Atomic Absorption Spectrophotometers AA-6300 …...TUBE ASSY,TEMPSENS 206-51033-94 TUBE ASSY,INLET...

Atomic Absorption Spectrophotometers

AA-6300 Series Consumables

SSI-6300-08-16

AA-6300 ...................................................................................................................... 3

Burner ASSY ......................................................................................................... 3 Drain ASSY ........................................................................................................... 3 Maintenance parts ................................................................................................ 4

ASC-6100 ..................................................................................................................... 5

Maintenance Parts ................................................................................................ 6

ASK-6100 ..................................................................................................................... 5

Maintenance Parts ................................................................................................ 6 GFA-EX7i ..................................................................................................................... 7

Maintenance Parts ................................................................................................ 7 Hydride Vapor Generator .......................................................................................... 8

Consumables ....................................................................................................... 9 Maintenance Parts ................................................................................................ 9

Atom Booster ........................................................................................................... 10 Chemical Compatibility ............................................................................................. 11

AA-6300 ............................................................................................................ 11 ASC-6100 ........................................................................................................... 12

Lamps ....................................................................................................................... 13

Single-Element .................................................................................................. 13 Multi-Element ................................................................................................... 14

Standards ................................................................................................................. 16

Contents

3

AA-6300

Burner ASSY

Drain ASSY

Item Part Number Part Name

1 016-35792-09 Tube, Super-Corn-Ace

2 206-50735-93 Level Switch Assy

3 206-63698-00 Drain Bottle

4 035-65014-14 Half Union, HZ10-02-PP

5 016-35792-09 Tubing

6 016-43201-02 DRAIN TUBING


1 206-50370-93 10 cm Titanium Burner Head

2 036-11222-84 O-RING, 4D P22

3 036-15551-16 O-Ring, AS56A

4 206-50123-00 PLUG FOR CHAMBER ASSY

5 036-11217-00 O-RING 4D P16,AA

6 206-50486-00 Mixer Paddle

7 036-11237-00 O-RING 4D P35

8 206-52213-91 DRAIN JOINT

9 036-11215-84 O-RING 4D P14

10 035-65903-03 Sleeve, PP 10

11 206-50321-00 CAP

12 200-31328-01 TUBING POLYETHYLENE

13 206-50230-91 CAPILLARY

14 206-52300-91 NEBULIZER

15 206-50761-00 BURNER SOCKET

16 035-65268-02 ELBOW

17 206-51389-00 RETAINTING PLATE

18 206-81812-00 HALF UNION

Back to contents Order at 800-477-1227, x1710 or online at store.shimadzu.com

4

Maintenance Parts: AA-6300

Part Name Part Number Remarks Replacement

D2-Lamp Lamp, D2 L6380 062-65055-05 Deuterium lamp 1 Year

O-Ring Sets O-Ring Set 206-82037-92 STD O-ring (Fluorine-containing rubber)

*See Chemical Compatibility

O-Ring Set, Organics O-Ring Set, Silicon

206-82037-96 206-82037-94

Perfluoroelastomer (FFKM) Silicon Rubber (VQM)

*See Chemical Compatibility *See Chemical Compatibility

Burner Head Burner Head ASSY 206-50370-93 Titanium, 10 cm 3 Years

High Temp Burner Head 206-50300-93 Titanium, N2O-C2H2, 5 cm 3 Years

Hoses Hose, 8×2B-BK 016-02101-04 For support gas (Air/Argon), Black 3 Years

Hose, 8×2B-R 016-02101-03 For fuel gas (C2H2), Red 3 Years

Hose, 8×2B-G 016-02101-01 For support gas (N2O), Green 3 Years

Atomizer Nebulizer Set 206-52300-91 With Impact bead & Nebulizer 2 Years

Burner Socket 206-50762-91 3 Years

Chamber ASSY 206-50363-91 Engineering plastic PP 6 Years

Mixer 206-50486-00 6 Years

Tubing Sampling tube 204-05899-01 Teflon tube for sample uptake *See Chemical Compatibility

Sampling tube ASSY 206-50772-91 Polyethylene tube for sample uptake *See Chemical Compatibility

Drain ASSY 206-52033-92 Overflow-type drainage trap

Polyethylene capillary No.3 200-31328-01 For sealing the capillary

PE tube, 8x1 016-43201-02 Drain tube, connects to drain bottle. Specify 3 meters.

