APPENDIX D - Department of Defence...Geologists Log Drillers Log From (m) To (m) Thickness (m)...
Transcript of APPENDIX D - Department of Defence...Geologists Log Drillers Log From (m) To (m) Thickness (m)...
PSI - BLAMEY BARRACKS KAPOOKA (0315)
APPENDIX D Other searches
14 June 2017 Report No. 1669283_001_R_Rev0 48
PSI - BLAMEY BARRACKS KAPOOKA (0315)
APPENDIX E Registered bore search
14 June 2017 Report No. 1669283_001_R_Rev0 49
NSW Office of WaterWork Summary
GW414660
Licence: 40BL192510 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): STOCK, DOMESTIC
Work Type: Bore
Work Status: Supply Obtained
Construct.Method: Rotary - Percussion (Down Hole Hammer)
Owner Type: Private
Commenced Date: Final Depth: 66.00 mCompletion Date: 15/03/2010 Drilled Depth: 66.00 m
Contractor Name: Alpine Drilling Pty Ltd
Driller: Robert Mark Mclean
Assistant Driller: Paul Gooden
Property: N/A LOT 25 RIVERVIEW DRIVE MOORONG VIA WAGGA WAGGA 2650
Standing Water Level:
3.000
GWMA: Salinity:GW Zone: Yield: 1.000
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.38 25//1148845
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6114314.0 Latitude: 35°06'48.9"SElevation
Source:Unknown Easting: 528753.0 Longitude: 147°18'55.9"E
GS Map: - MGA Zone: 0 Coordinate Source:
GIS - Geographic Information System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 54.00 165 Rotary - Percussion (Down Hole Hammer)
1 Hole Hole 54.00 66.00 120 Rotary - Percussion (Down Hole Hammer)
1 1 Casing Pvc Class 9 0.00 54.00 137 125 Seated on Bottom, Welded, S: 64.00-66.00m
1 1 Opening Slots - Vertical
48.00 54.00 137 1 Casing - Hand Sawn Slot, PVC Class 9, Screwed and Glued, SL: 45.0mm
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw414660.wsr.htm
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
48.00 66.00 18.00 Unknown 3.00 1.00 01:00:00 2200.00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 6.00 6.00 CLAY - RED Clay6.00 20.00 14.00 SILTSTONE - WHITE Siltstone
20.00 54.00 34.00 SILTSTONE - ORANGE Siltstone54.00 66.00 12.00 SILTSTONE - GREEN Siltstone
Remarks
15/03/2010: Form A Remarks: ENTERED BY PATRICIA EWERS ON 6TH APRIL 2011
*** End of GW414660 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw414660.wsr.htm
NSW Office of WaterWork Summary
GW414472
Licence: 40BL192478 Licence Status: ACTIVE
Authorised Purpose(s):
MONITORING BORE
Intended Purpose(s): MONITORING BORE
Work Type: Bore
Work Status: Supply Obtained
Construct.Method:Owner Type: Private
Commenced Date: Final Depth: 5.00 mCompletion Date: 25/06/2010 Drilled Depth: 5.00 m
Contractor Name:Driller: David, Michael Mcmahon
Assistant Driller:
Property: VARIOUS SITES AROUND WAGGA WAGGA TOWNSHIP WAGGA WAGGA 2650
Standing Water Level: 3.600
GWMA: Salinity:GW Zone: Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.38 19//1108268
Licensed:
Region: 40 - Murrumbidgee CMA Map:River Basin: - Unknown Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6114558.0 Latitude: 35°06'41.1"SElevation
Source:Unknown Easting: 528281.0 Longitude: 147°18'37.2"E
GS Map: - MGA Zone: 0 Coordinate Source:
GPS - Global Positioning System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Pvc Class 18 0.00 2.00 501 1 Opening Slots 2.00 5.00 1 PVC Class 18
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw414472.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 5.00 5.00 Clay, loam Clay5.00 5.00 0.00 Rock Rock
Remarks
25/06/2010: Form A Remarks: Marie Campbell 20/10/10
*** End of GW414472 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw414472.wsr.htm
NSW Office of WaterWork Summary
GW414471
Licence: 40BL192478 Licence Status: ACTIVE
Authorised Purpose(s):
MONITORING BORE
Intended Purpose(s): MONITORING BORE
Work Type: Bore
Work Status: Supply Obtained
Construct.Method:Owner Type: Private
Commenced Date: Final Depth: 9.00 mCompletion Date: 25/06/2010 Drilled Depth: 9.20 m
Contractor Name:Driller: David, Michael Mcmahon
Assistant Driller:
Property: VARIOUS SITES AROUND WAGGA WAGGA TOWNSHIP WAGGA WAGGA 2650
Standing Water Level: 8.000
GWMA: Salinity:GW Zone: Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.38 9//1108268
Licensed:
Region: 40 - Murrumbidgee CMA Map:River Basin: - Unknown Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6114517.0 Latitude: 35°06'42.4"SElevation
Source:Unknown Easting: 528702.0 Longitude: 147°18'53.9"E
GS Map: - MGA Zone: 0 Coordinate Source:
GPS - Global Positioning System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Pvc Class 18 0.00 3.00 501 1 Opening Slots 3.00 6.00 1 PVC Class 18
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw414471.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 3.00 3.00 Clay Clay3.00 7.00 4.00 Loam Loam7.00 9.00 2.00 Sand Sand9.00 9.20 0.20 Gravel Gravel
Remarks
25/06/2010: Form A Remarks: Marie Campbell 20/10/10
*** End of GW414471 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw414471.wsr.htm
NSW Office of WaterWork Summary
GW414469
Licence: 40BL192478 Licence Status: ACTIVE
Authorised Purpose(s):
MONITORING BORE
Intended Purpose(s): MONITORING BORE
Work Type: Bore
Work Status: Supply Obtained
Construct.Method:Owner Type: Private
Commenced Date: Final Depth: 5.70 mCompletion Date: 25/06/2010 Drilled Depth: 6.00 m
Contractor Name:Driller: David, Michael Mcmahon
Assistant Driller:
Property: VARIOUS SITES AROUND WAGGA WAGGA TOWNSHIP WAGGA WAGGA 2650
Standing Water Level:
GWMA: Salinity:GW Zone: Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.38 9//1108268
Licensed:
Region: 40 - Murrumbidgee CMA Map:River Basin: - Unknown Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6114222.0 Latitude: 35°06'51.9"SElevation
Source:Unknown Easting: 528697.0 Longitude: 147°18'53.7"E
GS Map: - MGA Zone: 0 Coordinate Source:
GPS - Global Positioning System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Pvc Class 18 0.00 2.70 501 1 Opening Slots 2.70 5.70 1 PVC Class 18
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw414469.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 6.00 6.00 Clay Clay
Remarks
25/06/2010: Form A Remarks: Marie Campbell 15/10/10
*** End of GW414469 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw414469.wsr.htm
NSW Office of WaterWork Summary
GW405097
Licence: 40BL191768 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): STOCK, DOMESTIC
Work Type: Bore
Work Status: Supply Obtained
Construct.Method: Rotary - Percussion (Down Hole Hammer)
Owner Type: Private
Commenced Date: Final Depth: 115.00 mCompletion Date: 24/04/2008 Drilled Depth: 115.00 m
Contractor Name: Dalton Water Drilling Services PTY LTD
Driller: John Michael Dalton
Assistant Driller: A. Dalton
Property: N/A 12 HENSCHKE AVENUE SAN ISIDORE 2650
Standing Water Level:
15.000
GWMA: Salinity:GW Zone: Yield: 2.500
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.33 5//730048
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1S
River Basin: 410 - MURRUMBIDGEE RIVER Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6111854.0 Latitude: 35°08'09.1"SElevation
Source:Unknown Easting: 526019.0 Longitude: 147°17'08.2"E
GS Map: - MGA Zone: 0 Coordinate Source:
GIS - Geographic Information System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 115.00 150 Rotary - Percussion (Down Hole Hammer)
1 1 Casing Pvc Class 9 0.00 33.00 150 138 Driven into Hole, Glued, S: 93.00-115.00m
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
87.00 87.20 0.20 Unknown 15.00 1.50 00:30:00
Page 1 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw405097.wsr.htm
93.00 93.20 0.20 Unknown 15.00 1.00 00:30:00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 1.00 1.00 TOPSOIL Topsoil1.00 5.00 4.00 CLAY Clay5.00 15.00 10.00 SHALE - WEATHERED Shale
15.00 17.00 2.00 SHALE - HARD Shale17.00 31.00 14.00 CLAY Clay31.00 115.00 84.00 SHALE - BLUE Shale
Remarks
24/04/2008: Form A Remarks: ENTERED BY PATRICIA EWERS ON 25TH NOVEMBER 2009
INFORMATION NOT PROVIDED ON FORM A:
NO INFORMATION ON DRAWDOWN LEVEL NO INFORMATION ON SALINITY AND WATER TASTE NO INFORMATION ON PUMPING TESTS ON BORE COMPLETION NO DETAILS ON SLOTS OR SCREENS FOR WATER ENTRY NO DETAILS ON GRAVEL PACK
*** End of GW405097 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw405097.wsr.htm
NSW Office of WaterWork Summary
GW403806
Licence: 40BL191308 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): STOCK, DOMESTIC
Work Type: Bore
Work Status: New Bore
Construct.Method: Auger - Solid Flight
Owner Type: Private
Commenced Date: Final Depth: 10.90 mCompletion Date: 09/02/2007 Drilled Depth: 10.90 m
Contractor Name:Driller: Leo Murray Moloney
Assistant Driller:
Property: N/A 146 ROACH ROAD WAGGA WAGGA 2650
Standing Water Level:
7.000
GWMA: Salinity:GW Zone: Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.38 4//831298
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6115523.0 Latitude: 35°06'09.8"SElevation
Source:Unknown Easting: 528201.0 Longitude: 147°18'34.0"E
GS Map: - MGA Zone: 0 Coordinate Source:
Unknown
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 10.90 900 Auger - Solid Flight1 Annulus Waterworn/Rounded 4.00 4.50 Graded, Q:3.000m3,
PL:Poured/Shovelled1 Annulus Waterworn/Rounded 6.60 10.90 Graded, Q:2.000m3,
PL:Poured/Shovelled1 1 Casing Pvc Class 9 0.00 10.90 165 155 Seated on Bottom, Glued1 1 Opening Slots - Horizontal 7.80 10.90 165 1 Casing - Machine Slotted, PVC
Class 9, Glued, SL: 100.0mm, A: 5.00mm
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403806.wsr.htm
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
7.20 10.90 3.70 Unknown 7.00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 4.50 4.50 BLAY CLAY STIFF Invalid Code4.50 6.30 1.80 GREY/BLACK CLAY Invalid Code6.30 6.60 0.30 FINE DAMP SAND Invalid Code6.60 7.20 0.60 FINE SILTY SAND AND MICA Invalid Code7.20 10.90 3.70 VERY CLEAN COARSE SAND AND
RIVER GRAVELInvalid Code
Remarks
09/02/2007: Form A Remarks: ENTERED BY PATRICIA EWERS 9TH OCTOBER 2007
INFORMATION NOT INCLUDED ON FORM:
NO INFORMATION ON YIELD AND DRAWDOWN LEVEL NO INFORMATION ON SALINITY AND WATER TASTE
*** End of GW403806 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403806.wsr.htm
NSW Office of WaterWork Summary
GW403781
Licence: 40BL191145 Licence Status: ACTIVE
Authorised Purpose(s):
MONITORING BORE
Intended Purpose(s): MONITORING BORE
Work Type: Bore
Work Status: New Bore
Construct.Method: Rotary Mud
Owner Type: Private
Commenced Date: Final Depth: 27.50 mCompletion Date: 20/09/2007 Drilled Depth: 27.50 m
Contractor Name: AQUA DRILLING & GROUTING PTY LTD
Driller: Lee Anthony Strutton
Assistant Driller: Jamie McKenna
Property: WAGGA WAGGA QUARRY ROACH ROAD WAGGA WAGGA 2650
Standing Water Level: 9.000
GWMA: Salinity:GW Zone: Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.38 B//381991
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6116276.0 Latitude: 35°05'45.4"SElevation
Source:Unknown Easting: 527581.0 Longitude: 147°18'09.4"E
GS Map: - MGA Zone: 0 Coordinate Source:
GIS - Geographic Information System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 27.50 200 Rotary Mud1 Annulus Waterworn/Rounded 6.00 16.60 Graded1 Annulus Bentonite/Grout 8.00 9.001 1 Casing Pvc Class 18 0.00 9.60 114 100 Screwed1 1 Opening Slots - Horizontal 9.60 15.60 114 1 Casing - Machine Slotted, PVC
Class 18, Screwed1 1 Casing Pvc Class 18 15.60 16.60 114 100 Screwed, S: 15.60-16.60m
Water Bearing Zones
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403781.wsr.htm
From(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
9.00 27.50 18.50 Unknown 9.00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 1.50 1.50 SILT Silt1.50 11.00 9.50 CLAY Clay
11.00 13.00 2.00 SAND AND GRAVEL Sand13.00 25.00 12.00 GRAVEL AND SAND Gravel
Remarks
20/09/2007: Form A Remarks: ENTERED BY PATRICIA EWERS 4TH OCTOBER 2007
BORE WG 0707 (1 OF 7 MONITORING BORES)
STRATA DETAILS TAKEN FROM GRAPHIC LOG PROVIDED BY CONSULTANT
INFORMATION NOT PROVIDED ON FORM:
NO INFORMATION ON YIELD AND DRAWDOWN LEVEL NO INFORMATION ON SALINITY AND WATER TASTE NO INFORMATION ON PUMPING TESTS ON BORE COMPLETION
*** End of GW403781 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403781.wsr.htm
NSW Office of WaterWork Summary
GW403780
Licence: 40BL191145 Licence Status: ACTIVE
Authorised Purpose(s):
MONITORING BORE
Intended Purpose(s): MONITORING BORE
Work Type: Bore
Work Status: New Bore
Construct.Method: Rotary Mud
Owner Type: Private
Commenced Date: Final Depth: 30.00 mCompletion Date: 20/09/2007 Drilled Depth: 30.00 m
Contractor Name: AQUA DRILLING & GROUTING PTY LTD
Driller: Lee Anthony Strutton
Assistant Driller: Jamie McKenna
Property: WAGGA WAGGA QUARRY ROACH ROAD WAGGA WAGGA 2650
Standing Water Level: 9.000
GWMA: Salinity:GW Zone: Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.38 B//381991
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6116939.0 Latitude: 35°05'23.9"SElevation
Source:Unknown Easting: 527075.0 Longitude: 147°17'49.3"E
GS Map: - MGA Zone: 0 Coordinate Source:
GIS - Geographic Information System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 30.00 200 Rotary Mud1 Annulus Bentonite/Grout 5.00 6.001 Annulus Waterworn/Rounded 6.00 16.50 Graded1 1 Casing Pvc Class 18 0.00 9.50 114 100 Screwed1 1 Opening Slots - Horizontal 9.50 15.50 114 1 Casing - Machine Slotted, PVC
Class 18, Screwed1 1 Casing Pvc Class 18 15.50 16.50 114 100 Screwed, S: 15.50-16.50m
Water Bearing Zones
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403780.wsr.htm
From(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
9.00 30.00 21.00 Unknown 9.00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 2.00 2.00 SILT Silt2.00 8.00 6.00 SAND AND GRAVEL Sand8.00 9.00 1.00 GRAVEL AND SAND Gravel9.00 12.00 3.00 SILT Silt
12.00 22.00 10.00 SAND AND GRAVEL Sand22.00 29.60 7.60 SAND Sand29.60 30.00 0.40 BASEMENT Invalid Code
Remarks
20/09/2007: Form A Remarks: ENTERED BY PATRICIA EWERS 3RD OCTOBER 2007
BORE WG 0706 (1 OF 7 MONITORING BORES)
STRATAT DETAIL TAKEN FROM GRAPHIC LOG PROVIDED BY CONSULTANT
INFORMATION NOT PROVIDED ON FORM:-
NO INFORMATION ON YIELD AND DRAWDOWN LEVEL NO INFORMATION ON SALINITY AND WATER TASTE NO INFORMATION ON PUMPING TESTS ON BORE COMPLETION
*** End of GW403780 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403780.wsr.htm
NSW Office of WaterWork Summary
GW403776
Licence: 40BL191145 Licence Status: ACTIVE
Authorised Purpose(s):
MONITORING BORE
Intended Purpose(s): MONITORING BORE
Work Type: Bore
Work Status: New Bore
Construct.Method: Rotary Mud
Owner Type: Private
Commenced Date: Final Depth: 24.00 mCompletion Date: 20/09/2007 Drilled Depth: 24.00 m
Contractor Name: AQUA DRILLING & GROUTING PTY LTD
Driller: Lee Anthony Strutton
Assistant Driller: Jamie McKenna
Property: WAGGA WAGGA QUARRY ROACH ROAD WAGGA WAGGA 2650
Standing Water Level: 9.000
GWMA: Salinity:GW Zone: Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.38 B//381991
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6116795.0 Latitude: 35°05'28.5"SElevation
Source:Unknown Easting: 527527.0 Longitude: 147°18'07.2"E
GS Map: - MGA Zone: 0 Coordinate Source:
GIS - Geographic Information System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 24.00 200 Rotary Mud1 Annulus Waterworn/Rounded 12.00 20.00 Graded1 1 Casing Pvc Class 18 0.00 9.00 114 100 Screwed, S: 15.00-16.00m1 1 Opening Slots - Horizontal 9.00 15.00 114 1 Casing - Machine Slotted, PVC
Class 18, Screwed
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Duration(hr)
Salinity(mg/L)
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403776.wsr.htm
Hole Depth(m)
9.00 24.00 15.00 Unknown 9.00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 8.00 8.00 SILT Silt8.00 9.00 1.00 SANDY SILT Invalid Code9.00 10.00 1.00 SAND Sand
10.00 24.00 14.00 GRAVEL AND SAND Gravel
Remarks
20/09/2007: Form A Remarks: ENTERED BY PATRICIA EWERS 3RD OCTOBER 2007
BORE WG 0702 (1 OF 7 MONITORING BORES)
STRATA INFORMATION TAKEN FROM GRAPHIC LOG PROVIDED BY CONSULTANT
INFORMATION NOT PROVIDED ON FORM:-
NO INFORMATION ON YIELD AND DRAWDOWN LEVEL NO INFORMATION ON SALINITY AND WATER TASTE NO INFORMATION ON PUMPING TESTS ON BORE COMPLETION
*** End of GW403776 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403776.wsr.htm
NSW Office of WaterWork Summary
GW403775
Licence: 40BL191145 Licence Status: ACTIVE
Authorised Purpose(s):
MONITORING BORE
Intended Purpose(s): MONITORING BORE
Work Type: Bore
Work Status: New Bore
Construct.Method: Rotary Mud
Owner Type: Private
Commenced Date: Final Depth: 30.00 mCompletion Date: 20/09/2007 Drilled Depth: 30.00 m
Contractor Name: AQUA DRILLING & GROUTING PTY LTD
Driller: Lee Anthony Strutton
Assistant Driller: Jamie McKenna
Property: WAGGA WAGGA QUARRY ROACH ROAD WAGGA WAGGA 2650
Standing Water Level: 9.000
GWMA: Salinity:GW Zone: Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.38 B//381991
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6116467.0 Latitude: 35°05'39.2"SElevation
Source:Unknown Easting: 527754.0 Longitude: 147°18'16.2"E
GS Map: - MGA Zone: 0 Coordinate Source:
GIS - Geographic Information System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 30.00 200 Rotary Mud1 Annulus Waterworn/Rounded 12.00 20.00 Graded1 1 Casing Pvc Class 18 0.00 13.00 114 100 Screwed1 1 Opening Slots - Horizontal 13.00 19.00 114 1 Casing - Machine Slotted, PVC
Class 18, Screwed1 1 Casing Pvc Class 18 19.00 20.00 114 100 Screwed, S: 19.00-20.00m
Water Bearing ZonesWBZ Type
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403775.wsr.htm
From(m)
To(m)
Thickness(m)
S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
9.00 30.00 21.00 Unknown 9.00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 2.00 2.00 SILT Silt2.00 8.00 6.00 SANDY SILT Invalid Code8.00 11.00 3.00 SAND Sand
11.00 13.00 2.00 GRAVEL AND SAND Gravel13.00 16.00 3.00 SAND Sand16.00 30.00 14.00 GRAVEL AND SAND Gravel
Remarks
03/10/2007: Form A Remarks: ENTERED BY PATRICIA EWERS ON 3RD OCTOBER 2007
DETAILS FOR BORE WG0701 (1 OF 7 MONITORING BORES)
STRATA DETAIL OBTAINED FROM GRAPHIC LOG PROVIDED BY CONSULTANT
INFORMATION NOT PROVIDED ON FORM:-
NO INFORMATION ON YIELD AND DRAWDOWN LEVEL NO INFORMATION ON SALINITY OR WATER TASTE NO INFORMATION ON PUMPING TESTS ON BORE COMPLETION NO INFORMATION ON WHO CHOSE BORE LOCATION
*** End of GW403775 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403775.wsr.htm
NSW Office of WaterWork Summary
GW403648
Licence: 40BL191103 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK
Intended Purpose(s):
Work Type: Bore
Work Status: New Bore
Construct.Method: Auger - Hollow Flight
Owner Type: Private
Commenced Date: Final Depth: 13.30 mCompletion Date: 19/01/2007 Drilled Depth: 13.30 m
Contractor Name: Leo Murray MOLONEY
Driller: Leo Murray Moloney
Assistant Driller:
Property: TS & CR 34463 STURT HIGHWAY YARRAGUNDRY VIA WAGGA WAGGA 2650
Standing Water Level:
6.000
GWMA: - Salinity:GW Zone: - Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.33 LOT 207
DP754567Licensed: MITCHELL URANQUINTY Whole Lot
207//754567
Region: 40 - Murrumbidgee CMA Map:River Basin: - Unknown Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6114143.0 Latitude: 35°06'55.0"SElevation
Source:Unknown Easting: 523815.0 Longitude: 147°15'40.8"E
GS Map: - MGA Zone: 0 Coordinate Source: GIS - Geographic Information System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 13.30 900 Auger - Hollow Flight1 Annulus Waterworn/Rounded 6.00 13.30 Graded, Q:4.000m3,
PL:Poured/Shovelled1 1 Casing Pvc Class 9 0.00 13.30 164 150 Seated on Bottom, Glued1 1 Opening Slots - Horizontal 10.90 12.80 164 1 Casing - Hand Sawn Slot, PVC
Class 9, Glued, SL: 100.0mm, A: 5.00mm
Page 1 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw403648.wsr.htm
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
10.90 22.80 11.90 Unknown 6.00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.30 0.30 TOPSOIL Topsoil0.30 6.00 5.70 BROWN CLAY Clay6.00 10.30 4.30 GREY BROWN CLAY Invalid Code
10.30 10.90 0.60 STIFF BROWN CLAY Invalid Code10.90 12.80 1.90 CLEAN GREY GRAVEL Invalid Code12.80 13.30 0.50 SILTY GRAVEL Invalid Code
Remarks
*** End of GW403648 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw403648.wsr.htm
NSW Office of WaterWork Summary
GW403437
Licence: 40BL190788 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): TEST BORE
Work Type: Bore
Work Status:Construct.Method:
Owner Type:
Commenced Date: Final Depth: 58.00 mCompletion Date: 07/03/2006 Drilled Depth: 58.00 m
Contractor Name: STRATHMERTON DRILLING PTY LTD
Driller: Gordon George Chatterton
Assistant Driller:
Property: PARAFIELD CLOUGHS ROAD YARRAGUNDRY VIA WAGGA WAGGA 2650
Standing Water Level:
29.000
GWMA: - Salinity:GW Zone: - Yield: 0.400
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.39 59 754573
Licensed: MITCHELL YARRAGUNDRY Whole Lot 59//754573
Region: 40 - Murrumbidgee CMA Map:River Basin: - Unknown Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6111098.0 Latitude: 35°08'34.0"SElevation
Source:Unknown Easting: 521658.0 Longitude: 147°14'15.9"E
GS Map: - MGA Zone: 0 Coordinate Source: Map Interpretation
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 58.00 200 Rotary Mud1 Annulus Waterworn/Rounded 45.00 48.001 1 Casing P.V.C. 0.00 53.00 130 Screwed1 1 Opening Slots 53.00 54.00 130 1 Stainless Steel1 1 Opening Slots 57.00 58.00 130 1 Stainless Steel
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Duration(hr)
Salinity(mg/L)
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403437.wsr.htm
Hole Depth(m)
53.00 58.00 5.00 Unknown 29.00 04:00:00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 2.00 2.00 Sand, dry Sand2.00 53.00 51.00 Clay, pink granite Clay
53.00 58.00 5.00 Granite, decomposed Granite
Remarks
*** End of GW403437 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403437.wsr.htm
NSW Office of WaterWork Summary
GW403324
Licence: 40BL190084 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): STOCK, DOMESTIC
Work Type: Bore
Work Status:Construct.Method:
Owner Type:
Commenced Date: Final Depth: 39.00 mCompletion Date: 27/04/2005 Drilled Depth: 39.00 m
Contractor Name: BRIAN DAYMAN
Driller: Brian Keith Dayman
Assistant Driller:
Property: N/A 75 CLOUGHS ROAD YARRAGUNDRY VIA WAGGA WAGGA 2650
Standing Water Level:
6.300
GWMA: - Salinity:GW Zone: - Yield: 1.500
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.33 LT1 DP33709
Licensed: MITCHELL URANQUINTY Whole Lot 1//33709
Region: 40 - Murrumbidgee CMA Map: 8327-4N
River Basin: - Unknown Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6113634.0 Latitude: 35°07'11.6"SElevation
Source:(Unknown) Easting: 522558.0 Longitude: 147°14'51.3"E
GS Map: - MGA Zone: 0 Coordinate Source: Map Interpretation
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 39.00 280 Rotary Mud1 1 Casing Pvc Class 12 0.00 16.00 165 135 Suspended in Clamps, Glued1 1 Opening Slots 16.00 19.00 165 1 PVC Class 121 1 Casing Pvc Class 12 19.00 19.50 165 135 Glued
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
16.00 19.00 3.00 Unknown 6.30 12.00 1.50 15.00 04:00:00
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403324.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 2.00 2.00 Clay, grey Clay2.00 14.00 12.00 Clay, brown Clay
14.00 16.00 2.00 Clay, grey Clay16.00 19.00 3.00 Gravel, river Gravel19.00 20.00 1.00 Granite, white Granite20.00 34.00 14.00 Granite Granite34.00 35.00 1.00 Rock, hard Rock35.00 38.00 3.00 Granite, white Granite38.00 39.00 1.00 Rock, solid, hard Rock
Remarks
27/04/2005: Form A Remarks: Good supply shallow bore.
*** End of GW403324 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw403324.wsr.htm
NSW Office of WaterWork Summary
GW402526
Licence: 40BL189663 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): STOCK, DOMESTIC
Work Type: Bore
Work Status:Construct.Method: Auger - Solid Flight
Owner Type:
Commenced Date: Final Depth: 12.70 mCompletion Date: 30/06/2003 Drilled Depth: 12.70 m
Contractor Name:Driller: Leo Murray Moloney
Assistant Driller:
Property: N A 191 ROACH ROAD WAGGA WAGGA 2650
Standing Water Level:
6.000
GWMA: - Salinity:GW Zone: - Yield: 7.650
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.038 LT289 DP757249
Licensed: WYNYARD SOUTH WAGGA WAGGA
Whole Lot 92//1061888
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: - Unknown Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6115552.0 Latitude: 35°06'08.8"SElevation
Source:(Unknown) Easting: 528124.0 Longitude: 147°18'30.9"E
GS Map: - MGA Zone: 0 Coordinate Source:
Map Interpretation
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 12.72 900 Auger - Solid Flight1 Annulus Waterworn/Rounded 5.10 12.70 Graded, Q:4.000m31 1 Casing Pvc Class 9 0.00 12.70 125 115 Seated on Bottom, Glued1 1 Opening Slots - Horizontal 7.80 12.60 130 1 Casing - Machine Slotted, PVC
Class 9, SL: 50.0mm, A: 5.00mm
Water Bearing ZonesWBZ Type
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw402526.wsr.htm
From(m)
To(m)
Thickness(m)
S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
6.30 11.80 5.50 Unknown 6.00 7.03 7.65 04:00:00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.30 0.30 Topsoil Topsoil0.30 3.00 2.70 Clay, black Clay3.00 6.00 3.00 Clay, yellow grey Clay6.00 6.30 0.30 Gravel, and clay Gravel6.30 9.00 2.70 Gravel, clean Gravel9.00 10.60 1.60 Sand, fine grey Sand
10.60 11.80 1.20 Gravel, clean Gravel11.80 12.70 0.90 Gravel, silty Gravel
Remarks
*** End of GW402526 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw402526.wsr.htm
NSW Office of WaterWork Summary
GW402141
Licence: 40BL188868 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): STOCK, DOMESTIC
Work Type: Bore
Work Status:Construct.Method: Auger
Owner Type:
Commenced Date: Final Depth: 12.10 mCompletion Date: 27/04/2002 Drilled Depth: 12.10 m
Contractor Name:Driller: Leo Murray Moloney
Assistant Driller:
Property: N/A 191 ROACH ROAD WAGGA WAGGA 2650
Standing Water Level:
7.800
GWMA: - Salinity:GW Zone: - Yield: 7.000
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.038 LT289 DP757249
Licensed: WYNYARD SOUTH WAGGA WAGGA
Whole Lot 91//1061888
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: - Unknown Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6115477.0 Latitude: 35°06'11.3"SElevation
Source:(Unknown) Easting: 527734.0 Longitude: 147°18'15.5"E
GS Map: - MGA Zone: 0 Coordinate Source:
Map Interpretation
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 12.10 900 Auger1 Annulus Waterworn/Rounded 6.00 12.10 Graded, Q:4.000m31 1 Casing Pvc Class 9 0.00 11.80 160 150 Seated on Bottom, Glued1 1 Opening Slots - Horizontal 9.70 11.50 160 1 Mechanically Slotted, PVC
Class 9, SL: 100.0mm, A: 4.00mm
Water Bearing ZonesWBZ Type
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw402141.wsr.htm
From(m)
To(m)
Thickness(m)
S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
9.60 11.80 2.20 Unknown 7.80 8.70 7.00 02:00:00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.30 0.30 Topsoil Topsoil0.30 9.00 8.70 Clay, yellow brown Clay9.00 9.60 0.60 Sandy clay, light grey Invalid Code9.60 11.80 2.20 Sand, clean grey tending to river
gravelSand
11.80 12.10 0.30 Clay, silty grey Clay
Remarks
*** End of GW402141 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw402141.wsr.htm
NSW Office of WaterWork Summary
GW402132
Licence: 40BL187688 Licence Status: CONVERTED
Authorised Purpose(s):
IRRIGATION,FARMING
Intended Purpose(s): IRRIGATION
Work Type: Bore
Work Status:Construct.Method: Rotary
Owner Type:
Commenced Date: Final Depth: 63.50 mCompletion Date: 15/08/2001 Drilled Depth: 68.00 m
Contractor Name: watson drilling
Driller: David Wilton Watson
Assistant Driller:
Property: POMINGALARANA WAGGA WAGGA 2650
Standing Water Level:
9.000
GWMA: 013 - MID MURRUMBIDGEE (U/S NARRANDERA)
Salinity:
GW Zone: - Yield: 54.000
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.033 LTPT1 DP754567
Licensed: MITCHELL URANQUINTY Whole Lot 1//1090274
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: - Unknown Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6114911.0 Latitude: 35°06'30.1"SElevation
Source:(Unknown) Easting: 523489.0 Longitude: 147°15'27.9"E
GS Map: - MGA Zone: 0 Coordinate Source: Map Interpretation
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 43.00 300 Rotary Mud1 Hole Hole 43.00 63.50 225 Rotary Mud1 1 Casing Pvc Class 12 0.00 43.00 300 Heat Shrunk1 1 Opening Screen - Wire
Wound43.00 44.00 225 1 Stainless Steel, Welded, A: 1.75mm
1 1 Opening Screen - Wire Wound
44.00 47.00 225 1 Stainless Steel, Welded, A: 2.00mm
1 1 Casing Pvc Class 12 47.00 53.00 225 Heat Shrunk1 1 Opening Screen - Wire
Wound53.00 54.00 225 1 Stainless Steel, Welded, A: 2.25mm
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw402132.wsr.htm
1 1 Opening Screen - Wire Wound
54.00 55.00 225 1 Stainless Steel, Welded, A: 2.50mm
1 1 Opening Screen - Wire Wound
55.00 56.00 225 1 Stainless Steel, Welded, A: 2.75mm
1 1 Opening Screen - Wire Wound
56.00 63.50 225 1 Stainless Steel, Welded, A: 3.00mm
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
43.00 47.00 4.00 Unknown 9.00 17.0053.00 63.50 10.50 Unknown 9.00 17.00
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.30 0.30 Topsoil, sandy Topsoil0.30 6.00 5.70 Sandy clay Invalid Code6.00 7.00 1.00 Sandy clay, with ill sorted stones Invalid Code7.00 20.00 13.00 Gravel, river with large stones Gravel
20.00 21.00 1.00 Clay, with rocks Clay21.00 23.00 2.00 Clay, brown Clay23.00 25.00 2.00 Clay, dark brown Clay25.00 29.00 4.00 Sand, clay bound, brown Sand29.00 32.00 3.00 Sand, clay bound, grey brown Sand32.00 33.00 1.00 Sand, medium Sand33.00 34.00 1.00 Sand, clay bound, soft Sand34.00 38.00 4.00 Clay, silty grey Clay38.00 41.00 3.00 Sand, silty Sand41.00 42.00 1.00 Sand, grey Sand42.00 43.00 1.00 Sand, grey, dirty Sand43.00 44.00 1.00 Sand, grey, dirty Sand44.00 45.00 1.00 Sand, grey Sand45.00 46.00 1.00 Sand, with clay layer Sand46.00 47.00 1.00 Sand Sand47.00 50.00 3.00 Clay, grey Clay50.00 52.00 2.00 Clay, grey and brown Clay52.00 53.00 1.00 Sand, clean, medium Sand53.00 63.00 10.00 Sand, clean Sand63.00 63.50 0.50 Sand, coarser Sand63.50 65.00 1.50 Clay, light grey Clay65.00 68.00 3.00 Rock, decomposed, red grey Rock
Remarks
*** End of GW402132 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw402132.wsr.htm
NSW Office of WaterWork Summary
GW401710
Licence: 40BL186541 Licence Status: CONVERTED
Authorised Purpose(s):
IRRIGATION
Intended Purpose(s):
Work Type: Bore
Work Status:Construct.Method:
Owner Type:
Commenced Date: Final Depth: 14.00 mCompletion Date: 31/03/1997 Drilled Depth:
Contractor Name: DAN MOLONEY WELL DRILLING
Driller:Assistant Driller:
Property: PARAFIELD OLIVES CLOUGHS ROAD YARRAGUNDRY 2650 NSW
Standing Water Level:
5.000
GWMA: - Salinity:GW Zone: - Yield: 2.300
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.033 23
Licensed: MITCHELL YARRAGUNDRY Whole Lot 17//1124011
Region: 40 - Murrumbidgee CMA Map:River Basin: - Unknown Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6110935.0 Latitude: 35°08'39.3"SElevation
Source:Unknown Easting: 521988.0 Longitude: 147°14'29.0"E
GS Map: - MGA Zone: 0 Coordinate Source: Map Interpretation
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 14.00 152 (Unknown)1 1 Casing Pvc Class 9 0.00 14.00 1521 1 Opening Slots 11.00 14.00 152 1 PVC Class 9
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
11.00 14.00 3.00 Unknown 5.00 11.00 2.30
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw401710.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
Remarks
*** End of GW401710 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw401710.wsr.htm
NSW Office of WaterWork Summary
GW400462
Licence: 40BL186265 Licence Status: ACTIVE
Authorised Purpose(s):
MONITORING BORE
Intended Purpose(s): MONITORING BORE, TEST BORE
Work Type: Bore
Work Status:Construct.Method:
Owner Type:
Commenced Date: Final Depth: 17.00 mCompletion Date: 23/02/1995 Drilled Depth: 17.00 m
Contractor Name: DWR - GROUNDWATER DRILLING
Driller:Assistant Driller:
Property: N/A 2650 Standing Water Level:
GWMA: - Salinity:GW Zone: - Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.038 SALINITY BORE
FIELDLicensed: WYNYARD SOUTH WAGGA
WAGGAWhole Lot //
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6112569.0 Latitude: 35°07'45.8"SElevation
Source:Unknown Easting: 527196.0 Longitude: 147°17'54.6"E
GS Map: - MGA Zone: 0 Coordinate Source:
GPS - Global Positioning System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 17.00 50 Unknown1 1 Casing P.V.C. -0.72 17.00 501 1 Opening Slots 15.00 17.00 50 1 PVC
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw400462.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 2.00 2.00 Topsoil & light brown silty loam Unknown2.00 8.50 6.50 Clay Unknown8.50 10.00 1.50 Clay Unknown
10.00 14.00 4.00 Clay Unknown14.00 15.00 1.00 Clay Unknown15.00 17.00 2.00 Clay Unknown
Remarks
*** End of GW400462 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw400462.wsr.htm
NSW Office of WaterWork Summary
GW400458
Licence: 40BL186265 Licence Status: ACTIVE
Authorised Purpose(s):
MONITORING BORE
Intended Purpose(s): MONITORING BORE, TEST BORE
Work Type: Bore
Work Status:Construct.Method:
Owner Type:
Commenced Date: Final Depth: 11.00 mCompletion Date: 09/01/1995 Drilled Depth: 11.00 m
Contractor Name: DWR - GROUNDWATER DRILLING
Driller:Assistant Driller:
Property: N/A 2650 Standing Water Level:
GWMA: - Salinity:GW Zone: - Yield:
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.038 SALINITY BORE
FIELDLicensed: WYNYARD SOUTH WAGGA
WAGGAWhole Lot //
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER Grid Zone: Scale:Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6113214.0 Latitude: 35°07'24.6"SElevation
Source:Unknown Easting: 529316.0 Longitude: 147°19'18.3"E
GS Map: - MGA Zone: 0 Coordinate Source:
GPS - Global Positioning System
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Hole Hole 0.00 11.00 50 Unknown1 1 Casing P.V.C. -0.68 11.00 501 1 Opening Slots 9.00 11.00 50 1 PVC
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw400458.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.20 0.20 Garden Fill Unknown0.20 1.00 0.80 Clay Unknown1.00 2.00 1.00 Silty Clay Unknown2.00 3.00 1.00 Silty Clay Unknown3.00 5.00 2.00 Silt Unknown5.00 10.00 5.00 Silt Unknown
10.00 11.00 1.00 As for 5-10 but saturated Unknown
Remarks
*** End of GW400458 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw400458.wsr.htm
NSW Office of WaterWork Summary
GW051051
Licence: 40BL110501 Licence Status: CANCELLED
Authorised Purpose(s):
TEST BORE
Intended Purpose(s): RECREATION (GROUNDWATER)
Work Type: Bore
Work Status: Test Hole
Construct.Method: Rotary
Owner Type: Private
Commenced Date: Final Depth: 24.00 mCompletion Date: 01/08/1979 Drilled Depth: 24.00 m
Contractor Name:Driller:
Assistant Driller:
Property: N/A Standing Water Level (m):
GWMA: - Salinity Description: FairGW Zone: - Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.038 300
Licensed: WYNYARD SOUTH WAGGA WAGGA
Whole Lot //
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6113897.0 Latitude: 35°07'02.4"SElevation
Source:(Unknown) Easting: 529271.0 Longitude: 147°19'16.4"E
GS Map: - MGA Zone: 0 Coordinate Source:
GD.,ACC.MAP
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Withdrawn 0.00 0.00 102
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
10.00 14.00 4.00 Unconsolidated 6.4014.00 16.00 2.00 Unconsolidated
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw051051.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.50 0.50 Clay Soil Clay0.50 1.00 0.50 Clay Dark Brownish Clay1.00 2.00 1.00 Clay Light Greyish Clay2.00 5.50 3.50 Clay Clay5.50 7.50 2.00 Clay Light Brownish Grey Streaks Clay7.50 9.00 1.50 Clay Light Greyish Brown Streaks Clay9.00 10.00 1.00 Clay Grey Silty Fine Sand Clay
10.00 14.00 4.00 Sand Medium-coarse Sand14.00 16.00 2.00 Sand Fine Medium-coarse Free Water
BearingSand
16.00 19.00 3.00 Clay Grey Clay19.00 23.00 4.00 Clay Dark Greyish Silty Clay23.00 24.00 1.00 Slate Decomposed Slate10.00 14.00 4.00 Gravel Large Water Bearing Gravel
Remarks
*** End of GW051051 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw051051.wsr.htm
NSW Office of WaterWork Summary
GW044828
Licence: 40BL100147 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): STOCK, DOMESTIC
Work Type: Bore
Work Status:Construct.Method: Rotary
Owner Type: Private
Commenced Date: Final Depth: 36.90 mCompletion Date: 01/05/1974 Drilled Depth: 36.90 m
Contractor Name:Driller:
Assistant Driller:
Property: N/A Standing Water Level (m):
GWMA: - Salinity Description: GoodGW Zone: - Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.033 140
Licensed: MITCHELL URANQUINTY Whole Lot //
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6114708.0 Latitude: 35°06'36.4"SElevation
Source:(Unknown) Easting: 525831.0 Longitude: 147°17'00.4"E
GS Map: - MGA Zone: 0 Coordinate Source:
GD.,ACC.MAP
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Threaded Steel -0.20 36.90 152 Seated on Bottom1 1 Opening Slots 30.80 36.90 152 1
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
20.10 36.90 16.80 Unconsolidated 19.50 0.51
Page 1 of 2
20/03/2017http://allwaterdata.water.nsw.gov.au/wgen/users/897308348//gw044828.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.30 0.30 Topsoil Topsoil0.30 29.87 29.57 Clay Sand Water Supply Clay
29.87 36.88 7.01 Gravel Water Supply Gravel
Remarks
*** End of GW044828 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
20/03/2017http://allwaterdata.water.nsw.gov.au/wgen/users/897308348//gw044828.wsr.htm
NSW Office of WaterWork Summary
GW030269
Licence: Licence Status:
Authorised Purpose(s):
Intended Purpose(s): MONITORING BORE
Work Type: Bore
Work Status: Manual Observations,Monthly
Construct.Method: Rotary Mud
Owner Type: NSW Office of Water
Commenced Date: Final Depth: 24.30 mCompletion Date: 01/05/1972 Drilled Depth: 24.40 m
Contractor Name:Driller:
Assistant Driller:
Property: Standing Water Level (m):
GWMA: Salinity Description: 0-500 ppmGW Zone: Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCHELL URANQUINTRY 1//1090274
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 175.87 m (A.H.D.) Northing: 6114898.000 Latitude: 35°06'30.5"SElevation
Source:(unknown) Easting: 523286.000 Longitude: 147°15'19.9"E
GS Map: - MGA Zone: 55 Coordinate Source: GPS - Global
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Threaded Steel -1.20 23.80 2031 Casing Casing
Protector-1.10 0.00
1 1 Opening Slots 12.90 18.60 203 1
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
11.50 24.30 12.80 Unconsolidated 7.60 1.36
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw030269.wsr.htm
Drillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.61 0.61 Topsoil Topsoil0.61 11.58 10.97 Clay Clay
11.58 24.38 12.80 Gravel Large Stones Coarse Water Supply
Gravel
Remarks
14/04/1976: B/N 30268 ADJ HAS GEOL LOG. 09/05/1979: POMINGALARNA. 03/12/2001: GPS COORDS TAKEN 15/10/01 - OLD COORDS 522998/6114527. 19/01/2009: Nat Carling, 19-Jan-2009: Updated RL's, casing protector details (based on RL's) & cadastre (was entered as '3'), as provided in State Water Survey database.
