AR3UI+92SPROM: HARI PRASAD Vff MAHBOOBEH MECANIC INORGANIC DATA REVIEWER SENIOR OVERSIGHT CHEMIST...
Transcript of AR3UI+92SPROM: HARI PRASAD Vff MAHBOOBEH MECANIC INORGANIC DATA REVIEWER SENIOR OVERSIGHT CHEMIST...
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION mCENTRAL REGIONAL LABORATORY AOQTTOAW™
201 DEFENSE HIGHWAY **>?«™^ ^ SUITE 200 BRANCH
ANNAPOLIS, MARYLAND 214O1
DATE : November 10, 1994
SUBJECT: Region III Data QA Review
FROM : ' Susanne M. Stevens, ActingRegion III ESAT RPO (3ES30)
TO : Lisa MarinoRegional Project Manager (3HW42)
Attached is the organic data validation report for the Koppers Co.Fac. Plant Site (Case 22655) completed by the Region IIIEnvironmental Services Assistance Team (ESAT) contractor under thedirection of Region III BSD.
If you have any questions regarding this review, please call me at(410) 573-6832.
Attachment
cc: Chris Burns, TetraTech
TID File: 03941100
AR3UI+92SPrinted on Recycled Paper
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?̂LockheedEnvironmental Sen/ices Assistance Teams Phone; (410) 268-7705Region 3 Fax: (410) 268-84721419 Forest Drive, Suite 104Annapolis, Maryland 21403
DATE: OCTOBER 31, 1994
SUBJECT: INORGANIC DATA VALIDATION (IM1 LEVEL)Case 22655 SITE: KOPPERS CO. FAC. PLANT
PROM: HARI PRASAD Vff MAHBOOBEH MECANICINORGANIC DATA REVIEWER SENIOR OVERSIGHT CHEMIST
TO: SUSANNE STEVENSESAT ACTING REGIONAL PROJECT OFFICER
1̂THROUGH://DALE S. BOSHART 'T ESAT TEAM MANAGER
OVERVIEW
Case 22655 consisted of seventeen (17) soil samplesanalyzed for metals by Associated Laboratories Inc. (ALI)according to the Contract Laboratory Program (CLP)Routine Analytical Services (RAS) Statement of Work (SOW)ILM02.1.
SUMMARY
All analytes were successfully analyzed in all samples.The data were validated according to the IM1 Levelprocedure, which includes the review of all QC formsexcept the ones for the Contract Required Detection Limit(CRDL) standard recovery, and excludes the review of theraw data.
Areas of concern with respect to data usability aregiven below according to the seriousness of theproblem.
MINOR ISSUES
The continuing calibration blanks had reported resultsgreater than the Instrument Detection Limit (IDL) for thepotassium (K), selenium (So) and thallium (Tl) analytes.The reported results for these analytes in the affectedsamples which are less than five times the blankconcentration may be biased high and have been qualified"B".
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The ICP serial dilution results were outside the controllimit (10% D) for the calcium (Ca) and manganese (Mn)analytes. The reported results for these analytes areestimated and have been qualified "J".
The matrix spike recovery was low (30%-75%) for theantimony (Sb) analyte. The reported result andquantitation limits for this analyte may be biased lowand have been qualified ML" and "UL", respectively.
Sample MCND22 was collected on 9/19/1994 4nd wasanalyzed for the mercury (Hg) analyte on 10/18/1994,exceeding the twenty-eight (28) day holding period by one(1) day. The reported result for this analyte may bebiased low and has been qualified "L".
The preparation and continuing calibration blanks hadnegative results with absolute value greater than the IDLfor the Se and silver (Ag) analytes, respectively. Thequantitation limits for these analytes may be biased lowand have been qualified "UL".
NOTES
The laboratory flagged the aluminum (Al) analyte on theForm Is with an "*" denoting the laboratory duplicateresults outside the contractual control limit (20% RPD) .Since these results were within the technical controllimit for the soil samples (35% RPD), no action wastaken.
The laboratory analyzed the arsenic (As), lead (Pb),Se and Tl analytes using the ICP method, and had IDLvalues less than CRDL.