Misc. WizAArd 4.0 206-58480-91 Win 7, 32-bit Software

Agent Connection Kit 206-77741-92 Win 7, 32-bit

Cleaning wire 201-79229-01 For cleaning the capillary

Card 206-52046-91 For cleaning the burner/for checking the burner height

Window Panel w(30)-Q 205-82661-02 Optical windows, inside atomization

chamber Seal Joint Assy 204-27570-02 Gas leak checking

HCL Lamp Retainer 206-51843-00 Holds HCL in socket


5

ASC-6100

ASK-6100


1 037-02881-03 KNOB

2 206-50062-00 TURNTABLE FOR ASC-6100

3 206-50290-91 NOZZLE ASSY, F

4 206-50295-01 COVER, TURN TABLE

5 206-87284-91 2 LITER RINSE BOTTLE

6 206-50265-00 BOTTLE HOLDER

7 206-50468-91 RS232C CABLE

8 071-60816-12 POWER CABLE

9 037-51260-09 CANOE CLIP-WHITE

10 036-11206-00 O-RING, 4D P8

Item Part Number Part Name Item Part Number Part Name

1 206-50408-00 Port Guide, ASC 7 206-50856-01 Nut, AA

2 206-61966-01 Syringe Port 8 206-50857-01 Nipple, AA

3 206-50406-93 Syringe Tube Assy 9 016-37502-00 Teflon Tube

4 200-62075-00 LUER FITTING 10 204-63890-00 Filter

5 208-97211-01 SYRINGE, ASC6100 11 206-50407-00 PLUNGER PRESSER

6 037-61111-01 Clip, Hose 4.5 12 042-00405-11 Pump Head


6

Maintenance Parts: ASC-6100


Nozzles Nozzle ASSY, F 206-50290-91 Standard

Nozzle ASSY, GFA, Micro 206-50401-92 Requires Pipette Tip (046-00308-02)

Pipet tip 046-00308-02 For Dispensing Every 60 samples *4

Nozzle ASSY, G 206-50298-91 Optional

Nozzle ASSY, HVG 206-67563-00 For HVG

Syringe Parts Syringe 208-97211-01 Capacity 250 uL 5 years *3

Plunger Tip, TEF025 046-00043-15 Plunger for syringe 1 year *3,5

Pump Parts Pump tube 042-00405-24 Tube for Peristaltic pump 6 months *1,3,5 2 years *2,3,5

Pump Head 042-00405-11 Pump Head for Peristaltic pump 1 year *1,5 4 years *2,5

Vials & Cups 16 mL Sample vial 046-00147-04 Each, polypropylene, Flame Cont. *1: Flame continuous method

16 mL Sample vial 220-95369-00 1000/PK, polypropylene, Flame Cont. *2: Furnace/ micro sampling method

53 mL Glass Vial 200-93113-05 Each, glass, Flame Cont. *3: When distilled water is used

20 mL Vials 038-00179-03 Each, polypropylene, GFA, Micro. *4: Recommended for low conc.

2 mL Cup 038-00259-02 Each, polypropylene, GFA, Micro. *5: 60 samples per day usage

2 mL Cup 220-95196-00 1000/PK, Polystyrene, GFA, Micro.