*** End of GW030269 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw030269.wsr.htm
NSW Office of WaterWork Summary
GW030268
Licence: Licence Status:
Authorised Purpose(s):
Intended Purpose(s): MONITORING BORE
Work Type: Bore
Work Status: Manual Observations,Monthly
Construct.Method: Cable Tool
Owner Type: NSW Office of Water
Commenced Date: Final Depth: 96.90 mCompletion Date: 01/03/1972 Drilled Depth: 97.80 m
Contractor Name:Driller:
Assistant Driller:
Property: Standing Water Level (m):
GWMA: Salinity Description: 0-500 ppmGW Zone: Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCHELL URANQUINTRY 1//1090274
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 175.60 m (A.H.D.) Northing: 6114898.000 Latitude: 35°06'30.5"SElevation
Source:(unknown) Easting: 523286.000 Longitude: 147°15'19.9"E
GS Map: - MGA Zone: 55 Coordinate Source: GPS - Global
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Backfill Backfill 97.00 97.90 1271 Casing Casing
Protector-0.79 0.00
1 1 Casing Threaded Steel -0.70 97.00 1271 1 Casing Withdrawn 0.00 2.90 1331 1 Casing Withdrawn 0.00 96.60 2031 1 Opening Slots 79.20 82.20 127 1 A: 3.17mm1 1 Opening Slots 88.30 91.30 127 2 A: 3.17mm
Water Bearing Zones
Page 1 of 3
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw030268.wsr.htm
From(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
11.50 24.90 13.40 Unconsolidated 7.7025.20 39.80 14.60 Unconsolidated 8.2045.70 60.30 14.60 Unconsolidated 13.70 1.0661.50 63.60 2.10 Unconsolidated77.70 94.10 16.40 Unconsolidated 7.90 0.91
Drillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.61 0.61 Topsoil Topsoil0.61 3.05 2.44 Loam Sandy Loam3.05 4.57 1.52 Silt Sandy Silt4.57 6.40 1.83 Clay Grey Clay6.40 11.58 5.18 Silt Grey Sandy Silt
11.58 14.02 2.44 Gravel Grey Stoney Sand Coarse Water Supply
Gravel
14.02 17.07 3.05 Gravel Sand Water Supply Gravel17.07 24.38 7.31 Gravel Stoney Water Supply Gravel24.38 24.99 0.61 Gravel Yellow Silty Sand Fine Water
SupplyGravel
24.99 25.30 0.31 Clay Grey Clay25.30 30.78 5.48 Gravel Yellow Stoney Sand Coarse
Water SupplyGravel
30.78 33.22 2.44 Gravel Yellow Silty Sand Coarse Water Supply
Gravel
33.22 35.66 2.44 Sand Yellow Silty Fine-coarse Water Supply
Sand
35.66 37.49 1.83 Gravel Fine Water Supply Gravel37.49 38.71 1.22 Sand Purple Silty Fine Water Supply Sand38.71 39.93 1.22 Sand Purple Coarse Water Supply Sand39.93 40.23 0.30 Clay Grey Clay40.23 45.11 4.88 Silt Silt45.11 45.72 0.61 Clay Black Clay45.72 48.77 3.05 Sand Yellow Fine Water Supply Sand48.77 50.60 1.83 Gravel Coarse Water Supply Gravel50.60 54.25 3.65 Sand Yellow Very Coarse Water
SupplySand
54.25 60.35 6.10 Sand Cream Sand Coarse Water Supply
Sand
60.35 61.57 1.22 Clay Grey Silty Clay61.57 62.79 1.22 Sand Yellow Coarse Water Supply Sand62.79 63.70 0.91 Sand Grey Coarse Water Supply Sand63.70 65.53 1.83 Clay Grey Sandy Clay65.53 71.32 5.79 Clay Light Grey Sandy Clay71.32 74.68 3.36 Clay Grey Clay74.68 77.72 3.04 Silt Sandy Silt77.72 81.99 4.27 Sand White Coarse Water Supply Sand81.99 85.65 3.66 Sand White Silty Coarse Water
SupplySand
85.65 86.87 1.22 Silt White Sandy Water Supply Silt86.87 91.14 4.27 Gravel Coarse Water Supply Gravel91.14 94.18 3.04 Sand Silty Fine-coarse Water Supply Sand94.18 97.84 3.66 Granite Decomposed Granite17.07 24.38 7.31 Sand Silty Sand30.78 33.22 2.44 Clay Bands Clay35.66 37.49 1.83 Clay Bands Clay45.72 48.77 3.05 Gravel Medium Gravel48.77 50.60 1.83 Sand Yellow Sand86.87 91.14 4.27 Sand White Silty Water Supply Sand
Remarks
09/12/1978: POMINGALARNA. 03/12/2001: GPS COORDS TAKEN 15/10/01 - OLD COORDS 522998/6114527. 19/01/2009: Nat Carling, 19-Jan-2009: Updated RL's, casing protector details (based on RL's) & cadastre (was entered as '3'), as provided in State Water Survey database. 07/05/2012: Karla Abbs, 7-May-2012: Entered geology log24/10/2014: M.Debono, deleted measurement taken on 03/02/2004 as 7.96m recorded, incorrect based on measurements obtained in Jan and March 2004..
Page 2 of 3
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw030268.wsr.htm
*** End of GW030268 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 3 of 3
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw030268.wsr.htm
NSW Office of WaterWork Summary
GW030065
Licence: Licence Status:
Authorised Purpose(s):
Intended Purpose(s): MONITORING BORE
Work Type: Bore - Nested (2)
Work Status: Manual Observations,6-12 Months
Construct.Method: Cable Tool
Owner Type: NSW Office of Water
Commenced Date: Final Depth: 75.50 mCompletion Date: 01/05/1970 Drilled Depth: 75.60 m
Contractor Name:Driller:
Assistant Driller:
Property: Standing Water Level (m):
GWMA: Salinity Description:GW Zone: Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCHELL URANQUINTRY 13
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 176.60 m (A.H.D.) Northing: 6115755.000 Latitude: 35°06'02.6"SElevation
Source:(unknown) Easting: 524368.000 Longitude: 147°16'02.5"E
GS Map: - MGA Zone: 55 Coordinate Source: GPS - Global
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Casing Casing Protector
-0.95 1.40 203
1 1 Casing P.V.C. -0.30 21.00 631 1 Opening Slots 16.70 18.20 63 1 Slotted On Site1 1 Opening Slots 19.80 21.30 63 1 Slotted On Site1 Casing Casing
Protector-0.95 1.40 203
1 2 Casing P.V.C. -0.30 57.60 631 2 Casing Withdrawn 0.00 60.00 2031 2 Opening Slots 42.60 45.60 63 3 Slotted On Site1 2 Opening Slots 54.80 57.80 63 4 Slotted On Site
Page 1 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw030065.wsr.htm
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
12.80 21.30 8.50 Unconsolidated 6.4040.20 60.30 20.10 Unconsolidated 8.20
Drillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.60 0.60 Topsoil Topsoil0.60 6.70 6.10 Clay Sandy Clay6.70 8.53 1.83 Stones Large Sand Gravel Coarse Gravel8.53 11.58 3.05 Sand Gravel Coarse Stones Sand
11.58 12.80 1.22 Clay Silty Gravel Clay12.80 14.02 1.22 Sand Gravel Coarse Water Supply
StonesSand
14.02 15.24 1.22 Sand Grey Gravel Coarse Water Supply Stones
Sand
15.24 21.33 6.09 Sand Grey Gravel Coarse Water Supply Boulders
Sand
21.33 28.65 7.32 Sand Silty Clay Stones Sand28.65 32.61 3.96 Clay Silty Clay32.61 33.52 0.91 Clay Silty Sandy Clay33.52 34.74 1.22 Clay Silty Clay34.74 35.35 0.61 Clay Clay35.35 38.40 3.05 Clay Silty Sandy Clay38.40 40.84 2.44 Sand Silty Water Supply Stones Sand40.84 54.86 14.02 Sand Grey Coarse Water Supply Sand54.86 55.47 0.61 Gravel Grey Fine Water Supply Gravel55.47 58.52 3.05 Gravel Fine-medium Water Supply Gravel58.52 60.35 1.83 Sand Gravel Coarse Water Supply Sand60.35 61.56 1.21 Clay Sandy Clay61.56 62.78 1.22 Clay Clay62.78 64.61 1.83 Clay Grey Sticky Clay64.61 67.66 3.05 Clay Sticky Clay67.66 68.88 1.22 Clay Grey Clay68.88 75.59 6.71 Granite Decomposed Granite
Remarks
14/04/1976: 2 PVCS INSERTED IN ONE HOLE. 09/05/1979: POMINGALARNA. 03/12/2001: GPS COORDS TAKEN 15/10/01 - OLD COORDS 523999/6115269. 20/04/2009: Nat Carling, 20-Apr-2009: Updated RL's & casing protector details (based on RL's), as provided in State Water Survey database. 15/03/2012: Karla Abbs, 15-Mar-2012: Entered geology log
*** End of GW030065 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw030065.wsr.htm
NSW Office of WaterWork Summary
GW030055
Licence: Licence Status:
Authorised Purpose(s):
Intended Purpose(s): MONITORING BORE
Work Type: Bore - Nested (3)
Work Status: Manual Observations,6-12 Months
Construct.Method: Cable Tool
Owner Type: NSW Office of Water
Commenced Date: Final Depth: 80.10 mCompletion Date: 01/05/1970 Drilled Depth: 80.20 m
Contractor Name:Driller:
Assistant Driller:
Property: Standing Water Level (m):
GWMA: Salinity Description:GW Zone: Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCHELL URANQUINTRY 13
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 174.90 m (A.H.D.) Northing: 6115382.000 Latitude: 35°06'14.7"SElevation
Source:(unknown) Easting: 524443.000 Longitude: 147°16'05.5"E
GS Map: - MGA Zone: 55 Coordinate Source: GPS - Global
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Casing Casing Protector
-1.11 1.40 203
1 1 Casing P.V.C. -0.30 14.90 631 1 Opening Slots 9.10 15.10 63 1 Slotted On Site1 Casing Casing
Protector-1.11 1.40 203
1 2 Casing P.V.C. -0.30 45.40 631 2 Opening Slots 39.60 45.60 63 2 Slotted On Site1 Casing Casing
Protector-1.11 1.40 203
1 3 Casing P.V.C. -0.30 61.80 63
Page 1 of 3
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw030055.wsr.htm
1 3 Casing Withdrawn 0.00 69.10 2031 3 Opening Slots 56.00 62.00 63 3 Slotted On Site
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
10.90 20.60 9.70 Unconsolidated 7.1032.30 48.10 15.80 Unconsolidated 6.8048.70 51.10 2.40 Unconsolidated 7.1056.00 63.30 7.30 Unconsolidated 7.60
Drillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 2.13 2.13 Topsoil Topsoil2.13 3.04 0.91 Loam Sandy Loam3.04 4.87 1.83 Clay Grey Sandy Clay4.87 7.92 3.05 Clay Sandy Clay7.92 9.14 1.22 Sand Silty Sand9.14 10.97 1.83 Sand Silty Gravel Sand
10.97 12.19 1.22 Sand Gravel Coarse Water Supply Stones
Sand
12.19 15.24 3.05 Gravel Stones Coarse Water Supply Gravel15.24 16.45 1.21 Sand Gravel Coarse Water Supply
StonesSand
16.45 17.67 1.22 Gravel Large Water Supply Stones Large
Gravel
17.67 19.50 1.83 Sand Gravel Coarse Water Supply Stones
Sand
19.50 20.72 1.22 Gravel Coarse Water Supply Stones Large Clayey
Gravel
20.72 21.33 0.61 Clay Grey Clay21.33 23.16 1.83 Clay Silty Sandy Clay23.16 24.38 1.22 Clay Gravel Clay24.38 32.30 7.92 Clay Sandy Gravel Clay32.30 39.92 7.62 Sand Grey Coarse Water Supply Sand39.92 40.84 0.92 Basalt Large Boulder Water Supply
SandBasalt
40.84 41.45 0.61 Sand Grey Stones Coarse Water Supply
Sand
41.45 45.72 4.27 Gravel Grey Stones Coarse Water Supply
Gravel
45.72 47.54 1.82 Sand Gravel Coarse Water Supply Stones Large
Sand
47.54 48.15 0.61 Sand Gravel Water Supply Stones Sand48.15 48.76 0.61 Clay Grey Clay48.76 51.20 2.44 Gravel Grey Sand Coarse Water
Supply StonesGravel
51.20 56.08 4.88 Clay Dark Grey Silty Sandy Clay56.08 59.74 3.66 Gravel Grey Fine Water Supply Gravel59.74 62.17 2.43 Sand Gravel Coarse Water Supply
StonesSand
62.17 63.39 1.22 Sand Grey Stones Water Supply Sand63.39 64.00 0.61 Clay Grey Sticky Clay64.00 66.44 2.44 Clay Grey Clay66.44 67.66 1.22 Clay Clay67.66 68.88 1.22 Clay Grey Clay68.88 70.10 1.22 Clay Silty Clay70.10 70.71 0.61 Clay Clay70.71 71.62 0.91 Clay Hard Clay71.62 75.59 3.97 Clay Reddish Clay75.59 80.16 4.57 Clay Red Clay
Remarks
14/04/1976: 3 PVCS INSERTED IN ONE HOLE. 09/05/1979: POMINGALARNA. 03/12/2001: GPS COORDS TAKEN 15/10/01 - OLD COORDS 524250/6115007. 20/04/2009: Nat Carling, 20-Apr-2009: Updated RL's & casing protector details (based on RL's), as provided in State Water Survey database.
Page 2 of 3
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw030055.wsr.htm
15/03/2012: Karla Abbs, 15-mar-2012: Entered geology log
*** End of GW030055 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 3 of 3
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw030055.wsr.htm
NSW Office of WaterWork Summary
GW029570
Licence: 40BL022757 Licence Status: CANCELLED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): IRRIGATION
Work Type: Bore
Work Status:Construct.Method:
Owner Type: Federal Govt
Commenced Date: Final Depth: 76.20 mCompletion Date: 01/11/1967 Drilled Depth: 76.20 m
Contractor Name:Driller:
Assistant Driller:
Property: WERRINGTON Standing Water Level (m):
GWMA: - Salinity Description:GW Zone: - Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.033 115
Licensed: HARDEN CURRAWONG Whole Lot //
Region: 40 - Murrumbidgee CMA Map: 8327-1S
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6110519.0 Latitude: 35°08'52.4"SElevation
Source:(Unknown) Easting: 525541.0 Longitude: 147°16'49.4"E
GS Map: - MGA Zone: 0 Coordinate Source:
GD.,ACC.MAP
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing 0.00 26.20 152 Driven into Hole
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
Geologists Log
Page 1 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657/gw029570.gwgwpf_org....
Drillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.61 0.61 Silt Silt0.61 4.27 3.66 Clay Sand Clay4.27 5.18 0.91 Clay Gravel Clay5.18 12.19 7.01 Clay Soft Clay
12.19 19.51 7.32 Clay Sandy Clay19.51 23.77 4.26 Clay Soft Clay23.77 27.43 3.66 Sandstone Sandstone27.43 36.58 9.15 Clay Soft Clay36.58 48.77 12.19 Clay Sandstone Clay48.77 54.25 5.48 Clay Shale Sandstone Clay54.25 54.86 0.61 Clay Shale Clay54.86 56.08 1.22 Shale Grey Shale56.08 60.96 4.88 Sandstone Yellow Sandstone60.96 69.49 8.53 Clay Sandstone Clay69.49 71.93 2.44 Clay Sandstone Shale Clay71.93 76.20 4.27 Quartz Cream Clay Quartz
Remarks
*** End of GW029570 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657/gw029570.gwgwpf_org....
NSW Office of WaterWork Summary
GW029569
Licence: 40BL020709 Licence Status: ABANDONED
Authorised Purpose(s):
NOT KNOWN
Intended Purpose(s): NOT KNOWN
Work Type: Bore
Work Status:Construct.Method:
Owner Type: Federal Govt
Commenced Date: Final Depth: 91.40 mCompletion Date: 01/11/1967 Drilled Depth: 91.40 m
Contractor Name:Driller:
Assistant Driller:
Property: N/A Standing Water Level (m):
GWMA: - Salinity Description:GW Zone: - Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.033 108
Licensed: MITCHELL URANQUINTY Whole Lot //
Region: 40 - Murrumbidgee CMA Map: 8327-1S
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6110146.0 Latitude: 35°09'04.4"SElevation
Source:(Unknown) Easting: 527007.0 Longitude: 147°17'47.4"E
GS Map: - MGA Zone: 0 Coordinate Source:
GD.,ACC.MAP
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 Casing Casing Protector
0.00 0.00
1 1 Casing Threaded Steel 0.00 51.80 152 Driven into Hole
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
Page 1 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw029569.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 6.10 6.10 Topsoil Gravel Topsoil6.10 9.14 3.04 Clay Red Gravel Clay9.14 12.19 3.05 Clay Gravel Clay
12.19 15.85 3.66 Clay Red Gravel Clay15.85 17.07 1.22 Gravel Coarse Gravel17.07 19.20 2.13 Clay Clay19.20 21.34 2.14 Granite Decomposed Granite21.34 23.16 1.82 Gravel Gravel23.16 35.05 11.89 Clay Red Clay35.05 47.24 12.19 Clay Gravel Clay47.24 84.12 36.88 Shale Black Shale84.12 91.44 7.32 Shale Black Clay Shale
Remarks
12/06/1981: ARMY TRAINING IN BORING
*** End of GW029569 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw029569.wsr.htm
NSW Office of WaterWork Summary
GW029568
Licence: 40BL020707 Licence Status: CANCELLED
Authorised Purpose(s):
RECREATION (GROUNDWATER)
Intended Purpose(s): NOT KNOWN
Work Type: Bore open thru rock
Work Status:Construct.Method:
Owner Type: Federal Govt
Commenced Date: Final Depth: 86.60 mCompletion Date: 01/12/1967 Drilled Depth: 86.60 m
Contractor Name:Driller:
Assistant Driller:
Property: N/A Standing Water Level (m):
GWMA: - Salinity Description:GW Zone: - Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.033 42
Licensed: MITCHELL URANQUINTY Whole Lot //
Region: 40 - Murrumbidgee CMA Map: 8327-1S
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6111226.0 Latitude: 35°08'29.4"SElevation
Source:(Unknown) Easting: 526277.0 Longitude: 147°17'18.4"E
GS Map: - MGA Zone: 0 Coordinate Source:
GD.,ACC.MAP
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Threaded Steel 0.00 36.60 152 Driven into Hole
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
73.20 86.60 13.40 Fractured 67.10 0.30
Page 1 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw029568.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 6.10 6.10 Clay Gravel Clay6.10 22.86 16.76 Clay Sand Clay
22.86 25.91 3.05 Clay Clay25.91 42.67 16.76 Clay Red Clay42.67 51.82 9.15 Clay Yellow Clay51.82 54.86 3.04 Clay Gravel Clay54.86 73.76 18.90 Clay Yellow Clay73.76 86.26 12.50 Shale Black Water Supply Shale86.26 86.56 0.30 Shale Black Water Supply Shale
Remarks
12/06/1981: ARMY TRAINING IN BORING
*** End of GW029568 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw029568.wsr.htm
NSW Office of WaterWork Summary
GW020231
Licence: 40BL013278 Licence Status: ABANDONED
Authorised Purpose(s):
DOMESTIC
Intended Purpose(s): DOMESTIC
Work Type: Well
Work Status:Construct.Method:
Owner Type: Private
Commenced Date: Final Depth: 7.30 mCompletion Date: 01/11/1961 Drilled Depth: 7.30 m
Contractor Name:Driller:
Assistant Driller:
Property: N/A Standing Water Level (m):
GWMA: - Salinity Description:GW Zone: - Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.038 289
Licensed: WYNYARD SOUTH WAGGA WAGGA
Whole Lot //
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6115441.0 Latitude: 35°06'12.4"SElevation
Source:(Unknown) Easting: 528086.0 Longitude: 147°18'29.4"E
GS Map: - MGA Zone: 0 Coordinate Source:
GD.,ACC.MAP
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Concrete Cylnder
0.00 0.00 914
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
5.70 5.70 0.00 Unconsolidated 1.20 0.76
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw020231.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 4.57 4.57 Clay Clay4.57 7.31 2.74 Gravel River Water Supply Gravel
Remarks
*** End of GW020231 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw020231.wsr.htm
NSW Office of WaterWork Summary
GW020218
Licence: 40BL013256 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): GENERAL USE
Work Type: Well
Work Status: Supply Obtained
Construct.Method:Owner Type: Private
Commenced Date: Final Depth: 12.80 mCompletion Date: 01/05/1963 Drilled Depth: 12.80 m
Contractor Name:Driller:
Assistant Driller:
Property: RIVER PARK 86 ROACH ROAD WAGGA WAGGA 2650
Standing Water Level (m):
GWMA: - Salinity Description:GW Zone: - Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: WYNYA WYNYA.038 234
Licensed: WYNYARD SOUTH WAGGA WAGGA
Whole Lot 7//1025035
Region: 40 - Murrumbidgee CMA Map: 8327-1N
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6115593.0 Latitude: 35°06'07.4"SElevation
Source:(Unknown) Easting: 528770.0 Longitude: 147°18'56.4"E
GS Map: - MGA Zone: 0 Coordinate Source:
GD.,ACC.MAP
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Concrete Cylnder
-1.00 -1.00 914
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
6.70 12.80 6.10 Unconsolidated 6.70
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw020218.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 4.27 4.27 Loam Alluvial Loam4.27 6.71 2.44 Sand Dry Sand6.71 9.75 3.04 Sand Small Stones Water Supply Sand9.75 12.80 3.05 Gravel River Water Supply Gravel
Remarks
*** End of GW020218 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw020218.wsr.htm
NSW Office of WaterWork Summary
GW019674
Licence: Licence Status:
Authorised Purpose(s):
Intended Purpose(s): STOCK
Work Type: Bore
Work Status:Construct.Method: Cable Tool
Owner Type: Private
Commenced Date: Final Depth: 29.90 mCompletion Date: 01/01/1946 Drilled Depth:
Contractor Name:Driller:
Assistant Driller:
Property: Standing Water Level (m):
GWMA: Salinity Description: V.SaltyGW Zone: Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.033 23
Licensed:
Region: 40 - Murrumbidgee CMA Map: 8327-4S
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6110929.0 Latitude: 35°08'39.4"SElevation
Source:(Unknown) Easting: 522152.0 Longitude: 147°14'35.4"E
GS Map: - MGA Zone: 0 Coordinate Source:
GD.,ACC.MAP
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Threaded Steel 0.00 29.90 152 Seated on Bottom
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
Geologists Log
Page 1 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw019674.wsr.htm
Drillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
Remarks
*** End of GW019674 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
1/06/2017http://allwaterdata.water.nsw.gov.au/wgen/users/486633300//gw019674.wsr.htm
NSW Office of WaterWork Summary
GW018067
Licence: 40BL010266 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK,DOMESTIC
Intended Purpose(s): STOCK, DOMESTIC
Work Type: Well
Work Status:Construct.Method:
Owner Type: Private
Commenced Date: Final Depth: 16.50 mCompletion Date: 01/01/1960 Drilled Depth: 16.50 m
Contractor Name:Driller:
Assistant Driller:
Property: N/A Standing Water Level (m):
GWMA: - Salinity Description: GoodGW Zone: - Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.033 8 262372
Licensed: MITCHELL URANQUINTY Whole Lot 8//262372
Region: 40 - Murrumbidgee CMA Map: 8327-1S
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6114546.0 Latitude: 35°06'41.8"SElevation
Source:(Unknown) Easting: 524709.0 Longitude: 147°16'16.1"E
GS Map: - MGA Zone: 0 Coordinate Source:
PR.,ACC.MAP
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Concrete Cylnder
-0.80 -0.80 914
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
11.60 16.50 4.90 Unconsolidated 6.10 1.90
Page 1 of 2
20/03/2017http://allwaterdata.water.nsw.gov.au/wgen/users/897308348//gw018067.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 0.91 0.91 Loam Loam0.91 11.58 10.67 Clay Clay
11.58 16.46 4.88 Sand Clay Water Supply Sand
Remarks
*** End of GW018067 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
20/03/2017http://allwaterdata.water.nsw.gov.au/wgen/users/897308348//gw018067.wsr.htm
NSW Office of WaterWork Summary
GW018066
Licence: 40BL010273 Licence Status: CONVERTED
Authorised Purpose(s):
STOCK
Intended Purpose(s): STOCK, DOMESTIC
Work Type: Well
Work Status:Construct.Method:
Owner Type: Private
Commenced Date: Final Depth: 19.80 mCompletion Date: 01/01/1960 Drilled Depth: 19.80 m
Contractor Name:Driller:
Assistant Driller:
Property: N/A Standing Water Level (m):
GWMA: - Salinity Description: GoodGW Zone: - Yield (L/s):
Site Details
Site Chosen By:
County Parish CadastreForm A: MITCH MITCH.033 9 205379
Licensed: MITCHELL URANQUINTY Whole Lot 9//205379
Region: 40 - Murrumbidgee CMA Map: 8327-4S
River Basin: 410 - MURRUMBIDGEE RIVER
Grid Zone: Scale:
Area/District:
Elevation: 0.00 m (A.H.D.) Northing: 6111818.0 Latitude: 35°08'10.5"SElevation
Source:(Unknown) Easting: 522766.0 Longitude: 147°14'59.6"E
GS Map: - MGA Zone: 0 Coordinate Source:
GD.,ACC.MAP
ConstructionNegative depths indicate Above Ground Level; C-Cemented; SL-Slot Length; A-Aperture; GS-Grain Size; Q-Quantity; PL-Placement of Gravel Pack; PC-Pressure Cemented; S-Sump; CE-CentralisersHole Pipe Component Type From
(m)To(m)
Outside Diameter(mm)
Inside Diameter(mm)
Interval Details
1 1 Casing Concrete -0.60 -0.60 508
Water Bearing ZonesFrom(m)
To(m)
Thickness(m)
WBZ Type S.W.L.(m)
D.D.L.(m)
Yield(L/s)
Hole Depth(m)
Duration(hr)
Salinity(mg/L)
16.50 19.90 3.40 Unconsolidated 14.60 1.26
Page 1 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw018066.wsr.htm
Geologists LogDrillers LogFrom(m)
To(m)
Thickness(m)
Drillers Description Geological Material Comments
0.00 16.46 16.46 Loam Clay Loam16.46 19.81 3.35 Sand Gravel Water Supply Sand
Remarks
*** End of GW018066 ***
Warning To Clients: This raw data has been supplied to the NSW Office of Water by drillers, licensees and other sources. The NOW does not verify the accuracy of this data. The data is presented for use by you at your own risk. You should consider verifying this data before relying on it. Professional hydrogeological advice
should be sought in interpreting and using this data.
Page 2 of 2
19/04/2017http://allwaterdata.water.nsw.gov.au/wgen/users/484649657//gw018066.wsr.htm
PSI - BLAMEY BARRACKS KAPOOKA (0315)
APPENDIX F Borehole logs
14 June 2017 Report No. 1669283_001_R_Rev0 50
M
Silty CLAYmedium to high plasticity, brown
CLAYmedium to high plasticity, orange
CLAYmedium plasticity, pale grey with some orange
CLAYlow plasticity, pale grey
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.40
1.30
2.60
HA
PT
AD
T
0315_BH001_0.0DS 0.00-0.10 mR = 0A
0315_BH001_1.0DS 1.00-1.10 mR = 0A
0315_BH001_2.0DS 2.00-2.10 mR = 0A
0315_BH001_3.0DS 3.00-3.10 mR = 0A
0315_BH001_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 15/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH001
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526049.0 m E 6110145.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
M
H
Silty CLAYmedium to high plasticity, orange brown
CLAYhigh plasticity, orange
CLAYmedium plasticity, pale grey with some orange
CLAYlow plasticity, pale grey
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.40
2.60
3.00
HA
PT
AD
T
0315_BH002_0.0DS 0.00-0.10 mR = 0A
0315_BH002_1.0DS 1.00-1.10 mR = 0A
0315_BH002_2.0DS 2.00-2.10 mR = 0A
0315_BH002_3.0DS 3.00-3.10 mR = 0A
0315_BH002_4.0DS 3.90-4.00 mR = 0A
M
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 15/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH002
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526078.0 m E 6110144.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
L
H
H
FILL: Silty CLAYlow plasticity, brown, with some grey shale gravel
CLAYlow to medium plasticity, orange with some grey
CLAYmedium plasticity, grey with some orange
Clayey CLAYmedium to high plasticity, pale grey
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.80
1.60
2.40
HA
PT
AD
T
0315_BH003_0.0DS 0.00-0.10 mR = 0A
0315_BH003_1.0DS 1.00-1.10 mR = 0A
0315_BH003_2.0DS 2.00-2.10 mR = 0A
0315_BH003_3.0DS 3.00-3.10 mR = 0A
0315_BH003_4.0DS 3.90-4.00 mR = 0A
M
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 14/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH003
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526049.0 m E 6110117.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
L
H
Silty CLAYmedium plasticity, grey
CLAYlow to medium plasticity, brown orange
CLAYlow plasticity, pale grey
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.20
1.80
HA
PT
HA
0315_BH004_0.0DS 0.00-0.10 mR = 0APID = 0 ppm
0315_BH004_1.0DS 1.00-1.10 mR = 0A
0315_BH004_2.0DS 2.00-2.10 mR = 0A
0315_BH004_3.0DS 3.00-3.10 mR = 0A
0315_BH004_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 14/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH004
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526064.0 m E 6110113.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
M
H
M
Silty CLAYlow to medium plasticity, brown
CLAYmedium plasticity, brown orange
CLAYmedium plasticity, grey with some yellow
CLAYlow to medium plasticity, brown yellow
CLAYbrown yellow with some orange
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.20
0.60
1.20
2.40
HA
PT
0315_BH005_0.0DS 0.00-0.10 mR = 0A
0315_BH005_1.0DS 1.00-1.10 mR = 0A
0315_BH005_2.0DS 2.00-2.10 mR = 0A
0315_BH005_3.0DS 3.00-3.10 mR = 0A
0315_BH005_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 14/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH005
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526108.0 m E 6110076.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
M-H
H
FILL: Sandy CLAYlow plasticity, brown, fine to medium grained sand
CLAYmedium to high plasticity, red brown, with some ironstone gravel
CLAYmedium plasticity, grey with some red orange
CLAYmedium plasticity, grey orange with some white
CLAYmedium plasticity, red
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.40
1.30
2.20
3.00
HA
PT
AD
T
0315_BH006_0.0DS 0.00-0.10 mR = 0A
0315_BH006_1.0DS 1.00-1.10 mR = 0A
0315_BH006_2.0DS 2.00-2.10 mR = 0A
0315_BH006_3.0DS 3.00-3.10 mR = 0A
0315_BH006_3.0DS 3.90-4.00 mR = 0A
M
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 14/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH006
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526193.0 m E 6110265.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
H
CLAYhigh plasticity, brown orange
CLAYmedium plasticity, orange
CLAYpale grey with some orange
CLAYlow to medium plasticity, white with some orange
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
1.00
2.60
3.20
HA
PT
AD
T
0315_BH007_0.0DS 0.00-0.10 mR = 0A
0315_BH007_1.0DS 1.00-1.10 mR = 0A
0315_BH007_2.0DS 2.00-2.10 mR = 0A
0315_BH007_3.0DS 3.00-3.10 mR = 0A
0315_BH007_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 15/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH007
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526432.0 m E 6110951.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
M
Silty Gravelly CLAYbrown grey
CLAYlow plasticity, orange
CLAYlow to medium plasticity, brown with some orange
CLAYmedium plasticity, grey with some orange
CLAYmedium plasticity, orange with some pale grey
CLAYmedium plasticity, orange
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.40
1.20
2.30
3.20
3.90
HA
PT
0315_BH008_0.0DS 0.00-0.10 mR = 0A
0315_BH008_1.0DS 1.00-1.10 mR = 0A
0315_BH008_2.0DS 2.00-2.10 mR = 0A
0315_BH008_3.0DS 3.00-3.10 mR = 0A
0315_BH008_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 15/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH008
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
H
Silty CLAYlow plasticity, brown, with some angluar to subangular gravel
CLAYmedium plasticity, orange
CLAYmedium plasticity, yellow/orange
CLAYhigh plasticity, pale grey with some orange and black
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.80
2.20
3.60
HA
PT
0315_BH009_0.0DS 0.00-0.10 mR = 0A
0315_BH009_1.0DS 1.00-1.10 mR = 0A
0315_BH009_2.0DS 2.00-2.10 mR = 0A
0315_BH009_3.0DS 3.00-3.10 mR = 0A
0315_BH009_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 15/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH009
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526651.0 m E 6110714.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
M
Silty CLAYlow plasticity, grey brown, with some angular gravel
CLAYlow to medium plasticity, brown
CLAYhigh plasticity, pale brown with some yellow
CLAYhigh plasticity, yellow with some white
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.60
1.60
2.80
HA
PT
0315_BH010_0.0DS 0.00-0.10 mR = 0A
0315_BH010_1.0DS 1.00-1.10 mR = 0A
0315_BH010_2.0DS 2.00-2.10 mR = 0A
0315_BH010_3.0DS 3.00-3.10 mR = 0A
0315_BH010_4.0DS 3.90-4.00 mR = 0A
D
M
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 15/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH010
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526643.0 m E 6110697.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
H
Sandy CLAYlow plasticity, brown, medium to coarse grained, well gradedsand, with some angular gravel
CLAYmedium plasticity, brown, trace subangular gravel
CLAYmedium plasticity, brown with some red
CLAYmedium plasticity, brown
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.80
1.40
3.20
HA
PT
AD
T
0315_BH011_0.0DS 0.00-0.10 mR = 0A
0315_BH011_1.0DS 1.00-1.10 mR = 0A
0315_BH011_2.0DS 2.00-2.10 mR = 0A
0315_BH011_3.0DS 3.00-3.10 mR = 0A
0315_BH011_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 14/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH011
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526051.0 m E 6110389.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
H
Sandy CLAYlow to medium plasticity, brown red, fine to medium grained sand
Sandy CLAYmedium plasticity, brown red, medium grained sand
CLAYmedium plasticity, grey brown with some red
CLAYmedium plasticity, grey with some brown
CLAYlow plasticity, brown
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.90
1.30
2.20
3.40
HA
PT
AD
T
0315_BH012_0.0DS 0.00-0.10 mR = 0A
0315_BH012_1.0DS 1.00-1.10 mR = 0A
0315_BH012_2.0DS 2.00-2.10 mR = 0A
0315_BH012_3.0DS 3.00-3.10 mR = 0A
0315_BH012_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 14/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH012
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526029.0 m E 6110390.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
M
H
H
Sandy CLAYlow to medium plasticity, pale brown, subangular, poorley gradedsand
CLAYmedium plasticity, red
CLAYmedium plasticity, yellow brown
CLAYmedium plasticity, red
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.50
1.00
2.20
HA
PT
AD
T
0315_BH013_0.0DS 0.00-0.10 mR = 0A
0315_BH013_1.0DS 1.00-1.10 mR = 0A
0315_BH013_2.0DS 2.00-2.10 mR = 0A
0315_BH013_3.0DS 3.00-3.10 mR = 0A
0315_BH013_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 14/6/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH013
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526061.0 m E 6110402.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
H
CLAYlow plasticity, pale grey, with some angular gravel
CLAYmedium plasticity, orange
CLAYmedium plasticity, orange with some brown
CLAYmedium plasticity, yellow with some grey
CLAYmedium plasticity, yellow with some grey
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
1.00
2.00
2.40
3.90
HA
PT
0315_BH014_0.0DS 0.00-0.10 mR = 0A
0315_BH014_1.0DS 1.00-1.10 mR = 0A
0315_BH014_2.00DS 2.00-2.10 mR = 0A
0315_BH014_3.0DS 3.00-3.10 mR = 0A
0315_BH014_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 15/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH014
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526506.0 m E 6109566.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
CLAYmedium plasticity, grey, with some gravel
CLAYmedium plasticity, orange
CLAYmedium plasticity, grey with some orange and yellow
CLAYmedium to high plasticity, brown with some yellow
END OF BOREHOLE @ 4.00 mTARGET DEPTHGROUNDWATER NOT ENCOUNTEREDBACKFILLED
0.60
1.40
2.10
HA
PT
AD
T
0315_BH015_0.0DS 0.00-0.10 mR = 0A
0315_BH015_1.0DS 1.00-1.10 mR = 0A
0315_BH015_2.0DS 2.00-2.10 mR = 0A
0315_BH015_3.0DS 3.00-3.10 mR = 0A
0315_BH015_4.0DS 3.90-4.00 mR = 0A
D
SHEET: 1 OF 1
Field Material DescriptionSamplingDrilling
PE
NE
TR
AT
ION
RE
SIS
TA
NC
E
SOIL/ROCK MATERIAL DESCRIPTION
US
CS
SY
MB
OL
RE
CO
VE
RE
D
WA
TE
R
RLDEPTH
DE
PT
H(m
etre
s)
ME
TH
OD
GR
AP
HIC
LOG
SAMPLE ORFIELD TEST
GAP gINT FN. F01aRL3
CLIENT:
PROJECT:
LOCATION:
JOB NO:
DATE: 15/3/17
DATE: 26/4/17
This report of borehole must be read in conjunction with accompanying notes and abbreviations. It has been prepared forenvironmental purposes only, without attempt to consider geotechnical properties or the geotechnical significance of the materials
encountered. As such it should not be relied upon for geotechnical purposes.
