .5mg/L

L1 9083-01 DUP 07/08/1 4 1 0:08 1 960DUP 1 940 1mg/L 20

WG3671 55C CV8 07/08/1 4 1 0:08 1 08.2C CV WI1 31 028-1 54.1 2 90 1 1 0mg/L50

WG3671 55C CB8 07/08/1 4 1 0:08C CB U -1 .5 1 .5mg/L

Page 9 of 28L19014-1407111618


Inorganic QC

Summary




WG366352

WG366352ICV 06/23/1 4 23:26 97.5IC V II1 4051 2-2 1 .949 95 1 05mg/L2

WG366352ICB 06/23/1 4 23:32IC B U -0.03 0.03mg/L

WG366352PQV 06/23/1 4 23:35 87.8PQV II1 40609-2 .044 70 1 30mg/L.0501

WG366352SIC 06/23/1 4 23:39 90.8SIC II1 40602-1 .091 80 1 20mg/L.1 002

WG366352LFB 06/23/1 4 23:45 1 01LFB II1 4061 1 -2 .506 85 1 1 5mg/L.501

L1 901 4-01 AS 06/24/1 4 0:00 U 99.4AS II1 4061 1 -2 .498 85 1 1 5mg/L.501

L1 901 4-01 ASD 06/24/1 4 0:03 U 99.4ASD II1 4061 1 -2 .498 085 1 1 5mg/L 20.501

WG366352CCV1 06/24/1 4 0:1 6 97.6C CV II1 40506-1 .976 90 1 1 0mg/L1

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.03 0.03mg/L

WG366352CCV2 06/24/1 4 0:54 97C CV II1 40506-1 .97 90 1 1 0mg/L1

WG366352CCB2 06/24/1 4 0:57C CB U -0.03 0.03mg/L

WG366352CCV3 06/24/1 4 1 :1 6 98.2C CV II1 40506-1 .982 90 1 1 0mg/L1

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.03 0.03mg/L



WG366352

WG366352ICV 06/23/1 4 23:26 97.1IC V II1 4051 2-2 1 .941 95 1 05mg/L2

WG366352ICB 06/23/1 4 23:32IC B U -0.03 0.03mg/L

WG366352PQV 06/23/1 4 23:35 96PQV II1 40609-2 .048 70 1 30mg/L.05

WG366352SIC 06/23/1 4 23:39 94SIC II1 40602-1 .094 80 1 20mg/L.1

WG366352LFB 06/23/1 4 23:45 99.4LFB II1 4061 1 -2 .497 85 1 1 5mg/L.5

L1 901 4-01 AS 06/24/1 4 0:00 U 1 01 .4AS II1 4061 1 -2 .507 85 1 1 5mg/L.5

L1 901 4-01 ASD 06/24/1 4 0:03 U 1 01 .4ASD II1 4061 1 -2 .507 085 1 1 5mg/L 20.5

WG366352CCV1 06/24/1 4 0:1 6 98.1C CV II1 40506-1 .981 90 1 1 0mg/L1

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.03 0.03mg/L

WG366352CCV2 06/24/1 4 0:54 98.4C CV II1 40506-1 .984 90 1 1 0mg/L1

WG366352CCB2 06/24/1 4 0:57C CB U -0.03 0.03mg/L

WG366352CCV3 06/24/1 4 1 :1 6 97.9C CV II1 40506-1 .979 90 1 1 0mg/L1

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.03 0.03mg/L

Page 10 of 28L19014-1407111618


Inorganic QC

Summary


Fluoride SM4500F-C


WG367107

WG3671 07ICV 07/07/1 4 1 3:51 98IC V WC 1 40707- 1 .96 95 1 05mg/L2

WG3671 07ICB 07/07/1 4 1 3:56IC B .069 -0.1 5 0.1 5mg/L

WG3671 07PQV 07/07/1 4 1 4:00 87.7PQV WC 1 40707- .22 70 1 30mg/L.25075

WG3671 07LFB1 07/07/1 4 1 4:04 96.2LFB WC 1 40501 - 4.823 90 1 1 0mg/L5.01 5

L1 901 4-01 AS M207/07/1 4 1 4:1 2 .66 89.5AS WC 1 40501 - 5.1 49 90 1 1 0mg/L5.01 5

L1 901 4-01 DUP 07/07/1 4 1 4:1 7 .66DUP .591 1 1mg/L 20

WG3671 07C CV1 07/07/1 4 1 4:55 99.8C CV WC 1 40707- 1 .996 90 1 1 0mg/L2

WG3671 07C CB1 07/07/1 4 1 4:59C CB U -0.1 5 0.1 5mg/L

WG3671 07C CV2 07/07/1 4 1 5:51 1 02.1C CV WC 1 40707- 2.042 90 1 1 0mg/L2

WG3671 07C CB2 07/07/1 4 1 5:56C CB U -0.1 5 0.1 5mg/L

WG3671 07LFB2 07/07/1 4 1 6:1 8 97.5LFB WC 1 40501 - 4.888 90 1 1 0mg/L5.01 5

WG3671 07C CV3 07/07/1 4 1 6:42 1 04C CV WC 1 40707- 2.079 90 1 1 0mg/L2

WG3671 07C CB3 07/07/1 4 1 6:46C CB U -0.1 5 0.1 5mg/L

WG3671 07C CV4 07/07/1 4 1 7:39 1 02.1C CV WC 1 40707- 2.042 90 1 1 0mg/L2

WG3671 07C CB4 07/07/1 4 1 7:42C CB U -0.1 5 0.1 5mg/L

WG3671 07C CV5 07/07/1 4 1 8:52 1 00.3C CV WC 1 40707- 2.005 90 1 1 0mg/L2

WG3671 07C CB5 07/07/1 4 1 8:57C CB U -0.1 5 0.1 5mg/L

WG3671 07C CV6 07/07/1 4 1 9:1 5 1 05.9C CV WC 1 40707- 2.1 1 7 90 1 1 0mg/L2

WG3671 07C CB6 07/07/1 4 1 9:23C CB U -0.1 5 0.1 5mg/L



WG366352

WG366352ICV 06/23/1 4 23:26 98.6IC V II1 4051 2-2 1 .972 95 1 05mg/L2

WG366352ICB 06/23/1 4 23:32IC B U -0.06 0.06mg/L

WG366352PQV 06/23/1 4 23:35 99.9PQV II1 40609-2 .05 70 1 30mg/L.05007

WG366352SIC 06/23/1 4 23:39 95.4SIC II1 40602-1 1 91 .1 1 200mg/L200.33007

WG366352LFB 06/23/1 4 23:45 1 03LFB II1 4061 1 -2 1 .031 85 1 1 5mg/L1 .001 4

L1 901 4-01 AS 06/24/1 4 0:00 1 .02 95.9AS II1 4061 1 -2 1 .98 85 1 1 5mg/L1 .001 4

L1 901 4-01 ASD 06/24/1 4 0:03 1 .02 97.1ASD II1 4061 1 -2 1 .992 0.685 1 1 5mg/L 201 .001 4

WG366352CCV1 06/24/1 4 0:1 6 99C CV II1 40506-1 .99 90 1 1 0mg/L1

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.06 0.06mg/L

WG366352CCV2 06/24/1 4 0:54 98C CV II1 40506-1 .98 90 1 1 0mg/L1

WG366352CCB2 06/24/1 4 0:57C CB U -0.06 0.06mg/L

WG366352CCV3 06/24/1 4 1 :1 6 98.7C CV II1 40506-1 .987 90 1 1 0mg/L1

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.06 0.06mg/L

Page 11 of 28L19014-1407111618


Inorganic QC

Summary




WG367132

WG3671 32ICV 07/07/1 4 21 :38 1 00.7IC V MS1 4051 3-1 .05037 90 1 1 0mg/L.05

WG3671 32ICB 07/07/1 4 21 :41IC B U -0.0003 0.0003mg/L

WG3671 32LFB 07/07/1 4 21 :45 98.9LFB MS1 40625-3 .04952 85 1 1 5mg/L.05005

L1 91 1 7-02AS 07/07/1 4 21 :58 U 1 00.2AS MS1 40625-3 .0501 4 70 1 30mg/L.05005

L1 91 1 7-02ASD 07/07/1 4 22:01 U 1 00.5ASD MS1 40625-3 .05028 0.2870 1 30mg/L 20.05005

WG3671 32C CV1 07/07/1 4 22:1 4 1 01 .5C CV MS1 4051 3-2 .2541 90 1 1 0mg/L.25025

WG3671 32C CB1 07/07/1 4 22:1 7C CB U -0.0003 0.0003mg/L

WG3671 32C CV2 07/07/1 4 22:53 1 01 .8C CV MS1 4051 3-2 .2547 90 1 1 0mg/L.25025

WG3671 32C CB2 07/07/1 4 22:56C CB U -0.0003 0.0003mg/L

WG3671 32C CV3 07/07/1 4 23:1 9 1 00.9C CV MS1 4051 3-2 .2524 90 1 1 0mg/L.25025

WG3671 32C CB3 07/07/1 4 23:22C CB U -0.0003 0.0003mg/L



WG366352

WG366352ICV 06/23/1 4 23:26 97IC V II1 4051 2-2 97.04 95 1 05mg/L1 00

WG366352ICB 06/23/1 4 23:32IC B U -0.6 0.6mg/L

WG366352PQV 06/23/1 4 23:35 98.9PQV II1 40609-2 .99 70 1 30mg/L1 .0007

WG366352SIC 06/23/1 4 23:39 1 00.2SIC II1 40602-1 201 .6 1 200mg/L201 .1 407

WG366352LFB 06/23/1 4 23:45 1 00.6LFB II1 4061 1 -2 50.28 85 1 1 5mg/L50.001 31

L1 901 4-01 AS 06/24/1 4 0:00 21 2 84.6AS II1 4061 1 -2 254.3 85 1 1 5mg/L50.001 31