The data were reviewed in accordance with the InnovativeApproaches (IMl Level) For Validation of Inorganic Data,September, 1992 and the National Functional Guidelinesfor Evaluating Inorganic Analyses, with modifications foruse within Region III.
ATTACHMENTS
APPENDIX A ANNOTATED FORM Is
APPENDIX B GLOSSARY OF DATA QUALIFIER CODES
APPENDIX C SUPPORT DOCUMENTATION
HP410A06.KOP
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APPENDIX A
ANNOTATED FORM Is
AR3U14928
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U.S. EPA - CLP \_
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND17Lab Name: ASSOCIATED LABORATORIES Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water): SOIL_ Lab Sample ID: MCND17
Level (low/med): LOW_ Date Received: 09/16/94
% Solids: _83.2 0 Q'O 3
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
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U.S. EPA -
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND18Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: *" '"̂ DG No. : llCNDie'
Matrix (soil/water): SOIL_ Lab Sample ID: MCND18
Level (low/med): LOW_ Date Received: 09/16/94
% Solids: _96.5 (J (If) A
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
C682J)!5.70.56[38.8to. 6£0.60rT70(18.8
7.49.6
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1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
Lab Name: ASSOCIATEDLABORATORIES Contract: 68D20043MCND20
_Lab Code: ALI __ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water) : SOIL_ Lab Sample ID: MCND20
Level (low/med): LOW _ Date Received: 09/16/94
% Solids: _82.0 - li ' Ano
Concentration Units (ug/L or mg/kg dry weight) : MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration C
A7100J1 578 UrrrrlI 1071)U.eJ0.61JU/̂ B8\B/35.1I/ 10.4|1 13'7/ 1810013.3
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Comments:L
FORM I - IN ILM02.1
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U.S. EPA - CLP*X
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND21Lab Name: ASSOCIATED_LABORATORIES Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water): SOIL_ ' Lab Sample ID: MCND21
Level (low/med): LOW_ Date Received: 09/16/94
% Solids: _81.1 0 007
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmium .CalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
Cl97q£»—— 5^80.67tllS"U-3.0772
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FORM I - IN ILM02
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U.S. EPA
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND22Lab Name: ASSOCIATED LABORATORIES Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ S'DG No.: MCND16
Matrix (soil/water): SOIL_ Lab Sample ID: MCND22
Level (low/med): LOW_ Date Received: 09/21/94
% Solids: _86.5 0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
T2360Q,' "sTe0.55̂T1861 1-3^07297̂710"29.96.29.9
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Comments :STONES
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND23Lab Name: ASSOCIATED LABORATORIES Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water): SOIL_ Lab Sample ID: MCND23
Level (low/med): LOW_ Date Received: 09/21/94
% Solids: _83.8 0 009
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnes iuraManganeseMercuryNickelPotassiumSeleniumSilverSodiumThallium'VanadiumZincCyanide
Concentration
[11900:— 6T3r"2~:6(82.3\1.10 .__££_9̂ia
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1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND24Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043
I—oc-̂ ln 'tf-v̂ ', K-CjfSt
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND25Lab Name: ASSOCIATED LABORATORIES Contract: 68D20043
. U—1>Lab Code: ALI Case No.: 22655 SAS No.: SDG No.: MCNDlfe
Matrix (soil/water): SOIL_ Lab Sample ID: MCND25
Level (low/med): LOW_ Date Received: 09/21/94,
% Solids: _83.4 (j Q|j
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS NO.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
C2450Q,—— ET77T1.5(72.3\1.5,OT50Toeo^39.310.910.82810014.1
\ 3360\ 135.OTTO[15.0Vl920_0.340.36
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FORM I - IN ILM02.1
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND27Lab Name: ASSOCIATED LABORATORIES Contract: 68D20043
,Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water): SOIL__ Lab Sample ID: MCND27
Level (low/med): LOW_ Date Received: 09/23/94
% Solids: _83.5 0 013
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