Glass sample cup (2 mL) 200-93036-00 2 mL Glass

Glass Test tube (12 mL) 046-00150-27 12 mL Glass

Misc. Rinse liquid bottle 206-87284-91 2 L plastic tank for rinse liquid

Port 206-50089-01 Integrated port

Fuse 072-02004-11 250 V, 3.15 A, Type T

GFA-TV 206-52950-41 Assists with Nozzles Postioning

GFA-TV


7

GFA-EX7i

Maintenance Parts: GFA-EX7i

Item Part Name Part Number Replacement Item Part Name Part Number Replacement

1 Graphite Cap 206-50602-00 2 Years 8 O-ring, 4CP14 036-11015-00 3 Years

2 Seal 206-50621-00 2 Years 9 Bolt 206-50680-01

3 Graphite Holder 206-50603-00 2 Years 10 Guide ASSY 206-51016-91

4 Socket ASSY 206-51030-91 11 Lid 206-51074-00

5 Window plate, W(16)-Q 205-82654-02 12 Slide Cover 206-50608-00 2 Years

6 O-ring, 4CP14 036-11015-00 3 Years 13 Spring 206-51038-00

7 HOSE NIPPLE M 5H 6 035-60395-06 14 Electrode tool 206-51014-91

GFA Tubes Name Part Number

High-density tube 206-50587-00

Extended Life High-denisty 206-50587-11

Pyrolytic coated tube 206-50588-00

Extended Life Pyrolytic coated 206-50588-11

Platform tube 206-50887-02


Hose, 8×2B-BK 016-02101-04 For support gas (Air/Argon), Black 3 Years

Wire band, for 14 mm 037-61018-00 Gas hose clamp

Wire band, for 16 mm 037-61019-00 Cooling water hose clamp

O-ring, 4CP14 036-11015-00 Socket Assy 3 Years

Extension tube ASSY 206-64752-00 Cooling Water Outlet 3 Years

Cooling Water ASSY 206-51028-91 Cooling Water Inlet 3 Years

Tetron Sleeve, 10 x 16 018-31506-00 For Cooling Water 3 Years

TUBE ASSY, OUTER 206-51033-93

TUBE ASSY,TEMPSENS 206-51033-94

TUBE ASSY,INLET 206-51033-95

TUBE ASSY,OUTLET 206-51033-96

TUBE ASSY, INNER 206-51033-97


8

Hydride Vapor Generator

Item Part Name Part Number

1 Hydride vapor generator main body

2 Reagent bottle (poltethylene) 204-09363-01

3 Gas Hose 204-05845-02

4 Drain tube (Tygon) 206-60250-02

5 AC Cable (110-117 V) 206-13774-00

Power cable (220-240 V) 071-60814-05

6 Fluorinated rubber tube 206-60250-01

7 Guide plate 206-18033-00

8 Fuse 1 A (110-117 V) 072-01214-02

Fuse 0.3 A (220-240 V) 072-01664-12

9 Cell holder 206-77610-91

10 Absorption cell 206-77607-00

11 Hose clamp, 16 mm 037-61019-00

12 Pump tube 080 (reagent) 208-90038-08

13 Pump tube 130 (sample) 208-90038-13

14 Front cover 206-17878-00

15 Side cover 206-17879-00

16 Gas/liquid separator 206-17839-00

17 Manifold 206-17825-00

18 Reaction Coil 206-18037-00

19 Hose nipple 204-64601-00

20 O-ring, EPR 200-62522-00

21 Suction tube (yellow-marked) for NaBH4 206-18036-01

22 Suction tube (blue-marked) for HCl 206-18036-02

23 Suction tube (not marked, 30 cm) for sample 206-18036-03

24 Suction tube (not marked, 80 cm) for ASC 206-18036-04

25 Wire mark (yellow) 072-83083-03

26 Wire mark (blue) 072-83083-02

27 Vinyl cover 206-18068-00

28 Grounding line 202-32982-00

29 Label (flow path diagram) 206-18616-00

30 Hose nipple, HN802 035-61522-00

31 Hose clamp, 14 mm 037-61018-00

32 Instruction manual 206-96739-00


9

Consumables: HVG Unit

Part Name Part Number Appearance

Pump tube 080 (reagent) 208-90038-08

Pump tube 130 (sample) 208-90038-13

Absorption cell 206-77607-00

Maintenance Parts: HVG Unit

Part Name Part Number Appearance

Gas/liquid separator 206-17839-00

Manifold (except for O-ring, hose nipple) 206-17825-00

Reaction Coil 206-18037-00

Suction tube (yellow-marked) for NaBH4

206-18036-01


10

Suction tube (blue-marked) for HCl 206-18036-02

Suction tube (not marked, 30 cm) for sample 206-18036-03

Suction tube (not marked, 80 cm) for ASC 206-18036-04

Fluorinated rubber tube 206-60250-01

Joint (reagent) 206-17826-01

Joint (sample) 206-17826-02

Atom Booster


1 206-50957-91 Atom Booster Assembly

2 206-50937-01 Quartz Tube Replacement


11

Chemical Compatibility

AA-6300

Chemical Name Drain Tank Drain Tube O-Rings Chamber Conditions of

Use (Polyethlyene) Standard Optional

(PTFE) Standard FFKM VQM Nebulizer

Water1 A A A A A A A

Ethanol B B B B B B B

Hydrochloric acid

B B B B B B B

Nitric acid B B B B B B B

Sulfuric acid B B B B B B B

Hydrofluoric acid

B B B B B X B

Perchloric acid B B B B B X B

Methanol B B B C B B B Change O-rings Sodium

hydroxide B B B X B X B

Gasoline C C B B B X B Change the drain tank

once every month. Change the standard drain tube once every

month, or replace it with the optional product

Petroleum C C B B B C B

Acetic acid C C B X B B B Change the O-rings to the optional products. Change the drain tank

once every month. Change the standard drain tube once every

month, or replace it with the optional product.