L1 901 4-01 ASD 06/24/1 4 0:03 21 2 87ASD II1 4061 1 -2 255.5 0.4785 1 1 5mg/L 2050.001 31

WG366352CCV1 06/24/1 4 0:1 6 94.7C CV II1 40506-1 47.34 90 1 1 0mg/L50

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.6 0.6mg/L

WG366352CCV2 06/24/1 4 0:54 94.8C CV II1 40506-1 47.42 90 1 1 0mg/L50

WG366352CCB2 06/24/1 4 0:57C CB U -0.6 0.6mg/L

WG366352CCV3 06/24/1 4 1 :1 6 96C CV II1 40506-1 48.02 90 1 1 0mg/L50

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.6 0.6mg/L



WG366352

WG366352ICV 06/23/1 4 23:26 98.8IC V II1 4051 2-2 1 .9762 95 1 05mg/L2

WG366352ICB 06/23/1 4 23:32IC B U -0.01 5 0.01 5mg/L

WG366352PQV 06/23/1 4 23:35 82.8PQV II1 40609-2 .0207 70 1 30mg/L.025

WG366352SIC 06/23/1 4 23:39 98.6SIC II1 40602-1 49.44 1 200mg/L50.1 25

WG366352LFB 06/23/1 4 23:45 1 02.1LFB II1 4061 1 -2 .51 1 6 85 1 1 5mg/L.501

L1 901 4-01 AS 06/24/1 4 0:00 .373 98.6AS II1 4061 1 -2 .8669 85 1 1 5mg/L.501

L1 901 4-01 ASD 06/24/1 4 0:03 .373 98.5ASD II1 4061 1 -2 .8666 0.0385 1 1 5mg/L 20.501

WG366352CCV1 06/24/1 4 0:1 6 99.6C CV II1 40506-1 .9956 90 1 1 0mg/L1

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.01 5 0.01 5mg/L

WG366352CCV2 06/24/1 4 0:54 98.9C CV II1 40506-1 .9889 90 1 1 0mg/L1

WG366352CCB2 06/24/1 4 0:57C CB U -0.01 5 0.01 5mg/L

WG366352CCV3 06/24/1 4 1 :1 6 99.9C CV II1 40506-1 .9993 90 1 1 0mg/L1

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.01 5 0.01 5mg/L

Page 12 of 28L19014-1407111618


Inorganic QC

Summary


Mercury, dissolved M245.1 C VAA


WG366461

WG366461 IC V 06/25/1 4 1 2:56 97.3IC V II1 4061 6-2 .00487 95 1 05mg/L.005005

WG366461 IC B 06/25/1 4 1 2:58IC B U -0.0002 0.0002mg/L

WG366461 LRB 06/25/1 4 1 3:00LRB U -0.00044 0.00044mg/L

WG366461 LFB 06/25/1 4 1 3:02 88.4LFB II1 4061 6-4 .001 77 85 1 1 5mg/L.002002

WG366461 C CV1 06/25/1 4 1 3:22 97.5C CV II1 4061 6-2 .00488 90 1 1 0mg/L.005005

WG366461 C CB1 06/25/1 4 1 3:24C CB U -0.0002 0.0002mg/L

L1 9020-02LFM MA06/25/1 4 1 3:48 U 84.4LFM II1 4061 6-4 .001 69 85 1 1 5mg/L.002002

WG366461 C CV2 06/25/1 4 1 3:50 98.9C CV II1 4061 6-2 .00495 90 1 1 0mg/L.005005

WG366461 C CB2 06/25/1 4 1 3:53C CB U -0.0002 0.0002mg/L

L1 9020-02LFMD 06/25/1 4 1 3:55 U 94.4LFMD II1 4061 6-4 .001 89 1 1 .1 785 1 1 5mg/L 20.002002

WG366461 C CV3 06/25/1 4 1 4:09 98.7C CV II1 4061 6-2 .00494 90 1 1 0mg/L.005005

WG366461 C CB3 06/25/1 4 1 4:1 1C CB U -0.0002 0.0002mg/L



WG366352

WG366352ICV 06/23/1 4 23:26 1 00.7IC V II1 4051 2-2 2.01 3 95 1 05mg/L2

WG366352ICB 06/23/1 4 23:32IC B U -0.06 0.06mg/L

WG366352PQV 06/23/1 4 23:35 1 02PQV II1 40609-2 .1 02 70 1 30mg/L.1

WG366352SIC 06/23/1 4 23:39 88SIC II1 40602-1 .088 80 1 20mg/L.1

WG366352LFB 06/23/1 4 23:45 1 03.9LFB II1 4061 1 -2 .51 9 85 1 1 5mg/L.4995

L1 901 4-01 AS 06/24/1 4 0:00 U 1 05.1AS II1 4061 1 -2 .525 85 1 1 5mg/L.4995

L1 901 4-01 ASD 06/24/1 4 0:03 U 1 03.9ASD II1 4061 1 -2 .51 9 1 .1 585 1 1 5mg/L 20.4995

WG366352CCV1 06/24/1 4 0:1 6 99.8C CV II1 40506-1 .998 90 1 1 0mg/L1

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.06 0.06mg/L

WG366352CCV2 06/24/1 4 0:54 1 00C CV II1 40506-1 1 90 1 1 0mg/L1

WG366352CCB2 06/24/1 4 0:57C CB U -0.06 0.06mg/L

WG366352CCV3 06/24/1 4 1 :1 6 1 00.8C CV II1 40506-1 1 .008 90 1 1 0mg/L1

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.06 0.06mg/L



WG366352

WG366352ICV 06/23/1 4 23:26 99.1IC V II1 4051 2-2 1 .981 2 95 1 05mg/L2

WG366352ICB 06/23/1 4 23:32IC B U -0.024 0.024mg/L

WG366352PQV 06/23/1 4 23:35 1 00.5PQV II1 40609-2 .0402 70 1 30mg/L.04

WG366352SIC 06/23/1 4 23:39 1 03.6SIC II1 40602-1 .1 036 80 1 20mg/L.1

WG366352LFB 06/23/1 4 23:45 1 02.5LFB II1 4061 1 -2 .51 27 85 1 1 5mg/L.5

L1 901 4-01 AS 06/24/1 4 0:00 U 99.8AS II1 4061 1 -2 .4992 85 1 1 5mg/L.5

L1 901 4-01 ASD 06/24/1 4 0:03 U 1 00.4ASD II1 4061 1 -2 .501 9 0.5485 1 1 5mg/L 20.5

WG366352CCV1 06/24/1 4 0:1 6 97.1C CV II1 40506-1 .971 2 90 1 1 0mg/L1

WG366352CCB1 06/24/1 4 0:1 9C CB U -0.024 0.024mg/L

WG366352CCV2 06/24/1 4 0:54 96.7C CV II1 40506-1 .9671 90 1 1 0mg/L1

WG366352CCB2 06/24/1 4 0:57C CB U -0.024 0.024mg/L

WG366352CCV3 06/24/1 4 1 :1 6 98.1C CV II1 40506-1 .981 90 1 1 0mg/L1

WG366352CCB3 06/24/1 4 1 :1 9C CB U -0.024 0.024mg/L

Page 13 of 28L19014-1407111618


Inorganic QC

Summary




WG367215

WG367215ICV 07/08/14 22:09 97.7ICV WI140417-3 2.361 90 110mg/L2.416

WG367215ICB 07/08/14 22:11ICB U -0.06 0.06mg/L

WG367219

WG367219CCV1 07/09/14 0:04 99.5CCV WI140703-1 1.989 90 110mg/L2

WG367219CCB1 07/09/14 0:05CCB U -0.06 0.06mg/L

WG367219LFB1 07/09/14 0:06 97.7LFB WI140215-3 1.953 90 110mg/L2

L19014-01AS 07/09/14 0:09 U 96.8AS WI140215-3 1.936 90 110mg/L2

L19111-02DUP RA07/09/14 0:11 UDUP U 0mg/L 20

WG367219CCV2 07/09/14 0:18 100.2CCV WI140703-1 2.003 90 110mg/L2

WG367219CCB2 07/09/14 0:19CCB U -0.06 0.06mg/L

WG367219CCV3 07/09/14 0:32 99.7CCV WI140703-1 1.994 90 110mg/L2

WG367219CCB3 07/09/14 0:33CCB U -0.06 0.06mg/L

WG367219LFB2 07/09/14 0:40 99.7LFB WI140215-3 1.993 90 110mg/L2

WG367219CCV4 07/09/14 0:46 97.9CCV WI140703-1 1.958 90 110mg/L2

WG367219CCB4 07/09/14 0:47CCB U -0.06 0.06mg/L

WG367219CCV5 07/09/14 0:54 98.1CCV WI140703-1 1.962 90 110mg/L2

WG367219CCB5 07/09/14 0:55CCB U -0.06 0.06mg/L

WG367219CCV6 07/09/14 1:11 97.5CCV WI140703-1 1.949 90 110mg/L2

WG367219CCB6 07/09/14 1:12CCB U -0.06 0.06mg/L

WG367219CCV7 07/09/14 1:20 97.9CCV WI140703-1 1.958 90 110mg/L2

WG367219CCB7 07/09/14 1:21CCB U -0.06 0.06mg/L



WG366944

WG366944ICV 07/02/14 12:03 102.2ICV WI131021-1 1.025 90 110mg/L1.003

WG366944ICB 07/02/14 12:06ICB U -0.15 0.15mg/L

WG366993

WG366993CCV1 07/02/14 16:50 103.4CCV WI140113-6 2.068 90 110mg/L2

WG366993CCB1 07/02/14 16:51CCB U -0.15 0.15mg/L

WG366993LFB1 07/02/14 16:52 97.7LFB WI140113-8 .977 90 110mg/L1

L19014-01AS 07/02/14 16:54 .05 98.2AS WI140113-8 1.032 90 110mg/L1

L19107-01DUP RA07/02/14 16:57 UDUP U 0mg/L 20

WG366993CCV2 07/02/14 17:03 104.8CCV WI140113-6 2.095 90 110mg/L2

WG366993CCB2 07/02/14 17:04CCB U -0.15 0.15mg/L

WG366993CCV3 07/02/14 17:16 105.5CCV WI140113-6 2.11 90 110mg/L2

WG366993CCB3 07/02/14 17:17CCB U -0.15 0.15mg/L

WG366993LFB2 07/02/14 17:24 95.3LFB WI140113-8 .953 90 110mg/L1

WG366993CCV4 07/02/14 17:29 104.4CCV WI140113-6 2.087 90 110mg/L2

WG366993CCB4 07/02/14 17:30CCB U -0.15 0.15mg/L

WG366993CCV5 07/02/14 17:42 101.4CCV WI140113-6 2.027 90 110mg/L2

WG366993CCB5 07/02/14 17:43CCB U -0.15 0.15mg/L

WG366993CCV6 07/02/14 17:49 102.7CCV WI140113-6 2.054 90 110mg/L2

WG366993CCB6 07/02/14 17:50CCB U -0.15 0.15mg/L

Page 14 of 28L19014-1407111618


Inorganic QC

Summary




WG366352

WG366352ICV 06/23/14 23:26 98.8ICV II140512-2 19.75 95 105mg/L20

WG366352ICB 06/23/14 23:32ICB U -0.6 0.6mg/L

WG366352PQV 06/23/14 23:35 111PQV II140609-2 1.11 70 130mg/L1

WG366352SIC 06/23/14 23:39 107SIC II140602-1 1.07 80 120mg/L1

WG366352LFB 06/23/14 23:45 102LFB II140611-2 102 85 115mg/L99.99364

L19014-01AS 06/24/14 0:00 19.2 106.4AS II140611-2 125.6 85 115mg/L99.99364

L19014-01ASD 06/24/14 0:03 19.2 105.9ASD II140611-2 125.1 0.485 115mg/L 2099.99364

WG366352CCV1 06/24/14 0:16 100.1CCV II140506-1 10.01 90 110mg/L10

WG366352CCB1 06/24/14 0:19CCB U -0.6 0.6mg/L

WG366352CCV2 06/24/14 0:54 99.6CCV II140506-1 9.96 90 110mg/L10

WG366352CCB2 06/24/14 0:57CCB U -0.6 0.6mg/L

WG366352CCV3 06/24/14 1:16 99.3CCV II140506-1 9.93 90 110mg/L10

WG366352CCB3 06/24/14 1:19CCB U -0.6 0.6mg/L



WG366287

WG366287PBW 06/20/14 16:25PBW U -20 20mg/L


L19014-01DUP 06/20/14 17:09 1930DUP 1950 1mg/L 10



WG366357

WG366357PBW 06/23/14 13:31PBW U -15 15mg/L


L18973-04DUP RA06/23/14 14:16 UDUP U 0mg/L 10



WG367132

WG367132ICV 07/07/14 21:38 103.4ICV MS140513-1 .05171 90 110mg/L.05

WG367132ICB 07/07/14 21:41ICB U -0.0003 0.0003mg/L

WG367132LFB 07/07/14 21:45 101LFB MS140625-3 .05053 85 115mg/L.05005

L19117-02AS 07/07/14 21:58 .0002 116.1AS MS140625-3 .05829 70 130mg/L.05005

L19117-02ASD 07/07/14 22:01 .0002 114.8ASD MS140625-3 .05768 1.0570 130mg/L 20.05005

WG367132CCV1 07/07/14 22:14 101.5CCV MS140513-2 .254 90 110mg/L.25025

WG367132CCB1 07/07/14 22:17CCB U -0.0003 0.0003mg/L

WG367132CCV2 07/07/14 22:53 99.5CCV MS140513-2 .2489 90 110mg/L.25025

WG367132CCB2 07/07/14 22:56CCB U -0.0003 0.0003mg/L

WG367132CCV3 07/07/14 23:19 101.5CCV MS140513-2 .254 90 110mg/L.25025

WG367132CCB3 07/07/14 23:22CCB U -0.0003 0.0003mg/L

Page 15 of 28L19014-1407111618


Inorganic QC

Summary




WG366352

WG366352ICV 06/23/14 23:26 99.8ICV II140512-2 42.7 95 105mg/L42.8

WG366352ICB 06/23/14 23:32ICB U -0.6 0.6mg/L

WG366352PQV 06/23/14 23:35 96.1PQV II140609-2 1.03 70 130mg/L1.0714

WG366352SIC 06/23/14 23:39 86.8SIC II140602-1 .93 80 120mg/L1.0714

WG366352LFB 06/23/14 23:45 105.5LFB II140611-2 22.6 85 115mg/L21.428

L19014-01AS 06/24/14 0:00 15.5 104.6AS II140611-2 37.92 85 115mg/L21.428

L19014-01ASD 06/24/14 0:03 15.5 105.3ASD II140611-2 38.06 0.3785 115mg/L 2021.428

WG366352CCV1 06/24/14 0:16 98.8CCV II140506-1 21.15 90 110mg/L21.4

WG366352CCB1 06/24/14 0:19CCB U -0.6 0.6mg/L

WG366352CCV2 06/24/14 0:54 99.2CCV II140506-1 21.22 90 110mg/L21.4

WG366352CCB2 06/24/14 0:57CCB U -0.6 0.6mg/L

WG366352CCV3 06/24/14 1:16 99.7CCV II140506-1 21.34 90 110mg/L21.4

WG366352CCB3 06/24/14 1:19CCB U -0.6 0.6mg/L



WG366352

WG366352ICV 06/23/14 23:26 98.9ICV II140512-2 98.92 95 105mg/L100

WG366352ICB 06/23/14 23:32ICB U -0.6 0.6mg/L

WG366352PQV 06/23/14 23:35 102.9PQV II140609-2 1.03 70 130mg/L1.001

WG366352SIC 06/23/14 23:39 105.9SIC II140602-1 1.06 80 120mg/L1.001

WG366352LFB 06/23/14 23:45 102.4LFB II140611-2 102.4 85 115mg/L100.0393

L19014-01AS 06/24/14 0:00 23.2 106.2AS II140611-2 129.4 85 115mg/L100.0393

L19014-01ASD 06/24/14 0:03 23.2 106.1ASD II140611-2 129.3 0.0885 115mg/L 20100.0393

WG366352CCV1 06/24/14 0:16 99.4CCV II140506-1 49.69 90 110mg/L50

WG366352CCB1 06/24/14 0:19CCB U -0.6 0.6mg/L

WG366352CCV2 06/24/14 0:54 99.2CCV II140506-1 49.6 90 110mg/L50

WG366352CCB2 06/24/14 0:57CCB U -0.6 0.6mg/L

WG366352CCV3 06/24/14 1:16 98.7CCV II140506-1 49.36 90 110mg/L50

WG366352CCB3 06/24/14 1:19CCB U -0.6 0.6mg/L



WG366916

WG366916PBW 07/02/14 15:35PBW U -30 30mg/L


L19150-05DUP RA07/02/14 15:55 60DUP 48 22.2mg/L 20

Page 16 of 28L19014-1407111618


Inorganic QC

Summary




WG366363

WG366363ICV 06/23/14 15:35 101.5ICV WC140623- .356 90 110mg/L.35066

WG366363ICB 06/23/14 15:37ICB U -0.06 0.06mg/L

WG366363LFB 06/23/14 15:39 97.3LFB WC140623- .257 80 120mg/L.264

WG366363CCV1 06/23/14 16:04 103.5CCV WC140623- .205 90 110mg/L.198

WG366363CCB1 06/23/14 16:07CCB U -0.06 0.06mg/L

L18991-04AS 06/23/14 16:24 18.5 96.9AS WC140623- 28.09 75 125mg/L9.9

L18991-04DUP 06/23/14 16:26 18.5DUP 18.83 1.8mg/L 20

WG366363CCV2 06/23/14 16:34 101.5CCV WC140623- .201 90 110mg/L.198

WG366363CCB2 06/23/14 16:36CCB U -0.06 0.06mg/L

WG366363CCV3 06/23/14 16:51 100CCV WC140623- .198 90 110mg/L.198

WG366363CCB3 06/23/14 16:53CCB U -0.06 0.06mg/L



WG367132

WG367132ICV 07/07/14 21:38 103.4ICV MS140513-1 .05172 90 110mg/L.05

WG367132ICB 07/07/14 21:41ICB U -0.0003 0.0003mg/L

WG367132LFB 07/07/14 21:45 103LFB MS140625-3 .05154 85 115mg/L.05005

L19117-02AS 07/07/14 21:58 .0013 104.8AS MS140625-3 .05377 70 130mg/L.05005

L19117-02ASD 07/07/14 22:01 .0013 105.7ASD MS140625-3 .0542 0.870 130mg/L 20.05005

WG367132CCV1 07/07/14 22:14 101.7CCV MS140513-2 .1017 90 110mg/L.1

WG367132CCB1 07/07/14 22:17CCB U -0.0003 0.0003mg/L

WG367132CCV2 07/07/14 22:53 101.9CCV MS140513-2 .1019 90 110mg/L.1

WG367132CCB2 07/07/14 22:56CCB U -0.0003 0.0003mg/L

WG367132CCV3 07/07/14 23:19 103.5CCV MS140513-2 .1035 90 110mg/L.1

WG367132CCB3 07/07/14 23:22CCB U -0.0003 0.0003mg/L



WG366352

WG366352ICV 06/23/14 23:26 99.9ICV II140512-2 1.9972 95 105mg/L2

WG366352ICB 06/23/14 23:32ICB U -0.015 0.015mg/L

WG366352PQV 06/23/14 23:35 93.6PQV II140609-2 .0234 70 130mg/L.025

WG366352SIC 06/23/14 23:39 96.3SIC II140602-1 .0963 80 120mg/L.1

WG366352LFB 06/23/14 23:45 104.4LFB II140611-2 .522 85 115mg/L.5

L19014-01AS 06/24/14 0:00 U 105.2AS II140611-2 .5262 85 115mg/L.5

L19014-01ASD 06/24/14 0:03 U 104.3ASD II140611-2 .5214 0.9285 115mg/L 20.5

WG366352CCV1 06/24/14 0:16 100.1CCV II140506-1 1.001 90 110mg/L1

WG366352CCB1 06/24/14 0:19CCB U -0.015 0.015mg/L

WG366352CCV2 06/24/14 0:54 99.9CCV II140506-1 .9993 90 110mg/L1

WG366352CCB2 06/24/14 0:57CCB U -0.015 0.015mg/L

WG366352CCV3 06/24/14 1:16 100.4CCV II140506-1 1.004 90 110mg/L1

WG366352CCB3 06/24/14 1:19CCB U -0.015 0.015mg/L

Page 17 of 28L19014-1407111618


Inorganic QC

Summary




WG366352

WG366352ICV 06/23/14 23:26 97.3ICV II140512-2 1.946 95 105mg/L2

WG366352ICB 06/23/14 23:32ICB U -0.03 0.03mg/L

WG366352PQV 06/23/14 23:35 100PQV II140609-2 .05 70 130mg/L.05

WG366352SIC 06/23/14 23:39 96SIC II140602-1 .096 80 120mg/L.1

WG366352LFB 06/23/14 23:45 104.7LFB II140611-2 .524 85 115mg/L.5005

L19014-01AS 06/24/14 0:00 U 102.1AS II140611-2 .511 85 115mg/L.5005

L19014-01ASD 06/24/14 0:03 U 102.1ASD II140611-2 .511 085 115mg/L 20.5005

WG366352CCV1 06/24/14 0:16 96.6CCV II140506-1 .966 90 110mg/L1

WG366352CCB1 06/24/14 0:19CCB U -0.03 0.03mg/L

WG366352CCV2 06/24/14 0:54 96.5CCV II140506-1 .965 90 110mg/L1

WG366352CCB2 06/24/14 0:57CCB U -0.03 0.03mg/L

WG366352CCV3 06/24/14 1:16 98.4CCV II140506-1 .984 90 110mg/L1

WG366352CCB3 06/24/14 1:19CCB U -0.03 0.03mg/L

Page 18 of 28L19014-1407111618


Inorganic Extended

Qualifier Report



MA Recovery for either the spike or spike duplicate was outside of the acceptance limits; the RPD was within the acceptance limits.

M200.7 ICPAluminum, dissolvedL19014-01 WG366352

MA Recovery for either the spike or spike duplicate was outside of the acceptance limits; the RPD was within the acceptance limits.

M245.1 CVAAMercury, dissolvedWG366461



DF Sample required dilution due to high sediment.SM5310BCarbon, total organic (TOC)WG3669 37


SM5310B






SM2320B - TitrationHydroxide as CaCO3WG366660




M350.1 - Automated PhenateNitrogen, ammoniaWG3669 9 3


SM2540DResidue, Non-Filterable (TSS) @ 105CWG366357


SM4500 SO4-DSulfateWG3669 16

DD Sample required dilution due to matrix color or odor.SM4500S2-DSulfide as SWG366363

DF Sample required dilution due to high sediment.SM4500S2-D


SM4500S2-D

ZW Method deviation. The sample was centrifuged prior to

analysis due to high solid content.


REPAD.15.06.05.01

Page 19 of 28L19014-1407111618


Sample ID: MW8



Project ID:


Date Sampled: 06/16/14 12:40


Locator:

RadioChemistry

Analytical Results


M9 00.0

Prep Method:


Gross Alpha -4.1 6.4 9 .8 pCi/L * bsg07/03/14 0:15

Gross Beta 26 13 18 pCi/L bsg07/03/14 0:15

Lead 210, dissolved

EICHROM, OTW01

Prep Method:




M9 03.1

Prep Method:




M9 04.0

Prep Method:


Radium 228, dissolved 2.6 0.89 0.77 pCi/L jrd07/07/14 19 :31


ESM 4506

Prep Method:


Thorium 230, dissolved -0.19 0.36 0.61 pCi/L * nco07/09 /14 15:31


Page 20 of 28L19014-1407111618



Batch A dis tin ct s et of s amples an aly zed at a s pecif ic time

Error(+/-) Calcu lated s ample s pecif ic u n certain ty

Found V alu e of th e QC T y pe of in teres t

Limit U pper limit f or RPD, in % .

LCL L ower Con trol L imit, in % (except f or L CSS, mg / Kg )

LLD Calcu lated s ample s pecif ic L ower L imit of Detection

P CN/SCN A n u mb er as s ig n ed to reag en ts / s tan dards to trace to th e man u f actu rer's certif icate of an aly s is

P QL Practical Qu an titation L imit

QC T ru e V alu e of th e Con trol Sample or th e amou n t added to th e Spik e

Rec Amou n t of th e tru e valu e or s pik e added recovered, in % (except f or L CSS, mg / Kg )

RER Relative E rror Ratio, calcu lation u s ed f or Du p. QC tak in g in to accou n t th e error f actor.

RP D Relative Percen t Dif f eren ce, calcu lation u s ed f or Du plicate QC T y pes

UCL U pper Con trol L imit, in % (except f or L CSS, mg / Kg )

Sample V alu e of th e Sample of in teres t

QC Sample Types

DUP Sample Du plicate MS/MSD Matrix Spik e/ Matrix Spik e Du plicate

LCSS L ab oratory Con trol Sample - Soil P BS Prep B lan k - Soil

LCSW L ab oratory Con trol Sample - Water P BW Prep B lan k - Water


B lan k s V erif ies th at th ere is n o or min imal con tamin ation in th e prep meth od procedu re.

Con trol Samples V erif ies th e accu racy of th e meth od, in clu din g th e prep procedu re.

Du plicates V erif ies th e precis ion of th e in s tru men t an d/ or meth od.

Matrix Spik es Determin es s ample matrix in terf eren ces , if an y .


H An aly s is exceeded meth od h old time.


M E PA meth odolog y , in clu din g th os e u n der SDWA, CWA, an d RCRA

SM Stan dard Meth ods f or th e E xamin ation of Water an d Was tewater.

D AST M

RP DO E

E SM DO E / E SM

Comments

(1) Solid matrices are reported on a dry weig h t b as is .

(2) Preparation meth od: "Meth od" in dicates preparation def in ed in an aly tical meth od.

(3) QC res u lts calcu lated f rom raw data. Res u lts may vary s lig h tly if th e rou n ded valu es are u s ed in th e calcu lation s .

(4) An as teris k in th e "XQ" colu mn in dicates th ere is an exten ded q u alif ier an d/or certif ication

q u alif ier as s ociated with th e res u lt.

F or a complete lis t of ACZ's E xten ded Qu alif iers , pleas e click : h ttp://www.acz.com/pu b lic/extq u allis t.pdf

RE P003.09.12.01

Radiochemistry

Reference

Page 21 of 28L19014-1407111618


Radiochemistry QC

Summary


Alpha M9 00.0


pCi/L

Error LLDLLD

Units:

WG367075

WG366811PBW 07/03/14PBW .79 3.61.7 1.8

WG366811LCSWA 07/03/14 130LCSW PCN45450 130100 83 13311 1.8

L189 63-07DUP N107/03/14 43DUP-RER 6.1 28 2.4213 8.16.6

L19 033-07DUP 07/03/14 1.1DUP-RER -1.1 22.5 0.632.4 2.92.5

L19 033-08MSA M207/03/14 0.49 65.5MS PCN45450 66100 83 133102.2 2.92.4

Beta M9 00.0


pCi/L

Error LLDLLD

Units:

WG367075

WG366811PBW 07/03/14PBW .17 10.23.6 5.1

WG366811LCSWB 07/03/14 9 6LCSW PCN44650 9 6100 70 1297.3 4.9

L189 63-07DUP 07/03/14 6.6DUP-RER 4.8 210 0.139 .4 1413

L19 033-07DUP 07/03/14 4.7DUP-RER 7.9 24.6 0.524.1 5.95.4

L19 070-01MSB 07/03/14 2.7 117.3MS PCN44650 120100 70 1299 .33.6 65.3



pCi/L

Error LLDLLD

Units:

WG366950

WG366408LCSW 07/01/14 67.4LCSW PCN44122 669 7.89 55 1213.2 6.5

WG366408PBW 07/01/14PBW -14 14.81.9 7.4

L19 028-05MS 07/01/14 -9 .6 84.4MS PCN44122 739 7.89 55 12142.1 9 .27.7

L19 028-01DUP 07/01/14 21DUP-RER 26 22.5 1.392.6 6.27

L19 028-04DUP 07/01/14 -8DUP-RER -7.4 22 0.212 77.2

Page 22 of 28L19014-1407111618


Radiochemistry QC

Summary


Radium 226, dissolved M9 03.1


pCi/L

Error LLDLLD

Units:

WG367039

WG366581PBW 07/02/14PBW .1 0.340.08 0.17

WG366581LCSW 07/02/14 60LCSW PCN45815 1220 43 1480.41 0.17

L19 014-01DUP 07/02/14 0.71DUP-RER .54 20.11 10.13 0.210.19

L19 039 -01DUP 07/02/14 3.1DUP-RER 2.8 20.24 0.870.25 0.270.21

L19 039 -02MS 07/02/14 0.81 106MS PCN45815 2220 43 1480.610.14 0.190.18

Radium 228, dissolved M9 04.0


pCi/L

Error LLDLLD

Units:

WG367208

WG3669 70LCSW 07/07/14 119 .3LCSW PCN44321 2218.44 47 1231.9 0.87

WG3669 70PBW 07/07/14PBW .28 0.60.3 0.3

L189 40-02DUP 07/08/14 0.21DUP-RER .4 20.79 0.180.72 0.820.76

L19 014-01MS 07/08/14 2.6 56.4MS PCN44321 1318.44 47 1231.40.89 0.770.77

L19 028-10DUP 07/08/14 0.74DUP-RER .82 20.76 0.070.77 0.750.77



pCi/L

Error LLDLLD

Units:

WG367377

WG36679 9 PBW 07/09 /14PBW .41 1.060.3 0.53

WG36679 9 LCSW 07/09 /14 104.9LCSW RC130807-2 170162.12 9 1 1264.6 0.62

L18871-02DUP 07/09 /14 0.24DUP-RER .38 20.56 0.220.29 0.520.55

L19 014-01DUP 07/09 /14 -0.19DUP-RER .09 20.9 8 0.270.36 0.540.61

L18871-03MS 07/09 /14 0.14 104.8MS RC130807-2 170162.12 9 1 1264.50.31 0.610.57

Page 23 of 28L19014-1407111618


RadChem Extended

Qualifier Report




M9 00.0Gross AlphaL19014-01 WG367075

N1 See Case Narrative.M9 00.0

REPAD.15.06.05.01

Page 24 of 28L19014-1407111618


Certification

Qualifiers


Metals Analysis



Radiochemistry




Wet Chemistry



REPAD.05.06.05.01

Page 25 of 28L19014-1407111618


Sample

Receipt


Date Received:

Received By: ear

06/20/2014 10:17

L19 014




NANOYES

X

X

X

X

X

X









NANOYES

X

X

X

X

X

X

X


9 ) Are all labels on containers and are they intact and legible?










Samples/Containers

X

X

X

Shipping Containers



Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- --------------------2225 0.4 15 Yes

X



REPAD LPII 2012-03

Page 26 of 28L19014-1407111618

of 28L19014-1407111618


Analytical

Report



Lakewood, CO 80228

ACZ Project ID: L19 275

Kathy Weinel:

Enclosed are the analytical results for sample(s) submitted to ACZ Laboratories, Inc. (ACZ) on J uly 08, 2014. This project has been assigned to ACZ' s project number, L19 275. Please reference this number in all future inquiries.

All analyses were performed according to ACZ' s Quality Assurance Plan. The enclosed results relate only to the samples received under L19 275. Each section of this report has been reviewed and approved by the appropriate Laboratory Supervisor, or a qualified substitute.

Except as noted, the test results for the methods and parameters listed on ACZ' s current NELAC certificate letter (#ACZ) meet all requirements of NELAC.


All samples and sub-samples associated with this project will be disposed of after August 29 , 2014. If the samples are determined to be hazardous, additional charges apply for disposal (typically $11/sample). If you would like the samples to be held longer than ACZ' s stated policy or to be returned, please contact your Project Manager or Customer Service Representative for further details and associated costs. ACZ retains analytical raw data reports for ten years.


Kathy Weinel

J uly 30, 2014

Project ID:



Lakewood, CO 80228

Accounts Payable

Report to: Bill to:

Page 1 of 27L19275-1407301413


Sample ID: DAVIS WELL



Project ID:



Results

Date Sampled: 07/03/14 10:30



Metals Analys is

XQDilution

Aluminum, dis s olved M200.7 ICP mg /L 0.2U jjc0.03 07 /10/14 17 :081

Ars enic, dis s olved M200.8 ICP-MS 0.0015 mg /L 0.001 las0.0002 07 /25/14 16 :451

Barium, dis s olved M200.7 ICP 0.034 mg /L 0.02 jjc0.003 07 /10/14 17 :081

Boron, dis s olved M200.7 ICP 0.50 mg /L 0.05 jjc0.01 07 /10/14 17 :081

Cadmium, dis s olved M200.8 ICP-MS mg /L 0.0005U las0.0001 07 /25/14 16 :451

Calcium, dis s olved M200.7 ICP 41.3 mg /L 0.5 jjc0.1* 07 /10/14 17 :081

Ces ium, dis s olved M200.8 ICP-MS mg /L 0.001U las0.0002* 07 /25/14 16 :451

Chromium, dis s olved M200.7 ICP mg /L 0.05U jjc0.01 07 /10/14 17 :081

Copper, dis s olved M200.7 ICP mg /L 0.05U jjc0.01 07 /10/14 17 :081

Iron, dis s olved M200.7 ICP mg /L 0.05U jjc0.02 07 /10/14 17 :081

Lead, dis s olved M200.8 ICP-MS 0.0012 mg /L 0.0005 las0.0001 07 /25/14 16 :451

Mag nes ium, dis s olved M200.7 ICP 41.7 mg /L 1 jjc0.2 07 /10/14 17 :081

Mang anes e, dis s olved M200.7 ICP mg /L 0.03U jjc0.005 07 /10/14 17 :081

Mercury, dis s olved M245.1 CVAA mg /L 0.001U mfm0.0002 07 /14/14 12:531

Molyb denum, dis s olved M200.7 ICP 0.03 mg /L 0.1B jjc0.02 07 /10/14 17 :081

Nickel, dis s olved M200.7 ICP mg /L 0.04U jjc0.008 07 /10/14 17 :081

Potas s ium, dis s olved M200.7 ICP 19.1 mg /L 1 jjc0.2 07 /10/14 17 :081

Selenium, dis s olved M200.8 ICP-MS 0.0356 mg /L 0.0003 pmc0.0001 07 /27 /14 1:521

Silica, dis s olved M200.7 ICP 11.3 mg /L 1 jjc0.2* 07 /10/14 17 :081

Sodium, dis s olved M200.7 ICP 50.5 mg /L 1 jjc0.2* 07 /10/14 17 :081

Uranium, dis s olved M200.8 ICP-MS 0.027 4 mg /L 0.0005 las0.0001 07 /25/14 16 :451

Vanadium, dis s olved M200.7 ICP mg /L 0.03U jjc0.005 07 /10/14 17 :081

Zinc, dis s olved M200.7 ICP mg /L 0.05U jjc0.01 07 /10/14 17 :081

REPIN.02.06 .05.01 * Please refer to Qualifier Reports for details.

Page 2 of 27L19275-1407301413





Project ID:



Results

Date Sampled: 07/03/14 10:30



Wet Chemis try

XQDilution

Alkalinity as CaCO3 SM2320B - T itration


245 mg /L 20 ab d2 07 /10/14 0:001

Carb onate as CaCO3 mg /L 20U ab d2 07 /10/14 0:001

H ydroxide as CaCO3 mg /L 20U ab d2 07 /10/14 0:001

T otal Alkalinity 245 mg /L 20 ab d2* 07 /10/14 0:001

Carb on, total org anic (T OC)

SM5310B mg /L 5U mpb1* 07 /10/14 11:471


Cation-Anion Balance 5.8 % calc07 /30/14 13:09

Sum of Anions 7 .3 meq/L calc07 /30/14 13:09

Sum of Cations 8.2 meq/L calc07 /30/14 13:09

Chloride SM4500Cl-E 17 mg /L 2 mpb0.5 07 /22/14 10:511

Fluoride SM4500F-C 0.6 5 mg /L 0.3 ab d0.05 07 /21/14 13:001

Nitrate/Nitrite as N M353.2 - H 2SO4 pres erved 20.7 mg /L 1 pjb0.2 07 /26 /14 18:3810

Nitrog en, ammonia M350.1 - Automated Phenate mg /L 0.2U ms s 20.05* 07 /23/14 13:061

Res idue, Filterab le (T DS) @180C

SM2540C 480 mg /L 20 eaa10 07 /08/14 12:161

Res idue, Non-Filterab le (T SS) @105C

SM2540D 17 mg /L 20B nml5* 07 /08/14 12:251

Sulfate SM4500 SO4-D 90 mg /L 50 nml10 07 /11/14 16 :021

Sulfide as S SM4500S2-D 0.02 mg /L 0.1B enb0.02* 07 /08/14 13:381

T DS (calculated) Calculation 424 mg /L calc07 /30/14 13:09

T DS (ratio - meas ured/calculated)

Calculation 1.13 calc07 /30/14 13:09

Arizona license number: AZ0102

REPIN.02.06 .05.01 * Please refer to Qualifier Reports for details.

Page 3 of 27L19275-1407301413



Batch A distinct set of samples analyz ed at a specific time


Limit Upper limit for RPD, in % .



P CN/SCN A number assigned to reagents/standards to trace to the manufacturer' s certificate of analysis







QC Sample Types
























Method References

(1) EPA 600/4-83-020. Methods for Chemical Analysis of Water and Wastes, March 19 83.

(2) EPA 600/R-9 3-100. Methods for the Determination of Inorganic Substances in Environmental Samples, August 19 9 3.

(3) EPA 600/R-9 4-111. Methods for the Determination of Metals in Environmental Samples - Supplement I, May 19 9 4.



Comments



(3) Animal matrices for Inorganic analyses are reported on an " as received" basis.