REPORT OF BOREHOLE: BH015
Department of Defence
Defence AFFF Category 2 Site PSI - Kapooka
Kapooka
1669283
COORDS: 526525.0 m E 6109562.0 m N MGA94 56
SURFACE RL: DATUM: AHD
INCLINATION: -90°
HOLE DEPTH: 4.00 m
DRILL RIG: Geoprobe 66200DT
CONTRACTOR: Golder Associates
LOGGED: OB
CHECKED: JND
GA
P 8
_13.
0 LI
B.G
LB L
og G
AP
NO
N-C
OR
ED
FU
LL P
AG
E K
AP
OO
KA
.GP
J <
<D
raw
ingF
ile>
> 2
7/04
/201
7 15
:04
8.3
0.00
2 D
atge
l Too
ls
MO
IST
UR
EC
ON
DIT
ION
CO
NS
IST
EN
CY
DE
NS
ITY
STRUCTURE ANDADDITIONAL
OBSERVATIONS
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
PSI - BLAMEY BARRACKS KAPOOKA (0315)
APPENDIX G Data Validation
14 June 2017 Report No. 1669283_001_R_Rev0 51
Golder Associates Pty Ltd.Prepared by: SM 1/05/2013
Checked by:
Number of Primary Samples: Number of Triplicate Samples:Number of Duplicate Samples: Number of Other QAQC Samples:
TypeMBRBRBRB
Sample ID
Anonymous
Analyte Group Primary ID Duplicate IDAll 0315_BH013_0.0_170314 0315_QC100_170314
All 0315_BH005_2.0_170314 0315_QC101_170314
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates
(PFSAs)0315_BH002_1.0_170315 0315_QC102_170315
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates
(PFSAs)0315_BH007_2.0_170315 0315_QC103_170315
All 0315_BH010_1.0_170315 0315_QC104_170315
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates
(PFSAs)0315_BH009_0.0_170315 0315_QC105_170315
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates
(PFSAs)0315_BH014_0.0_170315 0315_QC106_170315
All 0315_BH015_0.0_170315 0315_QC107_170315Perfluoroalkane sulfonic acids &
Perfluoroalkane sulfonates (PFSAs)
0315_SD005_170315 0315_QC108_170315
All 0315_SW005_170315 0315_QC109_170315All 0315_MW006_170316 0315_QC110_170316
Analyte Group Primary ID Triplicate ID
All 0315_BH007_2.0_170315 0315_QC203_170315
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates
(PFSAs)0315_BH009_0.0_170315 0315_QC205_170315
All 0315_BH015_0.0_170315 0315_QC207_170315Perfluoroalkane sulfonic acids &
Perfluoroalkane sulfonates (PFSAs)
0315_SW005_170315 0315_QC209_170315
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates
(PFSAs)0315_MW006_170316 0315_QC210_170316
Analyte Group Analyte(s)
Note: Data validation assesses each analyte in terms of all the data validation variables and only the exceedances and outliers are reported in this form.
*When concentrations are less than the LOR for both primary and duplicate/triplicate results, no RPDs are calculated
Performed By: Olga Bukhteeva Checked By: Tegen AnningDate: 4/04/2017 Date: 4/04/2017
(n:2) Fluorotelomer Sulfonic Acids (ALS)MS recovery of 10:2 Fluorotelomer sulfonic acid (10:2 FTS) was less than lower data quality objective (50-130%) in sample 0315_BH001_0.0_170315 (9.36%).
Perfluoroalkyl Sulfonamides (ALS)MS recoveries of N-Ethyl perfluorooctane sulfonamide (EtFOSA) (22.0%) and N-Ethyl perfluorooctane sulfonamidoethanol (EtFOSE) (15.3%) were less than lower data quality objective (30-130%) in sample 0315_BH001_0.0_170315.
Perfluoroalkyl Carboxylic Acids (ALS) MS recovery of Perfluoropentanoic acid (PFPeA) was less than lower data quality objective (50-130%) in sample 0315_BH001_0.0_170315 (36.2%).
Perfluoroalkyl Carboxylic Acids (ALS)MS recovery of Perfluorotetradecanoic acid (PFTeDA) was less than lower data quality objective (30-130%) in sample 0315_BH001_0.0_170315 (18.2%).
RPD for Perfluorooctane sulfonic acid (PFOS) (36%) exceeded LOR-based control limits. All other FD RPDs were within the accepted LOR based control limits or less than LOR.
All FD RPDs were within the accepted LOR based control limits or less than LOR.
RPDs for Perfluorooctane sulfonic acid (PFOS) (40%) and Perfluorohexane sulfonic acid (PFHxS) (89%) exceeded LOR-based control limits. All other FD RPDs were within the accepted LOR based control limits or less than LOR.
RPD for Perfluorooctane sulfonic acid (PFOS) (122%) exceeded LOR-based control limits. All other FD RPDs were within the accepted LOR based control limits or less than LOR.
Laboratory Duplicates (LD) AnalysesComments
LD RPDs for Perfluorodecanesulfonic acid (PFDS) (200%), Perfluorododecanoic acid (PFDoA) (200%) and Perfluorotridecanoic acid (PFTrDA) (200%) exceeded LOR-based control limits (30%). See comments.
All other laboratory duplicate RPDs are within the laboratory based data quality objectives (Eurofins & ALS).Field Duplicates (FD) Analyses
Analyte Group
Matrix Spike (MS) AnalysesAnalyte Group Comments
Laboratory Control Spike (LCS) AnalysesAnalyte Group Comments
All results were below the LOR.
QAQC Sample Information (Method Blank - MB, Rinsate Blank - RB, Field Blank - FB, Trip Blank - TB)
0315_QC301_170315 All results were below the LOR.0315_QC300_170314 All results were below the LOR.
CommentsMethod Blank
0315_QC302_170316
All All laboratory control spike recoveries were within the laboratory based data quality objectives (Eurofins & ALS).
Sample ID
Comments
Project Name: PSI Cat 2 Blamey Barracks Kapooka (0315) Project Number: 1669283Primary Laboratory: ALS Workorder Number: ES1706394Secondary Laboratory: Eurofins MGT Workorder Number: 538644
14/03/2017 - 16/03/2017 Sample Medium: Soil / Water
Yes All: PFAS suite (standard and trace level)
YesAre there non-NATA accredited methods used? No
COC completed properly?
Yes All samples analysed within the appropriate holding times (Eurofins & ALS).
YesAll requested analysis completed?
This batch has been validated and is considered suitable for environmental interpretive use.
Eurofins & ALS: All surrogate recoveries were within the laboratory based data quality objectives.
As ALS stated: Poor Matrix Spike (MS) recoveries on various analytes is due to matrix interferences and effects. This was confirmed by re-extraction and re-analysis.
No Trip Spike was prepared in this batch.
Laboratory reports signed by authorised personnel? Yes All.
Perfluoroalkyl Sulfonic Acids, Perfluoroalkyl Carboxylic Acids,Perfluoroalkyl Sulfonamides and (n:2) Fluorotelomer
Sulfonic Acids (ALS)
MS recoveries of Perfluorohexane sulfonic acid (PFHxS), Perfluorooctane sulfonic acid (PFOS), Perfluorodecane sulfonic acid (PFDS), Perfluorohexanoic acid (PFHxA), Perfluorooctane sulfonamide (FOSA), 6:2 Fluorotelomer sulfonic acid (6:2 FTS) and 8:2 Fluorotelomer sulfonic acid (8:2 FTS) were not determined in samples 0315_BH001_0.0_170315, 0315_BH005_0.0_170314, 0315_BH009_0.0_170315 and 0315_BH013_0.0_170314. See comments.
Trip Spike Information
Analyte Spike Concentrations Recovery Concentration % Recovery
RPD outliers were reported in the interlaboratory duplicate analyses for Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs). These results are likely due to different sample dilution and preparation methods used between the laboratories or sample heterogeneity. As acceptable RPDs were reported in all other laboratory QA/QC tests performed by ALS/Eurofins and were within acceptable limits the results are not expected to affect the quality of the primary data. As a conservative measure, the highest value will be used for interpretation.
All other MS recoveries were within the laboratory based data quality objectives (Eurofins & ALS).
All results were below the LOR (Eurofins & ALS).
Field Triplicates (FT) AnalysesComments
Surrogate Compound Monitoring Analyses
DATA VALIDATION SUMMARY SHEET
11 3Documentation and Sample Handling Information
Sample Information89 6
Chromatograms supplied as appropriate? N/A
Y/N Comments
Samples received intact and chilled? Yes ALS: 5.7'c - Ice present. Intact. Eurofins: Attempt to chill evident.Samples analysed within appropriate holding times?
Signed by field staff and laboratory personnel.
Sample volumes sufficient for QC analysis?
Date Sampled:
RPDs in various field duplicate analysis exceeded LOR-based control limits. High RPDs are likely a result of sample heterogeneity. These results are not considered to affect the characterisation of the samples as both the primary and duplicate results are within the same order of magnitude.
Various MS recoveries (ALS) were not determined due to background levels being greater than or equal to 4x the spike level.
As stated by Eurofins: "Isotope dilution is used for calibration of each native compound for which an exact labelled analogue is available (Isotope Dilution Quantitation). The isotopically labelled analogues allow identification and recovery correction of the concentration of the associated native PFAS compounds. Where the native PFAS compound does not have labelled analogue then the quantification is made using the Extracted Internal Standard Analyte with the closest retention time to the analyte and no recovery correction has been made (Internal Standard Quantitation)."
The LD RPD reported passes Eurofins | mgt's QC - Acceptance Criteria as defined in the Internal Quality Control Review.
All FD RPDs were within the accepted LOR based control limits or less than LOR.
RPDs for Perfluorohexane sulfonic acid (PFHxS) (71%) and Perfluoropentanoic acid (PFPeA) (162%) exceeded LOR-based control limits. All other FT RPDs were within the accepted LOR based control limits or less than LOR.
RPDs for Perfluorooctanoic Acid (PFOA) (92%), Perfluorohexane sulfonic acid (PFHxS) (43%), Perfluorohexanoic acid (PFHxA) (136%), Perfluoroheptanoic acid (PFHpA) (120%) and Perfluoropentanoic acid (PFPeA) (117%) exceeded LOR-based control limits. All other FT RPDs were within the accepted LOR based control limits or less than LOR.
Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level (Eurofins)
RPD for Perfluorooctanesulfonic acid (PFOS) (43%) exceeded LOR-based control limits. All other FT RPDs were within the accepted LOR based control limits or less than LOR.
All FT RPDs were within the accepted LOR based control limits or less than LOR.
As stated by Eurofins: "Quantification of linear and branched isomers has been conducted as a single total response using the relative response factor for the corresponding linear/branched standard."
All FD RPDs were within the accepted LOR based control limits or less than LOR.
RPD for Perfluorooctane sulfonic acid (PFOS) (72%) exceeded LOR-based control limits. All other FD RPDs were within the accepted LOR based control limits or less than LOR.
All FD RPDs were within the accepted LOR based control limits or less than LOR.
RPDs for Perfluorooctane sulfonic acid (PFOS) (50%) and Perfluoroheptane sulfonic acid (PFHpS) (41%) exceeded LOR-based control limits. All other FD RPDs were within the accepted LOR based control limits or less than LOR.
All FD RPDs were within the accepted LOR based control limits or less than LOR.
Comments
Overall Comments
All FT RPDs were within the accepted LOR based control limits or less than LOR.
CommentsAll FD RPDs were within the accepted LOR based control limits or less than LOR.
Golder Associates Pty Ltd 2 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 MW006 170316 0315 QC110 170316 0315 QC210 170316Project No. : 1669283 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1706394 / 538644 Date Sampled 16/03/2017 16/03/2017 16/03/2017
Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePer- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) µg/L 0.001 <0.001 <0.001 <0.05 ND NDPerfluorodecane sulfonic acid (PFDS) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDPerfluorooctanoic Acid (PFOA) µg/L 0.0005 0.0185 0.023 0.05 21.69% 91.97%Perfluorooctane sulfonic acid (PFOS) µg/L 0.0003 0.0881 0.0888 0.11 0.79% 22.11%Perfluorohexane sulfonic acid (PFHxS) µg/L 0.0005 0.0519 0.0478 0.08 8.22% 42.61%Sum of PFHxS and PFOS (calculated) µg/L 0.0003 0.14 0.137 - 2.17% -PFAS (Sum of total - Lab Reported) µg/L 0.0003 0.204 0.202 - 0.99% -Sum of PFAS (WA DER 10, calculated) µg/L 0.0003 0.192 0.192 - 0.00% -Perfluorobutanoic acid (PFBA) µg/L 0.002 <0.002 <0.002 <0.05 ND NDPerfluorohexanoic acid (PFHxA) µg/L 0.0005 0.0057 0.0051 0.03 11.11% 136.13%Perfluoroheptanoic acid (PFHpA) µg/L 0.0005 0.005 0.0061 0.02 19.82% 120.00%Perfluorodecanoic acid (PFDA) µg/L 0.0005 0.0013 0.0013 <0.01 0.00% NDPerfluoropentanoic acid (PFPeA) µg/L 0.0005 0.0052 0.0048 0.02 8.00% 117.46%Perfluorononanoic acid (PFNA) µg/L 0.0005 0.0025 0.002 <0.01 22.22% NDPerfluorotetradecanoic acid (PFTeDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluorotridecanoic acid (PFTrDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluorododecanoic acid (PFDoDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluoroundecanoic acid (PFUnDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluoroheptane sulfonic acid (PFHpS) µg/L 0.0005 0.0028 0.0023 <0.01 19.61% NDPerfluoropentane sulfonic acid (PFPeS) µg/L 0.0005 0.0057 0.0047 <0.01 19.23% NDPerfluorobutane sulfonic acid (PFBS) µg/L 0.0005 0.0122 0.0113 0.01 7.66% 19.82%4:2 Fluorotelomer sulfonic acid (4:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) µg/L 0.001 0.005 0.005 <0.05 0.00% ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND NDN-Ethyl PFO sulfonamide (EtFOSA) µg/L 0.001 <0.001 <0.001 - ND -N-Ethyl PFO sulfonamidoethanol (EtFOSE) µg/L 0.001 <0.001 <0.001 <0.05 ND NDN-Methyl PFO sulfonamide (MeFOSA) µg/L 0.001 <0.001 <0.001 <0.05 ND NDPerfluorooctane sulfonamide (FOSA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDLegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
RPDs
Golder Associates Pty Ltd 3 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 BH013 0.0 170314 0315 QC100 170314Project No. : 1669283 Sample Type Primary Field DuplicateBatch/es: ES1706394 / 538644 Date Sampled 14/03/2017 14/03/2017
RPDsAnalyte Units LOR Primary vs Duplicate
Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 0.0014 0.0013 7.41%Perfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.0064 0.0062 3.17%Perfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0013 0.0014 7.41%Sum of PFHxS and PFOS (calculated) mg/kg 0.0002 0.0077 0.0076 1.31%PFAS (Sum of total - Lab Reported) mg/kg 0.0002 0.0246 0.0303 20.77%Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 0.0018 0.0017 5.71%Perfluoroheptanoic acid (PFHpA) mg/kg 0.0002 0.002 0.0019 5.13%Perfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 0.003 0.0026 14.29%Perfluorononanoic acid (PFNA) mg/kg 0.0002 0.0009 0.0009 0.00%Perfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 0.006 0.0098 48.10%8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 0.0018 0.0036 66.67%10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 0.0009 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 3.4 2.8 19.35%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
Golder Associates Pty Ltd 4 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 BH005 2.0 170314 0315 QC101 170314Project No. : 1669283 Sample Type Primary Field DuplicateBatch/es: ES1706394 / 538644 Date Sampled 14/03/2017 14/03/2017
RPDsAnalyte Units LOR Primary vs Duplicate
Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0004 0.0004 0.00%Sum of PFHxS and PFOS (calculated) mg/kg 0.0002 0.0004 0.0004 0.00%PFAS (Sum of total - Lab Reported) mg/kg 0.0002 0.0007 0.0004 54.55%Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 0.0003 <0.0002 NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 11.6 10.1 13.82%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
Golder Associates Pty Ltd 5 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 BH002 1.0 170315 0315 QC102 170315Project No. : 1669283 Sample Type Primary Field DuplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017
RPDsAnalyte Units LOR Primary vs Duplicate
Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 0.0003 0.0005 50.00%Perfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.178 0.119 39.73%Perfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0034 0.0089 89.43%Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 0.0009 0.0008 11.76%Perfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 0.0014 NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 0.0003 NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 0.0002 ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 15.7 12.5 22.70%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
Golder Associates Pty Ltd 6 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 BH007 2.0 170315 0315 QC103 170315 0315 QC203 170315Project No. : 1669283 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017 15/03/2017
Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePer- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 <0.01 ND NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 0.0015 0.0005 <0.005 100.00% NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.0054 0.0013 <0.005 122.39% NDPerfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0007 0.0004 <0.005 54.55% NDPerfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 <0.005 ND NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 0.0003 <0.0002 <0.005 ND NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.01 ND ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 - ND -N-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 0.0011 0.0006 <0.01 58.82% NDMoisture % 1 11 13 10 16.67% 9.52%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
RPDs
Golder Associates Pty Ltd 7 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 BH010 1.0 170315 0315 QC104 170315Project No. : 1669283 Sample Type Primary Field DuplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017
RPDsAnalyte Units LOR Primary vs Duplicate
Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 <0.0002 <0.0002 NDSum of PFHxS and PFOS (calculated) mg/kg 0.0002 <0.0002 <0.0002 NDPFAS (Sum of total - Lab Reported) mg/kg 0.0002 0.0008 <0.0002 NDPerfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 0.0008 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 14.4 9 46.15%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
Golder Associates Pty Ltd 8 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 BH009 0.0 170315 0315 QC105 170315 0315 QC205 170315Project No. : 1669283 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017 15/03/2017
Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePer- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 0.0014 <0.005 ND NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 <0.01 ND NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 0.0006 0.0007 <0.005 15.38% NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.324 0.467 0.5 36.16% 42.72%Perfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0038 0.0047 <0.005 21.18% NDPerfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 <0.005 ND NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 0.0009 0.0012 <0.005 28.57% NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 0.0002 <0.005 ND NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 0.0008 <0.005 ND NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 0.0003 <0.005 ND NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 0.002 0.0008 <0.005 85.71% NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 0.0003 <0.005 ND NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 0.0002 <0.005 ND ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.01 ND ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 - ND -N-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 0.001 0.0014 <0.005 33.33% NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 <0.01 ND NDMoisture % 1 3 1.7 2.1 55.32% 35.29%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
RPDs
Golder Associates Pty Ltd 9 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 BH014 0.0 170315 0315 QC106 170315Project No. : 1669283 Sample Type Primary Field DuplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017
RPDsAnalyte Units LOR Primary vs Duplicate
Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 0.0048 0.0037 25.88%Perfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.116 0.0695 50.13%Perfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0483 0.0414 15.38%Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 0.0029 0.0019 41.67%Perfluoroheptanoic acid (PFHpA) mg/kg 0.0002 0.0006 0.0004 40.00%Perfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 0.0012 NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 0.0102 0.0067 41.42%Perfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 0.001 0.0008 22.22%Perfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 0.0012 0.0007 52.63%4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 2 1.2 50.00%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
Golder Associates Pty Ltd 10 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 BH015 0.0 170315 0315 QC107 170315 0315 QC207 170315Project No. : 1669283 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017 15/03/2017
Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePer- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 <0.01 ND NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.0012 0.0006 <0.005 66.67% NDPerfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 <0.0002 0.0002 <0.005 ND NDSum of PFHxS and PFOS (calculated) mg/kg 0.0002 0.0012 0.0008 - 40.00% -PFAS (Sum of total - Lab Reported) mg/kg 0.0002 0.0012 0.0008 - 40.00% -Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 <0.005 ND NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.01 ND ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 - ND -N-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 <0.005 ND NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 <0.005 ND NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 <0.01 ND NDMoisture % 1 2.9 2 2.3 36.73% 23.08%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
RPDs
Golder Associates Pty Ltd 11 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 SD005 170315 0315 QC108 170315Project No. : 1669283 Sample Type Primary Field DuplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017
RPDsAnalyte Units LOR Primary vs Duplicate
Per- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorodecane sulfonic acid (PFDS) mg/kg 0.0002 <0.0002 <0.0002 NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctanoic Acid (PFOA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorooctane sulfonic acid (PFOS) mg/kg 0.0002 0.0053 0.0025 71.79%Perfluorohexane sulfonic acid (PFHxS) mg/kg 0.0002 0.0005 0.0006 18.18%Perfluorobutanoic acid (PFBA) mg/kg 0.001 <0.001 <0.001 NDPerfluorohexanoic acid (PFHxA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptanoic acid (PFHpA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorodecanoic acid (PFDA) mg/kg 0.0002 <0.0002 0.0002 NDPerfluoropentanoic acid (PFPeA) mg/kg 0.0002 <0.0002 0.0072 NDPerfluorononanoic acid (PFNA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorotetradecanoic acid (PFTeDA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorotridecanoic acid (PFTrDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorododecanoic acid (PFDoDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroundecanoic acid (PFUnDA) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoroheptane sulfonic acid (PFHpS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluoropentane sulfonic acid (PFPeS) mg/kg 0.0002 <0.0002 <0.0002 NDPerfluorobutane sulfonic acid (PFBS) mg/kg 0.0002 <0.0002 <0.0002 ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamide (EtFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDN-Ethyl PFO sulfonamidoethanol (EtFOSE) mg/kg 0.0005 <0.0005 <0.0005 NDN-Methyl PFO sulfonamide (MeFOSA) mg/kg 0.0005 <0.0005 <0.0005 NDPerfluorooctane sulfonamide (FOSA) mg/kg 0.0002 <0.0002 <0.0002 NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) mg/kg 0.0002 <0.0002 <0.0002 NDMoisture % 1 66.1 78 16.52%LegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
Golder Associates Pty Ltd 12 of 12
Prepared by: COChecked by: LA
Duplicate Analysis RPDs Sample ID 0315 SW005 170315 0315 QC109 170315 0315 QC209 170315Project No. : 1669283 Sample Type Primary Field Duplicate Field TriplicateBatch/es: ES1706394 / 538644 Date Sampled 15/03/2017 15/03/2017 15/03/2017
Analyte Units LOR Primary vs Duplicate Primary vs Inter DuplicatePer- and polyfluoroalkyl substances (PFAS)N-Methyl PFO sulfonamidoethanol (MeFOSE) µg/L 0.001 <0.001 <0.001 <0.05 ND NDPerfluorodecane sulfonic acid (PFDS) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDN-methyl-PFO sulfonamidoacetic acid (MeFOSAA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDPerfluorooctanoic Acid (PFOA) µg/L 0.0005 0.006 0.0071 <0.01 16.79% NDPerfluorooctane sulfonic acid (PFOS) µg/L 0.0003 0.0551 0.0429 0.07 24.90% 23.82%Perfluorohexane sulfonic acid (PFHxS) µg/L 0.0005 0.0428 0.0388 0.09 9.80% 71.08%Sum of PFHxS and PFOS (calculated) µg/L 0.0003 0.0979 0.0817 - 18.04% -PFAS (Sum of total - Lab Reported) µg/L 0.0003 0.145 0.13 - 10.91% -Sum of PFAS (WA DER 10, calculated) µg/L 0.0003 0.136 0.122 - 10.85% -Perfluorobutanoic acid (PFBA) µg/L 0.002 <0.002 <0.002 <0.05 ND NDPerfluorohexanoic acid (PFHxA) µg/L 0.0005 0.0036 0.0039 < 0.05 8.00% NDPerfluoroheptanoic acid (PFHpA) µg/L 0.0005 0.0023 0.0024 < 0.01 4.26% NDPerfluorodecanoic acid (PFDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluoropentanoic acid (PFPeA) µg/L 0.0005 0.0042 0.0047 0.04 11.24% 161.99%Perfluorononanoic acid (PFNA) µg/L 0.0005 0.0013 0.0015 <0.01 14.29% NDPerfluorotetradecanoic acid (PFTeDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluorotridecanoic acid (PFTrDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluorododecanoic acid (PFDoDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluoroundecanoic acid (PFUnDA) µg/L 0.0005 <0.0005 <0.0005 <0.01 ND NDPerfluoroheptane sulfonic acid (PFHpS) µg/L 0.0005 0.0023 0.0017 <0.01 30.00% NDPerfluoropentane sulfonic acid (PFPeS) µg/L 0.0005 0.0051 0.0049 <0.01 4.00% NDPerfluorobutane sulfonic acid (PFBS) µg/L 0.0005 0.022 0.0217 <0.01 1.37% ND4:2 Fluorotelomer sulfonic acid (4:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND ND6:2 Fluorotelomer sulfonic acid (6:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.05 ND ND8:2 Fluorotelomer sulfonic acid (8:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND ND10:2 Fluorotelomer sulfonic acid (10:2 FTSA) µg/L 0.001 <0.001 <0.001 <0.01 ND NDN-Ethyl PFO sulfonamide (EtFOSA) µg/L 0.001 <0.001 <0.001 - ND -N-Ethyl PFO sulfonamidoethanol (EtFOSE) µg/L 0.001 <0.001 <0.001 <0.05 ND NDN-Methyl PFO sulfonamide (MeFOSA) µg/L 0.001 <0.001 <0.001 <0.05 ND NDPerfluorooctane sulfonamide (FOSA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDN-ethyl-PFO sulfonamidoacetic acid (EtFOSAA) µg/L 0.0005 <0.0005 <0.0005 <0.05 ND NDLegendND = Not Detected (RPDs not calculated if both primary and duplicate results are below LOR) - = Not analysed/calculated
Acceptable RPDs: RPD <= 30%RPD > 30%, Analyis result < 10 times LORRPD <= 50%, Analysis result > 10 times LOR and < 20 times LOR
Project: PSI Cat 2 Blamey Barracks Kapooka (0315)
RPDs
PSI - BLAMEY BARRACKS KAPOOKA (0315)
APPENDIX H Laboratory Certificates
14 June 2017 Report No. 1669283_001_R_Rev0 52
True
Environmental
QA/QC Compliance Assessment to assist with Quality ReviewWork Order : ES1706394 Page : 1 of 18
:Amendment 2
:: LaboratoryClient Environmental Division SydneyGOLDER ASSOCIATES
:Contact MS OLGA BUKHTEEVA Telephone : +61-2-8784 8555
:Project 1652034 Date Samples Received : 17-Mar-2017
Site : Kapooka Issue Date : 10-Apr-2017
OLGA BUKHTEEVA:Sampler No. of samples received : 110
:Order number PO01472 No. of samples analysed : 103
This report is automatically generated by the ALS LIMS through interpretation of the ALS Quality Control Report and several Quality Assurance parameters measured by ALS. This automated
reporting highlights any non-conformances, facilitates faster and more accurate data validation and is designed to assist internal expert and external Auditor review. Many components of this
report contribute to the overall DQO assessment and reporting for guideline compliance.
Brief method summaries and references are also provided to assist in traceability.
Summary of Outliers
Outliers : Quality Control Samples
This report highlights outliers flagged in the Quality Control (QC) Report.
l NO Method Blank value outliers occur.
l NO Duplicate outliers occur.
l NO Laboratory Control outliers occur.
l Matrix Spike outliers exist - please see following pages for full details.
l For all regular sample matrices, NO surrogate recovery outliers occur.
Outliers : Analysis Holding Time Compliance
l NO Analysis Holding Time Outliers exist.
Outliers : Frequency of Quality Control Samples
l Quality Control Sample Frequency Outliers exist - please see following pages for full details.
R I G H T S O L U T I O N S | R I G H T P A R T N E R
2 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Outliers : Quality Control Samples
Duplicates, Method Blanks, Laboratory Control Samples and Matrix Spikes
Matrix: SOIL
Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number
Matrix Spike (MS) Recoveries
ES1706394--001 355-46-4Perfluorohexane
sulfonic acid
(PFHxS)
0315_BH001_0.0_170315 MS recovery not determined,
background level greater than or
equal to 4x spike level.
----Not
Determined
EP231A: Perfluoroalkyl Sulfonic Acids
ES1706394--001 1763-23-1Perfluorooctane
sulfonic acid (PFOS)
0315_BH001_0.0_170315 MS recovery not determined,
background level greater than or
equal to 4x spike level.
----Not
Determined
EP231A: Perfluoroalkyl Sulfonic Acids
ES1706394--021 1763-23-1Perfluorooctane
sulfonic acid (PFOS)
0315_BH005_0.0_170314 MS recovery not determined,
background level greater than or
equal to 4x spike level.
----Not
Determined
EP231A: Perfluoroalkyl Sulfonic Acids
ES1706394--041 1763-23-1Perfluorooctane
sulfonic acid (PFOS)
0315_BH009_0.0_170315 MS recovery not determined,
background level greater than or
equal to 4x spike level.
----Not
Determined
EP231A: Perfluoroalkyl Sulfonic Acids
ES1706394--061 1763-23-1Perfluorooctane
sulfonic acid (PFOS)
0315_BH013_0.0_170314 MS recovery not determined,
background level greater than or
equal to 4x spike level.
----Not
Determined
EP231A: Perfluoroalkyl Sulfonic Acids
ES1706394--001 335-77-3Perfluorodecane
sulfonic acid (PFDS)
0315_BH001_0.0_170315 MS recovery not determined,
background level greater than or
equal to 4x spike level.
----Not
Determined
EP231A: Perfluoroalkyl Sulfonic Acids
ES1706394--001 2706-90-3Perfluoropentanoic
acid (PFPeA)
0315_BH001_0.0_170315 Recovery less than lower data quality
objective
50-130%36.2 %EP231B: Perfluoroalkyl Carboxylic Acids
ES1706394--001 307-24-4Perfluorohexanoic acid
(PFHxA)
0315_BH001_0.0_170315 MS recovery not determined,
background level greater than or
equal to 4x spike level.
----Not
Determined
EP231B: Perfluoroalkyl Carboxylic Acids
ES1706394--001 376-06-7Perfluorotetradecanoic
acid (PFTeDA)
0315_BH001_0.0_170315 Recovery less than lower data quality
objective
30-130%18.2 %EP231B: Perfluoroalkyl Carboxylic Acids
ES1706394--001 754-91-6Perfluorooctane
sulfonamide (FOSA)
0315_BH001_0.0_170315 MS recovery not determined,
background level greater than or
equal to 4x spike level.
----Not
Determined
EP231C: Perfluoroalkyl Sulfonamides
ES1706394--001 4151-50-2N-Ethyl perfluorooctane
sulfonamide
(EtFOSA)
0315_BH001_0.0_170315 Recovery less than lower data quality
objective
30-130%22.0 %EP231C: Perfluoroalkyl Sulfonamides
ES1706394--001 1691-99-2N-Ethyl perfluorooctane
sulfonamidoethanol
(EtFOSE)
0315_BH001_0.0_170315 Recovery less than lower data quality
objective
30-130%15.3 %EP231C: Perfluoroalkyl Sulfonamides
ES1706394--061 27619-97-26:2 Fluorotelomer
sulfonic acid (6:2
FTS)
0315_BH013_0.0_170314 MS recovery not determined,
background level greater than or
equal to 4x spike level.
----Not
Determined
EP231D: (n:2) Fluorotelomer Sulfonic Acids
ES1706394--001 39108-34-48:2 Fluorotelomer
sulfonic acid (8:2
FTS)
0315_BH001_0.0_170315 MS recovery not determined,
background level greater than or
equal to 4x spike level.
----Not
Determined
EP231D: (n:2) Fluorotelomer Sulfonic Acids
3 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL
Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number
Matrix Spike (MS) Recoveries - Continued
ES1706394--001 120226-60-010:2 Fluorotelomer
sulfonic acid (10:2
FTS)
0315_BH001_0.0_170315 Recovery less than lower data quality
objective
50-130%9.36 %EP231D: (n:2) Fluorotelomer Sulfonic Acids
Outliers : Frequency of Quality Control Samples
Matrix: SOIL
Quality Control SpecificationQuality Control Sample Type
Method ExpectedQC Regular Actual
Rate (%)Quality Control Sample Type Count
Laboratory Duplicates (DUP)
NEPM 2013 B3 & ALS QC StandardMoisture Content 9.80 10.0010 102
Matrix: WATER
Quality Control SpecificationQuality Control Sample Type
Method ExpectedQC Regular Actual
Rate (%)Quality Control Sample Type Count
Matrix Spikes (MS)
NEPM 2013 B3 & ALS QC StandardPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS 0.00 5.000 9
Analysis Holding Time Compliance
Holding times for VOC in soils vary according to analytes of interest. Vinyl Chloride and Styrene holding time is 7 days; others 14 days. A recorded breach does not guarantee a breach for all VOC analytes and
should be verified in case the reported breach is a false positive or Vinyl Chloride and Styrene are not key analytes of interest/concern.
Holding time for leachate methods (e.g. TCLP) vary according to the analytes reported. Assessment compares the leach date with the shortest analyte holding time for the equivalent soil method. These are: organics
14 days, mercury 28 days & other metals 180 days. A recorded breach does not guarantee a breach for all non-volatile parameters.
If samples are identified below as having been analysed or extracted outside of recommended holding times, this should be taken into consideration when interpreting results.
This report summarizes extraction / preparation and analysis times and compares each with ALS recommended holding times (referencing USEPA SW 846, APHA, AS and NEPM) based on the sample container
provided. Dates reported represent first date of extraction or analysis and preclude subsequent dilutions and reruns. A listing of breaches (if any) is provided herein.