\1360Q)" — 6T4^2.3(96.6V 1.0£-&&ri9io:"17.08.65.3
1120010.51920
V 139(T.091
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1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND28Lab Name: ASSOCIATED LABORATORIES Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No. : MCND15
Matrix (soil/water) : SOIL__ Lab Sample ID: MCND28
Level (low/med): LOW_ Date Received: 09/23/94
% Solids: _84.7 0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
ri34ogj6.3
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FORM I - IN ILM02.1
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND30Lab Name: ASSOCIATED_LABORATORIES Contract: 68D20043
~ LoLab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water): SOIL_ Lab Sample ID: MCND30
Level (low/med): LOW_ Date Received: 09/23/94
% Solids: _83.3 0 015
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
nssoji)6.4
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FORM I - IN ILM02.1
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND31Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043
L-oLab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water): SOIL_ Lab Sample ID: MCND31
Level (low/med): LOW_ Date Received: 09/23/94
% Solids: _81.0 ' 0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
(21300\ 10.3
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1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND32Lab Name: ASSOCIATED LABORATORIES Contract: 68D20043
_ - •Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ StiG No.: MCND16
Matrix (soil/water): SOIL_ Lab Sample ID: MCND32
Level (low/med): LOW_ Date Received: 09/24/94
% Solids: _81.2 0 017
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
r 15700;6.0
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/ 19.95.26.6
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FORM I - IN ILM02.1
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MCND33Lab Name: ASSOCIATED LABORATORIES Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water): SOIL_ Lab Sample ID: MCND33
Level (low/med): LOW_ Date Received: 09/24/94•
% Solids: _83.4 O'Otfi
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
. 14300)6.3
rs.v57.6Vl.4.OT57r~533>27.61̂9.29.7
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*N
E
E
-
APPENDIX B
GLOSSARY OF QUALIFIER CODES
-
GLOSSARY OF DATA QUALIFIER CODES (INORGANIC)
CODES RELATED TO IDENTIFICATION(confidence concerning presence or absence of analytes):
U « Not detected. The associated number indicatesapproximate sample concentration necessary to bedetected.
(NO CODE) - Confirmed identification.
B = Not detected substantially above the level reportedin laboratory or field blanks.
R • Unusable result. Analyte may or may not be presentin the sample. Supporting data necessary toconfirm result.
CODES RELATED TO OUANTITATION(can be used for both positive results and sample quantitationlimits):
J = Analyte Present. Reported value may not beaccurate or precise.
K = Analyte present. Reported value may be biasedhigh. Actual value is expected to be lower.
L ~ Analyte present. Reported value may be biased low.Actual value is expected to be higher.
[ ] • Analyte present. As values approach the IDL thequantitation may not be accurate.
UJ = Not detected, quantitation limit may be inaccurateor imprecise.
UL - Not detected, quantitation limit is probablyhigher.
OTHER CODES
Q * No analytical result.
AR3GU9l*7
-
APPENDIX C
SUPPORT DOCUMENTATION
-
U.S. EPA - CLP
COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655 SAS No.: _____ SDG No.:MCND16
SOW No.: ILM02.1
EPA Sample No. Lab Sample ID (J 001_MCND16______ _MCND16________MCND17 MCND17MCND18______ _MCND18"MCND19______ _MCND19IMCND20______ _MCND20MCND21______ _MCND21"MCND21D_____ _MCND21D"MCND21S_____ _MCND21S"MCND22______ _MCND22"MCND23______ _MCND23"MCND24______ _MCND24"MCND25______ _MCND25"MCND26______ _MCND26"MCND27______ _MCND27"MCND28______ _MCND28"MCND30______ _MCND30"MCND31______ _MCND31"MCND32______ _MCND32"MCND33 MCND33
Were ICP interelement corrections applied ? Yes/No YES
Were ICP background corrections applied ? Yes/No YESIf yes - were raw data generated beforeapplication of background corrections ? Yes/No NO_
Comments:
j/Z»*9̂ C jo*, 2.? V N , Frf/tfT~ rti&U I•* —————— * — 3-1 ———— «*— i ———— ' *'-r-ir ———— bL/X(V )̂xv >&;->/
-
in«g-2
AR3UU950
-
intxg-2
-
•) Q O m|J3 21 3 M 3«> ' 5 Sin If !•§ -i5*2il ?0
tnoro-2
see
-
O O O mJ.'ss. 3 =0 Tl
>I-U)s £z
-
d C D-3 2 ̂ ̂O co O' O
-
O
I-AV
C!)O
T xV) Din OUJ o;^ X| £^ UJ
V) ga.