(4) An asterisk in the " XQ" column indicates there is an extended qualifier and/or certification qualifier



For a complete list of ACZ' s Extended Qualifiers, please click: http://www.acz.com/public/extquallist.pdf

REP001.09 .12.01

Inorganic

Reference

Page 4 of 27L19275-1407301413


Inorganic QC

Summary




WG367375

WG367375PBW1 B4 B7 BF07/10/14 16:29PBW 21.7 -20 20mg/L

WG367375LCSW3 07/10/14 16:44 100.3LCSW WC140630- 822.5 9 0 110mg/L820.0001

L19 278-05DUP RA07/10/14 18:59 UDUP U 0mg/L 20

WG367375LCSW6 07/10/14 19 :13 100.4LCSW WC140630- 823 9 0 110mg/L820.0001

WG367375PBW2 B4 B7 BF07/10/14 19 :19PBW 23.5 -20 20mg/L

WG367375LCSW9 07/10/14 22:02 100.9LCSW WC140630- 827.3 9 0 110mg/L820.0001



WG367339

WG367339 ICV 07/10/14 16:21 101.2ICV II140701-2 2.023 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.09 0.09mg/L

WG367339 PQV 07/10/14 16:30 107.9PQV II140709 -2 .162 70 130mg/L.150165

WG367339 SIC 07/10/14 16:34 104.1SIC II140707-3 208.6 1 200mg/L200.450165

WG367339 LFB 07/10/14 16:40 109 .5LFB II140611-2 1.09 6 85 115mg/L1.0011

L19 266-04AS 07/10/14 16:46 .06 112.1AS II140611-2 1.182 85 115mg/L1.0011

L19 266-04ASD 07/10/14 16:49 .06 111.9ASD II140611-2 1.18 0.1785 115mg/L 201.0011

WG367339 CCV1 07/10/14 17:11 100.9CCV II140506-1 1.009 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.09 0.09mg/L

WG367339 CCV2 07/10/14 17:49 100.2CCV II140506-1 1.002 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.09 0.09mg/L

WG367339 CCV3 07/10/14 18:07 100.6CCV II140506-1 1.006 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.09 0.09mg/L



WG368334

WG368334ICV 07/25/14 16:35 104.5ICV MS140723-1 .05224 9 0 110mg/L.05

WG368334ICB 07/25/14 16:38ICB U -0.0006 0.0006mg/L

WG368334LFB 07/25/14 16:41 9 7.5LFB MS140625-3 .04884 85 115mg/L.0501

L19 409 -03AS 07/25/14 17:08 U 112.9AS MS140625-3 .05658 70 130mg/L.0501

L19 409 -03ASD 07/25/14 17:11 U 109 .4ASD MS140625-3 .05481 3.1870 130mg/L 20.0501

WG368334CCV1 07/25/14 17:15 9 6.7CCV MS140723-2 .09 689 9 0 110mg/L.1002

WG368334CCB1 07/25/14 17:18CCB .00021 -0.0006 0.0006mg/L

WG368334CCV2 07/25/14 17:55 9 9 .3CCV MS140723-2 .09 9 45 9 0 110mg/L.1002

WG368334CCB2 07/25/14 17:58CCB U -0.0006 0.0006mg/L

WG368334CCV3 07/25/14 18:18 9 8.6CCV MS140723-2 .09 876 9 0 110mg/L.1002

WG368334CCB3 07/25/14 18:21CCB U -0.0006 0.0006mg/L

Page 5 of 27L19275-1407301413


Inorganic QC

Summary




WG367339

WG367339 ICV 07/10/14 16:21 9 9 .9ICV II140701-2 1.9 9 87 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.009 0.009mg/L

WG367339 PQV 07/10/14 16:30 106PQV II140709 -2 .0159 70 130mg/L.015

WG367339 SIC 07/10/14 16:34 103SIC II140707-3 .103 80 120mg/L.1

WG367339 LFB 07/10/14 16:40 102.8LFB II140611-2 .5142 85 115mg/L.5

L19 266-04AS 07/10/14 16:46 .39 7 9 9 .9AS II140611-2 .89 64 85 115mg/L.5

L19 266-04ASD 07/10/14 16:49 .39 7 101.4ASD II140611-2 .9 042 0.8785 115mg/L 20.5

WG367339 CCV1 07/10/14 17:11 101.3CCV II140506-1 1.013 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.009 0.009mg/L

WG367339 CCV2 07/10/14 17:49 102.3CCV II140506-1 1.023 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.009 0.009mg/L

WG367339 CCV3 07/10/14 18:07 101.7CCV II140506-1 1.017 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.009 0.009mg/L



WG367339

WG367339 ICV 07/10/14 16:21 101.3ICV II140701-2 2.026 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.03 0.03mg/L

WG367339 PQV 07/10/14 16:30 103.9PQV II140709 -2 .052 70 130mg/L.05005

WG367339 SIC 07/10/14 16:34 100.9SIC II140707-3 .101 80 120mg/L.1001

WG367339 LFB 07/10/14 16:40 103.7LFB II140611-2 .519 85 115mg/L.5005

L19 266-04AS 07/10/14 16:46 .49 9 8.5AS II140611-2 .9 83 85 115mg/L.5005

L19 266-04ASD 07/10/14 16:49 .49 101.3ASD II140611-2 .9 9 7 1.4185 115mg/L 20.5005

WG367339 CCV1 07/10/14 17:11 102.5CCV II140506-1 1.025 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.03 0.03mg/L

WG367339 CCV2 07/10/14 17:49 102.1CCV II140506-1 1.021 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.03 0.03mg/L

WG367339 CCV3 07/10/14 18:07 102CCV II140506-1 1.02 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.03 0.03mg/L



WG368334

WG368334ICV 07/25/14 16:35 9 8.2ICV MS140723-1 .049 11 9 0 110mg/L.05

WG368334ICB 07/25/14 16:38ICB U -0.0003 0.0003mg/L

WG368334LFB 07/25/14 16:41 9 8.5LFB MS140625-3 .049 34 85 115mg/L.0501

L19 409 -03AS 07/25/14 17:08 .0001 110.6AS MS140625-3 .05553 70 130mg/L.0501

L19 409 -03ASD 07/25/14 17:11 .0001 110ASD MS140625-3 .05521 0.5870 130mg/L 20.0501

WG368334CCV1 07/25/14 17:15 9 9 .9CCV MS140723-2 .1001 9 0 110mg/L.1002

WG368334CCB1 07/25/14 17:18CCB U -0.0003 0.0003mg/L

WG368334CCV2 07/25/14 17:55 9 9 .3CCV MS140723-2 .09 9 53 9 0 110mg/L.1002

WG368334CCB2 07/25/14 17:58CCB U -0.0003 0.0003mg/L

WG368334CCV3 07/25/14 18:18 9 8.7CCV MS140723-2 .09 89 1 9 0 110mg/L.1002

WG368334CCB3 07/25/14 18:21CCB U -0.0003 0.0003mg/L

Page 6 of 27L19275-1407301413


Inorganic QC

Summary




WG367339

WG367339 ICV 07/10/14 16:21 9 9 .5ICV II140701-2 9 9 .54 9 5 105mg/L100

WG367339 ICB 07/10/14 16:27ICB U -0.3 0.3mg/L

WG367339 PQV 07/10/14 16:30 106PQV II140709 -2 .53 70 130mg/L.5

WG367339 SIC 07/10/14 16:34 9 8.6SIC II140707-3 19 7.6 1 200mg/L200.5

WG367339 LFB 07/10/14 16:40 107.8LFB II140611-2 73.3 85 115mg/L67.9 809 9

L19 266-04AS M307/10/14 16:46 363 79 .3AS II140611-2 416.9 85 115mg/L67.9 809 9

L19 266-04ASD M307/10/14 16:49 363 81.3ASD II140611-2 418.3 0.3485 115mg/L 2067.9 809 9

WG367339 CCV1 07/10/14 17:11 9 9 .5CCV II140506-1 49 .74 9 0 110mg/L50

WG367339 CCB1 07/10/14 17:14CCB U -0.3 0.3mg/L

WG367339 CCV2 07/10/14 17:49 9 9 .4CCV II140506-1 49 .7 9 0 110mg/L50

WG367339 CCB2 07/10/14 17:52CCB U -0.3 0.3mg/L

WG367339 CCV3 07/10/14 18:07 9 9 .5CCV II140506-1 49 .77 9 0 110mg/L50

WG367339 CCB3 07/10/14 18:10CCB U -0.3 0.3mg/L



WG358122

WG358122ICV 01/22/14 11:52 102ICV WI131209 -3 102 9 0 110mg/L100

WG358122ICB 01/22/14 11:52ICB U -3 3mg/L

WG367342

WG367342CCV1 07/10/14 11:47 9 8.2CCV WI140710-1 49 .1 9 0 110mg/L50

WG367342CCB1 07/10/14 11:47CCB U -3 3mg/L

WG367342PQV 07/10/14 11:47 9 8PQV WI140502-3 4.9 70 130mg/L5

WG367342LFB 07/10/14 11:47 9 8.6LFB WI140502-2 49 .3 9 0 110mg/L50

WG367342CCV2 07/10/14 11:47 9 7.8CCV WI140710-1 48.9 9 0 110mg/L50

WG367342CCB2 07/10/14 11:47CCB U -3 3mg/L

L19 207-05DUP RA07/10/14 11:47 5.4DUP 5.2 3.8mg/L 20

L19 207-06AS 07/10/14 11:47 3.9 9 8.8AS WI140502-2 53.3 9 0 110mg/L50

WG367342CCV3 07/10/14 11:47 9 8.8CCV WI140710-1 49 .4 9 0 110mg/L50

WG367342CCB3 07/10/14 11:47CCB U -3 3mg/L



WG368334

WG368334ICV 07/25/14 16:35 101.1ICV MS140723-1 .05056 9 0 110mg/L.05

WG368334ICB 07/25/14 16:38ICB U -0.0006 0.0006mg/L

WG368334LFB 07/25/14 16:41 103LFB MS140625-3 .05151 85 115mg/L.05

L19 409 -03AS 07/25/14 17:08 U 112.6AS MS140625-3 .05629 70 130mg/L.05

L19 409 -03ASD 07/25/14 17:11 U 111.9ASD MS140625-3 .0559 6 0.5970 130mg/L 20.05

WG368334CCV1 07/25/14 17:15 100.6CCV MS140723-2 .1006 9 0 110mg/L.1

WG368334CCB1 07/25/14 17:18CCB U -0.0006 0.0006mg/L

WG368334CCV2 07/25/14 17:55 100.1CCV MS140723-2 .1001 9 0 110mg/L.1

WG368334CCB2 07/25/14 17:58CCB U -0.0006 0.0006mg/L

WG368334CCV3 07/25/14 18:18 9 9 .7CCV MS140723-2 .09 9 66 9 0 110mg/L.1

WG368334CCB3 07/25/14 18:21CCB U -0.0006 0.0006mg/L

Page 7 of 27L19275-1407301413


Inorganic QC

Summary


Chloride SM4500Cl-E


WG368030

WG368030ICB 07/22/14 10:18ICB U -1.5 1.5mg/L

WG368030ICV 07/22/14 10:18 104.6ICV WI140701-3 57.54 9 0 110mg/L55

WG368030CCV1 07/22/14 10:51 108.2CCV WI131028-1 54.09 9 0 110mg/L50

WG368030CCB1 07/22/14 10:51CCB U -1.5 1.5mg/L

WG368030LFB1 07/22/14 10:51 107.1LFB WI140508-1 32.14 9 0 110mg/L30

L19 275-01AS 07/22/14 10:51 17 108.1AS WI140508-1 49 .44 9 0 110mg/L30

WG368030CCV2 07/22/14 10:53 108.7CCV WI131028-1 54.36 9 0 110mg/L50

WG368030CCB2 07/22/14 10:53CCB U -1.5 1.5mg/L

WG368030CCV3 07/22/14 10:55 108.4CCV WI131028-1 54.22 9 0 110mg/L50

WG368030CCB3 07/22/14 10:55CCB U -1.5 1.5mg/L

WG368030LFB2 07/22/14 10:55 108LFB WI140508-1 32.41 9 0 110mg/L30

WG368030CCV4 07/22/14 11:01 107.2CCV WI131028-1 53.58 9 0 110mg/L50

WG368030CCB4 07/22/14 11:01CCB U -1.5 1.5mg/L

WG368030CCV5 07/22/14 11:01 107.2CCV WI131028-1 53.61 9 0 110mg/L50

WG368030CCB5 07/22/14 11:01CCB U -1.5 1.5mg/L

L19 312-01DUP 07/22/14 11:03 850DUP 855 0.6mg/L 20

WG368030CCV6 07/22/14 11:06 107.2CCV WI131028-1 53.62 9 0 110mg/L50

WG368030CCB6 07/22/14 11:06CCB U -1.5 1.5mg/L

WG368030CCV7 07/22/14 11:10 107.9CCV WI131028-1 53.9 7 9 0 110mg/L50

WG368030CCB7 07/22/14 11:10CCB U -1.5 1.5mg/L

WG368030CCV8 07/22/14 11:53 106.9CCV WI131028-1 53.45 9 0 110mg/L50

WG368030CCB8 07/22/14 11:53CCB U -1.5 1.5mg/L

WG368030CCV9 07/22/14 11:53 107.5CCV WI131028-1 53.77 9 0 110mg/L50

WG368030CCB9 07/22/14 11:53CCB U -1.5 1.5mg/L



WG367339

WG367339 ICV 07/10/14 16:21 9 7.8ICV II140701-2 1.9 55 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.03 0.03mg/L

WG367339 PQV 07/10/14 16:30 9 3.8PQV II140709 -2 .047 70 130mg/L.0501

WG367339 SIC 07/10/14 16:34 9 2.8SIC II140707-3 .09 3 80 120mg/L.1002

WG367339 LFB 07/10/14 16:40 100.8LFB II140611-2 .505 85 115mg/L.501

L19 266-04AS 07/10/14 16:46 U 100AS II140611-2 .501 85 115mg/L.501

L19 266-04ASD 07/10/14 16:49 U 100ASD II140611-2 .501 085 115mg/L 20.501

WG367339 CCV1 07/10/14 17:11 9 8.3CCV II140506-1 .9 83 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.03 0.03mg/L

WG367339 CCV2 07/10/14 17:49 9 8.1CCV II140506-1 .9 81 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.03 0.03mg/L

WG367339 CCV3 07/10/14 18:07 9 8CCV II140506-1 .9 8 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.03 0.03mg/L

Page 8 of 27L19275-1407301413


Inorganic QC

Summary




WG367339

WG367339 ICV 07/10/14 16:21 9 9ICV II140701-2 1.9 8 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.03 0.03mg/L

WG367339 PQV 07/10/14 16:30 102.1PQV II140709 -2 .051 70 130mg/L.049 9 5

WG367339 SIC 07/10/14 16:34 100.1SIC II140707-3 .1 80 120mg/L.09 9 9

WG367339 LFB 07/10/14 16:40 102.2LFB II140611-2 .511 85 115mg/L.5

L19 266-04AS 07/10/14 16:46 .01 106.2AS II140611-2 .541 85 115mg/L.5

L19 266-04ASD 07/10/14 16:49 .01 105.4ASD II140611-2 .537 0.7485 115mg/L 20.5

WG367339 CCV1 07/10/14 17:11 9 9 .4CCV II140506-1 .9 9 4 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.03 0.03mg/L

WG367339 CCV2 07/10/14 17:49 9 9 .9CCV II140506-1 .9 9 9 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.03 0.03mg/L

WG367339 CCV3 07/10/14 18:07 100CCV II140506-1 1 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.03 0.03mg/L

Fluoride SM4500F-C


WG367937

WG3679 37ICV 07/21/14 12:42 100.3ICV WC140717- 2.006 9 5 105mg/L2

WG3679 37ICB 07/21/14 12:46ICB .051 -0.15 0.15mg/L

WG3679 37PQV 07/21/14 12:50 110.1PQV WC140721- .276 70 130mg/L.25075

WG3679 37LFB1 07/21/14 12:56 9 7.4LFB WC140501- 4.886 9 0 110mg/L5.015

L19 275-01AS 07/21/14 13:03 .65 9 9 .1AS WC140501- 5.621 9 0 110mg/L5.015

L19 275-01DUP 07/21/14 13:08 .65DUP .611 6.2mg/L 20

WG3679 37CCV1 07/21/14 13:55 9 4.1CCV WC140717- 1.881 9 0 110mg/L2

WG3679 37CCB1 07/21/14 13:59CCB U -0.15 0.15mg/L

WG3679 37CCV2 07/21/14 15:12 102.7CCV WC140717- 2.053 9 0 110mg/L2

WG3679 37CCB2 07/21/14 15:19CCB U -0.15 0.15mg/L

WG3679 37LFB2 07/21/14 15:44 9 6.1LFB WC140501- 4.82 9 0 110mg/L5.015

WG3679 37CCV3 07/21/14 16:02 100.8CCV WC140717- 2.015 9 0 110mg/L2

WG3679 37CCB3 07/21/14 16:10CCB U -0.15 0.15mg/L

WG3679 37CCV4 07/21/14 17:08 9 9 .4CCV WC140717- 1.9 88 9 0 110mg/L2

WG3679 37CCB4 07/21/14 17:15CCB U -0.15 0.15mg/L

WG3679 37CCV5 07/21/14 18:34 100.3CCV WC140717- 2.006 9 0 110mg/L2

WG3679 37CCB5 07/21/14 18:42CCB U -0.15 0.15mg/L

WG3679 37CCV6 07/21/14 18:53 103.1CCV WC140717- 2.062 9 0 110mg/L2

WG3679 37CCB6 07/21/14 19 :00CCB U -0.15 0.15mg/L

Page 9 of 27L19275-1407301413


Inorganic QC

Summary




WG367339

WG367339 ICV 07/10/14 16:21 9 9 .1ICV II140701-2 1.9 82 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.06 0.06mg/L

WG367339 PQV 07/10/14 16:30 9 5.9PQV II140709 -2 .048 70 130mg/L.05007

WG367339 SIC 07/10/14 16:34 9 5.2SIC II140707-3 19 0.7 1 200mg/L200.33007

WG367339 LFB 07/10/14 16:40 102.4LFB II140611-2 1.025 85 115mg/L1.0014

L19 266-04AS 07/10/14 16:46 .09 100.4AS II140611-2 1.09 5 85 115mg/L1.0014

L19 266-04ASD 07/10/14 16:49 .09 100.7ASD II140611-2 1.09 8 0.2785 115mg/L 201.0014

WG367339 CCV1 07/10/14 17:11 9 9 .2CCV II140506-1 .9 9 2 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.06 0.06mg/L

WG367339 CCV2 07/10/14 17:49 9 9CCV II140506-1 .9 9 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.06 0.06mg/L

WG367339 CCV3 07/10/14 18:07 9 9 .3CCV II140506-1 .9 9 3 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.06 0.06mg/L



WG368334

WG368334ICV 07/25/14 16:35 101.2ICV MS140723-1 .05061 9 0 110mg/L.05

WG368334ICB 07/25/14 16:38ICB U -0.0003 0.0003mg/L

WG368334LFB 07/25/14 16:41 100LFB MS140625-3 .05003 85 115mg/L.05005

L19 409 -03AS 07/25/14 17:08 U 108.8AS MS140625-3 .05444 70 130mg/L.05005

L19 409 -03ASD 07/25/14 17:11 U 109 .9ASD MS140625-3 .0549 8 0.9 970 130mg/L 20.05005

WG368334CCV1 07/25/14 17:15 101.3CCV MS140723-2 .2535 9 0 110mg/L.25025

WG368334CCB1 07/25/14 17:18CCB U -0.0003 0.0003mg/L

WG368334CCV2 07/25/14 17:55 100.2CCV MS140723-2 .2508 9 0 110mg/L.25025

WG368334CCB2 07/25/14 17:58CCB U -0.0003 0.0003mg/L

WG368334CCV3 07/25/14 18:18 9 9 .5CCV MS140723-2 .249 9 0 110mg/L.25025

WG368334CCB3 07/25/14 18:21CCB U -0.0003 0.0003mg/L



WG367339

WG367339 ICV 07/10/14 16:21 9 6.7ICV II140701-2 9 6.72 9 5 105mg/L100

WG367339 ICB 07/10/14 16:27ICB .2 -0.6 0.6mg/L

WG367339 PQV 07/10/14 16:30 115.9PQV II140709 -2 1.16 70 130mg/L1.0007

WG367339 SIC 07/10/14 16:34 100.5SIC II140707-3 202.2 1 200mg/L201.1407

WG367339 LFB 07/10/14 16:40 9 9 .6LFB II140611-2 49 .82 85 115mg/L50.00131

L19 266-04AS 07/10/14 16:46 133 9 0.4AS II140611-2 178.2 85 115mg/L50.00131

L19 266-04ASD 07/10/14 16:49 133 9 1.4ASD II140611-2 178.7 0.2885 115mg/L 2050.00131

WG367339 CCV1 07/10/14 17:11 9 5.9CCV II140506-1 47.9 4 9 0 110mg/L50

WG367339 CCB1 07/10/14 17:14CCB U -0.6 0.6mg/L

WG367339 CCV2 07/10/14 17:49 9 5.7CCV II140506-1 47.86 9 0 110mg/L50

WG367339 CCB2 07/10/14 17:52CCB U -0.6 0.6mg/L

WG367339 CCV3 07/10/14 18:07 9 6.4CCV II140506-1 48.18 9 0 110mg/L50

WG367339 CCB3 07/10/14 18:10CCB U -0.6 0.6mg/L

Page 10 of 27L19275-1407301413


Inorganic QC

Summary




WG367339

WG367339 ICV 07/10/14 16:21 9 9ICV II140701-2 1.9 808 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.015 0.015mg/L

WG367339 PQV 07/10/14 16:30 9 3.2PQV II140709 -2 .0233 70 130mg/L.025

WG367339 SIC 07/10/14 16:34 9 7.7SIC II140707-3 48.9 6 1 200mg/L50.125

WG367339 LFB 07/10/14 16:40 102.9LFB II140611-2 .5157 85 115mg/L.501

L19 266-04AS 07/10/14 16:46 .062 100.8AS II140611-2 .5668 85 115mg/L.501

L19 266-04ASD 07/10/14 16:49 .062 101.3ASD II140611-2 .569 3 0.4485 115mg/L 20.501

WG367339 CCV1 07/10/14 17:11 100.3CCV II140506-1 1.003 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.015 0.015mg/L

WG367339 CCV2 07/10/14 17:49 100.4CCV II140506-1 1.004 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.015 0.015mg/L

WG367339 CCV3 07/10/14 18:07 100.8CCV II140506-1 1.008 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.015 0.015mg/L



WG367460

WG367460ICV 07/14/14 12:32 9 7.1ICV II140701-1 .00486 9 5 105mg/L.005005

WG367460ICB 07/14/14 12:34ICB U -0.0002 0.0002mg/L

WG367460LRB 07/14/14 12:37LRB U -0.00044 0.00044mg/L

WG367460LFB 07/14/14 12:39 9 1.9LFB II140616-4 .00184 85 115mg/L.002002

L19 274-02LFM 07/14/14 12:46 U 9 2.9LFM II140616-4 .00186 85 115mg/L.002002

L19 274-02LFMD 07/14/14 12:49 U 9 1.9LFMD II140616-4 .00184 1.0885 115mg/L 20.002002

WG367460CCV1 07/14/14 13:00 9 6.5CCV II140701-1 .00483 9 0 110mg/L.005005

WG367460CCB1 07/14/14 13:02CCB U -0.0002 0.0002mg/L

WG367460CCV2 07/14/14 13:27 9 5.1CCV II140701-1 .00476 9 0 110mg/L.005005

WG367460CCB2 07/14/14 13:29CCB U -0.0002 0.0002mg/L

WG367460CCV3 07/14/14 13:43 9 6.5CCV II140701-1 .00483 9 0 110mg/L.005005

WG367460CCB3 07/14/14 13:45CCB U -0.0002 0.0002mg/L



WG367339

WG367339 ICV 07/10/14 16:21 102ICV II140701-2 2.04 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.06 0.06mg/L

WG367339 PQV 07/10/14 16:30 106.1PQV II140709 -2 .106 70 130mg/L.09 9 9

WG367339 SIC 07/10/14 16:34 9 3.1SIC II140707-3 .09 3 80 120mg/L.09 9 9

WG367339 LFB 07/10/14 16:40 103.9LFB II140611-2 .519 85 115mg/L.49 9 5

L19 266-04AS 07/10/14 16:46 U 105.3AS II140611-2 .526 85 115mg/L.49 9 5

L19 266-04ASD 07/10/14 16:49 U 106.5ASD II140611-2 .532 1.1385 115mg/L 20.49 9 5

WG367339 CCV1 07/10/14 17:11 102.2CCV II140506-1 1.022 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.06 0.06mg/L

WG367339 CCV2 07/10/14 17:49 102.9CCV II140506-1 1.029 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.06 0.06mg/L

WG367339 CCV3 07/10/14 18:07 102.3CCV II140506-1 1.023 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.06 0.06mg/L

Page 11 of 27L19275-1407301413


Inorganic QC

Summary




WG367339

WG367339 ICV 07/10/14 16:21 9 9 .2ICV II140701-2 1.9 84 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.024 0.024mg/L

WG367339 PQV 07/10/14 16:30 114.9PQV II140709 -2 .0461 70 130mg/L.04012

WG367339 SIC 07/10/14 16:34 101.9SIC II140707-3 .1022 80 120mg/L.1003

WG367339 LFB 07/10/14 16:40 101.7LFB II140611-2 .5087 85 115mg/L.5

L19 266-04AS 07/10/14 16:46 .014 9 9 .4AS II140611-2 .5111 85 115mg/L.5

L19 266-04ASD 07/10/14 16:49 .014 9 9 .8ASD II140611-2 .5129 0.3585 115mg/L 20.5

WG367339 CCV1 07/10/14 17:11 9 8.2CCV II140506-1 .9 815 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.024 0.024mg/L

WG367339 CCV2 07/10/14 17:49 9 9 .4CCV II140506-1 .9 9 35 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.024 0.024mg/L

WG367339 CCV3 07/10/14 18:07 9 8.4CCV II140506-1 .9 84 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.024 0.024mg/L



