Basic Sciences - Universidad de...
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Basic Sciences
Division
Deparment of Chemistry
Inorganic Chemistry Lab II
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1.- GENERAL INFORMATION
Learning unit: Inorganic Chemistry Lab II
Department: Chemistry
Course format Lab
Prerequisites(P) None
Corequisites (CO) Inorganic Chemistry II
Ascribed Academy Chemistry
Module M2: Synthesis, purification and chemical transformation.
Type Basic particular mandatory
Lecture hours 0
Practice Hours 3 hrs. per week
Total hours 51 hrs.
Credits 3
Degree in which this class is taught: B.S in Chemistry.
2. GENERIC COMPETENCIES
Students ... - apply the acquired knowledge in Inorganic Chemistry II to carry out the lab practices. - are able to analyze the chemical structures and bonds of the compounds with metals of blocks d and f. - are able to then synthesize this type of compounds by analyzing their chemical, magnetic and spectroscopic
properties. - recognize the transcendence and application of coordination chemistry in labs and industries.
3.- SPECIFIC CHARACTERISTICS OF THE COMPETENCIES
Knowledge
• Coordination complexes structures and isomers. • Coordination complexes linking bond theories. • Electronic spectra of the coordination complexes. • Coordination complexes reactions and mechanisms.
Skills
• Adequate handling of lab reagents, materials and equipment. • Use of simple separation techniques. • Handling waste from the lab practices. • Use of a lab logbook. • Strict respect for the hygiene and safety rules of the lab.
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Aptitudes
• Team work •. Analysis, synthesis and evaluation skills. • Critical thinking • Work culture
Values
• Solidarity • Honesty • Responsibility • Discipline
4.- TRANSVERSAL COMPETENCIES
Foreign Language (English)
Critical, analytical and synthetic thinking.
Oral and written expression
Professional ethics
Administration of human and material resources
Leadership and sustainability
Creativity, innovation and entrepreneurship
Other
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5.- COURSE CONTENT OF THE LEARNING UNIT
Practices
Practice 1: Properties of the transition metals part 1.
Practice 2: Properties of the transition metals part 2.
Practice 3: Synthesis of the chloride-amine cobalt complexes.(III)
Practice 4: Characterization of coordination complexes.
Practice 5: Copper and Dimethyl sulfoxide (DMSO) complexes.
Practice 6: Synthesis of linkage isomers [Co(NH3)5(ONO)]Cl2 and [Co(NH3)5(NO2)Cl2]
Practice 7: Synthesis of geometric isomers: cis and trans - bis copper (glycinate) (II) monohydrate
Practice 8: Synthesis of tris sulfate (thiourea) copper (I)
Practice 9: Preparation of copper acetate.
Practice 10: Chemical equilibrium and influence of temperature in cobalt complexes.
Practice 11: Solubility equilibrium of complex ions.
Practice 12: Synthesis of chrome tris (acetylacetonate) (III)
Practice 13: Preparation of tetrachloronickelate (II) from hexamine nickel (II)
Practice 14: Spectrochemistry series.
6.- ASSESSMENT
Numeric grade
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7.- GRADING CRITERIA OF THE LEARNING UNIT
7.- GRAIndicator of evaluation Percentage ITERIA
Departmental exams 0
Partial exam 0
Homework 0
Research activities 0
Practice reports 70
Class participation 0
Lab logbook 30
8.- REQUIRED MATERIAL (for students)
Calculator Periodic table Lab coat Text book Workbook Tables of standard potential, table of mobility, etc.
9.-SPECIFIC CONTENT BY LEARNING UNITS
Content unit
Generic
competency
of the content
unit
Topics
Clas
s
hour
s
Professor
activities
Student
activities Bibliography
Unit 1
Chemistry of transition
metals.
Recognize and predict the physical and chemical properties of
Practice 1: Properties of the transition metals part 1.
Practice 2: Properties of
3 Professor…
-guides students through the practices, making sure
Students...
-carry out each one of the practices in due time and manner,
Brown Le May, Química General,
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block b elements.
the transition metals part 2.
they carry out all the steps in order to reach the objectives in due time and manner.
-makes sure students follow the lab rules.
following all the lab rules.
-read and understand each practice before the actual day in order to reach the stated objectives
Use their logbook, make calculations and turn in a report after each practice.