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EA055: Moisture Content
HDPE Soil Jar (EA055-103)
0315_BH003_0.0_170314, 0315_BH003_1.0_170314,
0315_BH003_2.0_170314, 0315_BH003_3.0_170314,
0315_BH003_4.0_170314, 0315_BH004_0.0_170314,
0315_BH004_1.0_170314, 0315_BH004_2.0_170314,
0315_BH004_3.0_170314, 0315_BH004_4.0_170314,
0315_BH005_0.0_170314, 0315_BH005_1.0_170314,
0315_BH005_2.0_170314, 0315_BH005_3.0_170314,
0315_BH005_4.0_170314, 0315_BH006_0.0_170314,
0315_BH006_1.0_170314, 0315_BH006_2.0_170314,
0315_BH006_3.0_170314
28-Mar-2017---- 20-Mar-2017----14-Mar-2017 ---- ü
HDPE Soil Jar (EA055-103)
4 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EA055: Moisture Content - Continued
0315_BH006_4.0_170314, 0315_BH011_0.0_170314,
0315_BH011_1.0_170314, 0315_BH011_2.0_170314,
0315_BH011_3.0_170314, 0315_BH011_4.0_170314,
0315_BH012_0.0_170314, 0315_BH012_1.0_170314,
0315_BH012_2.0_170314, 0315_BH012_3.0_170314,
0315_BH012_4.0_170314, 0315_BH013_0.0_170314,
0315_BH013_1.0_170314, 0315_BH013_2.0_170314,
0315_BH013_3.0_170314, 0315_BH013_4.0_170314,
0315_SD001_170314, 0315_SD002_170314,
0315_QC100_170314, 0315_QC101_170314
28-Mar-2017---- 21-Mar-2017----14-Mar-2017 ---- ü
HDPE Soil Jar (EA055-103)
0315_BH001_0.0_170315, 0315_BH001_1.0_170315,
0315_BH001_2.0_170315, 0315_BH001_3.0_170315,
0315_BH001_4.0_170315, 0315_BH002_0.0_170315,
0315_BH002_1.0_170315, 0315_BH002_2.0_170315,
0315_BH002_3.0_170315, 0315_BH002_4.0_170315
29-Mar-2017---- 20-Mar-2017----15-Mar-2017 ---- ü
HDPE Soil Jar (EA055-103)
0315_BH007_0.0_170315, 0315_BH007_1.0_170315,
0315_BH007_2.0_170315, 0315_BH007_3.0_170315,
0315_BH007_4.0_170315, 0315_BH008_0.0_170315,
0315_BH008_1.0_170315, 0315_BH008_2.0_170315,
0315_BH008_3.0_170315, 0315_BH008_4.0_170315,
0315_BH009_0.0_170315, 0315_BH009_1.0_170315,
0315_BH009_2.0_170315, 0315_BH009_3.0_170315,
0315_BH009_4.0_170315, 0315_BH010_0.0_170315,
0315_BH010_1.0_170315, 0315_BH010_2.0_170315,
0315_BH010_3.0_170315, 0315_BH010_4.0_170315,
0315_BH014_0.0_170315, 0315_BH014_1.0_170315,
0315_BH014_2.0_170315, 0315_BH014_3.0_170315,
0315_BH014_4.0_170315, 0315_BH015_0.0_170315,
0315_BH015_1.0_170315, 0315_BH015_2.0_170315,
0315_BH015_3.0_170315, 0315_BH015_4.0_170315,
0315_SD005_170315, 0315_SD007_170315,
0315_QC102_170315, 0315_QC103_170315,
0315_QC104_170315, 0315_QC105_170315,
0315_QC106_170315, 0315_QC107_170315,
0315_QC108_170315
29-Mar-2017---- 21-Mar-2017----15-Mar-2017 ---- ü
HDPE Soil Jar (EA055-103)
0315_SD003_170316, 0315_SD004_170316,
0315_SD006_170316
30-Mar-2017---- 21-Mar-2017----16-Mar-2017 ---- ü
5 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231A: Perfluoroalkyl Sulfonic Acids
HDPE Soil Jar (EP231X)
0315_BH003_0.0_170314, 0315_BH003_1.0_170314,
0315_BH003_2.0_170314, 0315_BH003_3.0_170314,
0315_BH003_4.0_170314, 0315_BH004_0.0_170314,
0315_BH004_1.0_170314, 0315_BH004_2.0_170314,
0315_BH004_3.0_170314, 0315_BH004_4.0_170314,
0315_BH005_0.0_170314, 0315_BH005_1.0_170314,
0315_BH005_2.0_170314, 0315_BH005_3.0_170314,
0315_BH005_4.0_170314, 0315_BH006_0.0_170314,
0315_BH006_1.0_170314, 0315_BH006_2.0_170314,
0315_BH006_3.0_170314, 0315_BH006_4.0_170314
30-Apr-201710-Sep-2017 21-Mar-201721-Mar-201714-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_BH011_0.0_170314, 0315_BH011_1.0_170314,
0315_BH011_2.0_170314, 0315_BH011_3.0_170314,
0315_BH011_4.0_170314, 0315_BH012_0.0_170314,
0315_BH012_1.0_170314, 0315_BH012_2.0_170314,
0315_BH012_3.0_170314, 0315_BH012_4.0_170314,
0315_BH013_0.0_170314, 0315_BH013_1.0_170314,
0315_BH013_2.0_170314, 0315_BH013_3.0_170314,
0315_BH013_4.0_170314, 0315_SD001_170314,
0315_SD002_170314, 0315_QC100_170314,
0315_QC101_170314
01-May-201710-Sep-2017 22-Mar-201722-Mar-201714-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_BH001_0.0_170315, 0315_BH001_1.0_170315,
0315_BH001_2.0_170315, 0315_BH001_3.0_170315,
0315_BH001_4.0_170315, 0315_BH002_0.0_170315,
0315_BH002_1.0_170315, 0315_BH002_2.0_170315,
0315_BH002_3.0_170315, 0315_BH002_4.0_170315,
0315_BH007_0.0_170315, 0315_BH007_1.0_170315,
0315_BH007_2.0_170315, 0315_BH007_3.0_170315,
0315_BH007_4.0_170315, 0315_BH008_0.0_170315,
0315_BH008_1.0_170315, 0315_BH008_2.0_170315,
0315_BH008_3.0_170315, 0315_BH008_4.0_170315
30-Apr-201711-Sep-2017 21-Mar-201721-Mar-201715-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
6 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231A: Perfluoroalkyl Sulfonic Acids - Continued
0315_BH009_0.0_170315, 0315_BH009_1.0_170315,
0315_BH009_2.0_170315, 0315_BH009_3.0_170315,
0315_BH009_4.0_170315, 0315_BH010_0.0_170315,
0315_BH010_1.0_170315, 0315_BH010_2.0_170315,
0315_BH010_3.0_170315, 0315_BH010_4.0_170315,
0315_BH014_0.0_170315, 0315_BH014_1.0_170315,
0315_BH014_2.0_170315, 0315_BH014_3.0_170315,
0315_BH014_4.0_170315, 0315_BH015_0.0_170315,
0315_BH015_1.0_170315, 0315_BH015_2.0_170315,
0315_BH015_3.0_170315, 0315_BH015_4.0_170315,
0315_SD005_170315, 0315_SD007_170315,
0315_QC102_170315, 0315_QC103_170315,
0315_QC104_170315, 0315_QC105_170315,
0315_QC106_170315, 0315_QC107_170315,
0315_QC108_170315
01-May-201711-Sep-2017 22-Mar-201722-Mar-201715-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_SD003_170316, 0315_SD004_170316,
0315_SD006_170316
01-May-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü ü
7 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231B: Perfluoroalkyl Carboxylic Acids
HDPE Soil Jar (EP231X)
0315_BH003_0.0_170314, 0315_BH003_1.0_170314,
0315_BH003_2.0_170314, 0315_BH003_3.0_170314,
0315_BH003_4.0_170314, 0315_BH004_0.0_170314,
0315_BH004_1.0_170314, 0315_BH004_2.0_170314,
0315_BH004_3.0_170314, 0315_BH004_4.0_170314,
0315_BH005_0.0_170314, 0315_BH005_1.0_170314,
0315_BH005_2.0_170314, 0315_BH005_3.0_170314,
0315_BH005_4.0_170314, 0315_BH006_0.0_170314,
0315_BH006_1.0_170314, 0315_BH006_2.0_170314,
0315_BH006_3.0_170314, 0315_BH006_4.0_170314
30-Apr-201710-Sep-2017 21-Mar-201721-Mar-201714-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_BH011_0.0_170314, 0315_BH011_1.0_170314,
0315_BH011_2.0_170314, 0315_BH011_3.0_170314,
0315_BH011_4.0_170314, 0315_BH012_0.0_170314,
0315_BH012_1.0_170314, 0315_BH012_2.0_170314,
0315_BH012_3.0_170314, 0315_BH012_4.0_170314,
0315_BH013_0.0_170314, 0315_BH013_1.0_170314,
0315_BH013_2.0_170314, 0315_BH013_3.0_170314,
0315_BH013_4.0_170314, 0315_SD001_170314,
0315_SD002_170314, 0315_QC100_170314,
0315_QC101_170314
01-May-201710-Sep-2017 22-Mar-201722-Mar-201714-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_BH001_0.0_170315, 0315_BH001_1.0_170315,
0315_BH001_2.0_170315, 0315_BH001_3.0_170315,
0315_BH001_4.0_170315, 0315_BH002_0.0_170315,
0315_BH002_1.0_170315, 0315_BH002_2.0_170315,
0315_BH002_3.0_170315, 0315_BH002_4.0_170315,
0315_BH007_0.0_170315, 0315_BH007_1.0_170315,
0315_BH007_2.0_170315, 0315_BH007_3.0_170315,
0315_BH007_4.0_170315, 0315_BH008_0.0_170315,
0315_BH008_1.0_170315, 0315_BH008_2.0_170315,
0315_BH008_3.0_170315, 0315_BH008_4.0_170315
30-Apr-201711-Sep-2017 21-Mar-201721-Mar-201715-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
8 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231B: Perfluoroalkyl Carboxylic Acids - Continued
0315_BH009_0.0_170315, 0315_BH009_1.0_170315,
0315_BH009_2.0_170315, 0315_BH009_3.0_170315,
0315_BH009_4.0_170315, 0315_BH010_0.0_170315,
0315_BH010_1.0_170315, 0315_BH010_2.0_170315,
0315_BH010_3.0_170315, 0315_BH010_4.0_170315,
0315_BH014_0.0_170315, 0315_BH014_1.0_170315,
0315_BH014_2.0_170315, 0315_BH014_3.0_170315,
0315_BH014_4.0_170315, 0315_BH015_0.0_170315,
0315_BH015_1.0_170315, 0315_BH015_2.0_170315,
0315_BH015_3.0_170315, 0315_BH015_4.0_170315,
0315_SD005_170315, 0315_SD007_170315,
0315_QC102_170315, 0315_QC103_170315,
0315_QC104_170315, 0315_QC105_170315,
0315_QC106_170315, 0315_QC107_170315,
0315_QC108_170315
01-May-201711-Sep-2017 22-Mar-201722-Mar-201715-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_SD003_170316, 0315_SD004_170316,
0315_SD006_170316
01-May-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü ü
9 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231C: Perfluoroalkyl Sulfonamides
HDPE Soil Jar (EP231X)
0315_BH003_0.0_170314, 0315_BH003_1.0_170314,
0315_BH003_2.0_170314, 0315_BH003_3.0_170314,
0315_BH003_4.0_170314, 0315_BH004_0.0_170314,
0315_BH004_1.0_170314, 0315_BH004_2.0_170314,
0315_BH004_3.0_170314, 0315_BH004_4.0_170314,
0315_BH005_0.0_170314, 0315_BH005_1.0_170314,
0315_BH005_2.0_170314, 0315_BH005_3.0_170314,
0315_BH005_4.0_170314, 0315_BH006_0.0_170314,
0315_BH006_1.0_170314, 0315_BH006_2.0_170314,
0315_BH006_3.0_170314, 0315_BH006_4.0_170314
30-Apr-201710-Sep-2017 21-Mar-201721-Mar-201714-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_BH011_0.0_170314, 0315_BH011_1.0_170314,
0315_BH011_2.0_170314, 0315_BH011_3.0_170314,
0315_BH011_4.0_170314, 0315_BH012_0.0_170314,
0315_BH012_1.0_170314, 0315_BH012_2.0_170314,
0315_BH012_3.0_170314, 0315_BH012_4.0_170314,
0315_BH013_0.0_170314, 0315_BH013_1.0_170314,
0315_BH013_2.0_170314, 0315_BH013_3.0_170314,
0315_BH013_4.0_170314, 0315_SD001_170314,
0315_SD002_170314, 0315_QC100_170314,
0315_QC101_170314
01-May-201710-Sep-2017 22-Mar-201722-Mar-201714-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_BH001_0.0_170315, 0315_BH001_1.0_170315,
0315_BH001_2.0_170315, 0315_BH001_3.0_170315,
0315_BH001_4.0_170315, 0315_BH002_0.0_170315,
0315_BH002_1.0_170315, 0315_BH002_2.0_170315,
0315_BH002_3.0_170315, 0315_BH002_4.0_170315,
0315_BH007_0.0_170315, 0315_BH007_1.0_170315,
0315_BH007_2.0_170315, 0315_BH007_3.0_170315,
0315_BH007_4.0_170315, 0315_BH008_0.0_170315,
0315_BH008_1.0_170315, 0315_BH008_2.0_170315,
0315_BH008_3.0_170315, 0315_BH008_4.0_170315
30-Apr-201711-Sep-2017 21-Mar-201721-Mar-201715-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
10 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231C: Perfluoroalkyl Sulfonamides - Continued
0315_BH009_0.0_170315, 0315_BH009_1.0_170315,
0315_BH009_2.0_170315, 0315_BH009_3.0_170315,
0315_BH009_4.0_170315, 0315_BH010_0.0_170315,
0315_BH010_1.0_170315, 0315_BH010_2.0_170315,
0315_BH010_3.0_170315, 0315_BH010_4.0_170315,
0315_BH014_0.0_170315, 0315_BH014_1.0_170315,
0315_BH014_2.0_170315, 0315_BH014_3.0_170315,
0315_BH014_4.0_170315, 0315_BH015_0.0_170315,
0315_BH015_1.0_170315, 0315_BH015_2.0_170315,
0315_BH015_3.0_170315, 0315_BH015_4.0_170315,
0315_SD005_170315, 0315_SD007_170315,
0315_QC102_170315, 0315_QC103_170315,
0315_QC104_170315, 0315_QC105_170315,
0315_QC106_170315, 0315_QC107_170315,
0315_QC108_170315
01-May-201711-Sep-2017 22-Mar-201722-Mar-201715-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_SD003_170316, 0315_SD004_170316,
0315_SD006_170316
01-May-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü ü
11 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231D: (n:2) Fluorotelomer Sulfonic Acids
HDPE Soil Jar (EP231X)
0315_BH003_0.0_170314, 0315_BH003_1.0_170314,
0315_BH003_2.0_170314, 0315_BH003_3.0_170314,
0315_BH003_4.0_170314, 0315_BH004_0.0_170314,
0315_BH004_1.0_170314, 0315_BH004_2.0_170314,
0315_BH004_3.0_170314, 0315_BH004_4.0_170314,
0315_BH005_0.0_170314, 0315_BH005_1.0_170314,
0315_BH005_2.0_170314, 0315_BH005_3.0_170314,
0315_BH005_4.0_170314, 0315_BH006_0.0_170314,
0315_BH006_1.0_170314, 0315_BH006_2.0_170314,
0315_BH006_3.0_170314, 0315_BH006_4.0_170314
30-Apr-201710-Sep-2017 21-Mar-201721-Mar-201714-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_BH011_0.0_170314, 0315_BH011_1.0_170314,
0315_BH011_2.0_170314, 0315_BH011_3.0_170314,
0315_BH011_4.0_170314, 0315_BH012_0.0_170314,
0315_BH012_1.0_170314, 0315_BH012_2.0_170314,
0315_BH012_3.0_170314, 0315_BH012_4.0_170314,
0315_BH013_0.0_170314, 0315_BH013_1.0_170314,
0315_BH013_2.0_170314, 0315_BH013_3.0_170314,
0315_BH013_4.0_170314, 0315_SD001_170314,
0315_SD002_170314, 0315_QC100_170314,
0315_QC101_170314
01-May-201710-Sep-2017 22-Mar-201722-Mar-201714-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_BH001_0.0_170315, 0315_BH001_1.0_170315,
0315_BH001_2.0_170315, 0315_BH001_3.0_170315,
0315_BH001_4.0_170315, 0315_BH002_0.0_170315,
0315_BH002_1.0_170315, 0315_BH002_2.0_170315,
0315_BH002_3.0_170315, 0315_BH002_4.0_170315,
0315_BH007_0.0_170315, 0315_BH007_1.0_170315,
0315_BH007_2.0_170315, 0315_BH007_3.0_170315,
0315_BH007_4.0_170315, 0315_BH008_0.0_170315,
0315_BH008_1.0_170315, 0315_BH008_2.0_170315,
0315_BH008_3.0_170315, 0315_BH008_4.0_170315
30-Apr-201711-Sep-2017 21-Mar-201721-Mar-201715-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
12 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231D: (n:2) Fluorotelomer Sulfonic Acids - Continued
0315_BH009_0.0_170315, 0315_BH009_1.0_170315,
0315_BH009_2.0_170315, 0315_BH009_3.0_170315,
0315_BH009_4.0_170315, 0315_BH010_0.0_170315,
0315_BH010_1.0_170315, 0315_BH010_2.0_170315,
0315_BH010_3.0_170315, 0315_BH010_4.0_170315,
0315_BH014_0.0_170315, 0315_BH014_1.0_170315,
0315_BH014_2.0_170315, 0315_BH014_3.0_170315,
0315_BH014_4.0_170315, 0315_BH015_0.0_170315,
0315_BH015_1.0_170315, 0315_BH015_2.0_170315,
0315_BH015_3.0_170315, 0315_BH015_4.0_170315,
0315_SD005_170315, 0315_SD007_170315,
0315_QC102_170315, 0315_QC103_170315,
0315_QC104_170315, 0315_QC105_170315,
0315_QC106_170315, 0315_QC107_170315,
0315_QC108_170315
01-May-201711-Sep-2017 22-Mar-201722-Mar-201715-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_SD003_170316, 0315_SD004_170316,
0315_SD006_170316
01-May-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü ü
13 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231P: PFAS Sums
HDPE Soil Jar (EP231X)
0315_BH003_0.0_170314, 0315_BH003_1.0_170314,
0315_BH003_2.0_170314, 0315_BH003_3.0_170314,
0315_BH003_4.0_170314, 0315_BH004_0.0_170314,
0315_BH004_1.0_170314, 0315_BH004_2.0_170314,
0315_BH004_3.0_170314, 0315_BH004_4.0_170314,
0315_BH005_0.0_170314, 0315_BH005_1.0_170314,
0315_BH005_2.0_170314, 0315_BH005_3.0_170314,
0315_BH005_4.0_170314, 0315_BH006_0.0_170314,
0315_BH006_1.0_170314, 0315_BH006_2.0_170314,
0315_BH006_3.0_170314, 0315_BH006_4.0_170314
30-Apr-201710-Sep-2017 21-Mar-201721-Mar-201714-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_BH011_0.0_170314, 0315_BH011_1.0_170314,
0315_BH011_2.0_170314, 0315_BH011_3.0_170314,
0315_BH011_4.0_170314, 0315_BH012_0.0_170314,
0315_BH012_1.0_170314, 0315_BH012_2.0_170314,
0315_BH012_3.0_170314, 0315_BH012_4.0_170314,
0315_BH013_0.0_170314, 0315_BH013_1.0_170314,
0315_BH013_2.0_170314, 0315_BH013_3.0_170314,
0315_BH013_4.0_170314, 0315_SD001_170314,
0315_SD002_170314, 0315_QC100_170314,
0315_QC101_170314
01-May-201710-Sep-2017 22-Mar-201722-Mar-201714-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_BH001_0.0_170315, 0315_BH001_1.0_170315,
0315_BH001_2.0_170315, 0315_BH001_3.0_170315,
0315_BH001_4.0_170315, 0315_BH002_0.0_170315,
0315_BH002_1.0_170315, 0315_BH002_2.0_170315,
0315_BH002_3.0_170315, 0315_BH002_4.0_170315,
0315_BH007_0.0_170315, 0315_BH007_1.0_170315,
0315_BH007_2.0_170315, 0315_BH007_3.0_170315,
0315_BH007_4.0_170315, 0315_BH008_0.0_170315,
0315_BH008_1.0_170315, 0315_BH008_2.0_170315,
0315_BH008_3.0_170315, 0315_BH008_4.0_170315
30-Apr-201711-Sep-2017 21-Mar-201721-Mar-201715-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
14 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231P: PFAS Sums - Continued
0315_BH009_0.0_170315, 0315_BH009_1.0_170315,
0315_BH009_2.0_170315, 0315_BH009_3.0_170315,
0315_BH009_4.0_170315, 0315_BH010_0.0_170315,
0315_BH010_1.0_170315, 0315_BH010_2.0_170315,
0315_BH010_3.0_170315, 0315_BH010_4.0_170315,
0315_BH014_0.0_170315, 0315_BH014_1.0_170315,
0315_BH014_2.0_170315, 0315_BH014_3.0_170315,
0315_BH014_4.0_170315, 0315_BH015_0.0_170315,
0315_BH015_1.0_170315, 0315_BH015_2.0_170315,
0315_BH015_3.0_170315, 0315_BH015_4.0_170315,
0315_SD005_170315, 0315_SD007_170315,
0315_QC102_170315, 0315_QC103_170315,
0315_QC104_170315, 0315_QC105_170315,
0315_QC106_170315, 0315_QC107_170315,
0315_QC108_170315
01-May-201711-Sep-2017 22-Mar-201722-Mar-201715-Mar-2017 ü ü
HDPE Soil Jar (EP231X)
0315_SD003_170316, 0315_SD004_170316,
0315_SD006_170316
01-May-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü ü
Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231A: Perfluoroalkyl Sulfonic Acids
HDPE (no PTFE) (EP231X)
0315_QC300_170314 10-Sep-2017---- 20-Mar-2017----14-Mar-2017 ---- üHDPE (no PTFE) (EP231X)
0315_QC301_170315 11-Sep-2017---- 20-Mar-2017----15-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)
0315_SW005_170315, 0315_SW007_170315,
0315_QC109_170315
11-Sep-201711-Sep-2017 20-Mar-201720-Mar-201715-Mar-2017 ü ü
HDPE (no PTFE) (EP231X)
0315_QC302_170316 12-Sep-2017---- 20-Mar-2017----16-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)
0315_MW004_170316, 0315_MW005_170316,
0315_MW006_170316, 0315_QC110_170316
12-Sep-201712-Sep-2017 20-Mar-201720-Mar-201716-Mar-2017 ü ü
HDPE (no PTFE) (EP231X-ST)
0315_MW007_170316, 0315_MW008_170316 12-Sep-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü ü
15 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231B: Perfluoroalkyl Carboxylic Acids
HDPE (no PTFE) (EP231X)
0315_QC300_170314 10-Sep-2017---- 20-Mar-2017----14-Mar-2017 ---- üHDPE (no PTFE) (EP231X)
0315_QC301_170315 11-Sep-2017---- 20-Mar-2017----15-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)
0315_SW005_170315, 0315_SW007_170315,
0315_QC109_170315
11-Sep-201711-Sep-2017 20-Mar-201720-Mar-201715-Mar-2017 ü ü
HDPE (no PTFE) (EP231X)
0315_QC302_170316 12-Sep-2017---- 20-Mar-2017----16-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)
0315_MW004_170316, 0315_MW005_170316,
0315_MW006_170316, 0315_QC110_170316
12-Sep-201712-Sep-2017 20-Mar-201720-Mar-201716-Mar-2017 ü ü
HDPE (no PTFE) (EP231X-ST)
0315_MW007_170316, 0315_MW008_170316 12-Sep-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü üEP231C: Perfluoroalkyl Sulfonamides
HDPE (no PTFE) (EP231X)
0315_QC300_170314 10-Sep-2017---- 20-Mar-2017----14-Mar-2017 ---- üHDPE (no PTFE) (EP231X)
0315_QC301_170315 11-Sep-2017---- 20-Mar-2017----15-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)
0315_SW005_170315, 0315_SW007_170315,
0315_QC109_170315
11-Sep-201711-Sep-2017 20-Mar-201720-Mar-201715-Mar-2017 ü ü
HDPE (no PTFE) (EP231X)
0315_QC302_170316 12-Sep-2017---- 20-Mar-2017----16-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)
0315_MW004_170316, 0315_MW005_170316,
0315_MW006_170316, 0315_QC110_170316
12-Sep-201712-Sep-2017 20-Mar-201720-Mar-201716-Mar-2017 ü ü
HDPE (no PTFE) (EP231X-ST)
0315_MW007_170316, 0315_MW008_170316 12-Sep-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü üEP231D: (n:2) Fluorotelomer Sulfonic Acids
HDPE (no PTFE) (EP231X)
0315_QC300_170314 10-Sep-2017---- 20-Mar-2017----14-Mar-2017 ---- üHDPE (no PTFE) (EP231X)
0315_QC301_170315 11-Sep-2017---- 20-Mar-2017----15-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)
0315_SW005_170315, 0315_SW007_170315,
0315_QC109_170315
11-Sep-201711-Sep-2017 20-Mar-201720-Mar-201715-Mar-2017 ü ü
HDPE (no PTFE) (EP231X)
0315_QC302_170316 12-Sep-2017---- 20-Mar-2017----16-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)
0315_MW004_170316, 0315_MW005_170316,
0315_MW006_170316, 0315_QC110_170316
12-Sep-201712-Sep-2017 20-Mar-201720-Mar-201716-Mar-2017 ü ü
HDPE (no PTFE) (EP231X-ST)
0315_MW007_170316, 0315_MW008_170316 12-Sep-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü ü
16 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.
AnalysisExtraction / PreparationSample DateMethod
EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)
EP231P: PFAS Sums
HDPE (no PTFE) (EP231X)
0315_QC300_170314 10-Sep-2017---- 20-Mar-2017----14-Mar-2017 ---- üHDPE (no PTFE) (EP231X)
0315_QC301_170315 11-Sep-2017---- 20-Mar-2017----15-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)
0315_SW005_170315, 0315_SW007_170315,
0315_QC109_170315
11-Sep-201711-Sep-2017 20-Mar-201720-Mar-201715-Mar-2017 ü ü
HDPE (no PTFE) (EP231X)
0315_QC302_170316 12-Sep-2017---- 20-Mar-2017----16-Mar-2017 ---- üHDPE (no PTFE) (EP231X-ST)
0315_MW004_170316, 0315_MW005_170316,
0315_MW006_170316, 0315_QC110_170316
12-Sep-201712-Sep-2017 20-Mar-201720-Mar-201716-Mar-2017 ü ü
HDPE (no PTFE) (EP231X-ST)
0315_MW007_170316, 0315_MW008_170316 12-Sep-201712-Sep-2017 22-Mar-201722-Mar-201716-Mar-2017 ü ü
17 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Quality Control Parameter Frequency ComplianceThe following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which the submitted sample(s) was(were) processed. Actual rate should be greater than or equal to
the expected rate. A listing of breaches is provided in the Summary of Outliers.
Matrix: SOIL Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.
Quality Control SpecificationQuality Control Sample Type
ExpectedQC Regular Actual
Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method
Laboratory Duplicates (DUP)
NEPM 2013 B3 & ALS QC Standard 9.80 10.0010 102 ûMoisture Content EA055-103
NEPM 2013 B3 & ALS QC Standard 10.99 10.0010 91 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X
Laboratory Control Samples (LCS)
NEPM 2013 B3 & ALS QC Standard 5.49 5.005 91 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X
Method Blanks (MB)
NEPM 2013 B3 & ALS QC Standard 5.49 5.005 91 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X
Matrix Spikes (MS)
NEPM 2013 B3 & ALS QC Standard 5.49 5.005 91 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X
Matrix: WATER Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.
Quality Control SpecificationQuality Control Sample Type
ExpectedQC Regular Actual
Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method
Laboratory Duplicates (DUP)
NEPM 2013 B3 & ALS QC Standard 12.50 10.002 16 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X
NEPM 2013 B3 & ALS QC Standard 11.11 10.001 9 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X-ST
Laboratory Control Samples (LCS)
NEPM 2013 B3 & ALS QC Standard 6.25 5.001 16 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X
NEPM 2013 B3 & ALS QC Standard 22.22 5.002 9 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X-ST
Method Blanks (MB)
NEPM 2013 B3 & ALS QC Standard 6.25 5.001 16 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X
NEPM 2013 B3 & ALS QC Standard 22.22 5.002 9 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X-ST
Matrix Spikes (MS)
NEPM 2013 B3 & ALS QC Standard 6.25 5.001 16 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X
NEPM 2013 B3 & ALS QC Standard 0.00 5.000 9 ûPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X-ST
18 of 18:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Brief Method SummariesThe analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house
developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the
Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.
Analytical Methods Method DescriptionsMatrixMethod
In house: A gravimetric procedure based on weight loss over a 12 hour drying period at 103-105 degrees C.
This method is compliant with NEPM (2013) Schedule B(3) Section 7.1 and Table 1 (14 day holding time).
Moisture Content EA055-103 SOIL
In-House. A portion of soil is extracted with MTBE. The extract is taken to dryness, made up in mobile phase.
Analysis is by LC/MSMS, ESI Negative Mode using MRM. PFOS is quantified using a certified, traceable standard
consisting of linear and branched PFOS isomers.
Per- and Polyfluoroalkyl Substances
(PFAS) by LCMSMS
EP231X SOIL
In house: Direct injection analysis of fresh waters after dilution (1:1) with methanol. Analysis by
LC-Electrospray-MS-MS, Negative Mode using MRM. PFOS is quantified using a certified, traceable standard
consisting of linear and branched PFOS isomers.
Per- and Polyfluoroalkyl Substances
(PFAS) by LCMSMS
EP231X WATER
In-house: Analysis of fresh and saline waters by solid phase extraction and LC-Electrospray-MS-MS, Negative
Mode using MRM. This method is targetted to pristine environmental and drinking waters reportin at sub-parts
per trillion. PFOS is quantified using a certified, traceable standard consisting of linear and branched PFOS
isomers.
Per- and Polyfluoroalkyl Substances
(PFAS) by LCMSMS
EP231X-ST WATER
Preparation Methods Method DescriptionsMatrixMethod
In houseSample Extraction for PFAS EP231-PR SOIL
In house: Referenced to USEPA SW 846 - 5030A. 5g of solid is shaken with surrogate and 10mL methanol prior
to analysis by Purge and Trap - GC/MS.
Methanolic Extraction of Soils for Purge
and Trap
* ORG16 SOIL
In houseSPE preparation for LL and saline PFCs EP231-SPE WATER
A 5 mL aliquot or 5 mL of a diluted sample is added to a 40 mL VOC vial for sparging.Volatiles Water Preparation ORG16-W WATER
False
2 2.00True
Environmental
QUALITY CONTROL REPORTWork Order : ES1706394 Page : 1 of 31
:Amendment 2
:: LaboratoryClient Environmental Division SydneyGOLDER ASSOCIATES
:Contact MS OLGA BUKHTEEVA :Contact Customer Services ES
:Address LEVEL 1, 124 PACIFIC HIGHWAY
ST LEONARDS NSW, AUSTRALIA 2065
Address : 277-289 Woodpark Road Smithfield NSW Australia 2164
::Telephone +61 02 9478 3900 +61-2-8784 8555:Telephone
:Project 1652034 Date Samples Received : 17-Mar-2017
:Order number PO01472 Date Analysis Commenced : 20-Mar-2017
:C-O-C number ---- Issue Date : 10-Apr-2017
Sampler : OLGA BUKHTEEVA
Site : Kapooka
Quote number : BN/404/16
No. of samples received 110:
No. of samples analysed 103:
This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.
This Quality Control Report contains the following information:
l Laboratory Duplicate (DUP) Report; Relative Percentage Difference (RPD) and Acceptance Limits
l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits
l Matrix Spike (MS) Report; Recovery and Acceptance Limits
SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.
Signatories Accreditation CategoryPosition
Alex Rossi Organic Chemist Sydney Organics, Smithfield, NSW
Edwandy Fadjar Organic Coordinator Sydney Inorganics, Smithfield, NSW
R I G H T S O L U T I O N S | R I G H T P A R T N E R
2 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
General Comments
The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house
developed procedures are employed in the absence of documented standards or by client request.
Where moisture determination has been performed, results are reported on a dry weight basis.
Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.
Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot
CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.
LOR = Limit of reporting
RPD = Relative Percentage Difference
# = Indicates failed QC
Key :
Laboratory Duplicate (DUP) Report
The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges
for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:
No Limit; Result between 10 and 20 times LOR: 0% - 50%; Result > 20 times LOR: 0% - 20%.
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EA055: Moisture Content (QC Lot: 799429)
EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 7.9 7.7 3.38 No LimitAnonymous ES1706332-058
EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 20.1 21.2 4.95 0% - 20%0315_BH002_3.0_170315 ES1706394-009
EA055: Moisture Content (QC Lot: 799430)
EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 13.1 13.0 0.00 0% - 50%0315_BH004_2.0_170314 ES1706394-018
EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 11.3 12.5 10.4 0% - 50%0315_BH006_3.0_170314 ES1706394-029
EA055: Moisture Content (QC Lot: 801051)
EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 8.4 8.1 3.14 No Limit0315_BH007_1.0_170315 ES1706394-032
EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 11.3 13.5 17.6 0% - 50%0315_BH009_2.0_170315 ES1706394-043
EA055: Moisture Content (QC Lot: 801052)
EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 9.5 9.4 0.00 No Limit0315_BH011_1.0_170314 ES1706394-052
EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 12.7 10.7 17.3 0% - 50%0315_BH013_2.0_170314 ES1706394-063
EA055: Moisture Content (QC Lot: 801053)
EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 7.5 7.3 1.97 No Limit0315_BH015_1.0_170315 ES1706394-072
EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 2.8 2.9 0.00 No Limit0315_QC100_170314 ES1706394-091
EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798130)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg 0.0009 0.0009 0.00 No Limit0315_BH001_0.0_170315 ES1706394-001
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg 0.0015 0.0015 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0518 0.0534 3.17 0% - 20%
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg 0.0013 0.0014 7.26 No Limit
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 1.15 1.11 3.79 0% - 20%
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg 0.0172 0.0156 9.49 0% - 20%
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg 0.0020 0.0016 17.9 No Limit0315_BH003_0.0_170314 ES1706394-011
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg 0.0024 0.0021 11.4 0% - 50%
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0517 0.0499 3.60 0% - 20%
3 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798130) - continued
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg 0.0054 0.0052 3.59 0% - 20%0315_BH003_0.0_170314 ES1706394-011
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.462 0.474 2.70 0% - 20%
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg 0.0273 0.0279 2.10 0% - 20%
EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798131)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH005_0.0_170314 ES1706394-021
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0003 0.0004 0.00 No Limit
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.0124 0.0113 9.66 0% - 20%
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH007_0.0_170315 ES1706394-031
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0010 0.0011 0.00 No Limit
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.0159 0.0170 6.62 0% - 20%
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798132)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH009_0.0_170315 ES1706394-041
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 0.0002 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0038 0.0038 0.00 0% - 50%
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg 0.0020 0.0018 10.2 No Limit
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.324 0.340 4.78 0% - 20%
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH011_0.0_170314 ES1706394-051
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.0008 0.0008 0.00 No Limit
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798133)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH013_0.0_170314 ES1706394-061
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0013 0.0014 11.8 No Limit
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.0064 0.0063 2.52 0% - 20%
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH015_0.0_170315 ES1706394-071
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
4 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798133) - continued
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.0012 0.0014 13.5 No Limit0315_BH015_0.0_170315 ES1706394-071
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798138)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_SD006_170316 ES1706394-089
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.0015 0.0016 0.00 No Limit
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_QC108_170315 ES1706394-099
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0006 0.0005 24.0 No Limit
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.0025 0.0034 30.3 0% - 50%
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798130)
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH001_0.0_170315 ES1706394-001
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.0085 0.0091 6.33 0% - 20%
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg 0.0013 0.0015 16.0 No Limit
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0050 0.0052 4.40 0% - 20%
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg 0.0004 0.0005 0.00 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg 0.0009 0.0009 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg 0.014 0.013 0.00 0% - 50%
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg 0.0049 0.0046 6.10 0% - 20%0315_BH003_0.0_170314 ES1706394-011
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.0075 0.0068 8.82 0% - 20%
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg 0.0024 0.0021 14.3 0% - 50%
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0078 0.0075 4.38 0% - 20%
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg 0.0034 0.0032 6.40 0% - 50%
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg 0.0044 0.0041 5.55 0% - 20%
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg 0.0024 0.0027 9.41 0% - 50%
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg 0.0043 0.0046 5.03 0% - 20%
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg 0.0016 0.0015 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798131)
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH005_0.0_170314 ES1706394-021
5 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798131) - continued
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH005_0.0_170314 ES1706394-021
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 0.0002 0.00 No Limit
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 0.0002 0.00 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg 0.0006 <0.0002 105 No Limit0315_BH007_0.0_170315 ES1706394-031
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0002 0.0002 0.00 No Limit
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798132)
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH009_0.0_170315 ES1706394-041
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.0009 0.0010 15.0 No Limit
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0006 0.0007 0.00 No Limit
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH011_0.0_170314 ES1706394-051
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0003 0.0004 0.00 No Limit
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
6 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798132) - continued
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH011_0.0_170314 ES1706394-051
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798133)
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg 0.0030 0.0034 10.8 0% - 50%0315_BH013_0.0_170314 ES1706394-061
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.0018 0.0020 8.28 0% - 50%
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg 0.0020 0.0022 7.72 0% - 50%
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0014 0.0011 24.4 No Limit
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg 0.0009 0.0006 40.0 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH015_0.0_170315 ES1706394-071
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798138)
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_SD006_170316 ES1706394-089
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg 0.0072 0.0077 6.10 0% - 20%0315_QC108_170315 ES1706394-099
7 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798138) - continued
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_QC108_170315 ES1706394-099
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg 0.0002 <0.0002 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798130)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg 0.0112 0.0114 2.46 0% - 20%0315_BH001_0.0_170315 ES1706394-001
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg 0.0477 0.0470 1.51 0% - 20%0315_BH003_0.0_170314 ES1706394-011
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.0005 mg/kg 0.0007 0.0007 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798131)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH005_0.0_170314 ES1706394-021
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
8 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798131) - continued
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH005_0.0_170314 ES1706394-021
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH007_0.0_170315 ES1706394-031
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798132)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg 0.0010 0.0012 10.8 No Limit0315_BH009_0.0_170315 ES1706394-041
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 0.0005 0.00 No Limit
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH011_0.0_170314 ES1706394-051
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
9 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798132) - continued
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH011_0.0_170314 ES1706394-051
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.0005 mg/kg 0.0009 <0.0005 61.5 No Limit
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798133)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH013_0.0_170314 ES1706394-061
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_BH015_0.0_170315 ES1706394-071
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798138)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_SD006_170316 ES1706394-089
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
10 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798138) - continued
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_SD006_170316 ES1706394-089
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0315_QC108_170315 ES1706394-099
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 0.0002 0.00 No Limit
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798130)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_BH001_0.0_170315 ES1706394-001
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.0005 mg/kg 0.0032 0.0032 0.00 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.0005 mg/kg 0.0064 0.0053 19.0 0% - 50%
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_BH003_0.0_170314 ES1706394-011
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.0005 mg/kg 0.0036 0.0031 16.4 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.0005 mg/kg 0.0057 0.0050 13.1 0% - 50%
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.0005 mg/kg 0.0006 <0.0005 0.00 No Limit
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798131)
11 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798131) - continued
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_BH005_0.0_170314 ES1706394-021
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_BH007_0.0_170315 ES1706394-031
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798132)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_BH009_0.0_170315 ES1706394-041
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_BH011_0.0_170314 ES1706394-051
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798133)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_BH013_0.0_170314 ES1706394-061
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.0005 mg/kg 0.0060 0.0051 15.0 0% - 50%
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.0005 mg/kg 0.0018 0.0022 20.2 No Limit
12 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798133) - continued
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_BH013_0.0_170314 ES1706394-061
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_BH015_0.0_170315 ES1706394-071
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798138)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_SD006_170316 ES1706394-089
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0315_QC108_170315 ES1706394-099
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit
Sub-Matrix: WATER Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798141)
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 0.20 0.20 0.00 0% - 20%Anonymous EB1705137-001
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 0.04 0.04 0.00 No Limit
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 0.03 0.04 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 0.23 0.21 7.64 0% - 50%
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 0.03 0.04 0.00 No LimitAnonymous ES1706387-002
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 0.06 0.06 0.00 No Limit
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 <0.02 0.00 No Limit
13 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: WATER Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 798141) - continued
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No LimitAnonymous ES1706387-002
EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 803834)
EP231X-ST: Perfluorooctane sulfonic acid
(PFOS)
1763-23-1 0.0003 µg/L <0.0003 <0.0003 0.00 No Limit0315_MW007_170316 ES1706394-079
EP231X-ST: Perfluorobutane sulfonic acid
(PFBS)
375-73-5 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluoropentane sulfonic acid
(PFPeS)
2706-91-4 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluorohexane sulfonic acid
(PFHxS)
355-46-4 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluoroheptane sulfonic acid
(PFHpS)
375-92-8 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluorodecane sulfonic acid
(PFDS)
335-77-3 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 798141)
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L 0.03 0.03 0.00 No LimitAnonymous EB1705137-001
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L 0.05 0.04 0.00 No Limit
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 0.07 0.06 0.00 No Limit
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L 0.02 0.02 0.00 No Limit
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 <0.01 0.00 No LimitAnonymous ES1706387-002
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L 0.08 0.08 0.00 No Limit
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 0.12 0.12 0.00 No Limit
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 803834)
EP231X-ST: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit0315_MW007_170316 ES1706394-079
EP231X-ST: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
14 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: WATER Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 803834) - continued
EP231X-ST: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit0315_MW007_170316 ES1706394-079
EP231X-ST: Perfluorooctanoic acid (PFOA) 335-67-1 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluorononanoic acid (PFNA) 375-95-1 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluorodecanoic acid (PFDA) 335-76-2 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluorotetradecanoic acid
(PFTeDA)
376-06-7 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: Perfluorobutanoic acid (PFBA) 375-22-4 0.002 µg/L <0.002 <0.002 0.00 No Limit
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 798141)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No LimitAnonymous EB1705137-001
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No LimitAnonymous ES1706387-002
EP231X: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit
EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 803834)
EP231X-ST: Perfluorooctane sulfonamide
(FOSA)
754-91-6 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit0315_MW007_170316 ES1706394-079
15 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: WATER Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 803834) - continued
EP231X-ST: N-Methyl perfluorooctane
sulfonamidoacetic acid (MeFOSAA)
2355-31-9 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit0315_MW007_170316 ES1706394-079
EP231X-ST: N-Ethyl perfluorooctane
sulfonamidoacetic acid (EtFOSAA)
2991-50-6 0.0005 µg/L <0.0005 <0.0005 0.00 No Limit
EP231X-ST: N-Methyl perfluorooctane
sulfonamide (MeFOSA)
31506-32-8 0.001 µg/L <0.001 <0.001 0.00 No Limit
EP231X-ST: N-Ethyl perfluorooctane sulfonamide
(EtFOSA)
4151-50-2 0.001 µg/L <0.001 <0.001 0.00 No Limit
EP231X-ST: N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
2448-09-7 0.001 µg/L <0.001 <0.001 0.00 No Limit
EP231X-ST: N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
1691-99-2 0.001 µg/L <0.001 <0.001 0.00 No Limit
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 798141)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No LimitAnonymous EB1705137-001
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No LimitAnonymous ES1706387-002
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2
FTS)
120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 803834)
EP231X-ST: 4:2 Fluorotelomer sulfonic acid (4:2
FTS)
757124-72-4 0.001 µg/L <0.001 <0.001 0.00 No Limit0315_MW007_170316 ES1706394-079
EP231X-ST: 6:2 Fluorotelomer sulfonic acid (6:2
FTS)
27619-97-2 0.001 µg/L <0.001 <0.001 0.00 No Limit
EP231X-ST: 8:2 Fluorotelomer sulfonic acid (8:2
FTS)
39108-34-4 0.001 µg/L <0.001 <0.001 0.00 No Limit
EP231X-ST: 10:2 Fluorotelomer sulfonic acid
(10:2 FTS)
120226-60-0 0.001 µg/L <0.001 <0.001 0.00 No Limit
EP231P: PFAS Sums (QC Lot: 798141)
EP231X: Sum of PFAS ---- 0.01 µg/L 0.67 0.64 4.58 0% - 20%Anonymous EB1705137-001
EP231X: Sum of PFAS ---- 0.01 µg/L 0.29 0.30 3.39 0% - 20%Anonymous ES1706387-002
16 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: WATER Laboratory Duplicate (DUP) Report
Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)
EP231P: PFAS Sums (QC Lot: 803834)
EP231X-ST: Sum of PFAS ---- 0.0003 µg/L <0.0003 <0.0003 0.00 No Limit0315_MW007_170316 ES1706394-079
17 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Method Blank (MB) and Laboratory Control Spike (LCS) Report
The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC
parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Spike (LCS) refers to a certified reference material, or a known interference free matrix spiked with target
analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS.