.
-3
te
§^
Zz
toU
% I iZh• • • ^S II * ̂^iu ^ hc£Ou.QUJad ^^ II
-
U.S. EPA - CLP
3BLANKS
U'024Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Preparation Blank Matrix (soil/water): .SOIL_
Preparation Blank Concentration Units (ug/L or mg/kg): MG/KG
Analyte
AluminumAntimonyArsenicBarium __BerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel __PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
InitialCalib.Blank(ug/L) c
32.928.42.810;61.83.0
79.14.012.31.97.91.1
51.91.30.217.3449.81.71.8
84.84.35.55.1
UUUUBUUUUUUUUUUUBUUUBUU
Continuing CalibrationBlank (ug/L)
1 C 2 C 3 C
32.928.42.810.61.63.0
79.14.012.31.913.11.1
51.91.30.217.3
462.2C3.0J)1.8
S4.83.65.55.1
UUUUUUUUUUBUUUUUBBUUUUU
32.928.42.810.61.63.0
79.14.012.32.615.71.151.91.30.217.3
831.9
C-1.8O^*O
3.6, 8.4
5.1
UUUUUUUUUBBUUUUUB&
%UBU
32.928.42.810.61.63.0
84.04.012.31.912.21.151.91.30.217.3
_̂ L52.0l
> 1.884.8C4.07.05.1
UUUUUUBUUUBUUUUUBUUUBBU
Prepa-rationBlank c
6.5805.6800.5602.1200.3200.60015.8200.8002.4600.3802.2200.22010.3800.2600.1003.460
-154.020
0.36016,9600.720-1.4001.020
UUUUUUUUUUBUUUUUBBUUUBU
M
PPPPT-
^
P
P
P
P
P
P
P
cvPPPPPPPPNR
FORM III - IN
AR3UU957
-
U.S. EPA - CLP
3BLANKS
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Preparation Blank Matrix (soil/water): SOIL_
Preparation Blank Concentration Units (ug/L or mg/kg): MG/KG
Analyte
Aluminum\ntimonyrsenicârium __BerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
InitialCalib.Blank(ug/L) C
-
Continuing CalibrationBlank (ug/L)
1 C 2 C 3 C
32.928.42.8
10.61.63.0
79.14.012.31.99.8
-1.751.91.30.2
17.3622.41.7
C-3 . Q>84.83.65.55.1
UUuuuuuuuuBBUUUUBUBUUuu
Prepa-rationBlank C
0.100 u
M
PPPPPPPPPPPPPPcvppppppppNR
FORM III - IN ILM02.1
AR3Ql*958
-
U.S. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY
MCND21SLab Name: ASSOCIATED LABORATORIES Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water): SOIL_ Level (low/med): LOW_
% Solids for Sample: _81.1 0 031
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
ControlLimit%R
75-12575-12575-12575-12575-125
75-12575-12575-125
75-125
75-12575-12575-125
75-12575-125
75-12575-12575-125
Spiked SampleResult (SSR)
34.8469406.3711555.835511.487712.7165
84.6620115.177265.0190
121.5641
284.35100.5897
123.1973
460.61019.1781
426.2381142.3685153.2837
CSample
Result (SR)
6.79970.6704
117.98931.31450.7183
41.15748.571513.0487
11.4882
157.75800.098618.7471
0.40700.4310
0.861936.704151.0936
C
UU
U
B
U
UU
U
SpikeAdded (SA)
107.22428.89428.8910.7210.72
42.89107.2253.61
107.22
107.220.54
107.22
428.8910.72
428.89107.22107.22
%R
32.594.7102.194.9118.6
101.499.496.9
102.7
118.1109.297.4
107.485.6
99.498.595.3
Q
N
M
NRPPPPPNRP
fn?PNRPcvPNRPPNRPPPNR
Comments:
FORM V (Part 1) - IN ILM02.1
AR30i»959
-
U.S. EPA - CLP
5B EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY
MCND21ALab Name: ASSOCIATED LABORATORIES Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water) : SOIL_ Level (low/med): LOW
Concentration Units: ug/L "' 032
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalcium"''•vromiumbait
i— opperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
ControlLimit%R
Spiked SampleResult (SSR)
134.20
CSample
Result (SR)
28.40
C
U
Added (SA)
120.0
%R
111.8
Q M
NRPNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNR
Comments:
FORM V (Part 2} - IN ILM02.1
AR30U960
-
U.S. EPA - CLP
6 EPA SAMPLE NO.DUPLICATES