WG368358

WG368358ICV 07/26/14 15:09 9 9 .5ICV WI140718-9 2.404 9 0 110mg/L2.416

WG368358ICB 07/26/14 15:10ICB U -0.06 0.06mg/L

WG368365

WG368365CCV1 07/26/14 18:32 102.6CCV WI140719 -1 2.052 9 0 110mg/L2

WG368365CCB1 07/26/14 18:34CCB U -0.06 0.06mg/L

WG368365LFB 07/26/14 18:35 102LFB WI140719 -4 2.04 9 0 110mg/L2

L19 267-01AS 07/26/14 18:37 U 102.6AS WI140719 -4 2.051 9 0 110mg/L2

L19 275-01DUP 07/26/14 18:40 20.7DUP 20.84 0.7mg/L 20

WG368365CCV2 07/26/14 18:47 101.9CCV WI140719 -1 2.037 9 0 110mg/L2

WG368365CCB2 07/26/14 18:48CCB U -0.06 0.06mg/L

WG368365CCV3 07/26/14 18:55 102.5CCV WI140719 -1 2.049 9 0 110mg/L2

WG368365CCB3 07/26/14 18:56CCB U -0.06 0.06mg/L

Page 12 of 27L19275-1407301413


Inorganic QC

Summary




WG368113

WG368113ICV 07/23/14 12:01 100.7ICV WI131021-1 1.01 9 0 110mg/L1.003

WG368113ICB 07/23/14 12:05ICB U -0.15 0.15mg/L

WG368114

WG368114CCV1 07/23/14 13:03 100.7CCV WI140113-6 2.014 9 0 110mg/L2

WG368114CCB1 07/23/14 13:04CCB U -0.15 0.15mg/L

WG368114LFB1 07/23/14 13:05 102.7LFB WI140113-8 1.027 9 0 110mg/L1

L19 275-01AS 07/23/14 13:07 U 101.8AS WI140113-8 1.018 9 0 110mg/L1

L19 312-01DUP RA07/23/14 13:09 UDUP U 0mg/L 20

WG368114CCV2 07/23/14 13:16 9 9 .5CCV WI140113-6 1.9 89 9 0 110mg/L2

WG368114CCB2 07/23/14 13:17CCB U -0.15 0.15mg/L

WG368114CCV3 07/23/14 13:29 103CCV WI140113-6 2.059 9 0 110mg/L2

WG368114CCB3 07/23/14 13:30CCB U -0.15 0.15mg/L

WG368114LFB2 07/23/14 13:36 100.1LFB WI140113-8 1.001 9 0 110mg/L1

WG368114CCV4 07/23/14 13:42 100.5CCV WI140113-6 2.01 9 0 110mg/L2

WG368114CCB4 07/23/14 13:43CCB U -0.15 0.15mg/L

WG368114CCV5 07/23/14 13:55 9 8.8CCV WI140113-6 1.9 76 9 0 110mg/L2

WG368114CCB5 07/23/14 13:56CCB U -0.15 0.15mg/L

WG368114CCV6 07/23/14 14:23 102.7CCV WI140113-6 2.053 9 0 110mg/L2

WG368114CCB6 07/23/14 14:24CCB U -0.15 0.15mg/L

WG368114CCV7 07/23/14 14:29 100.9CCV WI140113-6 2.018 9 0 110mg/L2

WG368114CCB7 07/23/14 14:30CCB U -0.15 0.15mg/L



WG367339

WG367339 ICV 07/10/14 16:21 9 8.8ICV II140701-2 19 .76 9 5 105mg/L20

WG367339 ICB 07/10/14 16:27ICB U -0.6 0.6mg/L

WG367339 PQV 07/10/14 16:30 112PQV II140709 -2 1.12 70 130mg/L1

WG367339 SIC 07/10/14 16:34 110SIC II140707-3 1.1 80 120mg/L1

WG367339 LFB 07/10/14 16:40 101.4LFB II140611-2 101.4 85 115mg/L9 9 .9 9 364

L19 266-04AS 07/10/14 16:46 23.1 103.4AS II140611-2 126.5 85 115mg/L9 9 .9 9 364

L19 266-04ASD 07/10/14 16:49 23.1 103.4ASD II140611-2 126.5 085 115mg/L 209 9 .9 9 364

WG367339 CCV1 07/10/14 17:11 9 9 .2CCV II140506-1 9 .9 2 9 0 110mg/L10

WG367339 CCB1 07/10/14 17:14CCB U -0.6 0.6mg/L

WG367339 CCV2 07/10/14 17:49 9 9 .6CCV II140506-1 9 .9 6 9 0 110mg/L10

WG367339 CCB2 07/10/14 17:52CCB U -0.6 0.6mg/L

WG367339 CCV3 07/10/14 18:07 100CCV II140506-1 10 9 0 110mg/L10

WG367339 CCB3 07/10/14 18:10CCB U -0.6 0.6mg/L



WG367184

WG367184PBW 07/08/14 11:50PBW U -20 20mg/L

WG367184LCSW 07/08/14 11:51 9 6.2LCSW PCN46082 250 80 120mg/L260

L19 269 -01DUP RO07/08/14 12:07 340DUP 344 1.2mg/L 10

Page 13 of 27L19275-1407301413


Inorganic QC

Summary




WG367186

WG367186PBW 07/08/14 12:00PBW U -6 6mg/L


L19 277-06DUP RA07/08/14 12:39 UDUP 2.4 200mg/L 10



WG368366

WG368366ICV 07/27/14 1:42 9 9 .6ICV MS140723-1 .049 79 9 0 110mg/L.05

WG368366ICB 07/27/14 1:45ICB U -0.0003 0.0003mg/L

WG368366LFB1 07/27/14 1:49 9 7.5LFB MS140625-3 .04878 85 115mg/L.05005

L19 429 -03AS 07/27/14 2:15 U 119AS MS140625-3 .119 08 70 130mg/L.1001

L19 429 -03ASD 07/27/14 2:18 U 115.6ASD MS140625-3 .11568 2.970 130mg/L 20.1001

WG368366CCV1 07/27/14 2:22 100.2CCV MS140723-2 .2513 9 0 110mg/L.25075

WG368366CCB1 07/27/14 2:25CCB U -0.0003 0.0003mg/L

WG368366CCV2 07/27/14 3:01 9 9 .9CCV MS140723-2 .2506 9 0 110mg/L.25075

WG368366CCB2 07/27/14 3:04CCB U -0.0003 0.0003mg/L



WG367339

WG367339 ICV 07/10/14 16:21 9 7.9ICV II140701-2 41.9 2 9 5 105mg/L42.8

WG367339 ICB 07/10/14 16:27ICB U -0.6 0.6mg/L

WG367339 PQV 07/10/14 16:30 9 6.1PQV II140709 -2 1.03 70 130mg/L1.0714

WG367339 SIC 07/10/14 16:34 84.9SIC II140707-3 .9 1 80 120mg/L1.0714

WG367339 LFB 07/10/14 16:40 103.7LFB II140611-2 22.23 85 115mg/L21.428

L19 266-04AS M307/10/14 16:46 133 75.6AS II140611-2 149 .2 85 115mg/L21.428

L19 266-04ASD M307/10/14 16:49 133 81.7ASD II140611-2 150.5 0.8785 115mg/L 2021.428

WG367339 CCV1 07/10/14 17:11 9 9 .2CCV II140506-1 21.22 9 0 110mg/L21.4

WG367339 CCB1 07/10/14 17:14CCB U -0.6 0.6mg/L

WG367339 CCV2 07/10/14 17:49 9 9 .3CCV II140506-1 21.25 9 0 110mg/L21.4

WG367339 CCB2 07/10/14 17:52CCB U -0.6 0.6mg/L

WG367339 CCV3 07/10/14 18:07 9 8.5CCV II140506-1 21.07 9 0 110mg/L21.4

WG367339 CCB3 07/10/14 18:10CCB U -0.6 0.6mg/L

Page 14 of 27L19275-1407301413


Inorganic QC

Summary




WG367339

WG367339 ICV 07/10/14 16:21 9 8ICV II140701-2 9 7.9 8 9 5 105mg/L100

WG367339 ICB 07/10/14 16:27ICB U -0.6 0.6mg/L

WG367339 PQV 07/10/14 16:30 101.9PQV II140709 -2 1.02 70 130mg/L1.001

WG367339 SIC 07/10/14 16:34 100.9SIC II140707-3 1.01 80 120mg/L1.001

WG367339 LFB 07/10/14 16:40 101.6LFB II140611-2 101.6 85 115mg/L100.039 3

L19 266-04AS M307/10/14 16:46 436 78.5AS II140611-2 514.5 85 115mg/L100.039 3

L19 266-04ASD M307/10/14 16:49 436 81.7ASD II140611-2 517.7 0.6285 115mg/L 20100.039 3

WG367339 CCV1 07/10/14 17:11 9 8CCV II140506-1 49 .02 9 0 110mg/L50

WG367339 CCB1 07/10/14 17:14CCB U -0.6 0.6mg/L

WG367339 CCV2 07/10/14 17:49 9 8.4CCV II140506-1 49 .22 9 0 110mg/L50

WG367339 CCB2 07/10/14 17:52CCB U -0.6 0.6mg/L

WG367339 CCV3 07/10/14 18:07 9 8CCV II140506-1 49 .01 9 0 110mg/L50

WG367339 CCB3 07/10/14 18:10CCB U -0.6 0.6mg/L



WG367463

WG367463PBW 07/11/14 13:40PBW U -30 30mg/L


L19 29 5-01DUP 07/11/14 16:31 1370DUP 1325 3.3mg/L 20



WG367192

WG36719 2ICV 07/08/14 13:06 9 8.4ICV WC140707- .278 9 0 110mg/L.28266

WG36719 2ICB 07/08/14 13:12ICB U -0.06 0.06mg/L

WG36719 2LFB 07/08/14 13:19 116.7LFB WC140707- .249 80 120mg/L.2133333

L19 275-01AS M207/08/14 13:45 .02 72.7AS WC140707- .175 75 125mg/L.2133333

L19 275-01DUP RA07/08/14 13:51 .02DUP .02 0mg/L 20

WG36719 2CCV 07/08/14 13:58 100.6CCV WC140707- .161 9 0 110mg/L.16

WG36719 2CCB 07/08/14 14:04CCB U -0.06 0.06mg/L



WG368334

WG368334ICV 07/25/14 16:35 103.8ICV MS140723-1 .05189 9 0 110mg/L.05

WG368334ICB 07/25/14 16:38ICB U -0.0003 0.0003mg/L

WG368334LFB 07/25/14 16:41 101.8LFB MS140625-3 .0509 5 85 115mg/L.05005

L19 409 -03AS 07/25/14 17:08 U 109AS MS140625-3 .05456 70 130mg/L.05005

L19 409 -03ASD 07/25/14 17:11 U 109 .4ASD MS140625-3 .05476 0.3770 130mg/L 20.05005

WG368334CCV1 07/25/14 17:15 9 8.1CCV MS140723-2 .09 817 9 0 110mg/L.1001

WG368334CCB1 07/25/14 17:18CCB U -0.0003 0.0003mg/L

WG368334CCV2 07/25/14 17:55 9 9CCV MS140723-2 .09 9 09 9 0 110mg/L.1001

WG368334CCB2 07/25/14 17:58CCB U -0.0003 0.0003mg/L

WG368334CCV3 07/25/14 18:18 9 8.2CCV MS140723-2 .09 828 9 0 110mg/L.1001

WG368334CCB3 07/25/14 18:21CCB U -0.0003 0.0003mg/L

Page 15 of 27L19275-1407301413


Inorganic QC

Summary




WG367339

WG367339 ICV 07/10/14 16:21 100ICV II140701-2 2.0002 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.015 0.015mg/L

WG367339 PQV 07/10/14 16:30 9 3.6PQV II140709 -2 .0234 70 130mg/L.025

WG367339 SIC 07/10/14 16:34 9 6.1SIC II140707-3 .09 61 80 120mg/L.1

WG367339 LFB 07/10/14 16:40 104.9LFB II140611-2 .5245 85 115mg/L.5

L19 266-04AS 07/10/14 16:46 .01 104.5AS II140611-2 .5327 85 115mg/L.5

L19 266-04ASD 07/10/14 16:49 .01 104.8ASD II140611-2 .5339 0.2385 115mg/L 20.5

WG367339 CCV1 07/10/14 17:11 100.8CCV II140506-1 1.008 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.015 0.015mg/L

WG367339 CCV2 07/10/14 17:49 100.1CCV II140506-1 1.001 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.015 0.015mg/L

WG367339 CCV3 07/10/14 18:07 100.4CCV II140506-1 1.004 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.015 0.015mg/L



WG367339

WG367339 ICV 07/10/14 16:21 9 6.9ICV II140701-2 1.9 38 9 5 105mg/L2

WG367339 ICB 07/10/14 16:27ICB U -0.03 0.03mg/L

WG367339 PQV 07/10/14 16:30 103.9PQV II140709 -2 .052 70 130mg/L.05005

WG367339 SIC 07/10/14 16:34 9 7SIC II140707-3 .09 7 80 120mg/L.10005

WG367339 LFB 07/10/14 16:40 103.5LFB II140611-2 .518 85 115mg/L.5005

L19 266-04AS 07/10/14 16:46 U 100.9AS II140611-2 .505 85 115mg/L.5005

L19 266-04ASD 07/10/14 16:49 U 101.5ASD II140611-2 .508 0.5985 115mg/L 20.5005

WG367339 CCV1 07/10/14 17:11 9 8.3CCV II140506-1 .9 83 9 0 110mg/L1

WG367339 CCB1 07/10/14 17:14CCB U -0.03 0.03mg/L

WG367339 CCV2 07/10/14 17:49 9 8CCV II140506-1 .9 8 9 0 110mg/L1

WG367339 CCB2 07/10/14 17:52CCB U -0.03 0.03mg/L

WG367339 CCV3 07/10/14 18:07 9 7.8CCV II140506-1 .9 78 9 0 110mg/L1

WG367339 CCB3 07/10/14 18:10CCB U -0.03 0.03mg/L

Page 16 of 27L19275-1407301413


Inorganic Extended

Qualifier Report




M200.7 ICPCalcium, dissolvedL19275-01 WG367339


M200.7 ICPSilica, dissolved








SM2540DResidue, Non-Filterable (TSS) @ 105CWG367186


SM4500S2-DSulfide as SWG36719 2


SM4500S2-D

B7 Target analyte detected in prep / method blank at or above acceptance limit. Sample value is > 10X the concentration in the method blank.



SM2320B - Titration

REPAD.15.06.05.01

Page 17 of 27L19275-1407301413





Project ID:


Date Sampled: 07/03/14 10:30


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 11 4.7 3 pCi/L * bsg07/22/14 0:17


Lead 210, dissolved

EICHROM, OTW01

Prep Method:




M903.1

Prep Method:




M904.0

Prep Method:




ESM 4506

Prep Method:


Thorium 230, dissolved 0.29 0.31 0.56 pCi/L * thf07/15/14 0:00



Page 18 of 27L19275-1407301413




Error(+/-) C alculated sample specific uncertainty

Found V alue of the QC Type of interest

Limit U pper limit for RPD , in % .

LCL Low er C ontrol Limit, in % ( ex cept for LC SS, mg/K g)

LLD C alculated sample specific Low er Limit of D etection

PCN/SCN A number assigned to reagents/standards to trace to the manufacturer's certificate of analy sis

PQL Practical Q uantitation Limit

QC True V alue of the C ontrol Sample or the amount added to the Spik e

Rec Amount of the true value or spik e added recovered, in % ( ex cept for LC SS, mg/K g)

RER Relative Error Ratio, calculation used for D up. Q C tak ing into account the error factor.

RPD Relative Percent D ifference, calculation used for D uplicate Q C Ty pes

UCL U pper C ontrol Limit, in % ( ex cept for LC SS, mg/K g)

Sample V alue of the Sample of interest

QC Sample Types

DUP Sample D uplicate MS/MSD Matrix Spik e/Matrix Spik e D uplicate

LCSS Laboratory C ontrol Sample - Soil PBS Prep B lank - Soil

LCSW Laboratory C ontrol Sample - Water PBW Prep B lank - Water


B lank s V erifies that there is no or minimal contamination in the prep method procedure.

C ontrol Samples V erifies the accuracy of the method, including the prep procedure.

D uplicates V erifies the precision of the instrument and/or method.

Matrix Spik es D etermines sample matrix interferences, if any .


H Analy sis ex ceeded method hold time.


M EPA methodology , including those under SD WA, C WA, and RC RA

SM Standard Methods for the Ex amination of Water and Wastew ater.

D ASTM

RP D OE

ESM D OE/ESM

Comments

( 1) Solid matrices are reported on a dry w eight basis.

( 2) Preparation method: " Method" indicates preparation defined in analy tical method.

( 3) Q C results calculated from raw data. Results may vary slightly if the rounded values are used in the calculations.

( 4) An asterisk in the " X Q " column indicates there is an ex tended q ualifier and/or certification

q ualifier associated w ith the result.

F or a complete list of AC Z 's Ex tended Q ualifiers, please click : http://w w w .acz .com/public/ex tq uallist.pdf

REP003.09.12.01

Radiochemistry

Reference

Page 19 of 27L19275-1407301413


Radiochemistry QC

Summary


Alpha M900.0


pC i/L

Error LLDLLD

Units:

WG368012

WG367557PB W 07/22/14PB W -.1 2.40.89 1.2

WG367557LCSWA 07/22/14 129LCSW PCN45451 8666.67 83 1337.2 1.2

L19216-02DUP 07/22/14 0.05DUP-RER .75 22 0.252 2.42.4

L19311-01DUP 07/22/14 4.9DUP-RER 5.2 24.5 0.054.2 3.63.6

L19216-04MSA M207/22/14 1.9 72.1MS PCN45451 6283.33 83 1339.92.5 2.92.5

Beta M900.0


pC i/L

Error LLDLLD

Units:

WG368012

WG367557PBW 07/22/14PBW 1.6 6.82.5 3.4

WG367557LCSWB 07/22/14 115.5LCSW PCN44659 7766.67 70 1295.3 3.3

L19216-02DUP 07/22/14 6.8DUP-RER 3.7 23.7 0.623.4 4.44.2

L19311-01DUP 07/22/14 5.3DUP-RER 9.7 25 0.634.8 6.36.3

L19311-02MSB 07/22/14 12 108MS PCN44659 120100 70 1299.55.4 6.56.5



pC i/L

Error LLDLLD

Units:

WG368100

WG367774PBW 07/22/14PBW -.07 4.80.61 2.4

WG367774LCSW 07/22/14 79.8LCSW PCN44125 7897.72 55 1213.8 9.6

L19253-01DUP 07/22/14 -1.5DUP-RER -2.4 21.7 0.391.6 6.76.3

L19275-01MS 07/22/14 -9.1 89.1MS PCN44125 7897.71 55 1213.51.8 8.47.7

WG367774LCSWD 07/22/14 90.1LCSWD PCN44125 8897.71 55 121 203.5 7.8 12

Page 20 of 27L19275-1407301413


Radiochemistry QC

Summary




pC i/L

Error LLDLLD

Units:

WG368214

WG367763PB W 07/23/14PB W .15 0.340.08 0.17

WG367763LCSW 07/23/14 90LCSW PCN45815 1820 43 1480.51 0.17

L19275-01DUP 07/23/14 0.27DUP-RER .58 20.18 1.540.09 0.280.12

L19367-01MS 07/23/14 1.2 94MS PCN45815 2020 43 1480.550.15 0.240.23



pC i/L

Error LLDLLD

Units:

WG367784

WG367317LCSW 07/15/14 65.2LCSW PCN44321 1218.39 47 1231 0.45

WG367317PBW 07/15/14PBW .39 0.50.26 0.25

L19156-03DUP 07/16/14 1.7DUP-RER 3.6 21.2 1.240.96 1.10.91

L19253-01DUP 07/16/14 2.2DUP-RER 3.2 20.68 0.990.74 0.510.64

L19275-01MS 07/16/14 0.65 61.7MS PCN44321 1218.39 47 1231.40.53 0.830.52



pC i/L

Error LLDLLD

Units:

WG367670

L19253-01MS 07/15/14 0.5 98.4MS RC130807-2 160162.12 91 1264.60.42 0.680.71

WG367510LCSW 07/15/14 92.5LCSW RC130807-2 150162.12 91 1264 0.56

WG367510LCSWD 07/15/14 98.7LCSWD RC130807-2 160162.12 91 126 204.3 0.58 6.5

WG367510PBW 07/15/14PBW .04 0.30.07 0.15

Page 21 of 27L19275-1407301413


RadChem Extended

Qualifier Report



M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB ) was acceptable.


REPAD.15.06.05.01

Page 22 of 27L19275-1407301413


Certification

Qualifiers


Metals Analysis

The following parameters are not offered for certification or are not cov ered by AZ certificate #AZ0102.


The following parameters are not offered for certification or are not cov ered by NELAC certificate #ACZ.


Radiochemistry







Wet C hemistry





REPAD.05.06.05.01

Page 23 of 27L19275-1407301413


Sample

Receipt


Date Received:

Received By: mtb

07/08/2014 09:57

L19275




NANOYES

X

X

X

X

X









NANOYES

X

X

X

X

X

X

X












Samples/Containers

X

X

X

X

Shipping Containers



A change was made in the # of Containers and Relinquished Date:Time section prior to ACZ custody.

Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- --------------------NA19982 5.3 13 Yes

X



REPAD LPII 2012-03

Page 24 of 27L19275-1407301413


Sample

Receipt


Date Received:

Received By: mtb

07/08/2014 09:57

L19275


REPAD LPII 2012-03

Page 25 of 27L19275-1407301413

of 27L19275-1407301413


Analytical

Report


225 Union B lvd. ,Suite 600

Lakewood, CO 80228


K athy Weinel:

Enclosed are the analytical results for sample(s) submitted to ACZ Laboratories, Inc. (ACZ) on July 23, 2014. This project has been assigned to ACZ's project number, L19607. Please reference this number in all future inquiries.




All samples and sub-samples associated with this project will be disposed of after September 19, 2014. If the samples are determined to be haz ardous, additional charges apply for disposal (typically $ 11/sample). If you would like the samples to be held longer than ACZ's stated policy or to be returned, please contact your Project Manager or C ustomer Service Representative for further details and associated costs. ACZ retains analytical raw data reports for ten years.