Sub-Matrix: SOIL Method Blank (MB)
Report
Laboratory Control Spike (LCS) Report
Spike Spike Recovery (%) Recovery Limits (%)
Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798130)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 58.80.00125 mg/kg 12157
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 58.80.00125 mg/kg 12555
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 54.70.00125 mg/kg 12652
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 83.80.00125 mg/kg 12354
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg <0.0002 79.20.00125 mg/kg 12755
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 69.00.00125 mg/kg 12554
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798131)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 84.30.00125 mg/kg 12157
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 62.90.00125 mg/kg 12555
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 56.00.00125 mg/kg 12652
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 72.30.00125 mg/kg 12354
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg <0.0002 78.40.00125 mg/kg 12755
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 67.90.00125 mg/kg 12554
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798132)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 65.00.00125 mg/kg 12157
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 75.20.00125 mg/kg 12555
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 93.40.00125 mg/kg 12652
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 86.00.00125 mg/kg 12354
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg <0.0002 99.00.00125 mg/kg 12755
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 99.40.00125 mg/kg 12554
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798133)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 74.20.00125 mg/kg 12157
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 83.00.00125 mg/kg 12555
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 88.80.00125 mg/kg 12652
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 87.80.00125 mg/kg 12354
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg <0.0002 90.10.00125 mg/kg 12755
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 93.00.00125 mg/kg 12554
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798138)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 70.20.00125 mg/kg 12157
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 74.20.00125 mg/kg 12555
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 84.10.00125 mg/kg 12652
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 73.00.00125 mg/kg 12354
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg <0.0002 74.60.00125 mg/kg 12755
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 73.90.00125 mg/kg 12554
18 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Method Blank (MB)
Report
Laboratory Control Spike (LCS) Report
Spike Spike Recovery (%) Recovery Limits (%)
Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798130)
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 52.30.00625 mg/kg 12852
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 72.50.00125 mg/kg 12954
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 66.60.00125 mg/kg 12758
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 76.20.00125 mg/kg 12857
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 1070.00125 mg/kg 13460
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 1160.00125 mg/kg 13063
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 1120.00125 mg/kg 13055
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 86.50.00125 mg/kg 13062
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 1010.00125 mg/kg 13453
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 85.40.00125 mg/kg 12949
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 94.90.00312 mg/kg 12959
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798131)
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 96.60.00625 mg/kg 12852
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 60.00.00125 mg/kg 12954
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 61.10.00125 mg/kg 12758
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 73.50.00125 mg/kg 12857
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 97.30.00125 mg/kg 13460
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 1050.00125 mg/kg 13063
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 1000.00125 mg/kg 13055
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 70.90.00125 mg/kg 13062
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 55.20.00125 mg/kg 13453
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 78.40.00125 mg/kg 12949
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 78.00.00312 mg/kg 12959
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798132)
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 79.80.00625 mg/kg 12852
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 99.00.00125 mg/kg 12954
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 82.50.00125 mg/kg 12758
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 1020.00125 mg/kg 12857
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 76.10.00125 mg/kg 13460
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 1070.00125 mg/kg 13063
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 95.30.00125 mg/kg 13055
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 1070.00125 mg/kg 13062
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 95.00.00125 mg/kg 13453
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 97.50.00125 mg/kg 12949
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 1170.00312 mg/kg 12959
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798133)
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 1230.00625 mg/kg 12852
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 90.00.00125 mg/kg 12954
19 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Method Blank (MB)
Report
Laboratory Control Spike (LCS) Report
Spike Spike Recovery (%) Recovery Limits (%)
Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798133) - continued
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 82.80.00125 mg/kg 12758
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 97.70.00125 mg/kg 12857
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 91.20.00125 mg/kg 13460
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 1030.00125 mg/kg 13063
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 85.40.00125 mg/kg 13055
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 95.40.00125 mg/kg 13062
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 82.60.00125 mg/kg 13453
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 82.00.00125 mg/kg 12949
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 1030.00312 mg/kg 12959
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798138)
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 87.30.00625 mg/kg 12852
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 89.50.00125 mg/kg 12954
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 77.30.00125 mg/kg 12758
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 1040.00125 mg/kg 12857
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 1090.00125 mg/kg 13460
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 1090.00125 mg/kg 13063
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 85.50.00125 mg/kg 13055
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 1060.00125 mg/kg 13062
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 1240.00125 mg/kg 13453
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 1220.00125 mg/kg 12949
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 1250.00312 mg/kg 12959
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798130)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 89.50.00125 mg/kg 13252
EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.0005 mg/kg <0.0005 92.60.00312 mg/kg 12665
EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.0005 mg/kg <0.0005 73.50.00312 mg/kg 12664
EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 76.10.00312 mg/kg 12463
EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 69.70.00312 mg/kg 12558
EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid
(MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 1060.00125 mg/kg 13061
EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid
(EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 72.30.00125 mg/kg 13055
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798131)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 68.80.00125 mg/kg 13252
EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.0005 mg/kg <0.0005 65.10.00312 mg/kg 12665
EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.0005 mg/kg <0.0005 67.10.00312 mg/kg 12664
EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 68.10.00312 mg/kg 12463
20 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Method Blank (MB)
Report
Laboratory Control Spike (LCS) Report
Spike Spike Recovery (%) Recovery Limits (%)
Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798131) - continued
EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 66.20.00312 mg/kg 12558
EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid
(MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 1240.00125 mg/kg 13061
EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid
(EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 75.30.00125 mg/kg 13055
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798132)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 68.00.00125 mg/kg 13252
EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.0005 mg/kg <0.0005 1000.00312 mg/kg 12665
EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.0005 mg/kg <0.0005 95.50.00312 mg/kg 12664
EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 1230.00312 mg/kg 12463
EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 66.00.00312 mg/kg 12558
EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid
(MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 1290.00125 mg/kg 13061
EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid
(EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 1230.00125 mg/kg 13055
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798133)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 56.80.00125 mg/kg 13252
EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.0005 mg/kg <0.0005 91.40.00312 mg/kg 12665
EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.0005 mg/kg <0.0005 69.60.00312 mg/kg 12664
EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 1210.00312 mg/kg 12463
EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 70.00.00312 mg/kg 12558
EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid
(MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 1050.00125 mg/kg 13061
EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid
(EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 1010.00125 mg/kg 13055
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798138)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 66.80.00125 mg/kg 13252
EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.0005 mg/kg <0.0005 1080.00312 mg/kg 12665
EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.0005 mg/kg <0.0005 1000.00312 mg/kg 12664
EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
2448-09-7 0.0005 mg/kg <0.0005 1160.00312 mg/kg 12463
EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
1691-99-2 0.0005 mg/kg <0.0005 86.30.00312 mg/kg 12558
21 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Method Blank (MB)
Report
Laboratory Control Spike (LCS) Report
Spike Spike Recovery (%) Recovery Limits (%)
Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798138) - continued
EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid
(MeFOSAA)
2355-31-9 0.0002 mg/kg <0.0002 1230.00125 mg/kg 13061
EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid
(EtFOSAA)
2991-50-6 0.0002 mg/kg <0.0002 88.20.00125 mg/kg 13055
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798130)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.0005 mg/kg <0.0005 56.70.00125 mg/kg 13054
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.0005 mg/kg <0.0005 72.40.00125 mg/kg 13061
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.0005 mg/kg <0.0005 1100.00125 mg/kg 13062
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.0005 mg/kg <0.0005 1190.00125 mg/kg 13060
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798131)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.0005 mg/kg <0.0005 74.20.00125 mg/kg 13054
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.0005 mg/kg <0.0005 1150.00125 mg/kg 13061
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.0005 mg/kg <0.0005 1150.00125 mg/kg 13062
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.0005 mg/kg <0.0005 95.20.00125 mg/kg 13060
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798132)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.0005 mg/kg <0.0005 1160.00125 mg/kg 13054
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.0005 mg/kg <0.0005 74.50.00125 mg/kg 13061
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.0005 mg/kg <0.0005 1070.00125 mg/kg 13062
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.0005 mg/kg <0.0005 79.40.00125 mg/kg 13060
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798133)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.0005 mg/kg <0.0005 1170.00125 mg/kg 13054
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.0005 mg/kg <0.0005 1160.00125 mg/kg 13061
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.0005 mg/kg <0.0005 99.20.00125 mg/kg 13062
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.0005 mg/kg <0.0005 82.00.00125 mg/kg 13060
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798138)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.0005 mg/kg <0.0005 1140.00125 mg/kg 13054
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.0005 mg/kg <0.0005 91.30.00125 mg/kg 13061
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.0005 mg/kg <0.0005 82.90.00125 mg/kg 13062
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.0005 mg/kg <0.0005 74.40.00125 mg/kg 13060
Sub-Matrix: WATER Method Blank (MB)
Report
Laboratory Control Spike (LCS) Report
Spike Spike Recovery (%) Recovery Limits (%)
Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798127)
EP231X-ST: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0005 µg/L <0.0005 80.40.01 µg/L 13050
EP231X-ST: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0005 µg/L <0.0005 85.20.01 µg/L 13050
EP231X-ST: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0005 µg/L <0.0005 85.20.01 µg/L 13050
EP231X-ST: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0005 µg/L <0.0005 83.40.01 µg/L 13050
EP231X-ST: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0003 µg/L <0.0003 96.00.01 µg/L 13050
22 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: WATER Method Blank (MB)
Report
Laboratory Control Spike (LCS) Report
Spike Spike Recovery (%) Recovery Limits (%)
Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798127) - continued
EP231X-ST: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0005 µg/L <0.0005 1070.01 µg/L 13050
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798141)
EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 84.80.5 µg/L 13070
EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 1070.5 µg/L 13070
EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L <0.02 1120.5 µg/L 13070
EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 89.40.5 µg/L 13070
EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 1030.5 µg/L 13070
EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 93.00.5 µg/L 13070
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 803834)
EP231X-ST: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0005 µg/L <0.0005 1120.01 µg/L 13050
EP231X-ST: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0005 µg/L <0.0005 92.20.01 µg/L 13050
EP231X-ST: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0005 µg/L <0.0005 86.00.01 µg/L 13050
EP231X-ST: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0005 µg/L <0.0005 1000.01 µg/L 13050
EP231X-ST: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0003 µg/L <0.0003 1040.01 µg/L 13050
EP231X-ST: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0005 µg/L <0.0005 92.40.01 µg/L 13050
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798127)
EP231X-ST: Perfluorobutanoic acid (PFBA) 375-22-4 0.002 µg/L <0.002 77.60.05 µg/L 13050
EP231X-ST: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0005 µg/L <0.0005 80.80.01 µg/L 13050
EP231X-ST: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0005 µg/L <0.0005 83.60.01 µg/L 13050
EP231X-ST: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0005 µg/L <0.0005 81.00.01 µg/L 13050
EP231X-ST: Perfluorooctanoic acid (PFOA) 335-67-1 0.0005 µg/L <0.0005 85.80.01 µg/L 13050
EP231X-ST: Perfluorononanoic acid (PFNA) 375-95-1 0.0005 µg/L <0.0005 87.80.01 µg/L 13050
EP231X-ST: Perfluorodecanoic acid (PFDA) 335-76-2 0.0005 µg/L <0.0005 89.20.01 µg/L 13050
EP231X-ST: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0005 µg/L <0.0005 92.00.01 µg/L 13050
EP231X-ST: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0005 µg/L <0.0005 83.40.01 µg/L 13050
EP231X-ST: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0005 µg/L <0.0005 97.20.01 µg/L 13050
EP231X-ST: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 µg/L <0.0005 77.00.025 µg/L 13050
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798141)
EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 92.02.5 µg/L 13070
EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 91.60.5 µg/L 13070
EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 1040.5 µg/L 13070
EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 1140.5 µg/L 13070
EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 89.20.5 µg/L 13070
EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 96.80.5 µg/L 13070
EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 87.80.5 µg/L 13070
EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 82.00.5 µg/L 13070
EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 1160.5 µg/L 13070
EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 94.60.5 µg/L 13070
23 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: WATER Method Blank (MB)
Report
Laboratory Control Spike (LCS) Report
Spike Spike Recovery (%) Recovery Limits (%)
Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798141) - continued
EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 1111.25 µg/L 12470
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 803834)
EP231X-ST: Perfluorobutanoic acid (PFBA) 375-22-4 0.002 µg/L <0.002 84.20.05 µg/L 13050
EP231X-ST: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0005 µg/L <0.0005 66.60.01 µg/L 13050
EP231X-ST: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0005 µg/L <0.0005 81.40.01 µg/L 13050
EP231X-ST: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0005 µg/L <0.0005 83.40.01 µg/L 13050
EP231X-ST: Perfluorooctanoic acid (PFOA) 335-67-1 0.0005 µg/L <0.0005 87.80.01 µg/L 13050
EP231X-ST: Perfluorononanoic acid (PFNA) 375-95-1 0.0005 µg/L <0.0005 84.20.01 µg/L 13050
EP231X-ST: Perfluorodecanoic acid (PFDA) 335-76-2 0.0005 µg/L <0.0005 97.00.01 µg/L 13050
EP231X-ST: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0005 µg/L <0.0005 76.00.01 µg/L 13050
EP231X-ST: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0005 µg/L <0.0005 88.80.01 µg/L 13050
EP231X-ST: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0005 µg/L <0.0005 89.60.01 µg/L 13050
EP231X-ST: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 µg/L <0.0005 1100.025 µg/L 13050
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798127)
EP231X-ST: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0005 µg/L <0.0005 77.80.01 µg/L 13050
EP231X-ST: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.001 µg/L <0.001 89.00.025 µg/L 13050
EP231X-ST: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.001 µg/L <0.001 84.20.025 µg/L 13050
EP231X-ST: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
2448-09-7 0.001 µg/L <0.001 96.20.025 µg/L 13050
EP231X-ST: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
1691-99-2 0.001 µg/L <0.001 86.60.025 µg/L 13050
EP231X-ST: N-Methyl perfluorooctane sulfonamidoacetic
acid (MeFOSAA)
2355-31-9 0.0005 µg/L <0.0005 80.40.01 µg/L 13050
EP231X-ST: N-Ethyl perfluorooctane sulfonamidoacetic
acid (EtFOSAA)
2991-50-6 0.0005 µg/L <0.0005 83.00.01 µg/L 13050
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798141)
EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 1190.5 µg/L 13070
EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.05 µg/L <0.05 93.31.25 µg/L 13070
EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.05 µg/L <0.05 95.41.25 µg/L 12970
EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
2448-09-7 0.05 µg/L <0.05 87.91.25 µg/L 12970
EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
1691-99-2 0.05 µg/L <0.05 1041.25 µg/L 12670
EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid
(MeFOSAA)
2355-31-9 0.02 µg/L <0.02 1190.5 µg/L 13070
EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid
(EtFOSAA)
2991-50-6 0.02 µg/L <0.02 1040.5 µg/L 13070
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 803834)
24 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: WATER Method Blank (MB)
Report
Laboratory Control Spike (LCS) Report
Spike Spike Recovery (%) Recovery Limits (%)
Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 803834) - continued
EP231X-ST: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0005 µg/L <0.0005 99.60.01 µg/L 13050
EP231X-ST: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
31506-32-8 0.001 µg/L <0.001 80.40.025 µg/L 13050
EP231X-ST: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.001 µg/L <0.001 88.20.025 µg/L 13050
EP231X-ST: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
2448-09-7 0.001 µg/L <0.001 96.30.025 µg/L 13050
EP231X-ST: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
1691-99-2 0.001 µg/L <0.001 96.90.025 µg/L 13050
EP231X-ST: N-Methyl perfluorooctane sulfonamidoacetic
acid (MeFOSAA)
2355-31-9 0.0005 µg/L <0.0005 78.20.01 µg/L 13050
EP231X-ST: N-Ethyl perfluorooctane sulfonamidoacetic
acid (EtFOSAA)
2991-50-6 0.0005 µg/L <0.0005 85.40.01 µg/L 13050
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798127)
EP231X-ST: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.001 µg/L <0.001 82.40.01 µg/L 13050
EP231X-ST: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.001 µg/L <0.001 88.20.01 µg/L 13050
EP231X-ST: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.001 µg/L <0.001 79.80.01 µg/L 13050
EP231X-ST: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.001 µg/L <0.001 1100.01 µg/L 13050
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798141)
EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.05 µg/L <0.05 95.80.5 µg/L 13070
EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.05 µg/L <0.05 1190.5 µg/L 13070
EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.05 µg/L <0.05 1060.5 µg/L 13070
EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.05 µg/L <0.05 1130.5 µg/L 13070
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 803834)
EP231X-ST: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.001 µg/L <0.001 1180.01 µg/L 13050
EP231X-ST: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.001 µg/L <0.001 1140.01 µg/L 13050
EP231X-ST: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.001 µg/L <0.001 93.20.01 µg/L 13050
EP231X-ST: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.001 µg/L <0.001 90.00.01 µg/L 13050
EP231P: PFAS Sums (QCLot: 798127)
EP231X-ST: Sum of PFAS ---- 0.0003 µg/L <0.0003 -------- --------
EP231P: PFAS Sums (QCLot: 803834)
EP231X-ST: Sum of PFAS ---- 0.0003 µg/L <0.0003 -------- --------
Matrix Spike (MS) ReportThe quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on
analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.
Sub-Matrix: SOIL Matrix Spike (MS) Report
SpikeRecovery(%) Recovery Limits (%)Spike
25 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Matrix Spike (MS) Report
SpikeRecovery(%) Recovery Limits (%)Spike
HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798130)
0315_BH001_0.0_170315 ES1706394-001 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 51.20.00125 mg/kg 13050
2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 75.30.00125 mg/kg 13050
355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) # Not
Determined
0.00125 mg/kg 13050
375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 1040.00125 mg/kg 13050
1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) # Not
Determined
0.00125 mg/kg 13050
335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) # Not
Determined
0.00125 mg/kg 13050
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798131)
0315_BH005_0.0_170314 ES1706394-021 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 72.30.00125 mg/kg 13050
2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 62.00.00125 mg/kg 13050
355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 89.40.00125 mg/kg 13050
375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 68.20.00125 mg/kg 13050
1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) # Not
Determined
0.00125 mg/kg 13050
335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 1100.00125 mg/kg 13050
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798132)
0315_BH009_0.0_170315 ES1706394-041 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 87.00.00125 mg/kg 13050
2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 78.60.00125 mg/kg 13050
355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 66.90.00125 mg/kg 13050
375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 55.70.00125 mg/kg 13050
1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) # Not
Determined
0.00125 mg/kg 13050
335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 1070.00125 mg/kg 13050
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798133)
0315_BH013_0.0_170314 ES1706394-061 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 1110.00125 mg/kg 13050
2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 1070.00125 mg/kg 13050
355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 83.40.00125 mg/kg 13050
375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 77.40.00125 mg/kg 13050
1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) # Not
Determined
0.00125 mg/kg 13050
335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 56.00.00125 mg/kg 13050
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798138)
0315_SD006_170316 ES1706394-089 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 1080.00125 mg/kg 13050
2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 1020.00125 mg/kg 13050
355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 95.20.00125 mg/kg 13050
375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 90.40.00125 mg/kg 13050
26 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Matrix Spike (MS) Report
SpikeRecovery(%) Recovery Limits (%)Spike
HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798138) - continued
0315_SD006_170316 ES1706394-089 1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) 99.60.00125 mg/kg 13050
335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 77.20.00125 mg/kg 13050
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798130)
0315_BH001_0.0_170315 ES1706394-001 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 1250.00625 mg/kg 13030
2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) # 36.20.00125 mg/kg 13050
307-24-4EP231X: Perfluorohexanoic acid (PFHxA) # Not
Determined
0.00125 mg/kg 13050
375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 90.40.00125 mg/kg 13050
335-67-1EP231X: Perfluorooctanoic acid (PFOA) 99.60.00125 mg/kg 13050
375-95-1EP231X: Perfluorononanoic acid (PFNA) 90.00.00125 mg/kg 13050
335-76-2EP231X: Perfluorodecanoic acid (PFDA) 96.40.00125 mg/kg 13050
2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 58.80.00125 mg/kg 13050
307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 1200.00125 mg/kg 13050
72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 58.40.00125 mg/kg 13030
376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) # 18.20.00312 mg/kg 13030
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798131)
0315_BH005_0.0_170314 ES1706394-021 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 1140.00625 mg/kg 13030
2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 95.90.00125 mg/kg 13050
307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 74.60.00125 mg/kg 13050
375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 84.20.00125 mg/kg 13050
335-67-1EP231X: Perfluorooctanoic acid (PFOA) 88.30.00125 mg/kg 13050
375-95-1EP231X: Perfluorononanoic acid (PFNA) 90.00.00125 mg/kg 13050
335-76-2EP231X: Perfluorodecanoic acid (PFDA) 63.20.00125 mg/kg 13050
2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 55.30.00125 mg/kg 13050
307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 1150.00125 mg/kg 13050
72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 1160.00125 mg/kg 13030
376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 74.80.00312 mg/kg 13030
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798132)
0315_BH009_0.0_170315 ES1706394-041 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 86.60.00625 mg/kg 13030
2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 1200.00125 mg/kg 13050
307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 92.30.00125 mg/kg 13050
375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 1030.00125 mg/kg 13050
335-67-1EP231X: Perfluorooctanoic acid (PFOA) 80.90.00125 mg/kg 13050
375-95-1EP231X: Perfluorononanoic acid (PFNA) 1110.00125 mg/kg 13050
335-76-2EP231X: Perfluorodecanoic acid (PFDA) 53.80.00125 mg/kg 13050
2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 84.90.00125 mg/kg 13050
307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 1280.00125 mg/kg 13050
72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 37.20.00125 mg/kg 13030
27 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Matrix Spike (MS) Report
SpikeRecovery(%) Recovery Limits (%)Spike
HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798132) - continued
0315_BH009_0.0_170315 ES1706394-041 376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 1190.00312 mg/kg 13030
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798133)
0315_BH013_0.0_170314 ES1706394-061 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 1240.00625 mg/kg 13030
2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 1140.00125 mg/kg 13050
307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 1240.00125 mg/kg 13050
375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 89.60.00125 mg/kg 13050
335-67-1EP231X: Perfluorooctanoic acid (PFOA) 72.70.00125 mg/kg 13050
375-95-1EP231X: Perfluorononanoic acid (PFNA) 53.20.00125 mg/kg 13050
335-76-2EP231X: Perfluorodecanoic acid (PFDA) 61.60.00125 mg/kg 13050
2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 51.50.00125 mg/kg 13050
307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 83.20.00125 mg/kg 13050
72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 75.40.00125 mg/kg 13030
376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 38.30.00312 mg/kg 13030
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798138)
0315_SD006_170316 ES1706394-089 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 80.20.00625 mg/kg 13030
2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 1240.00125 mg/kg 13050
307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 94.80.00125 mg/kg 13050
375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 1170.00125 mg/kg 13050
335-67-1EP231X: Perfluorooctanoic acid (PFOA) 1140.00125 mg/kg 13050
375-95-1EP231X: Perfluorononanoic acid (PFNA) 1120.00125 mg/kg 13050
335-76-2EP231X: Perfluorodecanoic acid (PFDA) 1170.00125 mg/kg 13050
2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 83.20.00125 mg/kg 13050
307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 88.00.00125 mg/kg 13050
72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 1040.00125 mg/kg 13030
376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 1030.00312 mg/kg 13030
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798130)
0315_BH001_0.0_170315 ES1706394-001 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) # Not
Determined
0.00125 mg/kg 13050
31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
1040.00312 mg/kg 13030
4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) # 22.00.00312 mg/kg 13030
2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
1140.00312 mg/kg 13030
1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
# 15.30.00312 mg/kg 13030
2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic
acid (MeFOSAA)
48.40.00125 mg/kg 13030
2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic
acid (EtFOSAA)
31.60.00125 mg/kg 13030
28 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Matrix Spike (MS) Report
SpikeRecovery(%) Recovery Limits (%)Spike
HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798131)
0315_BH005_0.0_170314 ES1706394-021 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 99.70.00125 mg/kg 13050
31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
75.00.00312 mg/kg 13030
4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 86.20.00312 mg/kg 13030
2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
72.00.00312 mg/kg 13030
1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
1230.00312 mg/kg 13030
2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic
acid (MeFOSAA)
68.00.00125 mg/kg 13030
2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic
acid (EtFOSAA)
63.00.00125 mg/kg 13030
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798132)
0315_BH009_0.0_170315 ES1706394-041 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 1300.00125 mg/kg 13050
31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
49.10.00312 mg/kg 13030
4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 1060.00312 mg/kg 13030
2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
51.10.00312 mg/kg 13030
1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
31.60.00312 mg/kg 13030
2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic
acid (MeFOSAA)
52.80.00125 mg/kg 13030
2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic
acid (EtFOSAA)
55.50.00125 mg/kg 13030
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798133)
0315_BH013_0.0_170314 ES1706394-061 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 82.00.00125 mg/kg 13050
31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
81.10.00312 mg/kg 13030
4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 67.50.00312 mg/kg 13030
2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
46.00.00312 mg/kg 13030
1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
63.00.00312 mg/kg 13030
2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic
acid (MeFOSAA)
60.00.00125 mg/kg 13030
2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic
acid (EtFOSAA)
86.80.00125 mg/kg 13030
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798138)
29 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Matrix Spike (MS) Report
SpikeRecovery(%) Recovery Limits (%)Spike
HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798138) - continued
0315_SD006_170316 ES1706394-089 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 93.60.00125 mg/kg 13050
31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
1120.00312 mg/kg 13030
4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 1070.00312 mg/kg 13030
2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
99.50.00312 mg/kg 13030
1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
78.00.00312 mg/kg 13030
2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic
acid (MeFOSAA)
94.40.00125 mg/kg 13030
2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic
acid (EtFOSAA)
95.60.00125 mg/kg 13030
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798130)
0315_BH001_0.0_170315 ES1706394-001 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 93.10.00125 mg/kg 13050
27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 82.40.00125 mg/kg 13050
39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) # Not
Determined
0.00125 mg/kg 13050
120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) # 9.360.00125 mg/kg 13050
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798131)
0315_BH005_0.0_170314 ES1706394-021 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 89.60.00125 mg/kg 13050
27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 1030.00125 mg/kg 13050
39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 1030.00125 mg/kg 13050
120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 65.80.00125 mg/kg 13050
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798132)
0315_BH009_0.0_170315 ES1706394-041 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 1180.00125 mg/kg 13050
27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 1140.00125 mg/kg 13050
39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 63.70.00125 mg/kg 13050
120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 65.80.00125 mg/kg 13050
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798133)
0315_BH013_0.0_170314 ES1706394-061 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 94.80.00125 mg/kg 13050
27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) # Not
Determined
0.00125 mg/kg 13050
39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 53.80.00125 mg/kg 13050
120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 70.40.00125 mg/kg 13050
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798138)
0315_SD006_170316 ES1706394-089 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 1090.00125 mg/kg 13050
27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 1200.00125 mg/kg 13050
39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 82.80.00125 mg/kg 13050
30 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: SOIL Matrix Spike (MS) Report
SpikeRecovery(%) Recovery Limits (%)Spike
HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798138) - continued
0315_SD006_170316 ES1706394-089 120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 67.20.00125 mg/kg 13050
Sub-Matrix: WATER Matrix Spike (MS) Report
SpikeRecovery(%) Recovery Limits (%)Spike
HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number
EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 798141)
Anonymous EB1705137-001 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 1110.5 µg/L 13050
2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 97.80.5 µg/L 13050
355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 1120.5 µg/L 13050
375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 1070.5 µg/L 13050
1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) 1120.5 µg/L 13050
335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 1070.5 µg/L 13050
EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 798141)
Anonymous EB1705137-001 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 72.02.5 µg/L 13050
2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 1250.5 µg/L 13050
307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 95.80.5 µg/L 13050
375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 1030.5 µg/L 13050
335-67-1EP231X: Perfluorooctanoic acid (PFOA) 85.60.5 µg/L 13050
375-95-1EP231X: Perfluorononanoic acid (PFNA) 84.20.5 µg/L 13050
335-76-2EP231X: Perfluorodecanoic acid (PFDA) 81.40.5 µg/L 13050
2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 95.80.5 µg/L 13050
307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 93.00.5 µg/L 13050
72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 88.00.5 µg/L 13050
376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 90.61.25 µg/L 13050
EP231C: Perfluoroalkyl Sulfonamides (QCLot: 798141)
Anonymous EB1705137-001 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 1010.5 µg/L 13050
31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide
(MeFOSA)
1191.25 µg/L 13050
4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 89.91.25 µg/L 13050
2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol
(MeFOSE)
1091.25 µg/L 13050
1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol
(EtFOSE)
91.41.25 µg/L 13050
2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic
acid (MeFOSAA)
83.60.5 µg/L 13050
2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic
acid (EtFOSAA)
99.60.5 µg/L 13050
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798141)
Anonymous EB1705137-001 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 93.40.5 µg/L 13050
31 of 31:Page
Work Order :
:Client
ES1706394 Amendment 2
GOLDER ASSOCIATES
1652034:Project
Sub-Matrix: WATER Matrix Spike (MS) Report
SpikeRecovery(%) Recovery Limits (%)Spike
HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number
EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 798141) - continued
Anonymous EB1705137-001 27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 95.80.5 µg/L 13050
39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 95.40.5 µg/L 13050
120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 84.00.5 µg/L 13050
0 0.00 True
Environmental
CERTIFICATE OF ANALYSISWork Order : Page : 1 of 49ES1706394
:Amendment 2:: LaboratoryClient GOLDER ASSOCIATES Environmental Division Sydney
: :ContactContact MS OLGA BUKHTEEVA Customer Services ES
:: AddressAddress LEVEL 1, 124 PACIFIC HIGHWAY
ST LEONARDS NSW, AUSTRALIA 2065
277-289 Woodpark Road Smithfield NSW Australia 2164
:Telephone +61 02 9478 3900 :Telephone +61-2-8784 8555
:Project 1652034 Date Samples Received : 17-Mar-2017 12:00
:Order number PO01472 Date Analysis Commenced : 20-Mar-2017
:C-O-C number ---- Issue Date : 10-Apr-2017 17:37
Sampler : OLGA BUKHTEEVA
Site : Kapooka
Quote number : BN/404/16
110:No. of samples received
103:No. of samples analysed
This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.
This Certificate of Analysis contains the following information:
l General Comments
l Analytical Results
l Surrogate Control Limits
Additional information pertinent to this report will be found in the following separate attachments: Quality Control Report, QA/QC Compliance Assessment to assist with
Quality Review and Sample Receipt Notification.
SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.
Signatories Accreditation CategoryPosition
Alex Rossi Organic Chemist Sydney Organics, Smithfield, NSW
Edwandy Fadjar Organic Coordinator Sydney Inorganics, Smithfield, NSW
R I G H T S O L U T I O N S | R I G H T P A R T N E R
2 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
General Comments
The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house
developed procedures are employed in the absence of documented standards or by client request.
Where moisture determination has been performed, results are reported on a dry weight basis.
Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis.
Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.
When no sampling time is provided, the sampling time will default 00:00 on the date of sampling. If no sampling date is provided, the sampling date will be assumed by the laboratory and displayed in brackets without a
time component.
Where a result is required to meet compliance limits the associated uncertainty must be considered. Refer to the ALS Contact for details.
CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.
LOR = Limit of reporting
^ = This result is computed from individual analyte detections at or above the level of reporting
ø = ALS is not NATA accredited for these tests.
~ = Indicates an estimated value.