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Unit 2
Coordination complexes structure
Understand the structure and predict the properties of coordination complexes.
Practice 3: Synthesis of the chloride-amine cobalt complexes.(III)
Practice 4: Characterization of coordination complexes.
Practice 5: Copper and Dimethyl sulfoxide (DMSO) complexes.
3 Professor…
-guides students through the practices, making sure they carry out all the steps in order to reach the objectives in due time and manner.
-makes
sure students follow the lab rules.
Students...
-carry out each one of the practices in due time and manner, following all the lab rules.
-read and understand each practice before the actual day in order to reach the stated objectives
Use their logbook, make calculations and turn in a report after each practice.
Shriver, Atkins, 2009, Inorganic Chemistry. 5th Ed., W. H. Freeman,
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Unit 3
Coordination complex isomers
Distinguish different types of isomerism that are present in the coordination complexes.
Practice 6: Synthesis of linkage isomers [Co(NH3)5(ONO)]Cl2 and [Co(NH3)5(NO2)Cl2]
Practice 7: Synthesis of geometric isomers: cis and trans - bis copper (glycinate) (II) monohydrate
3 Professor…
-guides students through the practices, making sure they carry out all the steps in order to reach the objectives in due time and manner.
-makes
sure students follow the lab rules.
Students...
-carry out each one of the practices in due time and manner, following all the lab rules.
-read and understand each practice before the actual day in order to reach the stated objectives
Use their logbook, make calculations and turn in a report after each practice.
Shriver, Atkins, 2009, Inorganic Chemistry. 5th Ed., W. H. Freeman,
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Unit 4
Chemical coordination:
bonding theories.
Reaffirm the concepts about the current theories to describe chemical bonding in the compounds with metals from block b.
Practice 8: Synthesis of tris sulfate (thiourea) copper (I)
Practice 9: Preparation of copper acetate.
3 Professor…
-guides students through the practices, making sure they carry out all the steps in order to reach the objectives in due time and manner.
-makes
sure students follow the lab rules.
Students...
-carry out each one of the practices in due time and manner, following all the lab rules.
-read and understand each practice before the actual day in order to reach the stated objectives
Use their logbook, make calculations and turn in a report after each practice.
Miessler, Gary L., Tarr, Donald, A 2014. Inorganic Chemistry. 5th Ed., Pearson,
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Unit 5
Chemical coordination: reactions and mechanisms
Evaluate the reactivity of the coordination complexes and observe the effects of temperature and concentration changes over the chemical equilibrium.
Practice 10: Chemical equilibrium and influence of temperature in cobalt complexes.
Practice 11: Solubility equilibrium of complex ions.
Practice 12: Synthesis of chrome tris (acetylacetonate) (III)
Practice 13: Preparation of tetrachloronickelate (II) from hexamine nickel (II)
3 Professor…
-guides students through the practices, making sure they carry out all the steps in order to reach the objectives in due time and manner.
-makes
sure students follow the lab rules.
Students...
-carry out each one of the practices in due time and manner, following all the lab rules.
-read and understand each practice before the actual day in order to reach the stated objectives
Use their logbook, make calculations and turn in a report after each practice.
Shriver, Atkins, 2009, Inorganic Chemistry. 5th Ed., W. H. Freeman,
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Unit 6
Coordination chemistry: Electronic spectra.
Determine the spectroscopic properties of the coordination complexes.
Practice 14: Spectrochemistry series.
3 Professor…
-guides students through the practices, making sure they carry out all the steps in order to reach the objectives in due time and manner.
-makes
sure students follow the lab rules.
Students...
-carry out each one of the practices in due time and manner, following all the lab rules.
-read and understand each practice before the actual day in order to reach the stated objectives
Use their logbook, make calculations and turn in a report after each practice.
Miessler, Gary L., Tarr, Donald, A 2014. Inorganic Chemistry. 5th Ed., Pearson,
COURSE EVIDENCES (Deliverables)
- Reports - Logbook
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10.-PROFESSOR’S PROFILE
Bachelor, Master or Doctorate degree in Chemistry, Chemical Engineering or related degrees.
11.-AUTHORS OF THE LEARNING UNIT
Karina Viridiana Chávez Hernández, Saira Lizette Hernández Olmos, Sara Angélica Cortes Llamas, Irma Idalia
Rangel Salas
12.-MODIFICATION AND UPDATE
March 22, 2017