K athy Weinel

August 20, 2014

Project ID:


225 Union B lvd. ,Suite 600

Lakewood, CO 80228

Accounts Payable

Report to: B ill to:

Page 1 of 32L19607-1408200824


Sample ID: HURDLE WELL



Project ID:



Results

Date Sampled: 07/21/14 10:30



Metals Analysis

XQDilution













Manganese, dissolved M200.7 ICP mg/L 0.03U jjc0.005* 08/04/14 17:161










Zinc, dissolved M200.7 ICP 0.01 mg/L 0.05B aeb0.01 08/01/14 20:031


Page 2 of 32L19607-1408200824





Project ID:



Results

Date Sampled: 07/21/14 10:30



Wet Chemistry

XQDilution



211 mg/L 20 enb2 07/29/14 0:001





SM5310B mg/L 5U mpb1* 07/31/14 17:061





Chloride SM4500Cl-E 36.4 mg/L 2 tcd0.5 08/05/14 16:051


Nitrate/Nitrite as N M353.2 - H2SO4 preserved 33.1 mg/L 2 pjb0.3* 08/07/14 23:5715

Nitrogen, ammonia M350.1 - Automated Phenate mg/L 0.2U bsu0.05* 08/05/14 14:241


SM2540C 920 mg/L 20 nml10 07/23/14 14:441


SM2540D mg/L 20U eaa5* 07/23/14 16:511

Sulfate SM4500 SO4-D 320 mg/L 50 nml10 07/28/14 9:561






Page 3 of 32L19607-1408200824


Sample ID: B LM WELL



Project ID:



Results

Date Sampled: 07/21/14 11:20



Metals Analysis

XQDilution



B arium, dissolved M200.7 ICP 0.015 mg/L 0.02B jjc0.003 08/04/14 17:191

B oron, dissolved M200.7 ICP 0.21 mg/L 0.05 jjc0.01 08/04/14 17:191









Manganese, dissolved M200.7 ICP mg/L 0.03U jjc0.005* 08/04/14 17:191












Page 4 of 32L19607-1408200824


Sample ID: B LM WELL



Project ID:



Results

Date Sampled: 07/21/14 11:20



Wet C hemistry

XQDilution

Alkalinity as C aCO3 SM2320B - Titration

B icarbonate as C aCO3

237 mg/L 20 enb2 07/29/14 0:001

C arbonate as C aCO3 mg/L 20U enb2 07/29/14 0:001

Hydroxide as C aCO3 mg/L 20U enb2 07/29/14 0:001


Carbon, total organic (TOC )