MCND21DLab Name: ASSOCIATED LABORATORIES Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water): SOIL_ Level (low/med): _LOW_
% Solids for Sample: _81.1 % Solids for Duplicate: _82.3
0 033Concentration Units (ug/L or mg/kg dry weight): MG/KG
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
ControlLimit
47.91.2
6.0
1197.1
9.61197.1
12.0
Sample (S)
19747.88416.79970.6704
117.98931.31450.7183
1057.785541.15748.571513.0487
19716.758611.4882
3529.1442157.75800.098618.7471
1411.41820.40700.4310
332.80260.861936.704151.0936
C
UU
UB
B
U
UUBU
Duplicate (D)
15081.61866.42540.9849
110.02391.18330.6787
922.408635.74709.366612.0816
• 16473.037010.5191
3212.7060169.93400.102815.9278999.10630.38460.4072
307.92200.814529.050147.5797
C
UB
UB
B
U
BUUBU
RPD
26.8
200.07.0
10.5
13.714.18.97.7
17.98.89.47.4
16.334.2
7.8
23.37.1
Q
*
M
PPPPPPPPPPPPPPCVPPPPPPPPNR
FORM VI - IN ILM0271
AR3G496
-
U.S. EPA - CLP
9 EPA SAMPLE NO.ICP SERIAL DILUTION
MCND21LLab Name: ASSOCIATED LABORATORIES Contract: 68D20043
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
Matrix (soil/water): SOIL_ Level (low/med): LOW_
0 037Concentration Units: ug/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Initial SampleResult (I)
82480.0028.402.80
492.805.493.00
4418.00171.9035.8054.50
82350.0047.98
14740.00658.90
78.305895.00
1.701.80
1390.003.60
153.30213.40
C
Uu
UB
B
UUBU
SerialDilutionResult (S)
88450.00142.0014.00506.50
8.0015.00
5945.00191.0061.5054.50
90250.0047.94
15845.00738.50
108.0011915.00
8.509.00
3548.5038.92199.50311.00
C
UuBUuB
UB
B
BBUUBBB
%Differ-ence
7.2
2.8100.0
-Qî GTTTl100.00.09.60.17.5
_£3H237.9
102.1
155.3
30.145.7
Q
E
E
M
PPPPPPPPPPPPPPNRPPPPPPPP
FORM i x - I N AR3UH962 ILM°2'1
-
U.S. EPA - CLP
10Instrument Detection -Limits (Quarterly)
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
ICP ID Number: ICAP61_____ Date: 07/15/94
Flame AA ID Number : __________ (j 038
Furnace AA ID Number :
Comments:
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Wave-length(nm)
237.30206.80
493.40234.80228.80315.80267.70228.60324.70238.20
279.00257.60
231.60766.40
328.07589.50
292.40213.80
Back-ground
CRDL(ug/L)
200601020055
50001050251003
5000150.240
5000510
5000105020
IDL(ug/L)
32.928.4
10.61.63.0
79.14.012.31.97.9
51.91.3
17.3289.0
1.884.8
5.55.1
M
PPNRPPPPPPPPNRPPNRPPNRPPNRPP
FORM X - IN ILM02.1
-
U.S. EPA - CLP
10Instrument Detection-Limits (Quarterly)
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
ICP ID Number: ___________ Date: 07/15/94
Flame AA ID Number : HG-4_______ (J " fiOQ
Furnace AA ID Number :
Comments:
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Wave-length(nm)
253.70
Back-ground
CRDL(ug/L)
200601020055
5000105025100
35000
150.240
5000510
5000105020
IDL(ug/L)
0.2
M
NRNRNR.NRNRNRNRNRNRNRNRNRNRNRCVNRNRNRNRNRNRNRNR
FORM X - IN ILM02.1
-
U.S. EPA - CLP
10Instrument Detection' Limits (Quarterly)
Lab Name: ASSOCIATED__LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.: MCND16
ICP ID Number: 61E-TA_____ Date: 07/15/94
Flame AA ID Number : __________ O
Furnace AA ID Number :
Comments:
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Wave-length(nm)
189.04
220.35
196.02
190.86
Back-ground
CRDL(ug/L)
200601020055
5000105025100
35000
150.240
5000510
5000105020
IDL(ug/L)
2.8
1.1
1.7
3.6
M
NRNRPNRNRNRNRNRNRNRNRPNRNRNRNRNRPNRNRPNRNR
FORM X - IN ILM02.1
-
U.S. EPA - CLP
13PREPARATION LOG
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.;_22655_ SAS No.: _____ SDG No. :MCND16
Method: P_
U'046EPASampleNo.