Key :
EP231X: Poor Matrix Spike (MS) recoveries on various analytes is due to matrix interferences and effects. This was confirmed by re-extraction and re-analysis.l
Amendment (10/04/2017): This report has been amended with the removal of analysis for samples 105-110. All analysis results are as per the previous report.l
3 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH001_4.0_170
315
0315_BH001_3.0_170
315
0315_BH001_2.0_170
315
0315_BH001_1.0_170
315
0315_BH001_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-005ES1706394-004ES1706394-003ES1706394-002ES1706394-001UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
10.2 16.2 11.4 4.9 4.6%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
0.0009Perfluorobutane sulfonic acid
(PFBS)
0.0448 0.0342 0.0029 0.0009mg/kg0.0002375-73-5
0.0015Perfluoropentane sulfonic acid
(PFPeS)
0.0665 0.0582 0.0020 0.0005mg/kg0.00022706-91-4
0.0518Perfluorohexane sulfonic acid
(PFHxS)
0.741 0.342 0.0134 0.0068mg/kg0.0002355-46-4
0.0013Perfluoroheptane sulfonic acid
(PFHpS)
0.0577 0.0317 0.0009 0.0004mg/kg0.0002375-92-8
1.15Perfluorooctane sulfonic acid
(PFOS)
2.60 0.0859 0.0378 0.0128mg/kg0.00021763-23-1
0.0172Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
0.014Perfluorobutanoic acid (PFBA) 0.027 0.007 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) 0.0281 0.0206 <0.0002 <0.0002mg/kg0.00022706-90-3
0.0085Perfluorohexanoic acid (PFHxA) 0.143 0.0713 0.0035 0.0008mg/kg0.0002307-24-4
0.0013Perfluoroheptanoic acid (PFHpA) 0.0329 0.0093 0.0005 <0.0002mg/kg0.0002375-85-9
0.0050Perfluorooctanoic acid (PFOA) 0.0560 0.0129 0.0014 0.0004mg/kg0.0002335-67-1
0.0004Perfluorononanoic acid (PFNA) 0.0019 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
0.0009Perfluorodecanoic acid (PFDA) 0.0003 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
0.0112Perfluorooctane sulfonamide
(FOSA)
0.0018 0.0005 0.0004 0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
4 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH001_4.0_170
315
0315_BH001_3.0_170
315
0315_BH001_2.0_170
315
0315_BH001_1.0_170
315
0315_BH001_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-005ES1706394-004ES1706394-003ES1706394-002ES1706394-001UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
0.00326:2 Fluorotelomer sulfonic acid
(6:2 FTS)
0.0364 0.0038 <0.0005 <0.0005mg/kg0.000527619-97-2
0.00648:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
1.27 3.84 0.677 0.0628 0.0228mg/kg0.0002----Sum of PFAS
1.20Sum of PFHxS and PFOS 3.34 0.428 0.0512 0.0196mg/kg0.0002355-46-4/1763-23-
1
1.24 3.71 0.587 0.0595 0.0217mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
99.7 99.4 93.4 103 102%0.0002----13C4-PFOS
5 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH002_4.0_170
315
0315_BH002_3.0_170
315
0315_BH002_2.0_170
315
0315_BH002_1.0_170
315
0315_BH002_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-010ES1706394-009ES1706394-008ES1706394-007ES1706394-006UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
20.7 15.9 12.5 20.1 10.1%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
0.0005Perfluorobutane sulfonic acid
(PFBS)
<0.0002 0.0002 <0.0002 0.0018mg/kg0.0002375-73-5
0.0005Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 0.0003 <0.0002 0.0016mg/kg0.00022706-91-4
0.0152Perfluorohexane sulfonic acid
(PFHxS)
0.0066 0.0089 0.0039 0.0241mg/kg0.0002355-46-4
0.0007Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 0.0014 0.0004 0.0014mg/kg0.0002375-92-8
0.174Perfluorooctane sulfonic acid
(PFOS)
0.222 0.119 0.0303 0.0458mg/kg0.00021763-23-1
0.0028Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) 0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3
0.0022Perfluorohexanoic acid (PFHxA) 0.0015 0.0008 0.0003 0.0025mg/kg0.0002307-24-4
0.0008Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 0.0003mg/kg0.0002375-85-9
0.0020Perfluorooctanoic acid (PFOA) 0.0004 0.0005 0.0002 0.0010mg/kg0.0002335-67-1
0.0011Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
0.0008Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
0.0027Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
6 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH002_4.0_170
315
0315_BH002_3.0_170
315
0315_BH002_2.0_170
315
0315_BH002_1.0_170
315
0315_BH002_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-010ES1706394-009ES1706394-008ES1706394-007ES1706394-006UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
0.00068:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.204 0.232 0.131 0.0351 0.0785mg/kg0.0002----Sum of PFAS
0.189Sum of PFHxS and PFOS 0.229 0.128 0.0342 0.0699mg/kg0.0002355-46-4/1763-23-
1
0.195 0.232 0.129 0.0347 0.0755mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
98.3 99.4 101 101 100%0.0002----13C4-PFOS
7 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH003_4.0_170
314
0315_BH003_3.0_170
314
0315_BH003_2.0_170
314
0315_BH003_1.0_170
314
0315_BH003_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-015ES1706394-014ES1706394-013ES1706394-012ES1706394-011UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
15.3 15.9 20.6 7.8 7.5%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
0.0020Perfluorobutane sulfonic acid
(PFBS)
0.0411 0.0245 0.0022 0.0011mg/kg0.0002375-73-5
0.0024Perfluoropentane sulfonic acid
(PFPeS)
0.0516 0.0403 0.0022 0.0016mg/kg0.00022706-91-4
0.0517Perfluorohexane sulfonic acid
(PFHxS)
0.0484 0.456 0.0243 0.0181mg/kg0.0002355-46-4
0.0054Perfluoroheptane sulfonic acid
(PFHpS)
0.0686 0.0320 0.0015 0.0010mg/kg0.0002375-92-8
0.462Perfluorooctane sulfonic acid
(PFOS)
3.70 0.404 0.0386 0.0239mg/kg0.00021763-23-1
0.0273Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) 0.008 0.003 <0.001 <0.001mg/kg0.001375-22-4
0.0049Perfluoropentanoic acid (PFPeA) 0.0261 0.0075 <0.0002 <0.0002mg/kg0.00022706-90-3
0.0075Perfluorohexanoic acid (PFHxA) 0.0883 0.0512 0.0041 0.0026mg/kg0.0002307-24-4
0.0024Perfluoroheptanoic acid (PFHpA) 0.0116 0.0090 0.0004 0.0004mg/kg0.0002375-85-9
0.0078Perfluorooctanoic acid (PFOA) 0.0271 0.0163 0.0012 0.0009mg/kg0.0002335-67-1
0.0034Perfluorononanoic acid (PFNA) 0.0010 0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
0.0044Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
0.0024Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
0.0043Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
0.0016Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
0.0477Perfluorooctane sulfonamide
(FOSA)
0.0002 0.0010 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
8 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH003_4.0_170
314
0315_BH003_3.0_170
314
0315_BH003_2.0_170
314
0315_BH003_1.0_170
314
0315_BH003_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-015ES1706394-014ES1706394-013ES1706394-012ES1706394-011UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
0.0007N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
0.00366:2 Fluorotelomer sulfonic acid
(6:2 FTS)
0.0138 0.0010 <0.0005 <0.0005mg/kg0.000527619-97-2
0.00578:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
0.000610:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.648 4.08 1.05 0.0745 0.0496mg/kg0.0002----Sum of PFAS
0.514Sum of PFHxS and PFOS 3.75 0.860 0.0629 0.0420mg/kg0.0002355-46-4/1763-23-
1
0.548 3.96 0.972 0.0708 0.0470mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
99.9 101 99.0 103 99.3%0.0002----13C4-PFOS
9 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH004_4.0_170
314
0315_BH004_3.0_170
314
0315_BH004_2.0_170
314
0315_BH004_1.0_170
314
0315_BH004_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-020ES1706394-019ES1706394-018ES1706394-017ES1706394-016UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
7.5 12.6 13.1 7.2 7.6%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
0.0003Perfluorobutane sulfonic acid
(PFBS)
0.0006 0.0152 0.0048 0.0007mg/kg0.0002375-73-5
0.0004Perfluoropentane sulfonic acid
(PFPeS)
0.0006 0.0181 0.0039 0.0007mg/kg0.00022706-91-4
0.0084Perfluorohexane sulfonic acid
(PFHxS)
0.0130 0.209 0.0356 0.0081mg/kg0.0002355-46-4
0.0008Perfluoroheptane sulfonic acid
(PFHpS)
0.0016 0.231 0.0019 0.0005mg/kg0.0002375-92-8
0.124Perfluorooctane sulfonic acid
(PFOS)
0.394 0.789 0.0374 0.0129mg/kg0.00021763-23-1
0.0060Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 0.004 <0.001 <0.001mg/kg0.001375-22-4
0.0025Perfluoropentanoic acid (PFPeA) 0.0023 0.0148 0.0019 <0.0002mg/kg0.00022706-90-3
0.0025Perfluorohexanoic acid (PFHxA) 0.0034 0.0365 0.0066 0.0012mg/kg0.0002307-24-4
0.0016Perfluoroheptanoic acid (PFHpA) 0.0013 0.0099 0.0010 <0.0002mg/kg0.0002375-85-9
0.0031Perfluorooctanoic acid (PFOA) 0.0024 0.0214 0.0018 0.0004mg/kg0.0002335-67-1
0.0035Perfluorononanoic acid (PFNA) 0.0009 0.0013 <0.0002 <0.0002mg/kg0.0002375-95-1
0.0032Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
0.0010Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
0.0010Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
0.0047Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
10 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH004_4.0_170
314
0315_BH004_3.0_170
314
0315_BH004_2.0_170
314
0315_BH004_1.0_170
314
0315_BH004_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-020ES1706394-019ES1706394-018ES1706394-017ES1706394-016UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
0.00446:2 Fluorotelomer sulfonic acid
(6:2 FTS)
0.0083 0.0399 0.0016 <0.0005mg/kg0.000527619-97-2
0.00828:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.176 0.428 1.39 0.0965 0.0245mg/kg0.0002----Sum of PFAS
0.132Sum of PFHxS and PFOS 0.407 0.998 0.0730 0.0210mg/kg0.0002355-46-4/1763-23-
1
0.155 0.425 1.14 0.0907 0.0233mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
85.6 85.7 99.4 91.3 116%0.0002----13C4-PFOS
11 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH005_4.0_170
314
0315_BH005_3.0_170
314
0315_BH005_2.0_170
314
0315_BH005_1.0_170
314
0315_BH005_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-025ES1706394-024ES1706394-023ES1706394-022ES1706394-021UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
10.8 9.6 11.6 13.4 16.6%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4
0.0003Perfluorohexane sulfonic acid
(PFHxS)
0.0005 0.0004 <0.0002 0.0002mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.0124Perfluorooctane sulfonic acid
(PFOS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) 0.0011 0.0003 0.0007 <0.0002mg/kg0.00022706-90-3
<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9
<0.0002Perfluorooctanoic acid (PFOA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
12 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH005_4.0_170
314
0315_BH005_3.0_170
314
0315_BH005_2.0_170
314
0315_BH005_1.0_170
314
0315_BH005_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-025ES1706394-024ES1706394-023ES1706394-022ES1706394-021UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0127 0.0016 0.0007 0.0007 0.0002mg/kg0.0002----Sum of PFAS
0.0127Sum of PFHxS and PFOS 0.0005 0.0004 <0.0002 0.0002mg/kg0.0002355-46-4/1763-23-
1
0.0127 0.0016 0.0007 0.0007 0.0002mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
82.9 128 108 94.1 100%0.0002----13C4-PFOS
13 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH006_4.0_170
314
0315_BH006_3.0_170
314
0315_BH006_2.0_170
314
0315_BH006_1.0_170
314
0315_BH006_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-030ES1706394-029ES1706394-028ES1706394-027ES1706394-026UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
8.6 10.8 13.6 11.3 15.4%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4
0.0004Perfluorohexane sulfonic acid
(PFHxS)
0.0002 0.0008 <0.0002 0.0005mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.0155Perfluorooctane sulfonic acid
(PFOS)
0.0102 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
0.0002Perfluoropentanoic acid (PFPeA) <0.0002 0.0002 0.0004 0.0002mg/kg0.00022706-90-3
<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9
0.0002Perfluorooctanoic acid (PFOA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
14 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH006_4.0_170
314
0315_BH006_3.0_170
314
0315_BH006_2.0_170
314
0315_BH006_1.0_170
314
0315_BH006_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-030ES1706394-029ES1706394-028ES1706394-027ES1706394-026UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0163 0.0104 0.0010 0.0004 0.0007mg/kg0.0002----Sum of PFAS
0.0159Sum of PFHxS and PFOS 0.0104 0.0008 <0.0002 0.0005mg/kg0.0002355-46-4/1763-23-
1
0.0163 0.0104 0.0010 0.0004 0.0007mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
95.8 84.8 87.1 88.8 111%0.0002----13C4-PFOS
15 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH007_4.0_170
315
0315_BH007_3.0_170
315
0315_BH007_2.0_170
315
0315_BH007_1.0_170
315
0315_BH007_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-035ES1706394-034ES1706394-033ES1706394-032ES1706394-031UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
2.7 8.4 11.0 14.1 8.8%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4
0.0010Perfluorohexane sulfonic acid
(PFHxS)
0.0028 0.0007 <0.0002 0.0003mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.0159Perfluorooctane sulfonic acid
(PFOS)
0.0062 0.0054 <0.0002 <0.0002mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
0.0006Perfluoropentanoic acid (PFPeA) <0.0002 0.0003 <0.0002 0.0006mg/kg0.00022706-90-3
0.0002Perfluorohexanoic acid (PFHxA) 0.0006 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9
0.0002Perfluorooctanoic acid (PFOA) 0.0005 0.0015 <0.0002 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
16 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH007_4.0_170
315
0315_BH007_3.0_170
315
0315_BH007_2.0_170
315
0315_BH007_1.0_170
315
0315_BH007_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-035ES1706394-034ES1706394-033ES1706394-032ES1706394-031UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 0.0011 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0179 0.0101 0.0090 <0.0002 0.0009mg/kg0.0002----Sum of PFAS
0.0169Sum of PFHxS and PFOS 0.0090 0.0061 <0.0002 0.0003mg/kg0.0002355-46-4/1763-23-
1
0.0179 0.0101 0.0079 <0.0002 0.0009mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
88.4 128 96.4 80.7 76.4%0.0002----13C4-PFOS
17 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH008_4.0_170
315
0315_BH008_3.0_170
315
0315_BH008_2.0_170
315
0315_BH008_1.0_170
315
0315_BH008_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-040ES1706394-039ES1706394-038ES1706394-037ES1706394-036UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
1.3 8.1 17.3 16.8 26.0%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
0.0006Perfluorobutane sulfonic acid
(PFBS)
0.0008 0.0012 0.0110 0.0028mg/kg0.0002375-73-5
0.0008Perfluoropentane sulfonic acid
(PFPeS)
0.0014 0.0023 0.0095 0.0038mg/kg0.00022706-91-4
0.0034Perfluorohexane sulfonic acid
(PFHxS)
0.0330 0.0768 0.0074 0.0266mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
0.0055 0.0026 <0.0002 0.0019mg/kg0.0002375-92-8
0.0167Perfluorooctane sulfonic acid
(PFOS)
0.782 1.33 0.0003 0.0023mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
0.0011Perfluoropentanoic acid (PFPeA) 0.0006 0.0009 0.0028 0.0012mg/kg0.00022706-90-3
0.0029Perfluorohexanoic acid (PFHxA) 0.0043 0.0068 0.0192 0.0094mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) 0.0005 0.0013 0.0011 0.0011mg/kg0.0002375-85-9
<0.0002Perfluorooctanoic acid (PFOA) 0.0038 0.0025 <0.0002 0.0016mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
0.0006Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
0.0010 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
18 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH008_4.0_170
315
0315_BH008_3.0_170
315
0315_BH008_2.0_170
315
0315_BH008_1.0_170
315
0315_BH008_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-040ES1706394-039ES1706394-038ES1706394-037ES1706394-036UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0261 0.833 1.42 0.0513 0.0507mg/kg0.0002----Sum of PFAS
0.0201Sum of PFHxS and PFOS 0.815 1.41 0.0077 0.0289mg/kg0.0002355-46-4/1763-23-
1
0.0247 0.825 1.42 0.0418 0.0450mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
102 88.9 79.3 95.1 77.3%0.0002----13C4-PFOS
19 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH009_4.0_170
315
0315_BH009_3.0_170
315
0315_BH009_2.0_170
315
0315_BH009_1.0_170
315
0315_BH009_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-045ES1706394-044ES1706394-043ES1706394-042ES1706394-041UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
3.0 12.0 11.3 8.2 11.4%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
0.0006 0.0284 0.0024 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
0.0007 0.0210 0.0016 <0.0002mg/kg0.00022706-91-4
0.0038Perfluorohexane sulfonic acid
(PFHxS)
0.0138 0.109 0.0142 0.0007mg/kg0.0002355-46-4
0.0020Perfluoroheptane sulfonic acid
(PFHpS)
0.0157 0.0025 0.0002 <0.0002mg/kg0.0002375-92-8
0.324Perfluorooctane sulfonic acid
(PFOS)
0.556 0.0148 <0.0002 <0.0002mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 0.0063 <0.0002 <0.0002mg/kg0.00022706-90-3
0.0009Perfluorohexanoic acid (PFHxA) 0.0035 0.0481 0.0040 0.0002mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 0.0051 0.0004 <0.0002mg/kg0.0002375-85-9
0.0006Perfluorooctanoic acid (PFOA) 0.0014 0.0019 0.0002 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
0.0010Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
20 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH009_4.0_170
315
0315_BH009_3.0_170
315
0315_BH009_2.0_170
315
0315_BH009_1.0_170
315
0315_BH009_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-045ES1706394-044ES1706394-043ES1706394-042ES1706394-041UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
0.0016 <0.0005 <0.0005 0.0010mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.332 0.593 0.237 0.0230 0.0019mg/kg0.0002----Sum of PFAS
0.328Sum of PFHxS and PFOS 0.570 0.124 0.0142 0.0007mg/kg0.0002355-46-4/1763-23-
1
0.329 0.575 0.214 0.0212 0.0009mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
76.9 93.3 108 98.3 93.9%0.0002----13C4-PFOS
21 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH010_4.0_170
315
0315_BH010_3.0_170
315
0315_BH010_2.0_170
315
0315_BH010_1.0_170
315
0315_BH010_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-050ES1706394-049ES1706394-048ES1706394-047ES1706394-046UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
1.7 14.4 13.1 15.6 13.2%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4
0.0002Perfluorohexane sulfonic acid
(PFHxS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.0107Perfluorooctane sulfonic acid
(PFOS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3
<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 0.0003 <0.0002 <0.0002mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9
<0.0002Perfluorooctanoic acid (PFOA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
22 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH010_4.0_170
315
0315_BH010_3.0_170
315
0315_BH010_2.0_170
315
0315_BH010_1.0_170
315
0315_BH010_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-050ES1706394-049ES1706394-048ES1706394-047ES1706394-046UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
0.0036N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
0.0008 0.0005 0.0005 0.0006mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0145 0.0008 0.0008 0.0005 0.0006mg/kg0.0002----Sum of PFAS
0.0109Sum of PFHxS and PFOS <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4/1763-23-
1
0.0109 <0.0002 0.0003 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
99.4 114 89.4 102 92.4%0.0002----13C4-PFOS
23 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH011_4.0_170
314
0315_BH011_3.0_170
314
0315_BH011_2.0_170
314
0315_BH011_1.0_170
314
0315_BH011_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-055ES1706394-054ES1706394-053ES1706394-052ES1706394-051UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
4.1 9.5 8.6 9.5 8.6%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4
<0.0002Perfluorohexane sulfonic acid
(PFHxS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.0008Perfluorooctane sulfonic acid
(PFOS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3
<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9
0.0003Perfluorooctanoic acid (PFOA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
24 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH011_4.0_170
314
0315_BH011_3.0_170
314
0315_BH011_2.0_170
314
0315_BH011_1.0_170
314
0315_BH011_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-055ES1706394-054ES1706394-053ES1706394-052ES1706394-051UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
0.0009N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
0.0007 0.0007 0.0012 0.0008mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0020 0.0007 0.0007 0.0012 0.0008mg/kg0.0002----Sum of PFAS
0.0008Sum of PFHxS and PFOS <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4/1763-23-
1
0.0011 <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
112 108 125 105 116%0.0002----13C4-PFOS
25 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH012_4.0_170
314
0315_BH012_3.0_170
314
0315_BH012_2.0_170
314
0315_BH012_1.0_170
314
0315_BH012_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-060ES1706394-059ES1706394-058ES1706394-057ES1706394-056UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
5.9 16.6 13.6 20.3 12.8%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4
0.0009Perfluorohexane sulfonic acid
(PFHxS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.0011Perfluorooctane sulfonic acid
(PFOS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3
0.0006Perfluorohexanoic acid (PFHxA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9
<0.0002Perfluorooctanoic acid (PFOA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
26 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH012_4.0_170
314
0315_BH012_3.0_170
314
0315_BH012_2.0_170
314
0315_BH012_1.0_170
314
0315_BH012_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-060ES1706394-059ES1706394-058ES1706394-057ES1706394-056UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
0.0006 0.0007 0.0008 0.0008mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0031 0.0006 0.0007 0.0008 0.0008mg/kg0.0002----Sum of PFAS
0.0020Sum of PFHxS and PFOS <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4/1763-23-
1
0.0026 <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
102 95.6 106 104 82.8%0.0002----13C4-PFOS
27 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH013_4.0_170
314
0315_BH013_3.0_170
314
0315_BH013_2.0_170
314
0315_BH013_1.0_170
314
0315_BH013_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-065ES1706394-064ES1706394-063ES1706394-062ES1706394-061UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
3.4 11.9 12.7 11.6 7.2%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4
0.0013Perfluorohexane sulfonic acid
(PFHxS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.0064Perfluorooctane sulfonic acid
(PFOS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
0.0030Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3
0.0018Perfluorohexanoic acid (PFHxA) 0.0008 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4
0.0020Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9
0.0014Perfluorooctanoic acid (PFOA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1
0.0009Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
28 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH013_4.0_170
314
0315_BH013_3.0_170
314
0315_BH013_2.0_170
314
0315_BH013_1.0_170
314
0315_BH013_0.0_170
314
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-065ES1706394-064ES1706394-063ES1706394-062ES1706394-061UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
0.00606:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
0.00188:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0246 0.0008 <0.0002 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS
0.0077Sum of PFHxS and PFOS <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4/1763-23-
1
0.0237 0.0008 <0.0002 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
95.6 119 114 118 116%0.0002----13C4-PFOS
29 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH014_4.0_170
315
0315_BH014_3.0_170
315
0315_BH014_2.0_170
315
0315_BH014_1.0_170
315
0315_BH014_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-070ES1706394-069ES1706394-068ES1706394-067ES1706394-066UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
2.0 8.4 15.7 14.8 13.6%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
0.0012Perfluorobutane sulfonic acid
(PFBS)
0.0147 0.0012 <0.0002 <0.0002mg/kg0.0002375-73-5
0.0010Perfluoropentane sulfonic acid
(PFPeS)
0.0066 0.0007 0.0002 <0.0002mg/kg0.00022706-91-4
0.0483Perfluorohexane sulfonic acid
(PFHxS)
0.0085 0.0010 0.0002 <0.0002mg/kg0.0002355-46-4
0.0102Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.116Perfluorooctane sulfonic acid
(PFOS)
0.0017 0.0006 <0.0002 <0.0002mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3
0.0029Perfluorohexanoic acid (PFHxA) 0.0083 0.0012 0.0004 <0.0002mg/kg0.0002307-24-4
0.0006Perfluoroheptanoic acid (PFHpA) 0.0005 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9
0.0048Perfluorooctanoic acid (PFOA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
30 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH014_4.0_170
315
0315_BH014_3.0_170
315
0315_BH014_2.0_170
315
0315_BH014_1.0_170
315
0315_BH014_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-070ES1706394-069ES1706394-068ES1706394-067ES1706394-066UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.185 0.0403 0.0047 0.0008 <0.0002mg/kg0.0002----Sum of PFAS
0.164Sum of PFHxS and PFOS 0.0102 0.0016 0.0002 <0.0002mg/kg0.0002355-46-4/1763-23-
1
0.174 0.0337 0.0040 0.0006 <0.0002mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
115 115 117 104 121%0.0002----13C4-PFOS
31 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH015_4.0_170
315
0315_BH015_3.0_170
315
0315_BH015_2.0_170
315
0315_BH015_1.0_170
315
0315_BH015_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-075ES1706394-074ES1706394-073ES1706394-072ES1706394-071UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
2.9 7.5 9.1 10.9 12.8%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4
<0.0002Perfluorohexane sulfonic acid
(PFHxS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.0012Perfluorooctane sulfonic acid
(PFOS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3
<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9
<0.0002Perfluorooctanoic acid (PFOA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
32 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_BH015_4.0_170
315
0315_BH015_3.0_170
315
0315_BH015_2.0_170
315
0315_BH015_1.0_170
315
0315_BH015_0.0_170
315
Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-075ES1706394-074ES1706394-073ES1706394-072ES1706394-071UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0012 <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS
0.0012Sum of PFHxS and PFOS <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002355-46-4/1763-23-
1
0.0012 <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
106 104 79.7 105 100%0.0002----13C4-PFOS
33 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_SD005_1703150315_SD004_1703160315_SD003_1703160315_SD002_1703140315_SD001_170314Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][16-Mar-2017][16-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-088ES1706394-087ES1706394-086ES1706394-085ES1706394-084UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
8.9 26.4 6.7 3.7 66.1%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4
0.0006Perfluorohexane sulfonic acid
(PFHxS)
0.0041 0.0007 0.0018 0.0005mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.0102Perfluorooctane sulfonic acid
(PFOS)
0.0539 0.0040 0.0126 0.0053mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3
<0.0002Perfluorohexanoic acid (PFHxA) 0.0010 <0.0002 <0.0002 <0.0002mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) 0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-85-9
<0.0002Perfluorooctanoic acid (PFOA) 0.0005 <0.0002 <0.0002 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
0.0010 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
34 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_SD005_1703150315_SD004_1703160315_SD003_1703160315_SD002_1703140315_SD001_170314Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][16-Mar-2017][16-Mar-2017][14-Mar-2017][14-Mar-2017]Client sampling date / time
ES1706394-088ES1706394-087ES1706394-086ES1706394-085ES1706394-084UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0108 0.0607 0.0047 0.0144 0.0058mg/kg0.0002----Sum of PFAS
0.0108Sum of PFHxS and PFOS 0.0580 0.0047 0.0144 0.0058mg/kg0.0002355-46-4/1763-23-
1
0.0108 0.0597 0.0047 0.0144 0.0058mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
99.3 91.2 85.6 123 109%0.0002----13C4-PFOS
35 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_QC102_1703150315_QC101_1703140315_QC100_1703140315_SD007_1703150315_SD006_170316Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][14-Mar-2017][14-Mar-2017][15-Mar-2017][16-Mar-2017]Client sampling date / time
ES1706394-093ES1706394-092ES1706394-091ES1706394-090ES1706394-089UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
3.9 30.2 2.8 10.1 15.7%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022706-91-4
<0.0002Perfluorohexane sulfonic acid
(PFHxS)
<0.0002 0.0014 0.0004 0.0034mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-92-8
0.0015Perfluorooctane sulfonic acid
(PFOS)
0.0009 0.0062 <0.0002 0.178mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 0.0026 <0.0002 <0.0002mg/kg0.00022706-90-3
<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 0.0017 <0.0002 0.0009mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 0.0019 <0.0002 <0.0002mg/kg0.0002375-85-9
<0.0002Perfluorooctanoic acid (PFOA) <0.0002 0.0013 <0.0002 0.0003mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 0.0009 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
36 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_QC102_1703150315_QC101_1703140315_QC100_1703140315_SD007_1703150315_SD006_170316Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][14-Mar-2017][14-Mar-2017][15-Mar-2017][16-Mar-2017]Client sampling date / time
ES1706394-093ES1706394-092ES1706394-091ES1706394-090ES1706394-089UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 0.0098 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 0.0036 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 0.0009 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0015 0.0009 0.0303 0.0004 0.183mg/kg0.0002----Sum of PFAS
0.0015Sum of PFHxS and PFOS 0.0009 0.0076 0.0004 0.181mg/kg0.0002355-46-4/1763-23-
1
0.0015 0.0009 0.0285 0.0004 0.183mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
96.3 97.5 96.7 100 98.0%0.0002----13C4-PFOS
37 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_QC107_1703150315_QC106_1703150315_QC105_1703150315_QC104_1703150315_QC103_170315Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-098ES1706394-097ES1706394-096ES1706394-095ES1706394-094UnitLORCAS NumberCompound
Result Result Result Result Result
EA055: Moisture Content
13.0 9.0 1.7 1.2 2.0%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
<0.0002 0.0002 0.0007 <0.0002mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
<0.0002 0.0003 0.0008 <0.0002mg/kg0.00022706-91-4
0.0004Perfluorohexane sulfonic acid
(PFHxS)
<0.0002 0.0047 0.0414 0.0002mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
<0.0002 0.0008 0.0067 <0.0002mg/kg0.0002375-92-8
0.0013Perfluorooctane sulfonic acid
(PFOS)
<0.0002 0.467 0.0695 0.0006mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
<0.0002 0.0014 <0.0002 <0.0002mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 <0.001mg/kg0.001375-22-4
<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 0.0008 0.0012 <0.0002mg/kg0.00022706-90-3
<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 0.0012 0.0019 <0.0002mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 0.0004 <0.0002mg/kg0.0002375-85-9
0.0005Perfluorooctanoic acid (PFOA) <0.0002 0.0007 0.0037 <0.0002mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) <0.0002 <0.0002 <0.0002 <0.0002mg/kg0.0002375-95-1
<0.0002Perfluorodecanoic acid (PFDA) <0.0002 0.0002 <0.0002 <0.0002mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
<0.0002 0.0003 <0.0002 <0.0002mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
<0.0002 0.0014 <0.0002 <0.0002mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8
38 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_QC107_1703150315_QC106_1703150315_QC105_1703150315_QC104_1703150315_QC103_170315Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
[15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017][15-Mar-2017]Client sampling date / time
ES1706394-098ES1706394-097ES1706394-096ES1706394-095ES1706394-094UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9
0.0006N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0028 <0.0002 0.479 0.126 0.0008mg/kg0.0002----Sum of PFAS
0.0017Sum of PFHxS and PFOS <0.0002 0.472 0.111 0.0008mg/kg0.0002355-46-4/1763-23-
1
0.0022 <0.0002 0.475 0.119 0.0008mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
99.5 93.5 95.7 96.9 95.5%0.0002----13C4-PFOS
39 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
----------------0315_QC108_170315Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
----------------[15-Mar-2017]Client sampling date / time
--------------------------------ES1706394-099UnitLORCAS NumberCompound
Result ---- ---- ---- ----
EA055: Moisture Content
78.0 ---- ---- ---- ----%1----Moisture Content (dried @ 103°C)
EP231A: Perfluoroalkyl Sulfonic Acids
<0.0002Perfluorobutane sulfonic acid
(PFBS)
---- ---- ---- ----mg/kg0.0002375-73-5
<0.0002Perfluoropentane sulfonic acid
(PFPeS)
---- ---- ---- ----mg/kg0.00022706-91-4
0.0006Perfluorohexane sulfonic acid
(PFHxS)
---- ---- ---- ----mg/kg0.0002355-46-4
<0.0002Perfluoroheptane sulfonic acid
(PFHpS)
---- ---- ---- ----mg/kg0.0002375-92-8
0.0025Perfluorooctane sulfonic acid
(PFOS)
---- ---- ---- ----mg/kg0.00021763-23-1
<0.0002Perfluorodecane sulfonic acid
(PFDS)
---- ---- ---- ----mg/kg0.0002335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.001Perfluorobutanoic acid (PFBA) ---- ---- ---- ----mg/kg0.001375-22-4
0.0072Perfluoropentanoic acid (PFPeA) ---- ---- ---- ----mg/kg0.00022706-90-3
<0.0002Perfluorohexanoic acid (PFHxA) ---- ---- ---- ----mg/kg0.0002307-24-4
<0.0002Perfluoroheptanoic acid (PFHpA) ---- ---- ---- ----mg/kg0.0002375-85-9
<0.0002Perfluorooctanoic acid (PFOA) ---- ---- ---- ----mg/kg0.0002335-67-1
<0.0002Perfluorononanoic acid (PFNA) ---- ---- ---- ----mg/kg0.0002375-95-1
0.0002Perfluorodecanoic acid (PFDA) ---- ---- ---- ----mg/kg0.0002335-76-2
<0.0002Perfluoroundecanoic acid
(PFUnDA)
---- ---- ---- ----mg/kg0.00022058-94-8
<0.0002Perfluorododecanoic acid
(PFDoDA)
---- ---- ---- ----mg/kg0.0002307-55-1
<0.0002Perfluorotridecanoic acid
(PFTrDA)
---- ---- ---- ----mg/kg0.000272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
---- ---- ---- ----mg/kg0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0002Perfluorooctane sulfonamide
(FOSA)
---- ---- ---- ----mg/kg0.0002754-91-6
<0.0005N-Methyl perfluorooctane
sulfonamide (MeFOSA)
---- ---- ---- ----mg/kg0.000531506-32-8
40 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
----------------0315_QC108_170315Client sample IDSub-Matrix: SOIL
(Matrix: SOIL)
----------------[15-Mar-2017]Client sampling date / time
--------------------------------ES1706394-099UnitLORCAS NumberCompound
Result ---- ---- ---- ----
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.0005N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
---- ---- ---- ----mg/kg0.00054151-50-2
<0.0005N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
---- ---- ---- ----mg/kg0.00052448-09-7
<0.0005N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
---- ---- ---- ----mg/kg0.00051691-99-2
<0.0002N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
---- ---- ---- ----mg/kg0.00022355-31-9
<0.0002N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
---- ---- ---- ----mg/kg0.00022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.00054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
---- ---- ---- ----mg/kg0.0005757124-72-4
<0.00056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
---- ---- ---- ----mg/kg0.000527619-97-2
<0.00058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
---- ---- ---- ----mg/kg0.000539108-34-4
<0.000510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
---- ---- ---- ----mg/kg0.0005120226-60-0
EP231P: PFAS Sums
0.0105 ---- ---- ---- ----mg/kg0.0002----Sum of PFAS
0.0031Sum of PFHxS and PFOS ---- ---- ---- ----mg/kg0.0002355-46-4/1763-23-
1
0.0103 ---- ---- ---- ----mg/kg0.0002----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
96.8 ---- ---- ---- ----%0.0002----13C4-PFOS
41 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_MW008_1703160315_MW007_1703160315_MW006_1703160315_MW005_1703160315_MW004_170316Client sample IDSub-Matrix: WATER
(Matrix: WATER)
16-Mar-2017 00:0016-Mar-2017 00:0016-Mar-2017 00:0016-Mar-2017 00:0016-Mar-2017 00:00Client sampling date / time
ES1706394-080ES1706394-079ES1706394-078ES1706394-077ES1706394-076UnitLORCAS NumberCompound
Result Result Result Result Result
EP231A: Perfluoroalkyl Sulfonic Acids
0.0260Perfluorobutane sulfonic acid
(PFBS)
0.0072 0.0122 <0.0005 0.0145µg/L0.0005375-73-5
0.0188Perfluoropentane sulfonic acid
(PFPeS)
0.0058 0.0057 <0.0005 0.0088µg/L0.00052706-91-4
0.190Perfluorohexane sulfonic acid
(PFHxS)
0.0418 0.0519 <0.0005 0.0855µg/L0.0005355-46-4
0.0056Perfluoroheptane sulfonic acid
(PFHpS)
0.0036 0.0028 <0.0005 0.0034µg/L0.0005375-92-8
0.0205Perfluorooctane sulfonic acid
(PFOS)
0.0144 0.0881 <0.0003 0.0252µg/L0.00031763-23-1
<0.0005Perfluorodecane sulfonic acid
(PFDS)
<0.0005 <0.0005 <0.0005 <0.0005µg/L0.0005335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.002Perfluorobutanoic acid (PFBA) <0.002 <0.002 <0.002 0.023µg/L0.002375-22-4
0.0037Perfluoropentanoic acid (PFPeA) 0.0006 0.0052 <0.0005 <0.0005µg/L0.00052706-90-3
0.0150Perfluorohexanoic acid (PFHxA) 0.0010 0.0057 <0.0005 <0.0005µg/L0.0005307-24-4
0.0057Perfluoroheptanoic acid (PFHpA) 0.0008 0.0050 <0.0005 <0.0005µg/L0.0005375-85-9
0.0174Perfluorooctanoic acid (PFOA) 0.0076 0.0185 <0.0005 <0.0005µg/L0.0005335-67-1
<0.0005Perfluorononanoic acid (PFNA) <0.0005 0.0025 <0.0005 <0.0005µg/L0.0005375-95-1
<0.0005Perfluorodecanoic acid (PFDA) <0.0005 0.0013 <0.0005 <0.0005µg/L0.0005335-76-2
<0.0005Perfluoroundecanoic acid
(PFUnDA)
<0.0005 <0.0005 <0.0005 <0.0005µg/L0.00052058-94-8
<0.0005Perfluorododecanoic acid
(PFDoDA)
<0.0005 <0.0005 <0.0005 <0.0005µg/L0.0005307-55-1
<0.0005Perfluorotridecanoic acid
(PFTrDA)
<0.0005 <0.0005 <0.0005 <0.0005µg/L0.000572629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 <0.0005µg/L0.0005376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0005Perfluorooctane sulfonamide
(FOSA)
<0.0005 <0.0005 <0.0005 <0.0005µg/L0.0005754-91-6
<0.001N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.001 <0.001 <0.001 <0.001µg/L0.00131506-32-8
<0.001N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.001 <0.001 <0.001 <0.001µg/L0.0014151-50-2
42 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_MW008_1703160315_MW007_1703160315_MW006_1703160315_MW005_1703160315_MW004_170316Client sample IDSub-Matrix: WATER
(Matrix: WATER)
16-Mar-2017 00:0016-Mar-2017 00:0016-Mar-2017 00:0016-Mar-2017 00:0016-Mar-2017 00:00Client sampling date / time
ES1706394-080ES1706394-079ES1706394-078ES1706394-077ES1706394-076UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.001N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.001 <0.001 <0.001 <0.001µg/L0.0012448-09-7
<0.001N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.001 <0.001 <0.001 <0.001µg/L0.0011691-99-2
<0.0005N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0005 <0.0005 <0.0005 <0.0005µg/L0.00052355-31-9
<0.0005N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0005 <0.0005 <0.0005 <0.0005µg/L0.00052991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.0014:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.001 <0.001 <0.001 <0.001µg/L0.001757124-72-4
0.0046:2 Fluorotelomer sulfonic acid
(6:2 FTS)
0.013 0.005 <0.001 <0.001µg/L0.00127619-97-2
<0.0018:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.001 <0.001 <0.001 <0.001µg/L0.00139108-34-4
<0.00110:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.001 <0.001 <0.001 <0.001µg/L0.001120226-60-0
EP231P: PFAS Sums
0.307 0.0958 0.204 <0.0003 0.160µg/L0.0003----Sum of PFAS
0.210Sum of PFHxS and PFOS 0.0562 0.140 <0.0003 0.111µg/L0.0003355-46-4/1763-23-
1
0.282 0.0864 0.192 <0.0003 0.148µg/L0.0003----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
104 103 104 105 107%0.0005----13C4-PFOS
43 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_QC300_1703140315_QC110_1703160315_QC109_1703150315_SW007_1703150315_SW005_170315Client sample IDSub-Matrix: WATER
(Matrix: WATER)
14-Mar-2017 00:0016-Mar-2017 00:0015-Mar-2017 00:0015-Mar-2017 00:0015-Mar-2017 00:00Client sampling date / time
ES1706394-102ES1706394-101ES1706394-100ES1706394-083ES1706394-082UnitLORCAS NumberCompound
Result Result Result Result Result
EP231A: Perfluoroalkyl Sulfonic Acids
0.0220Perfluorobutane sulfonic acid
(PFBS)
0.0185 0.0217 0.0113 ----µg/L0.0005375-73-5
----Perfluorobutane sulfonic acid
(PFBS)
---- ---- ---- <0.02µg/L0.02375-73-5
0.0051Perfluoropentane sulfonic acid
(PFPeS)
0.0051 0.0049 0.0047 ----µg/L0.00052706-91-4
----Perfluoropentane sulfonic acid
(PFPeS)
---- ---- ---- <0.02µg/L0.022706-91-4
0.0428Perfluorohexane sulfonic acid
(PFHxS)
0.0692 0.0388 0.0478 ----µg/L0.0005355-46-4
----Perfluorohexane sulfonic acid
(PFHxS)
---- ---- ---- <0.02µg/L0.02355-46-4
0.0023Perfluoroheptane sulfonic acid
(PFHpS)
0.0046 0.0017 0.0023 ----µg/L0.0005375-92-8
----Perfluoroheptane sulfonic acid
(PFHpS)
---- ---- ---- <0.02µg/L0.02375-92-8
0.0551Perfluorooctane sulfonic acid
(PFOS)
0.0956 0.0429 0.0888 ----µg/L0.00031763-23-1
<0.0005Perfluorodecane sulfonic acid
(PFDS)
<0.0005 <0.0005 <0.0005 ----µg/L0.0005335-77-3
----Perfluorooctane sulfonic acid
(PFOS)
---- ---- ---- <0.01µg/L0.011763-23-1
----Perfluorodecane sulfonic acid
(PFDS)
---- ---- ---- <0.02µg/L0.02335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.002Perfluorobutanoic acid (PFBA) <0.002 <0.002 <0.002 ----µg/L0.002375-22-4
----Perfluorobutanoic acid (PFBA) ---- ---- ---- <0.1µg/L0.1375-22-4
0.0042Perfluoropentanoic acid (PFPeA) 0.0036 0.0047 0.0048 ----µg/L0.00052706-90-3
----Perfluoropentanoic acid (PFPeA) ---- ---- ---- <0.02µg/L0.022706-90-3
0.0036Perfluorohexanoic acid (PFHxA) 0.0048 0.0039 0.0051 ----µg/L0.0005307-24-4
----Perfluorohexanoic acid (PFHxA) ---- ---- ---- <0.02µg/L0.02307-24-4
0.0023Perfluoroheptanoic acid (PFHpA) 0.0023 0.0024 0.0061 ----µg/L0.0005375-85-9
----Perfluoroheptanoic acid (PFHpA) ---- ---- ---- <0.02µg/L0.02375-85-9
0.0060Perfluorooctanoic acid (PFOA) 0.0120 0.0071 0.0230 ----µg/L0.0005335-67-1
----Perfluorooctanoic acid (PFOA) ---- ---- ---- <0.01µg/L0.01335-67-1
0.0013Perfluorononanoic acid (PFNA) 0.0022 0.0015 0.0020 ----µg/L0.0005375-95-1
44 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_QC300_1703140315_QC110_1703160315_QC109_1703150315_SW007_1703150315_SW005_170315Client sample IDSub-Matrix: WATER
(Matrix: WATER)
14-Mar-2017 00:0016-Mar-2017 00:0015-Mar-2017 00:0015-Mar-2017 00:0015-Mar-2017 00:00Client sampling date / time
ES1706394-102ES1706394-101ES1706394-100ES1706394-083ES1706394-082UnitLORCAS NumberCompound
Result Result Result Result Result
EP231B: Perfluoroalkyl Carboxylic Acids - Continued
----Perfluorononanoic acid (PFNA) ---- ---- ---- <0.02µg/L0.02375-95-1
<0.0005Perfluorodecanoic acid (PFDA) 0.0006 <0.0005 0.0013 ----µg/L0.0005335-76-2
----Perfluorodecanoic acid (PFDA) ---- ---- ---- <0.02µg/L0.02335-76-2
<0.0005Perfluoroundecanoic acid
(PFUnDA)
<0.0005 <0.0005 <0.0005 ----µg/L0.00052058-94-8
----Perfluoroundecanoic acid
(PFUnDA)
---- ---- ---- <0.02µg/L0.022058-94-8
<0.0005Perfluorododecanoic acid
(PFDoDA)
<0.0005 <0.0005 <0.0005 ----µg/L0.0005307-55-1
----Perfluorododecanoic acid
(PFDoDA)
---- ---- ---- <0.02µg/L0.02307-55-1
<0.0005Perfluorotridecanoic acid
(PFTrDA)
<0.0005 <0.0005 <0.0005 ----µg/L0.000572629-94-8
----Perfluorotridecanoic acid
(PFTrDA)
---- ---- ---- <0.02µg/L0.0272629-94-8
<0.0005Perfluorotetradecanoic acid
(PFTeDA)
<0.0005 <0.0005 <0.0005 ----µg/L0.0005376-06-7
----Perfluorotetradecanoic acid
(PFTeDA)
---- ---- ---- <0.05µg/L0.05376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.0005Perfluorooctane sulfonamide
(FOSA)
<0.0005 <0.0005 <0.0005 ----µg/L0.0005754-91-6
----Perfluorooctane sulfonamide
(FOSA)
---- ---- ---- <0.02µg/L0.02754-91-6
<0.001N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.001 <0.001 <0.001 ----µg/L0.00131506-32-8
----N-Methyl perfluorooctane
sulfonamide (MeFOSA)
---- ---- ---- <0.05µg/L0.0531506-32-8
<0.001N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.001 <0.001 <0.001 ----µg/L0.0014151-50-2
----N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
---- ---- ---- <0.05µg/L0.054151-50-2
<0.001N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.001 <0.001 <0.001 ----µg/L0.0012448-09-7
----N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
---- ---- ---- <0.05µg/L0.052448-09-7
45 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_QC300_1703140315_QC110_1703160315_QC109_1703150315_SW007_1703150315_SW005_170315Client sample IDSub-Matrix: WATER
(Matrix: WATER)
14-Mar-2017 00:0016-Mar-2017 00:0015-Mar-2017 00:0015-Mar-2017 00:0015-Mar-2017 00:00Client sampling date / time
ES1706394-102ES1706394-101ES1706394-100ES1706394-083ES1706394-082UnitLORCAS NumberCompound
Result Result Result Result Result
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.001N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.001 <0.001 <0.001 ----µg/L0.0011691-99-2
----N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
---- ---- ---- <0.05µg/L0.051691-99-2
<0.0005N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.0005 <0.0005 <0.0005 ----µg/L0.00052355-31-9
----N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
---- ---- ---- <0.02µg/L0.022355-31-9
<0.0005N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.0005 <0.0005 <0.0005 ----µg/L0.00052991-50-6
----N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
---- ---- ---- <0.02µg/L0.022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.0014:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.001 <0.001 <0.001 ----µg/L0.001757124-72-4
----4:2 Fluorotelomer sulfonic acid
(4:2 FTS)
---- ---- ---- <0.05µg/L0.05757124-72-4
<0.0016:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.001 <0.001 0.005 ----µg/L0.00127619-97-2
----6:2 Fluorotelomer sulfonic acid
(6:2 FTS)
---- ---- ---- <0.05µg/L0.0527619-97-2
<0.0018:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.001 <0.001 <0.001 ----µg/L0.00139108-34-4
----8:2 Fluorotelomer sulfonic acid
(8:2 FTS)
---- ---- ---- <0.05µg/L0.0539108-34-4
<0.00110:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.001 <0.001 <0.001 ----µg/L0.001120226-60-0
----10:2 Fluorotelomer sulfonic acid
(10:2 FTS)
---- ---- ---- <0.05µg/L0.05120226-60-0
EP231P: PFAS Sums
0.145 0.218 0.130 0.202 ----µg/L0.0003----Sum of PFAS
---- ---- ---- ---- <0.01µg/L0.01----Sum of PFAS
46 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
0315_QC300_1703140315_QC110_1703160315_QC109_1703150315_SW007_1703150315_SW005_170315Client sample IDSub-Matrix: WATER
(Matrix: WATER)
14-Mar-2017 00:0016-Mar-2017 00:0015-Mar-2017 00:0015-Mar-2017 00:0015-Mar-2017 00:00Client sampling date / time
ES1706394-102ES1706394-101ES1706394-100ES1706394-083ES1706394-082UnitLORCAS NumberCompound
Result Result Result Result Result
EP231P: PFAS Sums - Continued
0.0979Sum of PFHxS and PFOS 0.165 0.0817 0.137 ----µg/L0.0003355-46-4/1763-23-
1
----Sum of PFHxS and PFOS ---- ---- ---- <0.01µg/L0.01355-46-4/1763-23-
1
0.136 0.206 0.122 0.192 ----µg/L0.0003----Sum of PFAS (WA DER List)
---- ---- ---- ---- <0.01µg/L0.01----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
105 99.8 104 106 ----%0.0005----13C4-PFOS
---- ---- ---- ---- 110%0.02----13C4-PFOS
47 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
------------0315_QC302_1703160315_QC301_170315Client sample IDSub-Matrix: WATER
(Matrix: WATER)
------------16-Mar-2017 00:0015-Mar-2017 00:00Client sampling date / time
------------------------ES1706394-104ES1706394-103UnitLORCAS NumberCompound
Result Result ---- ---- ----
EP231A: Perfluoroalkyl Sulfonic Acids
<0.02Perfluorobutane sulfonic acid
(PFBS)
<0.02 ---- ---- ----µg/L0.02375-73-5
<0.02Perfluoropentane sulfonic acid
(PFPeS)
<0.02 ---- ---- ----µg/L0.022706-91-4
<0.02Perfluorohexane sulfonic acid
(PFHxS)
<0.02 ---- ---- ----µg/L0.02355-46-4
<0.02Perfluoroheptane sulfonic acid
(PFHpS)
<0.02 ---- ---- ----µg/L0.02375-92-8
<0.01Perfluorooctane sulfonic acid
(PFOS)
<0.01 ---- ---- ----µg/L0.011763-23-1
<0.02Perfluorodecane sulfonic acid
(PFDS)
<0.02 ---- ---- ----µg/L0.02335-77-3
EP231B: Perfluoroalkyl Carboxylic Acids
<0.1Perfluorobutanoic acid (PFBA) <0.1 ---- ---- ----µg/L0.1375-22-4
<0.02Perfluoropentanoic acid (PFPeA) <0.02 ---- ---- ----µg/L0.022706-90-3
<0.02Perfluorohexanoic acid (PFHxA) <0.02 ---- ---- ----µg/L0.02307-24-4
<0.02Perfluoroheptanoic acid (PFHpA) <0.02 ---- ---- ----µg/L0.02375-85-9
<0.01Perfluorooctanoic acid (PFOA) <0.01 ---- ---- ----µg/L0.01335-67-1
<0.02Perfluorononanoic acid (PFNA) <0.02 ---- ---- ----µg/L0.02375-95-1
<0.02Perfluorodecanoic acid (PFDA) <0.02 ---- ---- ----µg/L0.02335-76-2
<0.02Perfluoroundecanoic acid
(PFUnDA)
<0.02 ---- ---- ----µg/L0.022058-94-8
<0.02Perfluorododecanoic acid
(PFDoDA)
<0.02 ---- ---- ----µg/L0.02307-55-1
<0.02Perfluorotridecanoic acid
(PFTrDA)
<0.02 ---- ---- ----µg/L0.0272629-94-8
<0.05Perfluorotetradecanoic acid
(PFTeDA)
<0.05 ---- ---- ----µg/L0.05376-06-7
EP231C: Perfluoroalkyl Sulfonamides
<0.02Perfluorooctane sulfonamide
(FOSA)
<0.02 ---- ---- ----µg/L0.02754-91-6
<0.05N-Methyl perfluorooctane
sulfonamide (MeFOSA)
<0.05 ---- ---- ----µg/L0.0531506-32-8
<0.05N-Ethyl perfluorooctane
sulfonamide (EtFOSA)
<0.05 ---- ---- ----µg/L0.054151-50-2
48 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Analytical Results
------------0315_QC302_1703160315_QC301_170315Client sample IDSub-Matrix: WATER
(Matrix: WATER)
------------16-Mar-2017 00:0015-Mar-2017 00:00Client sampling date / time
------------------------ES1706394-104ES1706394-103UnitLORCAS NumberCompound
Result Result ---- ---- ----
EP231C: Perfluoroalkyl Sulfonamides - Continued
<0.05N-Methyl perfluorooctane
sulfonamidoethanol (MeFOSE)
<0.05 ---- ---- ----µg/L0.052448-09-7
<0.05N-Ethyl perfluorooctane
sulfonamidoethanol (EtFOSE)
<0.05 ---- ---- ----µg/L0.051691-99-2
<0.02N-Methyl perfluorooctane
sulfonamidoacetic acid
(MeFOSAA)
<0.02 ---- ---- ----µg/L0.022355-31-9
<0.02N-Ethyl perfluorooctane
sulfonamidoacetic acid
(EtFOSAA)
<0.02 ---- ---- ----µg/L0.022991-50-6
EP231D: (n:2) Fluorotelomer Sulfonic Acids
<0.054:2 Fluorotelomer sulfonic acid
(4:2 FTS)
<0.05 ---- ---- ----µg/L0.05757124-72-4
<0.056:2 Fluorotelomer sulfonic acid
(6:2 FTS)
<0.05 ---- ---- ----µg/L0.0527619-97-2
<0.058:2 Fluorotelomer sulfonic acid
(8:2 FTS)
<0.05 ---- ---- ----µg/L0.0539108-34-4
<0.0510:2 Fluorotelomer sulfonic acid
(10:2 FTS)
<0.05 ---- ---- ----µg/L0.05120226-60-0
EP231P: PFAS Sums
<0.01 <0.01 ---- ---- ----µg/L0.01----Sum of PFAS
<0.01Sum of PFHxS and PFOS <0.01 ---- ---- ----µg/L0.01355-46-4/1763-23-
1
<0.01 <0.01 ---- ---- ----µg/L0.01----Sum of PFAS (WA DER List)
EP231S: PFAS Surrogate
111 106 ---- ---- ----%0.02----13C4-PFOS
49 of 49:Page
Work Order :
:Client
ES1706394 Amendment 2
1652034:Project
GOLDER ASSOCIATES
Surrogate Control Limits
Recovery Limits (%)Sub-Matrix: SOIL
Compound CAS Number Low High
EP231S: PFAS Surrogate
13C4-PFOS ---- 70 130
Recovery Limits (%)Sub-Matrix: WATER
Compound CAS Number Low High
EP231S: PFAS Surrogate
13C4-PFOS ---- 70 120
Environmental
SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES1706394
:: LaboratoryClient Environmental Division SydneyGOLDER ASSOCIATES
: :ContactContact MS OLGA BUKHTEEVA Customer Services ES
:: AddressAddress LEVEL 1, 124 PACIFIC HIGHWAY
ST LEONARDS NSW, AUSTRALIA
2065
277-289 Woodpark Road Smithfield
NSW Australia 2164
:: E-mailE-mail [email protected] [email protected]
:: TelephoneTelephone +61 02 9478 3900 +61-2-8784 8555
:: FacsimileFacsimile +61 02 9478 3901 +61-2-8784 8500
::Project 1652034 Page 1 of 6
:Order number PO01472 :Quote number EB2016GOLASS0004 (BN/404/16)
:C-O-C number ---- :QC Level NEPM 2013 B3 & ALS QC Standard
Site : Kapooka
Sampler : OLGA BUKHTEEVA
DatesDate Samples Received : Issue Date : 20-Mar-201717-Mar-2017 12:00
Scheduled Reporting Date: 24-Mar-2017:Client Requested Due
Date
24-Mar-2017
Delivery DetailsMode of Delivery : :Undefined Intact.Security Seal
No. of coolers/boxes : :6 Temperature 5.7'c - Ice present
: : 110 / 108Receipt Detail No. of samples received / analysed
General Comments
This report contains the following information:l
- Sample Container(s)/Preservation Non-Compliances
- Summary of Sample(s) and Requested Analysis
- Proactive Holding Time Report
- Requested Deliverables
l This is an updated SRA which indicates added analysis for this work order.