SM5310B mg/L 5U mpb1* 07/31/14 17:061

Cation-Anion B alance Calculation

C ation-Anion B alance 0.0 % calc08/19/14 0:00


Sum of C ations 14 meq/L calc08/19/14 0:00

Chloride SM4500C l-E 22.1 mg/L 2 tcd0.5 08/05/14 16:051


Nitrate/Nitrite as N M353.2 - H2SO4 preserved 19 mg/L 1 pjb0.2* 08/07/14 23:5810

Nitrogen, ammonia M350.1 - Automated Phenate mg/L 0.2U bsu0.05* 08/05/14 14:251


SM2540C 900 mg/L 20 nml10 07/23/14 14:461


SM2540D mg/L 20U eaa5* 07/23/14 16:531

Sulfate SM4500 SO4-D 400 mg/L 50 nml10 07/28/14 10:271






Page 5 of 32L19607-1408200824















QC Sample Types
























Method References






Comments








REP001.09.12.01

Inorganic

Reference

Page 6 of 32L19607-1408200824


Inorganic QC

Summary




WG368462

WG368462PBW1 07/29/14 12:11PBW U -20 20mg/L

WG368462LCSW3 07/29/14 12:29 102LCSW WC140715- 836 90 110mg/L820

WG368462PQV2 07/29/14 12:38 107PQV WC140707- 21.4 50 150mg/L20

WG368462LCSW6 07/29/14 15:03 100.7LCSW WC140715- 826 90 110mg/L820

WG368462PBW2 07/29/14 15:09PBW U -20 20mg/L


WG368462PBW3 07/29/14 18:34PBW U -20 20mg/L

L19607-02DUP 07/29/14 21:50 237DUP 250 5.3mg/L 20


WG368462PBW4 07/29/14 22:14PBW U -20 20mg/L

WG368462LCSW15 07/30/14 1:33 103LCSW WC140715- 845 90 110mg/L820

WG368462PBW5 07/30/14 1:39PBW U -20 20mg/L


Aluminum, dissolv ed M200.7 ICP


WG368765

WG368765ICV 08/01/14 19:42 99.8IC V II140729-1 1.996 95 105mg/L2

WG368765IC B 08/01/14 19:48IC B U -0.09 0.09mg/L

WG368765PQV 08/01/14 19:51 71.3PQV II140709-2 .107 70 130mg/L.150165

WG368765SIC 08/01/14 19:54 103.1SIC II140707-2 206.7 1 200mg/L200.450165

WG368765LFB 08/01/14 20:00 100.2LFB II140722-2 1.004 85 115mg/L1.0015

L19681-03AS 08/01/14 20:25 3.01 99.9AS II140722-2 4.01 85 115mg/L1.0015

L19681-03ASD 08/01/14 20:28 3.01 94.4ASD II140722-2 3.955 1.3885 115mg/L 201.0015

WG368765CCV1 08/01/14 20:31 100.1C CV II140730-1 1.001 90 110mg/L1

WG368765CC B 1 08/01/14 20:34C C B U -0.09 0.09mg/L

WG368765CCV2 08/01/14 21:08 102.7C CV II140730-1 1.027 90 110mg/L1

WG368765CC B 2 08/01/14 21:11C C B U -0.09 0.09mg/L

WG368765CCV3 08/01/14 21:29 103.6C CV II140730-1 1.036 90 110mg/L1

WG368765CC B 3 08/01/14 21:33C C B U -0.09 0.09mg/L

Arsenic, dissolv ed M200.8 ICP-MS


WG369213

WG369213ICV 08/12/14 1:22 104.7IC V MS140723-1 .05235 90 110mg/L.05

WG369213IC B 08/12/14 1:25IC B U -0.0006 0.0006mg/L

WG369213LFB 08/12/14 1:28 100.1LFB MS140728-3 .05015 85 115mg/L.0501

L19601-03AS 08/12/14 1:41 .069 102.3AS MS140728-3 1.094 70 130mg/L1.002

L19601-03ASD 08/12/14 1:45 .069 103ASD MS140728-3 1.1008 0.6270 130mg/L 201.002

WG369213CCV1 08/12/14 1:58 99.8C CV MS140723-2 .09995 90 110mg/L.1002

WG369213CC B 1 08/12/14 2:01C C B U -0.0006 0.0006mg/L

WG369213CCV2 08/12/14 2:37 99.3C CV MS140723-2 .09947 90 110mg/L.1002

WG369213CC B 2 08/12/14 2:40C C B U -0.0006 0.0006mg/L

WG369213CCV3 08/12/14 3:04 100.3C CV MS140723-2 .1005 90 110mg/L.1002

WG369213CC B 3 08/12/14 3:07C C B U -0.0006 0.0006mg/L

Page 7 of 32L19607-1408200824


Inorganic QC

Summary




WG368838

WG368838ICV 08/04/14 16:54 99.9IC V II140729-1 1.9982 95 105mg/L2

WG368838IC B 08/04/14 17:00IC B U -0.009 0.009mg/L

WG368838PQV 08/04/14 17:03 93.3PQV II140709-2 .014 70 130mg/L.015

WG368838SIC 08/04/14 17:07 100.9SIC II140707-3 .1009 80 120mg/L.1

WG368838LFB 08/04/14 17:13 100.6LFB II140722-2 .5028 85 115mg/L.5

L19681-03AS 08/04/14 17:34 .023 100.3AS II140722-2 .5247 85 115mg/L.5

L19681-03ASD 08/04/14 17:37 .023 101.6ASD II140722-2 .5309 1.1785 115mg/L 20.5

WG368838CCV1 08/04/14 17:44 98.8C CV II140730-1 .9879 90 110mg/L1

WG368838CC B 1 08/04/14 17:47C C B U -0.009 0.009mg/L

WG368838CCV2 08/04/14 18:21 99.4C CV II140730-1 .9943 90 110mg/L1

WG368838CC B 2 08/04/14 18:24C C B U -0.009 0.009mg/L

WG368838CCV3 08/04/14 18:39 100.4C CV II140730-1 1.004 90 110mg/L1

WG368838CC B 3 08/04/14 18:42C C B U -0.009 0.009mg/L

Boron, dissolv ed M200.7 ICP


WG368838

WG368838ICV 08/04/14 16:54 102.5IC V II140729-1 2.049 95 105mg/L2

WG368838IC B 08/04/14 17:00IC B U -0.03 0.03mg/L

WG368838PQV 08/04/14 17:03 89.9PQV II140709-2 .045 70 130mg/L.05005

WG368838SIC 08/04/14 17:07 93.9SIC II140707-3 .094 80 120mg/L.1001

WG368838LFB 08/04/14 17:13 100.9LFB II140722-2 .505 85 115mg/L.5005

L19681-03AS 08/04/14 17:34 U 103.1AS II140722-2 .516 85 115mg/L.5005

L19681-03ASD 08/04/14 17:37 U 107.5ASD II140722-2 .538 4.1785 115mg/L 20.5005

WG368838CCV1 08/04/14 17:44 101C CV II140730-1 1.01 90 110mg/L1

WG368838CC B 1 08/04/14 17:47C C B U -0.03 0.03mg/L

WG368838CCV2 08/04/14 18:21 102.1C CV II140730-1 1.021 90 110mg/L1

WG368838CC B 2 08/04/14 18:24C C B U -0.03 0.03mg/L

WG368838CCV3 08/04/14 18:39 103.1C CV II140730-1 1.031 90 110mg/L1

WG368838CC B 3 08/04/14 18:42C C B U -0.03 0.03mg/L

Cadmium, dissolv ed M200.8 ICP-MS


WG369213

WG369213ICV 08/12/14 1:22 98.4IC V MS140723-1 .04918 90 110mg/L.05

WG369213IC B 08/12/14 1:25IC B U -0.0003 0.0003mg/L

WG369213LFB 08/12/14 1:28 98LFB MS140728-3 .04912 85 115mg/L.0501

L19601-03AS 08/12/14 1:41 .45 95.7AS MS140728-3 1.4086 70 130mg/L1.002

L19601-03ASD 08/12/14 1:45 .45 95.3ASD MS140728-3 1.4048 0.2770 130mg/L 201.002

WG369213CCV1 08/12/14 1:58 99.3C CV MS140723-2 .0995 90 110mg/L.1002

WG369213CC B 1 08/12/14 2:01C C B U -0.0003 0.0003mg/L

WG369213CCV2 08/12/14 2:37 99.8C CV MS140723-2 .1 90 110mg/L.1002

WG369213CC B 2 08/12/14 2:40C C B U -0.0003 0.0003mg/L

WG369213CCV3 08/12/14 3:04 98C CV MS140723-2 .09822 90 110mg/L.1002

WG369213CC B 3 08/12/14 3:07C C B U -0.0003 0.0003mg/L

Page 8 of 32L19607-1408200824


Inorganic QC

Summary




WG368765

WG368765ICV 08/01/14 19:42 99.8IC V II140729-1 99.8 95 105mg/L100

WG368765IC B 08/01/14 19:48IC B U -0.3 0.3mg/L

WG368765PQV 08/01/14 19:51 108PQV II140709-2 .54 70 130mg/L.5

WG368765SIC 08/01/14 19:54 97.8SIC II140707-2 196.1 1 200mg/L200.5

WG368765LFB 08/01/14 20:00 103.3LFB II140722-2 70.23 85 115mg/L67.99189

L19681-03AS 08/01/14 20:25 25.3 102.2AS II140722-2 94.8 85 115mg/L67.99189

L19681-03ASD 08/01/14 20:28 25.3 100ASD II140722-2 93.31 1.5885 115mg/L 2067.99189

WG368765CCV1 08/01/14 20:31 102.1C CV II140730-1 51.03 90 110mg/L50

WG368765CC B 1 08/01/14 20:34C C B U -0.3 0.3mg/L

WG368765CCV2 08/01/14 21:08 103.2C CV II140730-1 51.61 90 110mg/L50

WG368765CC B 2 08/01/14 21:11C C B U -0.3 0.3mg/L

WG368765CCV3 08/01/14 21:29 103.9C CV II140730-1 51.96 90 110mg/L50

WG368765CC B 3 08/01/14 21:33C C B U -0.3 0.3mg/L



WG358122

WG358122ICV 01/22/14 11:52 102IC V WI131209-3 102 90 110mg/L100

WG358122IC B 01/22/14 11:52IC B U -3 3mg/L

WG368734

WG368734CCV1 07/31/14 17:06 91.8C CV WI140710-1 45.9 90 110mg/L50

WG368734CC B 1 07/31/14 17:06C C B U -3 3mg/L

WG368734PQV 07/31/14 17:06 90PQV WI140731-1 4.5 70 130mg/L5

WG368734LFB 1 07/31/14 17:06 91.6LFB WI140502-2 45.8 90 110mg/L50

L19607-01DUP RA07/31/14 17:06 UDUP U 0mg/L 20

L19607-02AS 07/31/14 17:06 U 96.8AS WI140502-2 48.4 90 110mg/L50

WG368734CCV2 07/31/14 17:06 98C CV WI140710-1 49 90 110mg/L50

WG368734CC B 2 07/31/14 17:06C C B U -3 3mg/L

WG368734CCV3 07/31/14 17:06 99.8C CV WI140710-1 49.9 90 110mg/L50

WG368734CC B 3 07/31/14 17:06C C B U -3 3mg/L

WG368734LFB 2 07/31/14 17:06 97.2LFB WI140502-2 48.6 90 110mg/L50

WG368734CCV4 07/31/14 17:06 98C CV WI140710-1 49 90 110mg/L50

WG368734CC B 4 07/31/14 17:06C C B U -3 3mg/L

WG368734CCV5 07/31/14 17:06 97.8C CV WI140710-1 48.9 90 110mg/L50

WG368734CC B 5 07/31/14 17:06C C B U -3 3mg/L

Page 9 of 32L19607-1408200824


Inorganic QC

Summary




WG369213

WG369213ICV 08/12/14 1:22 101.6IC V MS140723-1 .05079 90 110mg/L.05

WG369213IC B 08/12/14 1:25IC B U -0.0006 0.0006mg/L

WG369213LFB 08/12/14 1:28 102.6LFB MS140728-3 .05129 85 115mg/L.05

L19601-03AS 08/12/14 1:41 .018 104.9AS MS140728-3 1.0668 70 130mg/L1

L19601-03ASD 08/12/14 1:45 .018 104.6ASD MS140728-3 1.0644 0.2370 130mg/L 201

WG369213CCV1 08/12/14 1:58 99.8C CV MS140723-2 .09979 90 110mg/L.1

WG369213CC B 1 08/12/14 2:01C C B U -0.0006 0.0006mg/L

WG369213CCV2 08/12/14 2:37 100.6C CV MS140723-2 .1006 90 110mg/L.1

WG369213CC B 2 08/12/14 2:40C C B U -0.0006 0.0006mg/L

WG369213CCV3 08/12/14 3:04 100C CV MS140723-2 .09996 90 110mg/L.1

WG369213CC B 3 08/12/14 3:07C C B U -0.0006 0.0006mg/L

Chloride SM4500C l-E


WG368912

WG368912IC B 08/05/14 12:20IC B U -1.5 1.5mg/L

WG368912ICV 08/05/14 12:20 103.1IC V WI140701-3 56.68 90 110mg/L55

WG368912CCV1 08/05/14 16:05 105.4C CV WI140730-1 52.71 90 110mg/L50

WG368912CC B 1 08/05/14 16:05C C B U -1.5 1.5mg/L

WG368912LFB 1 08/05/14 16:05 103.2LFB WI140508-1 30.96 90 110mg/L30

L19607-01AS 08/05/14 16:05 36.4 90.6AS WI140508-1 63.57 90 110mg/L30

L19607-02DUP 08/05/14 16:05 22.1DUP 22.13 0.1mg/L 20

WG368912CCV2 08/05/14 16:06 105.5C CV WI140730-1 52.77 90 110mg/L50

WG368912CC B 2 08/05/14 16:06C C B U -1.5 1.5mg/L

WG368912CCV3 08/05/14 16:06 106.6C CV WI140730-1 53.3 90 110mg/L50

WG368912CC B 3 08/05/14 16:06C C B U -1.5 1.5mg/L

WG368912CCV4 08/05/14 16:13 107.9C CV WI140730-1 53.95 90 110mg/L50

WG368912CC B 4 08/05/14 16:13C C B U -1.5 1.5mg/L

WG368912LFB 2 08/05/14 16:14 103.7LFB WI140508-1 31.1 90 110mg/L30

WG368912CCV5 08/05/14 16:15 108.2C CV WI140730-1 54.1 90 110mg/L50

WG368912CC B 5 08/05/14 16:15C C B U -1.5 1.5mg/L

WG368912CCV6 08/05/14 16:16 107.7C CV WI140730-1 53.87 90 110mg/L50

WG368912CC B 6 08/05/14 16:16C C B U -1.5 1.5mg/L

WG368912CCV7 08/05/14 16:22 106.1C CV WI140730-1 53.07 90 110mg/L50

WG368912CC B 7 08/05/14 16:22C C B U -1.5 1.5mg/L

WG368912CCV8 08/05/14 16:25 106.3C CV WI140730-1 53.14 90 110mg/L50

WG368912CC B 8 08/05/14 16:25C C B U -1.5 1.5mg/L

WG368912CCV9 08/05/14 16:38 107.3C CV WI140730-1 53.63 90 110mg/L50

WG368912CC B 9 08/05/14 16:38C C B U -1.5 1.5mg/L

WG368912CCV10 08/05/14 16:39 106.9C CV WI140730-1 53.44 90 110mg/L50

WG368912CC B 10 08/05/14 16:39C C B U -1.5 1.5mg/L

Page 10 of 32L19607-1408200824


Inorganic QC

Summary




WG368838

WG368838ICV 08/04/14 16:54 99.3IC V II140729-1 1.986 95 105mg/L2

WG368838IC B 08/04/14 17:00IC B U -0.03 0.03mg/L

WG368838PQV 08/04/14 17:03 81.8PQV II140709-2 .041 70 130mg/L.0501

WG368838SIC 08/04/14 17:07 89.8SIC II140707-3 .09 80 120mg/L.1002

WG368838LFB 08/04/14 17:13 99.4LFB II140722-2 .498 85 115mg/L.501

L19681-03AS 08/04/14 17:34 U 98.2AS II140722-2 .492 85 115mg/L.501

L19681-03ASD 08/04/14 17:37 U 99.8ASD II140722-2 .5 1.6185 115mg/L 20.501

WG368838CCV1 08/04/14 17:44 98C CV II140730-1 .98 90 110mg/L1

WG368838CC B 1 08/04/14 17:47C C B U -0.03 0.03mg/L

WG368838CCV2 08/04/14 18:21 99.1C CV II140730-1 .991 90 110mg/L1

WG368838CC B 2 08/04/14 18:24C C B U -0.03 0.03mg/L

WG368838CCV3 08/04/14 18:39 99.6C CV II140730-1 .996 90 110mg/L1

WG368838CC B 3 08/04/14 18:42C C B U -0.03 0.03mg/L

Copper, dissolv ed M200.7 ICP


WG368765

WG368765ICV 08/01/14 19:42 99IC V II140729-1 1.98 95 105mg/L2

WG368765IC B 08/01/14 19:48IC B U -0.03 0.03mg/L

WG368765PQV 08/01/14 19:51 84.1PQV II140709-2 .042 70 130mg/L.04995

WG368765SIC 08/01/14 19:54 91.1SIC II140707-2 .091 80 120mg/L.0999

WG368765LFB 08/01/14 20:00 97.5LFB II140722-2 .487 85 115mg/L.4995

L19681-03AS 08/01/14 20:25 .02 98.1AS II140722-2 .51 85 115mg/L.4995

L19681-03ASD 08/01/14 20:28 .02 96.7ASD II140722-2 .503 1.3885 115mg/L 20.4995

WG368765CCV1 08/01/14 20:31 101.1C CV II140730-1 1.011 90 110mg/L1

WG368765CC B 1 08/01/14 20:34C C B U -0.03 0.03mg/L

WG368765CCV2 08/01/14 21:08 102.9C CV II140730-1 1.029 90 110mg/L1

WG368765CC B 2 08/01/14 21:11C C B U -0.03 0.03mg/L

WG368765CCV3 08/01/14 21:29 103.4C CV II140730-1 1.034 90 110mg/L1

WG368765CC B 3 08/01/14 21:33C C B U -0.03 0.03mg/L

Fluoride SM4500F-C


WG368880

WG368880ICV 08/05/14 12:37 94.9IC V WC140801- 1.897 95 105mg/L2

WG368880IC B 08/05/14 12:41IC B .051 -0.15 0.15mg/L

WG368881

WG368881CCV1 08/05/14 15:40 92.3C CV WC140801- 1.846 90 110mg/L2

WG368881CC B 1 08/05/14 15:45C C B U -0.15 0.15mg/L

WG368881LFB 1 08/05/14 15:53 91.5LFB WC140501- 4.589 90 110mg/L5.015

WG368881CCV2 08/05/14 16:40 97C CV WC140801- 1.94 90 110mg/L2

WG368881CC B 2 08/05/14 16:48C C B U -0.15 0.15mg/L

L19602-01AS 08/05/14 17:10 4.04 94.9AS WC140501- 8.801 90 110mg/L5.015

L19602-01DUP 08/05/14 17:18 4.04DUP 4.632 13.7mg/L 20

WG368881CCV3 08/05/14 17:42 98.3C CV WC140801- 1.966 90 110mg/L2

WG368881CC B 3 08/05/14 17:50C C B U -0.15 0.15mg/L

Page 11 of 32L19607-1408200824


Inorganic QC

Summary




WG368765

WG368765ICV 08/01/14 19:42 98.7IC V II140729-1 1.973 95 105mg/L2

WG368765IC B 08/01/14 19:48IC B U -0.06 0.06mg/L

WG368765PQV 08/01/14 19:51 77.9PQV II140709-2 .039 70 130mg/L.05007

WG368765SIC 08/01/14 19:54 95.4SIC II140707-2 191.1 1 200mg/L200.33007

WG368765LFB 08/01/14 20:00 113.7LFB II140722-2 1.139 85 115mg/L1.0014

L19681-03AS 08/01/14 20:25 .04 100.5AS II140722-2 1.046 85 115mg/L1.0014

L19681-03ASD 08/01/14 20:28 .04 100.2ASD II140722-2 1.043 0.2985 115mg/L 201.0014

WG368765CCV1 08/01/14 20:31 100.4C CV II140730-1 1.004 90 110mg/L1

WG368765CC B 1 08/01/14 20:34C C B U -0.06 0.06mg/L

WG368765CCV2 08/01/14 21:08 103.3C CV II140730-1 1.033 90 110mg/L1

WG368765CC B 2 08/01/14 21:11C C B U -0.06 0.06mg/L

WG368765CCV3 08/01/14 21:29 103.4C CV II140730-1 1.034 90 110mg/L1

WG368765CC B 3 08/01/14 21:33C C B U -0.06 0.06mg/L

Lead, dissolv ed M200.8 ICP-MS


WG369213

WG369213ICV 08/12/14 1:22 105.3IC V MS140723-1 .05267 90 110mg/L.05

WG369213IC B 08/12/14 1:25IC B U -0.0003 0.0003mg/L

WG369213LFB 08/12/14 1:28 102.5LFB MS140728-3 .05132 85 115mg/L.05005

L19601-03AS 08/12/14 1:41 U 105.3AS MS140728-3 1.0542 70 130mg/L1.001

L19601-03ASD 08/12/14 1:45 U 105.5ASD MS140728-3 1.0558 0.1570 130mg/L 201.001

WG369213CCV1 08/12/14 1:58 99.2C CV MS140723-2 .2483 90 110mg/L.25025

WG369213CC B 1 08/12/14 2:01C C B .00015 -0.0003 0.0003mg/L

WG369213CCV2 08/12/14 2:37 99.3C CV MS140723-2 .2485 90 110mg/L.25025

WG369213CC B 2 08/12/14 2:40C C B .00014 -0.0003 0.0003mg/L

WG369213CCV3 08/12/14 3:04 99.1C CV MS140723-2 .2479 90 110mg/L.25025

WG369213CC B 3 08/12/14 3:07C C B .00013 -0.0003 0.0003mg/L

Magnesium, dissolv ed M200.7 ICP


WG368765

WG368765ICV 08/01/14 19:42 97.7IC V II140729-1 97.73 95 105mg/L100

WG368765IC B 08/01/14 19:48IC B U -0.6 0.6mg/L

WG368765PQV 08/01/14 19:51 115.9PQV II140709-2 1.16 70 130mg/L1.0007

WG368765SIC 08/01/14 19:54 99.9SIC II140707-2 201 1 200mg/L201.1407

WG368765LFB 08/01/14 20:00 98LFB II140722-2 49.01 85 115mg/L50.00283

L19681-03AS 08/01/14 20:25 10.5 97.1AS II140722-2 59.03 85 115mg/L50.00283

L19681-03ASD 08/01/14 20:28 10.5 95.5ASD II140722-2 58.24 1.3585 115mg/L 2050.00283

WG368765CCV1 08/01/14 20:31 98.2C CV II140730-1 49.1 90 110mg/L50

WG368765CC B 1 08/01/14 20:34C C B .22 -0.6 0.6mg/L

WG368765CCV2 08/01/14 21:08 99.8C CV II140730-1 49.9 90 110mg/L50

WG368765CC B 2 08/01/14 21:11C C B .22 -0.6 0.6mg/L

WG368765CCV3 08/01/14 21:29 99.9C CV II140730-1 49.97 90 110mg/L50

WG368765CC B 3 08/01/14 21:33C C B .24 -0.6 0.6mg/L

Page 12 of 32L19607-1408200824


Inorganic QC

Summary


Manganese, dissolv ed M200.7 ICP


WG368838

WG368838ICV 08/04/14 16:54 100.2IC V II140729-1 2.0045 95 105mg/L2

WG368838IC B 08/04/14 17:00IC B U -0.015 0.015mg/L

WG368838PQV 08/04/14 17:03 72PQV II140709-2 .018 70 130mg/L.025

WG368838SIC 08/04/14 17:07 98.9SIC II140707-3 49.59 1 200mg/L50.125

WG368838LFB 08/04/14 17:13 102.6LFB II140722-2 .514 85 115mg/L.501

L19681-03AS M308/04/14 17:34 11.5 -27.9AS II140722-2 11.36 85 115mg/L.501

L19681-03ASD M308/04/14 17:37 11.5 4ASD II140722-2 11.52 1.485 115mg/L 20.501

WG368838CCV1 08/04/14 17:44 100C CV II140730-1 .9998 90 110mg/L1

WG368838CC B 1 08/04/14 17:47C C B U -0.015 0.015mg/L

WG368838CCV2 08/04/14 18:21 100.6C CV II140730-1 1.006 90 110mg/L1

WG368838CC B 2 08/04/14 18:24C C B U -0.015 0.015mg/L

WG368838CCV3 08/04/14 18:39 101.9C CV II140730-1 1.019 90 110mg/L1

WG368838CC B 3 08/04/14 18:42C C B U -0.015 0.015mg/L

Mercury, dissolv ed M245.1 CVAA


WG368785

WG368785ICV 08/05/14 11:15 99.9IC V II140724-1 .005 90 110mg/L.005005

WG368785IC B 08/05/14 11:17IC B U -0.0006 0.0006mg/L

WG368895

WG368895CCV1 08/05/14 14:53 94.3C CV II140724-1 .00472 90 110mg/L.005005

WG368895CC B 1 08/05/14 14:55C C B U -0.0002 0.0002mg/L

WG368895LRB 08/05/14 14:57LRB U -0.00044 0.00044mg/L

WG368895LFB 08/05/14 14:59 89.9LFB II140715-2 .0018 85 115mg/L.002002

WG368895CCV2 08/05/14 15:19 93.7C CV II140724-1 .00469 90 110mg/L.005005

WG368895CC B 2 08/05/14 15:21C C B U -0.0002 0.0002mg/L

L19717-01LFM 08/05/14 15:44 U 86.4LFM II140715-2 .00173 85 115mg/L.002002

WG368895CCV3 08/05/14 15:47 93.7C CV II140724-1 .00469 90 110mg/L.005005

WG368895CC B 3 08/05/14 15:49C C B U -0.0002 0.0002mg/L


WG368895CCV4 08/05/14 16:06 94.9C CV II140724-1 .00475 90 110mg/L.005005

WG368895CC B 4 08/05/14 16:09C C B U -0.0002 0.0002mg/L

Page 13 of 32L19607-1408200824


Inorganic QC

Summary


Molybdenum, dissolv ed M200.7 ICP


WG368765

WG368765ICV 08/01/14 19:42 103IC V II140729-1 2.06 95 105mg/L2

WG368765IC B 08/01/14 19:48IC B U -0.06 0.06mg/L

WG368765PQV 08/01/14 19:51 92.1PQV II140709-2 .092 70 130mg/L.0999

WG368765SIC 08/01/14 19:54 83.1SIC II140707-2 .083 80 120mg/L.0999

WG368765LFB 08/01/14 20:00 102.7LFB II140722-2 .513 85 115mg/L.4995

L19681-03AS 08/01/14 20:25 U 100.7AS II140722-2 .503 85 115mg/L.4995

L19681-03ASD 08/01/14 20:28 U 99.1ASD II140722-2 .495 1.685 115mg/L 20.4995

WG368765CCV1 08/01/14 20:31 105.2C CV II140730-1 1.052 90 110mg/L1

WG368765CC B 1 08/01/14 20:34C C B U -0.06 0.06mg/L

WG368765CCV2 08/01/14 21:08 106.4C CV II140730-1 1.064 90 110mg/L1

WG368765CC B 2 08/01/14 21:11C C B U -0.06 0.06mg/L

WG368765CCV3 08/01/14 21:29 106.4C CV II140730-1 1.064 90 110mg/L1

WG368765CC B 3 08/01/14 21:33C C B U -0.06 0.06mg/L

Nickel, dissolv ed M200.7 ICP


WG368765

WG368765ICV 08/01/14 19:42 98.6IC V II140729-1 1.9712 95 105mg/L2

WG368765IC B 08/01/14 19:48IC B U -0.024 0.024mg/L

WG368765PQV 08/01/14 19:51 94PQV II140709-2 .0377 70 130mg/L.04012

WG368765SIC 08/01/14 19:54 100.7SIC II140707-2 .101 80 120mg/L.1003

WG368765LFB 08/01/14 20:00 100.8LFB II140722-2 .5057 85 115mg/L.5015

L19681-03AS 08/01/14 20:25 .108 99.1AS II140722-2 .6052 85 115mg/L.5015

L19681-03ASD 08/01/14 20:28 .108 96.6ASD II140722-2 .5922 2.1785 115mg/L 20.5015

WG368765CCV1 08/01/14 20:31 101C CV II140730-1 1.01 90 110mg/L1

WG368765CC B 1 08/01/14 20:34C C B U -0.024 0.024mg/L

WG368765CCV2 08/01/14 21:08 102.3C CV II140730-1 1.023 90 110mg/L1

WG368765CC B 2 08/01/14 21:11C C B U -0.024 0.024mg/L

WG368765CCV3 08/01/14 21:29 102.6C CV II140730-1 1.026 90 110mg/L1

WG368765CC B 3 08/01/14 21:33C C B U -0.024 0.024mg/L

Page 14 of 32L19607-1408200824


Inorganic QC

Summary




WG369095

WG369095ICV 08/07/14 22:14 103.4IC V WI140718-9 2.498 90 110mg/L2.416

WG369095IC B 08/07/14 22:15IC B U -0.06 0.06mg/L

WG369096

WG369096CCV1 08/07/14 23:04 101.1C CV WI140806-3 2.021 90 110mg/L2

WG369096CC B 1 08/07/14 23:06C C B U -0.06 0.06mg/L

WG369096LFB 1 08/07/14 23:07 99.1LFB WI140719-4 1.981 90 110mg/L2

WG369096CCV2 08/07/14 23:19 100.6C CV WI140806-3 2.011 90 110mg/L2

WG369096CC B 2 08/07/14 23:20C C B U -0.06 0.06mg/L

L19602-03AS 08/07/14 23:26 U 100.7AS WI140719-4 2.014 90 110mg/L2

L19602-04DUP RA08/07/14 23:28 .05DUP .043 15.1mg/L 20

WG369096CCV3 08/07/14 23:33 101C CV WI140806-3 2.02 90 110mg/L2

WG369096CC B 3 08/07/14 23:34C C B U -0.06 0.06mg/L

WG369096LFB 2 08/07/14 23:41 99.5LFB WI140719-4 1.99 90 110mg/L2

WG369096CCV4 08/07/14 23:47 99.9C CV WI140806-3 1.997 90 110mg/L2

WG369096CC B 4 08/07/14 23:48C C B U -0.06 0.06mg/L

WG369096CCV5 08/08/14 0:02 101.4C CV WI140806-3 2.027 90 110mg/L2

WG369096CC B 5 08/08/14 0:04C C B U -0.06 0.06mg/L



WG368897

WG368897ICV 08/05/14 12:20 102.9IC V WI131021-1 1.032 90 110mg/L1.003

WG368897IC B 08/05/14 12:23IC B U -0.15 0.15mg/L

WG368918

WG368918CCV1 08/05/14 14:00 103.5C CV WI140113-6 2.07 90 110mg/L2

WG368918CC B 1 08/05/14 14:01C C B U -0.15 0.15mg/L

WG368918CCV2 08/05/14 14:13 102.2C CV WI140113-6 2.044 90 110mg/L2

WG368918CC B 2 08/05/14 14:15C C B U -0.15 0.15mg/L

L19601-04AS 08/05/14 14:20 .8 101.8AS WI140113-8 1.818 90 110mg/L1

L19602-01DUP RA08/05/14 14:22 .22DUP .226 2.7mg/L 20

WG368918CCV3 08/05/14 14:26 105.3C CV WI140113-6 2.105 90 110mg/L2

WG368918CC B 3 08/05/14 14:28C C B U -0.15 0.15mg/L

WG368918LFB 2 08/05/14 14:34 95LFB WI140113-8 .95 90 110mg/L1

WG368918CCV4 08/05/14 14:40 104.1C CV WI140113-6 2.082 90 110mg/L2

WG368918CC B 4 08/05/14 14:41C C B U -0.15 0.15mg/L

WG368918LFB 1 08/05/14 14:51 95.6LFB WI140113-8 .956 90 110mg/L1

WG368918CCV5 08/05/14 14:54 104C CV WI140113-6 2.079 90 110mg/L2

WG368918CC B 5 08/05/14 14:55C C B U -0.15 0.15mg/L

WG368918CCV6 08/05/14 15:09 102.2C CV WI140113-6 2.043 90 110mg/L2

WG368918CC B 6 08/05/14 15:10C C B U -0.15 0.15mg/L

WG368918CCV7 08/05/14 15:15 102.3C CV WI140113-6 2.045 90 110mg/L2

WG368918CC B 7 08/05/14 15:16C C B U -0.15 0.15mg/L

Page 15 of 32L19607-1408200824


Inorganic QC

Summary




WG368765

WG368765ICV 08/01/14 19:42 99.6ICV II140729-1 19.91 95 105mg/L20

WG368765ICB 08/01/14 19:48ICB U -0.6 0.6mg/L

WG368765PQV 08/01/14 19:51 110PQV II140709-2 1.1 70 130mg/L1

WG368765SIC 08/01/14 19:54 108SIC II140707-2 1.08 80 120mg/L1

WG368765LFB 08/01/14 20:00 100.3LFB II140722-2 98.38 85 115mg/L98.07852

L19681-03AS 08/01/14 20:25 4.4 99.2AS II140722-2 101.7 85 115mg/L98.07852

L19681-03ASD 08/01/14 20:28 4.4 98ASD II140722-2 100.5 1.1985 115mg/L 2098.07852

WG368765CCV1 08/01/14 20:31 100.9CCV II140730-1 10.09 90 110mg/L10

WG368765CCB1 08/01/14 20:34CCB U -0.6 0.6mg/L

WG368765CCV2 08/01/14 21:08 102.2CCV II140730-1 10.22 90 110mg/L10

WG368765CCB2 08/01/14 21:11CCB U -0.6 0.6mg/L

WG368765CCV3 08/01/14 21:29 102.9CCV II140730-1 10.29 90 110mg/L10

WG368765CCB3 08/01/14 21:33CCB U -0.6 0.6mg/L



WG368154

WG368154PBW 07/23/14 14:20PBW U -20 20mg/L


L19614-02DUP 07/23/14 14:59 720DUP 730 1.4mg/L 10



WG368178

WG368178PBW 07/23/14 16:22PBW U -15 15mg/L


L19610-02DUP RA07/23/14 16:58 5DUP 5 0mg/L 10



WG369213

WG369213ICV 08/12/14 1:22 101.2ICV MS140723-1 .05059 90 110mg/L.05

WG369213ICB 08/12/14 1:25ICB U -0.0003 0.0003mg/L

WG369213LFB 08/12/14 1:28 99.7LFB MS140728-3 .05 85 115mg/L.05015

L19601-03AS 08/12/14 1:41 .029 104.5AS MS140728-3 1.0768 70 130mg/L1.003

L19601-03ASD 08/12/14 1:45 .029 104.9ASD MS140728-3 1.0816 0.4470 130mg/L 201.003

WG369213CCV1 08/12/14 1:58 101.1CCV MS140723-2 .2535 90 110mg/L.25075

WG369213CCB1 08/12/14 2:01CCB .00015 -0.0003 0.0003mg/L

WG369213CCV2 08/12/14 2:37 100.3CCV MS140723-2 .2516 90 110mg/L.25075

WG369213CCB2 08/12/14 2:40CCB .00017 -0.0003 0.0003mg/L

WG369213CCV3 08/12/14 3:04 100.3CCV MS140723-2 .2514 90 110mg/L.25075

WG369213CCB3 08/12/14 3:07CCB .00015 -0.0003 0.0003mg/L

Page 16 of 32L19607-1408200824


Inorganic QC

Summary




WG368885

WG368885ICV 08/05/14 10:27 97.7ICV II140729-1 41.8 95 105mg/L42.8

WG368885ICB 08/05/14 10:33ICB U -0.6 0.6mg/L

WG368885PQV 08/05/14 10:36 98.9PQV II140709-2 1.06 70 130mg/L1.0714

WG368885SIC 08/05/14 10:39 91.5SIC II140707-3 .98 80 120mg/L1.0714

WG368885LFB 08/05/14 10:46 100.1LFB II140722-2 21.45 85 115mg/L21.428

L19611-02AS 08/05/14 11:01 8.2 99.7AS II140722-2 29.56 85 115mg/L21.428

L19611-02ASD 08/05/14 11:05 8.2 99.4ASD II140722-2 29.51 0.1785 115mg/L 2021.428

WG368885CCV1 08/05/14 11:17 99CCV II140730-1 21.18 90 110mg/L21.4

WG368885CCB1 08/05/14 11:20CCB U -0.6 0.6mg/L

WG368885CCV2 08/05/14 11:52 95.8CCV II140730-1 20.5 90 110mg/L21.4

WG368885CCB2 08/05/14 11:55CCB U -0.6 0.6mg/L

Sodium, dissolv ed M200.7 ICP


WG368765

WG368765ICV 08/01/14 19:42 98.7ICV II140729-1 98.72 95 105mg/L100

WG368765ICB 08/01/14 19:48ICB U -0.6 0.6mg/L

WG368765PQV 08/01/14 19:51 99.9PQV II140709-2 1 70 130mg/L1.001

WG368765SIC 08/01/14 19:54 101.9SIC II140707-2 1.02 80 120mg/L1.001

WG368765LFB 08/01/14 20:00 98.2LFB II140722-2 98.3 85 115mg/L100.0589

L19681-03AS 08/01/14 20:25 2.4 97.5AS II140722-2 99.93 85 115mg/L100.0589

L19681-03ASD 08/01/14 20:28 2.4 96.5ASD II140722-2 98.92 1.0285 115mg/L 20100.0589

WG368765CCV1 08/01/14 20:31 99.8CCV II140730-1 49.92 90 110mg/L50

WG368765CCB1 08/01/14 20:34CCB U -0.6 0.6mg/L

WG368765CCV2 08/01/14 21:08 101.9CCV II140730-1 50.97 90 110mg/L50

WG368765CCB2 08/01/14 21:11CCB U -0.6 0.6mg/L

WG368765CCV3 08/01/14 21:29 101.9CCV II140730-1 50.95 90 110mg/L50

WG368765CCB3 08/01/14 21:33CCB U -0.6 0.6mg/L



WG368368

WG368368PBW 07/28/14 8:55PBW U -30 30mg/L


L19619-02DUP 07/28/14 12:00 170DUP 174 2.3mg/L 20

Page 17 of 32L19607-1408200824


Inorganic QC

Summary




WG368123

WG368123ICV 07/23/14 10:10 91.8ICV WC140723- .284 90 110mg/L.30934

WG368123ICB 07/23/14 10:15ICB U -0.06 0.06mg/L

WG368162

WG368162CCV1 07/23/14 14:37 94.4CCV WC140723- .163 90 110mg/L.17267

WG368162CCB1 07/23/14 14:40CCB U -0.06 0.06mg/L

WG368162LFB 07/23/14 14:43 111.6LFB WC140723- .257 80 120mg/L.2302267

L19572-13AS 07/23/14 14:50 U 119AS WC140723- .411 75 125mg/L.34534005

L19572-13DUP RA07/23/14 14:54 UDUP U 0mg/L 20

WG368162CCV2 07/23/14 15:17 93.8CCV WC140723- .162 90 110mg/L.17267

WG368162CCB2 07/23/14 15:21CCB U -0.06 0.06mg/L

L19607-02AS 07/23/14 15:34 U 110.3AS WC140723- .254 75 125mg/L.2302267

L19607-02DUP RA07/23/14 15:38 UDUP U 0mg/L 20

WG368162CCV3 07/23/14 15:58 92.7CCV WC140723- .16 90 110mg/L.17267

WG368162CCB3 07/23/14 16:02CCB U -0.06 0.06mg/L

WG368162CCV4 07/23/14 16:15 91.5CCV WC140723- .158 90 110mg/L.17267

WG368162CCB4 07/23/14 16:19CCB U -0.06 0.06mg/L



WG369213

WG369213ICV 08/12/14 1:22 103ICV MS140723-1 .05149 90 110mg/L.05

WG369213ICB 08/12/14 1:25ICB U -0.0003 0.0003mg/L

WG369213LFB 08/12/14 1:28 102.6LFB MS140728-3 .05136 85 115mg/L.05005

L19601-03AS 08/12/14 1:41 3.46 112.1AS MS140728-3 4.582 70 130mg/L1.001

L19601-03ASD 08/12/14 1:45 3.46 106.7ASD MS140728-3 4.528 1.1970 130mg/L 201.001

WG369213CCV1 08/12/14 1:58 100.3CCV MS140723-2 .1004 90 110mg/L.1001

WG369213CCB1 08/12/14 2:01CCB U -0.0003 0.0003mg/L

WG369213CCV2 08/12/14 2:37 100CCV MS140723-2 .1001 90 110mg/L.1001

WG369213CCB2 08/12/14 2:40CCB U -0.0003 0.0003mg/L



WG368765

WG368765ICV 08/01/14 19:42 101.1ICV II140729-1 2.0222 95 105mg/L2

WG368765ICB 08/01/14 19:48ICB U -0.015 0.015mg/L

WG368765PQV 08/01/14 19:51 86PQV II140709-2 .0215 70 130mg/L.025

WG368765SIC 08/01/14 19:54 91.8SIC II140707-2 .0918 80 120mg/L.1

WG368765LFB 08/01/14 20:00 102.9LFB II140722-2 .5144 85 115mg/L.5

L19681-03AS 08/01/14 20:25 U 102.3AS II140722-2 .5113 85 115mg/L.5

L19681-03ASD 08/01/14 20:28 U 100.5ASD II140722-2 .5025 1.7485 115mg/L 20.5

WG368765CCV1 08/01/14 20:31 103.4CCV II140730-1 1.034 90 110mg/L1

WG368765CCB1 08/01/14 20:34CCB U -0.015 0.015mg/L

WG368765CCV2 08/01/14 21:08 105.6CCV II140730-1 1.056 90 110mg/L1

WG368765CCB2 08/01/14 21:11CCB U -0.015 0.015mg/L

WG368765CCV3 08/01/14 21:29 105.7CCV II140730-1 1.057 90 110mg/L1

WG368765CCB3 08/01/14 21:33CCB U -0.015 0.015mg/L

Page 18 of 32L19607-1408200824


Inorganic QC

Summary




WG368765

WG368765ICV 08/01/14 19:42 97.7ICV II140729-1 1.954 95 105mg/L2

WG368765ICB 08/01/14 19:48ICB U -0.03 0.03mg/L

WG368765PQV 08/01/14 19:51 81.9PQV II140709-2 .041 70 130mg/L.05005

WG368765SIC 08/01/14 19:54 88SIC II140707-2 .088 80 120mg/L.10005

WG368765LFB 08/01/14 20:00 99.9LFB II140722-2 .5 85 115mg/L.5005

L19681-03AS 08/01/14 20:25 .46 95.9AS II140722-2 .94 85 115mg/L.5005

L19681-03ASD 08/01/14 20:28 .46 93.1ASD II140722-2 .926 1.585 115mg/L 20.5005

WG368765CCV1 08/01/14 20:31 101.5CCV II140730-1 1.015 90 110mg/L1

WG368765CCB1 08/01/14 20:34CCB U -0.03 0.03mg/L

WG368765CCV2 08/01/14 21:08 102.8CCV II140730-1 1.028 90 110mg/L1

WG368765CCB2 08/01/14 21:11CCB U -0.03 0.03mg/L

WG368765CCV3 08/01/14 21:29 102.6CCV II140730-1 1.026 90 110mg/L1

WG368765CCB3 08/01/14 21:33CCB U -0.03 0.03mg/L

Page 19 of 32L19607-1408200824


Inorganic Extended

Qualifier Report




M200.7 ICPManganese, dissolvedL19607-01 WG368838












M200.7 ICPManganese, dissolvedL19607-02 WG368838




validation because the sample concentration is too low for accurate evaluation (< 10x MDL).









REPAD.15.06.05.01

Page 20 of 32L19607-1408200824





Project ID:


Date Sampled: 07/21/14 10:30


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 12 5.4 3.3 pCi/L * bsg08/07/14 0:10

Gross Beta 11 5.2 7 pCi/L bsg08/07/14 0:10

Lead 210, dissolved

EICHROM, OTW01

Prep Method:


Lead 210, dissolved 18 3 8.9 pCi/L * thf08/19/14 12:23


M903.1

Prep Method:




M904.0

Prep Method:




ESM 4506

Prep Method:




Page 21 of 32L19607-1408200824


Sample ID: BLM WELL



Project ID:


Date Sampled: 07/21/14 11:20


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 15 6.5 3.6 pCi/L * bsg08/07/14 0:11


Lead 210, dissolved

EICHROM, OTW01

Prep Method:


Lead 210, dissolved 4.7 2.5 8.2 pCi/L * thf08/19/14 12:23


M903.1

Prep Method:




M904.0

Prep Method:




ESM 4506

Prep Method:




Page 22 of 32L19607-1408200824

















QC Sample Types














D ASTM

RP DOE

ESM DOE/ESM

Comments




(4) An asterisk in the "XQ" column indicates there is an extended q ualifier and/or certification

q ualifier associated with the result.

For a complete list of ACZ's Extended Qualifiers, please click: http://www.acz.com/public/extq uallist.pdf

REP003.09.12.01

Radiochemistry

Reference

Page 23 of 32L19607-1408200824


Radiochemistry QC

Summary


Alpha M900.0


pCi/L

Error LLDLLD

Units:

WG369094

WG368943PBW 08/07/14PBW 0 31.7 1.5

WG368943LCSWA 08/07/14 120LCSW PCN45469 120100 83 1339.8 1.5

L19686-01DUP 08/07/14 0.33DUP-RER .22 22 0.042.1 21.9

L19686-02MSA M208/07/14 0 47MS PCN45469 47100 83 1337.92.4 2.42.4

Beta M900.0


pCi/L

Error LLDLLD

Units:

WG369094

WG368943PBW 08/07/14PBW .77 9.43.4 4.7

WG368943LCSWB 08/07/14 120LCSW PCN44710 120100 70 1297.4 4.4

L19686-01DUP 08/07/14 5.2DUP-RER 3.7 23.7 0.293.5 4.84.7

L19686-03MSB 08/07/14 0.58 119.4MS PCN44710 120100 70 12983 4.94.9



pCi/L

Error LLDLLD

Units:

WG369720

L19607-01DUP RM08/19/14 18DUP-RER 1.3 22.6 4.213 8.78.9

L19607-01MS 08/19/14 18 69.8MS PCN44108 8697.48 55 1214.33 9.58.9

WG369387LCSW 08/19/14 112.8LCSW PCN44108 11097.48 55 1214.3 8

WG369387PBW 08/19/14PBW 11 172.8 8.5

Page 24 of 32L19607-1408200824


Radiochemistry QC

Summary




pCi/L

Error LLDLLD

Units:

WG369245

WG368801PBW 08/11/14PBW .13 0.520.11 0.26

WG368801LCSW 08/11/14 85LCSW PCN45814 1720 43 1480.49 0.07

L19607-01DUP 08/11/14 0.09DUP-RER .13 20.08 0.350.08 0.250.17

L19674-04MS M308/11/14 650 -807.5MS PCN45814 48021.05 43 1482.53.4 0.120.23



pCi/L

Error LLDLLD

Units:

WG369125

WG368831LCSW 08/07/14 76.3LCSW PCN46178 1519.66 47 1231.2 0.51

WG368831PBW 08/07/14PBW .16 0.640.31 0.32

L19625-01MS 08/07/14 0.69 57.5MS PCN46178 1219.66 47 1231.10.64 0.570.63

L19722-02DUP 08/07/14 1.6DUP-RER 1.8 20.61 0.250.5 0.520.42

L19600-01DUP 08/07/14 2.7DUP-RER 3.2 20.62 0.570.62 0.440.46



pCi/L

Error LLDLLD

Units:

WG369523

WG369161PBW 08/14/14PBW .35 1.180.3 0.59

WG369161LCSW 08/14/14 92.5LCSW RC140811-1 150162.12 91 1263.9 0.53

L19607-01DUP 08/14/14 -0.06DUP-RER .19 20.27 0.620.3 0.540.61

L19607-02MS 08/14/14 0.14 92.4MS RC140811-1 150162.12 91 1264.20.31 0.590.56

Page 25 of 32L19607-1408200824


Radiochemistry QC

Summary


Alpha M900.0


pCi/L

Error LLDLLD

Units:

WG369094

WG368943PBW 08/07/14PBW 0 31.7 1.5

WG368943LCSWA 08/07/14 120LCSW PCN45469 120100 83 1339.8 1.5

L19686-01DUP 08/07/14 0.33DUP-RER .22 22 0.042.1 21.9

L19686-02MSA M208/07/14 0 47MS PCN45469 47100 83 1337.92.4 2.42.4

Beta M900.0


pCi/L

Error LLDLLD

Units:

WG369094

WG368943PBW 08/07/14PBW .77 9.43.4 4.7

WG368943LCSWB 08/07/14 120LCSW PCN44710 120100 70 1297.4 4.4

L19686-01DUP 08/07/14 5.2DUP-RER 3.7 23.7 0.293.5 4.84.7

L19686-03MSB 08/07/14 0.58 119.4MS PCN44710 120100 70 12983 4.94.9



pCi/L

Error LLDLLD

Units:

WG369720

L19607-01DUP RM08/19/14 18DUP-RER 1.3 22.6 4.213 8.78.9

L19607-01MS 08/19/14 18 69.8MS PCN44108 8697.48 55 1214.33 9.58.9

WG369387LCSW 08/19/14 112.8LCSW PCN44108 11097.48 55 1214.3 8

WG369387PBW 08/19/14PBW 11 172.8 8.5

Page 26 of 32L19607-1408200824


Radiochemistry QC

Summary




pCi/L

Error LLDLLD

Units:

WG369245

WG368801PBW 08/11/14PBW .13 0.520.11 0.26

WG368801LCSW 08/11/14 85LCSW PCN45814 1720 43 1480.49 0.07

L19607-01DUP 08/11/14 0.09DUP-RER .13 20.08 0.350.08 0.250.17

L19663-06DUP 08/11/14 70DUP-RPD 59 2011.2 0.220.14 17.1

L19663-06DUP RN08/11/14 70DUP-RER 59 21 7.041.2 0.220.14

L19674-04MS M308/11/14 650 -807.5MS PCN45814 48021.05 43 1482.53.4 0.120.23



pCi/L

Error LLDLLD

Units:

WG369125

WG368831LCSW 08/07/14 76.3LCSW PCN46178 1519.66 47 1231.2 0.51

WG368831PBW 08/07/14PBW .16 0.640.31 0.32

L19625-01MS 08/07/14 0.69 57.5MS PCN46178 1219.66 47 1231.10.64 0.570.63

L19722-02DUP 08/07/14 1.6DUP-RER 1.8 20.61 0.250.5 0.520.42

L19600-01DUP 08/07/14 2.7DUP-RER 3.2 20.62 0.570.62 0.440.46



pCi/L

Error LLDLLD

Units:

WG369523

WG369161PBW 08/14/14PBW .35 1.180.3 0.59

WG369161LCSW 08/14/14 92.5LCSW RC140811-1 150162.12 91 1263.9 0.53

L19607-01DUP 08/14/14 -0.06DUP-RER .19 20.27 0.620.3 0.540.61

L19607-02MS 08/14/14 0.14 92.4MS RC140811-1 150162.12 91 1264.20.31 0.590.56

Page 27 of 32L19607-1408200824


Certification

Qualifiers


Metals Analysis



Radiochemistry




Wet Chemistry



REPAD.05.06.05.01

Page 28 of 32L19607-1408200824


Sample

Receipt


Date Received:

Received By: mtb

07/23/2014 10:20

L19607




The 'Relinquished By' field on the COC was not completed. Left a message for Kathy Weinel on 7/23/14.