LCSSMCND16MCND17MCND18MCND19MCND20MCND21MCND21DMCND21SMCND22MCND23MCND24MCND25MCND26MCND27MCND28MCND30MCND31MCND32MCND33PBS
PreparationDate
09/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/9409/28/94
*
Weight(gram)
1.001.051.161.031.031.201.031.091.151.171.081.141.201.101.061.061.071.041.171.081.00
Volume(mL)
200200200200200200200200200200200200200200200200200200200200200
FORM XIII - IN ILM02.1
-
U.S. EPA - CLP
13PREPARATION LOG
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.:_22655_ SAS No.: _____ SDG No.:MCND16
Method: CV
EPASampleNo.
LCSSMCND16MCND17MCND18MCND19MCND20MCND21MCND21DMCND21SMCND22MCND23MCND24MCND25MCND26MCND27MCND28MCND30MCND3 1MCND32MCND33PBS
PreparationDate
10/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/9410/07/94
*
Weight(gram)
0.050.250.260.290.280.260.250.240.230.270.260.260.240.250.270.280.280.280.240.270.20
•
Volume(»L)
100100100100100100100100100100100100100100100100100100100100100
0'0'47
FORM XIII - IN ILM02.1
-
U.S. EPA - CLP
13PREPARATION LOG
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.:_22655_ SAS No.: _____ SDG No. :MCND16
Method: CV
0 0'48EPASampleNo.
LCSSMCND22PBS
PreparationDate
10/18/9410/18/9410/18/94
*
Weight(gram)
0.050.270.20
Volume(mL)
100100100
FORM XIII -flWo, i nro ILM02.1J U 4 j 0 0
-
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No. :MCND16
Instrument ID Number: ICAP61_____ Method: P_
Start Date: 10/05/94 End Date: 10/05/94 "48
EPASampleNo.
SOSsSICVICBCRIICSAICSABICSAICSABCCVCCB— 1PBSLCSSMCND21MCND21DMCND21SMCND16MCND17MCND18MCND19MCND21LCCVCCB -9MCND20MCND22MCND23MCND21AMCND21AMCND24MCND25
D/F
1.001.001.001.001.001.001.001.001.00
lO.O'O10.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.00
Time
09170920092409270928093009330943094709510954095609591002101210161019102210261030103310361040104210441047105110541057110011041107
% R
Analytes
AL
X
X
XX
XXXXXXXX
XXXXXXXXXX
XX
sB
X
X
XXXXX
XXXXXXXXXXXXXXXXXX
XX
As
—
—
BA
X
X
XX
XX
XXXXXXXXXXXXXXXX0(
XX
BE
—
cD
X
X
XXXXX
XXXXXXXXXXXXXXXXX
XX
cA
X
XXX
XX
XXXXXX
XXXXXXXXXX
XX
cR
X
X
XXXXX
XXXXXXXXXXXXXXXXX
XX
c0
X
X
XXXXX
XXXXXXXXXXXXXXXXX
XX
cuX
X
XXXXX
XXXXXXXXXXXXXXXXX
XX
FE
X
X
XX
XX
XXXXXX
XXXXXXXXXX
XX
pB
—
—
—
MG
X
XXX
XX
XXXXXX
XXXXXXXXXX
XX
MN
X
X
XXXXX
XXXXXXXXXXXXXXXXX
XXX
H/"•{j
NI
X
X
XXXXX
XXXXXXXXXXXXXXXXX
XX
K
X
XXX
XX
XXXXXX
XXXXXXXXXX
XX
sEAJ
XX
XXXXX
XXXXXXXXXXXXXXXXX
XX
NA
X
XXX
XX
XXXXXX
XXXXXXXXXX
XX
TL
—
V
X
X
XXXXX
XXXXXXXXXXXXXXXXX
XX
zN
X
X
XXXXX
TrXXXXXXXXXXXXXXXX
XX
cN
-
—
FORM XIV - IN ILM02.1
AR3049.69
-
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.:MCND16
Instrument ID Number: ICAP61_____ Method: P_
Start Date: 10/05/94 End Date: 10/05/94 "
EPASampleNo.