l Samples QC201, QC203, QC205, QC207, QC209, QC210 will be sent to Eurofins as per coc requestl Please refer to the Proactive Holding Time Report table below which summarises breaches of
recommended holding times that have occurred prior to samples/instructions being received at
the laboratory. The absence of this summary table indicates that all samples have been received
within the recommended holding times for the analysis requested.l Please direct any queries you have regarding this work order to the above ALS laboratory contact.
l Analytical work for this work order will be conducted at ALS Sydney.
l Sample Disposal - Aqueous (14 days), Solid (60 days) from date of completion of work order.
R I G H T S O L U T I O N S | R I G H T P A R T N E R
:Client GOLDER ASSOCIATES
Work Order : ES1706394 Amendment 02 of 6:Page
20-Mar-2017:Issue Date
Sample Container(s)/Preservation Non-Compliances
All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.
l No sample container / preservation non-compliance exists.
Any sample identifications that cannot be displayed entirely in the analysis summary table will be listed below.
ES1706394-001 : [ 15-Mar-2017 ] : 0315_BH001_0.0_170315
ES1706394-002 : [ 15-Mar-2017 ] : 0315_BH001_1.0_170315
ES1706394-003 : [ 15-Mar-2017 ] : 0315_BH001_2.0_170315
ES1706394-004 : [ 15-Mar-2017 ] : 0315_BH001_3.0_170315
ES1706394-005 : [ 15-Mar-2017 ] : 0315_BH001_4.0_170315
ES1706394-006 : [ 15-Mar-2017 ] : 0315_BH002_0.0_170315
ES1706394-007 : [ 15-Mar-2017 ] : 0315_BH002_1.0_170315
ES1706394-008 : [ 15-Mar-2017 ] : 0315_BH002_2.0_170315
ES1706394-009 : [ 15-Mar-2017 ] : 0315_BH002_3.0_170315
ES1706394-010 : [ 15-Mar-2017 ] : 0315_BH002_4.0_170315
ES1706394-011 : [ 14-Mar-2017 ] : 0315_BH003_0.0_170314
ES1706394-012 : [ 14-Mar-2017 ] : 0315_BH003_1.0_170314
ES1706394-013 : [ 14-Mar-2017 ] : 0315_BH003_2.0_170314
ES1706394-014 : [ 14-Mar-2017 ] : 0315_BH003_3.0_170314
ES1706394-015 : [ 14-Mar-2017 ] : 0315_BH003_4.0_170314
ES1706394-016 : [ 14-Mar-2017 ] : 0315_BH004_0.0_170314
ES1706394-017 : [ 14-Mar-2017 ] : 0315_BH004_1.0_170314
ES1706394-018 : [ 14-Mar-2017 ] : 0315_BH004_2.0_170314
ES1706394-019 : [ 14-Mar-2017 ] : 0315_BH004_3.0_170314
ES1706394-020 : [ 14-Mar-2017 ] : 0315_BH004_4.0_170314
ES1706394-021 : [ 14-Mar-2017 ] : 0315_BH005_0.0_170314
ES1706394-022 : [ 14-Mar-2017 ] : 0315_BH005_1.0_170314
ES1706394-023 : [ 14-Mar-2017 ] : 0315_BH005_2.0_170314
ES1706394-024 : [ 14-Mar-2017 ] : 0315_BH005_3.0_170314
ES1706394-025 : [ 14-Mar-2017 ] : 0315_BH005_4.0_170314
ES1706394-026 : [ 14-Mar-2017 ] : 0315_BH006_0.0_170314
ES1706394-027 : [ 14-Mar-2017 ] : 0315_BH006_1.0_170314
ES1706394-028 : [ 14-Mar-2017 ] : 0315_BH006_2.0_170314
ES1706394-029 : [ 14-Mar-2017 ] : 0315_BH006_3.0_170314
ES1706394-030 : [ 14-Mar-2017 ] : 0315_BH006_4.0_170314
ES1706394-031 : [ 15-Mar-2017 ] : 0315_BH007_0.0_170315
ES1706394-032 : [ 15-Mar-2017 ] : 0315_BH007_1.0_170315
ES1706394-033 : [ 15-Mar-2017 ] : 0315_BH007_2.0_170315
ES1706394-034 : [ 15-Mar-2017 ] : 0315_BH007_3.0_170315
ES1706394-035 : [ 15-Mar-2017 ] : 0315_BH007_4.0_170315
ES1706394-036 : [ 15-Mar-2017 ] : 0315_BH008_0.0_170315
ES1706394-037 : [ 15-Mar-2017 ] : 0315_BH008_1.0_170315
ES1706394-038 : [ 15-Mar-2017 ] : 0315_BH008_2.0_170315
ES1706394-039 : [ 15-Mar-2017 ] : 0315_BH008_3.0_170315
ES1706394-040 : [ 15-Mar-2017 ] : 0315_BH008_4.0_170315
ES1706394-041 : [ 15-Mar-2017 ] : 0315_BH009_0.0_170315
ES1706394-042 : [ 15-Mar-2017 ] : 0315_BH009_1.0_170315
ES1706394-043 : [ 15-Mar-2017 ] : 0315_BH009_2.0_170315
ES1706394-044 : [ 15-Mar-2017 ] : 0315_BH009_3.0_170315
ES1706394-045 : [ 15-Mar-2017 ] : 0315_BH009_4.0_170315
ES1706394-046 : [ 15-Mar-2017 ] : 0315_BH010_0.0_170315
ES1706394-047 : [ 15-Mar-2017 ] : 0315_BH010_1.0_170315
ES1706394-048 : [ 15-Mar-2017 ] : 0315_BH010_2.0_170315
ES1706394-049 : [ 15-Mar-2017 ] : 0315_BH010_3.0_170315
ES1706394-050 : [ 15-Mar-2017 ] : 0315_BH010_4.0_170315
ES1706394-051 : [ 14-Mar-2017 ] : 0315_BH011_0.0_170314
ES1706394-052 : [ 14-Mar-2017 ] : 0315_BH011_1.0_170314
ES1706394-053 : [ 14-Mar-2017 ] : 0315_BH011_2.0_170314
ES1706394-054 : [ 14-Mar-2017 ] : 0315_BH011_3.0_170314
ES1706394-055 : [ 14-Mar-2017 ] : 0315_BH011_4.0_170314
:Client GOLDER ASSOCIATES
Work Order : ES1706394 Amendment 03 of 6:Page
20-Mar-2017:Issue Date
ES1706394-056 : [ 14-Mar-2017 ] : 0315_BH012_0.0_170314
ES1706394-057 : [ 14-Mar-2017 ] : 0315_BH012_1.0_170314
ES1706394-058 : [ 14-Mar-2017 ] : 0315_BH012_2.0_170314
ES1706394-059 : [ 14-Mar-2017 ] : 0315_BH012_3.0_170314
ES1706394-060 : [ 14-Mar-2017 ] : 0315_BH012_4.0_170314
ES1706394-061 : [ 14-Mar-2017 ] : 0315_BH013_0.0_170314
ES1706394-062 : [ 14-Mar-2017 ] : 0315_BH013_1.0_170314
ES1706394-063 : [ 14-Mar-2017 ] : 0315_BH013_2.0_170314
ES1706394-064 : [ 14-Mar-2017 ] : 0315_BH013_3.0_170314
ES1706394-065 : [ 14-Mar-2017 ] : 0315_BH013_4.0_170314
ES1706394-066 : [ 15-Mar-2017 ] : 0315_BH014_0.0_170315
ES1706394-067 : [ 15-Mar-2017 ] : 0315_BH014_1.0_170315
ES1706394-068 : [ 15-Mar-2017 ] : 0315_BH014_2.0_170315
ES1706394-069 : [ 15-Mar-2017 ] : 0315_BH014_3.0_170315
ES1706394-070 : [ 15-Mar-2017 ] : 0315_BH014_4.0_170315
ES1706394-071 : [ 15-Mar-2017 ] : 0315_BH015_0.0_170315
ES1706394-072 : [ 15-Mar-2017 ] : 0315_BH015_1.0_170315
ES1706394-073 : [ 15-Mar-2017 ] : 0315_BH015_2.0_170315
ES1706394-074 : [ 15-Mar-2017 ] : 0315_BH015_3.0_170315
ES1706394-075 : [ 15-Mar-2017 ] : 0315_BH015_4.0_170315
Summary of Sample(s) and Requested Analysis
Some items described below may be part of a laboratory
process necessary for the execution of client requested
tasks. Packages may contain additional analyses, such
as the determination of moisture content and preparation
tasks, that are included in the package.
If no sampling time is provided, the sampling time will
default 00:00 on the date of sampling. If no sampling date
is provided, the sampling date will be assumed by the
laboratory and displayed in brackets without a time
component
SO
IL -
EA
05
5-1
03
Mo
istu
re C
on
ten
t
SO
IL -
EP
23
1X
(so
lids)
PF
AS
- F
ull
Su
ite (
28
an
aly
tes)
SO
IL -
S-1
8 (
NO
MO
IST
)
TR
H(C
6-C
9)/
BT
EX
N w
ith N
o M
ois
ture
fo
r T
Bs
ES1706394-001 [ 15-Mar-2017 ] 0315_BH001_0.0_170315 ü ü
ES1706394-002 [ 15-Mar-2017 ] 0315_BH001_1.0_170315 ü ü
ES1706394-003 [ 15-Mar-2017 ] 0315_BH001_2.0_170315 ü ü
ES1706394-004 [ 15-Mar-2017 ] 0315_BH001_3.0_170315 ü ü
ES1706394-005 [ 15-Mar-2017 ] 0315_BH001_4.0_170315 ü ü
ES1706394-006 [ 15-Mar-2017 ] 0315_BH002_0.0_170315 ü ü
ES1706394-007 [ 15-Mar-2017 ] 0315_BH002_1.0_170315 ü ü
ES1706394-008 [ 15-Mar-2017 ] 0315_BH002_2.0_170315 ü ü
ES1706394-009 [ 15-Mar-2017 ] 0315_BH002_3.0_170315 ü ü
ES1706394-010 [ 15-Mar-2017 ] 0315_BH002_4.0_170315 ü ü
ES1706394-011 [ 14-Mar-2017 ] 0315_BH003_0.0_170314 ü ü
ES1706394-012 [ 14-Mar-2017 ] 0315_BH003_1.0_170314 ü ü
ES1706394-013 [ 14-Mar-2017 ] 0315_BH003_2.0_170314 ü ü
ES1706394-014 [ 14-Mar-2017 ] 0315_BH003_3.0_170314 ü ü
ES1706394-015 [ 14-Mar-2017 ] 0315_BH003_4.0_170314 ü ü
ES1706394-016 [ 14-Mar-2017 ] 0315_BH004_0.0_170314 ü ü
ES1706394-017 [ 14-Mar-2017 ] 0315_BH004_1.0_170314 ü ü
ES1706394-018 [ 14-Mar-2017 ] 0315_BH004_2.0_170314 ü ü
ES1706394-019 [ 14-Mar-2017 ] 0315_BH004_3.0_170314 ü ü
ES1706394-020 [ 14-Mar-2017 ] 0315_BH004_4.0_170314 ü ü
ES1706394-021 [ 14-Mar-2017 ] 0315_BH005_0.0_170314 ü ü
ES1706394-022 [ 14-Mar-2017 ] 0315_BH005_1.0_170314 ü ü
Matrix: SOIL
Client sample IDLaboratory sample
ID
Client sampling
date / time
:Client GOLDER ASSOCIATES
Work Order : ES1706394 Amendment 04 of 6:Page
20-Mar-2017:Issue Date
SO
IL -
EA
055-1
03
Mois
ture
Conte
nt
SO
IL -
EP
231X
(so
lids)
PF
AS
- F
ull
Suite
(28 a
naly
tes)
SO
IL -
S-1
8 (
NO
MO
IST
)
TR
H(C
6-C
9)/
BT
EX
N w
ith N
o M
ois
ture
for
TB
s
ES1706394-023 [ 14-Mar-2017 ] 0315_BH005_2.0_170314 ü ü
ES1706394-024 [ 14-Mar-2017 ] 0315_BH005_3.0_170314 ü ü
ES1706394-025 [ 14-Mar-2017 ] 0315_BH005_4.0_170314 ü ü
ES1706394-026 [ 14-Mar-2017 ] 0315_BH006_0.0_170314 ü ü
ES1706394-027 [ 14-Mar-2017 ] 0315_BH006_1.0_170314 ü ü
ES1706394-028 [ 14-Mar-2017 ] 0315_BH006_2.0_170314 ü ü
ES1706394-029 [ 14-Mar-2017 ] 0315_BH006_3.0_170314 ü ü
ES1706394-030 [ 14-Mar-2017 ] 0315_BH006_4.0_170314 ü ü
ES1706394-031 [ 15-Mar-2017 ] 0315_BH007_0.0_170315 ü ü
ES1706394-032 [ 15-Mar-2017 ] 0315_BH007_1.0_170315 ü ü
ES1706394-033 [ 15-Mar-2017 ] 0315_BH007_2.0_170315 ü ü
ES1706394-034 [ 15-Mar-2017 ] 0315_BH007_3.0_170315 ü ü
ES1706394-035 [ 15-Mar-2017 ] 0315_BH007_4.0_170315 ü ü
ES1706394-036 [ 15-Mar-2017 ] 0315_BH008_0.0_170315 ü ü
ES1706394-037 [ 15-Mar-2017 ] 0315_BH008_1.0_170315 ü ü
ES1706394-038 [ 15-Mar-2017 ] 0315_BH008_2.0_170315 ü ü
ES1706394-039 [ 15-Mar-2017 ] 0315_BH008_3.0_170315 ü ü
ES1706394-040 [ 15-Mar-2017 ] 0315_BH008_4.0_170315 ü ü
ES1706394-041 [ 15-Mar-2017 ] 0315_BH009_0.0_170315 ü ü
ES1706394-042 [ 15-Mar-2017 ] 0315_BH009_1.0_170315 ü ü
ES1706394-043 [ 15-Mar-2017 ] 0315_BH009_2.0_170315 ü ü
ES1706394-044 [ 15-Mar-2017 ] 0315_BH009_3.0_170315 ü ü
ES1706394-045 [ 15-Mar-2017 ] 0315_BH009_4.0_170315 ü ü
ES1706394-046 [ 15-Mar-2017 ] 0315_BH010_0.0_170315 ü ü
ES1706394-047 [ 15-Mar-2017 ] 0315_BH010_1.0_170315 ü ü
ES1706394-048 [ 15-Mar-2017 ] 0315_BH010_2.0_170315 ü ü
ES1706394-049 [ 15-Mar-2017 ] 0315_BH010_3.0_170315 ü ü
ES1706394-050 [ 15-Mar-2017 ] 0315_BH010_4.0_170315 ü ü
ES1706394-051 [ 14-Mar-2017 ] 0315_BH011_0.0_170314 ü ü
ES1706394-052 [ 14-Mar-2017 ] 0315_BH011_1.0_170314 ü ü
ES1706394-053 [ 14-Mar-2017 ] 0315_BH011_2.0_170314 ü ü
ES1706394-054 [ 14-Mar-2017 ] 0315_BH011_3.0_170314 ü ü
ES1706394-055 [ 14-Mar-2017 ] 0315_BH011_4.0_170314 ü ü
ES1706394-056 [ 14-Mar-2017 ] 0315_BH012_0.0_170314 ü ü
ES1706394-057 [ 14-Mar-2017 ] 0315_BH012_1.0_170314 ü ü
ES1706394-058 [ 14-Mar-2017 ] 0315_BH012_2.0_170314 ü ü
ES1706394-059 [ 14-Mar-2017 ] 0315_BH012_3.0_170314 ü ü
ES1706394-060 [ 14-Mar-2017 ] 0315_BH012_4.0_170314 ü ü
ES1706394-061 [ 14-Mar-2017 ] 0315_BH013_0.0_170314 ü ü
ES1706394-062 [ 14-Mar-2017 ] 0315_BH013_1.0_170314 ü ü
ES1706394-063 [ 14-Mar-2017 ] 0315_BH013_2.0_170314 ü ü
:Client GOLDER ASSOCIATES
Work Order : ES1706394 Amendment 05 of 6:Page
20-Mar-2017:Issue Date
SO
IL -
EA
055-1
03
Mois
ture
Conte
nt
SO
IL -
EP
231X
(so
lids)
PF
AS
- F
ull
Suite
(28 a
naly
tes)
SO
IL -
S-1
8 (
NO
MO
IST
)
TR
H(C
6-C
9)/
BT
EX
N w
ith N
o M
ois
ture
for
TB
s
ES1706394-064 [ 14-Mar-2017 ] 0315_BH013_3.0_170314 ü ü
ES1706394-065 [ 14-Mar-2017 ] 0315_BH013_4.0_170314 ü ü
ES1706394-066 [ 15-Mar-2017 ] 0315_BH014_0.0_170315 ü ü
ES1706394-067 [ 15-Mar-2017 ] 0315_BH014_1.0_170315 ü ü
ES1706394-068 [ 15-Mar-2017 ] 0315_BH014_2.0_170315 ü ü
ES1706394-069 [ 15-Mar-2017 ] 0315_BH014_3.0_170315 ü ü
ES1706394-070 [ 15-Mar-2017 ] 0315_BH014_4.0_170315 ü ü
ES1706394-071 [ 15-Mar-2017 ] 0315_BH015_0.0_170315 ü ü
ES1706394-072 [ 15-Mar-2017 ] 0315_BH015_1.0_170315 ü ü
ES1706394-073 [ 15-Mar-2017 ] 0315_BH015_2.0_170315 ü ü
ES1706394-074 [ 15-Mar-2017 ] 0315_BH015_3.0_170315 ü ü
ES1706394-075 [ 15-Mar-2017 ] 0315_BH015_4.0_170315 ü ü
ES1706394-084 [ 14-Mar-2017 ] 0315_SD001_170314 ü ü
ES1706394-085 [ 14-Mar-2017 ] 0315_SD002_170314 ü ü
ES1706394-086 [ 16-Mar-2017 ] 0315_SD003_170316 ü ü
ES1706394-087 [ 16-Mar-2017 ] 0315_SD004_170316 ü ü
ES1706394-088 [ 15-Mar-2017 ] 0315_SD005_170315 ü ü
ES1706394-089 [ 16-Mar-2017 ] 0315_SD006_170316 ü ü
ES1706394-090 [ 15-Mar-2017 ] 0315_SD007_170315 ü ü
ES1706394-091 [ 14-Mar-2017 ] 0315_QC100_170314 ü ü
ES1706394-092 [ 14-Mar-2017 ] 0315_QC101_170314 ü ü
ES1706394-093 [ 15-Mar-2017 ] 0315_QC102_170315 ü ü
ES1706394-094 [ 15-Mar-2017 ] 0315_QC103_170315 ü ü
ES1706394-095 [ 15-Mar-2017 ] 0315_QC104_170315 ü ü
ES1706394-096 [ 15-Mar-2017 ] 0315_QC105_170315 ü ü
ES1706394-097 [ 15-Mar-2017 ] 0315_QC106_170315 ü ü
ES1706394-098 [ 15-Mar-2017 ] 0315_QC107_170315 ü ü
ES1706394-099 [ 15-Mar-2017 ] 0315_QC108_170315 ü ü
ES1706394-106 14-Mar-2017 00:00 0315_QC502_170314 ü
ES1706394-108 15-Mar-2017 00:00 0315_QC504_170315 ü
ES1706394-110 16-Mar-2017 00:00 0315_QC506_170316 ü
:Client GOLDER ASSOCIATES
Work Order : ES1706394 Amendment 06 of 6:Page
20-Mar-2017:Issue Date
(On H
old
) W
AT
ER
No a
naly
sis
request
ed
WA
TE
R -
EP
231X
PF
AS
- F
ull
Suite
(28 a
naly
tes)
WA
TE
R -
EP
231X
-ST
PF
AS
- F
ull
Suite
Drinki
ng W
ate
r (2
8 a
naly
tes)
WA
TE
R -
W-1
8
TR
H(C
6 -
C9)/
BT
EX
N
ES1706394-076 16-Mar-2017 00:00 0315_MW004_170316 ü
ES1706394-077 16-Mar-2017 00:00 0315_MW005_170316 ü
ES1706394-078 16-Mar-2017 00:00 0315_MW006_170316 ü
ES1706394-079 16-Mar-2017 00:00 0315_MW007_170316 ü
ES1706394-080 16-Mar-2017 00:00 0315_MW008_170316 ü
ES1706394-081 16-Mar-2017 00:00 0315_MW009_170316 ü
ES1706394-082 15-Mar-2017 00:00 0315_SW005_170315 ü
ES1706394-083 15-Mar-2017 00:00 0315_SW007_170315 ü
ES1706394-100 15-Mar-2017 00:00 0315_QC109_170315 ü
ES1706394-101 16-Mar-2017 00:00 0315_QC110_170316 ü
ES1706394-102 14-Mar-2017 00:00 0315_QC300_170314 ü
ES1706394-103 15-Mar-2017 00:00 0315_QC301_170315 ü
ES1706394-104 16-Mar-2017 00:00 0315_QC302_170316 ü
ES1706394-105 14-Mar-2017 00:00 0315_QC501_170314 ü
ES1706394-107 15-Mar-2017 00:00 0315_QC503_170315 ü
ES1706394-109 16-Mar-2017 00:00 0315_QC505_170316 ü
Matrix: WATER
Client sample IDLaboratory sample
ID
Client sampling
date / time
Proactive Holding Time Report
Sample(s) have been received within the recommended holding times for the requested analysis.
Requested Deliverables
ACCOUNTS PAYABLE
- A4 - AU Tax Invoice (INV) Email [email protected]
u
OLGA BUKHTEEVA
- *AU Certificate of Analysis - NATA (COA) Email [email protected]
- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]
- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]
- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]
- Chain of Custody (CoC) (COC) Email [email protected]
- EDI Format - ENMRG (ENMRG) Email [email protected]
- EDI Format - XTab (XTAB) Email [email protected]
Certificate of Analysis
Golder Associates
124 Pacific Hwy
St. Leonards
NSW 1585
Attention: Andrew Holloway
Report 538644-W
Project name KAPOOKA
Project ID 1652034
Received Date Mar 20, 2017
Client Sample ID 0315_QC209_170315
0315_QC210_170316
Sample Matrix Water Water
Eurofins | mgt Sample No. S17-Ma21088 S17-Ma21089
Date Sampled Mar 15, 2017 Mar 16, 2017
Test/Reference LOR Unit
Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level
Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L < 0.01 0.01
Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 < 0.05
Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N090.09 N090.08
Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.07 N090.11
Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 < 0.01
Perfluoropentanoic acid (PFPeA) 0.01 ug/L 0.04 0.02
Perfluorohexanoic acid (PFHxA) 0.01 ug/L < 0.01 0.03
Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 N090.02
Perfluorooctanoic acid (PFOA) 0.01 ug/L < 0.01 N090.05
Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01 < 0.01
Perfluorodecanoic acid (PFDA) 0.01 ug/L < 0.01 < 0.01
Perfluoroundecanoic acid (PFUnA) 0.01 ug/L < 0.01 < 0.01
Perfluorododecanoic acid (PFDoA) 0.01 ug/L < 0.01 < 0.01
Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01 < 0.01
Perfluorotetradecanoic acid (PFTeDA) 0.01 ug/L < 0.01 < 0.01
Perfluorooctane sulfonamide (FOSA) 0.05 ug/L < 0.05 < 0.05
N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 0.05 ug/L < 0.05 < 0.05
N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 0.05 ug/L < 0.05 < 0.05
1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 0.01 ug/L < 0.01 < 0.01
1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05 < 0.05
1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L < 0.01 < 0.01
13C5-PFHxA (surr.) 1 % 86 109
13C8-PFOS (surr.) 1 % 70 84
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 1 of 9
Report Number: 538644-W
NATA AccreditedAccreditation Number 1261Site Number 18217
Accredited for compliance with ISO/IEC 17025 – TestingThe results of the tests, calibrations and/ormeasurements included in this document are traceableto Australian/national standards.
Sample HistoryWhere samples are submitted/analysed over several days, the last date of extraction and analysis is reported.A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this, some of the method reference information on reports has changed. However,no substantive change has been made to our laboratory methods, and as such there is no change in the validity of current or previous results (regarding both quality and NATA accreditation).
If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised results should testing be performed outside the recommended holding time.
Description Testing Site Extracted Holding Time
Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level Brisbane Mar 23, 2017 14 Days
- Method: LTM-ORG-2100 Per- and Polyfluorinated Alkyl Substances by LC-MS/MS
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 2 of 9
Report Number: 538644-W
.Company Name: Golder Associates Pty Ltd (Syd) Order No.: Received: Mar 20, 2017 11:06 AMAddress: 124 Pacific Hwy Report #: 538644 Due: Mar 27, 2017
St. Leonards Phone: 02 9478 3900 Priority: 5 DayNSW 1585 Fax: 02 9478 3901 Contact Name: Andrew Holloway
Project Name: KAPOOKAProject ID: 1652034
Eurofins | mgt Analytical Services Manager : Nibha Vaidya
Sample Detail
Moisture S
et
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss) - T
race Level
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss)
Melbourne Laboratory - NATA Site # 1254 & 14271
Sydney Laboratory - NATA Site # 18217
Brisbane Laboratory - NATA Site # 20794 X X X
Perth Laboratory - NATA Site # 18217
External Laboratory
No Sample ID Sample Date SamplingTime
Matrix LAB ID
1 0315_QC201_170314
Mar 14, 2017 Soil S17-Ma21084 X X
2 0315_QC203_170315
Mar 15, 2017 Soil S17-Ma21085 X X
3 0315_QC205_170315
Mar 15, 2017 Soil S17-Ma21086 X X
4 0315_QC207_170315
Mar 15, 2017 Soil S17-Ma21087 X X
5 0315_QC209_170315
Mar 15, 2017 Water S17-Ma21088 X
6 0315_QC210_ Mar 16, 2017 Water S17-Ma21089 X
ABN– 50 005 085 521e.mail : [email protected] : www.eurofins.com.au
MelbourneMelbourneMelbourneMelbourne2-5 Kingston Town CloseOakleigh VIC 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271
SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217
BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794
PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261Site # 18217
Date Reported:Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 3 of 9
Report Number: 538644-W
Company Name: Golder Associates Pty Ltd (Syd) Order No.: Received: Mar 20, 2017 11:06 AMAddress: 124 Pacific Hwy Report #: 538644 Due: Mar 27, 2017
St. Leonards Phone: 02 9478 3900 Priority: 5 DayNSW 1585 Fax: 02 9478 3901 Contact Name: Andrew Holloway
Project Name: KAPOOKAProject ID: 1652034
Eurofins | mgt Analytical Services Manager : Nibha Vaidya
Sample Detail
Moisture S
et
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss) - T
race Level
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss)
Melbourne Laboratory - NATA Site # 1254 & 14271
Sydney Laboratory - NATA Site # 18217
Brisbane Laboratory - NATA Site # 20794 X X X
Perth Laboratory - NATA Site # 18217
170316
Test Counts 4 2 4
ABN– 50 005 085 521e.mail : [email protected] : www.eurofins.com.au
MelbourneMelbourneMelbourneMelbourne2-5 Kingston Town CloseOakleigh VIC 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271
SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217
BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794
PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261Site # 18217
Page 4 of 9
Report Number: 538644-W
Internal Quality Control Review and Glossary
General
Holding Times
Units
Terms
QC - Acceptance Criteria
QC Data General Comments
1. Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on
request.
2. All soil results are reported on a dry basis, unless otherwise stated.
3. Actual LORs are matrix dependant. Quoted LORs may be raised where sample extracts are diluted due to interferences.
4. Results are uncorrected for matrix spikes or surrogate recoveries.
5. SVOC analysis on waters are performed on homogenised, unfiltered samples, unless noted otherwise.
6. Samples were analysed on an 'as received' basis. 7. This report replaces any interim results previously issued.
Please refer to 'Sample Preservation and Container Guide' for holding times (QS3001).
For samples received on the last day of holding time, notification of testing requirements should have been received at least 6 hours prior to sample receipt deadlines as stated on the Sample
Receipt Advice.
If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues, suitably qualified results may still be reported.
Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control.
**NOTE: pH duplicates are reported as a range NOT as RPD
mg/kg: milligrams per Kilogram mg/l: milligrams per litre
ug/l: micrograms per litre ppm: Parts per million
ppb: Parts per billion %: Percentage
org/100ml: Organisms per 100 millilitres NTU: Nephelometric Turbidity Units
MPN/100mL: Most Probable Number of organisms per 100 millilitres
Dry Where a moisture has been determined on a solid sample the result is expressed on a dry basis.
LOR Limit of Reporting.
SPIKE Addition of the analyte to the sample and reported as percentage recovery.
RPD Relative Percent Difference between two Duplicate pieces of analysis.
LCS Laboratory Control Sample - reported as percent recovery
CRM Certified Reference Material - reported as percent recovery
Method Blank In the case of solid samples these are performed on laboratory certified clean sands.
In the case of water samples these are performed on de-ionised water.
Surr - Surrogate The addition of a like compound to the analyte target and reported as percentage recovery.
Duplicate A second piece of analysis from the same sample and reported in the same units as the result to show comparison.
Batch Duplicate A second piece of analysis from a sample outside of the clients batch of samples but run within the laboratory batch of analysis.
Batch SPIKE Spike recovery reported on a sample from outside of the clients batch of samples but run within the laboratory batch of analysis.
USEPA United States Environmental Protection Agency
APHA American Public Health Association
TCLP Toxicity Characteristic Leaching Procedure
COC Chain of Custody
SRA Sample Receipt Advice
CP Client Parent - QC was performed on samples pertaining to this report
NCP Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within
TEQ Toxic Equivalency Quotient
RPD Duplicates: Global RPD Duplicates Acceptance Criteria is 30% however the following acceptance guidelines are equally applicable:
Results <10 times the LOR : No Limit
Results between 10-20 times the LOR : RPD must lie between 0-50%
Results >20 times the LOR : RPD must lie between 0-30%
Surrogate Recoveries: Recoveries must lie between 50-150%-Phenols & PFASs 20-130%
1. Where a result is reported as a less than (<), higher than the nominated LOR, this is due to either matrix interference, extract dilution required due to interferences or contaminant levels within
the sample, high moisture content or insufficient sample provided.
2. Duplicate data shown within this report that states the word "BATCH" is a Batch Duplicate from outside of your sample batch, but within the laboratory sample batch at a 1:10 ratio. The Parent
and Duplicate data shown is not data from your samples.
3. Organochlorine Pesticide analysis - where reporting LCS data, Toxaphene & Chlordane are not added to the LCS.
4. Organochlorine Pesticide analysis - where reporting Spike data, Toxaphene is not added to the Spike.
5. Total Recoverable Hydrocarbons - where reporting Spike & LCS data, a single spike of commercial Hydrocarbon products in the range of C12-C30 is added and it's Total Recovery is reported
in the C10-C14 cell of the Report.
6. pH and Free Chlorine analysed in the laboratory - Analysis on this test must begin within 30 minutes of sampling.Therefore laboratory analysis is unlikely to be completed within holding time.
Analysis will begin as soon as possible after sample receipt.
7. Recovery Data (Spikes & Surrogates) - where chromatographic interference does not allow the determination of Recovery the term "INT" appears against that analyte.
8. Polychlorinated Biphenyls are spiked only using Aroclor 1260 in Matrix Spikes and LCS.
9. For Matrix Spikes and LCS results a dash " -" in the report means that the specific analyte was not added to the QC sample.