NANOYES

X

X

X

X

X

X









NANOYES

X

X

X

X

X

X

X












Samples/Containers

X

X

X

Shipping Containers


Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- --------------------NA20087 0.8 8 Yes

X



REPAD LPII 2012-03

Page 29 of 32L19607-1408200824


Sample

Receipt


Date Received:

Received By: mtb

07/23/2014 10:20

L19607


REPAD LPII 2012-03

Page 30 of 32L19607-1408200824

of 32L19607-1408200824


Analytical

Report

Western Water and Land Inc.

743 Horizon Court

Grand Junction, CO 81506


Bruce Smith:

Enclosed are the analytical results for sample(s) submitted to ACZ Laboratories, Inc. (ACZ) on December 11, 2014. This project has been assigned to ACZ's project number, L21970. Please reference this number in all future inquiries.




All samples and sub-samples associated with this project will be disposed of after October 04, 2017. If the samples are determined to be hazardous, additional charges apply for disposal (typically $11/sample). If you would like the samples to be held longer than ACZ's stated policy or to be returned, please contact your Project Manager or Customer Service Representative for further details and associated costs. ACZ retains analytical raw data reports for ten years.


Bruce Smith

January 09, 2015

Project ID:


743 Horizon Court

Grand Junction, CO 81506

Bruce Smith

Report to: Bill to:

Suite 330 Suite 330

Page 1 of 28L21970-1501091534



Sample Matrix: Surface Water


Project ID:



Results

Date Sampled: 12/10/14 12:30



Metals Analysis

XQDilution


Arsenic, dissolved M200.8 ICP-MS 0.0081 mg/L 0.001 pmc0.0002 12/18/14 6:081

Barium, dissolved M200.7 ICP 0.020 mg/L 0.02 aeb0.003 12/15/14 14:121


Cadmium, dissolved M200.8 ICP-MS mg/L 0.0005U pmc0.0001 12/18/14 6:081


Cesium, dissolved M200.8 ICP-MS mg/L 0.001U pmc0.0002* 12/18/14 6:081



Iron, dissolved M200.7 ICP 0.03 mg/L 0.05B aeb0.02 12/15/14 14:121

Lead, dissolved M200.8 ICP-MS mg/L 0.0005U pmc0.0001 12/18/14 6:081







Selenium, dissolved M200.8 ICP-MS 0.0219 mg/L 0.0003 pmc0.0001 12/18/14 6:081



Uranium, dissolved M200.8 ICP-MS 0.0598 mg/L 0.0005 pmc0.0001 12/18/14 6:081




Page 2 of 28L21970-1501091534





Project ID:



Results

Date Sampled: 12/10/14 12:30



Wet Chemistry

XQDilution



251 mg/L 20 id2 12/13/14 0:001

Carbonate as CaCO3 mg/L 20U id2 12/13/14 0:001

Hydroxide as CaCO3 mg/L 20U id2 12/13/14 0:001

Total Alkalinity 251 mg/L 20 id2 12/13/14 0:001


SM5310B mg/L 5U jlf1* 12/15/14 15:451





Chloride SM4500Cl-E 56.1 mg/L 2 bsu0.5* 12/22/14 16:581

Fluoride SM4500F-C 0.45 mg/L 0.3 enb0.05 12/17/14 12:221


Nitrogen, ammonia M350.1 - Automated Phenate mg/L 0.2U tcd0.05* 12/22/14 12:441


SM2540C 622 mg/L 20 enb10 12/16/14 9:191


SM2540D mg/L 20U abd5* 12/16/14 13:471


Sulfide as S SM4500S2-D mg/L 0.4U eaa0.08* 12/17/14 11:553.75






Page 3 of 28L21970-1501091534


Sample ID: STONE SPRING-SULFIDE BLANK



Project ID:



Results

Date Sampled: 12/10/14 12:30



Wet Chemistry

XQDilution

Sulfide as S SM4500S2-D mg/L 0.4U eaa0.08* 12/17/14 12:033.75



Page 4 of 28L21970-1501091534















QC Sample Types
























Method References






Comments




(4) An asterisk in the "XQ" column indicates there is an extended q ualifier and/or certification q ualifier


(5) If the MDL eq uals the PQL or the MDL column is omitted, the PQL is the reporting limit.


REP001.09.12.01

Inorganic

Reference

Page 5 of 28L21970-1501091534


Inorganic QC

Summary

ACZ Project ID: L21970Western Water and Land Inc.



WG376013

WG376013PBW1 12/12/14 14:13PBW 8.1 -20 20mg/L

WG376013LCSW3 12/12/14 14:29 90LCSW WC141204-1 735 90 110mg/L820


WG376013PBW2 12/12/14 18:13PBW U -20 20mg/L


WG376013PBW3 12/12/14 21:42PBW U -20 20mg/L


WG376013PBW4 12/13/14 2:54PBW U -20 20mg/L

L21970-01DUP 12/13/14 5:54 251DUP 250 0mg/L 20




WG376073

WG376073ICV 12/15/14 12:22 101ICV II141125-1 2.014 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.09 0.09mg/L

WG376073PQV 12/15/14 12:31 101PQV II141201-5 .151 70 130mg/L.150225

WG376073SIC 12/15/14 12:35 103SIC II141201-6 207.2 1 200mg/L200.450225

WG376073LFB 12/15/14 12:41 106LFB II141126-2 1.063 85 115mg/L1.0015

WG376073CCV1 12/15/14 13:13 102CCV II141211-3 1.018 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.09 0.09mg/L

L21922-01AS 12/15/14 13:36 U 111AS II141126-2 1.112 85 115mg/L1.0015

L21922-01ASD 12/15/14 13:39 U 109ASD II141126-2 1.093 285 115mg/L 201.0015

WG376073CCV2 12/15/14 13:52 101CCV II141211-3 1.014 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.09 0.09mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 1.008 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.09 0.09mg/L



WG376320

WG376320ICV 12/18/14 5:58 100ICV MS141027-2 .05004 90 110mg/L.05

WG376320ICB 12/18/14 6:01ICB U -0.0006 0.0006mg/L

WG376320LFB 12/18/14 6:05 93LFB MS141118-9 .04645 85 115mg/L.0501

L22029-01AS 12/18/14 6:18 .0004 99AS MS141118-9 .04992 70 130mg/L.0501

L22029-01ASD 12/18/14 6:21 .0004 99ASD MS141118-9 .04988 070 130mg/L 20.0501

WG376320CCV1 12/18/14 6:36 99CCV MS141205-5 .09882 90 110mg/L.1002

WG376320CCB1 12/18/14 6:40CCB U -0.0006 0.0006mg/L

WG376320CCV2 12/18/14 7:15 98CCV MS141205-5 .09777 90 110mg/L.1002

WG376320CCB2 12/18/14 7:18CCB U -0.0006 0.0006mg/L

WG376320CCV3 12/18/14 7:37 98CCV MS141205-5 .09817 90 110mg/L.1002

WG376320CCB3 12/18/14 7:40CCB U -0.0006 0.0006mg/L

Page 6 of 28L21970-1501091534


Inorganic QC

Summary




WG376073

WG376073ICV 12/15/14 12:22 98ICV II141125-1 1.9672 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.009 0.009mg/L

WG376073PQV 12/15/14 12:31 99PQV II141201-5 .0148 70 130mg/L.015

WG376073SIC 12/15/14 12:35 102SIC II141201-6 .1015 80 120mg/L.1

WG376073LFB 12/15/14 12:41 101LFB II141126-2 .5064 85 115mg/L.5

WG376073CCV1 12/15/14 13:13 101CCV II141211-3 1.008 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.009 0.009mg/L

L21922-01AS 12/15/14 13:36 .009 102AS II141126-2 .5177 85 115mg/L.5

L21922-01ASD 12/15/14 13:39 .009 101ASD II141126-2 .5158 085 115mg/L 20.5

WG376073CCV2 12/15/14 13:52 101CCV II141211-3 1.011 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.009 0.009mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 1.009 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.009 0.009mg/L



WG376073

WG376073ICV 12/15/14 12:22 103ICV II141125-1 2.051 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.03 0.03mg/L

WG376073PQV 12/15/14 12:31 106PQV II141201-5 .053 70 130mg/L.05005

WG376073SIC 12/15/14 12:35 93SIC II141201-6 .093 80 120mg/L.1001

WG376073LFB 12/15/14 12:41 105LFB II141126-2 .525 85 115mg/L.5005

WG376073CCV1 12/15/14 13:13 101CCV II141211-3 1.014 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.03 0.03mg/L

L21922-01AS 12/15/14 13:36 U 103AS II141126-2 .517 85 115mg/L.5005

L21922-01ASD 12/15/14 13:39 U 103ASD II141126-2 .516 085 115mg/L 20.5005

WG376073CCV2 12/15/14 13:52 101CCV II141211-3 1.01 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.03 0.03mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 1.012 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.03 0.03mg/L



WG376320

WG376320ICV 12/18/14 5:58 98ICV MS141027-2 .04881 90 110mg/L.05

WG376320ICB 12/18/14 6:01ICB U -0.0003 0.0003mg/L

WG376320LFB 12/18/14 6:05 94LFB MS141118-9 .04691 85 115mg/L.0501

L22029-01AS 12/18/14 6:18 U 95AS MS141118-9 .04754 70 130mg/L.0501

L22029-01ASD 12/18/14 6:21 U 95ASD MS141118-9 .0477 070 130mg/L 20.0501

WG376320CCV1 12/18/14 6:36 98CCV MS141205-5 .09788 90 110mg/L.1002

WG376320CCB1 12/18/14 6:40CCB U -0.0003 0.0003mg/L

WG376320CCV2 12/18/14 7:15 98CCV MS141205-5 .09815 90 110mg/L.1002

WG376320CCB2 12/18/14 7:18CCB U -0.0003 0.0003mg/L

WG376320CCV3 12/18/14 7:37 98CCV MS141205-5 .09857 90 110mg/L.1002

WG376320CCB3 12/18/14 7:40CCB U -0.0003 0.0003mg/L

Page 7 of 28L21970-1501091534


Inorganic QC

Summary




WG376073

WG376073ICV 12/15/14 12:22 99ICV II141125-1 99.48 95 105mg/L100

WG376073ICB 12/15/14 12:28ICB U -0.3 0.3mg/L

WG376073PQV 12/15/14 12:31 100PQV II141201-5 .5 70 130mg/L.5

WG376073SIC 12/15/14 12:35 98SIC II141201-6 195.9 1 200mg/L200.5

WG376073LFB 12/15/14 12:41 106LFB II141126-2 71.87 85 115mg/L67.99189

WG376073CCV1 12/15/14 13:13 103CCV II141211-3 51.58 90 110mg/L50

WG376073CCB1 12/15/14 13:16CCB U -0.3 0.3mg/L

L21922-01AS 12/15/14 13:36 5.7 108AS II141126-2 79.23 85 115mg/L67.99189

L21922-01ASD 12/15/14 13:39 5.7 106ASD II141126-2 77.94 285 115mg/L 2067.99189

WG376073CCV2 12/15/14 13:52 103CCV II141211-3 51.72 90 110mg/L50

WG376073CCB2 12/15/14 13:55CCB U -0.3 0.3mg/L

WG376073CCV3 12/15/14 14:15 103CCV II141211-3 51.34 90 110mg/L50

WG376073CCB3 12/15/14 14:18CCB U -0.3 0.3mg/L



WG375443

WG375443ICV 12/03/14 13:00 100ICV WI141203-2 100 90 110mg/L100

WG375443ICB 12/03/14 13:00ICB U -3 3mg/L

WG376102

WG376102CCV1 12/15/14 15:45 107CCV WI141203-1 53.6 90 110mg/L50

WG376102CCB1 12/15/14 15:45CCB U -3 3mg/L

WG376102PQV 12/15/14 15:45 114PQV WI141105-2 5.7 70 130mg/L5

WG376102LFB1 12/15/14 15:45 99LFB WI141105-3 49.3 90 110mg/L50

WG376102CCV2 12/15/14 15:45 109CCV WI141203-1 54.4 90 110mg/L50

WG376102CCB2 12/15/14 15:45CCB U -3 3mg/L

WG376102CCV3 12/15/14 15:45 107CCV WI141203-1 53.7 90 110mg/L50

WG376102CCB3 12/15/14 15:45CCB U -3 3mg/L

WG376102LFB2 12/15/14 15:45 108LFB WI141105-3 53.8 90 110mg/L50

L21948-03DUP RA12/15/14 15:45 2.8DUP 2.5 11mg/L 20

WG376102CCV4 12/15/14 15:45 107CCV WI141203-1 53.3 90 110mg/L50

WG376102CCB4 12/15/14 15:45CCB U -3 3mg/L

L21950-01AS 12/15/14 15:45 U 102AS WI141105-3 51 90 110mg/L50

WG376102CCV5 12/15/14 15:45 105CCV WI141203-1 52.4 90 110mg/L50

WG376102CCB5 12/15/14 15:45CCB U -3 3mg/L

Page 8 of 28L21970-1501091534


Inorganic QC

Summary




WG376320

WG376320ICV 12/18/14 5:58 100ICV MS141027-2 .0498 90 110mg/L.05

WG376320ICB 12/18/14 6:01ICB U -0.0006 0.0006mg/L

WG376320LFB 12/18/14 6:05 97LFB MS141118-9 .04862 85 115mg/L.05

L22029-01AS 12/18/14 6:18 .0002 95AS MS141118-9 .04786 70 130mg/L.05

L22029-01ASD 12/18/14 6:21 .0002 97ASD MS141118-9 .04861 270 130mg/L 20.05

WG376320CCV1 12/18/14 6:36 102CCV MS141205-5 .102 90 110mg/L.1

WG376320CCB1 12/18/14 6:40CCB U -0.0006 0.0006mg/L

WG376320CCV2 12/18/14 7:15 102CCV MS141205-5 .1024 90 110mg/L.1

WG376320CCB2 12/18/14 7:18CCB U -0.0006 0.0006mg/L

WG376320CCV3 12/18/14 7:37 103CCV MS141205-5 .103 90 110mg/L.1

WG376320CCB3 12/18/14 7:40CCB U -0.0006 0.0006mg/L

Chloride SM4500Cl-E


WG376549

WG376549ICB 12/22/14 15:48ICB U -1.5 1.5mg/L

WG376549ICV 12/22/14 15:48 102ICV WI141103-1 55.88 90 110mg/L54.835

WG376549CCV1 12/22/14 16:58 105CCV WI140730-1 52.32 90 110mg/L50

WG376549CCB1 12/22/14 16:58CCB U -1.5 1.5mg/L

WG376549LFB1 12/22/14 16:58 101LFB WI141209-1 30.36 90 110mg/L30

L21970-01AS M212/22/14 16:58 56.1 87AS WI141209-1 82.22 90 110mg/L30

L22008-01DUP 12/22/14 16:58 13DUP 12.99 0mg/L 20

WG376549CCV2 12/22/14 16:59 105CCV WI140730-1 52.42 90 110mg/L50

WG376549CCB2 12/22/14 16:59CCB U -1.5 1.5mg/L

WG376549CCV3 12/22/14 17:00 105CCV WI140730-1 52.26 90 110mg/L50

WG376549CCB3 12/22/14 17:00CCB U -1.5 1.5mg/L

WG376549CCV4 12/22/14 17:08 104CCV WI140730-1 52.07 90 110mg/L50

WG376549CCB4 12/22/14 17:08CCB U -1.5 1.5mg/L

WG376549CCV5 12/22/14 17:14 105CCV WI140730-1 52.64 90 110mg/L50

WG376549CCB5 12/22/14 17:14CCB U -1.5 1.5mg/L

WG376549LFB2 12/22/14 17:15 101LFB WI141209-1 30.38 90 110mg/L30

WG376549CCV6 12/22/14 17:15 105CCV WI140730-1 52.34 90 110mg/L50

WG376549CCB6 12/22/14 17:15CCB U -1.5 1.5mg/L

WG376549CCV7 12/22/14 17:43 105CCV WI140730-1 52.47 90 110mg/L50

WG376549CCB7 12/22/14 17:43CCB U -1.5 1.5mg/L

WG376549CCV8 12/22/14 17:43 105CCV WI140730-1 52.65 90 110mg/L50

WG376549CCB8 12/22/14 17:43CCB U -1.5 1.5mg/L

Page 9 of 28L21970-1501091534


Inorganic QC

Summary




WG376073

WG376073ICV 12/15/14 12:22 99ICV II141125-1 1.97 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.03 0.03mg/L

WG376073PQV 12/15/14 12:31 96PQV II141201-5 .048 70 130mg/L.05005

WG376073SIC 12/15/14 12:35 92SIC II141201-6 .092 80 120mg/L.1001

WG376073LFB 12/15/14 12:41 101LFB II141126-2 .506 85 115mg/L.501

WG376073CCV1 12/15/14 13:13 103CCV II141211-3 1.025 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.03 0.03mg/L

L21922-01AS 12/15/14 13:36 U 102AS II141126-2 .512 85 115mg/L.501

L21922-01ASD 12/15/14 13:39 U 101ASD II141126-2 .508 185 115mg/L 20.501

WG376073CCV2 12/15/14 13:52 103CCV II141211-3 1.029 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.03 0.03mg/L

WG376073CCV3 12/15/14 14:15 102CCV II141211-3 1.024 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.03 0.03mg/L



WG376073

WG376073ICV 12/15/14 12:22 98ICV II141125-1 1.962 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.03 0.03mg/L

WG376073PQV 12/15/14 12:31 94PQV II141201-5 .047 70 130mg/L.04995

WG376073SIC 12/15/14 12:35 100SIC II141201-6 .1 80 120mg/L.0999

WG376073LFB 12/15/14 12:41 102LFB II141126-2 .507 85 115mg/L.4995

WG376073CCV1 12/15/14 13:13 102CCV II141211-3 1.016 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.03 0.03mg/L

L21922-01AS 12/15/14 13:36 U 104AS II141126-2 .518 85 115mg/L.4995

L21922-01ASD 12/15/14 13:39 U 102ASD II141126-2 .508 285 115mg/L 20.4995

WG376073CCV2 12/15/14 13:52 102CCV II141211-3 1.016 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.03 0.03mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 1.012 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.03 0.03mg/L

Page 10 of 28L21970-1501091534


Inorganic QC

Summary


Fluoride SM4500F-C


WG376230

WG376230ICV 12/17/14 11:26 99ICV WC141217-7 1.97 95 105mg/L2

WG376230ICB 12/17/14 11:33ICB U -0.15 0.15mg/L

WG376230PQV 12/17/14 11:41 95PQV WC141217-1 .237 70 130mg/L.25075

WG376230LFB1 12/17/14 11:48 93LFB WC140911-7 4.672 90 110mg/L5.015

L21946-07AS 12/17/14 12:11 73.2 95AS WC140911-7 120.65 90 110mg/L50.15

L21946-07DUP 12/17/14 12:19 73.2DUP 71.78 2mg/L 20

WG376230CCV1 12/17/14 12:50 97CCV WC141217-7 1.944 90 110mg/L2

WG376230CCB1 12/17/14 12:57CCB U -0.15 0.15mg/L

WG376230CCV2 12/17/14 13:44 99CCV WC141217-7 1.97 90 110mg/L2

WG376230CCB2 12/17/14 13:52CCB U -0.15 0.15mg/L

WG376230LFB2 12/17/14 14:17 91LFB WC140911-7 4.568 90 110mg/L5.015

WG376230CCV3 12/17/14 14:34 97CCV WC141217-7 1.935 90 110mg/L2

WG376230CCB3 12/17/14 14:41CCB U -0.15 0.15mg/L

WG376230CCV4 12/17/14 15:16 99CCV WC141217-7 1.979 90 110mg/L2

WG376230CCB4 12/17/14 15:23CCB U -0.15 0.15mg/L

WG376230CCV5 12/17/14 16:04 97CCV WC141217-7 1.935 90 110mg/L2

WG376230CCB5 12/17/14 16:11CCB U -0.15 0.15mg/L



WG376073

WG376073ICV 12/15/14 12:22 100ICV II141125-1 1.992 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.06 0.06mg/L

WG376073PQV 12/15/14 12:31 92PQV II141201-5 .046 70 130mg/L.050005

WG376073SIC 12/15/14 12:35 95SIC II141201-6 191 1 200mg/L200.070005

WG376073LFB 12/15/14 12:41 104LFB II141126-2 1.037 85 115mg/L1.0014

WG376073CCV1 12/15/14 13:13 105CCV II141211-3 1.047 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.06 0.06mg/L

L21922-01AS 12/15/14 13:36 .03 106AS II141126-2 1.096 85 115mg/L1.0014

L21922-01ASD 12/15/14 13:39 .03 104ASD II141126-2 1.075 285 115mg/L 201.0014

WG376073CCV2 12/15/14 13:52 104CCV II141211-3 1.042 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.06 0.06mg/L

WG376073CCV3 12/15/14 14:15 104CCV II141211-3 1.037 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.06 0.06mg/L