MIBK C C B X B C B

Butyl acetate C C B X B C B

Acetone C C B X B C B

1: Acid concentration less than 0.5%

A: Applicable. Replacement required once every 3 years

B: Applicable. Replacement required once a year

C: Applicable. Replacement required once a month

X: Cannot be used


12

ASC-6100


13

Lamps

Single Element Lamps

Name Symbol Part Number Name Symbol Part Number

Aluminum Al 200-38422-01 Nickel Ni 200-38422-15

Antimony Sb 200-38422-24 Niobium Nb 200-38422-32

Arsenic As 200-38422-42 Palladium Pd 200-38422-41

Barium Ba 200-38422-03 Platinum Pt 200-38422-20

Beryllium Be 200-38422-04 Potassium K 200-38422-22

Bismuth Bi 200-38422-43 Rhenium Re 200-38422-44

Boron B 200-38422-39 Rhodium Rh 200-38422-49

Cadmium Cd 200-38422-06 Rubidium Rb 200-38422-33

Calcium Ca 200-38422-05 Ruthenium Ru 200-38422-45

Cerium Ce 200-38422-26 Selenium Se 200-38422-46

Cesium Cs 200-38422-27 Silicon Si 200-38422-16

Chromium Cr 200-38422-07 Silver Ag 200-38422-02

Cobalt Co 200-38422-09 Sodium Na 200-38422-14

Copper Cu 200-38422-08 Strontium Sr 200-38422-34

Dysprosium Dy 200-38422-60 Tantalum Ta 200-38422-35

Gallium Ga 200-38422-40 Tellurium Te 200-38422-47

Germanium Ge 200-38422-11 Thallium Tl 200-38422-74

Gold Au 200-38422-25 Tin Sn 200-38422-18

Iron Fe 200-38422-10 Titanium Ti 200-38422-17

Lanthanum La 200-38422-29 Tungsten W 200-38422-36

Lead Pb 200-38422-21 Vanadium V 200-38422-19

Lithium Li 200-38422-30 Zinc Zn 200-38422-23

Magnesium Mg 200-38422-12 Zirconium Zr 200-38422-37

Manganese Mn 200-38422-13

Mercury Hg 200-38422-28

Molybdenum Mo 200-38422-31


14

Multi-Element-Special Order Items

Base Element Amalgam Metal/s P/N Base Element Amalgam Metal/s P/N

Aluminium Ca 80014625

Chromium Co+Fe+Mn+Ni 80018218

Ca + Fe + Mg 80018135 Cu 80014710

Ca + Mg 80014866 Cu + Co 80018205

Ca+Cu+Fe+Mg+Si+Zn 80018133 Cu + Fe 80018224

Mg 80014627 Cu + Fe + Mn 80018225

Si 80014630 Cu + Fe + Ni 80018227

Si + Ti 80014869 Cu + Mn 80018229

Ti 80014660 Cu + Mn + Ni 80018230

Antimony As + Bi 80014872 Cu + Ni 80018233

Arsenic Se + Te 80014874 Cu + Ni + Ag 80018234

Barium Ca + Mg + Sr 80018161 Cu+Fe+Mn+Ni 80018226

Sr 80014663 Cu+Fe+Ni+Ag 80018228

Cadmium Zn 80014666 Fe 80014713

Calcium Ba 80014669 Fe + Mn 80018236

Ba + Sr 80014876 Fe + Mn + Ni 80018237

Mg 80014672 Fe + Ni 80018239