10. Duplicate RPDs are calculated from raw analytical data thus it is possible to have two sets of data.
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 5 of 9
Report Number: 538644-W
Quality Control Results
Test Units Result 1 AcceptanceLimits
PassLimits
QualifyingCode
Method Blank
Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level
Perfluorobutanesulfonic acid (PFBS) ug/L < 0.01 0.01 Pass
Perfluorobutanoic acid (PFBA) ug/L < 0.05 0.05 Pass
Perfluorohexanesulfonic acid (PFHxS) ug/L < 0.01 0.01 Pass
Perfluorooctanesulfonic acid (PFOS) ug/L < 0.01 0.01 Pass
Perfluorodecanesulfonic acid (PFDS) ug/L < 0.01 0.01 Pass
Perfluoropentanoic acid (PFPeA) ug/L < 0.01 0.01 Pass
Perfluorohexanoic acid (PFHxA) ug/L < 0.01 0.01 Pass
Perfluoroheptanoic acid (PFHpA) ug/L < 0.01 0.01 Pass
Perfluorooctanoic acid (PFOA) ug/L < 0.01 0.01 Pass
Perfluorononanoic acid (PFNA) ug/L < 0.01 0.01 Pass
Perfluorodecanoic acid (PFDA) ug/L < 0.01 0.01 Pass
Perfluoroundecanoic acid (PFUnA) ug/L < 0.01 0.01 Pass
Perfluorododecanoic acid (PFDoA) ug/L < 0.01 0.01 Pass
Perfluorotridecanoic acid (PFTrDA) ug/L < 0.01 0.01 Pass
Perfluorotetradecanoic acid (PFTeDA) ug/L < 0.01 0.01 Pass
Perfluorooctane sulfonamide (FOSA) ug/L < 0.05 0.05 Pass
N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) ug/L < 0.05 0.05 Pass
N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) ug/L < 0.05 0.05 Pass
1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) ug/L < 0.01 0.01 Pass
1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) ug/L < 0.05 0.05 Pass
1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) ug/L < 0.01 0.01 Pass
LCS - % Recovery
Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level
Perfluorobutanesulfonic acid (PFBS) % 96 50-150 Pass
Perfluorobutanoic acid (PFBA) % 98 50-150 Pass
Perfluorohexanesulfonic acid (PFHxS) % 104 50-150 Pass
Perfluorooctanesulfonic acid (PFOS) % 105 50-150 Pass
Perfluorodecanesulfonic acid (PFDS) % 133 50-150 Pass
Perfluoropentanoic acid (PFPeA) % 111 50-150 Pass
Perfluorohexanoic acid (PFHxA) % 120 50-150 Pass
Perfluoroheptanoic acid (PFHpA) % 113 50-150 Pass
Perfluorooctanoic acid (PFOA) % 111 50-150 Pass
Perfluorononanoic acid (PFNA) % 113 50-150 Pass
Perfluorodecanoic acid (PFDA) % 99 50-150 Pass
Perfluoroundecanoic acid (PFUnA) % 99 50-150 Pass
Perfluorododecanoic acid (PFDoA) % 101 50-150 Pass
Perfluorotridecanoic acid (PFTrDA) % 92 50-150 Pass
Perfluorotetradecanoic acid (PFTeDA) % 102 50-150 Pass
Perfluorooctane sulfonamide (FOSA) % 102 50-150 Pass
N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) % 111 50-150 Pass
N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) % 95 50-150 Pass
1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) % 91 50-150 Pass
1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) % 90 50-150 Pass
1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) % 128 50-150 Pass
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 6 of 9
Report Number: 538644-W
Test Lab Sample ID QASource Units Result 1 Acceptance
LimitsPass
LimitsQualifying
Code
Spike - % Recovery
Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level Result 1
Perfluorobutanesulfonic acid(PFBS) M17-Ma16230 NCP % 93 50-150 Pass
Perfluorobutanoic acid (PFBA) M17-Ma16230 NCP % 102 50-150 Pass
Perfluorohexanesulfonic acid(PFHxS) M17-Ma16230 NCP % 102 50-150 Pass
Perfluorooctanesulfonic acid(PFOS) M17-Ma16230 NCP % 102 50-150 Pass
Perfluorodecanesulfonic acid(PFDS) M17-Ma16230 NCP % 96 50-150 Pass
Perfluoropentanoic acid (PFPeA) M17-Ma16230 NCP % 110 50-150 Pass
Perfluorohexanoic acid (PFHxA) M17-Ma16230 NCP % 120 50-150 Pass
Perfluoroheptanoic acid (PFHpA) M17-Ma16230 NCP % 106 50-150 Pass
Perfluorooctanoic acid (PFOA) M17-Ma16230 NCP % 107 50-150 Pass
Perfluorononanoic acid (PFNA) M17-Ma16230 NCP % 101 50-150 Pass
Perfluorodecanoic acid (PFDA) M17-Ma16230 NCP % 93 50-150 Pass
Perfluoroundecanoic acid (PFUnA) M17-Ma16230 NCP % 92 50-150 Pass
Perfluorododecanoic acid (PFDoA) M17-Ma16230 NCP % 82 50-150 Pass
Perfluorotridecanoic acid (PFTrDA) M17-Ma16230 NCP % 72 50-150 Pass
Perfluorotetradecanoic acid(PFTeDA) M17-Ma16230 NCP % 102 50-150 Pass
Perfluorooctane sulfonamide(FOSA) M17-Ma16230 NCP % 96 50-150 Pass
N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Ma16230 NCP % 99 50-150 Pass
N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Ma16230 NCP % 96 50-150 Pass
1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Ma16230 NCP % 86 50-150 Pass
1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Ma16230 NCP % 81 50-150 Pass
1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Ma16230 NCP % 115 50-150 Pass
Test Lab Sample ID QASource Units Result 1 Acceptance
LimitsPass
LimitsQualifying
Code
Duplicate
Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level Result 1 Result 2 RPD
Perfluorobutanesulfonic acid(PFBS) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluorobutanoic acid (PFBA) M17-Ma16230 NCP ug/L < 0.05 < 0.05 <1 30% Pass
Perfluorohexanesulfonic acid(PFHxS) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluorooctanesulfonic acid(PFOS) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluorodecanesulfonic acid(PFDS) M17-Ma16230 NCP ug/L 0.02 < 0.01 200 30% Fail Q15
Perfluoropentanoic acid (PFPeA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluorohexanoic acid (PFHxA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluoroheptanoic acid (PFHpA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluorooctanoic acid (PFOA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluorononanoic acid (PFNA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluorodecanoic acid (PFDA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluoroundecanoic acid (PFUnA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluorododecanoic acid (PFDoA) M17-Ma16230 NCP ug/L 0.02 < 0.01 200 30% Fail Q15
Perfluorotridecanoic acid (PFTrDA) M17-Ma16230 NCP ug/L 0.02 < 0.01 200 30% Fail Q15
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 7 of 9
Report Number: 538644-W
Test Lab Sample ID QASource Units Result 1 Acceptance
LimitsPass
LimitsQualifying
Code
Duplicate
Per- and Polyfluorinated Alkyl Substances (PFASs) - Trace Level Result 1 Result 2 RPD
Perfluorotetradecanoic acid(PFTeDA) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Perfluorooctane sulfonamide(FOSA) M17-Ma16230 NCP ug/L < 0.05 < 0.05 <1 30% Pass
N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Ma16230 NCP ug/L < 0.05 < 0.05 <1 30% Pass
N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Ma16230 NCP ug/L < 0.05 < 0.05 <1 30% Pass
1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Ma16230 NCP ug/L < 0.05 < 0.05 <1 30% Pass
1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Ma16230 NCP ug/L < 0.01 < 0.01 <1 30% Pass
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 8 of 9
Report Number: 538644-W
Comments
Sample IntegrityCustody Seals Intact (if used) N/A
Attempt to Chill was evident Yes
Sample correctly preserved Yes
Appropriate sample containers have been used Yes
Sample containers for volatile analysis received with minimal headspace Yes
Samples received within HoldingTime Yes
Some samples have been subcontracted No
Qualifier Codes/Comments
Code DescriptionN09 Quantification of linear and branched isomers has been conducted as a single total response using the relative response factor for the corresponding linear/branched standard.
N11
Isotope dilution is used for calibration of each native compound for which an exact labelled analogue is available (Isotope Dilution Quantitation). The isotopically labelledanalogues allow identification and recovery correction of the concentration of the associated native PFAS compounds. Where the native PFAS compound does not have labelledanalogue then the quantification is made using the Extracted Internal Standard Analyte with the closest retention time to the analyte and no recovery correction has been made(Internal Standard Quantitation).
Q15 The RPD reported passes Eurofins | mgt's QC - Acceptance Criteria as defined in the Internal Quality Control Review and Glossary page of this report.
Authorised By
Nibha Vaidya Analytical Services Manager
Jonathon Angell Senior Analyst-Organic (QLD)
Glenn Jackson
National Operations Manager
- Indicates Not Requested
* Indicates NATA accreditation does not cover the performance of this service
Measurement uncertainty of test data is available on request or please click here.Eurofins | mgt shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretation given in this report. In no case shall Eurofins | mgt be liable for consequential damages including, but notlimited to, lost profits, damages for failure to meet deadlines and lost production arising from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 9 of 9
Report Number: 538644-W
Certificate of Analysis
Golder Associates
124 Pacific Hwy
St. Leonards
NSW 1585
Attention: Andrew Holloway
Report 538644-S
Project name KAPOOKA
Project ID 1652034
Received Date Mar 20, 2017
Client Sample ID 0315_QC201_170314
0315_QC203_170315
0315_QC205_170315
0315_QC207_170315
Sample Matrix Soil Soil Soil Soil
Eurofins | mgt Sample No. S17-Ma21084 S17-Ma21085 S17-Ma21086 S17-Ma21087
Date Sampled Mar 14, 2017 Mar 15, 2017 Mar 15, 2017 Mar 15, 2017
Test/Reference LOR Unit
Perfluoroalkyl carboxylic acids (PFCAs)
Perfluorobutanoic acid (PFBA) 5 ug/kg < 5 < 5 < 5 < 5
13C4-PFBA (surr.) 1 % 92 78 103 100
Perfluoropentanoic acid (PFPeA) 5 ug/kg < 5 < 5 < 5 < 5
13C5-PFPeA (surr.) 1 % 77 66 89 92
Perfluorohexanoic acid (PFHxA) 5 ug/kg < 5 < 5 < 5 < 5
13C5-PFHxA (surr.) 1 % 95 73 108 104
Perfluoroheptanoic acid (PFHpA) 5 ug/kg < 5 < 5 < 5 < 5
13C4-PFHpA (surr.) 1 % 92 68 108 99
Perfluorooctanoic acid (PFOA) 5 ug/kg < 5 < 5 < 5 < 5
13C8-PFOA (surr.) 1 % 87 71 99 91
Perfluorononanoic acid (PFNA) 5 ug/kg < 5 < 5 < 5 < 5
13C5-PFNA (surr.) 1 % 90 75 105 93
Perfluorodecanoic acid (PFDA) 5 ug/kg < 5 < 5 < 5 < 5
13C6-PFDA (surr.) 1 % 95 80 105 99
Perfluoroundecanoic acid (PFUnA) 5 ug/kg < 5 < 5 < 5 < 5
13C2-PFUnDA (surr.) 1 % 90 88 107 98
Perfluorododecanoic acid (PFDoA) 5 ug/kg < 5 < 5 < 5 < 5
13C2-PFDoDA (surr.) 1 % 97 90 111 97
Perfluorotridecanoic acid (PFTrDA) 5 ug/kg < 5 < 5 < 5 < 5
Perfluorotetradecanoic acid (PFTeDA) 5 ug/kg < 5 < 5 < 5 < 5
13C2-PFTeDA (surr.) 1 % 87 87 100 90
Perfluoroalkane sulfonamides (PFASAs)
Perfluorooctane sulfonamide (FOSA) 5 ug/kg < 5 < 5 < 5 < 5
13C8-FOSA (surr.) 1 % 78 83 91 79
N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) 5 ug/kg < 5 < 5 < 5 < 5
D3-N-MeFOSA (surr.) 1 % 73 84 93 78
N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) 5 ug/kg < 5 < 5 < 5 < 5
D5-N-EtFOSA (surr.) 1 % 66 89 93 81
2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE) 5 ug/kg < 5 < 5 < 5 < 5
D7-N-MeFOSE (surr.) 1 % 82 78 86 89
2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) 5 ug/kg < 5 < 5 < 5 < 5
D9-N-EtFOSE (surr.) 1 % 71 81 89 75
N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 10 ug/kg < 10 < 10 < 10 < 10
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 1 of 11
Report Number: 538644-S
NATA AccreditedAccreditation Number 1261Site Number 18217
Accredited for compliance with ISO/IEC 17025 – TestingThe results of the tests, calibrations and/ormeasurements included in this document are traceableto Australian/national standards.
Client Sample ID 0315_QC201_170314
0315_QC203_170315
0315_QC205_170315
0315_QC207_170315
Sample Matrix Soil Soil Soil Soil
Eurofins | mgt Sample No. S17-Ma21084 S17-Ma21085 S17-Ma21086 S17-Ma21087
Date Sampled Mar 14, 2017 Mar 15, 2017 Mar 15, 2017 Mar 15, 2017
Test/Reference LOR Unit
Perfluoroalkane sulfonamides (PFASAs)
D5-N-EtFOSAA (surr.) 1 % 104 71 115 104
N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 10 ug/kg < 10 < 10 < 10 < 10
D3-N-MeFOSAA (surr.) 1 % 108 67 116 114
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs)
Perfluorobutanesulfonic acid (PFBS) 5 ug/kg < 5 < 5 < 5 < 5
13C3-PFBS (surr.) 1 % 97 91 109 102
Perfluoropentanesulfonic acid (PFPeS) 5 ug/kg < 5 < 5 < 5 < 5
Perfluorohexanesulfonic acid (PFHxS) 5 ug/kg < 5 < 5 < 5 < 5
18O2-PFHxS (surr.) 1 % 91 91 102 95
Perfluoroheptanesulfonic acid (PFHpS) 5 ug/kg < 5 < 5 < 5 < 5
Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg < 5 < 5 N09500 < 5
13C8-PFOS (surr.) 1 % 89 94 87 91
Perfluorodecanesulfonic acid (PFDS) 5 ug/kg < 5 < 5 < 5 < 5
n:2 Fluorotelomer sulfonic acids
1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 5 ug/kg < 5 < 5 < 5 < 5
13C2-4:2 FTS (surr.) 1 % 56 20 79 80
1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 10 ug/kg < 10 < 10 < 10 < 10
13C2-6:2 FTS (surr.) 1 % 54 23 66 62
1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 5 ug/kg < 5 < 5 < 5 < 5
13C2-8:2 FTS (surr.) 1 % 60 31 68 68
1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 5 ug/kg < 5 < 5 < 5 < 5
% Moisture 1 % 11 10.0 2.1 2.3
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 2 of 11
Report Number: 538644-S
Sample HistoryWhere samples are submitted/analysed over several days, the last date of extraction and analysis is reported.A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this, some of the method reference information on reports has changed. However,no substantive change has been made to our laboratory methods, and as such there is no change in the validity of current or previous results (regarding both quality and NATA accreditation).
If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised results should testing be performed outside the recommended holding time.
Description Testing Site Extracted Holding Time
Per- and Polyfluorinated Alkyl Substances (PFASs)
Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Mar 21, 2017 180 Day
- Method: LTM-ORG-2100 Per- and Polyfluorinated Alkyl Substances by LC-MS/MS
Perfluoroalkane sulfonamides (PFASAs) Brisbane Mar 21, 2017 180 Day
- Method: LTM-ORG-2100 Per- and Polyfluorinated Alkyl Substances by LC-MS/MS
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Mar 21, 2017 180 Day
- Method: LTM-ORG-2100 Per- and Polyfluorinated Alkyl Substances by LC-MS/MS
n:2 Fluorotelomer sulfonic acids Brisbane Mar 21, 2017 180 Day
- Method: LTM-ORG-2100 Per- and Polyfluorinated Alkyl Substances by LC-MS/MS
% Moisture Brisbane Mar 20, 2017 14 Day
- Method: LTM-GEN-7080 Moisture
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 3 of 11
Report Number: 538644-S
.Company Name: Golder Associates Pty Ltd (Syd) Order No.: Received: Mar 20, 2017 11:06 AMAddress: 124 Pacific Hwy Report #: 538644 Due: Mar 27, 2017
St. Leonards Phone: 02 9478 3900 Priority: 5 DayNSW 1585 Fax: 02 9478 3901 Contact Name: Andrew Holloway
Project Name: KAPOOKAProject ID: 1652034
Eurofins | mgt Analytical Services Manager : Nibha Vaidya
Sample Detail
Moisture S
et
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss) - T
race Level
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss)
Melbourne Laboratory - NATA Site # 1254 & 14271
Sydney Laboratory - NATA Site # 18217
Brisbane Laboratory - NATA Site # 20794 X X X
Perth Laboratory - NATA Site # 18217
External Laboratory
No Sample ID Sample Date SamplingTime
Matrix LAB ID
1 0315_QC201_170314
Mar 14, 2017 Soil S17-Ma21084 X X
2 0315_QC203_170315
Mar 15, 2017 Soil S17-Ma21085 X X
3 0315_QC205_170315
Mar 15, 2017 Soil S17-Ma21086 X X
4 0315_QC207_170315
Mar 15, 2017 Soil S17-Ma21087 X X
5 0315_QC209_170315
Mar 15, 2017 Water S17-Ma21088 X
6 0315_QC210_ Mar 16, 2017 Water S17-Ma21089 X
ABN– 50 005 085 521e.mail : [email protected] : www.eurofins.com.au
MelbourneMelbourneMelbourneMelbourne2-5 Kingston Town CloseOakleigh VIC 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271
SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217
BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794
PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261Site # 18217
Date Reported:Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 4 of 11
Report Number: 538644-S
Company Name: Golder Associates Pty Ltd (Syd) Order No.: Received: Mar 20, 2017 11:06 AMAddress: 124 Pacific Hwy Report #: 538644 Due: Mar 27, 2017
St. Leonards Phone: 02 9478 3900 Priority: 5 DayNSW 1585 Fax: 02 9478 3901 Contact Name: Andrew Holloway
Project Name: KAPOOKAProject ID: 1652034
Eurofins | mgt Analytical Services Manager : Nibha Vaidya
Sample Detail
Moisture S
et
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss) - T
race Level
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss)
Melbourne Laboratory - NATA Site # 1254 & 14271
Sydney Laboratory - NATA Site # 18217
Brisbane Laboratory - NATA Site # 20794 X X X
Perth Laboratory - NATA Site # 18217
170316
Test Counts 4 2 4
ABN– 50 005 085 521e.mail : [email protected] : www.eurofins.com.au
MelbourneMelbourneMelbourneMelbourne2-5 Kingston Town CloseOakleigh VIC 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271
SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217
BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794
PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261Site # 18217
Page 5 of 11
Report Number: 538644-S
Internal Quality Control Review and Glossary
General
Holding Times
Units
Terms
QC - Acceptance Criteria
QC Data General Comments
1. Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on
request.
2. All soil results are reported on a dry basis, unless otherwise stated.
3. Actual LORs are matrix dependant. Quoted LORs may be raised where sample extracts are diluted due to interferences.
4. Results are uncorrected for matrix spikes or surrogate recoveries.
5. SVOC analysis on waters are performed on homogenised, unfiltered samples, unless noted otherwise.
6. Samples were analysed on an 'as received' basis. 7. This report replaces any interim results previously issued.
Please refer to 'Sample Preservation and Container Guide' for holding times (QS3001).
For samples received on the last day of holding time, notification of testing requirements should have been received at least 6 hours prior to sample receipt deadlines as stated on the Sample
Receipt Advice.
If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues, suitably qualified results may still be reported.
Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control.
**NOTE: pH duplicates are reported as a range NOT as RPD
mg/kg: milligrams per Kilogram mg/l: milligrams per litre
ug/l: micrograms per litre ppm: Parts per million
ppb: Parts per billion %: Percentage
org/100ml: Organisms per 100 millilitres NTU: Nephelometric Turbidity Units
MPN/100mL: Most Probable Number of organisms per 100 millilitres
Dry Where a moisture has been determined on a solid sample the result is expressed on a dry basis.
LOR Limit of Reporting.
SPIKE Addition of the analyte to the sample and reported as percentage recovery.
RPD Relative Percent Difference between two Duplicate pieces of analysis.
LCS Laboratory Control Sample - reported as percent recovery
CRM Certified Reference Material - reported as percent recovery
Method Blank In the case of solid samples these are performed on laboratory certified clean sands.
In the case of water samples these are performed on de-ionised water.
Surr - Surrogate The addition of a like compound to the analyte target and reported as percentage recovery.
Duplicate A second piece of analysis from the same sample and reported in the same units as the result to show comparison.
Batch Duplicate A second piece of analysis from a sample outside of the clients batch of samples but run within the laboratory batch of analysis.
Batch SPIKE Spike recovery reported on a sample from outside of the clients batch of samples but run within the laboratory batch of analysis.
USEPA United States Environmental Protection Agency
APHA American Public Health Association
TCLP Toxicity Characteristic Leaching Procedure
COC Chain of Custody
SRA Sample Receipt Advice
CP Client Parent - QC was performed on samples pertaining to this report
NCP Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within
TEQ Toxic Equivalency Quotient
RPD Duplicates: Global RPD Duplicates Acceptance Criteria is 30% however the following acceptance guidelines are equally applicable:
Results <10 times the LOR : No Limit
Results between 10-20 times the LOR : RPD must lie between 0-50%
Results >20 times the LOR : RPD must lie between 0-30%
Surrogate Recoveries: Recoveries must lie between 50-150%-Phenols & PFASs 20-130%
1. Where a result is reported as a less than (<), higher than the nominated LOR, this is due to either matrix interference, extract dilution required due to interferences or contaminant levels within
the sample, high moisture content or insufficient sample provided.
2. Duplicate data shown within this report that states the word "BATCH" is a Batch Duplicate from outside of your sample batch, but within the laboratory sample batch at a 1:10 ratio. The Parent
and Duplicate data shown is not data from your samples.
3. Organochlorine Pesticide analysis - where reporting LCS data, Toxaphene & Chlordane are not added to the LCS.
4. Organochlorine Pesticide analysis - where reporting Spike data, Toxaphene is not added to the Spike.
5. Total Recoverable Hydrocarbons - where reporting Spike & LCS data, a single spike of commercial Hydrocarbon products in the range of C12-C30 is added and it's Total Recovery is reported
in the C10-C14 cell of the Report.
6. pH and Free Chlorine analysed in the laboratory - Analysis on this test must begin within 30 minutes of sampling.Therefore laboratory analysis is unlikely to be completed within holding time.
Analysis will begin as soon as possible after sample receipt.
7. Recovery Data (Spikes & Surrogates) - where chromatographic interference does not allow the determination of Recovery the term "INT" appears against that analyte.
8. Polychlorinated Biphenyls are spiked only using Aroclor 1260 in Matrix Spikes and LCS.
9. For Matrix Spikes and LCS results a dash " -" in the report means that the specific analyte was not added to the QC sample.
10. Duplicate RPDs are calculated from raw analytical data thus it is possible to have two sets of data.
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 6 of 11
Report Number: 538644-S
Quality Control Results
Test Units Result 1 AcceptanceLimits
PassLimits
QualifyingCode
Method Blank
Perfluoroalkyl carboxylic acids (PFCAs)
Perfluorobutanoic acid (PFBA) ug/kg < 5 5 Pass
Perfluoropentanoic acid (PFPeA) ug/kg < 5 5 Pass
Perfluorohexanoic acid (PFHxA) ug/kg < 5 5 Pass
Perfluoroheptanoic acid (PFHpA) ug/kg < 5 5 Pass
Perfluorooctanoic acid (PFOA) ug/kg < 5 5 Pass
Perfluorononanoic acid (PFNA) ug/kg < 5 5 Pass
Perfluorodecanoic acid (PFDA) ug/kg < 5 5 Pass
Perfluoroundecanoic acid (PFUnA) ug/kg < 5 5 Pass
Perfluorododecanoic acid (PFDoA) ug/kg < 5 5 Pass
Perfluorotridecanoic acid (PFTrDA) ug/kg < 5 5 Pass
Perfluorotetradecanoic acid (PFTeDA) ug/kg < 5 5 Pass
Method Blank
Perfluoroalkane sulfonamides (PFASAs)
Perfluorooctane sulfonamide (FOSA) ug/kg < 5 5 Pass
N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) ug/kg < 5 5 Pass
N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) ug/kg < 5 5 Pass
2-(N-methylperfluoro-1-octane sulfonamido)-ethanol (N-MeFOSE) ug/kg < 5 5 Pass
2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) ug/kg < 5 5 Pass
N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) ug/kg < 10 10 Pass
N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) ug/kg < 10 10 Pass
Method Blank
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs)
Perfluorobutanesulfonic acid (PFBS) ug/kg < 5 5 Pass
Perfluoropentanesulfonic acid (PFPeS) ug/kg < 5 5 Pass
Perfluorohexanesulfonic acid (PFHxS) ug/kg < 5 5 Pass
Perfluoroheptanesulfonic acid (PFHpS) ug/kg < 5 5 Pass
Perfluorooctanesulfonic acid (PFOS) ug/kg < 5 5 Pass
Perfluorodecanesulfonic acid (PFDS) ug/kg < 5 5 Pass
Method Blank
n:2 Fluorotelomer sulfonic acids
1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) ug/kg < 5 5 Pass
1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) ug/kg < 10 10 Pass
1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) ug/kg < 5 5 Pass
1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2 FTS) ug/kg < 5 5 Pass
LCS - % Recovery
Perfluoroalkyl carboxylic acids (PFCAs)
Perfluorobutanoic acid (PFBA) % 94 50-150 Pass
Perfluoropentanoic acid (PFPeA) % 109 50-150 Pass
Perfluorohexanoic acid (PFHxA) % 98 50-150 Pass
Perfluoroheptanoic acid (PFHpA) % 99 50-150 Pass
Perfluorooctanoic acid (PFOA) % 96 50-150 Pass
Perfluorononanoic acid (PFNA) % 101 50-150 Pass
Perfluorodecanoic acid (PFDA) % 101 50-150 Pass
Perfluoroundecanoic acid (PFUnA) % 96 50-150 Pass
Perfluorododecanoic acid (PFDoA) % 105 50-150 Pass
Perfluorotridecanoic acid (PFTrDA) % 108 50-150 Pass
Perfluorotetradecanoic acid (PFTeDA) % 106 50-150 Pass
LCS - % Recovery
Perfluoroalkane sulfonamides (PFASAs)
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 7 of 11
Report Number: 538644-S
Test Units Result 1 AcceptanceLimits
PassLimits
QualifyingCode
Perfluorooctane sulfonamide (FOSA) % 98 50-150 Pass
N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) % 111 50-150 Pass
N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) % 129 50-150 Pass
2-(N-methylperfluoro-1-octane sulfonamido)-ethanol (N-MeFOSE) % 85 50-150 Pass
2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) % 104 50-150 Pass
N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) % 102 50-150 Pass
N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) % 99 50-150 Pass
LCS - % Recovery
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs)
Perfluorobutanesulfonic acid (PFBS) % 97 50-150 Pass
Perfluoropentanesulfonic acid (PFPeS) % 95 50-150 Pass
Perfluorohexanesulfonic acid (PFHxS) % 95 50-150 Pass
Perfluoroheptanesulfonic acid (PFHpS) % 98 50-150 Pass
Perfluorooctanesulfonic acid (PFOS) % 94 50-150 Pass
Perfluorodecanesulfonic acid (PFDS) % 107 50-150 Pass
LCS - % Recovery
n:2 Fluorotelomer sulfonic acids
1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) % 107 50-150 Pass
1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) % 142 50-150 Pass
1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) % 137 50-150 Pass
1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2 FTS) % 101 50-150 Pass
Test Lab Sample ID QASource Units Result 1 Acceptance
LimitsPass
LimitsQualifying
Code
Spike - % Recovery
Perfluoroalkyl carboxylic acids (PFCAs) Result 1
Perfluorobutanoic acid (PFBA) M17-Ma19364 NCP % 93 50-150 Pass
Perfluoropentanoic acid (PFPeA) M17-Ma19364 NCP % 106 50-150 Pass
Perfluorohexanoic acid (PFHxA) M17-Ma19364 NCP % 97 50-150 Pass
Perfluoroheptanoic acid (PFHpA) M17-Ma19364 NCP % 96 50-150 Pass
Perfluorooctanoic acid (PFOA) M17-Ma19364 NCP % 98 50-150 Pass
Perfluorononanoic acid (PFNA) M17-Ma19364 NCP % 99 50-150 Pass
Perfluorodecanoic acid (PFDA) M17-Ma19364 NCP % 97 50-150 Pass
Perfluoroundecanoic acid (PFUnA) M17-Ma19364 NCP % 94 50-150 Pass
Perfluorododecanoic acid (PFDoA) M17-Ma19364 NCP % 100 50-150 Pass
Perfluorotridecanoic acid (PFTrDA) M17-Ma19364 NCP % 66 50-150 Pass
Perfluorotetradecanoic acid(PFTeDA) M17-Ma19364 NCP % 102 50-150 Pass
Spike - % Recovery
Perfluoroalkane sulfonamides (PFASAs) Result 1
Perfluorooctane sulfonamide(FOSA) M17-Ma19364 NCP % 99 50-150 Pass
N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Ma19364 NCP % 114 50-150 Pass
N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Ma19364 NCP % 129 50-150 Pass
2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Ma19364 NCP % 101 50-150 Pass
2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Ma19364 NCP % 80 50-150 Pass
N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Ma19364 NCP % 123 50-150 Pass
N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Ma19364 NCP % 130 50-150 Pass
Spike - % Recovery
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Result 1
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 8 of 11
Report Number: 538644-S
Test Lab Sample ID QASource Units Result 1 Acceptance
LimitsPass
LimitsQualifying
Code
Perfluorobutanesulfonic acid(PFBS) M17-Ma19364 NCP % 97 50-150 Pass
Perfluoropentanesulfonic acid(PFPeS) M17-Ma19364 NCP % 95 50-150 Pass
Perfluorohexanesulfonic acid(PFHxS) M17-Ma19364 NCP % 93 50-150 Pass
Perfluoroheptanesulfonic acid(PFHpS) M17-Ma19364 NCP % 97 50-150 Pass
Perfluorooctanesulfonic acid(PFOS) M17-Ma19364 NCP % 93 50-150 Pass
Perfluorodecanesulfonic acid(PFDS) M17-Ma19364 NCP % 87 50-150 Pass
Spike - % Recovery
n:2 Fluorotelomer sulfonic acids Result 1
1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Ma19364 NCP % 106 50-150 Pass
1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Ma19364 NCP % 140 50-150 Pass
1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Ma19364 NCP % 134 50-150 Pass
1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Ma19364 NCP % 135 50-150 Pass
Test Lab Sample ID QASource Units Result 1 Acceptance
LimitsPass
LimitsQualifying
Code
Duplicate
Perfluoroalkyl carboxylic acids (PFCAs) Result 1 Result 2 RPD
Perfluorobutanoic acid (PFBA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluoropentanoic acid (PFPeA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluorohexanoic acid (PFHxA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluoroheptanoic acid (PFHpA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluorooctanoic acid (PFOA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluorononanoic acid (PFNA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluorodecanoic acid (PFDA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluoroundecanoic acid (PFUnA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluorododecanoic acid (PFDoA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluorotridecanoic acid (PFTrDA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluorotetradecanoic acid(PFTeDA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Duplicate
Perfluoroalkane sulfonamides (PFASAs) Result 1 Result 2 RPD
Perfluorooctane sulfonamide(FOSA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Ma20923 NCP ug/kg < 10 < 10 <1 30% Pass
N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Ma20923 NCP ug/kg < 10 < 10 <1 30% Pass
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 9 of 11
Report Number: 538644-S
Duplicate
Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Result 1 Result 2 RPD
Perfluorobutanesulfonic acid(PFBS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluoropentanesulfonic acid(PFPeS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluorohexanesulfonic acid(PFHxS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluoroheptanesulfonic acid(PFHpS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluorooctanesulfonic acid(PFOS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Perfluorodecanesulfonic acid(PFDS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Duplicate
n:2 Fluorotelomer sulfonic acids Result 1 Result 2 RPD
1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Ma20923 NCP ug/kg < 10 < 10 <1 30% Pass
1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Ma20923 NCP ug/kg < 5 < 5 <1 30% Pass
Duplicate
Result 1 Result 2 RPD
% Moisture S17-Ma09089 NCP % 25 28 9.0 30% Pass
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 10 of 11
Report Number: 538644-S
Comments
Sample IntegrityCustody Seals Intact (if used) N/A
Attempt to Chill was evident Yes
Sample correctly preserved Yes
Appropriate sample containers have been used Yes
Sample containers for volatile analysis received with minimal headspace Yes
Samples received within HoldingTime Yes
Some samples have been subcontracted No
Qualifier Codes/Comments
Code DescriptionN09 Quantification of linear and branched isomers has been conducted as a single total response using the relative response factor for the corresponding linear/branched standard.
N11
Isotope dilution is used for calibration of each native compound for which an exact labelled analogue is available (Isotope Dilution Quantitation). The isotopically labelledanalogues allow identification and recovery correction of the concentration of the associated native PFAS compounds. Where the native PFAS compound does not have labelledanalogue then the quantification is made using the Extracted Internal Standard Analyte with the closest retention time to the analyte and no recovery correction has been made(Internal Standard Quantitation).
Authorised By
Nibha Vaidya Analytical Services Manager
Bryan Wilson Senior Analyst-Metal (QLD)
Jonathon Angell Senior Analyst-Inorganic (QLD)
Jonathon Angell Senior Analyst-Organic (QLD)
Glenn Jackson
National Operations Manager
- Indicates Not Requested
* Indicates NATA accreditation does not cover the performance of this service
Measurement uncertainty of test data is available on request or please click here.Eurofins | mgt shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretation given in this report. In no case shall Eurofins | mgt be liable for consequential damages including, but notlimited to, lost profits, damages for failure to meet deadlines and lost production arising from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.
Date Reported: Mar 31, 2017
Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066
ABN : 50 005 085 521 Telephone: +61 2 9900 8400
Page 11 of 11
Report Number: 538644-S
.Company Name: Golder Associates Pty Ltd (Syd) Order No.: Received: Mar 20, 2017 11:06 AMAddress: 124 Pacific Hwy Report #: 538644 Due: Mar 27, 2017
St. Leonards Phone: 02 9478 3900 Priority: 5 DayNSW 1585 Fax: 02 9478 3901 Contact Name: Andrew Holloway
Project Name: KAPOOKAProject ID: 1652034
Eurofins | mgt Analytical Services Manager : Nibha Vaidya
Sample Detail
Moisture S
et
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss) - T
race Level
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss)
Melbourne Laboratory - NATA Site # 1254 & 14271
Sydney Laboratory - NATA Site # 18217
Brisbane Laboratory - NATA Site # 20794 X X X
Perth Laboratory - NATA Site # 18217
External Laboratory
No Sample ID Sample Date SamplingTime
Matrix LAB ID
1 0315_QC201_170314
Mar 14, 2017 Soil S17-Ma21084 X X
2 0315_QC203_170315
Mar 15, 2017 Soil S17-Ma21085 X X
3 0315_QC205_170315
Mar 15, 2017 Soil S17-Ma21086 X X
4 0315_QC207_170315
Mar 15, 2017 Soil S17-Ma21087 X X
5 0315_QC209_170315
Mar 15, 2017 Water S17-Ma21088 X
6 0315_QC210_ Mar 16, 2017 Water S17-Ma21089 X
ABN– 50 005 085 521e.mail : [email protected] : www.eurofins.com.au
MelbourneMelbourneMelbourneMelbourne2-5 Kingston Town CloseOakleigh VIC 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271
SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217
BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794
PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261Site # 18217
Company Name: Golder Associates Pty Ltd (Syd) Order No.: Received: Mar 20, 2017 11:06 AMAddress: 124 Pacific Hwy Report #: 538644 Due: Mar 27, 2017
St. Leonards Phone: 02 9478 3900 Priority: 5 DayNSW 1585 Fax: 02 9478 3901 Contact Name: Andrew Holloway
Project Name: KAPOOKAProject ID: 1652034
Eurofins | mgt Analytical Services Manager : Nibha Vaidya
Sample Detail
Moisture S
et
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss) - T
race Level
Per- and P
olyfluorinated Alkyl S
ubstances(P
FA
Ss)
Melbourne Laboratory - NATA Site # 1254 & 14271
Sydney Laboratory - NATA Site # 18217
Brisbane Laboratory - NATA Site # 20794 X X X
Perth Laboratory - NATA Site # 18217
170316
Test Counts 4 2 4
ABN– 50 005 085 521e.mail : [email protected] : www.eurofins.com.au
MelbourneMelbourneMelbourneMelbourne2-5 Kingston Town CloseOakleigh VIC 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271
SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217
BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794
PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261Site # 18217
ABN – 50 005 085 521 e.mail : [email protected] web : www.eurofins.com.au
MelbourneMelbourneMelbourneMelbourne3-5 Kingston Town CloseOakleigh Vic 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271
SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217
BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794
PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261 Site # 18217
Environmental LaboratoryAir AnalysisWater AnalysisSoil Contamination Analysis
NATA AccreditationStack Emission Sampling & AnalysisTrade Waste Sampling & AnalysisGroundwater Sampling & Analysis
38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience
Sample Receipt AdviceSample Receipt AdviceSample Receipt AdviceSample Receipt Advice
Company name: Golder Associates Pty Ltd (Syd)Golder Associates Pty Ltd (Syd)Golder Associates Pty Ltd (Syd)Golder Associates Pty Ltd (Syd)
Contact name: Andrew HollowayProject name: KAPOOKAProject ID: 1652034COC number: Not providedTurn around time: 5 DayDate/Time received: Mar 20, 2017 11:06 AMEurofins | mgt reference: 538644538644538644538644
Sample informationSample informationSample informationSample information
☑ A detailed list of analytes logged into our LIMS, is included in the attached summary table.
☑ Sample Temperature of a random sample selected from the batch as recorded by Eurofins | mgtSample Receipt : 24.5 degrees Celsius.
☑ All samples have been received as described on the above COC.
☑ COC has been completed correctly.
☑ Attempt to chill was evident.
☑ Appropriately preserved sample containers have been used.
☑ All samples were received in good condition.
☑ Samples have been provided with adequate time to commence analysis in accordance with therelevant holding times.
☑ Appropriate sample containers have been used.
☑ Sample containers for volatile analysis received with zero headspace.
☒ Some samples have been subcontracted.
N/A Custody Seals intact (if used).
Contact notesContact notesContact notesContact notes
If you have any questions with respect to these samples please contact:
Nibha Vaidya on Phone : +61 (2) 9900 8400 or by e.mail: [email protected]
Results will be delivered electronically via e.mail to Andrew Holloway - [email protected].
Note: A copy of these results will also be delivered to the general Golder Associates Pty Ltd (Syd) email address.
PSI - BLAMEY BARRACKS KAPOOKA (0315)
APPENDIX I Calibration Certificates
14 June 2017 Report No. 1669283_001_R_Rev0 53
PSI - BLAMEY BARRACKS KAPOOKA (0315)
APPENDIX J Report Limitations
14 June 2017 Report No. 1669283_001_R_Rev0 54
IMPORTANT INFORMATION RELATING TO THIS REPORT
The document (“Report”) to which this page is attached and which this page forms a part of, has been issued by Golder Associates Pty Ltd (“Golder”) subject to the important limitations and other qualifications set out below.
This Report constitutes or is part of services (“Services”) provided by Golder to its client (“Client”) under and subject to a contract between Golder and its Client (“Contract”). The contents of this page are not intended to and do not alter Golder’s obligations (including any limits on those obligations) to its Client under the Contract.
This Report is provided for use solely by Golder’s Client and persons acting on the Client’s behalf, such as its professional advisers. Golder is responsible only to its Client for this Report. Golder has no responsibility to any other person who relies or makes decisions based upon this Report or who makes any other use of this Report. Golder accepts no responsibility for any loss or damage suffered by any person other than its Client as a result of any reliance upon any part of this Report, decisions made based upon this Report or any other use of it.
This Report has been prepared in the context of the circumstances and purposes referred to in, or derived from, the Contract and Golder accepts no responsibility for use of the Report, in whole or in part, in any other context or circumstance or for any other purpose.
The scope of Golder’s Services and the period of time they relate to are determined by the Contract and are subject to restrictions and limitations set out in the Contract. If a service or other work is not expressly referred to in this Report, do not assume that it has been provided or performed. If a matter is not addressed in this Report, do not assume that any determination has been made by Golder in regards to it.
At any location relevant to the Services conditions may exist which were not detected by Golder, in particular due to the specific scope of the investigation Golder has been engaged to undertake. Conditions can only be verified at the exact location of any tests undertaken. Variations in conditions may occur between tested locations and there may be conditions which have not been revealed by the investigation and which have not therefore been taken into account in this Report.
Golder accepts no responsibility for and makes no representation as to the accuracy or completeness of the information provided to it by or on behalf of the Client or sourced from any third party. Golder has assumed that such information is correct unless otherwise stated and no responsibility is accepted by Golder for incomplete or inaccurate data supplied by its Client or any other person for whom Golder is not responsible. Golder has not taken account of matters that may have existed when the Report was prepared but which were only later disclosed to Golder.
Having regard to the matters referred to in the previous paragraphs on this page in particular, carrying out the Services has allowed Golder to form no more than an opinion as to the actual conditions at any relevant location. That opinion is necessarily constrained by the extent of the information collected by Golder or otherwise made available to Golder. Further, the passage of time may affect the accuracy, applicability or usefulness of the opinions, assessments or other information in this Report. This Report is based upon the information and other circumstances that existed and were known to Golder when the Services were performed and this Report was prepared. Golder has not considered the effect of any possible future developments including physical changes to any relevant location or changes to any laws or regulations relevant to such location.
Where permitted by the Contract, Golder may have retained subconsultants affiliated with Golder to provide some or all of the Services. However, it is Golder which remains solely responsible for the Services and there is no legal recourse against any of Golder’s affiliated companies or the employees, officers or directors of any of them.
By date, or revision, the Report supersedes any prior report or other document issued by Golder dealing with any matter that is addressed in the Report.
Any uncertainty as to the extent to which this Report can be used or relied upon in any respect should be referred to Golder for clarification.
GAP Form No. LEG04RL2July 2015 1/1