MCND26MCND27MCND32CCVCCBMCND28MCND30MCND31-;ND33.{I
riCSAICSABICSAICSABCCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.00
10.0010.001.001.00
Time
1110111311171119112111241127113011331137113911441148115111531155
% R AL
XXXXXXXXX
XXXX
sB
XXXXXXXXXXXX
XX
AsBA
XXXXXXXXX
XX
XX
BECD
XXXXXXXXXXXX
XX
•
cA
XXXXXXXXX
XX
XX
cR
XXXXXXXXXXXX
XX
•
coXXXXXXXXXXXX
XX
Ar
CuXXXXXXXXXXXX
XX
laJ
FE
XXXXXXXXX
XX
XX
ytpB
.es
MG
XXXXXXXXX
XX
XX
MN
XXXXXXXXXXXX
XX
HG
NI
XXXXXXXXXXXX
XX
K
XXXXXXXXX
XX
XX
sEAG
XXXXXXXXXXXX
XX
NA
XXXXXXXXX
XX
XX
TLV
XXXXXXXXXXXX
XX
zN
XXXXXXXXXXXX
XX
cN
FORM XIV - IN ILM02.1
-
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No. :MCND16
Instrument ID Number: 61E-TA __ Method: P ,. . _—— - u 056Start Date: 10/05/94 End Date: 10/05/94
EPASampleNo.
SOSSSSSSSICVICBCRIICSAICSABCCVCCBiPBSLCSSLCSSMCND21MCND21DMCND21SMCND21SMCND16MCND17MCND21LCCVCCS IMCND18MCND19MCND20MCND22MCND23
D/F
1.001.001.001.001.001.001.001.001.001.001.00
10.0010.001.001.001.001.00
10.001.001.001.005.001.001.005.001.001.001.001.001.001.001.00
Time
09010903090509070908090909110912091709190923092609290931093309390942094409460949095109550957100010021004100710101012101410171019
% R ALSB
AS
XX
XXXXXXXX
XXX
XXXXXXXXXXX
BA
BECDCACRCO
An
CU
al
FE
ytpB
XX
XXXXXXXX
XXXX
XXXXXXXXXX
es
MG
MNHG
NIK SEAG
NATL
XX
XXXXXXXXX
XX
XXXXXXXXXXX
V
s
zN
*^ II *
cN
'
FORM XIV - IN ILM02.1
AR30WI
-
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No.:MCND16
Instrument ID Number: 61E-TA______ Method: P_
Start Date: 10/05/94 End Date: 10/05/94 0 057
EPASampleNo.
MCND24MCND25MCND26MCND27MCND28CCVCCB}MCND30-7ND31JND32
rMCND33CRIICSAICSABCCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.00
10.0010.001.001.00
Time
1022102410271029103110341036103810411043104510481055105811001102
% R ALSB
AS
XXXXXXXXXXXXXXXX
BA
BECDCACRC0
Ar
CU
lai
FE
ytpB
XXXXXXXXXXXXXXXX
.es
MG
MNHG
NIK SEAG
NATL
XXXXXXXXXXXXXXXX
V zNCN
FORM XIV - IN ILM02.1
-
U.S. EPA - CLP
14ANALYSIS RUN LOG
0*058Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No. :MCND16
Instrument ID Number: 61E-TA______ Method: P_
Start Date: 10/05/94 End Date: 10/05/94
EPASampleNo.