WG376320

WG376320ICV 12/18/14 5:58 101ICV MS141027-2 .05035 90 110mg/L.05

WG376320ICB 12/18/14 6:01ICB U -0.0003 0.0003mg/L

WG376320LFB 12/18/14 6:05 92LFB MS141118-9 .04614 85 115mg/L.05005

L22029-01AS 12/18/14 6:18 .0002 92AS MS141118-9 .04645 70 130mg/L.05005

L22029-01ASD 12/18/14 6:21 .0002 93ASD MS141118-9 .04698 170 130mg/L 20.05005

WG376320CCV1 12/18/14 6:36 101CCV MS141205-5 .2532 90 110mg/L.25025

WG376320CCB1 12/18/14 6:40CCB U -0.0003 0.0003mg/L

WG376320CCV2 12/18/14 7:15 100CCV MS141205-5 .2507 90 110mg/L.25025

WG376320CCB2 12/18/14 7:18CCB U -0.0003 0.0003mg/L

WG376320CCV3 12/18/14 7:37 101CCV MS141205-5 .2528 90 110mg/L.25025

WG376320CCB3 12/18/14 7:40CCB U -0.0003 0.0003mg/L

Page 11 of 28L21970-1501091534


Inorganic QC

Summary




WG376073

WG376073ICV 12/15/14 12:22 98ICV II141125-1 97.65 95 105mg/L100

WG376073ICB 12/15/14 12:28ICB U -0.6 0.6mg/L

WG376073PQV 12/15/14 12:31 98PQV II141201-5 .98 70 130mg/L1.0007

WG376073SIC 12/15/14 12:35 99SIC II141201-6 199.1 1 200mg/L201.1407

WG376073LFB 12/15/14 12:41 101LFB II141126-2 50.38 85 115mg/L50.00283

WG376073CCV1 12/15/14 13:13 101CCV II141211-3 50.59 90 110mg/L50

WG376073CCB1 12/15/14 13:16CCB U -0.6 0.6mg/L

L21922-01AS 12/15/14 13:36 1.2 104AS II141126-2 53.13 85 115mg/L50.00283

L21922-01ASD 12/15/14 13:39 1.2 102ASD II141126-2 52.33 285 115mg/L 2050.00283

WG376073CCV2 12/15/14 13:52 102CCV II141211-3 50.89 90 110mg/L50

WG376073CCB2 12/15/14 13:55CCB U -0.6 0.6mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 50.4 90 110mg/L50

WG376073CCB3 12/15/14 14:18CCB U -0.6 0.6mg/L



WG376073

WG376073ICV 12/15/14 12:22 99ICV II141125-1 1.9792 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.015 0.015mg/L

WG376073PQV 12/15/14 12:31 72PQV II141201-5 .0179 70 130mg/L.025025

WG376073SIC 12/15/14 12:35 97SIC II141201-6 48.64 1 200mg/L50.125025

WG376073LFB 12/15/14 12:41 103LFB II141126-2 .5174 85 115mg/L.501

WG376073CCV1 12/15/14 13:13 104CCV II141211-3 1.039 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.015 0.015mg/L

L21922-01AS 12/15/14 13:36 U 106AS II141126-2 .5301 85 115mg/L.501

L21922-01ASD 12/15/14 13:39 U 104ASD II141126-2 .5207 285 115mg/L 20.501

WG376073CCV2 12/15/14 13:52 104CCV II141211-3 1.04 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.015 0.015mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 1.014 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.015 0.015mg/L

Page 12 of 28L21970-1501091534


Inorganic QC

Summary




WG376240

WG376240ICV 12/18/14 11:45 96ICV II141211-2 .00479 95 105mg/L.005005

WG376240ICB 12/18/14 11:47ICB U -0.0002 0.0002mg/L

WG376351

WG376351CCV1 12/18/14 14:30 99CCV II141211-2 .00497 90 110mg/L.005005

WG376351CCB1 12/18/14 14:32CCB U -0.0002 0.0002mg/L

WG376351LRB 12/18/14 14:34LRB U -0.00044 0.00044mg/L

WG376351LFB 12/18/14 14:36 104LFB II141202-3 .00209 85 115mg/L.002002

L21970-01LFM 12/18/14 14:40 U 97LFM II141202-3 .00194 85 115mg/L.002002

L21970-01LFMD 12/18/14 14:42 U 100LFMD II141202-3 .00201 485 115mg/L 20.002002

WG376351CCV2 12/18/14 14:56 102CCV II141211-2 .0051 90 110mg/L.005005

WG376351CCB2 12/18/14 14:58CCB U -0.0002 0.0002mg/L

WG376351CCV3 12/18/14 15:21 99CCV II141211-2 .00496 90 110mg/L.005005

WG376351CCB3 12/18/14 15:23CCB U -0.0002 0.0002mg/L

WG376351CCV4 12/18/14 15:39 99CCV II141211-2 .00494 90 110mg/L.005005

WG376351CCB4 12/18/14 15:41CCB U -0.0002 0.0002mg/L



WG376073

WG376073ICV 12/15/14 12:22 101ICV II141125-1 2.029 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.06 0.06mg/L

WG376073PQV 12/15/14 12:31 102PQV II141201-5 .102 70 130mg/L.0999

WG376073SIC 12/15/14 12:35 94SIC II141201-6 .094 80 120mg/L.0999

WG376073LFB 12/15/14 12:41 104LFB II141126-2 .518 85 115mg/L.4995

WG376073CCV1 12/15/14 13:13 103CCV II141211-3 1.025 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.06 0.06mg/L

L21922-01AS 12/15/14 13:36 U 107AS II141126-2 .532 85 115mg/L.4995

L21922-01ASD 12/15/14 13:39 U 104ASD II141126-2 .521 285 115mg/L 20.4995

WG376073CCV2 12/15/14 13:52 102CCV II141211-3 1.017 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.06 0.06mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 1.009 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.06 0.06mg/L

Page 13 of 28L21970-1501091534


Inorganic QC

Summary




WG376073

WG376073ICV 12/15/14 12:22 99ICV II141125-1 1.979 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.024 0.024mg/L

WG376073PQV 12/15/14 12:31 96PQV II141201-5 .0387 70 130mg/L.04012

WG376073SIC 12/15/14 12:35 92SIC II141201-6 .0927 80 120mg/L.1003

WG376073LFB 12/15/14 12:41 102LFB II141126-2 .5106 85 115mg/L.5015

WG376073CCV1 12/15/14 13:13 104CCV II141211-3 1.035 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.024 0.024mg/L

L21922-01AS 12/15/14 13:36 U 104AS II141126-2 .5231 85 115mg/L.5015

L21922-01ASD 12/15/14 13:39 U 101ASD II141126-2 .5089 385 115mg/L 20.5015

WG376073CCV2 12/15/14 13:52 102CCV II141211-3 1.023 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.024 0.024mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 1.013 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.024 0.024mg/L



WG376598

WG376598ICV 12/23/14 18:33 96ICV WI141018-1 2.316 90 110mg/L2.416

WG376598ICB 12/23/14 18:34ICB U -0.06 0.06mg/L

WG376603

WG376603CCV1 12/23/14 22:24 99CCV WI141218-9 1.987 90 110mg/L2

WG376603CCB1 12/23/14 22:25CCB U -0.06 0.06mg/L

WG376603LFB1 12/23/14 22:26 99LFB WI140719-4 1.983 90 110mg/L2

L21847-01AS 12/23/14 22:29 U 102AS WI140719-4 2.037 90 110mg/L2

L21847-02DUP RA12/23/14 22:31 UDUP U 0mg/L 20

WG376603CCV2 12/23/14 22:38 98CCV WI141218-9 1.968 90 110mg/L2

WG376603CCB2 12/23/14 22:40CCB U -0.06 0.06mg/L

WG376603CCV3 12/23/14 22:53 98CCV WI141218-9 1.963 90 110mg/L2

WG376603CCB3 12/23/14 22:54CCB U -0.06 0.06mg/L

WG376603LFB2 12/23/14 23:01 99LFB WI140719-4 1.979 90 110mg/L2

WG376603CCV4 12/23/14 23:07 98CCV WI141218-9 1.963 90 110mg/L2

WG376603CCB4 12/23/14 23:08CCB U -0.06 0.06mg/L

WG376603CCV5 12/23/14 23:16 97CCV WI141218-9 1.948 90 110mg/L2

WG376603CCB5 12/23/14 23:17CCB U -0.06 0.06mg/L

Page 14 of 28L21970-1501091534


Inorganic QC

Summary




WG376509

WG376509ICV 12/22/14 12:31 103ICV WI141103-10 1.029 90 110mg/L.999

WG376509ICB 12/22/14 12:34ICB U -0.15 0.15mg/L

WG376509LFB1 12/22/14 12:35 101LFB WI140113-8 1.011 90 110mg/L1

L21946-05AS 12/22/14 12:37 3.3 109AS WI140113-8 4.389 90 110mg/L1

L21952-01DUP RA12/22/14 12:39 UDUP .082 200mg/L 20

WG376509CCV1 12/22/14 12:46 105CCV WI140113-6 2.093 90 110mg/L2

WG376509CCB1 12/22/14 12:47CCB U -0.15 0.15mg/L

WG376509CCV2 12/22/14 12:59 105CCV WI140113-6 2.093 90 110mg/L2

WG376509CCB2 12/22/14 13:00CCB U -0.15 0.15mg/L

WG376509LFB2 12/22/14 13:06 97LFB WI140113-8 .966 90 110mg/L1

WG376509CCV3 12/22/14 13:12 104CCV WI140113-6 2.072 90 110mg/L2

WG376509CCB3 12/22/14 13:13CCB U -0.15 0.15mg/L

WG376509CCV4 12/22/14 13:27 104CCV WI140113-6 2.089 90 110mg/L2

WG376509CCB4 12/22/14 13:28CCB U -0.15 0.15mg/L

WG376509CCV5 12/22/14 13:34 106CCV WI140113-6 2.122 90 110mg/L2

WG376509CCB5 12/22/14 13:35CCB U -0.15 0.15mg/L

WG376509CCV6 12/22/14 13:39 106CCV WI140113-6 2.113 90 110mg/L2

WG376509CCB6 12/22/14 13:41CCB U -0.15 0.15mg/L



WG376073

WG376073ICV 12/15/14 12:22 98ICV II141125-1 19.56 95 105mg/L20

WG376073ICB 12/15/14 12:28ICB U -0.6 0.6mg/L

WG376073PQV 12/15/14 12:31 112PQV II141201-5 1.12 70 130mg/L1.002

WG376073SIC 12/15/14 12:35 106SIC II141201-6 1.06 80 120mg/L1.002

WG376073LFB 12/15/14 12:41 100LFB II141126-2 98.21 85 115mg/L98.07852

WG376073CCV1 12/15/14 13:13 101CCV II141211-3 10.12 90 110mg/L10

WG376073CCB1 12/15/14 13:16CCB U -0.6 0.6mg/L

L21922-01AS 12/15/14 13:36 1 102AS II141126-2 101.4 85 115mg/L98.07852

L21922-01ASD 12/15/14 13:39 1 101ASD II141126-2 100.4 185 115mg/L 2098.07852

WG376073CCV2 12/15/14 13:52 101CCV II141211-3 10.08 90 110mg/L10

WG376073CCB2 12/15/14 13:55CCB U -0.6 0.6mg/L

WG376073CCV3 12/15/14 14:15 100CCV II141211-3 10.03 90 110mg/L10

WG376073CCB3 12/15/14 14:18CCB U -0.6 0.6mg/L



WG376141

WG376141PBW 12/16/14 9:10PBW U -20 20mg/L


L21974-01DUP 12/16/14 9:33 414DUP 414 0mg/L 10

Page 15 of 28L21970-1501091534


Inorganic QC

Summary




WG376186

WG376186PBW 12/16/14 13:45PBW U -15 15mg/L


L22028-03DUP RA12/16/14 14:00 UDUP U 0mg/L 10



WG376320

WG376320ICV 12/18/14 5:58 102ICV MS141027-2 .0508 90 110mg/L.05

WG376320ICB 12/18/14 6:01ICB .00011 -0.0003 0.0003mg/L

WG376320LFB 12/18/14 6:05 94LFB MS141118-9 .04705 85 115mg/L.05015

L22029-01AS 12/18/14 6:18 .0001 99AS MS141118-9 .04993 70 130mg/L.05015

L22029-01ASD 12/18/14 6:21 .0001 101ASD MS141118-9 .05095 270 130mg/L 20.05015

WG376320CCV1 12/18/14 6:36 98CCV MS141205-5 .2455 90 110mg/L.25075

WG376320CCB1 12/18/14 6:40CCB U -0.0003 0.0003mg/L

WG376320CCV2 12/18/14 7:15 98CCV MS141205-5 .2461 90 110mg/L.25075

WG376320CCB2 12/18/14 7:18CCB U -0.0003 0.0003mg/L

WG376320CCV3 12/18/14 7:37 98CCV MS141205-5 .245 90 110mg/L.25075

WG376320CCB3 12/18/14 7:40CCB U -0.0003 0.0003mg/L



WG376073

WG376073ICV 12/15/14 12:22 101ICV II141125-1 43.33 95 105mg/L42.8

WG376073ICB 12/15/14 12:28ICB U -0.6 0.6mg/L

WG376073PQV 12/15/14 12:31 92PQV II141201-5 .99 70 130mg/L1.0714

WG376073SIC 12/15/14 12:35 94SIC II141201-6 1.01 80 120mg/L1.0714

WG376073LFB 12/15/14 12:41 104LFB II141126-2 22.31 85 115mg/L21.428

WG376073CCV1 12/15/14 13:13 101CCV II141211-3 21.7 90 110mg/L21.4

WG376073CCB1 12/15/14 13:16CCB U -0.6 0.6mg/L

L21922-01AS 12/15/14 13:36 11.1 107AS II141126-2 33.97 85 115mg/L21.428

L21922-01ASD 12/15/14 13:39 11.1 105ASD II141126-2 33.58 185 115mg/L 2021.428

WG376073CCV2 12/15/14 13:52 101CCV II141211-3 21.62 90 110mg/L21.4

WG376073CCB2 12/15/14 13:55CCB U -0.6 0.6mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 21.57 90 110mg/L21.4

WG376073CCB3 12/15/14 14:18CCB U -0.6 0.6mg/L

Page 16 of 28L21970-1501091534


Inorganic QC

Summary




WG376073

WG376073ICV 12/15/14 12:22 97ICV II141125-1 96.8 95 105mg/L100

WG376073ICB 12/15/14 12:28ICB U -0.6 0.6mg/L

WG376073PQV 12/15/14 12:31 106PQV II141201-5 1.06 70 130mg/L1.002

WG376073SIC 12/15/14 12:35 108SIC II141201-6 1.08 80 120mg/L1.002

WG376073LFB 12/15/14 12:41 100LFB II141126-2 100.3 85 115mg/L100.0589

WG376073CCV1 12/15/14 13:13 99CCV II141211-3 49.57 90 110mg/L50

WG376073CCB1 12/15/14 13:16CCB U -0.6 0.6mg/L

L21922-01AS 12/15/14 13:36 2.6 102AS II141126-2 104.4 85 115mg/L100.0589

L21922-01ASD 12/15/14 13:39 2.6 101ASD II141126-2 103.9 085 115mg/L 20100.0589

WG376073CCV2 12/15/14 13:52 99CCV II141211-3 49.72 90 110mg/L50

WG376073CCB2 12/15/14 13:55CCB U -0.6 0.6mg/L

WG376073CCV3 12/15/14 14:15 99CCV II141211-3 49.41 90 110mg/L50

WG376073CCB3 12/15/14 14:18CCB .21 -0.6 0.6mg/L



WG376444

WG376444PBW 12/19/14 11:45PBW U -30 30mg/L

WG376444LCSW 12/19/14 11:47 112LCSW WC140825-2 112 80 120mg/L100

L22050-02DUP 12/19/14 12:11 1970DUP 1976 0mg/L 20



WG376244

WG376244ICV 12/17/14 11:30 96ICV WC141217-12 .257 90 110mg/L.26666

WG376244ICB 12/17/14 11:38ICB U -0.06 0.06mg/L

WG376244LFB 12/17/14 11:46 115LFB WC141217-15 .233 80 120mg/L.2026667

WG376244CCV1 12/17/14 13:10 109CCV WC141217-13 .165 90 110mg/L.152

WG376244CCB1 12/17/14 13:18CCB U -0.06 0.06mg/L

L22023-01AS M212/17/14 13:35 U 24AS WC141217-15 .184 75 125mg/L.760000125

L22023-01DUP RA12/17/14 13:43 UDUP U 0mg/L 20

WG376244CCV2 12/17/14 14:50 106CCV WC141217-13 .161 90 110mg/L.152

WG376244CCB2 12/17/14 14:59CCB U -0.06 0.06mg/L

WG376244CCV3 12/17/14 15:49 103CCV WC141217-13 .157 90 110mg/L.152



WG376320

WG376320ICV 12/18/14 5:58 103ICV MS141027-2 .05163 90 110mg/L.05

WG376320ICB 12/18/14 6:01ICB U -0.0003 0.0003mg/L

WG376320LFB 12/18/14 6:05 95LFB MS141118-9 .04735 85 115mg/L.05

L22029-01AS 12/18/14 6:18 U 96AS MS141118-9 .0481 70 130mg/L.05

L22029-01ASD 12/18/14 6:21 U 98ASD MS141118-9 .04878 170 130mg/L 20.05

WG376320CCV1 12/18/14 6:36 102CCV MS141205-5 .1021 90 110mg/L.1

WG376320CCB1 12/18/14 6:40CCB U -0.0003 0.0003mg/L

WG376320CCV2 12/18/14 7:15 101CCV MS141205-5 .1012 90 110mg/L.1

WG376320CCB2 12/18/14 7:18CCB U -0.0003 0.0003mg/L

Page 17 of 28L21970-1501091534


Inorganic QC

Summary




WG376073

WG376073ICV 12/15/14 12:22 99ICV II141125-1 1.984 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.015 0.015mg/L

WG376073PQV 12/15/14 12:31 94PQV II141201-5 .0236 70 130mg/L.025

WG376073SIC 12/15/14 12:35 89SIC II141201-6 .0889 80 120mg/L.1

WG376073LFB 12/15/14 12:41 105LFB II141126-2 .5253 85 115mg/L.5

WG376073CCV1 12/15/14 13:13 102CCV II141211-3 1.022 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.015 0.015mg/L

L21922-01AS 12/15/14 13:36 U 108AS II141126-2 .5402 85 115mg/L.5

L21922-01ASD 12/15/14 13:39 U 105ASD II141126-2 .5266 385 115mg/L 20.5

WG376073CCV2 12/15/14 13:52 101CCV II141211-3 1.013 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.015 0.015mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 1.014 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.015 0.015mg/L



WG376073

WG376073ICV 12/15/14 12:22 97ICV II141125-1 1.93 95 105mg/L2

WG376073ICB 12/15/14 12:28ICB U -0.03 0.03mg/L

WG376073PQV 12/15/14 12:31 98PQV II141201-5 .049 70 130mg/L.05005

WG376073SIC 12/15/14 12:35 96SIC II141201-6 .096 80 120mg/L.1

WG376073LFB 12/15/14 12:41 104LFB II141126-2 .52 85 115mg/L.5005

WG376073CCV1 12/15/14 13:13 102CCV II141211-3 1.016 90 110mg/L1

WG376073CCB1 12/15/14 13:16CCB U -0.03 0.03mg/L

L21922-01AS 12/15/14 13:36 U 109AS II141126-2 .548 85 115mg/L.5005

L21922-01ASD 12/15/14 13:39 U 106ASD II141126-2 .533 385 115mg/L 20.5005

WG376073CCV2 12/15/14 13:52 101CCV II141211-3 1.014 90 110mg/L1

WG376073CCB2 12/15/14 13:55CCB U -0.03 0.03mg/L

WG376073CCV3 12/15/14 14:15 101CCV II141211-3 1.007 90 110mg/L1

WG376073CCB3 12/15/14 14:18CCB U -0.03 0.03mg/L

Page 18 of 28L21970-1501091534


Inorganic Extended

Qualifier Report




SM5310BCarbon, total organic (TOC)L21970-01 WG376102









D1 Sample required dilution due to matrix.SM4500S2-DSulfide as SWG376244


SM4500S2-D



SM4500S2-D

D1 Sample required dilution due to matrix.SM4500S2-DSulfide as SL21970-02 WG376244


SM4500S2-D


SM4500S2-D

REPAD.15.06.05.01

Page 19 of 28L21970-1501091534





Project ID:


Date Sampled: 12/10/14 12:30


Locator:

RadioChemistry

Analytical Results


M900.0

Prep Method:


Gross Alpha 31 6.5 2.4 pCi/L * djc12/16/14 0:18

Gross Beta 27 4.6 5 pCi/L * djc12/16/14 0:18

Lead 210, dissolved

EICHROM, OTW01

Prep Method:


Lead 210, dissolved -1.3 1.2 3.7 pCi/L * nco12/21/14 13:28


M903.1

Prep Method:




M904.0

Prep Method:


Radium 228, dissolved 0.99 0.58 0.55 pCi/L bsg01/08/15 12:05


ESM 4506

Prep Method:


Thorium 230, dissolved -0.05 0.29 0.6 pCi/L * thf12/17/14 0:07



Page 20 of 28L21970-1501091534

















QC Sample Types














D ASTM

RP DOE

ESM DOE/ESM

Comments







REP003.09.12.01

Radiochemistry

Reference

Page 21 of 28L21970-1501091534


Radiochemistry QC

Summary


Alpha M900.0


pCi/L

Error LLDLLD

Units:

WG376236

WG376132PBW 12/16/14PBW 0 31.6 1.5

WG376132LCSWA 12/16/14 120LCSW PCN45463 120100 83 1339.4 1.5

L21848-02DUP 12/16/14 0DUP-RER 2.1 22.3 0.692 1.81.9

L21970-01DUP 12/16/14 31DUP-RER 32 27 0.16.5 2.52.4

L21874-01MSA M212/16/14 1.4 41MS PCN45463 42100 83 1336.92.5 2.12.1

Beta M900.0


pCi/L

Error LLDLLD

Units:

WG376236

WG376132PBW 12/16/14PBW 2.1 93.4 4.5

WG376132LCSWB 12/16/14 110LCSW PCN44675 110100 70 1297.4 4.6

L21848-02DUP 12/16/14 0.01DUP-RER 2.1 23.3 0.433.5 4.64.8

L21970-01DUP 12/16/14 27DUP-RER 22 24.9 0.744.6 55

L21874-02MSB M112/16/14 0 130MS PCN44675 130100 70 1298.33.7 55.2



pCi/L

Error LLDLLD

Units:

WG376497

WG376020PBW 12/21/14PBW .06 9.21.5 4.6

WG376020LCSW 12/21/14 85LCSW PCN44159 8296.46 55 1212.8 4

L21742-02DUP 12/21/14 2.4DUP-RER .16 21.1 1.321.3 3.43.8

L21961-01MS 12/21/14 1.5 70MS PCN44159 6996.46 55 12141.9 7.55.5

Page 22 of 28L21970-1501091534


Radiochemistry QC

Summary




pCi/L

Error LLDLLD

Units:

WG376887

WG376607PBW 01/02/15PBW .35 1.320.2 0.66

WG376607LCSW 01/02/15 95LCSW PCN47456 1920 43 1480.72 0.14

L21970-01DUP 01/02/15 0.21DUP-RER -.02 20.17 1.160.1 0.380.2

L22105-02DUP 01/02/15 0.43DUP-RER .23 20.26 0.510.29 0.520.46

L21990-04MS 01/02/15 0.91 95MS PCN47456 2020 43 1480.680.16 0.120.12



pCi/L

Error LLDLLD

Units:

WG377139

WG376866LCSW 01/07/15 70LCSW PCN46182 1318.69 47 1231.1 0.48

WG376866PBW 01/07/15PBW -.32 0.640.28 0.32

L21961-01DUP 01/08/15 2.7DUP-RER 2.5 20.59 0.220.69 0.460.57

L21970-01MS 01/08/15 0.99 64MS PCN46182 1318.68 47 12310.58 0.480.55

L21990-05DUP 01/08/15 1.3DUP-RER 1.2 20.29 0.220.34 0.230.28



pCi/L

Error LLDLLD

Units:

WG376333

WG376105PBW 12/17/14PBW .64 1.140.38 0.57

WG376105LCSW 12/17/14 93LCSW RC140811-1 150162.12 91 1264.4 0.63

L21608-01DUP 12/17/14 0.38DUP-RER -.34 20.44 1.350.3 0.640.56

L21608-02MS M212/17/14 0.45 80MS RC140811-1 130162.12 91 1263.80.41 0.590.62

Page 23 of 28L21970-1501091534


RadChem Extended

Qualifier Report





M1 Matrix spike recovery was high, the recovery of the associated control sample (LCS or LFB) was acceptable.

M900.0Gross Beta


ESM 4506Thorium 230, dissolvedWG376333

REPAD.15.06.05.01

Page 24 of 28L21970-1501091534


Certification

Qualifiers


Metals Analysis

The following parameters are not offered for certification or are not covered by AZ certificate #AZ0102.




Radiochemistry







Wet Chemistry





REPAD.05.06.05.01

Page 25 of 28L21970-1501091534


Sample

Receipt

Western Water and Land Inc. ACZ Project ID:

Date Received:

Received By: ddp

12/11/2014 13:04

L21970




NANOYES

X

X

X

X

X

X









NANOYES

X

X

X

X

X

X

X












Samples/Containers

X

X

X

Shipping Containers


Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- --------------------3226 3 17 Yes

X



REPAD LPII 2012-03

Page 26 of 28L21970-1501091534

of 28L21970-1501091534

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