Mg + Si 80014879 Mn 80014716

Mg + Zn 80014882 Mn + Ni 80018241

Si 80014676 Mo 80014719

Sr 80014680 Ni 80014722

Zn 80014683 Cobalt

Cu 80014725

Chromium Co 80014688 Cu + Fe 80018177

Co + Cu + Fe 80018206 Cu + Fe + Mn 80018178

Co + Cu + Mn 80018213 Cu + Fe + Ni 80018183

Co + Cu + Ni 80018215 Cu + Mn 80018185

Co + Fe 80018216 Cu + Mn + Ni 80018187

Co + Fe + Mn 80018217 Cu+Fe+Mn+Mo 80018179

Co + Fe + Ni 80018219 Cu+Fe+Mn+Ni 80018180

Co + Mn 80018220 Fe 80014728

Co + Mn + Ni 80018221 Fe + Mn + Ni 80018193

Co + Ni 80018223 Mn 80014731

Co+Cu+Fe+Mn 80018207 Mn + Ni 80018199

Co+Cu+Fe+Mn+Mo 80018208 Mo 80014734

Co+Cu+Fe+Mn+Ni 80018209 Ni 80014737

Co+Cu+Fe+Ni 80018212

Co+Cu+Mn+Ni 80018214


15

Multi-Element – Special Order Items

Base Element Amalgam Metal/s P/N Base Element Amalgam Metal/s P/N

Copper Fe 80014740

Molybdenum Co + Cu 80018189

Fe + Mn 80018245 Co + Cu + Fe 80018182

Fe + Mn + Ni 80018247 Co + Cu + Mn 80018186

Fe + Mn + Zn 80018249 Co + Fe 80018196

Fe + Mo 80018251 Co + Fe + Mn 80018192

Fe + Ni 80018252 Co + Mn 80018198

Fe + Ni + Ag 80018253 Cr + Co 80018222

Fe + Zn 80018254 Cr + Cu 80018232

Mn 80014743 Cr + Fe 80018238

Mn + Ni 80018258 Cr + Mn 80018240

Mn + Zn 80018260 Cu + Fe 80018251

Mo 80014746 Cu + Fe + Mn 80018246

Ni 80014748 Cu + Mn 80018257

Zn 80014751 Fe + Mn 80018265

Gold Ag 80014810

Platinum Ag 80014849

Cu 80014755 Silicon

Ti 80014852

Cu + Ni 80018152 Silver

Cr 80014855

Ni 80014758 Cr + Cu 80018128

Pt 80014761 Cu 80014858

Pt + Ag 80018155 Cu + Ni 80018130

Iron Mn 80014814

Sodium K 80014861

Mn + Ni 80018266

Mn + Zn 80018268

Mo 80014817

Ni 80014819

Zn 80014822

Magnesium Si 80014825

Zn 80018278

Manganese Mo 80014828

Ni 80014840

Zn 80014844


16

Single Element Standards

1000 mg/L, (ppm)

Element Name Element Symbol & Matrix Part number Element Name Element Symbol & Matrix Part number

Aluminum Al in 2% HNO3 220-95366-02 Neodymium Nd in 2% HNO3 220-95366-29

Antimony Sb in 5% HNO3 + 0.1% HF 220-95366-14 Nickel Ni in 2% HNO3 220-95366-30

Antimony Sb in 5% Tartaric Acid + 2% HNO3 220-95366-15 Niobium Nb in 2% HNO3 + 0.5% HF 220-95366-31

Arsenic As in 2% HNO3 220-95366-24 Palladium Pd in 10% HNO3 + TrHF 220-95366-32

Barium Ba in 2% HNO3 220-95366-36 Phosphorus P from KH2PO4 in 0.05% HNO3 220-95366-34