SOsssssssICVICBCRIICSAICSABCCVCCB,PBSLCSSMCND21MCND21DMCND21SMCND21SMCND16MCND17MCND21LCCVCCBMCND18MCND19MCND20MCND22MCND23MCND24
D/F
1.001.001.001.001.001.001.001.001.001.001.0010.0010.001.001.001.001.001.001.001.005.001.001.005.001.001.001.001.001.001.001.001.00
Time
13261328133013311332133313351336133713391343134613501352135513571359140114041406140814111413141514181420142214251427142914321434
% R ALSB
ASBA
BECDCA
CRCO
Ar
CU
lal
FE
ytPB
es
MGMNHG
NIK SE
XX
XXXXXXXXXXX
XXXXXXXXXXXX
AG
,
NATL
V
\
zNCN
>
FORM XIV - IN IL.
-
U.S. EPA - CLP
14ANALYSIS RUN LOG ..
Lab Name: ASSOCIATED_LABORATORIES _ Contract: 68D20043 _
Lab Code: ALI __ Case No.: 22655_ SAS No.: _____ SDG No. :MCND16
Instrument ID Number: 61E-TA _____ Method: P_
Start Date: 10/05/94 End Date: 10/05/94
EPASampleNo.
MCND25MCND26MCND27MCND28CCVCCBMCND30MCND31"ND32.1033
[•crtlICSAICSABCCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.0010.0010.001.001.00
Time
143614381441144314451447145014521454145615021506150815101512
% R ALSBAS
•
BA
BECD
•
CACRCo
Ar
CU
laJ
FE
Lyt
PB
:es
MGMNHG
NIK SE
XXXXXXXXXXXXXXX
AG
NATLV z
NCN
FORM XIV - IN ILM02.1
AR3l)l*97l*
-
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: ASSOCIATED_LABORATORIES_ Contract: 68D20043_
Lab Code: ALI__ Case No.: 22655_ SAS No.: _____ SDG No. :MCND16
Instrument ID Number: HG-4_______ Method: CV———— 0'055Start Date: 10/18/94 End Date: 10/18/94
EPASampleNo.
SOS.5SIS5S10ICVICBCRACCVCCBPBSLCSSZZZZZZMCND22CCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
1340134413481352135614001404140814121416142014241428143214361440
% R ALSBASBA
BECDCA
CR
i.
co
Ar
CU
laJ
FE
Lyt
PB
:es
MGMNHG
XXXXXXXXXXXX
XXX
NIK S
EAGNATLV z
NCN
s
FORM XIV - IN ILM02.1
-
In Reference to Case No(s):22655 KOPPERS————————————03940404
Contract Laboratory ProgramREGIONAL/LABORATORY COMMUNICATION SYSTEM
Telephone Record Log
Date of Call: NOVEMBER 1.1994___________________
Sampler Name: ______TETRA TECH________________
Sampler Contact: BETSY RODGERS_______
Region: _____________III____________________________
Regional Contact: J. Janz. ESAT/A. Laae. EPA____________
Call Initiated by: ____ Laboratory X Region ___ SMO
In reference to data for the following sample number(s):
CNF24,CKS98,CKS99,CNF11 TO 14
Summary of Questions/Issues Discussed:
THE FOLLOWING SAMPLE PHASE IS LISTED INCORRECTLY ON THE SHIPPINGLOG. FOR SAMPLE CNF24 THE PHASE IS LISTED AS SOL AND THE SAMPLEIS A TRIP BLANK. THE PHASE NEEDS TO BE LISTED AS AQ. FOR SAMPLECKS98,CKS99,AND CNF11 TO 14 THE PHASE IS LISTED AS AQ AND IT SHOULDBE SOL.
Summary of Resolution:
BETSY RODGERS WILL SEND A REVISED SHIPPING LOG.
tion) Date
Signature (Affixation) Date
Distribution: (1) ORIGINAL TO SAMPLER TETRA TECH BETSY RODGERS 2)EPA RPM- LISA MARINO 3HW42 3) SHIPPING LOG