Beryllium Be in 2% HNO3 220-95366-44 Phosphorus P in 0.05% HNO3 220-95366-33

Bismuth Bi in 2% HNO3 220-95366-54 Potassium K in 1% HNO3 220-95366-35

Cadmium Cd in 2% HNO3 220-95366-64 Praseodymium Pr in 2% HNO3 220-95366-37

Calcium Ca in 2% HNO3 220-95366-65 Rhenium Re in 2% HNO3 220-95366-38

Cerium Ce in 2% HNO3 220-95366-01 Rubidium Rb in 1% HNO3 220-95366-39

Cesium Cs in 1% HNO3 220-95366-03 Samarium Sm in 2% HNO3 220-95366-40

Chromium Cr in 2% HNO3 220-95366-04 Scandium Sc in 2% HNO3 220-95366-41

Cobalt Co in 2% HNO3 220-95366-05 Selenium Se in 2% HNO3 220-95366-42

Copper Cu in 2% HNO3 220-95366-06 Silver Ag in 2% HNO3 220-95366-43

Dysprosium Dy in 2% HNO3 220-95366-07 Sodium Na in 1% HNO3 220-95366-45

Erbium Er in 2% HNO3 220-95366-08 Strontium Sr in 1% HNO3 220-95366-46

Europium Eu in 2% HNO3 220-95366-09 Tantalum Ta in 2% HNO3 + 0.5% HF 220-95366-47

Gadolinium Gd in 2% HNO3 220-95366-10 Tellurium Te in 2% HNO3 + 0.2% HF 220-95366-48

Gallium Ga in 2% HNO3 220-95366-11 Terbium Tb in 2% HNO3 220-95366-49

Germanium Ge (NH4)2GeF5 in 1% HNO3 220-95366-12 Thallium Tl in 2% HNO3 220-95366-50

Germanium Ge in 2% HNO3 + 0.5% HF 220-95366-13 Thorium Th in 2% HNO3 220-95366-51

Hafnium Hf in 2% HNO3 + 0.5% HF 220-95366-16 Thulium Tm in 2% HNO3 220-95366-52

Holmium Ho in 2% HNO3 220-95366-17 Tin Sn in 2% HNO3 + 0.5% HF 220-95366-53

Indium In in 2% HNO3 220-95366-18 Titanium Ti in 2% HNO3 + 0.1% HF 220-95366-55

Iron Fe in 2% HNO3 220-95366-19 Tungsten W in 2% HNO3 + 1% HF 220-95366-56

Lanthanum La in 2% HNO3 220-95366-20 Uranium U in 2% HNO3 220-95366-57

Lead Pb in 2% HNO3 220-95366-21 Vanadium V in 2% HNO3 220-95366-58

Lithium Li in 1% HNO3 220-95366-22 Ytterbium Yb in 2% HNO3 220-95366-59

Lutetium Lu in 2% HNO3 220-95366-23 Yttrium Y in 2% HNO3 220-95366-60

Magnesium Mg in 2% HNO3 220-95366-25 Zinc Zn in 2% HNO3 220-95366-61

Manganese Mn in 2% HNO3 220-95366-26 Zirconium Zr from ZrO(NO3)2 in 0.5% HNO3 220-95366-62

Mercury Hg in 2% HNO3 220-95366-27 Zirconium Zr in 2% HNO3 + 0.5% HF 220-95366-63

Molybdenum Mo in 2% HNO3 + 0.1% HF 220-95366-28


▶

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For Research Use Only. Not for use in diagnostic procedures.The contents of this publication are provided to you “as is” without warranty of any kind, and are subject to change without notice. Shimadzu does not assume any responsibility or liability for any damage, whether direct or indirect, relating to the use of this publication.

Shimadzu CorporationURL: www.shimadzu.com/AN/

Shimadzu Scientific Instruments7102 Riverwood Drive, Columbia, Maryland 21046, U.S.A.Phone: 800-477-1227/410-381-1227, Fax: 410-381-1222URL: www.ssi.shimadzu.com

Atomic Absorption Spectrophotometers AA-6300 …...TUBE ASSY,TEMPSENS 206-51033-94 TUBE ASSY,INLET...

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Transcript of Atomic Absorption Spectrophotometers AA-6300 …...TUBE ASSY,TEMPSENS 206-51033-94 TUBE ASSY,INLET...